1 ICP Test Report Certification Packet Company name: Littelfuse, Inc. Product Series: 5x20 Fuse Product #: 0477016.MXEP Issue Date: October 10, 2013 It is hereby certified by Littelfuse, Inc. that there is neither RoHS (2011/65/EU – recast of EU Directive 2002/95/EC)-restricted substance nor such use, for materials to be used for unit parts, for packing/packaging materials, and for additives and the like in the manufacturing processes. In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing processes, are all composed of the following components. Issued by: <Global EHS Engineer> (1) Parts, sub-materials and unit parts This document covers the 477P Fuse RoHS-Compliant series products manufactured by Littelfuse, Inc. < Raw Materials Used Please see Table 1 (2) The ICP data on all measurable substances Please see appropriate pages as identifed in Table 1 Remarks:.
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1
ICP Test Report Certification Packet
Company name : Littelfuse, Inc. Product Series: 5x20 Fuse Product #: 0477016.MXEP Issue Date: October 10, 2013 It is hereby certified by Littelfuse, Inc. that there is neither RoHS (2011/65/EU – recast of EU Directive 2002/95/EC)-restricted substance nor such use, for materials to be used for unit parts, for packing/packaging materials, and for additives and the like in the manufacturing processes. In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing processes, are all composed of the following components.
Issued by:
<Global EHS Engineer>
(1) Parts, sub-materials and unit parts This document covers the 477P Fuse RoHS-Compliant series products manufactured by Littelfuse, Inc. < Raw Materials Used
Please see Table 1 (2) The ICP data on all measurable substances Please see appropriate pages as identifed in Table 1
Remarks:.
2
Table 1: List of Raw Materials covered by this report
Total Parts Raw Material Part
Number Raw Material Description Page(s) 1 901-556 Cap base & plating 3-6 2 C610 (909-449) Body Ceramic tube 7-35 3 311.7374.5000 Filler Sand 36-45 4 082xxx/ 0823xx-001 Wire - Cu99.9MSn 46-50
5 YTW102
(692539-002) Solder 51-56
6 C030204/ 934-077/ 934-071/ 934-078 Overcap - Cap Base & Plating 57-60
The following sample(s) was/werc submitted and identified by/on behatf of the client as:
Sample DesoriptionStyle/ltem No.Sample Receiving DateTesting Period
CERAMICc6102013t1tl42013t1tl4 10 2013tO1n1
Test Re3ult(s)
Conclusion
: Please lefer to next page(s).
: Based on the pedomed test6 on 6ubmitted 6amples, the test results of Cadmium, Lead,I\rercury, Hexavalent Chromium Cr(Vl), PBBS and PBDES comply with tho limits as set byRoHS Dircctive 201'1/65/EU Annex ll; recasting 2002/95/EC.
Efnrd fr. aod
Chqdcd frbot bry-Trlgd
tHl5";vtr^:,)n*$i"d h8 T.u:lM
I d!'€'' ledn'"Jg onr oi.-i"oiji.--," **o o n"c.ru rcele o1r{ o'd.r'"€.o*or
Wilh reference to EPA 600/R-93'/1 I 6method. Analysis was performed byStereo l\Iicroscope (SM), DispersionStaining Polarized Light Microscope(DS-PLlr) and X-ray DiffractionSpectrometef (XFID).
m9Kg With reference to LFGB 82.02-2.Analy6is was performed by GC/lltS.
3 n.d.
fi ' ' !,"l;*'"*.;*.-".:;". ' ' ' ,.""""...].,";..":"'.s"*"...*"-':.."'"."."-, i l ; , .n i ' jn . i , .n t tomaroi - . "* . -d€o6|er ,ardcotro|3|oLeiii, iil.-niiniiv-iiiiiinnn-in,ii^?,aitd;*uBdlin6dthe;;^i i i i i i i"i,i ir,i*o' -ry-"*ri tr. -'borc ctihqrudm' Ir'l -tcomdars ea s!oo!oi,.i"*.i- m * os no a i r.' q*
" o o'qa'o* -0.'- nino;r'doe-44 n s do' -d -moin. ?erc!L("d P e0
li;fiii rii;" r;;a; tao: b's;t "abi"r.d*
oJ rhe @;;;;;i;;;;;i $ n@*i' "
*h*tu sa otundds mai be prcsdcd b '
, " , . , , , . : i l i i ; i l . r , qno*' t r"aFt i r i . l i . { rrr * f : rr}L s d ..::i-:-1' 9P !.ll!!.r.1
Test Report No. : CE/2013/13191 Dale:2013101121 Paqe | 5 of 29
mg/Kg With reference to US EPA 5021method. Analysis was performed byGC/MS.
n .d .
Chlorof luorocarbon-1 2 (CAS No. :75-714]
mg/Kg With reference to US EPA 5021method. Analysis was performed byGC/MS.
n-d.
;ii; i;i;;; ; ,!,.i .d '; ri. c.-,;;' ',ti; b iL; &ne'ar condi om d;; ;;;;i i;; d;-tu:^a 3uh;ed b rem! ano co.o @ns h' rrqd. b;{.I d{w.{s.o- e.i ; ; d ; l a ' ' h " i j . ' i - * ' ; . d i $a fnn ' 3 . "dddh .F 'ha rme or i! 'meilerton onrv and -; ; ; ; - ; ; h : ; . ; n . d J , ' i . i ' . c ' o i d 0 a f ; i " ' d f u r 1 a " .
mg/Kg With reference to US EPA 502 1method. Analysis was performed byGC/t S.
1 n.d.
Chlorcfluorocarbon-1 14 (CAS No.l7efi-2)
mg/Kg With reference to US EPA 5021method. Analysis was performed byGC/MS.
1 n.o.
Chlorotluorocarbon-l 15 (CAS No.:76-15-3)
msasWith reference to US EPA 5021method. Analysis was performed byGC/MS,
1 n . d .
Group lllChlorof luoroca6on-1 3 (CAS No.:75-72-9)
mg/kg With reference to US EPA 502 1method. Analysis wEs perfomed byGC/MS.
1 n.d-
Chlorof luoroca6on-'1 1 1 (CAS No.:354-56-3)
mg/Kg With reference to US EPA 5021method. Analysis was performed byGC/MS.
1 n.d-
Chlorofluoroc€rbon-'112 (CAS No.:76-12-O)
mlyKg With reference to US EPA 5021method. Analysis was performed byGC/MS.
'I n . d .
Chlorof luorocarbon-2l 1 (CAS No.:422-78-8)
mgikg With reference to US EPA 5021method. Analysis was pertormed byGC/MS.
'I n.d.
Chlorof luorocarbon-21 2 (CAS No. :3182-%-1)
mg/Kg With refefence to US EPA 5021method. Analysis wEs performed byGC/MS.
1 n.d.
Chlorof luoocarbon-21 3 (CAS No.:2354{6-5)
mg/kg With reference to US EPA 5021method- Analysis was performed byGC/[rS.
1 n.d.
Chlorof luoroca6on-214 (CAS No.:29255-31-0)
mgKg With reference to US EPA 5021method. Analysis was performed byGC/MS.
n.d.
Chlorof luorocarbon-215 (CAS No.:425943-2)
mgi Kg With reference to US EPA 5021method. Analysis w€s performed byGC/MS.
n .d .
. ! . .;
"'.i;-.. ; *d b' h6 cmou
,no b' e€dM c romar dnoments rd pd 6 hr3 and cot ions b' Lrecl;;;;tmh ;A;ii-6; md :.$-r,sr3ne . reo rE 'n r . ne f l ono -vdFowt i n ' h . 'mbo rca -s iF taon< 3 l ponqb f t v ' r o c iP "d t r sdo* *o , j " t ' o . i * - " " 0 a i r
" mo l imdmb- i 5doo - t ' a t b pno ' l de roo t l a o . i c
( omod i Mv r s ! o zao arasrca o's.ry o' r;sfr-ton ol I e d+n d
.-""'.,ii::lliiillr: r l Y"!:1t]:rt"pjrtrg:.11':11j'-
Test Report No.: CE/201313191 DaIe 2013101121 Paoe 7 of 29
i J6 i i " oJ . i t i j a ' . i ' . n " , ' " ' , qa i 6 re - , ddod id ' b 'F3ad i , { do ' *La€ - . d t ?n &
rhermed b deiudio onl! d{sh F. aborc ens'n{rdo'' ' l;;;;" b; ;;-ii!i;,;. ilis i; ;'q;,r"";, iir" r*a;m;ry ay lmdb';d *sdon. ro@ery o, disddoi dr he 6n,ent o
Test Report No.: CE/2013/13191 Date:2013101121 Page: 8 of 29
HCFC-133a (CAS No.: 75-88-7) mg/Kg With reference to US EPA 5021method. Analysis was performed byGC/t S.
n.cl.
HCFCI4lb (CAS No.: 1717-00€) mgKg With reference to US EPA 5021method. Anaiysis was performed byGC/MS.
I n.d.
HCFC-142b (CAS No.: 75-68-3) mg/Kg With reference to US EPA 5021method. Analysis was performed byGC/MS.
1 n-d.
HCFC-221 (CAS No.: 422-264) mg/kg With reference to US EPA 502 1method. Analysis was performed byGC/l\rs.
1 n.d.
HCFC-222 (CAS No.r 422-49-1) mg/Kg With reference to US EPA 5021melhod. Analysis was performed byGC/MS.
1 n.d-
HCFC-223 (cAs No.: 422-526) mg/Kg With reference to US EPA 5021method. Analysis was performed byGC/MS.
'I n.d.
HCFC-224 (CAS No.: 422-54-8) mg/Kg With reference to US EPA 5021method. Analysis was performed byGC/MS.
1 n.d.
HCFC-22sca (CAS No.: 422-56-0) mg/Kg With reference to US EPA 502'lmethod. Analysis u/as performed byGC/MS.
1 n.d.
HCFC-22scb (CAS No.i 507-55-1) mg/Kg With reference to US EPA 5021method. Analysis was perfomed byGC/MS.
n.d.
HCFC-226 (CAS No.: 431-87-8) mg/Kg With reference to US EPA 502'1method. Analysis wes performed byGC/MS.
n.d.
HCFC-231 (CAS No.r 421-94-3) m9Kg With reference to tJS EPA 502'1method. Analysis was Performed bYGC/[iS.
't n.d.
HCFC-232 (CAS No.: 460-89-9) mg/Kg With reference to US EPA 502 1method. Analysis was Performed bYGC/MS.
1 n.d.
ow. m h's 3s B@. FF ul b ne 3
.;;.";;-", is ,rd b, h c-ps y sD.eq,o 6 Gr6rcdoj:i.,.*,pffii;F"1;f;*&,;:,#"r,,!;ri:\t,itr,:xi{.y;%1"iffT"1_i;j ?;:jli:i:",Sblecl lo rems and @ndhons ftr.,m. o. ar .* dstrnra,o, nd.inedd 'nu*"- "t:lll.lj;;1.;:t*"*;,f;:::*i;;fjl,,". if;ti* ilf,;'"-;le:'i:";i;; -?":ig:";',?lli0,:"ii
* * " " "a - , * ' - " - , - . J i i - a ; l ,mom.EF .do - -a ' 6 fdc r e . , & y l 1 a n 1 o n z e d " s d d , . - ' # i ; ; ; ; : ; ; i ; ; * : l i " ^ r ' r o b r o - d i b ' r e * d b r r l l e ' " ' { r o L h e b n
r\eift peicivft rs/:r";iii i ) i il i i 4firb
Test Report No- : CE/201313191 Date:2013101121 Paoe i gof 29
mg/kg With reference to US EPA 5021method. Analysis wEs perfomed byGC/MS.
1 n.d.
'l,}Dichloropropane (CAS No. :142-2&9)-
mg/Kg With referenc€ to US EPA 5021method. Analysis was performed byGC/MS.
1 n.o.
z,2-Dichloropropane (CAS No.:53+20-7',)
mg/Kg with reference to us EPA 5021method. Analysis wa6 performed byGC/MS.
I n.d.
Carbon tetrachloride (CAS No.i56-23-5)
mgikg Wath reference to US EPA 5021method. Analysis was pertormed byGC/MS.
1 n . d .
Chloroethane (CAS No.: 7$00-3) mg/Kg With reference to US EPA 502 1method. Analysis was porformed byGC/MS.
1 n.d.
Chlorofom {CAS No.: 67-66-3) mg/Kg With reference to US EPA 5021method. Analysis was performed byGC/[rS.
1 n.o.
Chloromethane (CAS No.: 74-87-3)
mg/Kg With reference to US EPA 5021method. Analysis wEs performed byGC/MS.
1 n.d.
cis-1,2-Dichloroethene (CAS No.:15G59-2)
mdkg With reference to uS EPA 5021method. Analysis\ ras pertormed byGC/MS.
1 n . d .
ci6-l,3-Dichloropropene (CAS No.l10061-01-5)
mg/Kg with reference to us EPA 502 1method. Analysis was performed byGC/MS,
1 n.d.
Hexachlorobutadiene (CAS No.i8768-3)
mg/Kg With reference to US EPA 5021method. Analysis was performed byGC/MS.
'I n-d.
Methylene Chloride (CAS No.: 75-09-2)
mg/kg With referenc€ to US EPA 5021method. Analysis was performed byGC/MS.
n.d.
Tetrachloroethene (CAS No.: 127-184)
mgI(g With reference to uS EPA 5021method. Analysis was performed byGC/MS,
n.d.
s r lEk t repo ld - r t bs ' s
i ;T f t :k" ' ' ' , . " " " "* - , " . " . " " . " - ; - . " ' " " ' " : . . i " , ' i ' . "s . . *p**"" . i .a 'a-uu"" ' l .osdo!esbA-"e!o 'o 'i * i i " i
" an ' i n t ma r ; i e r c i . r i d . db -em, ' bco r ' . " r ' ' edonLOo@f t1Rd"ms { ' , o -
a1 eas , dco ,d tuo s r8Tseooai ; ; ; ; j b ; i i ; # ; i i " ; ; i ; ; . i " " " ; . ^ d ' * h . * , e ' ' d o . t r | ' 0 r ' a ' ' a d . gh " | - . d k FE ; \ ed on odv and w ,h i d he im so c rems nsMros ' L r v i b i s r r . l a d lF tum"d6;;;(-;;;;;;-;;;;6;i;;oi:a ;; ;;J;, . ;. :ie r,..obidd-.-d -n, oo@r1 d "o 0- re o! @o "oo;#ffi;:p;;;;,-,i;;;:d i;i,;: i;a;t ;iai,n-i;";i h" -"bd
"; r . : r i r ! r ' i ' i t - l r .
Test Report No.:CE/2013/13191 Dale 201310121 Paoe:12 ot 29
Not. :'1. mg/kg = ppm | 0.1wt% = loooppm2. n.d. = Not Detecled3. MDL = Method Detection Limit4. "-"= Not Regulated5. - = Qualitative analysis (No Unit)6. N€gative = Undet€ctable / Positive = DetectableT Testing range of asbestos qualitative analysis is from less than 0.1% to 1OO%. The judgment crjterion: asbestos fibers
being found is shown as "Positive'; asbeslos fibers not being found is shown as,'Negative..
PFOS Refe.ence Intormetion : POPS - (EU) 757m10Outlawing PFOS as substances or preparations in concentrations above O.OOl% (lOppm), in s€mi-finished products ofarticle6 or parts at a level above 0.1%(1000ppm), in textiles or other coated materials above 1pg/m,.
a;; . : : ' ' . <we p" 'ed owtd ars dbir oll, :T i ;e1d; : - . ;F ; l ;u . ; " ;o€ ; '6hr 'mdcordb4u i ;n rc : .oo . - . ' l dMa ' jdq |
" ' , , . . - ' * * . . " ' , , " , , " ;r i , i j t i i o is ; ; l *m, - rv - " - ' . ,n " . ,uo |cs '+n ' .d ;n i; a ; i i i i ' . i # a j g . * , g , ' r - ' g t : T o o ] g ! j l o B J n d e l ' 9 ? n % d f ' @ o - 4 k T i 3 d o (
u ' { i;:;; ;;;;r;;: : 'oeft | s 5d|" oo'arc"a -dib'
l i i i ,: r !l I {lii:rri
Test Report No. : CE/2013/13191 Dale:20131O1n1Page : 18 of 29
r Name ofthe person who made measurement Bafiy Tsengr Nameoftheperson incharge of measurcment: Troy Chang
Data
lll |ltt][ttlllt
M ti rhlsresr €Don rerer ont ro be tpdorMtbpembsondrE
rhsiftinmr'a €sid b! lh€ cmoanv eubEci ro 'ls Gne'arcndiions orseruie or ed o6'ldat a$ abeonie ms .M,@iditons lrhand ror € adrof, c romd dntum.nb e 6 e d 6 re' ms and C.d ton s lo' Ered msad.Cond( ons/rerm* Dotuft
d u'is. dion isues derned bere i tuv s Ihe companvs nnd'nqs ari heheo ib i n l e iwn1ono i vandw id i n l he ] im$o l c i e i 1sns1 rc i ons f ; nyTheco Inpas$ |e Iespon3b |ftnsdon rrom err"vnq ri h., adFioftJml' hEoodm"lrConprnJ diy iaLtdzeo arleu on
Test Report No. : CE/2013i13191Dale:2013101121Page : 19 of 29
r Name oflhe person who made measurement: Bary Tsengr Nam€ of the person in charge of measuremenl Troy Chang
Data
tl][ || t|:ll]I
a m o € ' : e e e d I i ' 6 r ? o o ' € o' , t . - I . t i ,
i i i i i . i . * . " * . * o " o e c o . o a ; ' ' o d b ' i c s t . | L d d ' o ' ' d . o l , o ' 3 e e * o A d e 3 s 9 J - l;; ;i; ;.;;; ;;;' ;r;. ;;;B &;ed b rems rm cdiGmb 0 Eranrcn( ooom.{ . ar "B {- "o_ .innn;iiri,h ,omnta;.; d :1d'do sr! d,,rd h.r,he ru or r 'n,ei!en, on oi v dnd dbinher+aorcrcn \'ran01"; ; ; ; ; ; ; ; ' ; " ^ n ; ; i ; ; i o i " * o o t a " . ' ' c . * . u " ' * . ' o , ' o o J m ' 6 i I o o J - e { o ' '( dmoa., hr ,rd bo zen ,n4no'
N€r tdFi.[r ri iwri / i i-: ' !: ]. ' i : . r {iLli! l i
Test Report No. : CE/2013/13191D?[e:2013101121Page:20 ol 29
I Name ofthe person who made measuremenl: Victor KaoI Name of the person in charge of measurementt Wendy Wei
( Reie.ence method: EPA 600/R-93/l 16l
Sampling
Contai ning AsbestovPositive Not conhining Asbesto6/ N€gative
!]l[ttt ltt]l
" i t , 1rh6 do.irm.m E Lsusd s rha com"nd b . l . {on . r .mar o@merb . . ' iF - d re- 'dndco ld ro 's ro Fsa vdm(odor - " -3€Dor_ena
ndemnrca( on and 'LlNd d6 6su6rheriftdl6 d.iwi{on otrlv a qsi r;nrTh?com0anyssercspoi5br'ry'' 'o Lsc'en and'hsdocum.ndt r sdo hma . G ro a r i t e nConpaiy ay unauhdzad a lsrdion
k { 4 r t P ( r y r . e d / i . l : i . i 1 1 i t * j : t j r
Continue when probl€rnsarc encournefed withDS-PLM and/or for quality assurance pufposes
Asbestos identifc€lion by dispetsion stainingpola zed light micrcscope (DS-PLM)
Asbe€tos idenlifcation by X-faydiff raclion speclrometer (XRD)
Test Report No. : CEl2013i/13191 Date : 2013101121 Paae : 21 of 29
CERAI,iITEC GMBHGESCHAFTSBEREICH
!
I
Analytical flow chan of Organic-Tin content
Name ofthe person who made measurement: Ginny ChenName ofthe person in charge of measuremenl Troy Chang
Analytical flow chart of halogen content'1) Name of the oerson vt/t|o made measurement: Rita Chen2) Name of the person in charge of measurement: Troy Chang
||l ||tt]tI|tttll
9fj] iH*"", ';:* ' ' ,*.- '"], ' ' , ;;"...""*.l"i"".-".n.*,." ' '-"*"'.n-.*'."1' ; ; t i ; d f u .bmddmmmE' *oFdhh rsmdcodbn 'b ; ; i . nn . cDo6m{ | J# { , od 'ri,:"luri6'in
'rn,r Ardbs; ;jlnri'n dhatu-.in in i
" l " d* . " - , , " * i ' r . . , so - t "n .c i " . , ; ' ; ' : ;a ; . ; ; ; ' - ; - "F*br ' rv rb c* r id ' '<dc ' -c
r i in i i , " j r . * lo i rua i r " monoodm. . ' i ' doo .ne1rcomoanv try unau,tu'z& abad.,-q.ry * I'kh*- drb-tu;it;iFt€ne or th sdturud smawtu
i. ., + i _ri;\l
lFli33!1
Sample pretreatment / separation
Wdghting and putting sample in cell
Oxygen Bomb Cornbustion / Absorption
Dilution to fixed volume
Analysis was performed by lC
Test Report No. : CE/20'13/13191Dai'e : 2O13101n1 Page : 28 of 29
One (1) group of submitted samples said to be : Part Description : Sand Part Number : 311.7374.5000 Date Sample Received : Mar 14, 2013 Date Test Started : Mar 14, 2013
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
With reference to IEC 62321: 2008, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.
ND 5
Halogen Content
Fluorine (F) ppm ND 50
Chlorine (Cl) ppm 154 50
Bromine (Br) ppm ND 50
Iodine (I) ppm
With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by Ion Chromatograph. ND 50
Remarks: ppm = parts per million based on weight of tested sample = mg/kg
ND = Not detected
RL = Reporting Limit, Quantitation limit of analyte in sample Responsibility of Chemist: Kevin Liu/ Irene Chiou/ Vico Lin Date Sample Received : Mar 14,2013 Test Period : Mar 14,2013 to Mar 19,2013
Test For Hexabromocyclododecane (HBCDD) Reference Standard:USEPA 3540C
End of Report
This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct.
Sampling/grinding or cutting
Weigh sample and add organic solvent
By soxhlet extraction
Concentrate the extract and make up with organic solvent
Applicant: ELSCHUKOM ELEKTROSCHUTZKOMPONENTENBAU Date: JAN 18, 2013 GMBH
GEWERBESTRASSE 87,D-98669 VEILSDORF, GERMANY
Sample Description: Two (2) pieces of submitted samples said to be : (1)Substrate. (2)Plating. Item Name : Wire With Plating. Item No. : 101 -- 271.0 --- tin plated,copper wire,Cu,Sn --%. Country Of Origin : Germany.
As requested by the applicant, for details refer to attached page(s). ************************************************************************************************************************************************************
To be continued
Test Report Number: SHAH00362261
Tests Conducted
Page 2 Of 5 Intertek Testing Services Ltd., Shanghai
The above limits were quoted from RoHS Directive 2011/65/EU for homogeneous material.
(C) Test method: Testing item Testing method Reporting limit
Cadmium (Cd) content With reference to IEC 62321 Edition 1.0: 2008, by acid digestion until the tested sample was totally dissolved, and determined by ICP-OES.
2 mg/kg
Lead (Pb) content With reference to IEC 62321 Edition 1.0: 2008, by acid digestion until the tested sample was totally dissolved, and determined by ICP-OES.
2 mg/kg
Mercury (Hg) content With reference to IEC 62321 Edition 1.0: 2008, by acid digestion until the tested sample was totally dissolved, and determined by ICP-OES.
2 mg/kg
Chromium (VI) (Cr6+) content (for metal)
With reference to IEC 62321 Edition 1.0: 2008, by boiling water extraction and determined by UV-VIS Spectrophotometer.
0.02mg/kg with 50cm2
(in testing solution)
Date sample received:Jan.14, 2013 Testing period: Jan.14, 2013 To Jan.17, 2013
************************************************************************************************************************************************************ To be continued
Test Report Number: SHAH00362261
Tests Conducted
Page 3 Of 5 Intertek Testing Services Ltd., Shanghai
Test for Cd/Pb/Hg/Cr (VI)/PBBs/PBDEs contents Reference standard: IEC 62321 Edition 1.0: 2008
Remarks: *1: list of appropriate acid:
Material Acid added for digestion Polymers HNO3,HCL,HF,H2O2,H3BO3 Metals HNO3,HCL,HF Electronics HNO3,HCL,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
************************************************************************************************************************************************************ To be continued
Sampling/grinding or cutting
Weigh sample and for different material, digest
the sample with appropriate acid*1
Make up with deionized water
Cd/Pb/Hg
Analyzed by ICP-OES
Weigh sample and add alkaline
solution
Definite temp. Extraction
Make up with deionized waterand add diphenyl-carbazide
solution
Cr6+
Weigh sample and add organic
solvent
Soxhlet extractionor
Solvent extraction
Concentrate the extract and make up with organic
solvent
PBBs/PBDEs
Analyzed by UV-VIS
Analyzed by GC-MSD
Spot test
Get 50cm2 samples
Boiling water extraction
Metal Polymers / electronics
Positive*2
Confirm the tested samples are totally
dissolved
No
Cool and filter the extract
Yes
Test Report Number: SHAH00362261
Tests Conducted
Page 4 Of 5 Intertek Testing Services Ltd., Shanghai
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Test Report. No. SHAEC1317518847 Date: 06 Sep 2013 . Page 1 of 6.
ZHEJIANG ASIA GENERAL SOLDERING&BRAZING MATERIAL CO., LTD .
XIHU INDUSTRIAL PARK, SANDUN, HANGZHOU CITY, ZHEJIANG, PROVINCE, CHINA
.
.
The following sample(s) was/were submitted and identified on behalf of the clients as : LEAD-FREE SOLDER
WIRE.
SGS Job No. : SP13-026309 - SH .
Model No. :. YTW102(692539-002).
Composition : . Sn2.0CuRE.
Date of Sample Received : . 03 Sep 2013.
Testing Period : . 03 Sep 2013 - 06 Sep 2013 .
Test Requested : . Selected test(s) as requested by client. .
Please refer to next page(s). .
Please refer to next page(s). .
Test Method : .
Test Results : .
Based on the performed tests on submitted samples, the results of Lead,
Test Report. No. SHAEC1317518847 Date: 06 Sep 2013 . Page 2 of 6.
Test Results : .
Test Part Description : .
Specimen No.. SGS Sample ID. Description.
1. SHA13-175188.040 Silvery metal wire .
Remarks :.
(1) 1 mg/kg = 1 ppm = 0.0001% .
(2) MDL = Method Detection Limit .
(3) ND = Not Detected ( < MDL ) .
(4) "-" = Not Regulated .
RoHS Directive 2011/65/EU.
Test Method : . (1) With reference to IEC 62321-5:2013, determination of Cadmium by ICP-OES.
(2) With reference to IEC 62321-5:2013, determination of Lead by ICP-OES.
(3) With reference to IEC 62321-4:2013, determination of Mercury by ICP-OES.
(4) With reference to IEC 62321:2008, determination of Hexavalent Chromium by spot test /
Colorimetric Method using UV-Vis.
(5) With reference to IEC 62321:2008, determination of PBBs and PBDEs by GC-MS. .
040.
Cadmium (Cd) . 100 mg/kg. 2 ND
Lead (Pb). 1000 mg/kg. 2 140
Mercury (Hg). 1000 mg/kg. 2 ND
Hexavalent Chromium (Cr(VI)) . - - ♢ Negative
Sum of PBBs. 1000 mg/kg. - ND
Monobromobiphenyl . - mg/kg. 5 ND
Dibromobiphenyl . - mg/kg. 5 ND
Tribromobiphenyl . - mg/kg. 5 ND
Tetrabromobiphenyl . - mg/kg. 5 ND
Pentabromobiphenyl . - mg/kg. 5 ND
Hexabromobiphenyl . - mg/kg. 5 ND
Heptabromobiphenyl . - mg/kg. 5 ND
Octabromobiphenyl . - mg/kg. 5 ND
Nonabromobiphenyl . - mg/kg. 5 ND
Decabromobiphenyl . - mg/kg. 5 ND
Sum of PBDEs. 1000 mg/kg. - ND
Monobromodiphenyl ether . - mg/kg. 5 ND
Test Item(s). Limit. Unit. MDL.
Test Report. No. SHAEC1317518847 Date: 06 Sep 2013 . Page 3 of 6.
Test Item(s). Limit. Unit. MDL. 040.
Dibromodiphenyl ether . - mg/kg. 5 ND
Tribromodiphenyl ether . - mg/kg. 5 ND
Tetrabromodiphenyl ether . - mg/kg. 5 ND
Pentabromodiphenyl ether . - mg/kg. 5 ND
Hexabromodiphenyl ether . - mg/kg. 5 ND
Heptabromodiphenyl ether . - mg/kg. 5 ND
Octabromodiphenyl ether . - mg/kg. 5 ND
Nonabromodiphenyl ether . - mg/kg. 5 ND
Decabromodiphenyl ether . - mg/kg. 5 ND
Notes :.
(1) The maximum permissible limit is quoted from directive 2011/65/EU, Annex II
(2) ◇Spot-test:
Negative = Absence of Cr(VI) coating, Positive = Presence of Cr(VI) coating;
(The tested sample should be further verified by boiling-water-extraction method if the spot test result
is Negative or cannot be confirmed.)
◇Boiling-water-extraction:
Negative = Absence of Cr(VI) coating
Positive = Presence of Cr(VI) coating; the detected concentration in boiling-water-extraction solution is
equal or greater than 0.02 mg/kg with 50 cm² sample surface area.
Information on storage conditions and production date of the tested sample is unavailable and thus
Cr(VI) results represent status of the sample at the time of testing. .
Halogen.
Test Method : . With reference to EN 14582: 2007, analysis was performed by Ion Chromatograph (IC). .
Test Item(s). Unit. MDL. 040.
Fluorine (F). mg/kg. 50 ND
Chlorine (Cl). mg/kg. 50 354
Bromine (Br). mg/kg. 50 ND
Iodine (I). mg/kg. 50 ND
Test Report. No. SHAEC1317518847 Date: 06 Sep 2013 . Page 4 of 6.
ATTACHMENTS
RoHS Testing Flow Chart
1) Name of the person who made testing: Jan Shi/Star Wang/Shara Wang/Gary Xu 2) Name of the person in charge of testing: Jeff Zhang/George Xu/ Jessy Huang 3) These samples were dissolved totally by pre-conditioning method according to below flow chart. (Cr
6+
and PBBs/PBDEs test method excluded)
Cr6+
Adding 1,5- diphenylcarbazide
for color development
UV-Vis
Nonmetallic material
Metallic material
Adding digestion reagent
DATA
A red color indicates the
presence of Cr6+
. If necessary, confirm with
UV-Vis.
Sample Preparation
Sample Measurement
PBBs/PBDEs
Sample solvent extraction
Concentration/ Dilution of extraction
solution
Filtration
GC/MS
DATA
ICP-OES
Solution
Filtration
Residue
1) Alkali Fusion / Dry Ashing
2) Acid to dissolve
Pb/Cd/Hg
Acid digestion with microwave/ hotplate
DATA
Heating to 90~95℃ for extraction
Filtration and pH adjustment
Boiling water extraction
Adding 1,5- diphenylcarbazide
for color development
Spot test Positive
Negative
DATA
Test Report. No. SHAEC1317518847 Date: 06 Sep 2013 . Page 5 of 6.
Halogen Testing (oxygen bomb) Flow Chart
1) Name of the person who made testing: Sisily Yin
2) Name of the person in charge of testing: Linda Li
Sample cutting/preparation
Sample measurement
Combustion in oxygen bomb
Dissolved in an absorption
solution
Filtration
Analyzed by ion
chromatography. Double confirm
by other instruments, if
necessary
DATA
Test Report. No. SHAEC1317518847 Date: 06 Sep 2013 . Page 6 of 6.
Sample photo: .
SHAEC1317518847
SHA13-175188.040 .
SGS authenticate the photo on original report only .
*** End of Report *** .
TEST REPORTNO. : 4002R1 30403070-2R02 oate: Apr08, 2013
Customer: Suzhou FuHong Electronic IndustrialCo., Ltd.Add'€gs: NO.89WEI DU RoAD, WANGTING ToVvN, XIANGCHENG DISTRICT, sUzHoU. cHINAReport on th€ submittad sample said to beSample name: r{Q copper shell
Page 1 of4
in the submitted samole in
itod€l:,
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uatertat;/ I iEuyer: / \Supptier: \,_--_./tlanufacturer: /
Samplo recelved dato;TeEtlng perlod; From Apr03,
Testinc Rsouested \
As specified by client, to determine the Lead, Cadaccordanca with Directive 20't1l65/EU (RoHS).
Tostinq m6thod:
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Conclusion:
Wlen tested as specified, the submitted sample complied with the requirements of Directive 2011/6S/EU (RoHS).
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