FORT MEADE, MARYLAND 20755-5350 · PDF fileMC0085, MC0087, MC0088, MC0098 All Samples Except MCOOA7, MCOOB3, MC0068, MC0080, MC0085, MC0087, MC0088, MC0098 All Samples MCOOA7, MCOOA9

\UJ

UNITED STATES ENVIRONMENTAL PROTECTION AGENCYREGION III

ENVIRONMENTAL SCIENCE CENTER x

701 MAPES ROADFORT MEADE, MARYLAND 20755-5350

SDMS DocID 2060883

DATE : May 6, 2005

SUBJECT: Region III Data QA Review

FROM :

TO

Khin-Cho ThaungRegion in ESAT RPO (3EA21)

Christian MattaRegional Project Manager (3HS23)

Attached is the inorganic data validation report for the Big John Savaage - Hoult Road Site(Case#:34031, SDG#:MC0072, MCOOH2) completed by the Region III Environmental ServicesAssistance Team (ESAT) contractor under the direction of Region III EAID.

If you have any questions regarding this review, please call me at(410)305-2743.

Attachments

cc: Tad Yancheski (TETRA)

TO File #: 0023 TDF#: 0479

ANALYTICAL SERVICES AND QUALITY ASSURANCE BRANCH

Printed on 100% recycled/recyclable paper with 100% post-consumer fiber and process chlorine free.Customer Service Hotline: 1-800-438-2474

117911

Lockheed Martin Information TechnologyESAT Region 3US EPA Environmental Science Center701 Mapes Road Ft. Meade, MD 20755-5350Telephone 410-305-3037 Facsimile 410-305-3597

L O C K H E E D M A R T I NWe never forget who \ve 're working for"'

DATE:

TO:

May 2, 2005

SUBJECT: Inorganic Data Validation (M2 Level)Case: 34031SDGs: MC0072 and MCOOH2Site: Big John Salvage - Hoult Road

FROM: Donald M. BrownInorganic Data Reviewer

"^i,^Mahboobeh MecanicSenior Oversight Chemist

Khin-Cho ThaungESAT Region 3 Project Officer

OVERVIEW

Case 34031, Sample Delivery Groups (SDGs) MC0072 and MCOOH2, consisted of forty (40) soilsamples analyzed for total metals and cyanide (GST) by Chemtech Consulting Group (CHEM).The sample set contained no field Quality Control (QC) samples. Samples were analyzed inaccordance with Contract Laboratory Program (CLP) Statement of Work (SOW) ILM05.3through Routine Analytical Services (RAS) program.

SUMMARY

All samples were successfully analyzed for all Target Analyte List (TAL) parameters. Areas ofconcern with respect to data usability are listed below.

Data in this case have been impacted by outliers present in the laboratory blanks as well as thematrix spike, laboratory duplicate and serial dilution analyses. Details of these outliers arediscussed under "Minor Problems"; specific samples affected are outlined in "Table 1 A" andqualified analytical results for all samples are summarized on the Data Summary Forms (DSFs).

117912

Page 2 of 4

MINOR PROBLEMS

Continuing Calibration (CCB) and/or Preparation (PB) Blanks had reported results greater thanthe Method Detection Limits (MDLs) for the analytes listed below. Positive results reported inaffected samples which are less than or equal to five times (^5X) the blank concentrations maybe biased high and have been qualified "B" on the DSFs.

Blank Affected AnalvtesMC0072 CCB cadmium (Cd), selenium (Se)

PB CN"MCOOH2 CCB arsenic (As), Cd, thallium (Tl), CN"

PB Se, CN-

CCBs and/or PBs had negative values greater than the absolute value of the MDL regarding theanalyte listed below. Positive results reported in affected samples which are less than two times(<2X) the absolute value of the blank concentrations may be biased low. The "L" qualifier forthese outliers have been superseded by "J" on the DSFs. Quantitation limits in affected samplesmay be biased low and have been qualified "UL" on the DSFs.

SPG Affected AnalvtesMC0072 silver (Ag)MCOOH2 Ag

Matrix spike recoveries were low (<75% but >30%) for antimony (Sb) in both SDGs as well asfor As in SDG MC0072. Low recoveries may be attributed to matrix interferences or analyte lostduring the digestion process. Positive results reported for these analytes in affected samples inthese SDGs may be biased low. The "L" qualifier for these outliers has been superseded by "J"on the DSFs. Quantitation limits for Sb in affected samples in both SDGs may be biased low andhave been qualified "UL" on the DSFs.

B

The Relative Percent Difference (RPD) for the laboratory duplicate analysis was outside controllimits (35% RPD, ±2XCRDL) for copper (Cu) in SDG MC0072. Positive results reported forthis analyte in this SDG are estimated and have been qualified "J" on the DSFs.

Percent Differences (%Ds) for the TCP serial dilution analysis were outside control limits (>10%)for aluminum (Al), As, magnesium (Mg), nickel (Ni) and potassium (K) in SDG MC0072.Positive results reported for these analytes in this SDG are estimated due to possible matrixinterferences and have been qualified "J" on the DSFs.

117913

Page 3 of 4

NOTES

Reported results between MDLs and Contract Required Quantitation Limits (CRQLs) werequalified "J" on the DSFs unless superseded by "B".

RPDs for the laboratory duplicate analysis were outside contractual control limits (20% RPD,±CRQL) for Al, As and chromium (Cr) in SDG MCOOH2. However, RPDs for these analyteswere within Region 3 established control limits (35% RPD, ±2XCRQL) for soil analysis. Nodata were qualified for these analytes in this SDG based on laboratory duplicate imprecision.

In both SDGs, one (1) of the CRQL check standard recoveries (CRI02) in the second analyticalrun for mercury (Hg) was low (<70%). Therefore, the laboratory reanalyzed the CRQL checkstandard as CRI03, which was inside the control limits. No data were qualified based on thisrinding.

In SDG MC0072, one (1) of the CRQL check standard recoveries (CRI02) in the third analyticalrun for Hg was high (>130%). Therefore, the laboratory reanalyzed the CRQL check standard asCRI03, which was inside the control limits. No data were qualified based on this finding.

The following samples in SDG MC0072 were reanalyzed at the dilutions listed below for Hg inorder to bring concentrations within the linear range of the instrument. Results for this analyte inthese samples were reported from the diluted analyses, annotated with a "+" on the DSFs andnoted below.

Sample ID Dilution FactorMC0087 2.0MC0098 5.0

Data for Case 34031, SDGs MC0072 and MCOOH2, were reviewed in accordance with NationalFunctional Guidelines for Evaluating Inorganic Analyses with Modification for use withinRegion ffl.

117914

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Page 4 of 4

ATTACHMENTS

INFORMATION REGARDING REPORT CONTENT

Table 1A is a summary of qualifiers applied to the laboratory-generated results during datavalidation.

TABLE 1A SUMMARY OF QUALIFIERS ON DATA SUMMARY FORMS AFTERDATA VALIDATION

TABLE IB CODES USED IN COMMENTS COLUMN OF TABLE 1AAPPENDIX A GLOSSARY OF DATA QUALIFIER CODESAPPENDIX B DATA SUMMARY FORMSAPPENDIX C CHAIN OF CUSTODY RECORDSAPPENDIX D LABORATORY CASE NARRATIVE

DCN: 34031.MC0072IM2.wpd

117915

Page 1 of4

TABLE 1ASUMMARY OF QUALIFIERS ON DATA SUMMARY" FORM AFTER DATA VALIDATION

Case 34031,SDGMC0072

SAMPLES POSITIVEANALYTE AFFECTED VALUES

Al

Sb

As

Cd

Cu

Mg

Ni

K

All Samples

MCOOA7, MCOOB3,MC0068, MC0080,MC0085, MC0087,MC0088, MC0098

All Samples ExceptMCOOA7, MCOOB3,MC0068, MC0080,MC0085, MC0087,MC0088, MC0098

All Samples

MCOOA7, MCOOA9

MC0072

All Samples

All Samples

All Samples

All Samples

J

J

J

B

B

J

J

J

J

NON-DETECTEDVALUES BIAS

UL Low

High

High

COMMENTS*

ISD (12%)

>MDL<CRQLMSL (63%)

MSL (63%)

ISD (11%)MSL (35%)

CCB (0.850 J

CCB (0.720 J ng/L)

DUP (54%)

ISD (11%)

ISD (19%)

ISD (10.2%)

See explanation of comments in Table IB

117916

o'

Page 2 of4

TABLE 1ASUMMARY OF QUALIFIERS ON DATA SUMMARY

~~ FORM AFTER DATA VALIDATION

Case 34031.SDGMC0072

SAMPLESANALYTE AFFECTED

Se

Ag

All Samples ExceptMCOOA3, MCOOA7,MCOOA8, MCOOA9,MCOOB3, MCOOB5,MC0072, MC0091

MCOOA4, MCOOA8,MC0068, MC0078,MC0079, MC0080

MCOOA2, MCOOA3,MCOOB5, MC0072,MC0091

All Samples"ExceptMCOOA7, MCOOB5,MC0068, MC0079,MC0080

POSITIVEVALUES

B

B


High

UL Low

High

COMMENTS*

CCB (6.950 J

>MDL<CRQLPBN(-0.16Jmg/Kg)

PBN(-0.16Jmg/Kg)

PB (0.07 J mg/Kg)

* See explanation of comments in Table IB

117917

o-s

Page 3 of4

TABLE 1ASUMMARY OF QUALIFIERS ON DATA SUMMARY~ FORM AFTER DATA VALIDATION

Case 34031, SDG MCOOH2


POSITIVEVALUES

Sb

As

Cd

Se

Ag

MCOOH4, MCOOH5,MCOOJ1,MCOOJ4,MC0064

All Samples ExceptMCOOH4, MCOOH5,MCOOJl", MCOOJ4,MC0064

MC0071

MCOOH3

MCOOH6

MC0065

MC0069, MC0070,MC0071

All Samples ExceptMC0065, MC0069,MC0071

MC0064

MC0065

MC0069, MC0070,MC0071

B


UL

UL

UL

Low

B

B

B

B

B

High

High

High

High

High

High

Low

Low

COMMENTS*

>MDL<CRQLMSL (47%)

MSL (47%)

CCB (4.060 J ng/L)

CCB (0.720 J

CCB'(0.620 J

CCB (0.580 J

CCB (0.720 J ng/L)

PB (0.69 J mg/Kg)

>MDL<CRQLCBN(-1.140Jng/L)

CBN(-1.140Jng/L)

CBN (-0.930 J


117918

Page 4 of4

TABLE1ASUMMARY OF QUALIFIERS ON DATA SUMMARY" FORM AFTER DATA VALIDATION

Case 34031, SDG MCOOH2


Tl

osr

MCOOH2, MCOOH4

MCOOH3, MCOOJ6

MCOOH4, MCOOH5,MCOOH6, MCOOH7,MC0064, MC0065,MC0067, MC0069,MC0070, MC0071

POSITIVEVALUES

B

B

B


High

High

High

COMMENTS*

CCB (14.035 J jig/L)

CCB(4.100Jng/L)

PB(0.11 Jmg/Kg)


117919

'>,Vv

Page 1 of 1

TABLE IBCODES USED IN COMMENTS COLUMN

ISD = Percent Differences (%Ds) for the serial dilution analysis were outside controllimits (>10%) [%Ds are in parenthesis]. Positive results reported are estimated.

>MDL = Reported results are greater than MDLs but less than CRQLs and are considered<CRQL estimated.

MSL = Matrix spike recoveries were low (<75% but >30%) [% recoveries are inparenthesis]. Reported results and quantitation limits may be biased low.

CCB = Continuing calibration blanks had results >MDLs [results are in parenthesis].Reported results which are <.5X the blank concentrations may be biased high.

DUP = The Relative Percent Difference (RPD) for the laboratory duplicate analysis wasoutside control limits (35% RPD, ±2XCRQL) [RPD is in parenthesis]. Positiveresults reported are estimated.

PBN = The preparation blank had a negative result with an absolute value >MDL [resultis in parenthesis]. Reported results which are <2X the absolute value of the blankconcentration and quantitation limits may be biased low.

PB = Preparation blanks had results >MDLs [results are in parenthesis]. Reportedresults which are ^5X the blank concentrations may be biased high.

CBN = Continuing calibration blanks had negative results with absolute values >MDLs[results are in parenthesis]. Reported results which are <2X the absolute value ofthe blank concentrations and quantitation limits may be biased low.

'SV

117920

cv

Appendix A

Glossary of Data Qualifier Codes

117921

^

GLOSSARY OF DATA QUALIFIER CODES (INORGANIC)

CODES RELATED TO IDENTIFICATION(confidence concerning presence or absence of analytes):

U = Not detected. The associated number indicates approximate sampleconcentration necessary to be detected.

(NO CODE) = Confirmed identification.

B = Not detected substantially above the level reported in laboratory or fieldblanks.

R =• Unreliable result. Analyte may or may not be present in the sample.Supporting data necessary to confirm result.

CODES RELATED TO OUANTITATION(can be used for both positive results and sample quantitation limits):

J = Analyte Present. Reported value may not be accurate or precise.

K = Analyte present. Reported value may be biased high. Actual value isexpected to be lower.

L = Analyte present. Reported value may be biased low. Actual value is expectedto be higher.

UJ = Not detected, quantitation limit may be inaccurate or imprecise.

UL = Not detected, quantitation limit is probably higher.

OTHER CODES

Q = No analytical result.

117922

Appendix B

Data Summary Forms

117923

0,

DATA SUMMARY FORM: INORGANIC Page 1 of 8

Case * 34031

Site:

Lab.:

SDG : MC0072

BIG JOHN SALVAGE HOULT RD

CHEM

Number of Soil Samples : 20

Number of Water Samples : 0

MCOOA8

BJS-SBL2-0405

Soil

mg/Kg

4/7/2005

12:25

85.3

1.0

MCOOA2

BJS-SBK2-0405

Soil

mg/Kg

4/6/2005

14:3087.21.0

MCOOA3

BJS-SBK3-0405

Soil

mg/Kg

4/7/200508:2069.51.0

MCOOA4

BJS-SBK4-0405

Soil

mg/Kg

4/7/200509:5584.3

1.0

MCOOA7

BJS-SBL1-0405

Soil

mg/Kg

4/6/2005

12:48

87.8

1.0

ALUMINUM

ARSENIC

BERYLLIUM'(fSff-SS&S,

CALCIUM

IRON

HMAGNESIUM

BiK&i

MERCURY

1330 I J | 501

mmm$iUL 0.34

Sample Number:

Sampling Location :

Matrix:

Units:

Date Sampled:

Time Sampled :

%Solids:

Dilution Factor:

CRQL = Contract Required Quantitation Limit

To calculate sample quantitation limits: (CRQL' Dilution Factor) / (%Solids/100)

SEE NARRATIVE FOR.CODE DEFINITIONS

Revised 09/99

117924


Case #: 34031

Site:

Lab.:

SDG : MC0072


CHEM

MCOOB5

BJS-SBM3-0405

Soil

mg/Kg

4/7/200513:20

85.01.0

MCOOA9

BJS-SBL3-0405

Soil

mg/Kg

4/7/2005

11:30

77.3

1.0

MERCURY

ftKJKEjBjj!)

POTASSIUM

mSILVER

Sample Number:

Sampling Location :

Matrix:

Units:

Date Sampled:

Time Sampled:

%Solids:

Dilution Factor:


To calculate sample quantitation limits: (CRQL * Dilution Factor) / (%Solids/100)

SEE NARRATIVE FOR CODE DEFINITIONS

Revised 09/99

117925

DATA SUMMARY FORM: INORGANIC Page 3 of 8 "' O '

Case #: 34031

Site:

Lab. :

SDG : MC0072


CHEM

Sample Number:

Sampling Location

Matrix:

Units:

Date Sampled:

Time Sampled :

%Solids :

Dilution Factor:



+ = Result reported from diluted analysis.


Revised 09/99

117926


Case #: 34031

Site:

Lab. :

SDG : MC0072BIG JOHN SALVAGE HOULT RD

CHEM

MC0089

BJS-SBH6-0405

Soil

mg/Kg

4/5/2005

10:00

85.4

1.0

MC0088BJS-SBH5-0405

Soil

mg/Kg4/5/2005

10:3588.3

1.0

MC0098

BJS-SBJ3-405

Soil

mg/Kg

4/7/2005

09:20

83.7

1.0/5.0

POTASSIUM

HPSILVER

Sample Number:

Sampling Location:

Matrix:

Units :

Date Sampled:

Time Sampled :

%Solids :

Dilution Factor:

CRQL - Contract Required Quantitation Limit

To calculate sample quantitation limits: (CRQL * Dilution Factor) / (%Solids/100)+ = Result reported from diluted analysis.


Revised 09/99

117927

DATA SUMMARY FORM: INORGANIC

OYV

Page 5 of 8

Case #:- 34031

Site:

Lab.:

SDG : MCOOH2


CHEM

Number of Soil Samples : 20

Number of Water Samples : 0

MCOOH2

SD-UT1-11-0405

Soil

mg/Kg

4/4/2005

13:55

45.3

1.0

MCOOH3

SD-UT1-10-0405

Soil

mg/Kg

4/4/2005

14:0076.71.0

Sample Number:

Sampling Location : Prefix : BJS-

Matrix :

Units:

Date Sampled:

Time Sampled :

%Solids:

Dilution Factor:

MCOOH4

SD-UT2-1-0405

Soil

mg/Kg

4/4/200512:2062.31.0

MCOOH5

SD-UT2-2-0405

Soil

mg/Kg

4/4/2005

10:5064.61.0

MCOOH6

SD-UT2-7-0405

Soil

mg/Kg

4/4/2005

11:45

67.5

1.0

MERCURY

POTASSIUM

SILVER



Prefix : All sample locations are prefixed BJS-


Revised 09/99

117928

DATA SUMMARY FORM: INORGANIC Page _6_ of _8_

Case #: 34031

Site :

Lab. :

SDG : MCOOH2


CHEM

MCOOH7

SD-UT2-8-0405

Soil .

mg/Kg

4/4/2005

12:45

75.3

1.0

MCOOH9

SD-UT1-12S-0405

Soil

mg/Kg

4/5/200509:30

45.5

1.0

MCOOJO

SD-UT1-13S-0405

Soil

mg/Kg

4/5/200512:1540.71.0

MCOOJ2

SD-UT1-12D-0405

Soil

mg/Kg

4/5/200509:35

71.4

1.0

MCOOJ1

SD-UT1-14S-0405

Soil

mg/Kg

4/5/200511:20

59.01.0

MERCURY

POTASSIUM

Sample Number:

Sampling Location : Prefix: BJS-

Matrix:

Units:

Date Sampled :

Time Sampled :

%Solids:

Dilution Factor:





Revised 09/99

117929

o-DATA SUMMARY FORM: INORGANIC Page 7 of 8

Case #: 34031

Site:

Lab.:

SDG : MCOOH2


CHEM

MCOOJ5

SD-UT1-15D-0405

Soil

mg/Kg

4/5/2005

12:1560.11.0

MCOOJ3

SD-UT1-13D-0405

Soil

mg/Kg

4/5/2005

12:20 .61.11.0

MCOOJ4

SD-UT1-14D-0405

Soil

mg/Kg4/5/200511:2563.41.0

MC0064

SBD3-0405

Soil '

mg/Kg

4/5/200511:45

87.91.0

MCOOJ6

SD-UT1-15S-0405

Soil

mg/Kg

4/5/200512:0050.81.0

MAGNESIUM

Sample Number:


Matrix:

Units:

Date Sampled:

Time Sampled :

%Solids:

Dilution Factor:


To calculate sample quantitation limits: (CRQL * Dilution Factor) / (%Solids/


100)


Revised 09/99

117930


Case ft 34031

Site:

Lab. :

SDG : MCOOH2


CHEM

MC0065

SBD4-0405

Soil

mg/Kg

4/4/2005

10:40

88.0

1.0

MC0067

SBD6-0405

Soil

mg/Kg4/4/2005

13:1583.8

1.0

MC0069

SBE3-0405

Soilmg/Kg4/4/2005

16:3589.1

1.0

MC0070

SBE4-0405

Soil

mg/Kg

4/4/2005

16:10

89.1

1.0

MC0071

SBE5-0405

Soil

mg/Kg

4/4/2005

12:30

87.3

1.0

BERYLLIUM

11111CALCIUM

Sample Number:


Matrix:

Units:

Date Sampled:

Time Sampled:

%Solids:

Dilution Factor

CRQL = Contract Required Quantitation LimitTo calculate sample quantitation limits: (CRQL * Dilution Factor) / (%Solids/100)



Revised 09/99

117931

'"V >•>'

Appendix C

Chain-of-Custody Records

117932

U.S EPA Region III Analytical Request FormRAS CASE #; CT3328 DAS #: NSF #:Date: 3/7/2P05 QAPP/SAP: YES Data Validation Level: M3 & IM2Site: BIG JOHN SALVAGE -Address: 900 HOULT RD ity: FAIRMONT State: WVLatitude: 39° 29' 54" Longitude:-80° 7'12"Program: SUPERFUND CERCLIS#: WVD054827944 Activity: Rl/FSAccount #: 05703^302002003 71 LAPP Operable Unit: Spill ID: 0358Preparer: KYLE SWARTZWELDER Phone: 3P2-738-7551 Fax: 3P2-454-5988 E-mail: [email protected]/RPM: CHRISTIAN MATTA Phone:215-814-2317 Fax:215-814-3002 E-mail: [email protected] Leader: TAD YANCHESKl Phone:302-738-7551 Fax: 3P2-454-5988 E-mai!: [email protected] CO: JIM CLARK Contract Type: RACS Prime: TT/BV Sub:Analytical TAT: 14 days Analytical + Validation TAT: 30 daysShip Date From: 4/3/05 Ship Date To: 4/15/05Samples Method Parameter Matrix

OLM04.3 TCL - SVOCS, PEST/PCBS ONLY SOIL132 ILM05.3 ICP-AES TAL+Hg+CN SOIL86 OLM04.3 L.IRKTV TCL SOIL123 OLM04.3 TCL AQ

123 /ILM05.3 ICP-AES TAL +HG+CN AQILM05.3 5 ICP -AES TAL +HG - I>M AQ_

14 OLC03.2 TCL AQ.14 ILM05.3 T)f*mcL ICP-MS TAL+HG+CN AQ.

ILMOiJ" ICP-AES TAL+HU+CN SEDIMEI'JTInstruction: See Big John Salvage - Hoult Road Site Final Ri/Fs Work Plan - February 2005, Section 4.4 (Identification Of Potential Sampling Approaches AndAppropriate Analytical Methods) For A Complete Listing Of All Proposed Analytical Methods.

Please Provide Electronic Data Deliverables For All Data

•o117933

c FP/, USEPA Contract Laboratory Program Case No: 34031 r-\Inorganic Traffic Report & Chain of Custody Record DAS No |"\

Region:

Project Code:

Account Code:

CERCLIS ID:

P

Site Name/State

Project Leader:

Action:

Sampling Co:

INORGANICSAMPLE No.

MC0078

MC0080

MC0085

MC0087

MC0088

MC0089

MC0091

3

T47121 01032005T03W302DD2C

WVD054827944

: Big JohnSalvage CLP 34031/WV

Tad YancheskiRemedial Investigation

V

Tetra Tech, Inc.

MATRIX/SAMPLER

SubsurfaceSoil/DouglasSeaveySubsurfaceSoil/DouglasSeaveySubsurfaceSoil/DouglasSeaveySubsurfaceSoil/DouglasSeaveySubsurfaceSoil/DouglasSeaveySubsurfaceSoil/DouglasSeaveySubsurfaceSoil/DouglasSeavey

CONC;TYPE

/G

/G

/G

/G

/G

/G

/G

ANALYSIS/TURNAROUND

CN(21). TM(21)

CN(21), TM(21)

TM(21)

CN(21), TM(21)

CN(21), TM(21)

CN(21), TM(21)

CN(21), TM(21)

Date Shipped: 4/6/2005 , Chain of Custody Record SamplerSignature:

Carrier Name: FerlFvAirbill: R4flQ fl7fU -Wi Relinquished By (Date / Time) Received By (Date / Time)

Shipped to: ChemTech Consulting 1Group (CHEM)110 Route 4 2

Englewood NJ 07631(201 ) 568-7400 3

4

TAG No./ STATION SAMPLE COILECT ORGANIC * QCPRESERVATIVE/ Bottles LOCATION . DATE/TIME SAMPLE No. TVPe

1436 (Ice Only), 1442 (Ice BJS-SBF7-0405 //S: 4/4/2005 15:45 C0078Only) (2)

1454 (Ice Only), 1460 (Ice BJS-SBG3-0405 Jj S: 4/5/2005 13:20 C0080Only) (2)

1499 (Ice Only) (1) BJS-SBH2-0405 // S: 4/5/2005 14:00 C0085

//151 7 (Ice Only). 1523 (Ice BJS-SBH4-0405'' 8:4/5/2005 11:15 C0087Only) (2)

1526 (Ice Only), 1532 (Ice BJS-SBH5-0405 // S: 4/5/2005 10:35 C0088Only) (2)

..

S: 4/5/2005 10:00 C0089Only) (2)

y'

S: 4/5/2005 14:40 C0091Only) (2)

Shipment for CaseComplete? N

Analysis Key:

CN = Cyanide, TM = CL

Sample(s) to be used for laboratory QC:

MC0064

Additional Sampler Signature(s):

Concentration: ,\_ = Low, M = Low/Medium, H = High Type/Designate: Composite = C, Grab = G

Chain of Custody Seal Number:

Shipment Iced?

H" 7AL lotal Metals

TR Number: 3-035066262-040605-0004PR provides preliminary results. Requests for preliminary results will increase analytical costs.Send Copy to: Sample Management Office, Attn: Heather Bauer, CSC, 15000 Conference Center Dr., Chantilly, VA 20151-3819; Phone 703/818-4200: Fax F2V5.1.047 Page 2'of 2"^

' '.. 'N>

"0>

117934

^ PDA USEPA Contract Laboratory ProgramInorganic Traffic Report & Chain of Custody Record

Region: 3

Project Code: T47121 Q103Account Code: 2005T03W302DD2C

CERCLIS ID: WVD054827944

Spill ID:

Site Name/State: Big John Salvage CLP 34031 /WV

Project Leader: Jad Yancheski

Action: Remedial Investigation** \Sampling Co: Tetra Tech, Inc.

INORGANIC MATRIX/ CONC/ ANALYSIS/SAMPLE No. SAMPLER TYPE TURNAROUND

MC0068 Subsurface /G CN (21), TM (21)Soil/DouglasSeavey

MC0073 Subsurface /G CN (21). TM (21)Soil/DouglasSeavey




MCOOA2 Subsurface /G CN (21), TM (21)Soil/DouglasSeavey


Date Shipped: 4/8/2005 Chain of Custody

Carrier Name: PoHFv

Airbill: (Uft? 77M nfifiO Relinquished By

Shipped to: ChemTech Consulting 1

Group (CHEM)110 Route 4 2Englewood NJ 07631(201)568-7400 3

4

Case No: 34031 [^DAS No: fX

Record SamplerSignature:

(Date / Time) Received By (Date / Time)

TAGNoJ , STATION SAMPLE COLLECT ORGANIC * QCPRESERVATIVE/ Bottles LOCATION DATE/TIME SAMPLE No. TyP6

1346 (Ice Only), 1352 (Ice BJS-SBE2-0405 /yS: 4/6/2005Only) (2)

1391 (Ice Only), 1397 (Ice BJS-SBF2-0405 S: 4/6/2005Only) (2)

//1445 (Ice Only), 1451 (Ice BJS-SBG2-0405 ^ S: 4/6/2005Only) (2)

.1616 (Ice Only). 1622 (Ice BJS-SBJ3-405 /J S: 4/7/2005Only) (2)

/,1625 (Ice Only), 1631 (Ice BJS-SBJ4-405 /J 5:4/7/2005Only) (2)

1652 (Ice Only), 1658 (Ice BJS-SBK2-0405// 5:4/6/2005Only) (2)

/1661 (Ice Only), 1667 (Ice BJS-SBK3-0405 // S: 4/7/2005Only) (2)

8:20 C0068 MS/MSD

8:55 C0073 MS/MSD/

11:18 C0079

9:20 C0098

8:55 C0099

14:30 COOA2

8:20 COOA3


Analysis Key:



MC0068, MC0073


Concentration: |_ = Low. M = Low/Medium, H = High Type/Designate: Composite = C, Grab = G


Shipment Iced?

P TAL 1 otal Metals

TR Number: 3-035066262-040805-0001PR provides preliminary results. Requests for preliminary results will increase analytical costs.Send Copy to: Sample Management Office. Artn: Heather Bauer, CSC, 15000 Conference Center Dr.. Chantilly, VA 20151-3819; Phone 703/818-4200; Fax

"v"' " '';v'" ''"" " ^ JF2V5.1.047 page 1|of--3 J"

117935

^ypPA USEPA Contract Laboratory Program Case NO:Inorganic Traffic Report & Chain of Custody Record DAS No:

Region: 3

Project Code: T47121 0103

Account Code: 2005T03W302DD2C


Spill ID:

Site Name/State: Big John Salvage CLP 34031/WV

Project Leader: jad Yancheski

Action: Remedial Investigation

Sampling Co: Tetra Tech, Inc.

INORGANIC MATRIX/ CONC/ ANALYSIS/SAMPLE No. SAMPLER TYPE TURNAROUND





MCOOB3 Subsurface /G CN (21 ), TM (21 )Soil/DouglasSeavey

MCOOB5 Subsurface /G CN (21), TM (21)Soil/DouglasSeavey

MCOOB6 Subsurface /G CN (21). TM (21)Soil/DouglasSeavey

Date Shipped: 4/8/2005 Chain of Custody RecordCarrier Name: FeriFxAirbill: fi4fl?77R3nfifiO Relinquished By (Date /Time)

Shipped to: ChemTech Consulting 1Group (CHEM)110 Route 4 2

Englewood NJ 07631(201 ) 568-7400 3

4

TAG No./ STATION SAMPLE COILECT

34031 p

rvSamplerSignature:

Received By (Date / Time)

ORGANIC l QCPRESERVATIVE Bottles LOCATION DATE/TIME SAMPLE No. Type

1670 (Ice Only), 1676 (Ice BJS-SBK4-0405// S: 4/7/2005 9:55 COOA4Only) (2)

,1697 (Ice Only), 1703 (Ice BJS-SBL1 -0405 '* S: 4/6/2005 12:48 COOA7Only) (2)

i /uojice umyj, mz(ice UJS-SULZ-IMUO 8:4/7/2005 12:25 COOA8Only) (2)

/171 5 (Ice Only), 1721 (Ice BJS-SBL3-0405 • S: 4/7/2005 11:30 COOA9Only) (2)

1751 (Ice Only), 1757 (Ice BJS-SBM1-0405,//S: 4/6/2005 12:38 COOB3Only) (2)

1769 (Ice Only), 1775 (Ice BJS-SBM3-0405 // S: 4/7/2005 13:20 COOB5Only) (2) "

1778 (Ice Only), 1784 (Ice BJS-SBM4-0405 5:4/7/2005 14:30 COOB6Only) (2)


Analysis Key:



MC0068, MC0073


Concentration: L = Low. M = Low/Medium, H = High Type/Designate: Composite = C. Grab = G


Shipment Iced?

P TAL 1 otai Metals

TR Number: 3-035066262-040805-0001PR provides preliminary results. Requests for preliminary results will increase analytical costs.Send Copy to: Sample Management Office. Attn: Heather Bauer, CSC, 15000 Conference Center Dr., Chantilly. VA 20151-3819; Phone 703/818-4200; Fax

• -oF2V5.1.047 PageZ:of-3V

117936

&EPA USEPA Contract Laboratory Program^ Inorganic Traffic Report & Chain of Custody Record

Region: 3

Project Code: T47121 0103



Spill ID.

Site Name/State: Big John Salvage CLP 34031/WV

Project Leader: jad Yancheski

Action: Remedial InvestigationV


INORGANIC MATRIX/ CONG/ ANALYSIS/SAMPLE No. SAMPLER TYPE TURNAROUND

MC0064 Subsurface IG CN (21), TM (21)Soil/DouglasSeavey


MC0067 Subsurface IG CN (21), TM (21)Soil/DouglasSeavey


MC0070 Subsurface /G CN (21). TM (21)Soil/DouglasSeavey


MC0072 Subsurface IG CN (21), TM (21)Soil/ .DouglasSeavey

Date Shipped: 4/6/2005 Chain Of Custody

Carrier Name: FprIFy

Airbill: S48C.87rUW.-W Relinquished By

Shipped to: ChemTech Consulting 1

Group (CHEM)110 Route 4 2

tngiewooo NJ u/bol(201)568-7400 3_

4

Case No: 34031 F}DAS No: IX

Record SamplerSignature:

(Date / Time) Received By (Date / Time)

TAG No./ STATION SAMPLE COLLECT ORGANIC l " QCPRESERVATIVE/ Bottles LOCATION DATE/TIME SAMPLE No. Type

1310 (Ice Only), 1316 (Ice BJS-SBD3-0405 </ S: 4/5/2005Only) (2)

1 31 9 (Ice Only), 1 325 (Ice B JS-SBD4-0405 ^ S: 4/4/2005Only) (2)

1337 (Ice Only), 1343 (Ice BJS-SBD6-0405 ,/ 5:4/4/2005Only) (2) .

1355 (Ice Only), 1361 (Ice BJS-SBE3-0405 / 3:4/4/2005 ,Only) (2)

1364 (Ice Only), 1370 (Ice BJS-SBE4-0405 S S: 4/4/2005Only) (2)

1373 (Ice Only), 1379 (Ice BJS-SBE5-0405 / S: 4/4/2005Only) (2)

/,1382 (Ice Only), 1388 (Ice BJS-SBE6-0405 //fe: 4/4/2005Only) (2)

11:45 C0064 MS/MSD

10:40 C0065

13:15 C0067

16:35 C0069

16:10 C0070

12:30 C0071

14:40 C0072


Analysis Key:



MC0064


Concentration: \_ = Low. M = Low/Medium. H = High Type/Designate: Composite = C. Grab = G


Shipment Iced?

H I AL 1 otal Metals

TR Number: 3-035066262-040605-0004PR provides preliminary results. Requests for preliminary results will increase analytical costs.Send Copy to: Sample Management Office, Attn: Heather Bauer. CSC, 15000 Conference Center Dr., Chantilly. VA 20151-3819; Phone 703/818-4200; Fax F2V5.1.047 Page 1> of 2J

117937

£*CZDA USEPA Contract Laboratory Program^ Inorganic Traffic Report & Chain of Custody Record

Region:

Project Code:

Account Code:

CERCLIS ID:

Spill ID:

3

T47121 01032005T03W302DD2C

WVD054827944

Site Name/State: Big John

Project Leader:

Action:

Sampling Co:

INORGANICSAMPLE No.

MCOOH2

MCOOH3

MCOOH4

MCOOH5

MCOOH6

MCOOH7

MCOOH9

MCOOJO

MCOOJ1

MCOOJ2

Salvage SD Organics/Metals/WV

Tad YancheskiRemedial Investiaation

V

Tetra Tech, Inc.

MATRIX/SAMPLER

Sediment/Vadim Petrov

Sediment/DennisAndersonSediment/DennisAndersonSediment/DennisAndersonSediment/Vadim Petrov






CONC/TYPE

/G

/G

/G

/G

/G

/G

/G.

/G

/G

/G

CN

CN

ANALYSIS/TURNAROUND

(21),TM(21)

(21),TM(21)

CN(21), TM(21)

CN

CN

CN

CN

CN

CN

CN

(21), TM(21)

(21), TM(21)

(21), TM(21)

(21), TM(21)

(21), TM(21)

(21), TM(21)

(21), TM(21)

Date Shipped:

Carrier Name:

Airbill:

Shipped to:

4/6/2005

FedEx

8489 8704 5498

ChemTechGroup (CH

ConsultingEM)

110 Route 4C nnlfiiiirmr4 Kl 1 A7CQHbngiewood NJ U7ool(201)568-7400

Case No: 34031 [^

DAS No: "X

Chain of Custody Record SamplerSignature:

Relinquished By (Date / Time) Received By (Date / Time)

1

2

3

TAG No./PRESERVATIVE Bottles

2378 (Ice Only), 2381 (IceOnly) (2)

2374 (Ice Only),Only) (2)









2377 (Ice

2385 (Ice

2389 (Ice

2393 (Ice

2397 (Ice

2404 (Ice

2411 (Ice

2418 (Ice

2475 (Ice

•t

4

STATION SAMPLE COLLECT ORGANIC * QCLOCATION DATE/TIME SAMPLE No. Type

BJS-SD-UT1-11-0405/S: 4/4/2005 13:55 COOH2

BJS-SD-UT1-10-0405yS: 4/4/2005 14:00 COOH3

BJS-SD-UT2-1-0405 /S: 4/4/2005 12:20 COOH4

BJS-SD-UT2-2-0405 ' S: 4/4/2005 10:50 COOH5

BJS-SD-UT2-7-0405/S: 4/4/2005 11:45 COOH6

BJS-SD-UT2-8-0405y S: 4/4/2005 12:45 COOH7

BJS-SD-UT1-12S-0405 £: 4/5/2005 9.30 COOH9t-

BJS-SD-UT1-13S-0405/S: 4/5/2005 12:15 COOJO

BJS-SD-UT1-14S-0405/S: 4/5/2005 11:20 COOJ1

BJS-SD-UT1-12D-0405 4 4/5/2005 9:35 COOJ2


Analysis Key:


Sample(s) to be used for laboratory QC: Additional Sampler Signature(s):

Concentration: L = Low, M = Low/Medium. H = High Type/Designate: Composite = C. Grab = G


Shipment Iced?

P T AL Total Metals

TR Number: 3-035066262-040605-0003PR provides preliminary results. Requests for preliminary results will increase analytical costs.Send Copy to: Sample Management Office, Attn: Heather Bauer, CSC, 15000 Conference Center Dr., Chantilly, VA 20151-3819; Phone 703/818-4200; Fax F2V5.1.047 Rage 1| of 2

'117938

SEPA USEPA Contract Laboratory Program Case No: 34031 QInorga nic Traffic Report & Chain of Custody Record DAS NO: rV

Region: 3

Project Code: T47121.0103



Spill ID:

Site Name/State: Big John Salvage SD Organics/Metals/WV

Project Leader: Tad Yancheski

Action: Remedial Investigation


INORGANIC MATRIX/ CONC/SAMPLE No. SAMPLER TYPE

MCOOJ3 Sediment/ /GVadim Petrov

MCOOJ4 Sediment/ /GVadim Petrov

MCQOJ5 Sediment/ /GDennisAnderson

MCOOJ6 Sediment/ /GDennisAnderson

Date Shipped: 4/6/2005

Carrier Name: FedEx

Airbill: 8489 8704 5498

Shipped to: ChemTech ConsultingGroup (CHEM)110 Route 4Englewood NJ 07631(201)568-7400

Chain of Custody Record

Relinquished By (Date / Time)

1

2

3

4

SamplerSignature:

Received By (Date / Time)

ANALYSIS/ TAG NoV STATION SAMPLE COILECT ORGANIC l QCTUWJAROUND PRESERVATIVE/ Bottles LOCATION ' OA1E/TIME SAMPLE No. Type

CM (21), TM(21) 2479 (Ice Only), 2485 (Ice BJS-SD-UT1-13D-0405/S: 4/5/2005 12:20 COOJ3Only) (2)

CN(21), TM(21) 2489 (Ice Only), 2495 (Ice BJS-SD-UT1-14D-0405/S: 4/5/2005 11:25 COOJ4Only) (2)

CN(21), TM(21) 2499 (Ice Only), 2505 (Ice BJS-SD-UT1-15D-0405/S: 4/5/2005 12:15 COOJ5Only) (2) ,. .

CN(21), TM(21) 2508 (Ice Only), 2514 (Ice BJS-SD-UT1-15S-0405,S: 4/5/2005 12:00 COOJ6Only) (2)


Analysis Key:


Sample(s) to be used for laboratory QC: Additional Sampler Signature(s):

Concentration: L = Low, M = Low/Medium, H = High Type/Designate: Composite = C, Grab = G


Shipment Iced?

P I AL I otal Metals

TR Number: 3-035066262-040605-0003PR provides preliminary results. Requests for preliminary results will increase analytical costs.Send Copy to: Sample Management Office. Attn: Heather Bauer. CSC, 15000 Conference Center Dr., Chantilly, VA 20151-3819; Phone 703/818-4200; Fax F2V5.1.047 Page

117939

Appendix D

Laboratory Case Narrative

117940

USEPA - CLP

COVER PAGE

Lab Name CHEMTECH CONSULTING GROUP Contract: 68-WO-2068

Lab Code: CHEM Case No.: 34031 NRASNo.:

SOW No.: ILM05.3

EPA Sample No.

MC0068MC0068DMC0068SMC0072MC0078MC0079MC0080MC0085MC0087MC0088MC0089MC0091MC0098MC0099MCOOA2-MCOOA3MCOOA4MCOOA7MCOOA8MCOOA9MCOOB3MCOOB5

SDGNo.: MC0072

Lab Sample ID

T2230-09T2230-10T2230-11T2230-01T2230-02T2230-12T2230-03T2230-04T2230-05T2230-06T223Q-07T2230-08T2230-13T2230-14T2230-15T2230-16T2230-17T2230-18T2230-19T2230-20T2230-21T2230-22

Were ICP-AES and ICP-MS interelement corrections applied?

Were ICP-AES and ICP-MS background corrections applied?If yes, were raw data generated beforeapplication of background corrections?

Comments:

(Yes/No)

(Yes/No)

(Yes/No)

ICP-AES

YES

YES

NO

ICP-MS

I certify that this data package is in compliance with the terms and conditions of the contract, both technically and forcompleteness, for other than the conditions detailed above. Release of the data contained in this hardcopy data packageand in the computer-readable data submitted on diskette (or via an alternate means of electronic transmission, if approvedin advance by USEPA) has been authorized by the Laboratory Manager or the Manager's designee, as verified by thefollowing signature-

Signature;

Date:

Name: PAR VEEN HASAN

Title: EPA OA/OC OFFICER

COVER PAGE ILM05.3

117941

•$'

CHEMTECH284 Sheffield StreetMountainside, NJ 07092

SDG NARRATIVE

USEPASDG # MC0072CASE #34031CONTRACT # 68-WO-2068LAB NAME: CHEMTECH CONSULTING GROUPLAB CODE: CHEMCHEMTECH PROJECT #T2230

A. Number of Samples and Date of Receipt

20 Soil Samples were delivered to the laboratory intact on 04/07/05 and 04/09/05.

B. Parameters

Test requested for Total Metals and Cyanide,

C. Cooler Temp

Indicator Bottle: Presence/AbsenceCooler: ,4°C

D. Detail Documentation (related to Sample HandlingShipping, Analytical Problem, Temp of Cooler etc):

Issue: The TR did not designate samples for laboratory QC for a few SDGs. The lab would liketo choose samples MC0141, MCOOA1, and MC0180 for this purpose.

Issue: The lab indicated that each sample received for Case 34031 consisted of 2 soil jars (1Metals, 1 Cyanide), however sample MC0085 was only sent with one Metal jar. The lab wouldlike to know if they should use the Metals jar for sample MC0085 to analyze for Metals andCyanide.

Also,

Samples shipped to the incorrect laboratoryIssue 1: The lab received organic samples along with their inorganic shipment. The lab receivedsamples C0068-COOC1 (on 2 TR's). Please provide an address and billing information if thesamples should be trans-shipped.

Incorrect/duplicated sample numbersIssue 2: Sample MC0125 (station location: BJS-SDMON2C3-0405) was listed on the TR asC0125.

117942

O-


Discrepancies with tags, jars, and/or TR/COCIssue 3: All of the inorganic samples were listed on the TR/COC for DM and TM, however theseare all soil samples. The sample IDs affected are MC0117, MC0118, MC0119, MC0120,MC0121, MC0122, MC0123, MC0125, MC0126, MC0217, and MC0218.

E. Corrective Action taken for above:

Following is the resolution to the issue below:Issue: The TR did not designate samples for laboratory QC for a few SDGs. The lab would liketo choose samples MC0141, MCOOA1, and MC0180 for this purpose.Resolution: In accordance with previous direction from Region 3, for both Inorganic and OrganicMulti-Media samples, the laboratory will select a sample for laboratory QC as long as the sampleis not a PE, blank, or rinsate sample. The laboratory will note the issue in the Case/SDGNarrative, notify the SMO coordinator of the sample selected for laboratory QC, and proceedwith the analysis of the samples.SMO will note that the lab chose samples MC0141, MCOOA1, and MC0180 for laboratory QC.Please indicate which SDG each of these'samples is assigned to for laboratory QC.

Following is the resolution to the issue below:Issue: The lab indicated that each sample received for Case 34031 consisted of 2 soil jars (1Metals, 1 Cyanide), however sample MC0085 was only sent with one Metal jar. The lab wouldlike to know if they should use the Metals jar for sample MC0085 to analyze for Metals andCyanide.Resolution: Per Region 3, it is acceptable for the lab to analyze for Metals and Cyanide from theMetal jar for sample MC0085.

Also,

Following is an update to the Record of Communication of Case 34031. For issue 3, the sampleIDs affected are now listed.Samples shipped to the incorrect laboratoryIssue 1: The lab received organic samples along with their inorganic shipment. The lab receivedsamples C0068-COOC1 (oh 2 TR's). Please provide an address and billing information if thesamples should be trans-shipped.Resolution 1: Per Region 3, the Tetra Tech air bill voucher number for the organic samplesmistakenly sent to CHEM that require transshipment is: 0191-2082-1. The samples should besent to the following address:Liberty Analytical501 Madison Ave.Gary, NC 27513919-379-4081

117943


Incorrect/duplicated sample numbersIssue 2: Sample MC0125 (station location: BJS-SDMON2C3-0405) was listed on the TR asC0125.Resolution 2: Per Region 3, the laboratory should report sample C0125 under the new sample IDMC1AP2, note the situation in the Case/SDG Narrative, and proceed with the analysis of thesamples.Discrepancies with tags, jars, and/or TR/COCIssue 3: All of the inorganic samples were listed on the TR/COC for DM and TM, however theseare all soil samples. The sample IDs affected are MC0117, MC0118, MC0119, MC0120,MC0121, MC0122, MC0123, MC0125, MC0126, MC0217, and MC0218.Resolution 3: Per Region 3, the lab should only analyze the soil samples for total metals analysisand disregard the dissolved metals analysis. Please note this situation in the Case/SDG Narrativeand proceed with the analysis of the samples.

F. Analytical Techniques:

All analyses were based on CLP Methodology by method ILM05.3

G. Calculation:

Conversion of results from mg/L to mg/kg (Dry Weight Basis):

Mg/Kg = (Result in mg/L) X 1000 X 1OO/ % Solid X Fraction of Sample Amount Taken in Prep.

G. QA/ QC

Calibrations met requirements. Interference check met requirements. Blank analyses did not indicateany presence of contamination. Laboratory Control sample was within control limits. Spike sample didmet requirements except for Aluminum and Antimony. Duplicate sample did met requirements except forthe Copper. Serial Dilution did met requirements except for Few Elements.

•

I certify that the data package is in compliance with the terms and conditions of the contract bothtechnically and for completeness, for other than the conditions detailed above. Release of the datacontained in this hard copy data package has been authorized by the Laboratory Director or his designee,as verified by the following signature.

Name: Parveen Hasan

Title: EPA QA/QC OFFICER

117944

USEPA - CLP

COVER PAGE

Lab Name CHEMTECH CONSULTING GROUP Contract: 68-WO-2068

Lab Code: CHEM — Case No.: 34031 NRAS No.:

SOW No.: ILM05.3

EPA Sample No.

MC0064MC0064DMC0064SMC0065MC0067MC0069MC0070MC0071MCOOH2MCOOH3MCOOH4MCOOH5MCOOH6MCOOH7MCOOH9MCOOJOMCOOJ1MCOOJ2MCOOJ3MCOOJ4MCOOJ5MCOOJ6

SDGNo.: MCOOH2

Lab Sample ID

T2227-15T2227-16T2227-17T2227-18T2227-19T2227-20T2227-21T2227-22T2227-01T2227-02T2227-03T2227-04T2227-05T2227-06T2227-07T2227-08T2227-09T2227-10T2227-11T2227-12T2227-13T2227-14

Were ICP-AES and ICP-MS interelement corrections applied?

Were ICP-AES and ICP-MS background corrections applied?

If yes, were raw data generated beforeapplication of background corrections?

Comments:

(Yes/No)

(Yes/No)

(Yes/No)

ICP-AES

YES

YES

NO

ICP-MS

I certify that this data package is in compliance with the terms and conditions of the contract, both technically and forcompleteness, for other than the conditions detailed above. Release of the data contained in this hardcopy data packageand in the computer-readable data submitted on diskette (or via an alternate means of electronic transmission, if approvedin advance_by USEPA) has been authorized by the Laboratory Manager or the Manager's designee, as verified by thefollowing signature.

Signature:

Date:

Name: PAR VEEN HASAN

Title: EPA OA/OC OFFICER

COVER PAGE ILM05.3 3117945


SDG NARRATIVE

USEPASDG # MCOOH2CASE #34031CONTRACT # 68-WO-2068LAB NAME: CHEMTECH CONSULTING GROUPLAB CODE: CHEMCHEMTECH PROJECT #12221

A. Number of Samples and Date of Receipt

20 Soil Samples were delivered to the laboratory intact on 04/07/05.

B. Parameters

Test requested for Total Metals and Cyanide.

C. Cooler Temp

Indicator Bottle: Presence/AbsenceCooler: 4°C

D. Detail Documentation (related to Sample HandlingShipping, Analytical Problem, Temp of Cooler etc):

Issue: The TR did not designate samples for laboratory QC for a few SDGs. The lab would liketo choose samples MC0141, MCOOA1, and MC0180 for this purpose.

Issue: The lab indicated that each sample received for Case 34031 consisted of 2 soil jars (1Metals, 1 Cyanide), however sample MC0085 was only sent with one Metal jar. The lab wouldlike to know if they should use the Metals jar for sample MC0085 to analyze for Metals andCyanide.

Also,

Samples shipped to the incorrect laboratoryIssue 1: The lab received organic samples along with their inorganic shipment. The lab receivedsamples C0068-COOC1 (on 2 TR's). Please provide an address and billing information if thesamples should be trans-shipped.

Incorrect/duplicated sample numbersIssue 2: Sample MC0125 (station location: BJS-SDMON2C3-0405) was listed on the TR asC0125.

117946


Discrepancies with tags, jars, and/or TR/COCIssue 3: All of the inorganic samples were listed on the TR/COC for DM and TM, however theseare all soil samples. The sample IDs affected are MC0117, MC0118, MC0119, MC0120,MC0121, MC0122, MC0123, MC0125, MC0126, MC0217, and MC0218.

E. Corrective Action taken for above:

Following is the resolution to the issue below:Issue: The TR did not designate samples for laboratory QC for a few SDGs. The lab would liketo choose samples MCO141, MCOOA1, and MCO180 for this purpose.Resolution: In accordance with previous direction from Region 3, for both Inorganic and OrganicMulti-Media samples, the laboratory will select a sample for laboratory QC as long as the sampleis not a PE, blank, or rinsate sample. The laboratory will note the issue in the Case/SDGNarrative, notify the SMO coordinator of the sample selected for laboratory QC, and proceedwith the analysis of the samples.SMO will note that the lab chose samples MC0141, MCOOA 1, and MCO 180 for laboratory QC.Please indicate which SDG each of these samples is assigned to for laboratory QC.

/"•

Following is the resolution to the issue below:Issue: The lab indicated that each sample received for Case 34031 consisted of 2 soil jars (1Metals, 1 Cyanide), however sample MC0085 was only sent with one Metal jar. The lab wouldlike to know if they should use the Metals jar for sample MC0085 to analyze for Metals andCyanide.Resolution: Per Region 3, it is acceptable for the lab to analyze for Metals and Cyanide from theMetal jar for sample MC0085.

Also,

Following is an update to the Record of Communication of Case 34031. For issue 3, the sampleIDs affected are now listed.Samples shipped to the incorrect laboratoryIssue 1: The lab received organic samples along with their inorganic shipment. The lab receivedsamples C0068-COOC1 (on 2 TR's). Please provide an address and billing information if thesamples should be trans-shipped.Resolution 1: Per Region 3, the Tetra Tech air bill voucher number for the organic samplesmistakenly sent to CHEM that require transshipment is: 0191-2082-1. The samples should besent to the following address:Liberty Analytical501 Madison Ave.Gary, NC 27513919-379-4081

5117947


Incorrect/duplicated sample numbersIssue 2: Sample MC0125 (station location: BJS-SDMON2C3-0405) was listed on the TR asC0125.Resolution 2: Per Region 3, the laboratory should report sample CO 125 under the new sample IDMC1AP2, note the situation in the Case/SDG Narrative, and proceed with the analysis of thesamples.Discrepancies with tags, jars, and/or TR/COCIssue 3: All of the inorganic samples were listed on the TR/COC for DM and TM, however theseare all soil samples. The sample IDs affected are MC0117, MC0118, MC0119, MC0120,MC0121, MC0122, MC0123, MC0125, MC0126, MC0217, and MC0218.Resolution 3: Per Region 3, the lab should only analyze the soil samples for total metals analysisand disregard the dissolved metals analysis. Please note this situation in the Case/SDG Narrativeand proceed with the analysis of the samples.

F. Analytical Techniques: I

All analyses were based on CLP Methodology by method ELM05.3

G. Calculation:

Conversion of results from mg/L to rag/kg (Dry Weight Basis):

Mg/Kg = (Result in mg/L) X 1000 X 100/ % Solid X Fraction of Sample Amount Taken in Prep.

G. QA/ QC

Calibrations met requirements. Interference check met requirements. Blank analyses did not indicateany presence of contamination. Laboratory Control sample was within control limits. Spike sample didmet requirements except for the Antimony. Duplicate sample did met requirements except for FewElelemts. Serial Dilution did met requirements.

I certify that the data package is in compliance with the terms and conditions of the contract bothtechnically and for completeness, for other than the conditions detailed above. Release of the datacontained in this hard copy data package has been authorized by the Laboratory Director or his designee,as verified by the following signature.

Name: Parveen Hasan

Title: EPA QA/QC OFFICER

6117948

Message ' Page 1 of i

Parveen Hasan

From: Benhoff, totrchael [[email protected]]

Sent: Wednesday, April 13, 2005 11:33 AM

To: Divya Mehta (E-mail); Parveen Hasan (E-mail)

Cc: Betty Jeffery (E-mail); Dan Slizys (E-mail); John Kwedar (E-mail); Khin-Cho Thaung (E-mail)

Subject: Region 03 | Case 34031 | Lab CHEM | Issue Discrepancies with tags , jars, and/or TR/COC | FINAL

Hi Parveen:

Following is the resolution to the issue below:

Issue: The Scheduling Notification indicated the sample TAT as 14 day, however the TR listed the TAT as21 day.

Resolution: In accordance with previous direction from Region 3, the laboratory, will proceed with theturnaround time indicated on the Scheduling Notification Form, note the issue in the Case/SDG Narrative,and proceed with the analysis of the samples.

thanks,Mike '

Michael BenhoffComputer Sciences CorporationCLP Coordinator for Regions 1,2, and [email protected]: (703) 818-4357; Fax: (703)818-4602

•Tliis is a PRIVATE message. If you are not the intended recipient, please delete without copying and kindly advise us by e-mail ofthe mistake in delivery. NOTE: Regardless of coatent, this e-mail shall not operate to bind CSC to any order or other contractunless pursuant to explicit written agreement or government initiative expressly permitting the use of e-mail for such purpose.

Original Message—-^-From: Parveen Hasan [mailto:[email protected]]Sent: Wednesday, April 13, 2005 12:16 PMTo: 'Benhoff, Michael1

Subject: Region 03 | Case 34031 | Lab CHEM | Issue Insufficient/inappropri ate ate designation of laboratory QC

Mike,

The TA is 21 Days oh TR, but per Schedule Notification, its 14 Days. Lab wants to know what is the Correct TA?

ThanksParveen HasanCHEMTECH284 Sheffield StreetMountainside, NJ 07092(908) 789-8900 Ext. 210www.chemtech.net

3064/13/2005

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Message ' . --Page-2 of 3

Resolution 1: Per Region 3, the Tetra Tech air bill voucher number for the organic samples mistakenlysent to CHEM that require transshipment is: 0191-2082-1. The samples should be sent to the followingaddress: ' _

Liberty Analytical . ' •501 Madison Ave.Gary, NC 27513919-379-4081

Incorrect/duplicated sample numbersIssue 2: Sample MC0125 (station location: BJS-SDMQN2C3.-0405) was listed on the TR as C0125.Resolution 2: Per Region 3, the laboratory should report sample C0125 under the new sample ED

• MCI AP2, note the situation in the Case/SDG Narrative, and proceed with the analysis of the samples.

Discrepancies with tags, jars, and/or TR/COCIssue 3: All of the inorganic samples were listed on the TR/COC for DM and TM, however these areall soil samples.Resolution 3: Per Region 3, the lab should only analyze the soil samples for total metals analysisand disregard the dissolved metals analysis. Please note this situation in the Case/SDG Narrative andproceed with the analysis of the samples.

Please let Mike or me know if you have any questions or problems.


Original MessageFrom: [email protected]

. Sent: Tuesday, April 12,2005 6:44 AM " •To: Benhoff, MichaelCc: [email protected]; [email protected]_gov; [email protected]: Re: NEW ISSUE - Region 3 | Case 34031 | Lab CHEM | Issue Multiple

Mike, '*

Issue 1: SMO can provide trans-shipment information to the lab.Issue 2: No, SMO should not ask the lab to change CO 125 to MC0125. A memo to file from fieldpersonnel will clarify this issue. The lab will use CO 125 as sample ED when reporting results or SMOcan provide a new CLP sample ED number.Issue 3: Yes, the lab should only analyze for total metals. Disregard the dissolved metals analysis.

Original MessageFrom: Benhoff, MichaelSent: Monday, April 11, 2005 3:58 PMTo: Betty Jeffery (E-mail); Dan Slizy's (E-mail); John Kwedar (E-mail); Khin-Cho Thaung (E-mail)

. Subject: NEW ISSUE - Region 3 | Case 34031 | Lab CHEM | Issue Multiple.

This is Carolyn Mack - Mike is out of the office today.

3074/13/2005 117950

Message ..--Page-3 of 5

SMO received trans-shipment information for issue 1 from the sampler, however the sampler indicatedthat the other two issues would be resolved at a later date.

• Issue 1) Is it acceptable for SMO to send on the trans-shipment information?• Issue 2) Should SMO direct the inorganic laboratory to report sample C0125 as MC0125?• Issue 3) Should the laboratory only analyze the soil samples that were listed for TM and DM for

TM analysis (i.e., DM analysis is cancelled)?

Issue 1: The lab received organic samples along with their inorganic shipment. The lab receivedsamples C0068-COOC1 (on 2 TR's). Please provide an address and billing information if the samplesshould be trans-shipped.Resolution 1: Per Region 3, the Tetra Tech air bill voucher number for the organic samples mistakenly sent to CHEMthat require transshipment is: 0191-2082-1. The samples should be sent to the following address:

Liberty Analytical501 Madison Ave.Gary, NC 27513919-379-4081

Issue 2: Sample MCO125 (station location: BJS-SDMON2C3-0405) was listed on the TR as C0125.

Issue 3: All of the inorganic samples were listed on the TR for DM and TM, however these are all soilsamples.

Michael BenhoffComputer Sciences CorporationCLP Coordinator for Regions 1,2, and 3 •[email protected] • ~"Phone: (703) 818^357; Fax: (703)818-4602

e

Original Message—From: Parveen HasanSent: Monday, April 11, 2005 12:17 PMTo: 'Mack, Carolyn1

Subject: FW: Region 03 | >Case"34031 ,| Lab CHEM | Issue Multiple

Carol, .

Lab is waiting for the Resolution.

• ThanksParveen HasanCHEMTECH284 Sheffield Street • 'Mountainside, NJ 07092(908) 789-8900 Ext. 210www.chemtech.net

Original MessageFrom: Yancheski, Tad -- Tt, Inc. [mailto:[email protected]]Sent: Monday, April 11, 2005 10:38 AMTo: '[email protected] '; 'Benhoff, Michael'; Swartzwelder, Kyle --Tt, Inc.; Yancheski, Tad - Tt, Inc.Cc: '[email protected] '; '[email protected] '; '[email protected] '

308117951

Message . ..--Pase-4 of 5

. Subject: RE: NEW ISSUE | Case 34031 | Lab CHEM | Issue Multiple - Trans Sh ip Information

HiDan- _

The Tetra Tech air bill voucher number for the organic samples mistakenly sent to CHEM that require transshipment is:

0191-2082-1

Liberty Analytical.501 Madison Ave.Gary, NC 27513919-379-4081

Memo's to file will be prepared for the other issues at a later date.

Please advise if you have any questions.

Regards, <•t

Tad YancheskiTetra Tech

. 302-738-7551 ;

Original MessageFrom: [email protected]: Monday, April 11, 2005 9:46 AMTo: Benhoff, Michael; [email protected]: [email protected]: [email protected]; [email protected]: [email protected]: Re: NEW ISSUE | Case 34031 | Lab CHEM | Issue Multiple

Mike, '

The field pe-sonnel will be contacted. The lab should proceed with the analysis of samples anddocument all issues in the case narrative. Kyle and Tad, .

There are more issues which need your attention:Issue 1: The lab received organic samples that may have to be trans-shipped. We will need air billvoucher.Issue 2: MC0125 listed on the TR/COC as sample CO 125. Need a memo to file for clarification.IssueS: Soil samples on the TR/COC are listed as for total and dissolved metals analysis. Need a memoto file for clarification.

Original Message—From: Benhoff, Michael • 'Sent: Friday, April 08, 2005 4:45 PM •To: Betty Jeffery (E-mail); Dan Slizys (E-mail); John Kwedar (E-mail); Khin-Cho Thaung (E-mail)

. Subject: NEW ISSUE | Case 34031 | Lab CHEM | Issue Multiple •Dan:. •

Please advise on the following issues:

Issue 1: The lab received organic samples along with their inorganic shipment. The lab received

3094/13/2005 117952

Message . • .--"Page"5 or 5

samples C0068-COOC1 (on 2 TR's). Please provide an address and billing information if the samplesshould be trans-shipped.

. Issue 2: Sample MC0125 (station location: BJS-SDMON2C3-0405) was'listed on the TR as C0125.


thanks,Mike

Michael BenhoffComputer Sciences CorporationCLP Coordinator for Regions 1,2, and [email protected]: (703) 818-4357; Fax: (703)8.18-4602

This is a PRIVATE message. If you are not the intended recipient, please delete without copying and kindly advise iis by e-mail of the mistake in delivery. NOTE: Regardless of content, this e-mail shall not operate to bind CSC to any order orother contract unless pursuant'to explicit written agreement or government initiative expressly permitting the use of e-mailfor such purpose. (

Original Message—From: Parveen Hasan [mailto:[email protected]]Sent: Friday, April 08, 2005 4:30 PMTo: 'Benhoff, Michael1

Subject: Region 03 | Case 340311 Lab CHEM | Issue. Multiple

Mike,

The Following samples Lab found for Case# 34031:

lssue#1: Lab Received Organic samples along w/ Inorganic samples. .

lssue#2: Incomplete sample ID on TR as C0125 (for Station Location: BJS-SDMON2C3-0405)

lssue#3: Same sample ID reported on TR for TM and DM for all samples (w/ total number of bottles 3).Also, all these samples are Soil Samples!!! -

Thanks . . .Parveen HasanCHEMTECH284 Sheffield Street - 'Mountainside.'NJ 07092(908) 789-8900 Ext. 210www.chemtech.net

3104/13/2005 • ' 117953

Parveen Hasan

From: Benhoff, fJTchae! [[email protected]]

Sent: Wednesday, April 13, 2005 10:08 AM


Subject: Region 03 | Case 34031 | Lab CHEM | Issue Insufficient/inappropri ate designation .f laboratory QC

Hi Parveen:


Issue: The TR did not designate samples for laboratory QC for a few SDGs. The lab would like to choosesamples MC0141, MCOOA1, and MC0180 for this purpose.

Resolution: In accordance with previous direction frorn Region 3, for both Inorganic and Organic Multi-Media samples, the.laboratory will select a sample for laboratory QC as long as the sample is not a PE, blank,or rinsate sample. The laboratory will note the issue in the Case/SDG Narrative, notify the SMO coordinatorof the sample selected for laboratory QC, and proceed with the analysis of the samples.

SMO will note that the lab chose samples MC0141, MCOOA1, and MC0180 for laboratory QC. Pleaseindicate which SDG each of these samples is assigned to for laboratory QC.

thanks,Mike


This is a PRIVATE message. If you are not the intended recipient, please delete without copying and kindly advise us by e-inail ofthe mistake in. delivery. NOTE: Regardless of content, this e-rnail shall not operate to bind CSC to any order or oilier contractunless pursuant to explicit written agreement or government initiative expressly pemiining the use of e-mail for such purpose.

Original Message—--From: Parveen Hasan [mailto:[email protected]]Sent: Tuesday, April 12, 2005 4:57 PMTo: 'Benhoff, Michael1

Subject: RE: Regipn 03 | Case 34031 j'Lab CHEM | Issue Insufficient volume | FINAL

Mike,

No Lab QC samples assigned for few SDGs. Lab is planning to take sample MC0141, MCOOA1 and MC0180 as LabQC, as long these are not PE and Filed Blank. Its that OK w/ the Region?

Thanks

Parveen Hasan

4/13/2005311

117954

Message

CHEMTECH

284 Sheffield Street

Mountainside, NJ 07092

(908) 789-8900 Ext. 210

www.chemtech .net

4/13/2005

Original MessageFrom: Benhoff, Michael [mailto:[email protected]]Sent: Tuesday, April 12, 2005 2:44 PMTo: Divya Merita (E-mail); Parveen Hasan (E-mail)Cc: Betty Jeffery (E-mail); Dan Slizys (E-mail); John Kwedar (E-mail); Khin-Cho Thaung (E-mail)Subject: Region 03 | Case 34031 | Lab CHEM | Issue Insufficient volume | FINAL

Parveen:


Issue: The lab indicated that each sample received for Case 34031 consisted of 2 soil jars (1 Metals, 1Cyanide), however sample MC0085 was only sent with one Metal jar. The lab would like to know ifthey should use the Metals jar for sample MC0085 to analyze for Metals and Cyanide.

Resolution: Per Region 3, it is acceptable for the lab to analyze for Metals and Cyanide from the Metaljar for sample MC0085.

thanks,Mike

Michael Benhoff J

Computer Sciences CorporationCLP Coordinator for Regions 1,2, and [email protected]: (703) 818^357; Fax: (703)818-4602

Original Message-—From: [email protected] [mailto:[email protected]]Sent: Tuesday, April 12, 2005 1:26 PMTo: Benhoff, MichaelCc: [email protected]; [email protected];[email protected]: Re: NEW ISSUE | Case 34031 | Lab CHEM | Issue Insufficient volume

Mike,It isacceptable to the region for the lab to use the metals jar for CN for sample MC0085.

Original Message

312117955

From: Benhoff, MichaelSent: Tuesday, April 12, 2005 11:48 AMTo: Betty Jeffery (E-mail); Dan Slizys (E-mail); John Kwedar (E-mail); Khin-Cho Thaung (E-mail)Subject: NEWT5SUE | Case 34031 | Lab CHEM | Issue Insufficient volumeDan:

Please advise on the following issue.


Mike

Michael BenhoffComputer Sciences CorporationCLP Coordinator for Regions 1, 2, and [email protected]: (703) 818-4357; Fax: (703)818-4602 4

Original Message-—From: Benhoff, MichaelSent: Thursday, April 07, 2005 1:55 PMTo: Betty Jeffery (E-mail); Dan Slizys (E-mail); John Kwedar (E-mail); Khin-Cho Thaung (E-mail)Subject: NEW ISSUE |-Case 34031 | Lab CHEM | Issue Insufficient volume

Dan:

Please advise on the following issue:


thanks,Mike


Tliis is a PRIVATE message. If you are not the intended recipient, please delete without copying and kindly advise us byniail of the mistake in delivery. NOTE: Regardless ofcontent, this e-mail shall not operate to bind CSC to any order, orother contract unless pursuant to explicit written agreement or goveinitient initiative expressly permitting She use of e-maifor such purpose.

4/7/2005 Parveen Hasan, CHEM, contacted Mike Benhoff, SMO regarding Case 34031. The labindicated that each sample consisted of 2 soil jars (1 Metals, 1 Cyanide), however sample MC0085 wasonly sent with one Metal jar. The lab would like to know if they should use the Metals jar for sampleMC0085 to analyze for Metals and Cyanide.

4/13/2005313

117956

Parveen Hasan

From: Benhoff, IWchael [[email protected]]

Sent: Tuesday, ApriM 2, 2005 2:44 PM


Cc: Betty Jeffery (E-mail); Dan Slizys (E-mail); John Kwedar (E-mail); Khin-Cho Thaung (E-mail)

Subject: Region 03 | Case 34031 | Lab CHEM | Issue Insufficient volume | F INAL -

Parveen:


Issue: The lab indicated that each sample received for Case 34031 consisted of 2 soil jars (1 Metals, 1Cyanide), however sample MC0085 was only sent with one Metal jar. The lab would like to know if theyshould use the Metals jar for sample MC0085 to analyze for Metals and Cyanide.

Resolution: Per Region 3, it is acceptable for the lab to analyze for Metals and Cyanide from the Metal jar forsample MC0085.

thanks,Mike

Michael BenhoffComputer Sciences CorporationCLP Coordinator for Regions 1, 2, and [email protected]: (703) 818-4357; Fax: (703)818-4602

Original Message—-'From: [email protected] [mailto:[email protected]]Sent: Tuesday, April 12, 2005 1:26 PMTo: Benhoff, MichaelCc: [email protected]; [email protected];[email protected]: Re: NEW ISSUE | Case 34031 | Lab CHEM | Issue Insufficient volume

Mike,It isaceeptable to the region for the lab to use the metals jar for CN for sample MC0085.

—-Original MessageFrom: Benhoff, MichaelSent: Tuesday, April 12, 2005 11:48 AMTo: Betty Jeffery (E-mail); Dan Slizys (E-mail); John Kwedar (E-mail); Khin-Cho Thaung (E-mail)Subject: NEW ISSUE | Case 34031 | Lab CHEM | Issue Insufficient volumeDan:

Please advise on the following issue.

Issue: The lab indicated that each sample received for Case 34031 consisted of 2 soil jars (1 Metals, 1Cyanide), however sample MC0085 was only sent with one Metal jar. The lab would like to know if they

3144/12/2005

117957

rase 2 ot2

should use the Metals jar for sample MC0085 to 'analyze for Metals and Cyanide.

Mike _

Michael Benhoff *Computer Sciences CorporationCLP Coordinator for Regions 1,2, and 3michael.henho [email protected]: (703) 818-4357; Fax: (703)818-4602

Original MessageFrom: Benhoff, MichaelSent: Thursday, April 07, 2005 1:55 PMTo: Betty Jeffery (E-mail); Dan Slizys (E-mail); John Kwedar (E-mail); Khin-Cho Thaung (E-mail)Subject: NEW ISSUE 1 Case 34031 | Lab CHEM | Issue Insufficient volume

Dan:

Please advise on the following issue:•'•o •

Issue: The lab indicated that each sample received for Case 34031 consisted of 2 soil jars (1 Metals, 1Cyanide), however sample MC0085 was only sent with one Metal jar. The lab would like to know if theyshould use the Metals jar for sample MCOQ85 to analyze for Metals and Cyanide.

thanks,Mike


This is a PRIVATE message. If you are not the intended recipient, please delete without copying and kindly advise us by e-mail ofthe mistake in delivery. NOTE: Regardless of content, this e-mail shall not operate to bind CSC to any order or other contractunless pursuant to explicit written agreement or government initiative expressly permitting the use of e-mail for such purpose.

4/7/2005 Parveen Hasan, CHEM, contacted Mike Benhoff, SMO regarding Case 34031. The lab indicatedthat each sample consisted of 2 soil jars (1 Metals, 1 Cyanide), however sample MC0085 was only sent withone Metal jar. The lab would like to know if they should use the Metals jar for sample MC0085 to analyzefor Metals and Cyanide.

3154/12/2005

117958

- Message • ' .--pagel of:

Parveen Hasan

From: Parveen Hasan

Sent: Tuesday, April 12, 2005 12:35 PM

To: 'Benhoff, Michael1'

Subject: RE: Region 03 | Case 34031 | Lab CHEM | Issue Multiple | FINAL '

Mike,'

There is a Revision for Issue #2 and lssue#3:

Revised Issue#2: Lab didn't received sample MC0125 (station location: BJS-SDMON2C3-0405) was listed onthe TR as CO 125 and Renamed w/ a new sample ID MC1AP2. •

Revised Issue#3: Lab didn't received samples for DM even on TR its listed w/ number of Jars 3. Intact, labreceived 2 Sample Jars (for CN and TM) only. (Here to mention that, as per Region DM should be Disregard)

Sorry, for the Inconvenient.

Thanks ."

Parveen Hasan

CHEMTECH

284 Sheffield Street

Mountainside, NJ 07092

(908) 789-8900 Ext. 210

www.chemtech.net

Original MessageFrom: Benhoff, Michael [mailto:[email protected]]Sent: Tuesday, April 12, 2005 7:43 AMTo: Parveen Hasan (E-mail) .Cc: Betty Jeffery (E-mail); Dan Slizys (E-mail); John Kwedar (E-mail); Khin-Cho Thaung (E-mail)Subject: Region 03 | Case 34031 | Lab CHEM | Issue Multiple | FINAL .

This is Carolyn Mack - Mike should be in later today.

Samples shipped to the incorrect laboratoryIssue 1: The lab received organic samples along with their inorganic shipment. The lab receivedsamples C0068-COOC1 (on 2 TR'sj. Please provide an address and billing information if the samplesshould be trans-shipped.

3164/13/2005' 117959

Message . .--Page-2 of 5

Resolution 1: Per Region 3, the Tetra Tech air bill voucher number for the organic samples mistakenly. sent to CHEM that require transshipment is: 0191 -2082-1, The samples should be sent to the following

address: —

Liberty'Analytical501 Madison Ave. .Gary, NC 27513919-379-4081

Incorrect/duplicated sample numbersIssue 2: Sample MC0125 (station location: BJS-SDMON2C3-0405) was listed on the TR as C0125.Resolution 2: Per Region 3, the laboratory should report sample C0125 under the new sample ID

• MC1AP2, note the situation in the Case/SDG Narrative, and proceed with the analysis of the samples.

Discrepancies with, tags, jars, and/or TR/COCIssue 3: All of the inorganic samples were listed on the TR/COC for DM and TM, however these areall soil samples.Resolution 3: Per Region 3, the lab should only analyze the soil samples for total metals analysisand disregard the dissolved metals analysis. Please note this situation in the Case/SDG Narrative andproceed with the analysis of the samples.

Please let Mike or me know if you have any questions or problems.


Original Message—-From: [email protected] '_Sent: Tuesday, April 12, 2005 6:44 AMTo: Benhoff, MichaelCc: [email protected]; [email protected]; [email protected]: Re: NEW ISSUE - Region 3 j Case 34031 | Lab CHEM | Issue Multiple

Mike,

Issue 1: SMO can provide trans-shipment information to the lab.Issue 2: No, SMO should not ask the lab to change C0125 to MC0125. A memo to file from fieldpersonnel wjll clarify this issue. The lab will use CO 125 as sample ED when reporting results or SMOcan provide a new CLP sample ID number.Issue 3: Yes, the lab should only analyze for total metals. Disregard the dissolved metals analysis.

Original MessageFrom: Benhoff, MichaelSent: Monday, April 11, 2005 3:58 PMTo: Betty Jeffery (E-mail); Dan Slizys (E-mail); John Kwedar (E-mail); Khin-Cho Thaung (E-mail)

. Subject: NEW ISSUE - Region 3 | Case 34031 | Lab CHEM | Issue Multiple.

This is Carolyn Mack - Mike is out of the office today.

3174/13/2005 117960

Message . .--Pase-3 of 5

SMO received trans-shipment information for issue 1 from the sampler, however the sampler indicatedthat the other two issues would be resolved at a later date.

• Issue 1) Is it acceptable for SMO to send on the trans-shipment information?• Issue 2) Should SMO direct the inorganic laboratory to report sample CO 125 as MC0125?• Issue 3) Should the laboratory only analyze the soil samples that were listed for TM and DM for

TM analysis (i.e., DM analysis is cancelled)?

Issue 1: The lab received organic samples along with their inorganic shipment. The lab receivedsamples C0068-COOC1 (on 2 TR's). Please provide an address and billing information if the samplesshould be trans-shipped.Resolution 1: Per Region 3, the Tetra Tech air bill voucher number for the organic samples mistakenly sent to CHEMthat require transshipment is: 0191-2082-1. The samples should be sent to the following address:

Liberty Analytical501 Madison Ave.Gary, NC 27513-919-379-4081 . .

Issue 2: Sample MC0125 (station location: BJS-SDMON2C3-0405) was listed on the TR as C0125.

Issue 3: AH of the inorganic samples' were listed on the TR for DM and TM, however these are all soilsamples.

Michael BenhoffComputer Sciences CorporationCLP Coordinator for Regions 1,2, and 3 • •[email protected]: <703) 818^357; Fax: (703)818-4602

—Original Message—From: Parveen HasanSent: Monday, April 11, 2005 12:17 PMTo: 'Mack, Carolyn'Subject: FW: Region 03 |£ase"34031 ,| Lab CHEM | Issue Multiple

Carol,

Lab is waiting for the Resolution.

• ThanksParveen HasanCHEMTECH284 Sheffield Street 'Mountainside, NJ 07092(9.08) 789-8900 Ext. 210www.chemtech.net .

—Original Message—From: Yanches(d, Tad - Tt, Inc. [mailto:[email protected]]Sent: Monday, April 11, 2005 10:38 AMTo: '[email protected]'; 'Benhoff, Michael'; Swartzwelder, Kyle -- Tt, Inc.; Yancheski, Tad - Tt, Inc.Cc: '[email protected]'; '[email protected]'; '[email protected] '

3184/13/2005 117961

Message ...--? age-4 of 5

Subject: RE: NEW ISSUE | Case 34031 | Lab CHEM | Issue Multiple - Trans Sh ip Information

Hi Dan - __

The Tetra Tech air bill voucher number for the organic samples mistakenly sent to CHEM that require transshipment is:

0191-2082-1

Liberty Analytical501 Madison Ave.Gary, NC 27513919-379-4081

Memo's to file will be prepared for the other issues at a later date.»

Please advise if you have any questions.

Regards,

Tad YancheskiTetra Tech . . . . . . . .302-738-7551 ;

Original MessageFrom: SlJ2ys.Dan@epamail. epa. govSent: Monday, April 11, 2005 9:46 AMTo: Benhoff, Michael; [email protected]: [email protected]: [email protected]; kwedar.john@epamaiil. epa. go v: tbaung.kbia-cho@epamail. epa. govSubject: Re: NEW ISSUE | Case 34031 | Lab CHEM | Issue Multiple

Mike, '

The field personnel will b'e contacted. The lab should proceed with the analysis of samples anddocument all issues in the case narrative. Kyle and Tad,

There are more issues which need your attention:Issue 1: The lab received organic samples that may have to be trans-shipped. We will need air billvoucher.Issue 2: MC0125 listed on the TR/COC as sample C0125. Need a memo to file for clarification.Issue3: Soil samples on the TR/COC are listed as for total and dissolved metals analysis. Need a memoto file for clarification.

Original MessageFrom: BenhofF, MichaelSent: Friday, April 08, 2005 4:45 PM :To: Betty Jeffery (E-mail); Dan Slizys (E-mail); John Kwedar (E-mail); Khin-Cho Thaung (E-mail)

. Subject: NEW ISSUE | Case 34031 | Lab CHEM | Issue MultipleDan:. \

Please advise on the following issues: ;

Issue 1: The lab received organic samples along with their inorganic shipment. The lab received

3194/13/2005 117962

Message . • • • " page 5 of 5

samples C0068-COOC1 (on 2 TR's). Please provide an address and billing information if the samplesshould be trans-shipped.

. Issue 2: Sample MC0125 (station location: BJS-SDMON2C3-0405) was listed on the TR as C0125.


thanks,Mike

Michael Benhoff ^Computer Sciences CorporationCLP Coordinator for Regions 1, 2, and [email protected]: (703) 818-4357; Fax: (703)818-4602

This is a PRIVATE message. If you are not the intended recipient, please delete without .copying and kindly advise us by e-mail of the mistake in delivery. NOTE: Regardless of content, this s-mail shall not operate to bind CSC to any order orother contract unless pursuant'to explicit written agreement or government initiative expressly permitting the use of e-mailfor such purpose.

Original MessageFrom: Parveen Hasan [mailto:[email protected]]•'Sent: Friday, April 08, 2005 4:30 PMTo: 'Benhoff, Michael1

Subject: Region 03 | Case 34031 | Lab CHEM | Issue. Multiple

Mike,

The Following samples Lab found for Case# 34031:

lssue#1: Lab Received Organic samples along w/ Inorganic samples. .

lssue#2: Incomplete sample ID on TR as C0125 (for Station Location: BJS-SDMON2C3-0405)

lssue#3: Same sample ID reported on TR for TM and DM for all samples (w/ total number of bottles 3).Also, all these samples are Soil Samples !!! -

ThanksParveen HasanCHEMTECH284 Sheffield Street .Mountainside.'NJ 07092(908) 789-8900 Ext. 210www.chemtech .net

3204/13/2005 117963

FORT MEADE, MARYLAND 20755-5350 · PDF fileMC0085, MC0087, MC0088, MC0098 All Samples Except MCOOA7, MCOOB3, MC0068, MC0080, MC0085, MC0087, MC0088, MC0098 All Samples MCOOA7, MCOOA9

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