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PAGE 1 www.geodf.com 1-800-GETS GEO Lost Circulation Plug Description Uses Benefits GEO STOP LOSS High Filtration Lost Circulation Squeeze GEO STOP LOSS is a high filtraon lost circulaon treatment that has been found to meet a number of drilling needs. Mixed without weight material, the squeeze has a density of 9.3 ppg, a design which helps minimize further fracturing associated with losses. The fundamental process of the squeeze relies on uncontrolled filtraon to concentrate the ingredients producing a thick, tough and stable cake. Mixing of the GEO STOP LOSS can be performed ahead of me. A separate pit (50 to 100 bbls) with an agitator will keep the prepared slurry ready for use. This can be prepared while drilling to save me in the event of losses. Obviously this is a procedure to be used when losses are ancipated or when losses have occurred and addional losses may be expected. The “pill” may be held for an extended period (days or perhaps even weeks) with out degradaon of the materials. Placement of this lost circulaon treatment may be performed without dropping the bit, MWD or mud motor (depending on addional LCM addions). By placing the material above a loss, the weight of the fluid above
4

High Filtration Lost Circulation SqueezeMud Weight 9.3 ppg 12.0 ppg 13.0 ppg 14.0 ppg Water or LVT 41.5 k 37bb 35bb 33bb STOP LOSS 200 sacks 170 k 140 k 120 k Barite none 76bb 104

Mar 10, 2020

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Page 1: High Filtration Lost Circulation SqueezeMud Weight 9.3 ppg 12.0 ppg 13.0 ppg 14.0 ppg Water or LVT 41.5 k 37bb 35bb 33bb STOP LOSS 200 sacks 170 k 140 k 120 k Barite none 76bb 104

PAGE 1 www.geodf.com 1-800-GETS GEO

Lost Circulation Plug

Description

Uses

Benefits

GEO�STOP�LOSS

High Filtration Lost Circulation Squeeze

GEO�STOP�LOSS is a high filtra�on lost circula�on treatment that

has been found to meet a number of drilling needs. Mixed without

weight material, the squeeze has a density of 9.3 ppg, a design which

helps minimize further fracturing associated with losses. The

fundamental process of the squeeze relies on uncontrolled filtra�on to

concentrate the ingredients producing a thick, tough and stable cake.

Mixing of the GEO�STOP�LOSS can be performed ahead of �me. A

separate pit (50 to 100 bbls) with an agitator will keep the prepared

slurry ready for use. This can be prepared while drilling to save �me in

the event of losses. Obviously this is a procedure to be used when

losses are an�cipated or when losses have occurred and addi�onal

losses may be expected. The “pill” may be held for an extended period

(days or perhaps even weeks) with out degrada�on of the materials.

Placement of this lost circula�on treatment may be performed without

dropping the bit, MWD or mud motor (depending on addi�onal LCM

addi�ons). By placing the material above a loss, the weight of the fluid above

Page 2: High Filtration Lost Circulation SqueezeMud Weight 9.3 ppg 12.0 ppg 13.0 ppg 14.0 ppg Water or LVT 41.5 k 37bb 35bb 33bb STOP LOSS 200 sacks 170 k 140 k 120 k Barite none 76bb 104

PAGE 2 www.geodf.com 1-800-GETS GEO

Lost Circulation Plug

Drillout

Rubble Stabilization

Procedure

will push the pill into the loss zone where the water will quickly leave. GEO�STOP�LOSS�(Continued)�

The residual material forms a thick tough cake that bridges and seals

both fractures and extremely high permeability.

Drillout of GEO�STOP�LOSS is not as damaging to a fresh water based

mud system as a cement plug would be. While the pH of the plug is

12.3 and the filtrate pH is 12.1, the Pf of the filtrate is only 1.2. Most of

the alkalinity is lost to the forma�on as the plug dewaters. Lower pH

and Calcium levels than cement allow Bentonite to con�nue to

func�on as a viscosity and fluid loss agent a5er drillout. The risk of

sidetracking the hole is reduced because this material though hard

does not have compressive strength great enough to cause a sidetrack.

Rubble stabiliza�on is also an appropriate applica�on. By gently

squeezing the material into the coarse spaces between unconsolidated

rubble a new and stronger matrix material is subs�tuted for the

original. Because of its lower alkalinity this plug has a minimal effect on

forma�ons that are prone to swell or slough when exposed to hydroxyl

ions.

Simula�on of the plugging ac�on at the surface is not as simple as

allowing a cement plug to harden. Allowing a sample of the pill to sit in

a container will not result in dewatering and produc�on of a cake. In

order to observe the nature of the cake deposited, a sample of the

finished mix should be placed in a filter press and filtered at 30 psi. In a

ma:er of minutes all the free water will be expelled and a sample of

the cake can be observed.

GEO�STOP�LOSS�cakes from development series .

Page 3: High Filtration Lost Circulation SqueezeMud Weight 9.3 ppg 12.0 ppg 13.0 ppg 14.0 ppg Water or LVT 41.5 k 37bb 35bb 33bb STOP LOSS 200 sacks 170 k 140 k 120 k Barite none 76bb 104

PAGE 3 www.geodf.com 1-800-GETS GEO

Lost Circulation Plug

Mixing Procedure

STOP�LOSS�(Continued)�

GEO�STOP�LOSS�PROCEDURE

1. GEO�STOP�LOSS is a high solids/high filtra�on lost circula�on squeeze. It will not suspend well without agita�on although it does

not se:le out hard or set up if held unagitated for prolonged

periods.

2. Select a mixing pit that has excellent agita�on and a good suc�on

directly to the mud pump. Remove any drilling fluid or Gel based

LCM. The more mud le5 behind the less effec�ve the GEO�STOP�

LOSS will be. Fill the pit with water or oil to 83% of the final desired volume, leaving space for expansion while adding material.

3. Add 100 pounds per barrel GEO�STOP� LOSS. For 50 bbls of finished volume start with 41 bbls of water (or oil) and mix 5,000

pounds (200 of the 25-pound sacks) of GEO STOP LOSS blended

LCM material.

4. For a weighted pill see the table below. Mix GEO�STOP�LOSS�first, then add Barite.

5.

6. Allow this slurry to mix un�l the rig crew is ready to spot the pill. Make

sure everyone knows what to do and that all valves operate properly.

7. If the slurry is too thick, add water (or oil) to thin. DO NOT use any

chemical thinner.

8. Pump the pill away with or without the bit, hanging the pipe at or below

the loss zone. Calcula�ons for hydrosta�c pressure should use 9.3 ppg for

Mud Weight 9.3 ppg 12.0 ppg 13.0 ppg 14.0 ppg

Water or LVT 41.5

sacks

37 bbls 35 bbls 33 bbls

STOP LOSS 200 sacks

170 sacks 140 sacks 120 sacks

Barite none 76 bbls 104 sacks 140 sacks

To Build 50 bbls of GEO STOP LOSS

Page 4: High Filtration Lost Circulation SqueezeMud Weight 9.3 ppg 12.0 ppg 13.0 ppg 14.0 ppg Water or LVT 41.5 k 37bb 35bb 33bb STOP LOSS 200 sacks 170 k 140 k 120 k Barite none 76bb 104

PAGE 4 www.geodf.com 1-800-GETS GEO

Mixing Procedure (cont.)

Typical Physical Properties

Safe Handling Recommendations

Packaging

the density of the pill unless weighted with Barite. Displace the GEO�

STOP�LOSS�pill to the bit.

STOP�LOSS�(Continued)�

9. Flush the mixing pit with water (or mud or oil). This may be used as part

of the displacement fluid.

10. Pull the drill pipe above the theore�cal top of the plug and flush the pipe.

Trying to fill the hole at this point may help gently squeeze the plug into

the forma�on. If the loss is due to natural fractures in a competent

forma�on, squeezing with up to 200 psi is effec�ve in geFng the material

away from the well bore and into the fractures. In weak forma�ons where

the loss is pressure induced do not squeeze (shut in).

11. To gently squeeze calculate the volume of squeeze to leave in the hole.

For instance 100 lineal feet in 12 ¼” hole would be 14.6 bbls. Pump no

more fluid than the pill volume less the amount to be le5 in the hole. Thus

for a 50 bbl pill as above, only 35.4 bbls would be pumped. Too much

volume may propagate the fractures as well as ini�a�ng new fractures

and push the plug so far from the well bore that it looses its effec�veness.

12. Allow the GEO�STOP�LOSS�plug to dewater. This reduces the volume by

approximately 50% and may require an addi�onal pill to fill the loss zone.

13. Wait 2-4 hours before drilling out to allow the plug to dewater.

14. Treat for calcium contamina�on with Bicarb if needed while drilling out.

Many �mes this is unnecessary so wait un�l seeing signs of contamina�on

before trea�ng.

15. GEO�STOP�LOSS�may also be used as a sweep in whole mud or as a pill

spo:ed on trips.

Physical Appearance ..................Gray Powder

Specific Gravity ...........................

Hygroscopic ................................no

pH in water .................................Slightly Alkaline

U�lize normal precau�ons for employee protec�on when handling

chemical products. Use approved dust mask for silica dust. Use of

appropriate respirator, gloves, goggles and apron is recommended for

employee comfort and protec�on. See Material Safety Data Sheet

(MSDS) for this prodyuct prior to use.

GEO�STOP�LOSS�is packaged in 40 pound mul�-wall bags.