Page 1
() y - - -
1) Consultants Engineers Contractors
I
April 15 2009
US Enviromnental Protection Agency Mail Code CMU One Congress Street Boston MA 02114-2023 Attn Shelly Puleo Enviromnental Assistant
RE NOI Submittal Former Speedway Service Station 181 East Broadway Gardner Massachusetts 01440 MassDEP Release Tracking No 2-0707
To Whom It May Concern
On behalf of cK Smith Company Inc (CK Smith) Corporate Enviromnental Advisors Inc
(CEA) is submitting this Notice of Intent (NOI) for the above-referenced site The NOI is being
submitted in accordance with the Provision for Contaminated Construction Dewatering under the Remediation General Permit (RGP) Construction-related dewatering is necessary at this location to facilitate the excavation of petroleum-impacted soil On-site treatment of the extracted groundwater wil be performed as outlined in the attached NOI prior to the proposed discharge
If you have any questions please feel free to contact us at 508-835-8822
Sincerely corpo 0rnental Advisors I
nia4 c4 -c- L-
Michael 1 Dziura P
r Enviromnental Scientist Sr Enviromnental Engineer
Pc Mr Dana Morse AJJ Realty Inc Ms Janine Perley CK Smith Bureau of Waste Site Cleanup MassDEP CERO CEA File No 2920shy
ADDRESS Hartwell Business Park
127 Hartell StreetWest Boylston MA 01583
TE 508835 8822 8003587960
FAX 508 835 8812 Massachusetts Connecticut New HampshireRhode Island
WEB wwwcea- inc com
~~~~
B SU22ested Form
for Notice of Intent (N
OI) for the R
emediation G
eneral Permit
General site inform
ation Please provide the following inform
ation about the site
Facilitysite address
a) Name of faciltysite
Fonner S
peedway S
ervice Station
Location of facilitysite
Street
longitude 71
58 35 latitude 42 33 15
4471 181 E
ast Broadw
ayI Facility SIC
code (s) b) N
ame offacilitysite ow
ner T
own
AJJ R
ealty Inc G
ardner
Em
ail address of owner
State Z
ip C
ounty 01440
Worcester
Telephone no of facilitysite ow
ner 978- 632-0089
Fax no offacilitysite owner
Ow
ner is (check one) 1 Federal 2 S
tateTribal
3 Private
other 0 if so describe
Address of ow
ner (if different from site)
Street 207 H
igh Street T
own
State Z
ip G
ardner I C
ounty01440
Worcester
) Legal name of operator
Operator telephone no
Corporate E
nvironmental A
dvisors Inc 508-835- 8822
Oper
tor fax no
508-835-8812 M
Dziura
cea- inccom
I Operator em
ail O
perator contact name and title
Michael D
ziura Sr Env E
ngineer
Address of operator (if different from
owner)
Street 127 H
artwell Street
Tow
n State
West Boylston
Worcester
I County
d) Check yes or
for the following
I Has a prior N
PD
ES
permit exclusion been granted for the discharge Y
es No rg if yes num
ber
2 Has a prior N
PDE
S application (Form 1 amp
2C) ever been fied for the discharge Y
es N
o rg if yes date and tracking
3 Is the discharge a new discharge as defined by 40 C
FR 1222 Y
es rg No D
4 For sites in M
assachusetts is the discharge covered under the MA
Contingency Plan (M
CP) and exem
pt from state perm
itting Yes rg N
o D
Rem
ediation General Perm
it - Notice of Intent
f) Is the sitefacility covered by any other EP A
permit including
e) Is sitefacilty subject to any State permitting or other action w
hich is causing the generation of discharge Y
es rg No D
1 m
ulti-sector storm w
ater general permit Y
es D No rg
if Y
number
If yes please list
2 phase I or II construction storm w
ater general permit Y
es No rg
1 site identification assigned by the state ofNH
or MA
MA
DE
P ifY
number
2 permit or license assigned
Release T
racking Num
ber 2- 0707 3 individual N
PDE
S permit Y
es No rg ifY
number
3 state agency contact information nam
e location and telephone num
ber 4 any other w
ater quality related permit Y
es No rg ifY
number
MA
EP B
ureau of Waste Site C
leanup 627 Main Street W
orcester MA
2 Dischare inform
ation Please provide information about the discharge (attaching additional sheets as needed) includin
Describe the discharge activities for w
hich the ownerapplicant is seeking coverage
Dew
atering during excavation of approximately 1 000 cubic yards of petroleum
- impacted soil G
roundwater w
ill be extracted from the excavation and pum
ped into a 21 000shygallon frac tank for sedim
ent removal W
ater wil be treated w
ith granular activated carbon to remove petroleum
compounds prior to discharge to the local storm
water
drainage system A
pprox stormw
ater drainage outfall is depicted on Figure 4 attached
b) Provide the 1) N
umber of
2) What is the m
aximum
and average flow rate of discharge (in cubic feet per second W
s) Max flow
0 067 fesec follow
ing discharge
Average flow
0033 fesee Is m
aximum
flow a design value Y
es rg No D
information
points For average flow
include the units and appropriate notation if this value is a design value or estimate if not available
about each
discharge
3) Latitude and longitude of each discharge w
ithin 100 feet pt long 58 35 lat 42
33 15 pt2 long lat -
pt3 long _ lat shypt4long _ lat -
pt5 long lat
pt6long _ lat - pt7 long _ lat -
pt8long _ lat - etc
4) If hydrostatic testing total volume of the discharge (gals)
5) Is the discharge intennittent rg Or seasonal
Is discharge ongoing Yes
No rg
Discharge is tem
porary in nature and is only related to excavation activities (dewatering)
NA
c) Expected dates of discharge (m
mddyy) star
090109 end
100109
d) Please attach a line drawing or flow
schematic show
ing water flow
through the facility including See attached fi ures 4 amp
5
1 sources of intake water 2 contributing flow
fiom the operation
3 treatment units and 4 discharge points and receiving w
aters(s)
Rem
ediation General Perm
it - Notice of Intent
----
3 Contam
inant information In order to com
plete this section the applicant
il need to take a minim
um of one sam
ple of the untreated water and have it analyzed for all of the
parameters listed in A
ppendix III Historical data (i
data taken no more than 2 years prior to the effective date of the perm
it) may be used if obtained pursuant to i
Massachusetts regulations 310 C
MR
40 0000 the Massachusetts C
ontingency Plan (Chapter 21E ) ii N
ew H
ampshire s T
itle 50 RSA
485- A W
ater Pollution and Waste
Disposal or T
itle 50 RSA
485- C G
roundwater Protection A
ct or iii an EPA
pennit exclusion letter issued pursuant to 40 CFR
122 provided the data w
as analyzed with test
methods that m
eet the requirements of this perm
it Otherw
ise a new sam
ple shall be taken and analyzed
a) Based on the analysis of the sam
ple(s) of the untreated influent the applicant must check the box of the sub-categories that the potential discharge falls w
ithin
Gasoline O
nly V
OC
Only
Primarily M
etals U
rban Fill Sites C
ontaminated Sum
ps Mixed Contaminants
Aquifer T
esting
VO
C w
ith Other
Petroleum w
ith Other
Listed C
ontaminated
Contam
inated H
ydrostatic Testing of
Well D
evelopment or
Other O
ils) only C
ontaminants
Contam
inants Sites
Dredge C
ondensates PipelinesT
anks R
ehabilitation F
uel Oils (and
b) Based on the analysis of the untreated influent the applicant m
ust indicate whether each listed chem
ical is believed present or believed absent in the potential discharge A
ttach additional sheets as needed
PAR
AM
ET
ER
B
elieve B
elieve of
Type of
Analytical
Minim
um
Maxim
um daily value
Avg daily value
Absent
Present Sam
ples Sam
ple M
ethod L
evel (ML
) of
(1 min-
(eg grab) U
sed T
est Method
concentration m
ass concentration
mass
imum
) (m
ethod ) (ugI)
( ugI) (kgday)
(ugI) (kgday)
1 Total Suspended Solids
GR
A
SM 2540D
000
580 000 215
SW-846
GR
A
100 c 500
2 Total R
esidual 9012A
C
hlorine
3 Total Petroleum
G
RA
1664
000 600
12
Hydrocarbons
4 Cyanide
GR
A
9012A
cl0
c20S B
enzene G
RA
B
5030
6 Toluene
GR
A
5030 c20
7 Ethylbcnzene
GR
A
5030 411
8 (m
o) Xylenes
GR
A
5030 10
472
9 Total B
TE
X
GR
A
5030 883
04
BT
EX
= SU
IU of B
enzene Toluene
Ethylbenzene
total Xylenes
Rem
ediation General Perm
it - Notice of Intent
PAR
AM
ET
ER
B
elieve B
elieve of
Type of
Absent
Present Sam
ples S
ample (eg
(1 min-
grab)
imum
)
10 Ethylene
Dibrom
ide G
RA
B
(1 2- Dibrom
o-methane)
11 Methyl-tert-B
utyl G
RA
Ether (M
tBE
)
12 tert-
Butyl
Alcohol
GR
AB
(TB
A)
13 tert-A
myl
Methyl
GR
A
Ether (T
AM
E)
14 Naphthalene
GR
AB
15 Carbon T
etra-G
RA
chloride
16 1
Dichlorobenzene
GR
A
17 D
iehlorobenzene G
RA
GR
A18 1
Dichlorobenzene
19 1
Dich1oroethane
GR
A
20 1
Dichloroethane
GR
A
21 1
Dichloroethylene
GR
A
22 cis-D
ichloro-G
RA
B
ethylene
GR
A
(Methylene C
hloride)
23 D
ichloromethane
24 T
etrachloroethylene G
RA
B
Rem
ediation General Perm
it - Notice of Intent
Analytical
Minim
um
Maxim
um daily value
Avg daily value
Method
Level (M
L) of
Used
Test M
ethod concentration
mass
concentration m
ass
(method )
(ugI) ( ug)
(kgday) (ugI)
(kgday)
504 010
0 0
5030 05
020
5030 0200
5030 020
625 247
5030 020
5030 020
5030 05
020
5030 020
5030 020
5030 020
5030 05
020
5030 020
5030 10
0200
5030 020
PAR
AM
ET
ER
B
elieve B
elieve of
Type of
Absent
Present Sam
ples Sam
ple (e
(l min-
grab)
imum
)
25 1
1 Trichloroethane
GR
AB
26 1
2 Trichloroethane
GR
A
27 Trichloroethylene
GR
AB
28 Vinyl C
hloride G
RA
B
29 Acetone
GR
A
30 14 D
ioxane G
RA
B
31 Total Phenols
GR
AB
32 Pentachlorophenol
GR
AB
33 Total Phthalates 6
GR
AB
(phthalate esthers)
34 Bis (2-E
thylhexyl) G
RA
B
Phthalate (D
ishy(ethylhexyl) P
hthalate)
35 Total G
roup 1 G
RA
P
olycyclic Arom
atic H
ydrocarbons (PA
H)
a Benzo(a) A
nthracene G
RA
B
b Benzo(a) P
yrene G
RA
c Benzo(b )F
luoranthene G
RA
B
d Benzo(k) F
luoranthene G
RA
e Chrysene
GR
AB
The slim
of iijdividual phthalate compounds
Rem
ediation General Perm
it - Notice of Intent
Analytical
Minim
um L
evel M
aximum
daily value A
vg daiJy Value
Method Used
(ML) ofT est
(method )
Method
concentration m
ass concentration
mass
(ugI) (ugI)
(kgday) (ugl)
(kgday)
5030 20
5030 20
5030 20
5030 ~20
5030 400
5030 200
625 50
625 50
625 All phthalates are
BD
L see lab report
625 50
625 A
ll Group I P A
Hs
are BD
L
625 50
625 50
625 50
625 50
625 50
g
PAR
AM
ET
ER
B
elieve B
elieve of
Type of
Analytical
Minim
um
Maxim
um daily value
Average daily value
Absent
Present Sam
ples Sam
ple (e M
ethod Used
Level (M
L) of
(lmin -
grab) (m
ethod ) T
est Method
concentration m
ass concentration
mass
imum
) (ug1)
(ugl) (kgday)
(ugl) (kgday)
f Dibenzo(a
GR
AB
625
-(50
anthracene
Indeno(I 23-cd) G
RA
B
625 -(50
Pyrene
36 Total G
roup II G
RA
B
625 247
Polycyclic A
romatiC
H
ydrocarbons (pAR
)
h Acenaphthene
GR
AB
625
-(10
i Acenaphthylene
GR
A
625 -(50
j Anthracene
GR
A
625 -(50
k Benzo(ghi)
Perylene G
RA
B
625 -(50
I Fluoranthene G
RA
B
625 -(50
m F
luorene G
RA
B
625 -(50
n Naphthalene-
GR
AB
625
247
o Phenanthrene
GR
AB
625
-(50
p Pyrene
GR
AB
625
-(50
37 Total
POlychlorinated
GR
AB
608
065 -(0065
Biphenyls (PC
Bs)
38 Antim
ony G
RA
B
200 03
4Eshy
39 Arsenic
GR
AB
200
468
40 Cadm
ium
GR
AB
200
-( 0
41 Chrom
ium II
(1) G
RA
B
calculated calculated
-(5
42 Chrom
ium V
I G
RA
7196A
-( 125
NO
TE
S (1) Chrom
ium m
= T
otal Chrom
ium - H
exavalent Chrom
ium A
ccording to lab personnel the trivalent chromium
is calculated to be greater or equal to 5 ugI but less than 125 ugl Total
Chrom
ium w
as -(5 ugI and the Hexavalent C
hromium
was less than 125 ugl
Rem
ediation General Perm
it - Notice of Intent
--------
--------
-------
--------
---
PAR
AM
ET
ER
B
elieve B
elieve of
Type of
Analytical
Minim
um
Maxim
um daily value
Avg daily value
Absent
Present Sam
ples Sam
ple (e M
ethod L
evel (ML
) of grab)
Used
Test M
ethod concentration
mass
concentration m
ass(1 m
inshy
imum
) (m
ethod ) (ug1)
(ug1) (kgday)
(ug1) (kgday)
43 Copper
GR
A
200 (5
44 Lead G
RA
200
0001
45 Mercury
GR
A
7470A
(020
46 Nickel
GR
AB
200
(5
GR
AB
200
( 1547 Selenium
48 Silver G
RA
B
200 (0
49 Zinc
GR
A
200 18
0025
50 Iron G
RA
B
200 400
25
Other (describe)
c For discharges where m
etals are believed present please fill out the following
If yes which m
etals A
rsenic and Iron Step
I Do any of the m
etals in the influent have a reasonable potential to exceed the
etIluent limits in A
ppendix II (i the limits set at zero to five dilutions) Y
rg N D
Step 2 For any m
etals which have reasonable potential to exceed the A
ppendix III limits
Look up the lim
it calculated at the corresponding dilution factor in
calculate the dilution factor (DF) using the form
ula in Part I A 3 c) (step 2) of the N
O
Appendix IV
Do any of the m
etals in the influent have the potential to instructions or as determ
ined by the State prior to the submission of this N
OI
exceed the corresponding effuent lim
its in Appendix IV
(i is the
What is the dilution factor for applicable m
etals in1uent concentration above the lim
it set at the calculated dilution M
etals A
rsenic and Iron factor)
yrgND
If Y
es list which m
etals A
rsenic and Iron
DF
Rem
ediation General Pem
lit - Notice of Intent
4 Treatm
ent system inform
ation Please describe the treatment system
using separate sheets as necessary including
a) A description of the treatm
ent system including a schem
atic of the proposed or existing treatment system
S
ee Figures 4 and 5
Frac tank Air stripper
Oilw
ater separator Equalization tanks
Bag filter rg
GA
C filter rg
b) Identity each applicable
treatment unit (check alJ
that apply)
Chlorination
Dechlorination
Other (please describe)
c) Proposed average and maxim
um flow
rates (gallons per minute) for the discharge and the design flow
rate(s) (gallons per minute) ofthe treatm
ent system
Average flow
rate of discharge 15 G
PM
Maxim
um flow
rate oftreatment system
0 G
PM
Design flow
rate of treatment system
0 G
PM
d) A description of chem
ical additives being used or planned to be used (attach MSD
S sheets) Not A
pplicable
5 Receiving surface water(s) Please provide information about the receiving water (s) using separate sheets as necessary including
Identity the discharge pathway
I Direct
I Within facility
I Stonn drain rg I R
iverbrook I W
etlands _ I Other (describe)
Provide a narrative description ofthe discharge pathway including the nam
e(s) of the receiving waters
Discharge to catchbasin and stonnw
ater drainage system in E
ast Broadw
ay which discharges to M
ahoney Brook (S
ee Figure 4)
c) Attach a detailed m
ap(s) indicating the site location and location of the outfall to the receiving water
1 For multiple discharges num
ber the discharges sequentialJy 2 For indirect dischargers indicate the location of the discharge to the indirect conveyance and the discharge to surface w
ater T
he map should also include the location and distance to the nearest sanitary sew
er as well as the locus of nearby sensitive receptors (based on U
SGS topographical
mapping) such as surface w
aters drinking water supplies and w
etland areas d) Provide the state w
ater quality classification of the receiving water
e) Provide the reported or calculated seven day- ten year low flow
(7QlO
) of the receiving water Jcfs
Please attach any calculation sheets used to support stream flow
and dilution calculations See A
ttachment B
f) Is the receiving water a listed 303(d) w
ater quality impaired or lim
ited water Y
es 0 No rg
If yes for which polJutant(s) N
A
Is there a TM
DL
Yes 0
No rg If yes for w
hich pollutant(s) NA
Rem
ediation General Perm
it - Notice of Intent
6 Results of C
onsultation with Federal Services Please p
rovide the following information according to requirements of Par
lBA
and A
ppendices II and VII
a) Are any listed threatened or endangered species or designated critical habitat in proxim
ity to the discharge Yes 0
No rg
Has any consultation w
ith the federal services been completed Y
es 0 No rg
or is consultation underway Y
es 0 No rg
What w
ere the results of the consultation with the U
S Fish and Wildlife Service andor N
ational Marine Fisheries Service (check one) N
ot applicable
a nojeopardy opinion
or written concurrenceD
on a finding that the discharges are not likely to adversely affect any endangered species or critical habitat
b) Are any historic properties listed or eligible for listing on the N
ational Register of H
istoric Places located on the facilty or site or in proximity to the discharge
Yes D
No
Have any state or tribal historic preservation offcer been consulted in this determ
ination (Massachusetts only) Y
es O N
o
7 SU
DD
lemental inform
ation
Please provide any supplemental information Attach any analytical data used to support the application A
ttach any celtification(s) required by the general permit
Attachm
ent A - Figures
Figure I - Site Locus M
ap
Figure 2 - MassD
EP Site Scoring M
ap
Figure 3 - Aerial M
ap
Figure 4 - Proposed Soil Excavation A
rea Map
Figure 5 - T
reatment S
ystem Line D
iagram
Attachm
ent B - D
ilution factor Calculations
Attachment C - L
aboratory Analytical R
eport Groundw
ater
Rem
ediation General Perm
it - Notice of 1ntenl
=-
including the following
8 Signature Requirements
The N
otice ofIntent must be signed by the operator in accordance w
ith the signatory requirements of 40 C
FR Section 122
certification
J certif under penalty of law that this docum
ent and all attachments w
ere prepared under my direction or supervision in accordance w
ith a system
designed to assure that qualifed personnel properly gather and evaluate the information subm
itted Based on m
y inquiry of the person or persons who
manage the system
or those persons directly responsible for gathering the information I certif that t
he information submitted
is to the best of m
y
knowledge and belief true accurate and com
plete J certif that I am aw
are that there are signifcant penalties for submitting false inform
ation including
the possibilty of fine and imprisonm
ent for knowing violations
FacilitySite Name
Form
er Speedw
ay Service S
tation 181 East B
roadwav G
ardner MA
01440
Operator signature
Title
Michael 1 D
ziura Sf Env E
ngineer
Date
4150- q
Rem
ediation General Perm
it - Notice of Intent
-
D- 0
0 0
il (J tu
Bw
o(0 -I
NJW
gQb
J(JZc o c
rou a -10
0 J 6shy
a 0
I-tDC
aJ Qj
E aJshy
ro ro ro
~~~ ~~~~- -- - _ - -_ - ~~~ ~~~~ ~~~ - - _- _- -- -- p __(
MA DEP - Bureau of Waste Site CleanupSITE NME Site S aP 5 MiFlII Former Speeway Station _-II181 Eat Broaday b b d IS I i I GARDNER MA 0144 v ri) i P f f 1 me- 1 5ylmI I L shy J --I 423315n 715835e SiteLocation y o oCop1odQcn Ofof W-_ l
1 1 I
r
r
iBARBER HILL
A c
Cf1 f o s
0
5
Roads Uned Acss Divd Mar Roed Conntor Street Track 1 EPA Sola Source Aquilar FEMA 100yaar iloodplain 0 c Puc Watar SLo GrunSelaceNon Corrty 0
Bounars lOwn Couny DE Region Tian Powerln Ine Aqedut ApprOld Zona2 tNPA Sue Wster Supp Zone A bStZ F--shy--rle
8os Mat Sub SUeor Porenrial Inermtent Man lvo8 Ste Dfm Hyro1apy Wmer FeatllePLio Suleee Wat S H-- L otlMds FrslSaltN-ES WeIMd Habat L
Potentia Prdutiv AqlJlers ModHig Yield Proteoted Opn Space ACC nIL c= Non-Potential Drng Water Sollce AIea ModumHi Yo1d ll DEP Pormrd SoidWes1 FsiIi6s cnifud Verne Pools f0
1I2 KIWUmR$ MtL
January 30 2004 SCALE 1 15000
-
LE
GE
ND
APX PROPER BONDA
- APPROXOiSPO SIT BOUNDA
-GR
OU
ND
WA
TE F1 D
IRE
cnON
SCA
LE
30 60 FE
(APR
OX
CORPORATE ENVIRONMENTAL
)i
AD
VISO
RS
INC
SC
AS SH
OW
D
R B
Y K
HA
EL
DA
TE
10407
JOB
NO
2920-96
AERIAL MAP
FO
RM
ER
SP
EE
DW
AY
ST
AT
ION
FlGURE -3
181 EA
BR
OA
AY
GA
NE
R fo
age 1 ot 1Streamflow Statistics Report
Streamstats Ungaged Site Report Date Wed Dec 31 2008 124908 Site Location Massachusetts NAD83 Latitude 425545 (42 3316) NAD83 Longitude -719758 (-71 58 32) NAD27 Latitude 425545 (423316) NAD27 Longitude - 9763 (-71 58 34) Drainage Area 502 mi2
IPeak Flow Basin Characteristics 1100 Statewide Low Flow (S02 mi2)
Regression Equation Valid Rang
I Min II Max1 Value III Parameter Drainage Area (square miles) 161 149
Mean Basin Slope from 250K DEM (percent) 032 24
Stratified Drift per Stream Length (square mile per mile) 129
Massachusetts Region (dimensionless)
Streamflow Statistics
gO-Percent Prediction Interval Prediction Error
MaximumStatistic Flow (ft s) (percent) Minimum
I D50 IIII 11 1811 II 24511 993
I D60 II 35511 2011 II 03611 35111 2411 II 041 I 201I D70 24111 2611 II 03811 151I D75 11 2811 II 0911 3761I D80 981I D85 1 I 3211 II o6311
1 I 3711 II 0441 1 2 2911 D90 11 4611 II 02411 15511 D95I D98 04511 6011 II 01511 11
I D99 03411 6511 II ol1ll 1021
5011 II 02611 11I M7D2Y 1111 3311 II odl 3 541
I AUGD50
IIIIIIIIIIIIIIIIIIIIII 0311 7111 II 0088411 0981I M7Dl0Y
1010
12312008httpstreamstatsagscrusgsgovgisimgReportsFlowStatsReport3494 - 2008123112498
Dilution Factor Calculation Former Speedway Service Station 181 East Broadway Gardner Ma
DF=(Od+Os)Od
DF = Dilution factor
Od = Max flow rate of discharge in cubic feet per second Os = receiving water flow in cubic feet per seconds 7010 flow rate Mahoney Brook 7010 = min flow for seven consecutive days with a recurrence interval of 10 years
7010 flow based on data obtained from USGS Steamflow Statistics Report Data attached
067
Semivolatile Organic Compounds by GCMS - Quality Control
Analyte( s)
Batch 8051216 - SW846 3510C
Blank 8051216BLK1)
Prepared amp Analyzed 16May-
Acenaphthene
Acenaphthylene
Aniline
Anthracene
AzobenzenelDi phenyld iazi ne
Benzidine
Benzo (a) anthracene
Benzo (a) pyrene
Benzo (b) fiuoranthene
Benzo (g i) perylene
Benzo (k) fiuoranthene
Benzoic acid
Benzyl alcohol
Bis(2-ch loroethoxy) methane
Bis(2-ch loroethyl)ether
Bis(2-ch loroi sopropyl)ether
Bis(2ethylhexyl) phthalate
Bromophenyl phenyl ether
Butyl benzyl phthalate
Carbazole
Ch loro-3-methyl phenol
Chloroaniline
Chloronaphthalene
Chlorophenol
Chlorophenyl phenyl ether
Chrysene
Dibenzo (a h) anthracene
Dibenzofuran
Dichlorobenzene
Dichlorobenzene
14- Dichlorobenzene
3 - Dichlorobenzidine
24-Dichlorophenol
Diethyl phthalate
Dimethyl phthalate
24- Dimethylphenol
Din-butyl phthalate
Dinitro-2-methylphenol
Dinitrophenol
Dinitrotoluene
Dinitrotoluene
Di-noctyl phthalate
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopehtadiene
Hexachloroethane
Indeno (1 cd) pyrene
Spike Source REC RPD
Result Flag Units RDL Level Result REC Limits RPD Limit
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gl
BRL gI
BRL gl
BRL gl
BRL gl
BRL gI
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gll
BRL gl
BRL gll
BRL gl
BRL gl
BRL gI
BRL gI
BRL gI
BRL gl
BRL gI
BRL gI
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gI
BRL gI
BRL gl
This laboratory report is IlOt valid without all authorized sigllature 011 the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page t4 of25
Volatie Organic Compounds - Quality Control
p (
Spike Source REC RPD
RDL Level Result REC Limits RPD Limit Analyte(s) Result Flag Units
Batch 8051244 - SW846 5030 Water MS
Matrix S ike Du 8051244-MSD1 Source SA78629shy
Prepared 16-May-08 Analyzed 17-May-BRL 106 251
Vinyl chloride 21 gl 20
101 70- 130 Surrogate 4-Bromofluorobenzene 50 gl 50
70- 13049 gl 50 111 70- 130
Surrogate Toluene-Surrogate 1 Dichloroethane- 55 gl 50
50 70- 130494 glSurrogate Dibromofluoromethane
Microextractable Organic Compounds - Quality Control
Spike Source REC RPD
Flag Units RDL Level Result REC Limits RPD Limit Analyte(s) Result
Batch 8051105 - SW846 3510C
Blank 8051105-BLK
Prepared amp Analyzed 15-May-
BRL gl 01001 Dibromoethane (ED B)
LCS 8051105-BS1
Prepared amp Analyzed 15-Mayshy50- 1500770 gl 0100 100
licate 8051105-DUP1 Source SA7B583shy
Prepared amp Analyzed 15-May-
BRL gl 0100 BRL
1 Dibromoethane (EDB)
1 Dibromoethane (EDB)
This laborntOlY report is not valid without an authorized signature 011 the cover page
Page 13 of2S Reportable Detection Limit BRL = Below Reporting Limit
Sam le Identification Client Pro ect Matrix Collection DateTime ReceivedMWshy
2920-96- Ground Water 13-May-081030 14-May-SA 78602shy
CAS No Analyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Volatile Organic Compounds
Volatile Or anic Com ounds b GCMS
Prepared by method SW846 5030 Water MS
123-91- Dioxane BRL 1-91 200 EPA 624 16-May-08 17-May-08 8051244
994-05-8 Ter-amyl methyl ether BRL 1-911 20
755- Tert-Butanoll butyl alcohol BRL 1-91 200
67-B4- Acetone BRL 1-91 400
71-43- Benzene BRL 1-91 20
75-27-4 Bromodichloromethane BRL 1-91 20
75-25- Bromoform BRL 1-91 20
74-83- Bromomethane BRL 1-91 40
78-93- Butanone (MEK) BRL 1-91 200
56-23- Carbon tetrachloride BRL 1-91 20
108-90- Chlorobenzene BRL 1-91 20
75-00- Chloroethane BRL 1-91 40
676- Chloroform BRL 1-91 20
74-87- Chloromethane BRL 1-91 40
124-48- Dibromochloromethane BRL 1-91 20
95-50- Dichlorobenzene BRL 1-911 20
541-73- Dichlorobenzene BRL 1-91 20
106-46- Dichlorobenzene BRL 1-91 20
75-34- 1- Dichloroethane BRL 1-91 20
107-06- Dichloroethane BRL 1-91 20
75-35-4 1- Dichloroethene BRL 1-91 20
156-59 cis- Dichloroethene BRL 1-91 20
156-60- trans- Dichloroethene BRL 1-91 20
78-87- 2- Dichloropropane BRL 1-91 20
10061-01-5 cis- Dichloropropene BRL 1-91 20
10061-02-B trans- Dichloropropene BRL 1-91 20
100-41-4 Ethylbenzene 411 1-911 20
591-78-B BRL 200Hexanone (MBK) 1-91
1634-04 -4 Methyl tert-butyl ether BRL 1-91 20
108-10- Methyl- pentanone (MIBK) BRL 1-91 200
75-09- Methylene chloride BRL 1-91 200
100-42- Styrene BRL 1-91 20
79-34- 1 Tetrachloroethane BRL 1-91 20
127- 18-4 T etrachloroethene BRL 1-91 20
108-88- Toluene BRL 1-91 20
71-55 1- Trichloroethane BRL 1-91 20
79-00- 2- Trichloroethane BRL 1-91 20
79-01-B Trichloroethene BRL 1-91 20
759-4 Trichlorofluoromethane (Freon 11) BRL 1-91 20
75-01-4 Vinyl chloride BRL 1-91 20
179601-23-1 m Xylene 390 1-91 40
95-47 Xylene 82 1-91 20
Surrogate recoveries 460-00- Bromofluorobenzene 70- 130
2037-26- Toluene- 100 70- 130
17060-07-0 1 Dichloroethane- 111 70- 130
1868-53- Dibromofluoromethane 70- 130
Microextractable Organic Compounds
106-93-4 1 Dibromoethane (EDB) BRL 1-91 0100 EPA 504 15-May- 15-May-08 8051105
Semivolatile Organic Compounds by GCMS
This laboratory report is not valid without all autllOrized signature 011 the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page 5 of 25
Sam le Identification Client Pro ect Matrix Collection DateTime Received
MWshy2920-96- Ground Water 13-May-081030 14-May-
SA 78602shy
CAS No Analyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Semivolatie Organic Compounds by GCMS
Semi volatile Or anic Com ounds b EPA 625
Prepared by method SW846 3510C 50 EPA 625 16-May- 19-May-08 805121683-32- Acenaphthene BRL IJgl
208-96-8 Acenaphthylene BRL IJgl 50
62-53- BRL IJgll 50Aniline
120- 12- Anthracene BRL 1J91 50
103-33- AzobenzenefDiphenyldiazine BRL IJgl 50
92-87 - Benzidine BRL IJgl 50
56-55- Benzo (a) anthracene BRL 1J91 50
50-32 - Benzo (a) pyrene IJglBRL 50
205-99- Benzo (b) fluoranthene BRL IJgl 50
191-24- Benzo (g i) perylene BRL IJgl 50
50207-08- Benzo (k) fluoranthene BRL IJgl
65-85 Benzoic acid BRL 1J91 50
100-51-6 Benzyl alcohol 1J91BRL 50
50111-91- Bis(2-chloroethoxy)methane BRL 1J91
111-4-4 Bis(2-chloroethyl)ether BRL IJgl 50
501 08-60- Bis(2-chloroisopropyl)ether BRL IJgl
117-81- Bis(2-ethylhexyl)phthalate BRL 1J91 50
101-55- Bromophenyl phenyl ether BRL IJgl 50
5085-68- Butyl benzyl phthalate BRL IJgl
5086-74- Carbazole BRL IJgl
5059-50- C hloro-3-methylphenol BRL IJgl
106-47- Chloroaniline BRL IJgl 50
91-58- Chloronaphthalene IJglBRL 50
5095-57 - Chlorophenol BRL 1J91
507005-72- Chlorophenyl phenyl ether BRL IJgl
216-01- Chrysene tJ91BRL 50
5053-70- Dibenzo (a h) anthracene BRL IJgl
50132-64- Dibenzofuran BRL IJgl
95-50- Dichlorobenzene IJglBRL 50
541-73- 13- Dichlorobenzene BRL IJgl 50
106-46- Dichlorobenzene 1J91BRL 50
5091-94- 3 - Dichlorobenzidine BRL IJgl
120-83- Dichlorophenol BRL IJgl 50
84-66- Diethyl phthalate BRL IJgl 50
131-11- Dimethyl phthalate BRL IJgll 50
105-67- Dimethylphenol BRL 1J91 50
5084-74- Di-n- butyl phthalate BRL 1J91
534-52 - Dinitro-2-methylphenol BRL IJgl 50
51-28- Dinitrophenol IJglBRL 50
50121-14- Dinitrotoluene BRL 1J91
606-20- Dinitrotoluene IJglBRL 50
50117-84-0 Di-n-octyl phthalate BRL IJgl
206-44-0 Fluoranthene 1J91BRL 50
BRL 50
50 86-73- Fluorene IJgi
118-74- Hexachlorobenzene BRL 1J91
87-68- Hexachlorobutadiene 1J91BRL 50
5077-47-4 Hexachlorocyclopentadiene BRL IJgl
67-72- Hexachloroethane IJglBRL 50
50193-39- Indeno (1 3-cd) pyrene BRL IJgl
5078-59- Isophorone BRL IJgl
Tfls laboratory report is not valid without all authorized signature 011 the coverpage
Page 6 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Sam le Identification Client Pro ect Matrix Collection DateTime ReceivedMWshy
2920-96- Ground Water I3-May-081030 14-May-SA 78602shy
CAS No Analyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Semivolatile Organic Compounds by GCMS
Semi volatile Or anic Com ounds b EPA 625
Prepared by method SW846 3510C
91-57 -6 Methylnaphthalene 367 1-91 50 EPA 625 16-May- 19-May-08 8051216
95-48- Methylphenol BRL 1-91 50
108-39-4 3 amp 4-Methylphenol BRL I-gl 100 106-44shy91-20- Naphthalene 247 1-91 50
88-74-4 Nitroaniline BRL 1-91 50
99-09- Nitroaniline BRL 1-91 50
100-01-6 Nitroaniline BRL 1-91 50
98-95- Nitrobenzene BRL 1-91 50
88-75- Nitrophenol BRL 1-91 50
100-02- Nitrophenol BRL 1-91 50
62-75- Nitrosodimethylamine BRL 1-91 50
621-64- N- Nitrosodi-n-propylamine BRL 1-91 50
86-30-6 Nitrosodiphenylamine BRL 1-91 50
87 -86- Pentachlorophenol BRL 1-91 50
85-0- Phenanthrene BRL 1-91 50
108-95- Phenol BRL 1-91 50
129-00-0 Pyrene BRL 1-91 50
110-86- Pyridine BRL 1-91 50
120-82- 4- Trichlorobenzene BRL 1-91 50
95-95- 5- Trichlorophenol BRL 1-91 50
88-06- 6- T richlorophenol BRL 1-91 50
Surrogate recoveries
321-60- Fluorobipheny 30- 130
367- 12- Fuorophenol 15- 110
4165-60- Nitrobenzene- 30- 130
4165-62- Pheno- 15- 110
1718-51- Terpheny-d4 30- 130
118- 79- 6- Tribromophenol 15- 110
Semivolatile Organic Compounds by GC
Pol chlorinated Bi hen ls b EPA 608
Prepared by method SW846 3510C
12674- 11-2 Aroclor- 1016 BRL 1-91 0650 EPA 608 15- May- 16-May-08 8051106
11104-28-2 Aroclor-1221 BRL IJgl 0650
11141-16-5 Aroclor- 1232 BRL 1-91 0650
53469-21-9 Aroclor- 1242 BRL 1-91 0650
12672-29-6 Aroclor- 1248 BRL 1-91 0650
11097-69-1 Aroclor- 1254 BRL 1-91 0650
11096-82-5 Aroclor -1260 BRL 1-91 0650
37324-23-5 Aroclor-1262 BRL 1-91 0650
11100-14-4 Aroclor-1268 BRL IJgl 0650
Surrogate recoveries
2051-24- Decachlorobipheny (Sr) 105 30- 150
10386-84-2 4 DB-Octafluorobiphenyl (Sr) 30- 150
Extractable Petroleum Hydrocarbons
mgl EPA 1664 Rev A 15-May- 19-May-08 8051102Non-polar material (SGT- HEM)
Soluble Metals by EPA 2006000 Series Metbods
Field Filtered NA EPA 200 73005A 15- May- 15-May-08 8051192Filtration
Soluble Metals by EPA 200 Series Methods
7440-22-4 Silver BRL mgl 0002 EPA 200 21-May- 27- May-08 8051249
This laboratory report is IlOt mlid without (II authorized signature on the cover page
Reportble Detection Limit BRL = Below Reporting Limit Page 7 of 25
Sam le Identification MW-
Client Pro ect 2920-96shy
Matrix Ground Water
Collection DateTime 13-May-08 1030
Received 14-May-
SA 78602shy
CAS No A nalyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Soluble Metals by EPA 200 Series Methods
7440-38shy Arsenic 0468 mg1 0040 EPA 200 21-Mayshy 21-May-08 80511 50
7440-43shy Cadmium BRL mg1 0002 EPA 200 21-May-088051249
7440-47shy Chromium BRL mg1 0050 EPA 200 21-May-088051150
7440-50-8 Copper BRL mg1 0050
7439-89-6 Iron 184 mg1 0150
7439-97-6 Mercury BRL mg1 00020 EPA 245 17470A 21-May-088051152
7440-02-0 Nickel BRL mg1 0050 EPA 200 21-May-088051150
7439-92shy Lead 0011 mg1 0002 EPA 200 21-May-088051249
7440-36-0 Antimony 0003 mg1 0002
7782-49shy Selenium BRL mg1 0150 EPA 200 21-May-08 8051150
7440-66-6 Zinc 0186 mgl 0050
General Chemistry Parameters
Filtration Completed NA Varies 14-Mayshy 14-May-08 8051095
18540-29-9 Hexavalent Chromium (soluble) BRL HT2 mg1 125 SM3500CrDI796A 14-Mayshy 14-May-08 8051094 R01 2013 2016
57-12shy Cyanide (total) BRL mg1 0100 EPA 3354 19-Mayshy 19-May-088051374
7782-50shy Total Residual Chlorine BRL CIHT mg1 500 Hach 8167 14-Mayshy 14-May-08 8051049 R01 1900 2001
Total Suspended Solids 580 mg1 25 SM2540D 16-Mayshy 16-May-08 8051275
This lahomtOlY report is not valid without an authorized signature on the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page 8 of 25
Volatie Organic Compounds - Quality Control
Analyte( s)
Batch 8051244 - SW846 5030 Water MS
Blank 8051244-BLK1
Prepared 16-May-08 Analyzed 17-May-
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromochloromethane
1 Dichlorobenzene
1 Dichlorobenzene
1 Dichlorobenzene
1-Dichloroethane
1 Dichloroethane
1 1-Dichloroethene
cis- Dichloroethene
trans- 1 Dichloroethene
1 Dichloropropane
cis- 1 Dichloropropene
trans- 1 Dichloropropene
Ethylbenzene
Hexanone (MBK)
Methyl tert-butyl ether
Methyl- pentanone (MIBK)
Methylene chloride
Styrene
2- Tetrachloroethane
Tetrachloroethene
Toluene
1- Trichloroethane
2- Trichloroethane
Trichloroethene
Trichlorofluoromethane (Freon 11)
Vinyl chloride
p-Xylene
Xylene
Surrogate 4-Bromofluorobenzene Surrogate Toluene-
Surrogate 1 Dichloroethane-Surrogate Dibromofluoromethane
LCS B051244-BS1
Prepared 16-May-08 Analyzed 17 -May-
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Spike Source REC RPD
Result Flag Units RDL Level Result REC Limits RPD Limit
BRL gl 20
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl 10
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gll
BRL gi
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl 10
BRL gll
BRL gll 10
BRL gl 10
BRL gll
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
41 gl 50 70- 130 49 gl 50 70- 130 59 gl 50 119 70- 130 52 gl 50 105 70- 130
QC2 jgl 20 70- 130
18 jgl 20 70- 130
192 jgl 20 35- 155
18 jgl 20 45- 169
19 jgl 20 242
This laboratOlY repol1 is lot valid without 011 authorized sigllature 011 the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page 9 of 25
Volatie Organic Compounds - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051244 - SW846 5030 Water MS
LC5 8051244B51
Prepared 16-May-08 Analyzed 17-May-
Butanone (MEK) 10 QC2 gl 20 70- 130
Carbon tetrachloride 204 gl 20 102 70- 140
Chlorobenzene 18 gl 20 70- 130
Chloroethane 164 gl 20 14-230
Chloroform 18 gll 20 51- 138
Chloromethane 21 gl 20 106 273
Dibromochloromethane 18 gl 20 53- 149
1 Dichlorobenzene 20 gl 20 104 18- 190
1 Dichlorobenzene 19 gl 20 59- 156
1 A-Dichlorobenzene 18 gl 20 18- 190
1- Dichloroethane 19 gl 20 59- 155
1 Dichloroethane 19 gl 20 49- 155
1-Dichloroethene 16 gl 20 70- 130
cis- 1 Dichloroethene 17 gl 20 70- 130
trans- 1 Dichloroethene 16 gll 20 54- 156
1 Dichloropropane 18 gl 20 210
cis- Dichloropropene 17 gl 20 227
trans- 1 Dichloropropene 17 gl 20 17- 183
Ethylbenzene 19 gl 20 37- 162
Hexanone (MBK) 124 QC2 gl 20 70- 130
Methyl tert-butyl ether 19 gl 20 70- 130
Methylshy pentanone (MIBK) 17 gl 20 70- 130
Methylene chloride 16 gl 20 221
Styrene 17 gl 20 70- 130
1 Tetrachloroethane 194 gl 20 46- 157
Tetrachloroethene 15 gl 20 64- 148
Toluene 18 gl 20 70- 130
1- Trichloroethane 20 gl 20 100 52- 162
2- Trichloroethane 18 gl 20 52- 150
Trichloroethene 17 gl 20 71- 157
Trichlorofluoromethane (Freon 11) 19 gl 20 17- 181
Vinyl chloride 21 gl 20 106 251
p-Xylene 39 gl 40 70- 130
Xylene 20 gl 20 102 70- 130
Surrogate 4-Bromofluorobenzene Surrogate Toluene-
Surrogate 1 Dichloroethane-Surrogate Dibromofluoromethane
52 49 56
49
gl
gl
gl
gl
50 50 50
50
105
112 100
70- 130 70- 130 70- 130 70- 130
LC5 DUD (8051244-B5D1
Prepared 16-May-08 Analyzed 17-May-
Acetone QC2 gl 20 70- 130
Benzene 18 gl 20 70- 130
Bromodichloromethane 18 gl 200 35- 155
Bromoform 17 gl 20 45- 169
Bromomethane 18 gl 20 242
Butanone (MEK) 11 QC2 1-91 20 70- 130
Carbon tetrachloride 20 gl 20 100 70- 140
Chlorobenzene 17 gl 20 70- 130
Chloroethane 15 1-91 20 14-230
Chloroform 18 1-91 20 51- 138
This laboratory report is aot valid without a1 authorized sig1ature 01 the cover page
Reportble Detection Limit BRL = Below Reporting Limit Page 10 of25
Volatie Organic Compounds - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051244 - SW846 5030 Water MS
LCS Dup 18051244-BSD1
Prepared 16-May-08 Analyzed 17-May-
Chloromethane 18 1-91 20 273
Dibromochloromethane 174 1-91 20 53- 149
Dichlorobenzene 20 1-91 20 100 18- 190
Dichlorobenzene 18 1-91 20 59- 156
Dichlorobenzene 18 1-91 20 18- 190
Dichloroethane 18 1-91 20 59- 155
Dichloroethane 19 1-91 20 49- 155
Dichloroethene 16 1-91 20 70- 130
cis- Dichloroethene 16 1-91 20 70- 130
trans- Dichloroethene 15 1-91 20 54- 156
Dichloropropane 17 1-91 20 210
cis- Dichloropropene 164 IJgl 20 227
trans- 1 Dichloropropene 164 I-gl 20 17- 183
Etlwlbenzene 18 IJgl 20 37- 162
Hexanone (MBK) 124 QC2 IJgl 20 70- 130
Methyl tert-butyl ether 184 1J91 20 70- 130
Methyl- pentanone (MIBK) 17 IJgl 20 70- 130
Methylene chloride 16 IJgl 20 221
Styrene 16 IJgl 20 70- 130
2- Tetrachloroethane 19 IJgl 20 46- 157
Tetrachloroethene 15 IJgl 20 64- 148
Toluene 17 IJgl 20 70- 130
1- Trichloroethane 19 1-91 20 52- 162
2- Trichloroethane 16 IJgl 20 52- 150
Trichloroethene 15 IJgl 20 71- 157
Trichlorofluoromethane (Freon 11) 17 IJgl 20 17- 181
Vinyl chloride 19 IJglI 20 251
p-Xylene 37 1J91 40 70- 130
Xylene 20 IJgl 20 100 70- 130
Surrogate 4-Bromofluorobenzene 51 IJgl 50 104 70- 130
Surrogate Toluene- 4B gl 50 70- 130
Surrogate 1 0ichloroethane- 53 IJgl 50 106 70- 130 Surrogate Oibromofluoromethane 50 1J9i 50 102 70- 130
Matrix S ike B051244-MS1 Source SA7B629shy
Prepared 16-May-08 Analyzed 17-May-
Benzene 18 20 BRL 70- 130IJgl
Bromodichloromethane 19 IJgl 20 BRL 35- 155
Bromoform 18 IJgl 20 BRL 45- 169
Bromomethane 16 IJgl 20 BRL 242
Carbon tetrachloride 21 IJgl 20 BRL 106 70- 140
Chlorobenzene 18 IJgl 20 BRL 70- 130
Chloroethane 16 IJgl 20 BRL 14-230
Chloroform 18 IJgl 20 BRL 51- 138
Chloromethane 19 IJgl 20 BRL 273
Dibromochloromethane 17 IJgl 20 BRL 53- 149
1 Dichlorobenzene 22 IJgl 20 BRL 112 18- 190
1 Dichlorobenzene 22 IJgl 20 BRL 110 59-156
1 Dichlorobenzene 21 IJgl 20 BRL 109 18- 190
1- Dichloroethane 19 IJgl 20 BRL 59- 155
1 Dichloroethane 18 IJgl 20 BRL 49- 155
This laboratory report is 110t mUd without an authorized signature on the covel page
Reportble Detection Limit BRL = Below Reporting Limit Page It of25
Volatile Organic Compounds - Quality Control
p
Spike Source REC RPD
Result REC imits RPD LimitAnalyte(s) Result Flag Units RDL Level
Batch 8051244 - SW846 5030 Water MS
Matrix ike S051244-MS1 Source SA7B629shy
Prepared 16-May-08 Analyzed 17-Mayshy
17 20 BRL 70- 130 1- Dichloroethene IJgl
16 20 BRL 54- 156trans- 1 Dichloroethene IJgl
21020 BRL1 Dichloropropane 17 1J91
cis- 1 Dichloropropene 17 IJgl 20 BRL 227
17- 183trans- 1 Dichloropropene 184 1J91 20 BRL
20 20 BRL 103 37- 162Ethylbenzene IJgl
15 20 BRL 221Methylene chloride IJgl
20 BRL 46- 1572- Tetrachloroethane 19 1J91
20 BRL 64- 148Tetrachloroethene 18 1J91
BRL 70- 130Toluene 18 1J91 20
105 52-1621- Trichloroethane 211 IJgl 20 BRL
18 20 BRL 52- 1502- Trichloroethane IJgl
17 20 BRL 71- 157Trichloroethene 1J91
20 BRL 17- 181Trichloroluoromethane (Freon 11) 194 IJgl
20 BRL 103 251Vinyl chloride 20 IJgl
102 70- 130Surrogate 4-Bromofluorobenzene 50 IJgl 50 50 70- 130Surrogate Toluene- 49 1J91
56 50 112 70- 130Surrogate 1 Dichloroethane- IJgl
50 100 70- 130Surrogate Dibromofluoromethane 50 IJgl
Matrix S ike Du S051244-MSD1 Source SA7S629shy
Prepared 16-May-08 Analyzed 17-Mayshy
18 20 BRL 70- 130Benzene IJgl
18 20 BRL 35- 155Bromodichloromethane IJgl
17 20 BRL 45- 169Bromoform IJgl
20 BRL 242Bromomethane 17 IJgl
20 BRL 103 70- 140Carbon tetrachloride 20 IJgl
18 20 BRL 70- 130Chlorobenzene 1J91
14-230Chloroethane 16 IJgl 20 BRL
20 51- 138Chloroform 184 IJgl BRL
Chloromethane 19 1J91 20 BRL 273
18 20 BRL 53- 149Dibromochloromethane 1J91
20 BRL 117 18- 190Dichlorobenzene 234 IJgl
20 BRL 112 59- 156Dichlorobenzene 22 IJgl
BRL 108 18- 190Dichlorobenzene 21 1J91 20
20 59- 1551 Dichloroethane 19 IJgl BRL
18 20 BRL 49- 155Dichloroethane IJgl
16 20 BRL 70- 130Dichloroethene IJgl
20 BRL 54- 156trans- Dichloroethene 154 1J91
20 BRL 210Dichloropropane 17 IJgl
0420 BRL 227cis- Dichloropropene 17 IJgl
17- 183trans- Dichloropropene 17 1J91 20 BRL
BRL 37- 162Ethylbenzene 20 1J91 20 102
Methylene chloride 15 IJgl 20 BRL 221
20 BRL 46- 1572- Tetrachloroethane 192 IJgl
20 BRL 64- 148 04Tetrachloroethene 18 IJgl
BRL 70- 130Toluene 184 1J91 20
52- 1621- Trichloroethane 20 IJgl 20 BRL 104
17 20 BRL 52- 1502- Trichloroethane IJgl
17 20 BRL 71- 157Trichloroethene IJgl
20 BRL 17-181Trichlorofluoromethane (Freon 11) 19 IJgl
This laboratory report is IIOt valid without all authorized sigllllture 011 the cover page
Page 12 of25 Reportble Detection Limit BRL = Below Reporting Limit
Semivolatile Organic Compounds by GCMS - Quality Control
Analyte(s)
Batch 8051216 - SW846 3510C
Blank 8051216-BLK1
Prepared amp Analyzed 16-May-
Isophorone
Methylnaphthalene
Methylphenol
3 amp 4-Methylphenol
Naphthalene
Nitroaniline
Nitroaniline
Nitroaniline
Nitrobenzene
Nitrophenol
Nitrophenol
Nitrosodimethylamine
N- N itrosodi-n-pro pyla mine
N itrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Pyridine
1 24-Trichlorobenzene
24 5- Trichlorophenol
246- Trichlorophenol
Surrogate 2-Fuorobipheny Surrogate 2-Fuoropheno Surrogate Nitrobenzene-Surrogate PhenoshySurrogate Terpheny-d4 Surrogate 6- Tribromopheno
LCS B051216-BS1
Prepared amp Analyzed 16-May-
Acenaphthene
Acenaphthylene
Aniline
Anthracene
AzobenzenelDi phenyld lazine
Benzidine
Benzo (a) anthracene
Benzo (a) pyrene
Benzo (b) fluoranthene
Benzo (g i) perylene
Benzo (k) fluoranthene
Benzoic acid
Benzyl alcohol
B is(2-chloroethoxy)methane
B i s (2-ch loroethyl)eth e r
Bis(2-ch loroisopropyl) ether
B is(2-ethy Ih exyl) phtha late
Bromophenyl phenyl ether
Butyl benzyl phthalate
Carbazole
Spike Source REC RPD
Result Flag Units RDL Level Result REC Limits RPD Limit
BRL gl
BRL gl
BRL gl
BRL gl 10
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gll
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
370 gl 50 30- 130 40 gl 50 15- 110 39 gl 50 30- 130 43 gl 50 15- 110 36 gl 50 30- 130 40 gl 50 15- 110
41 gl 50 40- 140
43 gI 50 40- 140
41 gl 50 40- 140
38 gl 50 40- 140
45 gl 50 40- 140
49 gl 50 153
41 gl 50 40- 140
43 gl 50 40- 140
41 gl 50 40- 140
41 gll 50 40- 140
45 gl 50 40- 140
32 gl 50 12- 149
41 gl 50 40- 140
39 gl 50 40- 140
384 gl 50 40- 140
47 gl 50 40- 140
47 gl 50 40- 140
40 gl 50 40- 140
47 gI 50 40- 140
56 gI 50 112 200
This laboratory report is lIot valid witllOut a1l authorized sigllature 011 the coverpage
Reportble Detection Limit BRL = Below Reporting Limit Page 15 of25
Semivolatile Organic Compounds by GCMS - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051216 - SW846 3510C
LCS 8051216-BS1
Prepared amp Analyzed 16-Mayshy
50 30- 1304 -C hloro-3-methylphenol 42 IJgl
40- 140Chloroaniline 39 IJgl 50
Chloronaphthalene 37 IJgl 50 40- 140
Chlorophenol 37 IJgl 50 30- 130
50 40- 140
40- 140
Chlorophenyl phenyl ether 45 IJgl
Chrysene 43 IJgl 50
Dibenzo (a h) anthracene 43 IJgl 50 40- 140
Dibenzofuran IJgl38 50 40- 140
50 40- 1401 Dichlorobenzene 35 IJgl
40- 1401 Dichlorobenzene 264 IJgl 50
40- 1401 Dichlorobenzene 434 IJgl 50
58 50 116 40- 1403 - Dichlorobenzidine IJgl
50 30- 130
40- 140 24-Dichlorophenol 38 IJgl
Diethyl phthalate 484 IJgl 50
50 40- 140Dimethyl phthalate 464 IJgl
Dlmethylphenol 39 IJgl 50 30- 130
DI-n-butyl phthalate 44 IJgll 50 40- 140
30- 130 6-Di nitro- 2-methylphenol 38 1J91 50
30- 130Dinltrophenol 36 1J91 50
42 50 40- 14024-Dlnitrotoluene 1J91
Dlnitrotoluene 1J9141 50 40- 140
Di-n-octyl phthalate 52 IJgl 50 104 40- 140
40- 140Fluoranthene 40 IJgl 50
Fluorene 41 IJgl 50 40- 140
39 50 40- 140Hexachlorobenzene IJgl
50 40- 140Hexachlorobutadiene 40 IJgl
40- 140Hexach lorocyclopentad iene 294 IJgl 50
40 50 40- 140Hexachloroethane IJgl
42 50 40-140Indeno (1 3-cd) pyrene IJgl
50 40- 140Isophorone 40 IJgl
40- 140Methylnaphthalene 394 IJgl 50
40- 140Methylphenol 39 IJgl 50
40 10 50 40- 1403 amp 4-Methylphenol IJgl
37 50 40-140Naphthalene IJgl
50 40-140Nitroaniline 39 IJgl
Nitroaniline 51 IJgl 50 102 40- 140
48 50 40- 140Nltroaniline 1J91
50 40- 140Nitrobenzene 40 IJgl
30- 130Nitrophenol 36 IJgl 50
40 IJgl 50 30- 130Nitrophenol 40- 140Nitrosodimethylamine 32 1J91 50
50 40-140N- N itrosodi-n-propyla mine 46 IJgl
40- 140N itrosodi phenyla ml ne 44 IJgl 50
41 IJgl 50 30- 130Pentachlorophenol 40- 140Phenanthrene 38 IJgl 50
50 30- 130Phenol 38 IJgl
40- 140Pyrene 424 1J91 50
40- 140Pyridine 294 1J91 50
40- 14024- Trichlorobenzene 364 IJgl 50
This laboratory report is not mlid without an authorized signature 011 the cover page
Page 16 of25 Reportble Detection Limit BRL = Below Reporting Limit
Semivolatie Organic Compounds by GCMS - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
BMch 8051216 - SW846 3510C
LC5 8051216-851
Prepared amp Analyzed 16-Mayshy
24 5- Trichlorophenol 404 gl 50 30- 130
246- Trichlorophenol 42 gl 50 30- 130
Surrogate 2-Fluorobiphenyl 29 gl 50 30- 130
Surrogate 2-Fluorophenot 27 gl 50 15- 110
Surrogate Nitrobenzene- 30 gl 50 30- 130
Surrogate Phenol- 29 gl 50 15- 110
Surrogate Terpheny-d4 30 gl 50 30- 130
Surrogate 6- Tribromopheno 324 gl 50 15- 110
This laboratory report is lIot valid without all authorized sigllature 011 tlle cover page
Reportble Detection Limit BRL = Below Reporting Limit Page 17 of25
Semivolatie Organic Compounds by GC - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051106 - SW846 3510C
Blank S051106-BLK1
Prepared amp Analyzed 15-Mayshy
Aroclor- 1016 BRL gI 0200
Aroclor- 1016 (2C) BRL gI 0200
Aroclor- 1221 BRL gI 0200
Aroclor- 1221 (2C) BRL gI 0200
Aroclor- 1232 BRL gI 0200
Aroclor- 1232 (2Cj BRL gI 0200
Aroclor- 1242 BRL gI 0200
Aroclor-1242 (2C) BRL gI 0200
Aroclor- 1248 BRL gI 0200
Aroclor- 1248 (2C) BRL gI 0200
Aroclor- 1254 BRL gI 0200
Aroclor- 1254(2Cj BRL gI 0200
Aroclor- 1260 BRL gI 0200
Aroclor- 1260 (2C) BRL gI 0200
Aroclor- 1262 BRL gI 0200
Aroclor- 1262 (2C) BRL gI 0200
Aroclor-1268 BRL gI 0200
Aroclor- 1268 (2C) BRL gI 0200
Surrogate Decachlorobiphenyl (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0231 0224 0194 0191
gI
gI
gI
gI
0200 0200 0200 0200
116 112
30- 150 30- 150 30- 150 30- 150
LC5 8051106-B51
Prepared 15-May-08 Analyzed 16-May-08
Aroclor- 1016 265 gI 0200 250 106 50- 114
Aroclor- 1 016 (2C) 240 gI 0200 250 50- 114
Aroclor- 1260 0269 gI 0200 250 107 40- 127
Aroclor-1260 (2Cj 270 gI 0200 250 108 40- 127
Surrogate Decachlorobiphenyl (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0225 0224 0188 0183
gI
gI
gI
gI
0200 0200 0200 0200
113 112
30- 150 30- 150 30- 150 30- 150
LC5 DUD rS051106-B5D1
Prepared 15-May-08 Analyzed 16-Mayshy
Aroclor- 1016 262 gl 0200 250 105 50- 114
Aroclor-1 016 (2Cj 241 gI 0200 250 50- 114
Aroclor- 1260 277 gI 0200 250 111 40- 127
Aroclor- 1260(2Cj 0260 gI 0200 250 104 40- 127
Surrogate Decachlorobipheny (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0238 0218 0189 0181
gI
gI
gI
gI
0200 0200 0200 0200
119 109
30- 150 30- 150 30- 150 30- 150
This laboratory report is lot valid without (II authorized sigllature 01 the cover page
Page 18 of25 Reportable Detection Limit BRL = Below Reporting Limit
Extractable Petroleum Hydrocarbons - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051102 - SW846 3510C
Blank 8051102-BLK1
Prepared 15-May-08 Analyzed 19-Mayshy
Non-polar material (SGT- HEM) BRL m91
LC8 8051102-B81
Prepared 15-May-08 Analyzed 19-Mayshy
Non-polar material (SGT- HEM) 184 m91 21 81 904
This laboratory report is not valid without an authorized signature 011 the cover page
Page 19 of25 Reportable Detection Limit BRL = Below Reporting Limit
Soluble Metals by EPA 200 Series Methods - Quality Control
Analyte(s) Result Flag Units RDL
Spike
Level
Source
Result REC
REC
Limits RPD
RPD
Limit
Batch 8051150 - EPA 200 Series
Blank 8051150-BLK1
Prepared amp Analyzed 21-May-
Iron
Zinc
Selenium
Nickel
Chromium
Copper
Arsenic
BRL
BRL
BRL
BRL
BRL
BRL
BRL
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0150
0050
0150
0050
0050
0050
0040
LCS 8051150-BS1
Prepared amp Analyzed 21-May-
Selenium
Zinc
Iron
Nickel
Chromium
Arsenic
Copper
123
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0150
0050
0150
0050
0050
0040
0050
103
105
101
100
85- 115
85- 115
85- 115
85- 115
85- 115
85-115
85- 115
licate B051150-DUP1 Source SA7B602shy
Prepared amp Analyzed 21-May-
Iron
Zinc
Selenium
Nickel
Copper
Chromium
Arsenic
17
0162
BRL
0015
0017
BRL
0450
QR8
mgl
mgl
mgl
mgl
mgl
mgl
mgi
0150
0050
0150
0050
0050
0050
0040
184
0186
BRL
0014
0023
BRL
0468
Matrix S ike 8051150-MS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Iron
Selenium
Nickel
Zinc
Copper
Chromium
Arsenic
19 QM2 mgl
mgll
mgl
mgl
mgl
mgl
mgl
0150
0150
0050
0050
0050
0050
0040
125
184
BRL
0014
0186
0023
BRL
0468
104
105
102
70- 130
70- 130
70-130
70- 130
70- 130
70-130
70- 130
Post S ike 8051150-PS1 Source SA78602shy
Prepared amp Analyzed 21-May-
Zinc
Iron
Selenium
Nickel
Copper
Arsenic
Chromium
18 QM2
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0050
0150
0150
0050
0050
0040
0050
0186
184
BRL
0014
0023
0468
BRL
104
104
101
85- 115
85- 115
85- 115
85-115
85-115
85- 115
85-115
Batch 8051152 - EPA200SW7000 Series
Blank B051152-BLK1
Prepared amp Analyzed 21-May-
Mercury BRL mgl 00020
This laboratory report is IIOt valid witllOut all authorized sigllature 011 the coverpage
Page 20 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Soluble Metals by EPA 200 Series Methods - Quality Control
Analyte(s) Result Flag Units RDL
Spike
Level
Source
Result REC
REC
Limits RPD
RPD
Limit
Batch 8051152 - EPA200SW7000 Series
LCS B051152-BS1
Prepared amp Analyzed 21-May-
Mercury 00576 m91 00020 00500 115 85- 115
licate B051152-DUP1 Source SA78602-01
Prepared amp Analyzed 21-May-
Mercury BRL m91 00020 BRL
Matrix S ike 8051152-MS1 Source SA78602shy
Prepared amp Analyzed 21-May-
Mercury 00632 OM m91 00020 00500 BRL 126 75- 125
Post S ike 8051152-PS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Mercury 00624 OC1 m91 00020 00500 BRL 125 85- 115
Batch 8051249 - 2008No digestion
Blank 8051249-BLK1
Prepared amp Analyzed 21-May-
Lead
Antimony
Cadmium
Silver
BRL
BRL
BRL
BRL
m91
m91
m91
m91
0002
0002
0002
0002
LCS B051249-BS1
Prepared amp Analyzed 21-May-
Antimony
Lead
Silver
Cadmium
143
145 OC2
m91
m91
m91
m91
0050
0050
0050
0040
103
115
107
116
85- 115
85- 115
85- 115
85- 115
licate 8051249-DUP1 Source SA7B602shy
Prepared amp Analyzed 21- May-
Lead
Antimony
Cadmium
Silver
0009
0002
00005
00002
ORB
m91
m91
m91
m91
0002
0002
0002
0002
0011
0003
00005
00003
Matrix S ike 8051249-MS1 Source SA78602shy
Prepared amp Analyzed 21- May-
Lead
Antimony
Cadmium
Silver
142
m91
m91
m91
m91
0050
0050
0040
0050
0011
0003
00005
00003
111
101
114
102
70- 130
70-130
70c130
70- 130
Post S ike 8051249-PS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Antimony
Cadmium
Silver
38
OC2
m91
m91
m91
0050
0040
0050
125
0003
00005
00003
110
121
109
85- 115
85- 115
85- 115
This laboratory report is flOt valid IVithout all authorized signature 011 the cOIer page
Reportable Detection Limit BRL Below Reporting Limit Page 21 of 25
General Chemistry Parameters - Quality Control
Spike Source REC RPD
Analyte( s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051049 - General Preparation
Blank S051 049-BLK1
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
Blank S051049-BLK2
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
Blank S051 049-BLK3
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
LCS S051049-BS1
Prepared amp Analyzed 14-May-
Total Residual Chlorine 046 mgl 020 0500 90- 110
LCS S051049-BS2
Prepared amp Analyzed 14-May-
Total Residual Chlorine 047 mgl 020 0500 90- 110
LCS S051049-BS3
Prepared amp Analyzed 14-May-
Total Residual Chlorine 054 mgl 020 0500 108 90-110
licate B051049-DUP1 Source SA7S544shy
Prepared amp Analyzed 14-May-
Total Residual Chlorine 012 mgl 020 010
licate S051049-DUP2 Source SA7S602-01
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020 BRL
Matrix S ike 8051049-MS1 Source SA78544-01
Prepared amp Analyzed 14-May-
Total Residual Chlorine 065 mgl 020 0500 010 110 80- 120
Matrix S ike 8051049-MS2 Source SA7B602shy
Prepared amp Analyzed 14-May-
Total Residual Chlorine mgl 500 125 BRL 108 80- 120
Reference 8051 049-SRM1
Prepared amp Analyzed 14-May-
Total Residual Chlorine 100 mgl 020 0967 103 85-115
Batch 8051094 - General Preparation
Blank 8051094-BLK1
Prepared amp Analyzed 14 May-
Hexavalent Chromium (soluble) BRL mgl 005
Blank 8051 094-BLK2
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) BRL mgl 005
LCS 8051094-BS1
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) 054 mgl 005 90- 110
licate 8051094-DUP1 Source SA78602-01
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) BRL mgl 125 BRL
Thi laboratory report is not valid without all authorized sigllature 011 the cover page
Page 22 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Page 2
~~~~
B SU22ested Form
for Notice of Intent (N
OI) for the R
emediation G
eneral Permit
General site inform
ation Please provide the following inform
ation about the site
Facilitysite address
a) Name of faciltysite
Fonner S
peedway S
ervice Station
Location of facilitysite
Street
longitude 71
58 35 latitude 42 33 15
4471 181 E
ast Broadw
ayI Facility SIC
code (s) b) N
ame offacilitysite ow
ner T
own
AJJ R
ealty Inc G
ardner
Em
ail address of owner
State Z
ip C
ounty 01440
Worcester
Telephone no of facilitysite ow
ner 978- 632-0089
Fax no offacilitysite owner
Ow
ner is (check one) 1 Federal 2 S
tateTribal
3 Private
other 0 if so describe
Address of ow
ner (if different from site)
Street 207 H
igh Street T
own
State Z
ip G
ardner I C
ounty01440
Worcester
) Legal name of operator
Operator telephone no
Corporate E
nvironmental A
dvisors Inc 508-835- 8822
Oper
tor fax no
508-835-8812 M
Dziura
cea- inccom
I Operator em
ail O
perator contact name and title
Michael D
ziura Sr Env E
ngineer
Address of operator (if different from
owner)
Street 127 H
artwell Street
Tow
n State
West Boylston
Worcester
I County
d) Check yes or
for the following
I Has a prior N
PD
ES
permit exclusion been granted for the discharge Y
es No rg if yes num
ber
2 Has a prior N
PDE
S application (Form 1 amp
2C) ever been fied for the discharge Y
es N
o rg if yes date and tracking
3 Is the discharge a new discharge as defined by 40 C
FR 1222 Y
es rg No D
4 For sites in M
assachusetts is the discharge covered under the MA
Contingency Plan (M
CP) and exem
pt from state perm
itting Yes rg N
o D
Rem
ediation General Perm
it - Notice of Intent
f) Is the sitefacility covered by any other EP A
permit including
e) Is sitefacilty subject to any State permitting or other action w
hich is causing the generation of discharge Y
es rg No D
1 m
ulti-sector storm w
ater general permit Y
es D No rg
if Y
number
If yes please list
2 phase I or II construction storm w
ater general permit Y
es No rg
1 site identification assigned by the state ofNH
or MA
MA
DE
P ifY
number
2 permit or license assigned
Release T
racking Num
ber 2- 0707 3 individual N
PDE
S permit Y
es No rg ifY
number
3 state agency contact information nam
e location and telephone num
ber 4 any other w
ater quality related permit Y
es No rg ifY
number
MA
EP B
ureau of Waste Site C
leanup 627 Main Street W
orcester MA
2 Dischare inform
ation Please provide information about the discharge (attaching additional sheets as needed) includin
Describe the discharge activities for w
hich the ownerapplicant is seeking coverage
Dew
atering during excavation of approximately 1 000 cubic yards of petroleum
- impacted soil G
roundwater w
ill be extracted from the excavation and pum
ped into a 21 000shygallon frac tank for sedim
ent removal W
ater wil be treated w
ith granular activated carbon to remove petroleum
compounds prior to discharge to the local storm
water
drainage system A
pprox stormw
ater drainage outfall is depicted on Figure 4 attached
b) Provide the 1) N
umber of
2) What is the m
aximum
and average flow rate of discharge (in cubic feet per second W
s) Max flow
0 067 fesec follow
ing discharge
Average flow
0033 fesee Is m
aximum
flow a design value Y
es rg No D
information
points For average flow
include the units and appropriate notation if this value is a design value or estimate if not available
about each
discharge
3) Latitude and longitude of each discharge w
ithin 100 feet pt long 58 35 lat 42
33 15 pt2 long lat -
pt3 long _ lat shypt4long _ lat -
pt5 long lat
pt6long _ lat - pt7 long _ lat -
pt8long _ lat - etc
4) If hydrostatic testing total volume of the discharge (gals)
5) Is the discharge intennittent rg Or seasonal
Is discharge ongoing Yes
No rg
Discharge is tem
porary in nature and is only related to excavation activities (dewatering)
NA
c) Expected dates of discharge (m
mddyy) star
090109 end
100109
d) Please attach a line drawing or flow
schematic show
ing water flow
through the facility including See attached fi ures 4 amp
5
1 sources of intake water 2 contributing flow
fiom the operation
3 treatment units and 4 discharge points and receiving w
aters(s)
Rem
ediation General Perm
it - Notice of Intent
----
3 Contam
inant information In order to com
plete this section the applicant
il need to take a minim
um of one sam
ple of the untreated water and have it analyzed for all of the
parameters listed in A
ppendix III Historical data (i
data taken no more than 2 years prior to the effective date of the perm
it) may be used if obtained pursuant to i
Massachusetts regulations 310 C
MR
40 0000 the Massachusetts C
ontingency Plan (Chapter 21E ) ii N
ew H
ampshire s T
itle 50 RSA
485- A W
ater Pollution and Waste
Disposal or T
itle 50 RSA
485- C G
roundwater Protection A
ct or iii an EPA
pennit exclusion letter issued pursuant to 40 CFR
122 provided the data w
as analyzed with test
methods that m
eet the requirements of this perm
it Otherw
ise a new sam
ple shall be taken and analyzed
a) Based on the analysis of the sam
ple(s) of the untreated influent the applicant must check the box of the sub-categories that the potential discharge falls w
ithin
Gasoline O
nly V
OC
Only
Primarily M
etals U
rban Fill Sites C
ontaminated Sum
ps Mixed Contaminants
Aquifer T
esting
VO
C w
ith Other
Petroleum w
ith Other
Listed C
ontaminated
Contam
inated H
ydrostatic Testing of
Well D
evelopment or
Other O
ils) only C
ontaminants
Contam
inants Sites
Dredge C
ondensates PipelinesT
anks R
ehabilitation F
uel Oils (and
b) Based on the analysis of the untreated influent the applicant m
ust indicate whether each listed chem
ical is believed present or believed absent in the potential discharge A
ttach additional sheets as needed
PAR
AM
ET
ER
B
elieve B
elieve of
Type of
Analytical
Minim
um
Maxim
um daily value
Avg daily value
Absent
Present Sam
ples Sam
ple M
ethod L
evel (ML
) of
(1 min-
(eg grab) U
sed T
est Method
concentration m
ass concentration
mass
imum
) (m
ethod ) (ugI)
( ugI) (kgday)
(ugI) (kgday)
1 Total Suspended Solids
GR
A
SM 2540D
000
580 000 215
SW-846
GR
A
100 c 500
2 Total R
esidual 9012A
C
hlorine
3 Total Petroleum
G
RA
1664
000 600
12
Hydrocarbons
4 Cyanide
GR
A
9012A
cl0
c20S B
enzene G
RA
B
5030
6 Toluene
GR
A
5030 c20
7 Ethylbcnzene
GR
A
5030 411
8 (m
o) Xylenes
GR
A
5030 10
472
9 Total B
TE
X
GR
A
5030 883
04
BT
EX
= SU
IU of B
enzene Toluene
Ethylbenzene
total Xylenes
Rem
ediation General Perm
it - Notice of Intent
PAR
AM
ET
ER
B
elieve B
elieve of
Type of
Absent
Present Sam
ples S
ample (eg
(1 min-
grab)
imum
)
10 Ethylene
Dibrom
ide G
RA
B
(1 2- Dibrom
o-methane)
11 Methyl-tert-B
utyl G
RA
Ether (M
tBE
)
12 tert-
Butyl
Alcohol
GR
AB
(TB
A)
13 tert-A
myl
Methyl
GR
A
Ether (T
AM
E)
14 Naphthalene
GR
AB
15 Carbon T
etra-G
RA
chloride
16 1
Dichlorobenzene
GR
A
17 D
iehlorobenzene G
RA
GR
A18 1
Dichlorobenzene
19 1
Dich1oroethane
GR
A
20 1
Dichloroethane
GR
A
21 1
Dichloroethylene
GR
A
22 cis-D
ichloro-G
RA
B
ethylene
GR
A
(Methylene C
hloride)
23 D
ichloromethane
24 T
etrachloroethylene G
RA
B
Rem
ediation General Perm
it - Notice of Intent
Analytical
Minim
um
Maxim
um daily value
Avg daily value
Method
Level (M
L) of
Used
Test M
ethod concentration
mass
concentration m
ass
(method )
(ugI) ( ug)
(kgday) (ugI)
(kgday)
504 010
0 0
5030 05
020
5030 0200
5030 020
625 247
5030 020
5030 020
5030 05
020
5030 020
5030 020
5030 020
5030 05
020
5030 020
5030 10
0200
5030 020
PAR
AM
ET
ER
B
elieve B
elieve of
Type of
Absent
Present Sam
ples Sam
ple (e
(l min-
grab)
imum
)
25 1
1 Trichloroethane
GR
AB
26 1
2 Trichloroethane
GR
A
27 Trichloroethylene
GR
AB
28 Vinyl C
hloride G
RA
B
29 Acetone
GR
A
30 14 D
ioxane G
RA
B
31 Total Phenols
GR
AB
32 Pentachlorophenol
GR
AB
33 Total Phthalates 6
GR
AB
(phthalate esthers)
34 Bis (2-E
thylhexyl) G
RA
B
Phthalate (D
ishy(ethylhexyl) P
hthalate)
35 Total G
roup 1 G
RA
P
olycyclic Arom
atic H
ydrocarbons (PA
H)
a Benzo(a) A
nthracene G
RA
B
b Benzo(a) P
yrene G
RA
c Benzo(b )F
luoranthene G
RA
B
d Benzo(k) F
luoranthene G
RA
e Chrysene
GR
AB
The slim
of iijdividual phthalate compounds
Rem
ediation General Perm
it - Notice of Intent
Analytical
Minim
um L
evel M
aximum
daily value A
vg daiJy Value
Method Used
(ML) ofT est
(method )
Method
concentration m
ass concentration
mass
(ugI) (ugI)
(kgday) (ugl)
(kgday)
5030 20
5030 20
5030 20
5030 ~20
5030 400
5030 200
625 50
625 50
625 All phthalates are
BD
L see lab report
625 50
625 A
ll Group I P A
Hs
are BD
L
625 50
625 50
625 50
625 50
625 50
g
PAR
AM
ET
ER
B
elieve B
elieve of
Type of
Analytical
Minim
um
Maxim
um daily value
Average daily value
Absent
Present Sam
ples Sam
ple (e M
ethod Used
Level (M
L) of
(lmin -
grab) (m
ethod ) T
est Method
concentration m
ass concentration
mass
imum
) (ug1)
(ugl) (kgday)
(ugl) (kgday)
f Dibenzo(a
GR
AB
625
-(50
anthracene
Indeno(I 23-cd) G
RA
B
625 -(50
Pyrene
36 Total G
roup II G
RA
B
625 247
Polycyclic A
romatiC
H
ydrocarbons (pAR
)
h Acenaphthene
GR
AB
625
-(10
i Acenaphthylene
GR
A
625 -(50
j Anthracene
GR
A
625 -(50
k Benzo(ghi)
Perylene G
RA
B
625 -(50
I Fluoranthene G
RA
B
625 -(50
m F
luorene G
RA
B
625 -(50
n Naphthalene-
GR
AB
625
247
o Phenanthrene
GR
AB
625
-(50
p Pyrene
GR
AB
625
-(50
37 Total
POlychlorinated
GR
AB
608
065 -(0065
Biphenyls (PC
Bs)
38 Antim
ony G
RA
B
200 03
4Eshy
39 Arsenic
GR
AB
200
468
40 Cadm
ium
GR
AB
200
-( 0
41 Chrom
ium II
(1) G
RA
B
calculated calculated
-(5
42 Chrom
ium V
I G
RA
7196A
-( 125
NO
TE
S (1) Chrom
ium m
= T
otal Chrom
ium - H
exavalent Chrom
ium A
ccording to lab personnel the trivalent chromium
is calculated to be greater or equal to 5 ugI but less than 125 ugl Total
Chrom
ium w
as -(5 ugI and the Hexavalent C
hromium
was less than 125 ugl
Rem
ediation General Perm
it - Notice of Intent
--------
--------
-------
--------
---
PAR
AM
ET
ER
B
elieve B
elieve of
Type of
Analytical
Minim
um
Maxim
um daily value
Avg daily value
Absent
Present Sam
ples Sam
ple (e M
ethod L
evel (ML
) of grab)
Used
Test M
ethod concentration
mass
concentration m
ass(1 m
inshy
imum
) (m
ethod ) (ug1)
(ug1) (kgday)
(ug1) (kgday)
43 Copper
GR
A
200 (5
44 Lead G
RA
200
0001
45 Mercury
GR
A
7470A
(020
46 Nickel
GR
AB
200
(5
GR
AB
200
( 1547 Selenium
48 Silver G
RA
B
200 (0
49 Zinc
GR
A
200 18
0025
50 Iron G
RA
B
200 400
25
Other (describe)
c For discharges where m
etals are believed present please fill out the following
If yes which m
etals A
rsenic and Iron Step
I Do any of the m
etals in the influent have a reasonable potential to exceed the
etIluent limits in A
ppendix II (i the limits set at zero to five dilutions) Y
rg N D
Step 2 For any m
etals which have reasonable potential to exceed the A
ppendix III limits
Look up the lim
it calculated at the corresponding dilution factor in
calculate the dilution factor (DF) using the form
ula in Part I A 3 c) (step 2) of the N
O
Appendix IV
Do any of the m
etals in the influent have the potential to instructions or as determ
ined by the State prior to the submission of this N
OI
exceed the corresponding effuent lim
its in Appendix IV
(i is the
What is the dilution factor for applicable m
etals in1uent concentration above the lim
it set at the calculated dilution M
etals A
rsenic and Iron factor)
yrgND
If Y
es list which m
etals A
rsenic and Iron
DF
Rem
ediation General Pem
lit - Notice of Intent
4 Treatm
ent system inform
ation Please describe the treatment system
using separate sheets as necessary including
a) A description of the treatm
ent system including a schem
atic of the proposed or existing treatment system
S
ee Figures 4 and 5
Frac tank Air stripper
Oilw
ater separator Equalization tanks
Bag filter rg
GA
C filter rg
b) Identity each applicable
treatment unit (check alJ
that apply)
Chlorination
Dechlorination
Other (please describe)
c) Proposed average and maxim
um flow
rates (gallons per minute) for the discharge and the design flow
rate(s) (gallons per minute) ofthe treatm
ent system
Average flow
rate of discharge 15 G
PM
Maxim
um flow
rate oftreatment system
0 G
PM
Design flow
rate of treatment system
0 G
PM
d) A description of chem
ical additives being used or planned to be used (attach MSD
S sheets) Not A
pplicable
5 Receiving surface water(s) Please provide information about the receiving water (s) using separate sheets as necessary including
Identity the discharge pathway
I Direct
I Within facility
I Stonn drain rg I R
iverbrook I W
etlands _ I Other (describe)
Provide a narrative description ofthe discharge pathway including the nam
e(s) of the receiving waters
Discharge to catchbasin and stonnw
ater drainage system in E
ast Broadw
ay which discharges to M
ahoney Brook (S
ee Figure 4)
c) Attach a detailed m
ap(s) indicating the site location and location of the outfall to the receiving water
1 For multiple discharges num
ber the discharges sequentialJy 2 For indirect dischargers indicate the location of the discharge to the indirect conveyance and the discharge to surface w
ater T
he map should also include the location and distance to the nearest sanitary sew
er as well as the locus of nearby sensitive receptors (based on U
SGS topographical
mapping) such as surface w
aters drinking water supplies and w
etland areas d) Provide the state w
ater quality classification of the receiving water
e) Provide the reported or calculated seven day- ten year low flow
(7QlO
) of the receiving water Jcfs
Please attach any calculation sheets used to support stream flow
and dilution calculations See A
ttachment B
f) Is the receiving water a listed 303(d) w
ater quality impaired or lim
ited water Y
es 0 No rg
If yes for which polJutant(s) N
A
Is there a TM
DL
Yes 0
No rg If yes for w
hich pollutant(s) NA
Rem
ediation General Perm
it - Notice of Intent
6 Results of C
onsultation with Federal Services Please p
rovide the following information according to requirements of Par
lBA
and A
ppendices II and VII
a) Are any listed threatened or endangered species or designated critical habitat in proxim
ity to the discharge Yes 0
No rg
Has any consultation w
ith the federal services been completed Y
es 0 No rg
or is consultation underway Y
es 0 No rg
What w
ere the results of the consultation with the U
S Fish and Wildlife Service andor N
ational Marine Fisheries Service (check one) N
ot applicable
a nojeopardy opinion
or written concurrenceD
on a finding that the discharges are not likely to adversely affect any endangered species or critical habitat
b) Are any historic properties listed or eligible for listing on the N
ational Register of H
istoric Places located on the facilty or site or in proximity to the discharge
Yes D
No
Have any state or tribal historic preservation offcer been consulted in this determ
ination (Massachusetts only) Y
es O N
o
7 SU
DD
lemental inform
ation
Please provide any supplemental information Attach any analytical data used to support the application A
ttach any celtification(s) required by the general permit
Attachm
ent A - Figures
Figure I - Site Locus M
ap
Figure 2 - MassD
EP Site Scoring M
ap
Figure 3 - Aerial M
ap
Figure 4 - Proposed Soil Excavation A
rea Map
Figure 5 - T
reatment S
ystem Line D
iagram
Attachm
ent B - D
ilution factor Calculations
Attachment C - L
aboratory Analytical R
eport Groundw
ater
Rem
ediation General Perm
it - Notice of 1ntenl
=-
including the following
8 Signature Requirements
The N
otice ofIntent must be signed by the operator in accordance w
ith the signatory requirements of 40 C
FR Section 122
certification
J certif under penalty of law that this docum
ent and all attachments w
ere prepared under my direction or supervision in accordance w
ith a system
designed to assure that qualifed personnel properly gather and evaluate the information subm
itted Based on m
y inquiry of the person or persons who
manage the system
or those persons directly responsible for gathering the information I certif that t
he information submitted
is to the best of m
y
knowledge and belief true accurate and com
plete J certif that I am aw
are that there are signifcant penalties for submitting false inform
ation including
the possibilty of fine and imprisonm
ent for knowing violations
FacilitySite Name
Form
er Speedw
ay Service S
tation 181 East B
roadwav G
ardner MA
01440
Operator signature
Title
Michael 1 D
ziura Sf Env E
ngineer
Date
4150- q
Rem
ediation General Perm
it - Notice of Intent
-
D- 0
0 0
il (J tu
Bw
o(0 -I
NJW
gQb
J(JZc o c
rou a -10
0 J 6shy
a 0
I-tDC
aJ Qj
E aJshy
ro ro ro
~~~ ~~~~- -- - _ - -_ - ~~~ ~~~~ ~~~ - - _- _- -- -- p __(
MA DEP - Bureau of Waste Site CleanupSITE NME Site S aP 5 MiFlII Former Speeway Station _-II181 Eat Broaday b b d IS I i I GARDNER MA 0144 v ri) i P f f 1 me- 1 5ylmI I L shy J --I 423315n 715835e SiteLocation y o oCop1odQcn Ofof W-_ l
1 1 I
r
r
iBARBER HILL
A c
Cf1 f o s
0
5
Roads Uned Acss Divd Mar Roed Conntor Street Track 1 EPA Sola Source Aquilar FEMA 100yaar iloodplain 0 c Puc Watar SLo GrunSelaceNon Corrty 0
Bounars lOwn Couny DE Region Tian Powerln Ine Aqedut ApprOld Zona2 tNPA Sue Wster Supp Zone A bStZ F--shy--rle
8os Mat Sub SUeor Porenrial Inermtent Man lvo8 Ste Dfm Hyro1apy Wmer FeatllePLio Suleee Wat S H-- L otlMds FrslSaltN-ES WeIMd Habat L
Potentia Prdutiv AqlJlers ModHig Yield Proteoted Opn Space ACC nIL c= Non-Potential Drng Water Sollce AIea ModumHi Yo1d ll DEP Pormrd SoidWes1 FsiIi6s cnifud Verne Pools f0
1I2 KIWUmR$ MtL
January 30 2004 SCALE 1 15000
-
LE
GE
ND
APX PROPER BONDA
- APPROXOiSPO SIT BOUNDA
-GR
OU
ND
WA
TE F1 D
IRE
cnON
SCA
LE
30 60 FE
(APR
OX
CORPORATE ENVIRONMENTAL
)i
AD
VISO
RS
INC
SC
AS SH
OW
D
R B
Y K
HA
EL
DA
TE
10407
JOB
NO
2920-96
AERIAL MAP
FO
RM
ER
SP
EE
DW
AY
ST
AT
ION
FlGURE -3
181 EA
BR
OA
AY
GA
NE
R fo
age 1 ot 1Streamflow Statistics Report
Streamstats Ungaged Site Report Date Wed Dec 31 2008 124908 Site Location Massachusetts NAD83 Latitude 425545 (42 3316) NAD83 Longitude -719758 (-71 58 32) NAD27 Latitude 425545 (423316) NAD27 Longitude - 9763 (-71 58 34) Drainage Area 502 mi2
IPeak Flow Basin Characteristics 1100 Statewide Low Flow (S02 mi2)
Regression Equation Valid Rang
I Min II Max1 Value III Parameter Drainage Area (square miles) 161 149
Mean Basin Slope from 250K DEM (percent) 032 24
Stratified Drift per Stream Length (square mile per mile) 129
Massachusetts Region (dimensionless)
Streamflow Statistics
gO-Percent Prediction Interval Prediction Error
MaximumStatistic Flow (ft s) (percent) Minimum
I D50 IIII 11 1811 II 24511 993
I D60 II 35511 2011 II 03611 35111 2411 II 041 I 201I D70 24111 2611 II 03811 151I D75 11 2811 II 0911 3761I D80 981I D85 1 I 3211 II o6311
1 I 3711 II 0441 1 2 2911 D90 11 4611 II 02411 15511 D95I D98 04511 6011 II 01511 11
I D99 03411 6511 II ol1ll 1021
5011 II 02611 11I M7D2Y 1111 3311 II odl 3 541
I AUGD50
IIIIIIIIIIIIIIIIIIIIII 0311 7111 II 0088411 0981I M7Dl0Y
1010
12312008httpstreamstatsagscrusgsgovgisimgReportsFlowStatsReport3494 - 2008123112498
Dilution Factor Calculation Former Speedway Service Station 181 East Broadway Gardner Ma
DF=(Od+Os)Od
DF = Dilution factor
Od = Max flow rate of discharge in cubic feet per second Os = receiving water flow in cubic feet per seconds 7010 flow rate Mahoney Brook 7010 = min flow for seven consecutive days with a recurrence interval of 10 years
7010 flow based on data obtained from USGS Steamflow Statistics Report Data attached
067
Semivolatile Organic Compounds by GCMS - Quality Control
Analyte( s)
Batch 8051216 - SW846 3510C
Blank 8051216BLK1)
Prepared amp Analyzed 16May-
Acenaphthene
Acenaphthylene
Aniline
Anthracene
AzobenzenelDi phenyld iazi ne
Benzidine
Benzo (a) anthracene
Benzo (a) pyrene
Benzo (b) fiuoranthene
Benzo (g i) perylene
Benzo (k) fiuoranthene
Benzoic acid
Benzyl alcohol
Bis(2-ch loroethoxy) methane
Bis(2-ch loroethyl)ether
Bis(2-ch loroi sopropyl)ether
Bis(2ethylhexyl) phthalate
Bromophenyl phenyl ether
Butyl benzyl phthalate
Carbazole
Ch loro-3-methyl phenol
Chloroaniline
Chloronaphthalene
Chlorophenol
Chlorophenyl phenyl ether
Chrysene
Dibenzo (a h) anthracene
Dibenzofuran
Dichlorobenzene
Dichlorobenzene
14- Dichlorobenzene
3 - Dichlorobenzidine
24-Dichlorophenol
Diethyl phthalate
Dimethyl phthalate
24- Dimethylphenol
Din-butyl phthalate
Dinitro-2-methylphenol
Dinitrophenol
Dinitrotoluene
Dinitrotoluene
Di-noctyl phthalate
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopehtadiene
Hexachloroethane
Indeno (1 cd) pyrene
Spike Source REC RPD
Result Flag Units RDL Level Result REC Limits RPD Limit
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gl
BRL gI
BRL gl
BRL gl
BRL gl
BRL gI
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gll
BRL gl
BRL gll
BRL gl
BRL gl
BRL gI
BRL gI
BRL gI
BRL gl
BRL gI
BRL gI
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gI
BRL gI
BRL gl
This laboratory report is IlOt valid without all authorized sigllature 011 the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page t4 of25
Volatie Organic Compounds - Quality Control
p (
Spike Source REC RPD
RDL Level Result REC Limits RPD Limit Analyte(s) Result Flag Units
Batch 8051244 - SW846 5030 Water MS
Matrix S ike Du 8051244-MSD1 Source SA78629shy
Prepared 16-May-08 Analyzed 17-May-BRL 106 251
Vinyl chloride 21 gl 20
101 70- 130 Surrogate 4-Bromofluorobenzene 50 gl 50
70- 13049 gl 50 111 70- 130
Surrogate Toluene-Surrogate 1 Dichloroethane- 55 gl 50
50 70- 130494 glSurrogate Dibromofluoromethane
Microextractable Organic Compounds - Quality Control
Spike Source REC RPD
Flag Units RDL Level Result REC Limits RPD Limit Analyte(s) Result
Batch 8051105 - SW846 3510C
Blank 8051105-BLK
Prepared amp Analyzed 15-May-
BRL gl 01001 Dibromoethane (ED B)
LCS 8051105-BS1
Prepared amp Analyzed 15-Mayshy50- 1500770 gl 0100 100
licate 8051105-DUP1 Source SA7B583shy
Prepared amp Analyzed 15-May-
BRL gl 0100 BRL
1 Dibromoethane (EDB)
1 Dibromoethane (EDB)
This laborntOlY report is not valid without an authorized signature 011 the cover page
Page 13 of2S Reportable Detection Limit BRL = Below Reporting Limit
Sam le Identification Client Pro ect Matrix Collection DateTime ReceivedMWshy
2920-96- Ground Water 13-May-081030 14-May-SA 78602shy
CAS No Analyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Volatile Organic Compounds
Volatile Or anic Com ounds b GCMS
Prepared by method SW846 5030 Water MS
123-91- Dioxane BRL 1-91 200 EPA 624 16-May-08 17-May-08 8051244
994-05-8 Ter-amyl methyl ether BRL 1-911 20
755- Tert-Butanoll butyl alcohol BRL 1-91 200
67-B4- Acetone BRL 1-91 400
71-43- Benzene BRL 1-91 20
75-27-4 Bromodichloromethane BRL 1-91 20
75-25- Bromoform BRL 1-91 20
74-83- Bromomethane BRL 1-91 40
78-93- Butanone (MEK) BRL 1-91 200
56-23- Carbon tetrachloride BRL 1-91 20
108-90- Chlorobenzene BRL 1-91 20
75-00- Chloroethane BRL 1-91 40
676- Chloroform BRL 1-91 20
74-87- Chloromethane BRL 1-91 40
124-48- Dibromochloromethane BRL 1-91 20
95-50- Dichlorobenzene BRL 1-911 20
541-73- Dichlorobenzene BRL 1-91 20
106-46- Dichlorobenzene BRL 1-91 20
75-34- 1- Dichloroethane BRL 1-91 20
107-06- Dichloroethane BRL 1-91 20
75-35-4 1- Dichloroethene BRL 1-91 20
156-59 cis- Dichloroethene BRL 1-91 20
156-60- trans- Dichloroethene BRL 1-91 20
78-87- 2- Dichloropropane BRL 1-91 20
10061-01-5 cis- Dichloropropene BRL 1-91 20
10061-02-B trans- Dichloropropene BRL 1-91 20
100-41-4 Ethylbenzene 411 1-911 20
591-78-B BRL 200Hexanone (MBK) 1-91
1634-04 -4 Methyl tert-butyl ether BRL 1-91 20
108-10- Methyl- pentanone (MIBK) BRL 1-91 200
75-09- Methylene chloride BRL 1-91 200
100-42- Styrene BRL 1-91 20
79-34- 1 Tetrachloroethane BRL 1-91 20
127- 18-4 T etrachloroethene BRL 1-91 20
108-88- Toluene BRL 1-91 20
71-55 1- Trichloroethane BRL 1-91 20
79-00- 2- Trichloroethane BRL 1-91 20
79-01-B Trichloroethene BRL 1-91 20
759-4 Trichlorofluoromethane (Freon 11) BRL 1-91 20
75-01-4 Vinyl chloride BRL 1-91 20
179601-23-1 m Xylene 390 1-91 40
95-47 Xylene 82 1-91 20
Surrogate recoveries 460-00- Bromofluorobenzene 70- 130
2037-26- Toluene- 100 70- 130
17060-07-0 1 Dichloroethane- 111 70- 130
1868-53- Dibromofluoromethane 70- 130
Microextractable Organic Compounds
106-93-4 1 Dibromoethane (EDB) BRL 1-91 0100 EPA 504 15-May- 15-May-08 8051105
Semivolatile Organic Compounds by GCMS
This laboratory report is not valid without all autllOrized signature 011 the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page 5 of 25
Sam le Identification Client Pro ect Matrix Collection DateTime Received
MWshy2920-96- Ground Water 13-May-081030 14-May-
SA 78602shy
CAS No Analyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Semivolatie Organic Compounds by GCMS
Semi volatile Or anic Com ounds b EPA 625
Prepared by method SW846 3510C 50 EPA 625 16-May- 19-May-08 805121683-32- Acenaphthene BRL IJgl
208-96-8 Acenaphthylene BRL IJgl 50
62-53- BRL IJgll 50Aniline
120- 12- Anthracene BRL 1J91 50
103-33- AzobenzenefDiphenyldiazine BRL IJgl 50
92-87 - Benzidine BRL IJgl 50
56-55- Benzo (a) anthracene BRL 1J91 50
50-32 - Benzo (a) pyrene IJglBRL 50
205-99- Benzo (b) fluoranthene BRL IJgl 50
191-24- Benzo (g i) perylene BRL IJgl 50
50207-08- Benzo (k) fluoranthene BRL IJgl
65-85 Benzoic acid BRL 1J91 50
100-51-6 Benzyl alcohol 1J91BRL 50
50111-91- Bis(2-chloroethoxy)methane BRL 1J91
111-4-4 Bis(2-chloroethyl)ether BRL IJgl 50
501 08-60- Bis(2-chloroisopropyl)ether BRL IJgl
117-81- Bis(2-ethylhexyl)phthalate BRL 1J91 50
101-55- Bromophenyl phenyl ether BRL IJgl 50
5085-68- Butyl benzyl phthalate BRL IJgl
5086-74- Carbazole BRL IJgl
5059-50- C hloro-3-methylphenol BRL IJgl
106-47- Chloroaniline BRL IJgl 50
91-58- Chloronaphthalene IJglBRL 50
5095-57 - Chlorophenol BRL 1J91
507005-72- Chlorophenyl phenyl ether BRL IJgl
216-01- Chrysene tJ91BRL 50
5053-70- Dibenzo (a h) anthracene BRL IJgl
50132-64- Dibenzofuran BRL IJgl
95-50- Dichlorobenzene IJglBRL 50
541-73- 13- Dichlorobenzene BRL IJgl 50
106-46- Dichlorobenzene 1J91BRL 50
5091-94- 3 - Dichlorobenzidine BRL IJgl
120-83- Dichlorophenol BRL IJgl 50
84-66- Diethyl phthalate BRL IJgl 50
131-11- Dimethyl phthalate BRL IJgll 50
105-67- Dimethylphenol BRL 1J91 50
5084-74- Di-n- butyl phthalate BRL 1J91
534-52 - Dinitro-2-methylphenol BRL IJgl 50
51-28- Dinitrophenol IJglBRL 50
50121-14- Dinitrotoluene BRL 1J91
606-20- Dinitrotoluene IJglBRL 50
50117-84-0 Di-n-octyl phthalate BRL IJgl
206-44-0 Fluoranthene 1J91BRL 50
BRL 50
50 86-73- Fluorene IJgi
118-74- Hexachlorobenzene BRL 1J91
87-68- Hexachlorobutadiene 1J91BRL 50
5077-47-4 Hexachlorocyclopentadiene BRL IJgl
67-72- Hexachloroethane IJglBRL 50
50193-39- Indeno (1 3-cd) pyrene BRL IJgl
5078-59- Isophorone BRL IJgl
Tfls laboratory report is not valid without all authorized signature 011 the coverpage
Page 6 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Sam le Identification Client Pro ect Matrix Collection DateTime ReceivedMWshy
2920-96- Ground Water I3-May-081030 14-May-SA 78602shy
CAS No Analyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Semivolatile Organic Compounds by GCMS
Semi volatile Or anic Com ounds b EPA 625
Prepared by method SW846 3510C
91-57 -6 Methylnaphthalene 367 1-91 50 EPA 625 16-May- 19-May-08 8051216
95-48- Methylphenol BRL 1-91 50
108-39-4 3 amp 4-Methylphenol BRL I-gl 100 106-44shy91-20- Naphthalene 247 1-91 50
88-74-4 Nitroaniline BRL 1-91 50
99-09- Nitroaniline BRL 1-91 50
100-01-6 Nitroaniline BRL 1-91 50
98-95- Nitrobenzene BRL 1-91 50
88-75- Nitrophenol BRL 1-91 50
100-02- Nitrophenol BRL 1-91 50
62-75- Nitrosodimethylamine BRL 1-91 50
621-64- N- Nitrosodi-n-propylamine BRL 1-91 50
86-30-6 Nitrosodiphenylamine BRL 1-91 50
87 -86- Pentachlorophenol BRL 1-91 50
85-0- Phenanthrene BRL 1-91 50
108-95- Phenol BRL 1-91 50
129-00-0 Pyrene BRL 1-91 50
110-86- Pyridine BRL 1-91 50
120-82- 4- Trichlorobenzene BRL 1-91 50
95-95- 5- Trichlorophenol BRL 1-91 50
88-06- 6- T richlorophenol BRL 1-91 50
Surrogate recoveries
321-60- Fluorobipheny 30- 130
367- 12- Fuorophenol 15- 110
4165-60- Nitrobenzene- 30- 130
4165-62- Pheno- 15- 110
1718-51- Terpheny-d4 30- 130
118- 79- 6- Tribromophenol 15- 110
Semivolatile Organic Compounds by GC
Pol chlorinated Bi hen ls b EPA 608
Prepared by method SW846 3510C
12674- 11-2 Aroclor- 1016 BRL 1-91 0650 EPA 608 15- May- 16-May-08 8051106
11104-28-2 Aroclor-1221 BRL IJgl 0650
11141-16-5 Aroclor- 1232 BRL 1-91 0650
53469-21-9 Aroclor- 1242 BRL 1-91 0650
12672-29-6 Aroclor- 1248 BRL 1-91 0650
11097-69-1 Aroclor- 1254 BRL 1-91 0650
11096-82-5 Aroclor -1260 BRL 1-91 0650
37324-23-5 Aroclor-1262 BRL 1-91 0650
11100-14-4 Aroclor-1268 BRL IJgl 0650
Surrogate recoveries
2051-24- Decachlorobipheny (Sr) 105 30- 150
10386-84-2 4 DB-Octafluorobiphenyl (Sr) 30- 150
Extractable Petroleum Hydrocarbons
mgl EPA 1664 Rev A 15-May- 19-May-08 8051102Non-polar material (SGT- HEM)
Soluble Metals by EPA 2006000 Series Metbods
Field Filtered NA EPA 200 73005A 15- May- 15-May-08 8051192Filtration
Soluble Metals by EPA 200 Series Methods
7440-22-4 Silver BRL mgl 0002 EPA 200 21-May- 27- May-08 8051249
This laboratory report is IlOt mlid without (II authorized signature on the cover page
Reportble Detection Limit BRL = Below Reporting Limit Page 7 of 25
Sam le Identification MW-
Client Pro ect 2920-96shy
Matrix Ground Water
Collection DateTime 13-May-08 1030
Received 14-May-
SA 78602shy
CAS No A nalyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Soluble Metals by EPA 200 Series Methods
7440-38shy Arsenic 0468 mg1 0040 EPA 200 21-Mayshy 21-May-08 80511 50
7440-43shy Cadmium BRL mg1 0002 EPA 200 21-May-088051249
7440-47shy Chromium BRL mg1 0050 EPA 200 21-May-088051150
7440-50-8 Copper BRL mg1 0050
7439-89-6 Iron 184 mg1 0150
7439-97-6 Mercury BRL mg1 00020 EPA 245 17470A 21-May-088051152
7440-02-0 Nickel BRL mg1 0050 EPA 200 21-May-088051150
7439-92shy Lead 0011 mg1 0002 EPA 200 21-May-088051249
7440-36-0 Antimony 0003 mg1 0002
7782-49shy Selenium BRL mg1 0150 EPA 200 21-May-08 8051150
7440-66-6 Zinc 0186 mgl 0050
General Chemistry Parameters
Filtration Completed NA Varies 14-Mayshy 14-May-08 8051095
18540-29-9 Hexavalent Chromium (soluble) BRL HT2 mg1 125 SM3500CrDI796A 14-Mayshy 14-May-08 8051094 R01 2013 2016
57-12shy Cyanide (total) BRL mg1 0100 EPA 3354 19-Mayshy 19-May-088051374
7782-50shy Total Residual Chlorine BRL CIHT mg1 500 Hach 8167 14-Mayshy 14-May-08 8051049 R01 1900 2001
Total Suspended Solids 580 mg1 25 SM2540D 16-Mayshy 16-May-08 8051275
This lahomtOlY report is not valid without an authorized signature on the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page 8 of 25
Volatie Organic Compounds - Quality Control
Analyte( s)
Batch 8051244 - SW846 5030 Water MS
Blank 8051244-BLK1
Prepared 16-May-08 Analyzed 17-May-
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromochloromethane
1 Dichlorobenzene
1 Dichlorobenzene
1 Dichlorobenzene
1-Dichloroethane
1 Dichloroethane
1 1-Dichloroethene
cis- Dichloroethene
trans- 1 Dichloroethene
1 Dichloropropane
cis- 1 Dichloropropene
trans- 1 Dichloropropene
Ethylbenzene
Hexanone (MBK)
Methyl tert-butyl ether
Methyl- pentanone (MIBK)
Methylene chloride
Styrene
2- Tetrachloroethane
Tetrachloroethene
Toluene
1- Trichloroethane
2- Trichloroethane
Trichloroethene
Trichlorofluoromethane (Freon 11)
Vinyl chloride
p-Xylene
Xylene
Surrogate 4-Bromofluorobenzene Surrogate Toluene-
Surrogate 1 Dichloroethane-Surrogate Dibromofluoromethane
LCS B051244-BS1
Prepared 16-May-08 Analyzed 17 -May-
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Spike Source REC RPD
Result Flag Units RDL Level Result REC Limits RPD Limit
BRL gl 20
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl 10
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gll
BRL gi
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl 10
BRL gll
BRL gll 10
BRL gl 10
BRL gll
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
41 gl 50 70- 130 49 gl 50 70- 130 59 gl 50 119 70- 130 52 gl 50 105 70- 130
QC2 jgl 20 70- 130
18 jgl 20 70- 130
192 jgl 20 35- 155
18 jgl 20 45- 169
19 jgl 20 242
This laboratOlY repol1 is lot valid without 011 authorized sigllature 011 the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page 9 of 25
Volatie Organic Compounds - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051244 - SW846 5030 Water MS
LC5 8051244B51
Prepared 16-May-08 Analyzed 17-May-
Butanone (MEK) 10 QC2 gl 20 70- 130
Carbon tetrachloride 204 gl 20 102 70- 140
Chlorobenzene 18 gl 20 70- 130
Chloroethane 164 gl 20 14-230
Chloroform 18 gll 20 51- 138
Chloromethane 21 gl 20 106 273
Dibromochloromethane 18 gl 20 53- 149
1 Dichlorobenzene 20 gl 20 104 18- 190
1 Dichlorobenzene 19 gl 20 59- 156
1 A-Dichlorobenzene 18 gl 20 18- 190
1- Dichloroethane 19 gl 20 59- 155
1 Dichloroethane 19 gl 20 49- 155
1-Dichloroethene 16 gl 20 70- 130
cis- 1 Dichloroethene 17 gl 20 70- 130
trans- 1 Dichloroethene 16 gll 20 54- 156
1 Dichloropropane 18 gl 20 210
cis- Dichloropropene 17 gl 20 227
trans- 1 Dichloropropene 17 gl 20 17- 183
Ethylbenzene 19 gl 20 37- 162
Hexanone (MBK) 124 QC2 gl 20 70- 130
Methyl tert-butyl ether 19 gl 20 70- 130
Methylshy pentanone (MIBK) 17 gl 20 70- 130
Methylene chloride 16 gl 20 221
Styrene 17 gl 20 70- 130
1 Tetrachloroethane 194 gl 20 46- 157
Tetrachloroethene 15 gl 20 64- 148
Toluene 18 gl 20 70- 130
1- Trichloroethane 20 gl 20 100 52- 162
2- Trichloroethane 18 gl 20 52- 150
Trichloroethene 17 gl 20 71- 157
Trichlorofluoromethane (Freon 11) 19 gl 20 17- 181
Vinyl chloride 21 gl 20 106 251
p-Xylene 39 gl 40 70- 130
Xylene 20 gl 20 102 70- 130
Surrogate 4-Bromofluorobenzene Surrogate Toluene-
Surrogate 1 Dichloroethane-Surrogate Dibromofluoromethane
52 49 56
49
gl
gl
gl
gl
50 50 50
50
105
112 100
70- 130 70- 130 70- 130 70- 130
LC5 DUD (8051244-B5D1
Prepared 16-May-08 Analyzed 17-May-
Acetone QC2 gl 20 70- 130
Benzene 18 gl 20 70- 130
Bromodichloromethane 18 gl 200 35- 155
Bromoform 17 gl 20 45- 169
Bromomethane 18 gl 20 242
Butanone (MEK) 11 QC2 1-91 20 70- 130
Carbon tetrachloride 20 gl 20 100 70- 140
Chlorobenzene 17 gl 20 70- 130
Chloroethane 15 1-91 20 14-230
Chloroform 18 1-91 20 51- 138
This laboratory report is aot valid without a1 authorized sig1ature 01 the cover page
Reportble Detection Limit BRL = Below Reporting Limit Page 10 of25
Volatie Organic Compounds - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051244 - SW846 5030 Water MS
LCS Dup 18051244-BSD1
Prepared 16-May-08 Analyzed 17-May-
Chloromethane 18 1-91 20 273
Dibromochloromethane 174 1-91 20 53- 149
Dichlorobenzene 20 1-91 20 100 18- 190
Dichlorobenzene 18 1-91 20 59- 156
Dichlorobenzene 18 1-91 20 18- 190
Dichloroethane 18 1-91 20 59- 155
Dichloroethane 19 1-91 20 49- 155
Dichloroethene 16 1-91 20 70- 130
cis- Dichloroethene 16 1-91 20 70- 130
trans- Dichloroethene 15 1-91 20 54- 156
Dichloropropane 17 1-91 20 210
cis- Dichloropropene 164 IJgl 20 227
trans- 1 Dichloropropene 164 I-gl 20 17- 183
Etlwlbenzene 18 IJgl 20 37- 162
Hexanone (MBK) 124 QC2 IJgl 20 70- 130
Methyl tert-butyl ether 184 1J91 20 70- 130
Methyl- pentanone (MIBK) 17 IJgl 20 70- 130
Methylene chloride 16 IJgl 20 221
Styrene 16 IJgl 20 70- 130
2- Tetrachloroethane 19 IJgl 20 46- 157
Tetrachloroethene 15 IJgl 20 64- 148
Toluene 17 IJgl 20 70- 130
1- Trichloroethane 19 1-91 20 52- 162
2- Trichloroethane 16 IJgl 20 52- 150
Trichloroethene 15 IJgl 20 71- 157
Trichlorofluoromethane (Freon 11) 17 IJgl 20 17- 181
Vinyl chloride 19 IJglI 20 251
p-Xylene 37 1J91 40 70- 130
Xylene 20 IJgl 20 100 70- 130
Surrogate 4-Bromofluorobenzene 51 IJgl 50 104 70- 130
Surrogate Toluene- 4B gl 50 70- 130
Surrogate 1 0ichloroethane- 53 IJgl 50 106 70- 130 Surrogate Oibromofluoromethane 50 1J9i 50 102 70- 130
Matrix S ike B051244-MS1 Source SA7B629shy
Prepared 16-May-08 Analyzed 17-May-
Benzene 18 20 BRL 70- 130IJgl
Bromodichloromethane 19 IJgl 20 BRL 35- 155
Bromoform 18 IJgl 20 BRL 45- 169
Bromomethane 16 IJgl 20 BRL 242
Carbon tetrachloride 21 IJgl 20 BRL 106 70- 140
Chlorobenzene 18 IJgl 20 BRL 70- 130
Chloroethane 16 IJgl 20 BRL 14-230
Chloroform 18 IJgl 20 BRL 51- 138
Chloromethane 19 IJgl 20 BRL 273
Dibromochloromethane 17 IJgl 20 BRL 53- 149
1 Dichlorobenzene 22 IJgl 20 BRL 112 18- 190
1 Dichlorobenzene 22 IJgl 20 BRL 110 59-156
1 Dichlorobenzene 21 IJgl 20 BRL 109 18- 190
1- Dichloroethane 19 IJgl 20 BRL 59- 155
1 Dichloroethane 18 IJgl 20 BRL 49- 155
This laboratory report is 110t mUd without an authorized signature on the covel page
Reportble Detection Limit BRL = Below Reporting Limit Page It of25
Volatile Organic Compounds - Quality Control
p
Spike Source REC RPD
Result REC imits RPD LimitAnalyte(s) Result Flag Units RDL Level
Batch 8051244 - SW846 5030 Water MS
Matrix ike S051244-MS1 Source SA7B629shy
Prepared 16-May-08 Analyzed 17-Mayshy
17 20 BRL 70- 130 1- Dichloroethene IJgl
16 20 BRL 54- 156trans- 1 Dichloroethene IJgl
21020 BRL1 Dichloropropane 17 1J91
cis- 1 Dichloropropene 17 IJgl 20 BRL 227
17- 183trans- 1 Dichloropropene 184 1J91 20 BRL
20 20 BRL 103 37- 162Ethylbenzene IJgl
15 20 BRL 221Methylene chloride IJgl
20 BRL 46- 1572- Tetrachloroethane 19 1J91
20 BRL 64- 148Tetrachloroethene 18 1J91
BRL 70- 130Toluene 18 1J91 20
105 52-1621- Trichloroethane 211 IJgl 20 BRL
18 20 BRL 52- 1502- Trichloroethane IJgl
17 20 BRL 71- 157Trichloroethene 1J91
20 BRL 17- 181Trichloroluoromethane (Freon 11) 194 IJgl
20 BRL 103 251Vinyl chloride 20 IJgl
102 70- 130Surrogate 4-Bromofluorobenzene 50 IJgl 50 50 70- 130Surrogate Toluene- 49 1J91
56 50 112 70- 130Surrogate 1 Dichloroethane- IJgl
50 100 70- 130Surrogate Dibromofluoromethane 50 IJgl
Matrix S ike Du S051244-MSD1 Source SA7S629shy
Prepared 16-May-08 Analyzed 17-Mayshy
18 20 BRL 70- 130Benzene IJgl
18 20 BRL 35- 155Bromodichloromethane IJgl
17 20 BRL 45- 169Bromoform IJgl
20 BRL 242Bromomethane 17 IJgl
20 BRL 103 70- 140Carbon tetrachloride 20 IJgl
18 20 BRL 70- 130Chlorobenzene 1J91
14-230Chloroethane 16 IJgl 20 BRL
20 51- 138Chloroform 184 IJgl BRL
Chloromethane 19 1J91 20 BRL 273
18 20 BRL 53- 149Dibromochloromethane 1J91
20 BRL 117 18- 190Dichlorobenzene 234 IJgl
20 BRL 112 59- 156Dichlorobenzene 22 IJgl
BRL 108 18- 190Dichlorobenzene 21 1J91 20
20 59- 1551 Dichloroethane 19 IJgl BRL
18 20 BRL 49- 155Dichloroethane IJgl
16 20 BRL 70- 130Dichloroethene IJgl
20 BRL 54- 156trans- Dichloroethene 154 1J91
20 BRL 210Dichloropropane 17 IJgl
0420 BRL 227cis- Dichloropropene 17 IJgl
17- 183trans- Dichloropropene 17 1J91 20 BRL
BRL 37- 162Ethylbenzene 20 1J91 20 102
Methylene chloride 15 IJgl 20 BRL 221
20 BRL 46- 1572- Tetrachloroethane 192 IJgl
20 BRL 64- 148 04Tetrachloroethene 18 IJgl
BRL 70- 130Toluene 184 1J91 20
52- 1621- Trichloroethane 20 IJgl 20 BRL 104
17 20 BRL 52- 1502- Trichloroethane IJgl
17 20 BRL 71- 157Trichloroethene IJgl
20 BRL 17-181Trichlorofluoromethane (Freon 11) 19 IJgl
This laboratory report is IIOt valid without all authorized sigllllture 011 the cover page
Page 12 of25 Reportble Detection Limit BRL = Below Reporting Limit
Semivolatile Organic Compounds by GCMS - Quality Control
Analyte(s)
Batch 8051216 - SW846 3510C
Blank 8051216-BLK1
Prepared amp Analyzed 16-May-
Isophorone
Methylnaphthalene
Methylphenol
3 amp 4-Methylphenol
Naphthalene
Nitroaniline
Nitroaniline
Nitroaniline
Nitrobenzene
Nitrophenol
Nitrophenol
Nitrosodimethylamine
N- N itrosodi-n-pro pyla mine
N itrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Pyridine
1 24-Trichlorobenzene
24 5- Trichlorophenol
246- Trichlorophenol
Surrogate 2-Fuorobipheny Surrogate 2-Fuoropheno Surrogate Nitrobenzene-Surrogate PhenoshySurrogate Terpheny-d4 Surrogate 6- Tribromopheno
LCS B051216-BS1
Prepared amp Analyzed 16-May-
Acenaphthene
Acenaphthylene
Aniline
Anthracene
AzobenzenelDi phenyld lazine
Benzidine
Benzo (a) anthracene
Benzo (a) pyrene
Benzo (b) fluoranthene
Benzo (g i) perylene
Benzo (k) fluoranthene
Benzoic acid
Benzyl alcohol
B is(2-chloroethoxy)methane
B i s (2-ch loroethyl)eth e r
Bis(2-ch loroisopropyl) ether
B is(2-ethy Ih exyl) phtha late
Bromophenyl phenyl ether
Butyl benzyl phthalate
Carbazole
Spike Source REC RPD
Result Flag Units RDL Level Result REC Limits RPD Limit
BRL gl
BRL gl
BRL gl
BRL gl 10
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gll
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
370 gl 50 30- 130 40 gl 50 15- 110 39 gl 50 30- 130 43 gl 50 15- 110 36 gl 50 30- 130 40 gl 50 15- 110
41 gl 50 40- 140
43 gI 50 40- 140
41 gl 50 40- 140
38 gl 50 40- 140
45 gl 50 40- 140
49 gl 50 153
41 gl 50 40- 140
43 gl 50 40- 140
41 gl 50 40- 140
41 gll 50 40- 140
45 gl 50 40- 140
32 gl 50 12- 149
41 gl 50 40- 140
39 gl 50 40- 140
384 gl 50 40- 140
47 gl 50 40- 140
47 gl 50 40- 140
40 gl 50 40- 140
47 gI 50 40- 140
56 gI 50 112 200
This laboratory report is lIot valid witllOut a1l authorized sigllature 011 the coverpage
Reportble Detection Limit BRL = Below Reporting Limit Page 15 of25
Semivolatile Organic Compounds by GCMS - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051216 - SW846 3510C
LCS 8051216-BS1
Prepared amp Analyzed 16-Mayshy
50 30- 1304 -C hloro-3-methylphenol 42 IJgl
40- 140Chloroaniline 39 IJgl 50
Chloronaphthalene 37 IJgl 50 40- 140
Chlorophenol 37 IJgl 50 30- 130
50 40- 140
40- 140
Chlorophenyl phenyl ether 45 IJgl
Chrysene 43 IJgl 50
Dibenzo (a h) anthracene 43 IJgl 50 40- 140
Dibenzofuran IJgl38 50 40- 140
50 40- 1401 Dichlorobenzene 35 IJgl
40- 1401 Dichlorobenzene 264 IJgl 50
40- 1401 Dichlorobenzene 434 IJgl 50
58 50 116 40- 1403 - Dichlorobenzidine IJgl
50 30- 130
40- 140 24-Dichlorophenol 38 IJgl
Diethyl phthalate 484 IJgl 50
50 40- 140Dimethyl phthalate 464 IJgl
Dlmethylphenol 39 IJgl 50 30- 130
DI-n-butyl phthalate 44 IJgll 50 40- 140
30- 130 6-Di nitro- 2-methylphenol 38 1J91 50
30- 130Dinltrophenol 36 1J91 50
42 50 40- 14024-Dlnitrotoluene 1J91
Dlnitrotoluene 1J9141 50 40- 140
Di-n-octyl phthalate 52 IJgl 50 104 40- 140
40- 140Fluoranthene 40 IJgl 50
Fluorene 41 IJgl 50 40- 140
39 50 40- 140Hexachlorobenzene IJgl
50 40- 140Hexachlorobutadiene 40 IJgl
40- 140Hexach lorocyclopentad iene 294 IJgl 50
40 50 40- 140Hexachloroethane IJgl
42 50 40-140Indeno (1 3-cd) pyrene IJgl
50 40- 140Isophorone 40 IJgl
40- 140Methylnaphthalene 394 IJgl 50
40- 140Methylphenol 39 IJgl 50
40 10 50 40- 1403 amp 4-Methylphenol IJgl
37 50 40-140Naphthalene IJgl
50 40-140Nitroaniline 39 IJgl
Nitroaniline 51 IJgl 50 102 40- 140
48 50 40- 140Nltroaniline 1J91
50 40- 140Nitrobenzene 40 IJgl
30- 130Nitrophenol 36 IJgl 50
40 IJgl 50 30- 130Nitrophenol 40- 140Nitrosodimethylamine 32 1J91 50
50 40-140N- N itrosodi-n-propyla mine 46 IJgl
40- 140N itrosodi phenyla ml ne 44 IJgl 50
41 IJgl 50 30- 130Pentachlorophenol 40- 140Phenanthrene 38 IJgl 50
50 30- 130Phenol 38 IJgl
40- 140Pyrene 424 1J91 50
40- 140Pyridine 294 1J91 50
40- 14024- Trichlorobenzene 364 IJgl 50
This laboratory report is not mlid without an authorized signature 011 the cover page
Page 16 of25 Reportble Detection Limit BRL = Below Reporting Limit
Semivolatie Organic Compounds by GCMS - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
BMch 8051216 - SW846 3510C
LC5 8051216-851
Prepared amp Analyzed 16-Mayshy
24 5- Trichlorophenol 404 gl 50 30- 130
246- Trichlorophenol 42 gl 50 30- 130
Surrogate 2-Fluorobiphenyl 29 gl 50 30- 130
Surrogate 2-Fluorophenot 27 gl 50 15- 110
Surrogate Nitrobenzene- 30 gl 50 30- 130
Surrogate Phenol- 29 gl 50 15- 110
Surrogate Terpheny-d4 30 gl 50 30- 130
Surrogate 6- Tribromopheno 324 gl 50 15- 110
This laboratory report is lIot valid without all authorized sigllature 011 tlle cover page
Reportble Detection Limit BRL = Below Reporting Limit Page 17 of25
Semivolatie Organic Compounds by GC - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051106 - SW846 3510C
Blank S051106-BLK1
Prepared amp Analyzed 15-Mayshy
Aroclor- 1016 BRL gI 0200
Aroclor- 1016 (2C) BRL gI 0200
Aroclor- 1221 BRL gI 0200
Aroclor- 1221 (2C) BRL gI 0200
Aroclor- 1232 BRL gI 0200
Aroclor- 1232 (2Cj BRL gI 0200
Aroclor- 1242 BRL gI 0200
Aroclor-1242 (2C) BRL gI 0200
Aroclor- 1248 BRL gI 0200
Aroclor- 1248 (2C) BRL gI 0200
Aroclor- 1254 BRL gI 0200
Aroclor- 1254(2Cj BRL gI 0200
Aroclor- 1260 BRL gI 0200
Aroclor- 1260 (2C) BRL gI 0200
Aroclor- 1262 BRL gI 0200
Aroclor- 1262 (2C) BRL gI 0200
Aroclor-1268 BRL gI 0200
Aroclor- 1268 (2C) BRL gI 0200
Surrogate Decachlorobiphenyl (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0231 0224 0194 0191
gI
gI
gI
gI
0200 0200 0200 0200
116 112
30- 150 30- 150 30- 150 30- 150
LC5 8051106-B51
Prepared 15-May-08 Analyzed 16-May-08
Aroclor- 1016 265 gI 0200 250 106 50- 114
Aroclor- 1 016 (2C) 240 gI 0200 250 50- 114
Aroclor- 1260 0269 gI 0200 250 107 40- 127
Aroclor-1260 (2Cj 270 gI 0200 250 108 40- 127
Surrogate Decachlorobiphenyl (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0225 0224 0188 0183
gI
gI
gI
gI
0200 0200 0200 0200
113 112
30- 150 30- 150 30- 150 30- 150
LC5 DUD rS051106-B5D1
Prepared 15-May-08 Analyzed 16-Mayshy
Aroclor- 1016 262 gl 0200 250 105 50- 114
Aroclor-1 016 (2Cj 241 gI 0200 250 50- 114
Aroclor- 1260 277 gI 0200 250 111 40- 127
Aroclor- 1260(2Cj 0260 gI 0200 250 104 40- 127
Surrogate Decachlorobipheny (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0238 0218 0189 0181
gI
gI
gI
gI
0200 0200 0200 0200
119 109
30- 150 30- 150 30- 150 30- 150
This laboratory report is lot valid without (II authorized sigllature 01 the cover page
Page 18 of25 Reportable Detection Limit BRL = Below Reporting Limit
Extractable Petroleum Hydrocarbons - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051102 - SW846 3510C
Blank 8051102-BLK1
Prepared 15-May-08 Analyzed 19-Mayshy
Non-polar material (SGT- HEM) BRL m91
LC8 8051102-B81
Prepared 15-May-08 Analyzed 19-Mayshy
Non-polar material (SGT- HEM) 184 m91 21 81 904
This laboratory report is not valid without an authorized signature 011 the cover page
Page 19 of25 Reportable Detection Limit BRL = Below Reporting Limit
Soluble Metals by EPA 200 Series Methods - Quality Control
Analyte(s) Result Flag Units RDL
Spike
Level
Source
Result REC
REC
Limits RPD
RPD
Limit
Batch 8051150 - EPA 200 Series
Blank 8051150-BLK1
Prepared amp Analyzed 21-May-
Iron
Zinc
Selenium
Nickel
Chromium
Copper
Arsenic
BRL
BRL
BRL
BRL
BRL
BRL
BRL
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0150
0050
0150
0050
0050
0050
0040
LCS 8051150-BS1
Prepared amp Analyzed 21-May-
Selenium
Zinc
Iron
Nickel
Chromium
Arsenic
Copper
123
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0150
0050
0150
0050
0050
0040
0050
103
105
101
100
85- 115
85- 115
85- 115
85- 115
85- 115
85-115
85- 115
licate B051150-DUP1 Source SA7B602shy
Prepared amp Analyzed 21-May-
Iron
Zinc
Selenium
Nickel
Copper
Chromium
Arsenic
17
0162
BRL
0015
0017
BRL
0450
QR8
mgl
mgl
mgl
mgl
mgl
mgl
mgi
0150
0050
0150
0050
0050
0050
0040
184
0186
BRL
0014
0023
BRL
0468
Matrix S ike 8051150-MS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Iron
Selenium
Nickel
Zinc
Copper
Chromium
Arsenic
19 QM2 mgl
mgll
mgl
mgl
mgl
mgl
mgl
0150
0150
0050
0050
0050
0050
0040
125
184
BRL
0014
0186
0023
BRL
0468
104
105
102
70- 130
70- 130
70-130
70- 130
70- 130
70-130
70- 130
Post S ike 8051150-PS1 Source SA78602shy
Prepared amp Analyzed 21-May-
Zinc
Iron
Selenium
Nickel
Copper
Arsenic
Chromium
18 QM2
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0050
0150
0150
0050
0050
0040
0050
0186
184
BRL
0014
0023
0468
BRL
104
104
101
85- 115
85- 115
85- 115
85-115
85-115
85- 115
85-115
Batch 8051152 - EPA200SW7000 Series
Blank B051152-BLK1
Prepared amp Analyzed 21-May-
Mercury BRL mgl 00020
This laboratory report is IIOt valid witllOut all authorized sigllature 011 the coverpage
Page 20 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Soluble Metals by EPA 200 Series Methods - Quality Control
Analyte(s) Result Flag Units RDL
Spike
Level
Source
Result REC
REC
Limits RPD
RPD
Limit
Batch 8051152 - EPA200SW7000 Series
LCS B051152-BS1
Prepared amp Analyzed 21-May-
Mercury 00576 m91 00020 00500 115 85- 115
licate B051152-DUP1 Source SA78602-01
Prepared amp Analyzed 21-May-
Mercury BRL m91 00020 BRL
Matrix S ike 8051152-MS1 Source SA78602shy
Prepared amp Analyzed 21-May-
Mercury 00632 OM m91 00020 00500 BRL 126 75- 125
Post S ike 8051152-PS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Mercury 00624 OC1 m91 00020 00500 BRL 125 85- 115
Batch 8051249 - 2008No digestion
Blank 8051249-BLK1
Prepared amp Analyzed 21-May-
Lead
Antimony
Cadmium
Silver
BRL
BRL
BRL
BRL
m91
m91
m91
m91
0002
0002
0002
0002
LCS B051249-BS1
Prepared amp Analyzed 21-May-
Antimony
Lead
Silver
Cadmium
143
145 OC2
m91
m91
m91
m91
0050
0050
0050
0040
103
115
107
116
85- 115
85- 115
85- 115
85- 115
licate 8051249-DUP1 Source SA7B602shy
Prepared amp Analyzed 21- May-
Lead
Antimony
Cadmium
Silver
0009
0002
00005
00002
ORB
m91
m91
m91
m91
0002
0002
0002
0002
0011
0003
00005
00003
Matrix S ike 8051249-MS1 Source SA78602shy
Prepared amp Analyzed 21- May-
Lead
Antimony
Cadmium
Silver
142
m91
m91
m91
m91
0050
0050
0040
0050
0011
0003
00005
00003
111
101
114
102
70- 130
70-130
70c130
70- 130
Post S ike 8051249-PS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Antimony
Cadmium
Silver
38
OC2
m91
m91
m91
0050
0040
0050
125
0003
00005
00003
110
121
109
85- 115
85- 115
85- 115
This laboratory report is flOt valid IVithout all authorized signature 011 the cOIer page
Reportable Detection Limit BRL Below Reporting Limit Page 21 of 25
General Chemistry Parameters - Quality Control
Spike Source REC RPD
Analyte( s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051049 - General Preparation
Blank S051 049-BLK1
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
Blank S051049-BLK2
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
Blank S051 049-BLK3
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
LCS S051049-BS1
Prepared amp Analyzed 14-May-
Total Residual Chlorine 046 mgl 020 0500 90- 110
LCS S051049-BS2
Prepared amp Analyzed 14-May-
Total Residual Chlorine 047 mgl 020 0500 90- 110
LCS S051049-BS3
Prepared amp Analyzed 14-May-
Total Residual Chlorine 054 mgl 020 0500 108 90-110
licate B051049-DUP1 Source SA7S544shy
Prepared amp Analyzed 14-May-
Total Residual Chlorine 012 mgl 020 010
licate S051049-DUP2 Source SA7S602-01
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020 BRL
Matrix S ike 8051049-MS1 Source SA78544-01
Prepared amp Analyzed 14-May-
Total Residual Chlorine 065 mgl 020 0500 010 110 80- 120
Matrix S ike 8051049-MS2 Source SA7B602shy
Prepared amp Analyzed 14-May-
Total Residual Chlorine mgl 500 125 BRL 108 80- 120
Reference 8051 049-SRM1
Prepared amp Analyzed 14-May-
Total Residual Chlorine 100 mgl 020 0967 103 85-115
Batch 8051094 - General Preparation
Blank 8051094-BLK1
Prepared amp Analyzed 14 May-
Hexavalent Chromium (soluble) BRL mgl 005
Blank 8051 094-BLK2
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) BRL mgl 005
LCS 8051094-BS1
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) 054 mgl 005 90- 110
licate 8051094-DUP1 Source SA78602-01
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) BRL mgl 125 BRL
Thi laboratory report is not valid without all authorized sigllature 011 the cover page
Page 22 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Page 3
f) Is the sitefacility covered by any other EP A
permit including
e) Is sitefacilty subject to any State permitting or other action w
hich is causing the generation of discharge Y
es rg No D
1 m
ulti-sector storm w
ater general permit Y
es D No rg
if Y
number
If yes please list
2 phase I or II construction storm w
ater general permit Y
es No rg
1 site identification assigned by the state ofNH
or MA
MA
DE
P ifY
number
2 permit or license assigned
Release T
racking Num
ber 2- 0707 3 individual N
PDE
S permit Y
es No rg ifY
number
3 state agency contact information nam
e location and telephone num
ber 4 any other w
ater quality related permit Y
es No rg ifY
number
MA
EP B
ureau of Waste Site C
leanup 627 Main Street W
orcester MA
2 Dischare inform
ation Please provide information about the discharge (attaching additional sheets as needed) includin
Describe the discharge activities for w
hich the ownerapplicant is seeking coverage
Dew
atering during excavation of approximately 1 000 cubic yards of petroleum
- impacted soil G
roundwater w
ill be extracted from the excavation and pum
ped into a 21 000shygallon frac tank for sedim
ent removal W
ater wil be treated w
ith granular activated carbon to remove petroleum
compounds prior to discharge to the local storm
water
drainage system A
pprox stormw
ater drainage outfall is depicted on Figure 4 attached
b) Provide the 1) N
umber of
2) What is the m
aximum
and average flow rate of discharge (in cubic feet per second W
s) Max flow
0 067 fesec follow
ing discharge
Average flow
0033 fesee Is m
aximum
flow a design value Y
es rg No D
information
points For average flow
include the units and appropriate notation if this value is a design value or estimate if not available
about each
discharge
3) Latitude and longitude of each discharge w
ithin 100 feet pt long 58 35 lat 42
33 15 pt2 long lat -
pt3 long _ lat shypt4long _ lat -
pt5 long lat
pt6long _ lat - pt7 long _ lat -
pt8long _ lat - etc
4) If hydrostatic testing total volume of the discharge (gals)
5) Is the discharge intennittent rg Or seasonal
Is discharge ongoing Yes
No rg
Discharge is tem
porary in nature and is only related to excavation activities (dewatering)
NA
c) Expected dates of discharge (m
mddyy) star
090109 end
100109
d) Please attach a line drawing or flow
schematic show
ing water flow
through the facility including See attached fi ures 4 amp
5
1 sources of intake water 2 contributing flow
fiom the operation
3 treatment units and 4 discharge points and receiving w
aters(s)
Rem
ediation General Perm
it - Notice of Intent
----
3 Contam
inant information In order to com
plete this section the applicant
il need to take a minim
um of one sam
ple of the untreated water and have it analyzed for all of the
parameters listed in A
ppendix III Historical data (i
data taken no more than 2 years prior to the effective date of the perm
it) may be used if obtained pursuant to i
Massachusetts regulations 310 C
MR
40 0000 the Massachusetts C
ontingency Plan (Chapter 21E ) ii N
ew H
ampshire s T
itle 50 RSA
485- A W
ater Pollution and Waste
Disposal or T
itle 50 RSA
485- C G
roundwater Protection A
ct or iii an EPA
pennit exclusion letter issued pursuant to 40 CFR
122 provided the data w
as analyzed with test
methods that m
eet the requirements of this perm
it Otherw
ise a new sam
ple shall be taken and analyzed
a) Based on the analysis of the sam
ple(s) of the untreated influent the applicant must check the box of the sub-categories that the potential discharge falls w
ithin
Gasoline O
nly V
OC
Only
Primarily M
etals U
rban Fill Sites C
ontaminated Sum
ps Mixed Contaminants
Aquifer T
esting
VO
C w
ith Other
Petroleum w
ith Other
Listed C
ontaminated
Contam
inated H
ydrostatic Testing of
Well D
evelopment or
Other O
ils) only C
ontaminants
Contam
inants Sites
Dredge C
ondensates PipelinesT
anks R
ehabilitation F
uel Oils (and
b) Based on the analysis of the untreated influent the applicant m
ust indicate whether each listed chem
ical is believed present or believed absent in the potential discharge A
ttach additional sheets as needed
PAR
AM
ET
ER
B
elieve B
elieve of
Type of
Analytical
Minim
um
Maxim
um daily value
Avg daily value
Absent
Present Sam
ples Sam
ple M
ethod L
evel (ML
) of
(1 min-
(eg grab) U
sed T
est Method
concentration m
ass concentration
mass
imum
) (m
ethod ) (ugI)
( ugI) (kgday)
(ugI) (kgday)
1 Total Suspended Solids
GR
A
SM 2540D
000
580 000 215
SW-846
GR
A
100 c 500
2 Total R
esidual 9012A
C
hlorine
3 Total Petroleum
G
RA
1664
000 600
12
Hydrocarbons
4 Cyanide
GR
A
9012A
cl0
c20S B
enzene G
RA
B
5030
6 Toluene
GR
A
5030 c20
7 Ethylbcnzene
GR
A
5030 411
8 (m
o) Xylenes
GR
A
5030 10
472
9 Total B
TE
X
GR
A
5030 883
04
BT
EX
= SU
IU of B
enzene Toluene
Ethylbenzene
total Xylenes
Rem
ediation General Perm
it - Notice of Intent
PAR
AM
ET
ER
B
elieve B
elieve of
Type of
Absent
Present Sam
ples S
ample (eg
(1 min-
grab)
imum
)
10 Ethylene
Dibrom
ide G
RA
B
(1 2- Dibrom
o-methane)
11 Methyl-tert-B
utyl G
RA
Ether (M
tBE
)
12 tert-
Butyl
Alcohol
GR
AB
(TB
A)
13 tert-A
myl
Methyl
GR
A
Ether (T
AM
E)
14 Naphthalene
GR
AB
15 Carbon T
etra-G
RA
chloride
16 1
Dichlorobenzene
GR
A
17 D
iehlorobenzene G
RA
GR
A18 1
Dichlorobenzene
19 1
Dich1oroethane
GR
A
20 1
Dichloroethane
GR
A
21 1
Dichloroethylene
GR
A
22 cis-D
ichloro-G
RA
B
ethylene
GR
A
(Methylene C
hloride)
23 D
ichloromethane
24 T
etrachloroethylene G
RA
B
Rem
ediation General Perm
it - Notice of Intent
Analytical
Minim
um
Maxim
um daily value
Avg daily value
Method
Level (M
L) of
Used
Test M
ethod concentration
mass
concentration m
ass
(method )
(ugI) ( ug)
(kgday) (ugI)
(kgday)
504 010
0 0
5030 05
020
5030 0200
5030 020
625 247
5030 020
5030 020
5030 05
020
5030 020
5030 020
5030 020
5030 05
020
5030 020
5030 10
0200
5030 020
PAR
AM
ET
ER
B
elieve B
elieve of
Type of
Absent
Present Sam
ples Sam
ple (e
(l min-
grab)
imum
)
25 1
1 Trichloroethane
GR
AB
26 1
2 Trichloroethane
GR
A
27 Trichloroethylene
GR
AB
28 Vinyl C
hloride G
RA
B
29 Acetone
GR
A
30 14 D
ioxane G
RA
B
31 Total Phenols
GR
AB
32 Pentachlorophenol
GR
AB
33 Total Phthalates 6
GR
AB
(phthalate esthers)
34 Bis (2-E
thylhexyl) G
RA
B
Phthalate (D
ishy(ethylhexyl) P
hthalate)
35 Total G
roup 1 G
RA
P
olycyclic Arom
atic H
ydrocarbons (PA
H)
a Benzo(a) A
nthracene G
RA
B
b Benzo(a) P
yrene G
RA
c Benzo(b )F
luoranthene G
RA
B
d Benzo(k) F
luoranthene G
RA
e Chrysene
GR
AB
The slim
of iijdividual phthalate compounds
Rem
ediation General Perm
it - Notice of Intent
Analytical
Minim
um L
evel M
aximum
daily value A
vg daiJy Value
Method Used
(ML) ofT est
(method )
Method
concentration m
ass concentration
mass
(ugI) (ugI)
(kgday) (ugl)
(kgday)
5030 20
5030 20
5030 20
5030 ~20
5030 400
5030 200
625 50
625 50
625 All phthalates are
BD
L see lab report
625 50
625 A
ll Group I P A
Hs
are BD
L
625 50
625 50
625 50
625 50
625 50
g
PAR
AM
ET
ER
B
elieve B
elieve of
Type of
Analytical
Minim
um
Maxim
um daily value
Average daily value
Absent
Present Sam
ples Sam
ple (e M
ethod Used
Level (M
L) of
(lmin -
grab) (m
ethod ) T
est Method
concentration m
ass concentration
mass
imum
) (ug1)
(ugl) (kgday)
(ugl) (kgday)
f Dibenzo(a
GR
AB
625
-(50
anthracene
Indeno(I 23-cd) G
RA
B
625 -(50
Pyrene
36 Total G
roup II G
RA
B
625 247
Polycyclic A
romatiC
H
ydrocarbons (pAR
)
h Acenaphthene
GR
AB
625
-(10
i Acenaphthylene
GR
A
625 -(50
j Anthracene
GR
A
625 -(50
k Benzo(ghi)
Perylene G
RA
B
625 -(50
I Fluoranthene G
RA
B
625 -(50
m F
luorene G
RA
B
625 -(50
n Naphthalene-
GR
AB
625
247
o Phenanthrene
GR
AB
625
-(50
p Pyrene
GR
AB
625
-(50
37 Total
POlychlorinated
GR
AB
608
065 -(0065
Biphenyls (PC
Bs)
38 Antim
ony G
RA
B
200 03
4Eshy
39 Arsenic
GR
AB
200
468
40 Cadm
ium
GR
AB
200
-( 0
41 Chrom
ium II
(1) G
RA
B
calculated calculated
-(5
42 Chrom
ium V
I G
RA
7196A
-( 125
NO
TE
S (1) Chrom
ium m
= T
otal Chrom
ium - H
exavalent Chrom
ium A
ccording to lab personnel the trivalent chromium
is calculated to be greater or equal to 5 ugI but less than 125 ugl Total
Chrom
ium w
as -(5 ugI and the Hexavalent C
hromium
was less than 125 ugl
Rem
ediation General Perm
it - Notice of Intent
--------
--------
-------
--------
---
PAR
AM
ET
ER
B
elieve B
elieve of
Type of
Analytical
Minim
um
Maxim
um daily value
Avg daily value
Absent
Present Sam
ples Sam
ple (e M
ethod L
evel (ML
) of grab)
Used
Test M
ethod concentration
mass
concentration m
ass(1 m
inshy
imum
) (m
ethod ) (ug1)
(ug1) (kgday)
(ug1) (kgday)
43 Copper
GR
A
200 (5
44 Lead G
RA
200
0001
45 Mercury
GR
A
7470A
(020
46 Nickel
GR
AB
200
(5
GR
AB
200
( 1547 Selenium
48 Silver G
RA
B
200 (0
49 Zinc
GR
A
200 18
0025
50 Iron G
RA
B
200 400
25
Other (describe)
c For discharges where m
etals are believed present please fill out the following
If yes which m
etals A
rsenic and Iron Step
I Do any of the m
etals in the influent have a reasonable potential to exceed the
etIluent limits in A
ppendix II (i the limits set at zero to five dilutions) Y
rg N D
Step 2 For any m
etals which have reasonable potential to exceed the A
ppendix III limits
Look up the lim
it calculated at the corresponding dilution factor in
calculate the dilution factor (DF) using the form
ula in Part I A 3 c) (step 2) of the N
O
Appendix IV
Do any of the m
etals in the influent have the potential to instructions or as determ
ined by the State prior to the submission of this N
OI
exceed the corresponding effuent lim
its in Appendix IV
(i is the
What is the dilution factor for applicable m
etals in1uent concentration above the lim
it set at the calculated dilution M
etals A
rsenic and Iron factor)
yrgND
If Y
es list which m
etals A
rsenic and Iron
DF
Rem
ediation General Pem
lit - Notice of Intent
4 Treatm
ent system inform
ation Please describe the treatment system
using separate sheets as necessary including
a) A description of the treatm
ent system including a schem
atic of the proposed or existing treatment system
S
ee Figures 4 and 5
Frac tank Air stripper
Oilw
ater separator Equalization tanks
Bag filter rg
GA
C filter rg
b) Identity each applicable
treatment unit (check alJ
that apply)
Chlorination
Dechlorination
Other (please describe)
c) Proposed average and maxim
um flow
rates (gallons per minute) for the discharge and the design flow
rate(s) (gallons per minute) ofthe treatm
ent system
Average flow
rate of discharge 15 G
PM
Maxim
um flow
rate oftreatment system
0 G
PM
Design flow
rate of treatment system
0 G
PM
d) A description of chem
ical additives being used or planned to be used (attach MSD
S sheets) Not A
pplicable
5 Receiving surface water(s) Please provide information about the receiving water (s) using separate sheets as necessary including
Identity the discharge pathway
I Direct
I Within facility
I Stonn drain rg I R
iverbrook I W
etlands _ I Other (describe)
Provide a narrative description ofthe discharge pathway including the nam
e(s) of the receiving waters
Discharge to catchbasin and stonnw
ater drainage system in E
ast Broadw
ay which discharges to M
ahoney Brook (S
ee Figure 4)
c) Attach a detailed m
ap(s) indicating the site location and location of the outfall to the receiving water
1 For multiple discharges num
ber the discharges sequentialJy 2 For indirect dischargers indicate the location of the discharge to the indirect conveyance and the discharge to surface w
ater T
he map should also include the location and distance to the nearest sanitary sew
er as well as the locus of nearby sensitive receptors (based on U
SGS topographical
mapping) such as surface w
aters drinking water supplies and w
etland areas d) Provide the state w
ater quality classification of the receiving water
e) Provide the reported or calculated seven day- ten year low flow
(7QlO
) of the receiving water Jcfs
Please attach any calculation sheets used to support stream flow
and dilution calculations See A
ttachment B
f) Is the receiving water a listed 303(d) w
ater quality impaired or lim
ited water Y
es 0 No rg
If yes for which polJutant(s) N
A
Is there a TM
DL
Yes 0
No rg If yes for w
hich pollutant(s) NA
Rem
ediation General Perm
it - Notice of Intent
6 Results of C
onsultation with Federal Services Please p
rovide the following information according to requirements of Par
lBA
and A
ppendices II and VII
a) Are any listed threatened or endangered species or designated critical habitat in proxim
ity to the discharge Yes 0
No rg
Has any consultation w
ith the federal services been completed Y
es 0 No rg
or is consultation underway Y
es 0 No rg
What w
ere the results of the consultation with the U
S Fish and Wildlife Service andor N
ational Marine Fisheries Service (check one) N
ot applicable
a nojeopardy opinion
or written concurrenceD
on a finding that the discharges are not likely to adversely affect any endangered species or critical habitat
b) Are any historic properties listed or eligible for listing on the N
ational Register of H
istoric Places located on the facilty or site or in proximity to the discharge
Yes D
No
Have any state or tribal historic preservation offcer been consulted in this determ
ination (Massachusetts only) Y
es O N
o
7 SU
DD
lemental inform
ation
Please provide any supplemental information Attach any analytical data used to support the application A
ttach any celtification(s) required by the general permit
Attachm
ent A - Figures
Figure I - Site Locus M
ap
Figure 2 - MassD
EP Site Scoring M
ap
Figure 3 - Aerial M
ap
Figure 4 - Proposed Soil Excavation A
rea Map
Figure 5 - T
reatment S
ystem Line D
iagram
Attachm
ent B - D
ilution factor Calculations
Attachment C - L
aboratory Analytical R
eport Groundw
ater
Rem
ediation General Perm
it - Notice of 1ntenl
=-
including the following
8 Signature Requirements
The N
otice ofIntent must be signed by the operator in accordance w
ith the signatory requirements of 40 C
FR Section 122
certification
J certif under penalty of law that this docum
ent and all attachments w
ere prepared under my direction or supervision in accordance w
ith a system
designed to assure that qualifed personnel properly gather and evaluate the information subm
itted Based on m
y inquiry of the person or persons who
manage the system
or those persons directly responsible for gathering the information I certif that t
he information submitted
is to the best of m
y
knowledge and belief true accurate and com
plete J certif that I am aw
are that there are signifcant penalties for submitting false inform
ation including
the possibilty of fine and imprisonm
ent for knowing violations
FacilitySite Name
Form
er Speedw
ay Service S
tation 181 East B
roadwav G
ardner MA
01440
Operator signature
Title
Michael 1 D
ziura Sf Env E
ngineer
Date
4150- q
Rem
ediation General Perm
it - Notice of Intent
-
D- 0
0 0
il (J tu
Bw
o(0 -I
NJW
gQb
J(JZc o c
rou a -10
0 J 6shy
a 0
I-tDC
aJ Qj
E aJshy
ro ro ro
~~~ ~~~~- -- - _ - -_ - ~~~ ~~~~ ~~~ - - _- _- -- -- p __(
MA DEP - Bureau of Waste Site CleanupSITE NME Site S aP 5 MiFlII Former Speeway Station _-II181 Eat Broaday b b d IS I i I GARDNER MA 0144 v ri) i P f f 1 me- 1 5ylmI I L shy J --I 423315n 715835e SiteLocation y o oCop1odQcn Ofof W-_ l
1 1 I
r
r
iBARBER HILL
A c
Cf1 f o s
0
5
Roads Uned Acss Divd Mar Roed Conntor Street Track 1 EPA Sola Source Aquilar FEMA 100yaar iloodplain 0 c Puc Watar SLo GrunSelaceNon Corrty 0
Bounars lOwn Couny DE Region Tian Powerln Ine Aqedut ApprOld Zona2 tNPA Sue Wster Supp Zone A bStZ F--shy--rle
8os Mat Sub SUeor Porenrial Inermtent Man lvo8 Ste Dfm Hyro1apy Wmer FeatllePLio Suleee Wat S H-- L otlMds FrslSaltN-ES WeIMd Habat L
Potentia Prdutiv AqlJlers ModHig Yield Proteoted Opn Space ACC nIL c= Non-Potential Drng Water Sollce AIea ModumHi Yo1d ll DEP Pormrd SoidWes1 FsiIi6s cnifud Verne Pools f0
1I2 KIWUmR$ MtL
January 30 2004 SCALE 1 15000
-
LE
GE
ND
APX PROPER BONDA
- APPROXOiSPO SIT BOUNDA
-GR
OU
ND
WA
TE F1 D
IRE
cnON
SCA
LE
30 60 FE
(APR
OX
CORPORATE ENVIRONMENTAL
)i
AD
VISO
RS
INC
SC
AS SH
OW
D
R B
Y K
HA
EL
DA
TE
10407
JOB
NO
2920-96
AERIAL MAP
FO
RM
ER
SP
EE
DW
AY
ST
AT
ION
FlGURE -3
181 EA
BR
OA
AY
GA
NE
R fo
age 1 ot 1Streamflow Statistics Report
Streamstats Ungaged Site Report Date Wed Dec 31 2008 124908 Site Location Massachusetts NAD83 Latitude 425545 (42 3316) NAD83 Longitude -719758 (-71 58 32) NAD27 Latitude 425545 (423316) NAD27 Longitude - 9763 (-71 58 34) Drainage Area 502 mi2
IPeak Flow Basin Characteristics 1100 Statewide Low Flow (S02 mi2)
Regression Equation Valid Rang
I Min II Max1 Value III Parameter Drainage Area (square miles) 161 149
Mean Basin Slope from 250K DEM (percent) 032 24
Stratified Drift per Stream Length (square mile per mile) 129
Massachusetts Region (dimensionless)
Streamflow Statistics
gO-Percent Prediction Interval Prediction Error
MaximumStatistic Flow (ft s) (percent) Minimum
I D50 IIII 11 1811 II 24511 993
I D60 II 35511 2011 II 03611 35111 2411 II 041 I 201I D70 24111 2611 II 03811 151I D75 11 2811 II 0911 3761I D80 981I D85 1 I 3211 II o6311
1 I 3711 II 0441 1 2 2911 D90 11 4611 II 02411 15511 D95I D98 04511 6011 II 01511 11
I D99 03411 6511 II ol1ll 1021
5011 II 02611 11I M7D2Y 1111 3311 II odl 3 541
I AUGD50
IIIIIIIIIIIIIIIIIIIIII 0311 7111 II 0088411 0981I M7Dl0Y
1010
12312008httpstreamstatsagscrusgsgovgisimgReportsFlowStatsReport3494 - 2008123112498
Dilution Factor Calculation Former Speedway Service Station 181 East Broadway Gardner Ma
DF=(Od+Os)Od
DF = Dilution factor
Od = Max flow rate of discharge in cubic feet per second Os = receiving water flow in cubic feet per seconds 7010 flow rate Mahoney Brook 7010 = min flow for seven consecutive days with a recurrence interval of 10 years
7010 flow based on data obtained from USGS Steamflow Statistics Report Data attached
067
Semivolatile Organic Compounds by GCMS - Quality Control
Analyte( s)
Batch 8051216 - SW846 3510C
Blank 8051216BLK1)
Prepared amp Analyzed 16May-
Acenaphthene
Acenaphthylene
Aniline
Anthracene
AzobenzenelDi phenyld iazi ne
Benzidine
Benzo (a) anthracene
Benzo (a) pyrene
Benzo (b) fiuoranthene
Benzo (g i) perylene
Benzo (k) fiuoranthene
Benzoic acid
Benzyl alcohol
Bis(2-ch loroethoxy) methane
Bis(2-ch loroethyl)ether
Bis(2-ch loroi sopropyl)ether
Bis(2ethylhexyl) phthalate
Bromophenyl phenyl ether
Butyl benzyl phthalate
Carbazole
Ch loro-3-methyl phenol
Chloroaniline
Chloronaphthalene
Chlorophenol
Chlorophenyl phenyl ether
Chrysene
Dibenzo (a h) anthracene
Dibenzofuran
Dichlorobenzene
Dichlorobenzene
14- Dichlorobenzene
3 - Dichlorobenzidine
24-Dichlorophenol
Diethyl phthalate
Dimethyl phthalate
24- Dimethylphenol
Din-butyl phthalate
Dinitro-2-methylphenol
Dinitrophenol
Dinitrotoluene
Dinitrotoluene
Di-noctyl phthalate
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopehtadiene
Hexachloroethane
Indeno (1 cd) pyrene
Spike Source REC RPD
Result Flag Units RDL Level Result REC Limits RPD Limit
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gl
BRL gI
BRL gl
BRL gl
BRL gl
BRL gI
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gll
BRL gl
BRL gll
BRL gl
BRL gl
BRL gI
BRL gI
BRL gI
BRL gl
BRL gI
BRL gI
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gI
BRL gI
BRL gl
This laboratory report is IlOt valid without all authorized sigllature 011 the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page t4 of25
Volatie Organic Compounds - Quality Control
p (
Spike Source REC RPD
RDL Level Result REC Limits RPD Limit Analyte(s) Result Flag Units
Batch 8051244 - SW846 5030 Water MS
Matrix S ike Du 8051244-MSD1 Source SA78629shy
Prepared 16-May-08 Analyzed 17-May-BRL 106 251
Vinyl chloride 21 gl 20
101 70- 130 Surrogate 4-Bromofluorobenzene 50 gl 50
70- 13049 gl 50 111 70- 130
Surrogate Toluene-Surrogate 1 Dichloroethane- 55 gl 50
50 70- 130494 glSurrogate Dibromofluoromethane
Microextractable Organic Compounds - Quality Control
Spike Source REC RPD
Flag Units RDL Level Result REC Limits RPD Limit Analyte(s) Result
Batch 8051105 - SW846 3510C
Blank 8051105-BLK
Prepared amp Analyzed 15-May-
BRL gl 01001 Dibromoethane (ED B)
LCS 8051105-BS1
Prepared amp Analyzed 15-Mayshy50- 1500770 gl 0100 100
licate 8051105-DUP1 Source SA7B583shy
Prepared amp Analyzed 15-May-
BRL gl 0100 BRL
1 Dibromoethane (EDB)
1 Dibromoethane (EDB)
This laborntOlY report is not valid without an authorized signature 011 the cover page
Page 13 of2S Reportable Detection Limit BRL = Below Reporting Limit
Sam le Identification Client Pro ect Matrix Collection DateTime ReceivedMWshy
2920-96- Ground Water 13-May-081030 14-May-SA 78602shy
CAS No Analyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Volatile Organic Compounds
Volatile Or anic Com ounds b GCMS
Prepared by method SW846 5030 Water MS
123-91- Dioxane BRL 1-91 200 EPA 624 16-May-08 17-May-08 8051244
994-05-8 Ter-amyl methyl ether BRL 1-911 20
755- Tert-Butanoll butyl alcohol BRL 1-91 200
67-B4- Acetone BRL 1-91 400
71-43- Benzene BRL 1-91 20
75-27-4 Bromodichloromethane BRL 1-91 20
75-25- Bromoform BRL 1-91 20
74-83- Bromomethane BRL 1-91 40
78-93- Butanone (MEK) BRL 1-91 200
56-23- Carbon tetrachloride BRL 1-91 20
108-90- Chlorobenzene BRL 1-91 20
75-00- Chloroethane BRL 1-91 40
676- Chloroform BRL 1-91 20
74-87- Chloromethane BRL 1-91 40
124-48- Dibromochloromethane BRL 1-91 20
95-50- Dichlorobenzene BRL 1-911 20
541-73- Dichlorobenzene BRL 1-91 20
106-46- Dichlorobenzene BRL 1-91 20
75-34- 1- Dichloroethane BRL 1-91 20
107-06- Dichloroethane BRL 1-91 20
75-35-4 1- Dichloroethene BRL 1-91 20
156-59 cis- Dichloroethene BRL 1-91 20
156-60- trans- Dichloroethene BRL 1-91 20
78-87- 2- Dichloropropane BRL 1-91 20
10061-01-5 cis- Dichloropropene BRL 1-91 20
10061-02-B trans- Dichloropropene BRL 1-91 20
100-41-4 Ethylbenzene 411 1-911 20
591-78-B BRL 200Hexanone (MBK) 1-91
1634-04 -4 Methyl tert-butyl ether BRL 1-91 20
108-10- Methyl- pentanone (MIBK) BRL 1-91 200
75-09- Methylene chloride BRL 1-91 200
100-42- Styrene BRL 1-91 20
79-34- 1 Tetrachloroethane BRL 1-91 20
127- 18-4 T etrachloroethene BRL 1-91 20
108-88- Toluene BRL 1-91 20
71-55 1- Trichloroethane BRL 1-91 20
79-00- 2- Trichloroethane BRL 1-91 20
79-01-B Trichloroethene BRL 1-91 20
759-4 Trichlorofluoromethane (Freon 11) BRL 1-91 20
75-01-4 Vinyl chloride BRL 1-91 20
179601-23-1 m Xylene 390 1-91 40
95-47 Xylene 82 1-91 20
Surrogate recoveries 460-00- Bromofluorobenzene 70- 130
2037-26- Toluene- 100 70- 130
17060-07-0 1 Dichloroethane- 111 70- 130
1868-53- Dibromofluoromethane 70- 130
Microextractable Organic Compounds
106-93-4 1 Dibromoethane (EDB) BRL 1-91 0100 EPA 504 15-May- 15-May-08 8051105
Semivolatile Organic Compounds by GCMS
This laboratory report is not valid without all autllOrized signature 011 the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page 5 of 25
Sam le Identification Client Pro ect Matrix Collection DateTime Received
MWshy2920-96- Ground Water 13-May-081030 14-May-
SA 78602shy
CAS No Analyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Semivolatie Organic Compounds by GCMS
Semi volatile Or anic Com ounds b EPA 625
Prepared by method SW846 3510C 50 EPA 625 16-May- 19-May-08 805121683-32- Acenaphthene BRL IJgl
208-96-8 Acenaphthylene BRL IJgl 50
62-53- BRL IJgll 50Aniline
120- 12- Anthracene BRL 1J91 50
103-33- AzobenzenefDiphenyldiazine BRL IJgl 50
92-87 - Benzidine BRL IJgl 50
56-55- Benzo (a) anthracene BRL 1J91 50
50-32 - Benzo (a) pyrene IJglBRL 50
205-99- Benzo (b) fluoranthene BRL IJgl 50
191-24- Benzo (g i) perylene BRL IJgl 50
50207-08- Benzo (k) fluoranthene BRL IJgl
65-85 Benzoic acid BRL 1J91 50
100-51-6 Benzyl alcohol 1J91BRL 50
50111-91- Bis(2-chloroethoxy)methane BRL 1J91
111-4-4 Bis(2-chloroethyl)ether BRL IJgl 50
501 08-60- Bis(2-chloroisopropyl)ether BRL IJgl
117-81- Bis(2-ethylhexyl)phthalate BRL 1J91 50
101-55- Bromophenyl phenyl ether BRL IJgl 50
5085-68- Butyl benzyl phthalate BRL IJgl
5086-74- Carbazole BRL IJgl
5059-50- C hloro-3-methylphenol BRL IJgl
106-47- Chloroaniline BRL IJgl 50
91-58- Chloronaphthalene IJglBRL 50
5095-57 - Chlorophenol BRL 1J91
507005-72- Chlorophenyl phenyl ether BRL IJgl
216-01- Chrysene tJ91BRL 50
5053-70- Dibenzo (a h) anthracene BRL IJgl
50132-64- Dibenzofuran BRL IJgl
95-50- Dichlorobenzene IJglBRL 50
541-73- 13- Dichlorobenzene BRL IJgl 50
106-46- Dichlorobenzene 1J91BRL 50
5091-94- 3 - Dichlorobenzidine BRL IJgl
120-83- Dichlorophenol BRL IJgl 50
84-66- Diethyl phthalate BRL IJgl 50
131-11- Dimethyl phthalate BRL IJgll 50
105-67- Dimethylphenol BRL 1J91 50
5084-74- Di-n- butyl phthalate BRL 1J91
534-52 - Dinitro-2-methylphenol BRL IJgl 50
51-28- Dinitrophenol IJglBRL 50
50121-14- Dinitrotoluene BRL 1J91
606-20- Dinitrotoluene IJglBRL 50
50117-84-0 Di-n-octyl phthalate BRL IJgl
206-44-0 Fluoranthene 1J91BRL 50
BRL 50
50 86-73- Fluorene IJgi
118-74- Hexachlorobenzene BRL 1J91
87-68- Hexachlorobutadiene 1J91BRL 50
5077-47-4 Hexachlorocyclopentadiene BRL IJgl
67-72- Hexachloroethane IJglBRL 50
50193-39- Indeno (1 3-cd) pyrene BRL IJgl
5078-59- Isophorone BRL IJgl
Tfls laboratory report is not valid without all authorized signature 011 the coverpage
Page 6 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Sam le Identification Client Pro ect Matrix Collection DateTime ReceivedMWshy
2920-96- Ground Water I3-May-081030 14-May-SA 78602shy
CAS No Analyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Semivolatile Organic Compounds by GCMS
Semi volatile Or anic Com ounds b EPA 625
Prepared by method SW846 3510C
91-57 -6 Methylnaphthalene 367 1-91 50 EPA 625 16-May- 19-May-08 8051216
95-48- Methylphenol BRL 1-91 50
108-39-4 3 amp 4-Methylphenol BRL I-gl 100 106-44shy91-20- Naphthalene 247 1-91 50
88-74-4 Nitroaniline BRL 1-91 50
99-09- Nitroaniline BRL 1-91 50
100-01-6 Nitroaniline BRL 1-91 50
98-95- Nitrobenzene BRL 1-91 50
88-75- Nitrophenol BRL 1-91 50
100-02- Nitrophenol BRL 1-91 50
62-75- Nitrosodimethylamine BRL 1-91 50
621-64- N- Nitrosodi-n-propylamine BRL 1-91 50
86-30-6 Nitrosodiphenylamine BRL 1-91 50
87 -86- Pentachlorophenol BRL 1-91 50
85-0- Phenanthrene BRL 1-91 50
108-95- Phenol BRL 1-91 50
129-00-0 Pyrene BRL 1-91 50
110-86- Pyridine BRL 1-91 50
120-82- 4- Trichlorobenzene BRL 1-91 50
95-95- 5- Trichlorophenol BRL 1-91 50
88-06- 6- T richlorophenol BRL 1-91 50
Surrogate recoveries
321-60- Fluorobipheny 30- 130
367- 12- Fuorophenol 15- 110
4165-60- Nitrobenzene- 30- 130
4165-62- Pheno- 15- 110
1718-51- Terpheny-d4 30- 130
118- 79- 6- Tribromophenol 15- 110
Semivolatile Organic Compounds by GC
Pol chlorinated Bi hen ls b EPA 608
Prepared by method SW846 3510C
12674- 11-2 Aroclor- 1016 BRL 1-91 0650 EPA 608 15- May- 16-May-08 8051106
11104-28-2 Aroclor-1221 BRL IJgl 0650
11141-16-5 Aroclor- 1232 BRL 1-91 0650
53469-21-9 Aroclor- 1242 BRL 1-91 0650
12672-29-6 Aroclor- 1248 BRL 1-91 0650
11097-69-1 Aroclor- 1254 BRL 1-91 0650
11096-82-5 Aroclor -1260 BRL 1-91 0650
37324-23-5 Aroclor-1262 BRL 1-91 0650
11100-14-4 Aroclor-1268 BRL IJgl 0650
Surrogate recoveries
2051-24- Decachlorobipheny (Sr) 105 30- 150
10386-84-2 4 DB-Octafluorobiphenyl (Sr) 30- 150
Extractable Petroleum Hydrocarbons
mgl EPA 1664 Rev A 15-May- 19-May-08 8051102Non-polar material (SGT- HEM)
Soluble Metals by EPA 2006000 Series Metbods
Field Filtered NA EPA 200 73005A 15- May- 15-May-08 8051192Filtration
Soluble Metals by EPA 200 Series Methods
7440-22-4 Silver BRL mgl 0002 EPA 200 21-May- 27- May-08 8051249
This laboratory report is IlOt mlid without (II authorized signature on the cover page
Reportble Detection Limit BRL = Below Reporting Limit Page 7 of 25
Sam le Identification MW-
Client Pro ect 2920-96shy
Matrix Ground Water
Collection DateTime 13-May-08 1030
Received 14-May-
SA 78602shy
CAS No A nalyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Soluble Metals by EPA 200 Series Methods
7440-38shy Arsenic 0468 mg1 0040 EPA 200 21-Mayshy 21-May-08 80511 50
7440-43shy Cadmium BRL mg1 0002 EPA 200 21-May-088051249
7440-47shy Chromium BRL mg1 0050 EPA 200 21-May-088051150
7440-50-8 Copper BRL mg1 0050
7439-89-6 Iron 184 mg1 0150
7439-97-6 Mercury BRL mg1 00020 EPA 245 17470A 21-May-088051152
7440-02-0 Nickel BRL mg1 0050 EPA 200 21-May-088051150
7439-92shy Lead 0011 mg1 0002 EPA 200 21-May-088051249
7440-36-0 Antimony 0003 mg1 0002
7782-49shy Selenium BRL mg1 0150 EPA 200 21-May-08 8051150
7440-66-6 Zinc 0186 mgl 0050
General Chemistry Parameters
Filtration Completed NA Varies 14-Mayshy 14-May-08 8051095
18540-29-9 Hexavalent Chromium (soluble) BRL HT2 mg1 125 SM3500CrDI796A 14-Mayshy 14-May-08 8051094 R01 2013 2016
57-12shy Cyanide (total) BRL mg1 0100 EPA 3354 19-Mayshy 19-May-088051374
7782-50shy Total Residual Chlorine BRL CIHT mg1 500 Hach 8167 14-Mayshy 14-May-08 8051049 R01 1900 2001
Total Suspended Solids 580 mg1 25 SM2540D 16-Mayshy 16-May-08 8051275
This lahomtOlY report is not valid without an authorized signature on the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page 8 of 25
Volatie Organic Compounds - Quality Control
Analyte( s)
Batch 8051244 - SW846 5030 Water MS
Blank 8051244-BLK1
Prepared 16-May-08 Analyzed 17-May-
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromochloromethane
1 Dichlorobenzene
1 Dichlorobenzene
1 Dichlorobenzene
1-Dichloroethane
1 Dichloroethane
1 1-Dichloroethene
cis- Dichloroethene
trans- 1 Dichloroethene
1 Dichloropropane
cis- 1 Dichloropropene
trans- 1 Dichloropropene
Ethylbenzene
Hexanone (MBK)
Methyl tert-butyl ether
Methyl- pentanone (MIBK)
Methylene chloride
Styrene
2- Tetrachloroethane
Tetrachloroethene
Toluene
1- Trichloroethane
2- Trichloroethane
Trichloroethene
Trichlorofluoromethane (Freon 11)
Vinyl chloride
p-Xylene
Xylene
Surrogate 4-Bromofluorobenzene Surrogate Toluene-
Surrogate 1 Dichloroethane-Surrogate Dibromofluoromethane
LCS B051244-BS1
Prepared 16-May-08 Analyzed 17 -May-
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Spike Source REC RPD
Result Flag Units RDL Level Result REC Limits RPD Limit
BRL gl 20
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl 10
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gll
BRL gi
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl 10
BRL gll
BRL gll 10
BRL gl 10
BRL gll
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
41 gl 50 70- 130 49 gl 50 70- 130 59 gl 50 119 70- 130 52 gl 50 105 70- 130
QC2 jgl 20 70- 130
18 jgl 20 70- 130
192 jgl 20 35- 155
18 jgl 20 45- 169
19 jgl 20 242
This laboratOlY repol1 is lot valid without 011 authorized sigllature 011 the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page 9 of 25
Volatie Organic Compounds - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051244 - SW846 5030 Water MS
LC5 8051244B51
Prepared 16-May-08 Analyzed 17-May-
Butanone (MEK) 10 QC2 gl 20 70- 130
Carbon tetrachloride 204 gl 20 102 70- 140
Chlorobenzene 18 gl 20 70- 130
Chloroethane 164 gl 20 14-230
Chloroform 18 gll 20 51- 138
Chloromethane 21 gl 20 106 273
Dibromochloromethane 18 gl 20 53- 149
1 Dichlorobenzene 20 gl 20 104 18- 190
1 Dichlorobenzene 19 gl 20 59- 156
1 A-Dichlorobenzene 18 gl 20 18- 190
1- Dichloroethane 19 gl 20 59- 155
1 Dichloroethane 19 gl 20 49- 155
1-Dichloroethene 16 gl 20 70- 130
cis- 1 Dichloroethene 17 gl 20 70- 130
trans- 1 Dichloroethene 16 gll 20 54- 156
1 Dichloropropane 18 gl 20 210
cis- Dichloropropene 17 gl 20 227
trans- 1 Dichloropropene 17 gl 20 17- 183
Ethylbenzene 19 gl 20 37- 162
Hexanone (MBK) 124 QC2 gl 20 70- 130
Methyl tert-butyl ether 19 gl 20 70- 130
Methylshy pentanone (MIBK) 17 gl 20 70- 130
Methylene chloride 16 gl 20 221
Styrene 17 gl 20 70- 130
1 Tetrachloroethane 194 gl 20 46- 157
Tetrachloroethene 15 gl 20 64- 148
Toluene 18 gl 20 70- 130
1- Trichloroethane 20 gl 20 100 52- 162
2- Trichloroethane 18 gl 20 52- 150
Trichloroethene 17 gl 20 71- 157
Trichlorofluoromethane (Freon 11) 19 gl 20 17- 181
Vinyl chloride 21 gl 20 106 251
p-Xylene 39 gl 40 70- 130
Xylene 20 gl 20 102 70- 130
Surrogate 4-Bromofluorobenzene Surrogate Toluene-
Surrogate 1 Dichloroethane-Surrogate Dibromofluoromethane
52 49 56
49
gl
gl
gl
gl
50 50 50
50
105
112 100
70- 130 70- 130 70- 130 70- 130
LC5 DUD (8051244-B5D1
Prepared 16-May-08 Analyzed 17-May-
Acetone QC2 gl 20 70- 130
Benzene 18 gl 20 70- 130
Bromodichloromethane 18 gl 200 35- 155
Bromoform 17 gl 20 45- 169
Bromomethane 18 gl 20 242
Butanone (MEK) 11 QC2 1-91 20 70- 130
Carbon tetrachloride 20 gl 20 100 70- 140
Chlorobenzene 17 gl 20 70- 130
Chloroethane 15 1-91 20 14-230
Chloroform 18 1-91 20 51- 138
This laboratory report is aot valid without a1 authorized sig1ature 01 the cover page
Reportble Detection Limit BRL = Below Reporting Limit Page 10 of25
Volatie Organic Compounds - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051244 - SW846 5030 Water MS
LCS Dup 18051244-BSD1
Prepared 16-May-08 Analyzed 17-May-
Chloromethane 18 1-91 20 273
Dibromochloromethane 174 1-91 20 53- 149
Dichlorobenzene 20 1-91 20 100 18- 190
Dichlorobenzene 18 1-91 20 59- 156
Dichlorobenzene 18 1-91 20 18- 190
Dichloroethane 18 1-91 20 59- 155
Dichloroethane 19 1-91 20 49- 155
Dichloroethene 16 1-91 20 70- 130
cis- Dichloroethene 16 1-91 20 70- 130
trans- Dichloroethene 15 1-91 20 54- 156
Dichloropropane 17 1-91 20 210
cis- Dichloropropene 164 IJgl 20 227
trans- 1 Dichloropropene 164 I-gl 20 17- 183
Etlwlbenzene 18 IJgl 20 37- 162
Hexanone (MBK) 124 QC2 IJgl 20 70- 130
Methyl tert-butyl ether 184 1J91 20 70- 130
Methyl- pentanone (MIBK) 17 IJgl 20 70- 130
Methylene chloride 16 IJgl 20 221
Styrene 16 IJgl 20 70- 130
2- Tetrachloroethane 19 IJgl 20 46- 157
Tetrachloroethene 15 IJgl 20 64- 148
Toluene 17 IJgl 20 70- 130
1- Trichloroethane 19 1-91 20 52- 162
2- Trichloroethane 16 IJgl 20 52- 150
Trichloroethene 15 IJgl 20 71- 157
Trichlorofluoromethane (Freon 11) 17 IJgl 20 17- 181
Vinyl chloride 19 IJglI 20 251
p-Xylene 37 1J91 40 70- 130
Xylene 20 IJgl 20 100 70- 130
Surrogate 4-Bromofluorobenzene 51 IJgl 50 104 70- 130
Surrogate Toluene- 4B gl 50 70- 130
Surrogate 1 0ichloroethane- 53 IJgl 50 106 70- 130 Surrogate Oibromofluoromethane 50 1J9i 50 102 70- 130
Matrix S ike B051244-MS1 Source SA7B629shy
Prepared 16-May-08 Analyzed 17-May-
Benzene 18 20 BRL 70- 130IJgl
Bromodichloromethane 19 IJgl 20 BRL 35- 155
Bromoform 18 IJgl 20 BRL 45- 169
Bromomethane 16 IJgl 20 BRL 242
Carbon tetrachloride 21 IJgl 20 BRL 106 70- 140
Chlorobenzene 18 IJgl 20 BRL 70- 130
Chloroethane 16 IJgl 20 BRL 14-230
Chloroform 18 IJgl 20 BRL 51- 138
Chloromethane 19 IJgl 20 BRL 273
Dibromochloromethane 17 IJgl 20 BRL 53- 149
1 Dichlorobenzene 22 IJgl 20 BRL 112 18- 190
1 Dichlorobenzene 22 IJgl 20 BRL 110 59-156
1 Dichlorobenzene 21 IJgl 20 BRL 109 18- 190
1- Dichloroethane 19 IJgl 20 BRL 59- 155
1 Dichloroethane 18 IJgl 20 BRL 49- 155
This laboratory report is 110t mUd without an authorized signature on the covel page
Reportble Detection Limit BRL = Below Reporting Limit Page It of25
Volatile Organic Compounds - Quality Control
p
Spike Source REC RPD
Result REC imits RPD LimitAnalyte(s) Result Flag Units RDL Level
Batch 8051244 - SW846 5030 Water MS
Matrix ike S051244-MS1 Source SA7B629shy
Prepared 16-May-08 Analyzed 17-Mayshy
17 20 BRL 70- 130 1- Dichloroethene IJgl
16 20 BRL 54- 156trans- 1 Dichloroethene IJgl
21020 BRL1 Dichloropropane 17 1J91
cis- 1 Dichloropropene 17 IJgl 20 BRL 227
17- 183trans- 1 Dichloropropene 184 1J91 20 BRL
20 20 BRL 103 37- 162Ethylbenzene IJgl
15 20 BRL 221Methylene chloride IJgl
20 BRL 46- 1572- Tetrachloroethane 19 1J91
20 BRL 64- 148Tetrachloroethene 18 1J91
BRL 70- 130Toluene 18 1J91 20
105 52-1621- Trichloroethane 211 IJgl 20 BRL
18 20 BRL 52- 1502- Trichloroethane IJgl
17 20 BRL 71- 157Trichloroethene 1J91
20 BRL 17- 181Trichloroluoromethane (Freon 11) 194 IJgl
20 BRL 103 251Vinyl chloride 20 IJgl
102 70- 130Surrogate 4-Bromofluorobenzene 50 IJgl 50 50 70- 130Surrogate Toluene- 49 1J91
56 50 112 70- 130Surrogate 1 Dichloroethane- IJgl
50 100 70- 130Surrogate Dibromofluoromethane 50 IJgl
Matrix S ike Du S051244-MSD1 Source SA7S629shy
Prepared 16-May-08 Analyzed 17-Mayshy
18 20 BRL 70- 130Benzene IJgl
18 20 BRL 35- 155Bromodichloromethane IJgl
17 20 BRL 45- 169Bromoform IJgl
20 BRL 242Bromomethane 17 IJgl
20 BRL 103 70- 140Carbon tetrachloride 20 IJgl
18 20 BRL 70- 130Chlorobenzene 1J91
14-230Chloroethane 16 IJgl 20 BRL
20 51- 138Chloroform 184 IJgl BRL
Chloromethane 19 1J91 20 BRL 273
18 20 BRL 53- 149Dibromochloromethane 1J91
20 BRL 117 18- 190Dichlorobenzene 234 IJgl
20 BRL 112 59- 156Dichlorobenzene 22 IJgl
BRL 108 18- 190Dichlorobenzene 21 1J91 20
20 59- 1551 Dichloroethane 19 IJgl BRL
18 20 BRL 49- 155Dichloroethane IJgl
16 20 BRL 70- 130Dichloroethene IJgl
20 BRL 54- 156trans- Dichloroethene 154 1J91
20 BRL 210Dichloropropane 17 IJgl
0420 BRL 227cis- Dichloropropene 17 IJgl
17- 183trans- Dichloropropene 17 1J91 20 BRL
BRL 37- 162Ethylbenzene 20 1J91 20 102
Methylene chloride 15 IJgl 20 BRL 221
20 BRL 46- 1572- Tetrachloroethane 192 IJgl
20 BRL 64- 148 04Tetrachloroethene 18 IJgl
BRL 70- 130Toluene 184 1J91 20
52- 1621- Trichloroethane 20 IJgl 20 BRL 104
17 20 BRL 52- 1502- Trichloroethane IJgl
17 20 BRL 71- 157Trichloroethene IJgl
20 BRL 17-181Trichlorofluoromethane (Freon 11) 19 IJgl
This laboratory report is IIOt valid without all authorized sigllllture 011 the cover page
Page 12 of25 Reportble Detection Limit BRL = Below Reporting Limit
Semivolatile Organic Compounds by GCMS - Quality Control
Analyte(s)
Batch 8051216 - SW846 3510C
Blank 8051216-BLK1
Prepared amp Analyzed 16-May-
Isophorone
Methylnaphthalene
Methylphenol
3 amp 4-Methylphenol
Naphthalene
Nitroaniline
Nitroaniline
Nitroaniline
Nitrobenzene
Nitrophenol
Nitrophenol
Nitrosodimethylamine
N- N itrosodi-n-pro pyla mine
N itrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Pyridine
1 24-Trichlorobenzene
24 5- Trichlorophenol
246- Trichlorophenol
Surrogate 2-Fuorobipheny Surrogate 2-Fuoropheno Surrogate Nitrobenzene-Surrogate PhenoshySurrogate Terpheny-d4 Surrogate 6- Tribromopheno
LCS B051216-BS1
Prepared amp Analyzed 16-May-
Acenaphthene
Acenaphthylene
Aniline
Anthracene
AzobenzenelDi phenyld lazine
Benzidine
Benzo (a) anthracene
Benzo (a) pyrene
Benzo (b) fluoranthene
Benzo (g i) perylene
Benzo (k) fluoranthene
Benzoic acid
Benzyl alcohol
B is(2-chloroethoxy)methane
B i s (2-ch loroethyl)eth e r
Bis(2-ch loroisopropyl) ether
B is(2-ethy Ih exyl) phtha late
Bromophenyl phenyl ether
Butyl benzyl phthalate
Carbazole
Spike Source REC RPD
Result Flag Units RDL Level Result REC Limits RPD Limit
BRL gl
BRL gl
BRL gl
BRL gl 10
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gll
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
370 gl 50 30- 130 40 gl 50 15- 110 39 gl 50 30- 130 43 gl 50 15- 110 36 gl 50 30- 130 40 gl 50 15- 110
41 gl 50 40- 140
43 gI 50 40- 140
41 gl 50 40- 140
38 gl 50 40- 140
45 gl 50 40- 140
49 gl 50 153
41 gl 50 40- 140
43 gl 50 40- 140
41 gl 50 40- 140
41 gll 50 40- 140
45 gl 50 40- 140
32 gl 50 12- 149
41 gl 50 40- 140
39 gl 50 40- 140
384 gl 50 40- 140
47 gl 50 40- 140
47 gl 50 40- 140
40 gl 50 40- 140
47 gI 50 40- 140
56 gI 50 112 200
This laboratory report is lIot valid witllOut a1l authorized sigllature 011 the coverpage
Reportble Detection Limit BRL = Below Reporting Limit Page 15 of25
Semivolatile Organic Compounds by GCMS - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051216 - SW846 3510C
LCS 8051216-BS1
Prepared amp Analyzed 16-Mayshy
50 30- 1304 -C hloro-3-methylphenol 42 IJgl
40- 140Chloroaniline 39 IJgl 50
Chloronaphthalene 37 IJgl 50 40- 140
Chlorophenol 37 IJgl 50 30- 130
50 40- 140
40- 140
Chlorophenyl phenyl ether 45 IJgl
Chrysene 43 IJgl 50
Dibenzo (a h) anthracene 43 IJgl 50 40- 140
Dibenzofuran IJgl38 50 40- 140
50 40- 1401 Dichlorobenzene 35 IJgl
40- 1401 Dichlorobenzene 264 IJgl 50
40- 1401 Dichlorobenzene 434 IJgl 50
58 50 116 40- 1403 - Dichlorobenzidine IJgl
50 30- 130
40- 140 24-Dichlorophenol 38 IJgl
Diethyl phthalate 484 IJgl 50
50 40- 140Dimethyl phthalate 464 IJgl
Dlmethylphenol 39 IJgl 50 30- 130
DI-n-butyl phthalate 44 IJgll 50 40- 140
30- 130 6-Di nitro- 2-methylphenol 38 1J91 50
30- 130Dinltrophenol 36 1J91 50
42 50 40- 14024-Dlnitrotoluene 1J91
Dlnitrotoluene 1J9141 50 40- 140
Di-n-octyl phthalate 52 IJgl 50 104 40- 140
40- 140Fluoranthene 40 IJgl 50
Fluorene 41 IJgl 50 40- 140
39 50 40- 140Hexachlorobenzene IJgl
50 40- 140Hexachlorobutadiene 40 IJgl
40- 140Hexach lorocyclopentad iene 294 IJgl 50
40 50 40- 140Hexachloroethane IJgl
42 50 40-140Indeno (1 3-cd) pyrene IJgl
50 40- 140Isophorone 40 IJgl
40- 140Methylnaphthalene 394 IJgl 50
40- 140Methylphenol 39 IJgl 50
40 10 50 40- 1403 amp 4-Methylphenol IJgl
37 50 40-140Naphthalene IJgl
50 40-140Nitroaniline 39 IJgl
Nitroaniline 51 IJgl 50 102 40- 140
48 50 40- 140Nltroaniline 1J91
50 40- 140Nitrobenzene 40 IJgl
30- 130Nitrophenol 36 IJgl 50
40 IJgl 50 30- 130Nitrophenol 40- 140Nitrosodimethylamine 32 1J91 50
50 40-140N- N itrosodi-n-propyla mine 46 IJgl
40- 140N itrosodi phenyla ml ne 44 IJgl 50
41 IJgl 50 30- 130Pentachlorophenol 40- 140Phenanthrene 38 IJgl 50
50 30- 130Phenol 38 IJgl
40- 140Pyrene 424 1J91 50
40- 140Pyridine 294 1J91 50
40- 14024- Trichlorobenzene 364 IJgl 50
This laboratory report is not mlid without an authorized signature 011 the cover page
Page 16 of25 Reportble Detection Limit BRL = Below Reporting Limit
Semivolatie Organic Compounds by GCMS - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
BMch 8051216 - SW846 3510C
LC5 8051216-851
Prepared amp Analyzed 16-Mayshy
24 5- Trichlorophenol 404 gl 50 30- 130
246- Trichlorophenol 42 gl 50 30- 130
Surrogate 2-Fluorobiphenyl 29 gl 50 30- 130
Surrogate 2-Fluorophenot 27 gl 50 15- 110
Surrogate Nitrobenzene- 30 gl 50 30- 130
Surrogate Phenol- 29 gl 50 15- 110
Surrogate Terpheny-d4 30 gl 50 30- 130
Surrogate 6- Tribromopheno 324 gl 50 15- 110
This laboratory report is lIot valid without all authorized sigllature 011 tlle cover page
Reportble Detection Limit BRL = Below Reporting Limit Page 17 of25
Semivolatie Organic Compounds by GC - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051106 - SW846 3510C
Blank S051106-BLK1
Prepared amp Analyzed 15-Mayshy
Aroclor- 1016 BRL gI 0200
Aroclor- 1016 (2C) BRL gI 0200
Aroclor- 1221 BRL gI 0200
Aroclor- 1221 (2C) BRL gI 0200
Aroclor- 1232 BRL gI 0200
Aroclor- 1232 (2Cj BRL gI 0200
Aroclor- 1242 BRL gI 0200
Aroclor-1242 (2C) BRL gI 0200
Aroclor- 1248 BRL gI 0200
Aroclor- 1248 (2C) BRL gI 0200
Aroclor- 1254 BRL gI 0200
Aroclor- 1254(2Cj BRL gI 0200
Aroclor- 1260 BRL gI 0200
Aroclor- 1260 (2C) BRL gI 0200
Aroclor- 1262 BRL gI 0200
Aroclor- 1262 (2C) BRL gI 0200
Aroclor-1268 BRL gI 0200
Aroclor- 1268 (2C) BRL gI 0200
Surrogate Decachlorobiphenyl (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0231 0224 0194 0191
gI
gI
gI
gI
0200 0200 0200 0200
116 112
30- 150 30- 150 30- 150 30- 150
LC5 8051106-B51
Prepared 15-May-08 Analyzed 16-May-08
Aroclor- 1016 265 gI 0200 250 106 50- 114
Aroclor- 1 016 (2C) 240 gI 0200 250 50- 114
Aroclor- 1260 0269 gI 0200 250 107 40- 127
Aroclor-1260 (2Cj 270 gI 0200 250 108 40- 127
Surrogate Decachlorobiphenyl (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0225 0224 0188 0183
gI
gI
gI
gI
0200 0200 0200 0200
113 112
30- 150 30- 150 30- 150 30- 150
LC5 DUD rS051106-B5D1
Prepared 15-May-08 Analyzed 16-Mayshy
Aroclor- 1016 262 gl 0200 250 105 50- 114
Aroclor-1 016 (2Cj 241 gI 0200 250 50- 114
Aroclor- 1260 277 gI 0200 250 111 40- 127
Aroclor- 1260(2Cj 0260 gI 0200 250 104 40- 127
Surrogate Decachlorobipheny (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0238 0218 0189 0181
gI
gI
gI
gI
0200 0200 0200 0200
119 109
30- 150 30- 150 30- 150 30- 150
This laboratory report is lot valid without (II authorized sigllature 01 the cover page
Page 18 of25 Reportable Detection Limit BRL = Below Reporting Limit
Extractable Petroleum Hydrocarbons - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051102 - SW846 3510C
Blank 8051102-BLK1
Prepared 15-May-08 Analyzed 19-Mayshy
Non-polar material (SGT- HEM) BRL m91
LC8 8051102-B81
Prepared 15-May-08 Analyzed 19-Mayshy
Non-polar material (SGT- HEM) 184 m91 21 81 904
This laboratory report is not valid without an authorized signature 011 the cover page
Page 19 of25 Reportable Detection Limit BRL = Below Reporting Limit
Soluble Metals by EPA 200 Series Methods - Quality Control
Analyte(s) Result Flag Units RDL
Spike
Level
Source
Result REC
REC
Limits RPD
RPD
Limit
Batch 8051150 - EPA 200 Series
Blank 8051150-BLK1
Prepared amp Analyzed 21-May-
Iron
Zinc
Selenium
Nickel
Chromium
Copper
Arsenic
BRL
BRL
BRL
BRL
BRL
BRL
BRL
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0150
0050
0150
0050
0050
0050
0040
LCS 8051150-BS1
Prepared amp Analyzed 21-May-
Selenium
Zinc
Iron
Nickel
Chromium
Arsenic
Copper
123
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0150
0050
0150
0050
0050
0040
0050
103
105
101
100
85- 115
85- 115
85- 115
85- 115
85- 115
85-115
85- 115
licate B051150-DUP1 Source SA7B602shy
Prepared amp Analyzed 21-May-
Iron
Zinc
Selenium
Nickel
Copper
Chromium
Arsenic
17
0162
BRL
0015
0017
BRL
0450
QR8
mgl
mgl
mgl
mgl
mgl
mgl
mgi
0150
0050
0150
0050
0050
0050
0040
184
0186
BRL
0014
0023
BRL
0468
Matrix S ike 8051150-MS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Iron
Selenium
Nickel
Zinc
Copper
Chromium
Arsenic
19 QM2 mgl
mgll
mgl
mgl
mgl
mgl
mgl
0150
0150
0050
0050
0050
0050
0040
125
184
BRL
0014
0186
0023
BRL
0468
104
105
102
70- 130
70- 130
70-130
70- 130
70- 130
70-130
70- 130
Post S ike 8051150-PS1 Source SA78602shy
Prepared amp Analyzed 21-May-
Zinc
Iron
Selenium
Nickel
Copper
Arsenic
Chromium
18 QM2
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0050
0150
0150
0050
0050
0040
0050
0186
184
BRL
0014
0023
0468
BRL
104
104
101
85- 115
85- 115
85- 115
85-115
85-115
85- 115
85-115
Batch 8051152 - EPA200SW7000 Series
Blank B051152-BLK1
Prepared amp Analyzed 21-May-
Mercury BRL mgl 00020
This laboratory report is IIOt valid witllOut all authorized sigllature 011 the coverpage
Page 20 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Soluble Metals by EPA 200 Series Methods - Quality Control
Analyte(s) Result Flag Units RDL
Spike
Level
Source
Result REC
REC
Limits RPD
RPD
Limit
Batch 8051152 - EPA200SW7000 Series
LCS B051152-BS1
Prepared amp Analyzed 21-May-
Mercury 00576 m91 00020 00500 115 85- 115
licate B051152-DUP1 Source SA78602-01
Prepared amp Analyzed 21-May-
Mercury BRL m91 00020 BRL
Matrix S ike 8051152-MS1 Source SA78602shy
Prepared amp Analyzed 21-May-
Mercury 00632 OM m91 00020 00500 BRL 126 75- 125
Post S ike 8051152-PS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Mercury 00624 OC1 m91 00020 00500 BRL 125 85- 115
Batch 8051249 - 2008No digestion
Blank 8051249-BLK1
Prepared amp Analyzed 21-May-
Lead
Antimony
Cadmium
Silver
BRL
BRL
BRL
BRL
m91
m91
m91
m91
0002
0002
0002
0002
LCS B051249-BS1
Prepared amp Analyzed 21-May-
Antimony
Lead
Silver
Cadmium
143
145 OC2
m91
m91
m91
m91
0050
0050
0050
0040
103
115
107
116
85- 115
85- 115
85- 115
85- 115
licate 8051249-DUP1 Source SA7B602shy
Prepared amp Analyzed 21- May-
Lead
Antimony
Cadmium
Silver
0009
0002
00005
00002
ORB
m91
m91
m91
m91
0002
0002
0002
0002
0011
0003
00005
00003
Matrix S ike 8051249-MS1 Source SA78602shy
Prepared amp Analyzed 21- May-
Lead
Antimony
Cadmium
Silver
142
m91
m91
m91
m91
0050
0050
0040
0050
0011
0003
00005
00003
111
101
114
102
70- 130
70-130
70c130
70- 130
Post S ike 8051249-PS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Antimony
Cadmium
Silver
38
OC2
m91
m91
m91
0050
0040
0050
125
0003
00005
00003
110
121
109
85- 115
85- 115
85- 115
This laboratory report is flOt valid IVithout all authorized signature 011 the cOIer page
Reportable Detection Limit BRL Below Reporting Limit Page 21 of 25
General Chemistry Parameters - Quality Control
Spike Source REC RPD
Analyte( s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051049 - General Preparation
Blank S051 049-BLK1
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
Blank S051049-BLK2
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
Blank S051 049-BLK3
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
LCS S051049-BS1
Prepared amp Analyzed 14-May-
Total Residual Chlorine 046 mgl 020 0500 90- 110
LCS S051049-BS2
Prepared amp Analyzed 14-May-
Total Residual Chlorine 047 mgl 020 0500 90- 110
LCS S051049-BS3
Prepared amp Analyzed 14-May-
Total Residual Chlorine 054 mgl 020 0500 108 90-110
licate B051049-DUP1 Source SA7S544shy
Prepared amp Analyzed 14-May-
Total Residual Chlorine 012 mgl 020 010
licate S051049-DUP2 Source SA7S602-01
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020 BRL
Matrix S ike 8051049-MS1 Source SA78544-01
Prepared amp Analyzed 14-May-
Total Residual Chlorine 065 mgl 020 0500 010 110 80- 120
Matrix S ike 8051049-MS2 Source SA7B602shy
Prepared amp Analyzed 14-May-
Total Residual Chlorine mgl 500 125 BRL 108 80- 120
Reference 8051 049-SRM1
Prepared amp Analyzed 14-May-
Total Residual Chlorine 100 mgl 020 0967 103 85-115
Batch 8051094 - General Preparation
Blank 8051094-BLK1
Prepared amp Analyzed 14 May-
Hexavalent Chromium (soluble) BRL mgl 005
Blank 8051 094-BLK2
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) BRL mgl 005
LCS 8051094-BS1
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) 054 mgl 005 90- 110
licate 8051094-DUP1 Source SA78602-01
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) BRL mgl 125 BRL
Thi laboratory report is not valid without all authorized sigllature 011 the cover page
Page 22 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Page 4
----
3 Contam
inant information In order to com
plete this section the applicant
il need to take a minim
um of one sam
ple of the untreated water and have it analyzed for all of the
parameters listed in A
ppendix III Historical data (i
data taken no more than 2 years prior to the effective date of the perm
it) may be used if obtained pursuant to i
Massachusetts regulations 310 C
MR
40 0000 the Massachusetts C
ontingency Plan (Chapter 21E ) ii N
ew H
ampshire s T
itle 50 RSA
485- A W
ater Pollution and Waste
Disposal or T
itle 50 RSA
485- C G
roundwater Protection A
ct or iii an EPA
pennit exclusion letter issued pursuant to 40 CFR
122 provided the data w
as analyzed with test
methods that m
eet the requirements of this perm
it Otherw
ise a new sam
ple shall be taken and analyzed
a) Based on the analysis of the sam
ple(s) of the untreated influent the applicant must check the box of the sub-categories that the potential discharge falls w
ithin
Gasoline O
nly V
OC
Only
Primarily M
etals U
rban Fill Sites C
ontaminated Sum
ps Mixed Contaminants
Aquifer T
esting
VO
C w
ith Other
Petroleum w
ith Other
Listed C
ontaminated
Contam
inated H
ydrostatic Testing of
Well D
evelopment or
Other O
ils) only C
ontaminants
Contam
inants Sites
Dredge C
ondensates PipelinesT
anks R
ehabilitation F
uel Oils (and
b) Based on the analysis of the untreated influent the applicant m
ust indicate whether each listed chem
ical is believed present or believed absent in the potential discharge A
ttach additional sheets as needed
PAR
AM
ET
ER
B
elieve B
elieve of
Type of
Analytical
Minim
um
Maxim
um daily value
Avg daily value
Absent
Present Sam
ples Sam
ple M
ethod L
evel (ML
) of
(1 min-
(eg grab) U
sed T
est Method
concentration m
ass concentration
mass
imum
) (m
ethod ) (ugI)
( ugI) (kgday)
(ugI) (kgday)
1 Total Suspended Solids
GR
A
SM 2540D
000
580 000 215
SW-846
GR
A
100 c 500
2 Total R
esidual 9012A
C
hlorine
3 Total Petroleum
G
RA
1664
000 600
12
Hydrocarbons
4 Cyanide
GR
A
9012A
cl0
c20S B
enzene G
RA
B
5030
6 Toluene
GR
A
5030 c20
7 Ethylbcnzene
GR
A
5030 411
8 (m
o) Xylenes
GR
A
5030 10
472
9 Total B
TE
X
GR
A
5030 883
04
BT
EX
= SU
IU of B
enzene Toluene
Ethylbenzene
total Xylenes
Rem
ediation General Perm
it - Notice of Intent
PAR
AM
ET
ER
B
elieve B
elieve of
Type of
Absent
Present Sam
ples S
ample (eg
(1 min-
grab)
imum
)
10 Ethylene
Dibrom
ide G
RA
B
(1 2- Dibrom
o-methane)
11 Methyl-tert-B
utyl G
RA
Ether (M
tBE
)
12 tert-
Butyl
Alcohol
GR
AB
(TB
A)
13 tert-A
myl
Methyl
GR
A
Ether (T
AM
E)
14 Naphthalene
GR
AB
15 Carbon T
etra-G
RA
chloride
16 1
Dichlorobenzene
GR
A
17 D
iehlorobenzene G
RA
GR
A18 1
Dichlorobenzene
19 1
Dich1oroethane
GR
A
20 1
Dichloroethane
GR
A
21 1
Dichloroethylene
GR
A
22 cis-D
ichloro-G
RA
B
ethylene
GR
A
(Methylene C
hloride)
23 D
ichloromethane
24 T
etrachloroethylene G
RA
B
Rem
ediation General Perm
it - Notice of Intent
Analytical
Minim
um
Maxim
um daily value
Avg daily value
Method
Level (M
L) of
Used
Test M
ethod concentration
mass
concentration m
ass
(method )
(ugI) ( ug)
(kgday) (ugI)
(kgday)
504 010
0 0
5030 05
020
5030 0200
5030 020
625 247
5030 020
5030 020
5030 05
020
5030 020
5030 020
5030 020
5030 05
020
5030 020
5030 10
0200
5030 020
PAR
AM
ET
ER
B
elieve B
elieve of
Type of
Absent
Present Sam
ples Sam
ple (e
(l min-
grab)
imum
)
25 1
1 Trichloroethane
GR
AB
26 1
2 Trichloroethane
GR
A
27 Trichloroethylene
GR
AB
28 Vinyl C
hloride G
RA
B
29 Acetone
GR
A
30 14 D
ioxane G
RA
B
31 Total Phenols
GR
AB
32 Pentachlorophenol
GR
AB
33 Total Phthalates 6
GR
AB
(phthalate esthers)
34 Bis (2-E
thylhexyl) G
RA
B
Phthalate (D
ishy(ethylhexyl) P
hthalate)
35 Total G
roup 1 G
RA
P
olycyclic Arom
atic H
ydrocarbons (PA
H)
a Benzo(a) A
nthracene G
RA
B
b Benzo(a) P
yrene G
RA
c Benzo(b )F
luoranthene G
RA
B
d Benzo(k) F
luoranthene G
RA
e Chrysene
GR
AB
The slim
of iijdividual phthalate compounds
Rem
ediation General Perm
it - Notice of Intent
Analytical
Minim
um L
evel M
aximum
daily value A
vg daiJy Value
Method Used
(ML) ofT est
(method )
Method
concentration m
ass concentration
mass
(ugI) (ugI)
(kgday) (ugl)
(kgday)
5030 20
5030 20
5030 20
5030 ~20
5030 400
5030 200
625 50
625 50
625 All phthalates are
BD
L see lab report
625 50
625 A
ll Group I P A
Hs
are BD
L
625 50
625 50
625 50
625 50
625 50
g
PAR
AM
ET
ER
B
elieve B
elieve of
Type of
Analytical
Minim
um
Maxim
um daily value
Average daily value
Absent
Present Sam
ples Sam
ple (e M
ethod Used
Level (M
L) of
(lmin -
grab) (m
ethod ) T
est Method
concentration m
ass concentration
mass
imum
) (ug1)
(ugl) (kgday)
(ugl) (kgday)
f Dibenzo(a
GR
AB
625
-(50
anthracene
Indeno(I 23-cd) G
RA
B
625 -(50
Pyrene
36 Total G
roup II G
RA
B
625 247
Polycyclic A
romatiC
H
ydrocarbons (pAR
)
h Acenaphthene
GR
AB
625
-(10
i Acenaphthylene
GR
A
625 -(50
j Anthracene
GR
A
625 -(50
k Benzo(ghi)
Perylene G
RA
B
625 -(50
I Fluoranthene G
RA
B
625 -(50
m F
luorene G
RA
B
625 -(50
n Naphthalene-
GR
AB
625
247
o Phenanthrene
GR
AB
625
-(50
p Pyrene
GR
AB
625
-(50
37 Total
POlychlorinated
GR
AB
608
065 -(0065
Biphenyls (PC
Bs)
38 Antim
ony G
RA
B
200 03
4Eshy
39 Arsenic
GR
AB
200
468
40 Cadm
ium
GR
AB
200
-( 0
41 Chrom
ium II
(1) G
RA
B
calculated calculated
-(5
42 Chrom
ium V
I G
RA
7196A
-( 125
NO
TE
S (1) Chrom
ium m
= T
otal Chrom
ium - H
exavalent Chrom
ium A
ccording to lab personnel the trivalent chromium
is calculated to be greater or equal to 5 ugI but less than 125 ugl Total
Chrom
ium w
as -(5 ugI and the Hexavalent C
hromium
was less than 125 ugl
Rem
ediation General Perm
it - Notice of Intent
--------
--------
-------
--------
---
PAR
AM
ET
ER
B
elieve B
elieve of
Type of
Analytical
Minim
um
Maxim
um daily value
Avg daily value
Absent
Present Sam
ples Sam
ple (e M
ethod L
evel (ML
) of grab)
Used
Test M
ethod concentration
mass
concentration m
ass(1 m
inshy
imum
) (m
ethod ) (ug1)
(ug1) (kgday)
(ug1) (kgday)
43 Copper
GR
A
200 (5
44 Lead G
RA
200
0001
45 Mercury
GR
A
7470A
(020
46 Nickel
GR
AB
200
(5
GR
AB
200
( 1547 Selenium
48 Silver G
RA
B
200 (0
49 Zinc
GR
A
200 18
0025
50 Iron G
RA
B
200 400
25
Other (describe)
c For discharges where m
etals are believed present please fill out the following
If yes which m
etals A
rsenic and Iron Step
I Do any of the m
etals in the influent have a reasonable potential to exceed the
etIluent limits in A
ppendix II (i the limits set at zero to five dilutions) Y
rg N D
Step 2 For any m
etals which have reasonable potential to exceed the A
ppendix III limits
Look up the lim
it calculated at the corresponding dilution factor in
calculate the dilution factor (DF) using the form
ula in Part I A 3 c) (step 2) of the N
O
Appendix IV
Do any of the m
etals in the influent have the potential to instructions or as determ
ined by the State prior to the submission of this N
OI
exceed the corresponding effuent lim
its in Appendix IV
(i is the
What is the dilution factor for applicable m
etals in1uent concentration above the lim
it set at the calculated dilution M
etals A
rsenic and Iron factor)
yrgND
If Y
es list which m
etals A
rsenic and Iron
DF
Rem
ediation General Pem
lit - Notice of Intent
4 Treatm
ent system inform
ation Please describe the treatment system
using separate sheets as necessary including
a) A description of the treatm
ent system including a schem
atic of the proposed or existing treatment system
S
ee Figures 4 and 5
Frac tank Air stripper
Oilw
ater separator Equalization tanks
Bag filter rg
GA
C filter rg
b) Identity each applicable
treatment unit (check alJ
that apply)
Chlorination
Dechlorination
Other (please describe)
c) Proposed average and maxim
um flow
rates (gallons per minute) for the discharge and the design flow
rate(s) (gallons per minute) ofthe treatm
ent system
Average flow
rate of discharge 15 G
PM
Maxim
um flow
rate oftreatment system
0 G
PM
Design flow
rate of treatment system
0 G
PM
d) A description of chem
ical additives being used or planned to be used (attach MSD
S sheets) Not A
pplicable
5 Receiving surface water(s) Please provide information about the receiving water (s) using separate sheets as necessary including
Identity the discharge pathway
I Direct
I Within facility
I Stonn drain rg I R
iverbrook I W
etlands _ I Other (describe)
Provide a narrative description ofthe discharge pathway including the nam
e(s) of the receiving waters
Discharge to catchbasin and stonnw
ater drainage system in E
ast Broadw
ay which discharges to M
ahoney Brook (S
ee Figure 4)
c) Attach a detailed m
ap(s) indicating the site location and location of the outfall to the receiving water
1 For multiple discharges num
ber the discharges sequentialJy 2 For indirect dischargers indicate the location of the discharge to the indirect conveyance and the discharge to surface w
ater T
he map should also include the location and distance to the nearest sanitary sew
er as well as the locus of nearby sensitive receptors (based on U
SGS topographical
mapping) such as surface w
aters drinking water supplies and w
etland areas d) Provide the state w
ater quality classification of the receiving water
e) Provide the reported or calculated seven day- ten year low flow
(7QlO
) of the receiving water Jcfs
Please attach any calculation sheets used to support stream flow
and dilution calculations See A
ttachment B
f) Is the receiving water a listed 303(d) w
ater quality impaired or lim
ited water Y
es 0 No rg
If yes for which polJutant(s) N
A
Is there a TM
DL
Yes 0
No rg If yes for w
hich pollutant(s) NA
Rem
ediation General Perm
it - Notice of Intent
6 Results of C
onsultation with Federal Services Please p
rovide the following information according to requirements of Par
lBA
and A
ppendices II and VII
a) Are any listed threatened or endangered species or designated critical habitat in proxim
ity to the discharge Yes 0
No rg
Has any consultation w
ith the federal services been completed Y
es 0 No rg
or is consultation underway Y
es 0 No rg
What w
ere the results of the consultation with the U
S Fish and Wildlife Service andor N
ational Marine Fisheries Service (check one) N
ot applicable
a nojeopardy opinion
or written concurrenceD
on a finding that the discharges are not likely to adversely affect any endangered species or critical habitat
b) Are any historic properties listed or eligible for listing on the N
ational Register of H
istoric Places located on the facilty or site or in proximity to the discharge
Yes D
No
Have any state or tribal historic preservation offcer been consulted in this determ
ination (Massachusetts only) Y
es O N
o
7 SU
DD
lemental inform
ation
Please provide any supplemental information Attach any analytical data used to support the application A
ttach any celtification(s) required by the general permit
Attachm
ent A - Figures
Figure I - Site Locus M
ap
Figure 2 - MassD
EP Site Scoring M
ap
Figure 3 - Aerial M
ap
Figure 4 - Proposed Soil Excavation A
rea Map
Figure 5 - T
reatment S
ystem Line D
iagram
Attachm
ent B - D
ilution factor Calculations
Attachment C - L
aboratory Analytical R
eport Groundw
ater
Rem
ediation General Perm
it - Notice of 1ntenl
=-
including the following
8 Signature Requirements
The N
otice ofIntent must be signed by the operator in accordance w
ith the signatory requirements of 40 C
FR Section 122
certification
J certif under penalty of law that this docum
ent and all attachments w
ere prepared under my direction or supervision in accordance w
ith a system
designed to assure that qualifed personnel properly gather and evaluate the information subm
itted Based on m
y inquiry of the person or persons who
manage the system
or those persons directly responsible for gathering the information I certif that t
he information submitted
is to the best of m
y
knowledge and belief true accurate and com
plete J certif that I am aw
are that there are signifcant penalties for submitting false inform
ation including
the possibilty of fine and imprisonm
ent for knowing violations
FacilitySite Name
Form
er Speedw
ay Service S
tation 181 East B
roadwav G
ardner MA
01440
Operator signature
Title
Michael 1 D
ziura Sf Env E
ngineer
Date
4150- q
Rem
ediation General Perm
it - Notice of Intent
-
D- 0
0 0
il (J tu
Bw
o(0 -I
NJW
gQb
J(JZc o c
rou a -10
0 J 6shy
a 0
I-tDC
aJ Qj
E aJshy
ro ro ro
~~~ ~~~~- -- - _ - -_ - ~~~ ~~~~ ~~~ - - _- _- -- -- p __(
MA DEP - Bureau of Waste Site CleanupSITE NME Site S aP 5 MiFlII Former Speeway Station _-II181 Eat Broaday b b d IS I i I GARDNER MA 0144 v ri) i P f f 1 me- 1 5ylmI I L shy J --I 423315n 715835e SiteLocation y o oCop1odQcn Ofof W-_ l
1 1 I
r
r
iBARBER HILL
A c
Cf1 f o s
0
5
Roads Uned Acss Divd Mar Roed Conntor Street Track 1 EPA Sola Source Aquilar FEMA 100yaar iloodplain 0 c Puc Watar SLo GrunSelaceNon Corrty 0
Bounars lOwn Couny DE Region Tian Powerln Ine Aqedut ApprOld Zona2 tNPA Sue Wster Supp Zone A bStZ F--shy--rle
8os Mat Sub SUeor Porenrial Inermtent Man lvo8 Ste Dfm Hyro1apy Wmer FeatllePLio Suleee Wat S H-- L otlMds FrslSaltN-ES WeIMd Habat L
Potentia Prdutiv AqlJlers ModHig Yield Proteoted Opn Space ACC nIL c= Non-Potential Drng Water Sollce AIea ModumHi Yo1d ll DEP Pormrd SoidWes1 FsiIi6s cnifud Verne Pools f0
1I2 KIWUmR$ MtL
January 30 2004 SCALE 1 15000
-
LE
GE
ND
APX PROPER BONDA
- APPROXOiSPO SIT BOUNDA
-GR
OU
ND
WA
TE F1 D
IRE
cnON
SCA
LE
30 60 FE
(APR
OX
CORPORATE ENVIRONMENTAL
)i
AD
VISO
RS
INC
SC
AS SH
OW
D
R B
Y K
HA
EL
DA
TE
10407
JOB
NO
2920-96
AERIAL MAP
FO
RM
ER
SP
EE
DW
AY
ST
AT
ION
FlGURE -3
181 EA
BR
OA
AY
GA
NE
R fo
age 1 ot 1Streamflow Statistics Report
Streamstats Ungaged Site Report Date Wed Dec 31 2008 124908 Site Location Massachusetts NAD83 Latitude 425545 (42 3316) NAD83 Longitude -719758 (-71 58 32) NAD27 Latitude 425545 (423316) NAD27 Longitude - 9763 (-71 58 34) Drainage Area 502 mi2
IPeak Flow Basin Characteristics 1100 Statewide Low Flow (S02 mi2)
Regression Equation Valid Rang
I Min II Max1 Value III Parameter Drainage Area (square miles) 161 149
Mean Basin Slope from 250K DEM (percent) 032 24
Stratified Drift per Stream Length (square mile per mile) 129
Massachusetts Region (dimensionless)
Streamflow Statistics
gO-Percent Prediction Interval Prediction Error
MaximumStatistic Flow (ft s) (percent) Minimum
I D50 IIII 11 1811 II 24511 993
I D60 II 35511 2011 II 03611 35111 2411 II 041 I 201I D70 24111 2611 II 03811 151I D75 11 2811 II 0911 3761I D80 981I D85 1 I 3211 II o6311
1 I 3711 II 0441 1 2 2911 D90 11 4611 II 02411 15511 D95I D98 04511 6011 II 01511 11
I D99 03411 6511 II ol1ll 1021
5011 II 02611 11I M7D2Y 1111 3311 II odl 3 541
I AUGD50
IIIIIIIIIIIIIIIIIIIIII 0311 7111 II 0088411 0981I M7Dl0Y
1010
12312008httpstreamstatsagscrusgsgovgisimgReportsFlowStatsReport3494 - 2008123112498
Dilution Factor Calculation Former Speedway Service Station 181 East Broadway Gardner Ma
DF=(Od+Os)Od
DF = Dilution factor
Od = Max flow rate of discharge in cubic feet per second Os = receiving water flow in cubic feet per seconds 7010 flow rate Mahoney Brook 7010 = min flow for seven consecutive days with a recurrence interval of 10 years
7010 flow based on data obtained from USGS Steamflow Statistics Report Data attached
067
Semivolatile Organic Compounds by GCMS - Quality Control
Analyte( s)
Batch 8051216 - SW846 3510C
Blank 8051216BLK1)
Prepared amp Analyzed 16May-
Acenaphthene
Acenaphthylene
Aniline
Anthracene
AzobenzenelDi phenyld iazi ne
Benzidine
Benzo (a) anthracene
Benzo (a) pyrene
Benzo (b) fiuoranthene
Benzo (g i) perylene
Benzo (k) fiuoranthene
Benzoic acid
Benzyl alcohol
Bis(2-ch loroethoxy) methane
Bis(2-ch loroethyl)ether
Bis(2-ch loroi sopropyl)ether
Bis(2ethylhexyl) phthalate
Bromophenyl phenyl ether
Butyl benzyl phthalate
Carbazole
Ch loro-3-methyl phenol
Chloroaniline
Chloronaphthalene
Chlorophenol
Chlorophenyl phenyl ether
Chrysene
Dibenzo (a h) anthracene
Dibenzofuran
Dichlorobenzene
Dichlorobenzene
14- Dichlorobenzene
3 - Dichlorobenzidine
24-Dichlorophenol
Diethyl phthalate
Dimethyl phthalate
24- Dimethylphenol
Din-butyl phthalate
Dinitro-2-methylphenol
Dinitrophenol
Dinitrotoluene
Dinitrotoluene
Di-noctyl phthalate
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopehtadiene
Hexachloroethane
Indeno (1 cd) pyrene
Spike Source REC RPD
Result Flag Units RDL Level Result REC Limits RPD Limit
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gl
BRL gI
BRL gl
BRL gl
BRL gl
BRL gI
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gll
BRL gl
BRL gll
BRL gl
BRL gl
BRL gI
BRL gI
BRL gI
BRL gl
BRL gI
BRL gI
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gI
BRL gI
BRL gl
This laboratory report is IlOt valid without all authorized sigllature 011 the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page t4 of25
Volatie Organic Compounds - Quality Control
p (
Spike Source REC RPD
RDL Level Result REC Limits RPD Limit Analyte(s) Result Flag Units
Batch 8051244 - SW846 5030 Water MS
Matrix S ike Du 8051244-MSD1 Source SA78629shy
Prepared 16-May-08 Analyzed 17-May-BRL 106 251
Vinyl chloride 21 gl 20
101 70- 130 Surrogate 4-Bromofluorobenzene 50 gl 50
70- 13049 gl 50 111 70- 130
Surrogate Toluene-Surrogate 1 Dichloroethane- 55 gl 50
50 70- 130494 glSurrogate Dibromofluoromethane
Microextractable Organic Compounds - Quality Control
Spike Source REC RPD
Flag Units RDL Level Result REC Limits RPD Limit Analyte(s) Result
Batch 8051105 - SW846 3510C
Blank 8051105-BLK
Prepared amp Analyzed 15-May-
BRL gl 01001 Dibromoethane (ED B)
LCS 8051105-BS1
Prepared amp Analyzed 15-Mayshy50- 1500770 gl 0100 100
licate 8051105-DUP1 Source SA7B583shy
Prepared amp Analyzed 15-May-
BRL gl 0100 BRL
1 Dibromoethane (EDB)
1 Dibromoethane (EDB)
This laborntOlY report is not valid without an authorized signature 011 the cover page
Page 13 of2S Reportable Detection Limit BRL = Below Reporting Limit
Sam le Identification Client Pro ect Matrix Collection DateTime ReceivedMWshy
2920-96- Ground Water 13-May-081030 14-May-SA 78602shy
CAS No Analyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Volatile Organic Compounds
Volatile Or anic Com ounds b GCMS
Prepared by method SW846 5030 Water MS
123-91- Dioxane BRL 1-91 200 EPA 624 16-May-08 17-May-08 8051244
994-05-8 Ter-amyl methyl ether BRL 1-911 20
755- Tert-Butanoll butyl alcohol BRL 1-91 200
67-B4- Acetone BRL 1-91 400
71-43- Benzene BRL 1-91 20
75-27-4 Bromodichloromethane BRL 1-91 20
75-25- Bromoform BRL 1-91 20
74-83- Bromomethane BRL 1-91 40
78-93- Butanone (MEK) BRL 1-91 200
56-23- Carbon tetrachloride BRL 1-91 20
108-90- Chlorobenzene BRL 1-91 20
75-00- Chloroethane BRL 1-91 40
676- Chloroform BRL 1-91 20
74-87- Chloromethane BRL 1-91 40
124-48- Dibromochloromethane BRL 1-91 20
95-50- Dichlorobenzene BRL 1-911 20
541-73- Dichlorobenzene BRL 1-91 20
106-46- Dichlorobenzene BRL 1-91 20
75-34- 1- Dichloroethane BRL 1-91 20
107-06- Dichloroethane BRL 1-91 20
75-35-4 1- Dichloroethene BRL 1-91 20
156-59 cis- Dichloroethene BRL 1-91 20
156-60- trans- Dichloroethene BRL 1-91 20
78-87- 2- Dichloropropane BRL 1-91 20
10061-01-5 cis- Dichloropropene BRL 1-91 20
10061-02-B trans- Dichloropropene BRL 1-91 20
100-41-4 Ethylbenzene 411 1-911 20
591-78-B BRL 200Hexanone (MBK) 1-91
1634-04 -4 Methyl tert-butyl ether BRL 1-91 20
108-10- Methyl- pentanone (MIBK) BRL 1-91 200
75-09- Methylene chloride BRL 1-91 200
100-42- Styrene BRL 1-91 20
79-34- 1 Tetrachloroethane BRL 1-91 20
127- 18-4 T etrachloroethene BRL 1-91 20
108-88- Toluene BRL 1-91 20
71-55 1- Trichloroethane BRL 1-91 20
79-00- 2- Trichloroethane BRL 1-91 20
79-01-B Trichloroethene BRL 1-91 20
759-4 Trichlorofluoromethane (Freon 11) BRL 1-91 20
75-01-4 Vinyl chloride BRL 1-91 20
179601-23-1 m Xylene 390 1-91 40
95-47 Xylene 82 1-91 20
Surrogate recoveries 460-00- Bromofluorobenzene 70- 130
2037-26- Toluene- 100 70- 130
17060-07-0 1 Dichloroethane- 111 70- 130
1868-53- Dibromofluoromethane 70- 130
Microextractable Organic Compounds
106-93-4 1 Dibromoethane (EDB) BRL 1-91 0100 EPA 504 15-May- 15-May-08 8051105
Semivolatile Organic Compounds by GCMS
This laboratory report is not valid without all autllOrized signature 011 the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page 5 of 25
Sam le Identification Client Pro ect Matrix Collection DateTime Received
MWshy2920-96- Ground Water 13-May-081030 14-May-
SA 78602shy
CAS No Analyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Semivolatie Organic Compounds by GCMS
Semi volatile Or anic Com ounds b EPA 625
Prepared by method SW846 3510C 50 EPA 625 16-May- 19-May-08 805121683-32- Acenaphthene BRL IJgl
208-96-8 Acenaphthylene BRL IJgl 50
62-53- BRL IJgll 50Aniline
120- 12- Anthracene BRL 1J91 50
103-33- AzobenzenefDiphenyldiazine BRL IJgl 50
92-87 - Benzidine BRL IJgl 50
56-55- Benzo (a) anthracene BRL 1J91 50
50-32 - Benzo (a) pyrene IJglBRL 50
205-99- Benzo (b) fluoranthene BRL IJgl 50
191-24- Benzo (g i) perylene BRL IJgl 50
50207-08- Benzo (k) fluoranthene BRL IJgl
65-85 Benzoic acid BRL 1J91 50
100-51-6 Benzyl alcohol 1J91BRL 50
50111-91- Bis(2-chloroethoxy)methane BRL 1J91
111-4-4 Bis(2-chloroethyl)ether BRL IJgl 50
501 08-60- Bis(2-chloroisopropyl)ether BRL IJgl
117-81- Bis(2-ethylhexyl)phthalate BRL 1J91 50
101-55- Bromophenyl phenyl ether BRL IJgl 50
5085-68- Butyl benzyl phthalate BRL IJgl
5086-74- Carbazole BRL IJgl
5059-50- C hloro-3-methylphenol BRL IJgl
106-47- Chloroaniline BRL IJgl 50
91-58- Chloronaphthalene IJglBRL 50
5095-57 - Chlorophenol BRL 1J91
507005-72- Chlorophenyl phenyl ether BRL IJgl
216-01- Chrysene tJ91BRL 50
5053-70- Dibenzo (a h) anthracene BRL IJgl
50132-64- Dibenzofuran BRL IJgl
95-50- Dichlorobenzene IJglBRL 50
541-73- 13- Dichlorobenzene BRL IJgl 50
106-46- Dichlorobenzene 1J91BRL 50
5091-94- 3 - Dichlorobenzidine BRL IJgl
120-83- Dichlorophenol BRL IJgl 50
84-66- Diethyl phthalate BRL IJgl 50
131-11- Dimethyl phthalate BRL IJgll 50
105-67- Dimethylphenol BRL 1J91 50
5084-74- Di-n- butyl phthalate BRL 1J91
534-52 - Dinitro-2-methylphenol BRL IJgl 50
51-28- Dinitrophenol IJglBRL 50
50121-14- Dinitrotoluene BRL 1J91
606-20- Dinitrotoluene IJglBRL 50
50117-84-0 Di-n-octyl phthalate BRL IJgl
206-44-0 Fluoranthene 1J91BRL 50
BRL 50
50 86-73- Fluorene IJgi
118-74- Hexachlorobenzene BRL 1J91
87-68- Hexachlorobutadiene 1J91BRL 50
5077-47-4 Hexachlorocyclopentadiene BRL IJgl
67-72- Hexachloroethane IJglBRL 50
50193-39- Indeno (1 3-cd) pyrene BRL IJgl
5078-59- Isophorone BRL IJgl
Tfls laboratory report is not valid without all authorized signature 011 the coverpage
Page 6 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Sam le Identification Client Pro ect Matrix Collection DateTime ReceivedMWshy
2920-96- Ground Water I3-May-081030 14-May-SA 78602shy
CAS No Analyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Semivolatile Organic Compounds by GCMS
Semi volatile Or anic Com ounds b EPA 625
Prepared by method SW846 3510C
91-57 -6 Methylnaphthalene 367 1-91 50 EPA 625 16-May- 19-May-08 8051216
95-48- Methylphenol BRL 1-91 50
108-39-4 3 amp 4-Methylphenol BRL I-gl 100 106-44shy91-20- Naphthalene 247 1-91 50
88-74-4 Nitroaniline BRL 1-91 50
99-09- Nitroaniline BRL 1-91 50
100-01-6 Nitroaniline BRL 1-91 50
98-95- Nitrobenzene BRL 1-91 50
88-75- Nitrophenol BRL 1-91 50
100-02- Nitrophenol BRL 1-91 50
62-75- Nitrosodimethylamine BRL 1-91 50
621-64- N- Nitrosodi-n-propylamine BRL 1-91 50
86-30-6 Nitrosodiphenylamine BRL 1-91 50
87 -86- Pentachlorophenol BRL 1-91 50
85-0- Phenanthrene BRL 1-91 50
108-95- Phenol BRL 1-91 50
129-00-0 Pyrene BRL 1-91 50
110-86- Pyridine BRL 1-91 50
120-82- 4- Trichlorobenzene BRL 1-91 50
95-95- 5- Trichlorophenol BRL 1-91 50
88-06- 6- T richlorophenol BRL 1-91 50
Surrogate recoveries
321-60- Fluorobipheny 30- 130
367- 12- Fuorophenol 15- 110
4165-60- Nitrobenzene- 30- 130
4165-62- Pheno- 15- 110
1718-51- Terpheny-d4 30- 130
118- 79- 6- Tribromophenol 15- 110
Semivolatile Organic Compounds by GC
Pol chlorinated Bi hen ls b EPA 608
Prepared by method SW846 3510C
12674- 11-2 Aroclor- 1016 BRL 1-91 0650 EPA 608 15- May- 16-May-08 8051106
11104-28-2 Aroclor-1221 BRL IJgl 0650
11141-16-5 Aroclor- 1232 BRL 1-91 0650
53469-21-9 Aroclor- 1242 BRL 1-91 0650
12672-29-6 Aroclor- 1248 BRL 1-91 0650
11097-69-1 Aroclor- 1254 BRL 1-91 0650
11096-82-5 Aroclor -1260 BRL 1-91 0650
37324-23-5 Aroclor-1262 BRL 1-91 0650
11100-14-4 Aroclor-1268 BRL IJgl 0650
Surrogate recoveries
2051-24- Decachlorobipheny (Sr) 105 30- 150
10386-84-2 4 DB-Octafluorobiphenyl (Sr) 30- 150
Extractable Petroleum Hydrocarbons
mgl EPA 1664 Rev A 15-May- 19-May-08 8051102Non-polar material (SGT- HEM)
Soluble Metals by EPA 2006000 Series Metbods
Field Filtered NA EPA 200 73005A 15- May- 15-May-08 8051192Filtration
Soluble Metals by EPA 200 Series Methods
7440-22-4 Silver BRL mgl 0002 EPA 200 21-May- 27- May-08 8051249
This laboratory report is IlOt mlid without (II authorized signature on the cover page
Reportble Detection Limit BRL = Below Reporting Limit Page 7 of 25
Sam le Identification MW-
Client Pro ect 2920-96shy
Matrix Ground Water
Collection DateTime 13-May-08 1030
Received 14-May-
SA 78602shy
CAS No A nalyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Soluble Metals by EPA 200 Series Methods
7440-38shy Arsenic 0468 mg1 0040 EPA 200 21-Mayshy 21-May-08 80511 50
7440-43shy Cadmium BRL mg1 0002 EPA 200 21-May-088051249
7440-47shy Chromium BRL mg1 0050 EPA 200 21-May-088051150
7440-50-8 Copper BRL mg1 0050
7439-89-6 Iron 184 mg1 0150
7439-97-6 Mercury BRL mg1 00020 EPA 245 17470A 21-May-088051152
7440-02-0 Nickel BRL mg1 0050 EPA 200 21-May-088051150
7439-92shy Lead 0011 mg1 0002 EPA 200 21-May-088051249
7440-36-0 Antimony 0003 mg1 0002
7782-49shy Selenium BRL mg1 0150 EPA 200 21-May-08 8051150
7440-66-6 Zinc 0186 mgl 0050
General Chemistry Parameters
Filtration Completed NA Varies 14-Mayshy 14-May-08 8051095
18540-29-9 Hexavalent Chromium (soluble) BRL HT2 mg1 125 SM3500CrDI796A 14-Mayshy 14-May-08 8051094 R01 2013 2016
57-12shy Cyanide (total) BRL mg1 0100 EPA 3354 19-Mayshy 19-May-088051374
7782-50shy Total Residual Chlorine BRL CIHT mg1 500 Hach 8167 14-Mayshy 14-May-08 8051049 R01 1900 2001
Total Suspended Solids 580 mg1 25 SM2540D 16-Mayshy 16-May-08 8051275
This lahomtOlY report is not valid without an authorized signature on the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page 8 of 25
Volatie Organic Compounds - Quality Control
Analyte( s)
Batch 8051244 - SW846 5030 Water MS
Blank 8051244-BLK1
Prepared 16-May-08 Analyzed 17-May-
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromochloromethane
1 Dichlorobenzene
1 Dichlorobenzene
1 Dichlorobenzene
1-Dichloroethane
1 Dichloroethane
1 1-Dichloroethene
cis- Dichloroethene
trans- 1 Dichloroethene
1 Dichloropropane
cis- 1 Dichloropropene
trans- 1 Dichloropropene
Ethylbenzene
Hexanone (MBK)
Methyl tert-butyl ether
Methyl- pentanone (MIBK)
Methylene chloride
Styrene
2- Tetrachloroethane
Tetrachloroethene
Toluene
1- Trichloroethane
2- Trichloroethane
Trichloroethene
Trichlorofluoromethane (Freon 11)
Vinyl chloride
p-Xylene
Xylene
Surrogate 4-Bromofluorobenzene Surrogate Toluene-
Surrogate 1 Dichloroethane-Surrogate Dibromofluoromethane
LCS B051244-BS1
Prepared 16-May-08 Analyzed 17 -May-
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Spike Source REC RPD
Result Flag Units RDL Level Result REC Limits RPD Limit
BRL gl 20
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl 10
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gll
BRL gi
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl 10
BRL gll
BRL gll 10
BRL gl 10
BRL gll
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
41 gl 50 70- 130 49 gl 50 70- 130 59 gl 50 119 70- 130 52 gl 50 105 70- 130
QC2 jgl 20 70- 130
18 jgl 20 70- 130
192 jgl 20 35- 155
18 jgl 20 45- 169
19 jgl 20 242
This laboratOlY repol1 is lot valid without 011 authorized sigllature 011 the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page 9 of 25
Volatie Organic Compounds - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051244 - SW846 5030 Water MS
LC5 8051244B51
Prepared 16-May-08 Analyzed 17-May-
Butanone (MEK) 10 QC2 gl 20 70- 130
Carbon tetrachloride 204 gl 20 102 70- 140
Chlorobenzene 18 gl 20 70- 130
Chloroethane 164 gl 20 14-230
Chloroform 18 gll 20 51- 138
Chloromethane 21 gl 20 106 273
Dibromochloromethane 18 gl 20 53- 149
1 Dichlorobenzene 20 gl 20 104 18- 190
1 Dichlorobenzene 19 gl 20 59- 156
1 A-Dichlorobenzene 18 gl 20 18- 190
1- Dichloroethane 19 gl 20 59- 155
1 Dichloroethane 19 gl 20 49- 155
1-Dichloroethene 16 gl 20 70- 130
cis- 1 Dichloroethene 17 gl 20 70- 130
trans- 1 Dichloroethene 16 gll 20 54- 156
1 Dichloropropane 18 gl 20 210
cis- Dichloropropene 17 gl 20 227
trans- 1 Dichloropropene 17 gl 20 17- 183
Ethylbenzene 19 gl 20 37- 162
Hexanone (MBK) 124 QC2 gl 20 70- 130
Methyl tert-butyl ether 19 gl 20 70- 130
Methylshy pentanone (MIBK) 17 gl 20 70- 130
Methylene chloride 16 gl 20 221
Styrene 17 gl 20 70- 130
1 Tetrachloroethane 194 gl 20 46- 157
Tetrachloroethene 15 gl 20 64- 148
Toluene 18 gl 20 70- 130
1- Trichloroethane 20 gl 20 100 52- 162
2- Trichloroethane 18 gl 20 52- 150
Trichloroethene 17 gl 20 71- 157
Trichlorofluoromethane (Freon 11) 19 gl 20 17- 181
Vinyl chloride 21 gl 20 106 251
p-Xylene 39 gl 40 70- 130
Xylene 20 gl 20 102 70- 130
Surrogate 4-Bromofluorobenzene Surrogate Toluene-
Surrogate 1 Dichloroethane-Surrogate Dibromofluoromethane
52 49 56
49
gl
gl
gl
gl
50 50 50
50
105
112 100
70- 130 70- 130 70- 130 70- 130
LC5 DUD (8051244-B5D1
Prepared 16-May-08 Analyzed 17-May-
Acetone QC2 gl 20 70- 130
Benzene 18 gl 20 70- 130
Bromodichloromethane 18 gl 200 35- 155
Bromoform 17 gl 20 45- 169
Bromomethane 18 gl 20 242
Butanone (MEK) 11 QC2 1-91 20 70- 130
Carbon tetrachloride 20 gl 20 100 70- 140
Chlorobenzene 17 gl 20 70- 130
Chloroethane 15 1-91 20 14-230
Chloroform 18 1-91 20 51- 138
This laboratory report is aot valid without a1 authorized sig1ature 01 the cover page
Reportble Detection Limit BRL = Below Reporting Limit Page 10 of25
Volatie Organic Compounds - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051244 - SW846 5030 Water MS
LCS Dup 18051244-BSD1
Prepared 16-May-08 Analyzed 17-May-
Chloromethane 18 1-91 20 273
Dibromochloromethane 174 1-91 20 53- 149
Dichlorobenzene 20 1-91 20 100 18- 190
Dichlorobenzene 18 1-91 20 59- 156
Dichlorobenzene 18 1-91 20 18- 190
Dichloroethane 18 1-91 20 59- 155
Dichloroethane 19 1-91 20 49- 155
Dichloroethene 16 1-91 20 70- 130
cis- Dichloroethene 16 1-91 20 70- 130
trans- Dichloroethene 15 1-91 20 54- 156
Dichloropropane 17 1-91 20 210
cis- Dichloropropene 164 IJgl 20 227
trans- 1 Dichloropropene 164 I-gl 20 17- 183
Etlwlbenzene 18 IJgl 20 37- 162
Hexanone (MBK) 124 QC2 IJgl 20 70- 130
Methyl tert-butyl ether 184 1J91 20 70- 130
Methyl- pentanone (MIBK) 17 IJgl 20 70- 130
Methylene chloride 16 IJgl 20 221
Styrene 16 IJgl 20 70- 130
2- Tetrachloroethane 19 IJgl 20 46- 157
Tetrachloroethene 15 IJgl 20 64- 148
Toluene 17 IJgl 20 70- 130
1- Trichloroethane 19 1-91 20 52- 162
2- Trichloroethane 16 IJgl 20 52- 150
Trichloroethene 15 IJgl 20 71- 157
Trichlorofluoromethane (Freon 11) 17 IJgl 20 17- 181
Vinyl chloride 19 IJglI 20 251
p-Xylene 37 1J91 40 70- 130
Xylene 20 IJgl 20 100 70- 130
Surrogate 4-Bromofluorobenzene 51 IJgl 50 104 70- 130
Surrogate Toluene- 4B gl 50 70- 130
Surrogate 1 0ichloroethane- 53 IJgl 50 106 70- 130 Surrogate Oibromofluoromethane 50 1J9i 50 102 70- 130
Matrix S ike B051244-MS1 Source SA7B629shy
Prepared 16-May-08 Analyzed 17-May-
Benzene 18 20 BRL 70- 130IJgl
Bromodichloromethane 19 IJgl 20 BRL 35- 155
Bromoform 18 IJgl 20 BRL 45- 169
Bromomethane 16 IJgl 20 BRL 242
Carbon tetrachloride 21 IJgl 20 BRL 106 70- 140
Chlorobenzene 18 IJgl 20 BRL 70- 130
Chloroethane 16 IJgl 20 BRL 14-230
Chloroform 18 IJgl 20 BRL 51- 138
Chloromethane 19 IJgl 20 BRL 273
Dibromochloromethane 17 IJgl 20 BRL 53- 149
1 Dichlorobenzene 22 IJgl 20 BRL 112 18- 190
1 Dichlorobenzene 22 IJgl 20 BRL 110 59-156
1 Dichlorobenzene 21 IJgl 20 BRL 109 18- 190
1- Dichloroethane 19 IJgl 20 BRL 59- 155
1 Dichloroethane 18 IJgl 20 BRL 49- 155
This laboratory report is 110t mUd without an authorized signature on the covel page
Reportble Detection Limit BRL = Below Reporting Limit Page It of25
Volatile Organic Compounds - Quality Control
p
Spike Source REC RPD
Result REC imits RPD LimitAnalyte(s) Result Flag Units RDL Level
Batch 8051244 - SW846 5030 Water MS
Matrix ike S051244-MS1 Source SA7B629shy
Prepared 16-May-08 Analyzed 17-Mayshy
17 20 BRL 70- 130 1- Dichloroethene IJgl
16 20 BRL 54- 156trans- 1 Dichloroethene IJgl
21020 BRL1 Dichloropropane 17 1J91
cis- 1 Dichloropropene 17 IJgl 20 BRL 227
17- 183trans- 1 Dichloropropene 184 1J91 20 BRL
20 20 BRL 103 37- 162Ethylbenzene IJgl
15 20 BRL 221Methylene chloride IJgl
20 BRL 46- 1572- Tetrachloroethane 19 1J91
20 BRL 64- 148Tetrachloroethene 18 1J91
BRL 70- 130Toluene 18 1J91 20
105 52-1621- Trichloroethane 211 IJgl 20 BRL
18 20 BRL 52- 1502- Trichloroethane IJgl
17 20 BRL 71- 157Trichloroethene 1J91
20 BRL 17- 181Trichloroluoromethane (Freon 11) 194 IJgl
20 BRL 103 251Vinyl chloride 20 IJgl
102 70- 130Surrogate 4-Bromofluorobenzene 50 IJgl 50 50 70- 130Surrogate Toluene- 49 1J91
56 50 112 70- 130Surrogate 1 Dichloroethane- IJgl
50 100 70- 130Surrogate Dibromofluoromethane 50 IJgl
Matrix S ike Du S051244-MSD1 Source SA7S629shy
Prepared 16-May-08 Analyzed 17-Mayshy
18 20 BRL 70- 130Benzene IJgl
18 20 BRL 35- 155Bromodichloromethane IJgl
17 20 BRL 45- 169Bromoform IJgl
20 BRL 242Bromomethane 17 IJgl
20 BRL 103 70- 140Carbon tetrachloride 20 IJgl
18 20 BRL 70- 130Chlorobenzene 1J91
14-230Chloroethane 16 IJgl 20 BRL
20 51- 138Chloroform 184 IJgl BRL
Chloromethane 19 1J91 20 BRL 273
18 20 BRL 53- 149Dibromochloromethane 1J91
20 BRL 117 18- 190Dichlorobenzene 234 IJgl
20 BRL 112 59- 156Dichlorobenzene 22 IJgl
BRL 108 18- 190Dichlorobenzene 21 1J91 20
20 59- 1551 Dichloroethane 19 IJgl BRL
18 20 BRL 49- 155Dichloroethane IJgl
16 20 BRL 70- 130Dichloroethene IJgl
20 BRL 54- 156trans- Dichloroethene 154 1J91
20 BRL 210Dichloropropane 17 IJgl
0420 BRL 227cis- Dichloropropene 17 IJgl
17- 183trans- Dichloropropene 17 1J91 20 BRL
BRL 37- 162Ethylbenzene 20 1J91 20 102
Methylene chloride 15 IJgl 20 BRL 221
20 BRL 46- 1572- Tetrachloroethane 192 IJgl
20 BRL 64- 148 04Tetrachloroethene 18 IJgl
BRL 70- 130Toluene 184 1J91 20
52- 1621- Trichloroethane 20 IJgl 20 BRL 104
17 20 BRL 52- 1502- Trichloroethane IJgl
17 20 BRL 71- 157Trichloroethene IJgl
20 BRL 17-181Trichlorofluoromethane (Freon 11) 19 IJgl
This laboratory report is IIOt valid without all authorized sigllllture 011 the cover page
Page 12 of25 Reportble Detection Limit BRL = Below Reporting Limit
Semivolatile Organic Compounds by GCMS - Quality Control
Analyte(s)
Batch 8051216 - SW846 3510C
Blank 8051216-BLK1
Prepared amp Analyzed 16-May-
Isophorone
Methylnaphthalene
Methylphenol
3 amp 4-Methylphenol
Naphthalene
Nitroaniline
Nitroaniline
Nitroaniline
Nitrobenzene
Nitrophenol
Nitrophenol
Nitrosodimethylamine
N- N itrosodi-n-pro pyla mine
N itrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Pyridine
1 24-Trichlorobenzene
24 5- Trichlorophenol
246- Trichlorophenol
Surrogate 2-Fuorobipheny Surrogate 2-Fuoropheno Surrogate Nitrobenzene-Surrogate PhenoshySurrogate Terpheny-d4 Surrogate 6- Tribromopheno
LCS B051216-BS1
Prepared amp Analyzed 16-May-
Acenaphthene
Acenaphthylene
Aniline
Anthracene
AzobenzenelDi phenyld lazine
Benzidine
Benzo (a) anthracene
Benzo (a) pyrene
Benzo (b) fluoranthene
Benzo (g i) perylene
Benzo (k) fluoranthene
Benzoic acid
Benzyl alcohol
B is(2-chloroethoxy)methane
B i s (2-ch loroethyl)eth e r
Bis(2-ch loroisopropyl) ether
B is(2-ethy Ih exyl) phtha late
Bromophenyl phenyl ether
Butyl benzyl phthalate
Carbazole
Spike Source REC RPD
Result Flag Units RDL Level Result REC Limits RPD Limit
BRL gl
BRL gl
BRL gl
BRL gl 10
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gll
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
370 gl 50 30- 130 40 gl 50 15- 110 39 gl 50 30- 130 43 gl 50 15- 110 36 gl 50 30- 130 40 gl 50 15- 110
41 gl 50 40- 140
43 gI 50 40- 140
41 gl 50 40- 140
38 gl 50 40- 140
45 gl 50 40- 140
49 gl 50 153
41 gl 50 40- 140
43 gl 50 40- 140
41 gl 50 40- 140
41 gll 50 40- 140
45 gl 50 40- 140
32 gl 50 12- 149
41 gl 50 40- 140
39 gl 50 40- 140
384 gl 50 40- 140
47 gl 50 40- 140
47 gl 50 40- 140
40 gl 50 40- 140
47 gI 50 40- 140
56 gI 50 112 200
This laboratory report is lIot valid witllOut a1l authorized sigllature 011 the coverpage
Reportble Detection Limit BRL = Below Reporting Limit Page 15 of25
Semivolatile Organic Compounds by GCMS - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051216 - SW846 3510C
LCS 8051216-BS1
Prepared amp Analyzed 16-Mayshy
50 30- 1304 -C hloro-3-methylphenol 42 IJgl
40- 140Chloroaniline 39 IJgl 50
Chloronaphthalene 37 IJgl 50 40- 140
Chlorophenol 37 IJgl 50 30- 130
50 40- 140
40- 140
Chlorophenyl phenyl ether 45 IJgl
Chrysene 43 IJgl 50
Dibenzo (a h) anthracene 43 IJgl 50 40- 140
Dibenzofuran IJgl38 50 40- 140
50 40- 1401 Dichlorobenzene 35 IJgl
40- 1401 Dichlorobenzene 264 IJgl 50
40- 1401 Dichlorobenzene 434 IJgl 50
58 50 116 40- 1403 - Dichlorobenzidine IJgl
50 30- 130
40- 140 24-Dichlorophenol 38 IJgl
Diethyl phthalate 484 IJgl 50
50 40- 140Dimethyl phthalate 464 IJgl
Dlmethylphenol 39 IJgl 50 30- 130
DI-n-butyl phthalate 44 IJgll 50 40- 140
30- 130 6-Di nitro- 2-methylphenol 38 1J91 50
30- 130Dinltrophenol 36 1J91 50
42 50 40- 14024-Dlnitrotoluene 1J91
Dlnitrotoluene 1J9141 50 40- 140
Di-n-octyl phthalate 52 IJgl 50 104 40- 140
40- 140Fluoranthene 40 IJgl 50
Fluorene 41 IJgl 50 40- 140
39 50 40- 140Hexachlorobenzene IJgl
50 40- 140Hexachlorobutadiene 40 IJgl
40- 140Hexach lorocyclopentad iene 294 IJgl 50
40 50 40- 140Hexachloroethane IJgl
42 50 40-140Indeno (1 3-cd) pyrene IJgl
50 40- 140Isophorone 40 IJgl
40- 140Methylnaphthalene 394 IJgl 50
40- 140Methylphenol 39 IJgl 50
40 10 50 40- 1403 amp 4-Methylphenol IJgl
37 50 40-140Naphthalene IJgl
50 40-140Nitroaniline 39 IJgl
Nitroaniline 51 IJgl 50 102 40- 140
48 50 40- 140Nltroaniline 1J91
50 40- 140Nitrobenzene 40 IJgl
30- 130Nitrophenol 36 IJgl 50
40 IJgl 50 30- 130Nitrophenol 40- 140Nitrosodimethylamine 32 1J91 50
50 40-140N- N itrosodi-n-propyla mine 46 IJgl
40- 140N itrosodi phenyla ml ne 44 IJgl 50
41 IJgl 50 30- 130Pentachlorophenol 40- 140Phenanthrene 38 IJgl 50
50 30- 130Phenol 38 IJgl
40- 140Pyrene 424 1J91 50
40- 140Pyridine 294 1J91 50
40- 14024- Trichlorobenzene 364 IJgl 50
This laboratory report is not mlid without an authorized signature 011 the cover page
Page 16 of25 Reportble Detection Limit BRL = Below Reporting Limit
Semivolatie Organic Compounds by GCMS - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
BMch 8051216 - SW846 3510C
LC5 8051216-851
Prepared amp Analyzed 16-Mayshy
24 5- Trichlorophenol 404 gl 50 30- 130
246- Trichlorophenol 42 gl 50 30- 130
Surrogate 2-Fluorobiphenyl 29 gl 50 30- 130
Surrogate 2-Fluorophenot 27 gl 50 15- 110
Surrogate Nitrobenzene- 30 gl 50 30- 130
Surrogate Phenol- 29 gl 50 15- 110
Surrogate Terpheny-d4 30 gl 50 30- 130
Surrogate 6- Tribromopheno 324 gl 50 15- 110
This laboratory report is lIot valid without all authorized sigllature 011 tlle cover page
Reportble Detection Limit BRL = Below Reporting Limit Page 17 of25
Semivolatie Organic Compounds by GC - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051106 - SW846 3510C
Blank S051106-BLK1
Prepared amp Analyzed 15-Mayshy
Aroclor- 1016 BRL gI 0200
Aroclor- 1016 (2C) BRL gI 0200
Aroclor- 1221 BRL gI 0200
Aroclor- 1221 (2C) BRL gI 0200
Aroclor- 1232 BRL gI 0200
Aroclor- 1232 (2Cj BRL gI 0200
Aroclor- 1242 BRL gI 0200
Aroclor-1242 (2C) BRL gI 0200
Aroclor- 1248 BRL gI 0200
Aroclor- 1248 (2C) BRL gI 0200
Aroclor- 1254 BRL gI 0200
Aroclor- 1254(2Cj BRL gI 0200
Aroclor- 1260 BRL gI 0200
Aroclor- 1260 (2C) BRL gI 0200
Aroclor- 1262 BRL gI 0200
Aroclor- 1262 (2C) BRL gI 0200
Aroclor-1268 BRL gI 0200
Aroclor- 1268 (2C) BRL gI 0200
Surrogate Decachlorobiphenyl (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0231 0224 0194 0191
gI
gI
gI
gI
0200 0200 0200 0200
116 112
30- 150 30- 150 30- 150 30- 150
LC5 8051106-B51
Prepared 15-May-08 Analyzed 16-May-08
Aroclor- 1016 265 gI 0200 250 106 50- 114
Aroclor- 1 016 (2C) 240 gI 0200 250 50- 114
Aroclor- 1260 0269 gI 0200 250 107 40- 127
Aroclor-1260 (2Cj 270 gI 0200 250 108 40- 127
Surrogate Decachlorobiphenyl (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0225 0224 0188 0183
gI
gI
gI
gI
0200 0200 0200 0200
113 112
30- 150 30- 150 30- 150 30- 150
LC5 DUD rS051106-B5D1
Prepared 15-May-08 Analyzed 16-Mayshy
Aroclor- 1016 262 gl 0200 250 105 50- 114
Aroclor-1 016 (2Cj 241 gI 0200 250 50- 114
Aroclor- 1260 277 gI 0200 250 111 40- 127
Aroclor- 1260(2Cj 0260 gI 0200 250 104 40- 127
Surrogate Decachlorobipheny (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0238 0218 0189 0181
gI
gI
gI
gI
0200 0200 0200 0200
119 109
30- 150 30- 150 30- 150 30- 150
This laboratory report is lot valid without (II authorized sigllature 01 the cover page
Page 18 of25 Reportable Detection Limit BRL = Below Reporting Limit
Extractable Petroleum Hydrocarbons - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051102 - SW846 3510C
Blank 8051102-BLK1
Prepared 15-May-08 Analyzed 19-Mayshy
Non-polar material (SGT- HEM) BRL m91
LC8 8051102-B81
Prepared 15-May-08 Analyzed 19-Mayshy
Non-polar material (SGT- HEM) 184 m91 21 81 904
This laboratory report is not valid without an authorized signature 011 the cover page
Page 19 of25 Reportable Detection Limit BRL = Below Reporting Limit
Soluble Metals by EPA 200 Series Methods - Quality Control
Analyte(s) Result Flag Units RDL
Spike
Level
Source
Result REC
REC
Limits RPD
RPD
Limit
Batch 8051150 - EPA 200 Series
Blank 8051150-BLK1
Prepared amp Analyzed 21-May-
Iron
Zinc
Selenium
Nickel
Chromium
Copper
Arsenic
BRL
BRL
BRL
BRL
BRL
BRL
BRL
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0150
0050
0150
0050
0050
0050
0040
LCS 8051150-BS1
Prepared amp Analyzed 21-May-
Selenium
Zinc
Iron
Nickel
Chromium
Arsenic
Copper
123
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0150
0050
0150
0050
0050
0040
0050
103
105
101
100
85- 115
85- 115
85- 115
85- 115
85- 115
85-115
85- 115
licate B051150-DUP1 Source SA7B602shy
Prepared amp Analyzed 21-May-
Iron
Zinc
Selenium
Nickel
Copper
Chromium
Arsenic
17
0162
BRL
0015
0017
BRL
0450
QR8
mgl
mgl
mgl
mgl
mgl
mgl
mgi
0150
0050
0150
0050
0050
0050
0040
184
0186
BRL
0014
0023
BRL
0468
Matrix S ike 8051150-MS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Iron
Selenium
Nickel
Zinc
Copper
Chromium
Arsenic
19 QM2 mgl
mgll
mgl
mgl
mgl
mgl
mgl
0150
0150
0050
0050
0050
0050
0040
125
184
BRL
0014
0186
0023
BRL
0468
104
105
102
70- 130
70- 130
70-130
70- 130
70- 130
70-130
70- 130
Post S ike 8051150-PS1 Source SA78602shy
Prepared amp Analyzed 21-May-
Zinc
Iron
Selenium
Nickel
Copper
Arsenic
Chromium
18 QM2
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0050
0150
0150
0050
0050
0040
0050
0186
184
BRL
0014
0023
0468
BRL
104
104
101
85- 115
85- 115
85- 115
85-115
85-115
85- 115
85-115
Batch 8051152 - EPA200SW7000 Series
Blank B051152-BLK1
Prepared amp Analyzed 21-May-
Mercury BRL mgl 00020
This laboratory report is IIOt valid witllOut all authorized sigllature 011 the coverpage
Page 20 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Soluble Metals by EPA 200 Series Methods - Quality Control
Analyte(s) Result Flag Units RDL
Spike
Level
Source
Result REC
REC
Limits RPD
RPD
Limit
Batch 8051152 - EPA200SW7000 Series
LCS B051152-BS1
Prepared amp Analyzed 21-May-
Mercury 00576 m91 00020 00500 115 85- 115
licate B051152-DUP1 Source SA78602-01
Prepared amp Analyzed 21-May-
Mercury BRL m91 00020 BRL
Matrix S ike 8051152-MS1 Source SA78602shy
Prepared amp Analyzed 21-May-
Mercury 00632 OM m91 00020 00500 BRL 126 75- 125
Post S ike 8051152-PS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Mercury 00624 OC1 m91 00020 00500 BRL 125 85- 115
Batch 8051249 - 2008No digestion
Blank 8051249-BLK1
Prepared amp Analyzed 21-May-
Lead
Antimony
Cadmium
Silver
BRL
BRL
BRL
BRL
m91
m91
m91
m91
0002
0002
0002
0002
LCS B051249-BS1
Prepared amp Analyzed 21-May-
Antimony
Lead
Silver
Cadmium
143
145 OC2
m91
m91
m91
m91
0050
0050
0050
0040
103
115
107
116
85- 115
85- 115
85- 115
85- 115
licate 8051249-DUP1 Source SA7B602shy
Prepared amp Analyzed 21- May-
Lead
Antimony
Cadmium
Silver
0009
0002
00005
00002
ORB
m91
m91
m91
m91
0002
0002
0002
0002
0011
0003
00005
00003
Matrix S ike 8051249-MS1 Source SA78602shy
Prepared amp Analyzed 21- May-
Lead
Antimony
Cadmium
Silver
142
m91
m91
m91
m91
0050
0050
0040
0050
0011
0003
00005
00003
111
101
114
102
70- 130
70-130
70c130
70- 130
Post S ike 8051249-PS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Antimony
Cadmium
Silver
38
OC2
m91
m91
m91
0050
0040
0050
125
0003
00005
00003
110
121
109
85- 115
85- 115
85- 115
This laboratory report is flOt valid IVithout all authorized signature 011 the cOIer page
Reportable Detection Limit BRL Below Reporting Limit Page 21 of 25
General Chemistry Parameters - Quality Control
Spike Source REC RPD
Analyte( s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051049 - General Preparation
Blank S051 049-BLK1
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
Blank S051049-BLK2
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
Blank S051 049-BLK3
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
LCS S051049-BS1
Prepared amp Analyzed 14-May-
Total Residual Chlorine 046 mgl 020 0500 90- 110
LCS S051049-BS2
Prepared amp Analyzed 14-May-
Total Residual Chlorine 047 mgl 020 0500 90- 110
LCS S051049-BS3
Prepared amp Analyzed 14-May-
Total Residual Chlorine 054 mgl 020 0500 108 90-110
licate B051049-DUP1 Source SA7S544shy
Prepared amp Analyzed 14-May-
Total Residual Chlorine 012 mgl 020 010
licate S051049-DUP2 Source SA7S602-01
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020 BRL
Matrix S ike 8051049-MS1 Source SA78544-01
Prepared amp Analyzed 14-May-
Total Residual Chlorine 065 mgl 020 0500 010 110 80- 120
Matrix S ike 8051049-MS2 Source SA7B602shy
Prepared amp Analyzed 14-May-
Total Residual Chlorine mgl 500 125 BRL 108 80- 120
Reference 8051 049-SRM1
Prepared amp Analyzed 14-May-
Total Residual Chlorine 100 mgl 020 0967 103 85-115
Batch 8051094 - General Preparation
Blank 8051094-BLK1
Prepared amp Analyzed 14 May-
Hexavalent Chromium (soluble) BRL mgl 005
Blank 8051 094-BLK2
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) BRL mgl 005
LCS 8051094-BS1
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) 054 mgl 005 90- 110
licate 8051094-DUP1 Source SA78602-01
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) BRL mgl 125 BRL
Thi laboratory report is not valid without all authorized sigllature 011 the cover page
Page 22 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Page 5
PAR
AM
ET
ER
B
elieve B
elieve of
Type of
Absent
Present Sam
ples S
ample (eg
(1 min-
grab)
imum
)
10 Ethylene
Dibrom
ide G
RA
B
(1 2- Dibrom
o-methane)
11 Methyl-tert-B
utyl G
RA
Ether (M
tBE
)
12 tert-
Butyl
Alcohol
GR
AB
(TB
A)
13 tert-A
myl
Methyl
GR
A
Ether (T
AM
E)
14 Naphthalene
GR
AB
15 Carbon T
etra-G
RA
chloride
16 1
Dichlorobenzene
GR
A
17 D
iehlorobenzene G
RA
GR
A18 1
Dichlorobenzene
19 1
Dich1oroethane
GR
A
20 1
Dichloroethane
GR
A
21 1
Dichloroethylene
GR
A
22 cis-D
ichloro-G
RA
B
ethylene
GR
A
(Methylene C
hloride)
23 D
ichloromethane
24 T
etrachloroethylene G
RA
B
Rem
ediation General Perm
it - Notice of Intent
Analytical
Minim
um
Maxim
um daily value
Avg daily value
Method
Level (M
L) of
Used
Test M
ethod concentration
mass
concentration m
ass
(method )
(ugI) ( ug)
(kgday) (ugI)
(kgday)
504 010
0 0
5030 05
020
5030 0200
5030 020
625 247
5030 020
5030 020
5030 05
020
5030 020
5030 020
5030 020
5030 05
020
5030 020
5030 10
0200
5030 020
PAR
AM
ET
ER
B
elieve B
elieve of
Type of
Absent
Present Sam
ples Sam
ple (e
(l min-
grab)
imum
)
25 1
1 Trichloroethane
GR
AB
26 1
2 Trichloroethane
GR
A
27 Trichloroethylene
GR
AB
28 Vinyl C
hloride G
RA
B
29 Acetone
GR
A
30 14 D
ioxane G
RA
B
31 Total Phenols
GR
AB
32 Pentachlorophenol
GR
AB
33 Total Phthalates 6
GR
AB
(phthalate esthers)
34 Bis (2-E
thylhexyl) G
RA
B
Phthalate (D
ishy(ethylhexyl) P
hthalate)
35 Total G
roup 1 G
RA
P
olycyclic Arom
atic H
ydrocarbons (PA
H)
a Benzo(a) A
nthracene G
RA
B
b Benzo(a) P
yrene G
RA
c Benzo(b )F
luoranthene G
RA
B
d Benzo(k) F
luoranthene G
RA
e Chrysene
GR
AB
The slim
of iijdividual phthalate compounds
Rem
ediation General Perm
it - Notice of Intent
Analytical
Minim
um L
evel M
aximum
daily value A
vg daiJy Value
Method Used
(ML) ofT est
(method )
Method
concentration m
ass concentration
mass
(ugI) (ugI)
(kgday) (ugl)
(kgday)
5030 20
5030 20
5030 20
5030 ~20
5030 400
5030 200
625 50
625 50
625 All phthalates are
BD
L see lab report
625 50
625 A
ll Group I P A
Hs
are BD
L
625 50
625 50
625 50
625 50
625 50
g
PAR
AM
ET
ER
B
elieve B
elieve of
Type of
Analytical
Minim
um
Maxim
um daily value
Average daily value
Absent
Present Sam
ples Sam
ple (e M
ethod Used
Level (M
L) of
(lmin -
grab) (m
ethod ) T
est Method
concentration m
ass concentration
mass
imum
) (ug1)
(ugl) (kgday)
(ugl) (kgday)
f Dibenzo(a
GR
AB
625
-(50
anthracene
Indeno(I 23-cd) G
RA
B
625 -(50
Pyrene
36 Total G
roup II G
RA
B
625 247
Polycyclic A
romatiC
H
ydrocarbons (pAR
)
h Acenaphthene
GR
AB
625
-(10
i Acenaphthylene
GR
A
625 -(50
j Anthracene
GR
A
625 -(50
k Benzo(ghi)
Perylene G
RA
B
625 -(50
I Fluoranthene G
RA
B
625 -(50
m F
luorene G
RA
B
625 -(50
n Naphthalene-
GR
AB
625
247
o Phenanthrene
GR
AB
625
-(50
p Pyrene
GR
AB
625
-(50
37 Total
POlychlorinated
GR
AB
608
065 -(0065
Biphenyls (PC
Bs)
38 Antim
ony G
RA
B
200 03
4Eshy
39 Arsenic
GR
AB
200
468
40 Cadm
ium
GR
AB
200
-( 0
41 Chrom
ium II
(1) G
RA
B
calculated calculated
-(5
42 Chrom
ium V
I G
RA
7196A
-( 125
NO
TE
S (1) Chrom
ium m
= T
otal Chrom
ium - H
exavalent Chrom
ium A
ccording to lab personnel the trivalent chromium
is calculated to be greater or equal to 5 ugI but less than 125 ugl Total
Chrom
ium w
as -(5 ugI and the Hexavalent C
hromium
was less than 125 ugl
Rem
ediation General Perm
it - Notice of Intent
--------
--------
-------
--------
---
PAR
AM
ET
ER
B
elieve B
elieve of
Type of
Analytical
Minim
um
Maxim
um daily value
Avg daily value
Absent
Present Sam
ples Sam
ple (e M
ethod L
evel (ML
) of grab)
Used
Test M
ethod concentration
mass
concentration m
ass(1 m
inshy
imum
) (m
ethod ) (ug1)
(ug1) (kgday)
(ug1) (kgday)
43 Copper
GR
A
200 (5
44 Lead G
RA
200
0001
45 Mercury
GR
A
7470A
(020
46 Nickel
GR
AB
200
(5
GR
AB
200
( 1547 Selenium
48 Silver G
RA
B
200 (0
49 Zinc
GR
A
200 18
0025
50 Iron G
RA
B
200 400
25
Other (describe)
c For discharges where m
etals are believed present please fill out the following
If yes which m
etals A
rsenic and Iron Step
I Do any of the m
etals in the influent have a reasonable potential to exceed the
etIluent limits in A
ppendix II (i the limits set at zero to five dilutions) Y
rg N D
Step 2 For any m
etals which have reasonable potential to exceed the A
ppendix III limits
Look up the lim
it calculated at the corresponding dilution factor in
calculate the dilution factor (DF) using the form
ula in Part I A 3 c) (step 2) of the N
O
Appendix IV
Do any of the m
etals in the influent have the potential to instructions or as determ
ined by the State prior to the submission of this N
OI
exceed the corresponding effuent lim
its in Appendix IV
(i is the
What is the dilution factor for applicable m
etals in1uent concentration above the lim
it set at the calculated dilution M
etals A
rsenic and Iron factor)
yrgND
If Y
es list which m
etals A
rsenic and Iron
DF
Rem
ediation General Pem
lit - Notice of Intent
4 Treatm
ent system inform
ation Please describe the treatment system
using separate sheets as necessary including
a) A description of the treatm
ent system including a schem
atic of the proposed or existing treatment system
S
ee Figures 4 and 5
Frac tank Air stripper
Oilw
ater separator Equalization tanks
Bag filter rg
GA
C filter rg
b) Identity each applicable
treatment unit (check alJ
that apply)
Chlorination
Dechlorination
Other (please describe)
c) Proposed average and maxim
um flow
rates (gallons per minute) for the discharge and the design flow
rate(s) (gallons per minute) ofthe treatm
ent system
Average flow
rate of discharge 15 G
PM
Maxim
um flow
rate oftreatment system
0 G
PM
Design flow
rate of treatment system
0 G
PM
d) A description of chem
ical additives being used or planned to be used (attach MSD
S sheets) Not A
pplicable
5 Receiving surface water(s) Please provide information about the receiving water (s) using separate sheets as necessary including
Identity the discharge pathway
I Direct
I Within facility
I Stonn drain rg I R
iverbrook I W
etlands _ I Other (describe)
Provide a narrative description ofthe discharge pathway including the nam
e(s) of the receiving waters
Discharge to catchbasin and stonnw
ater drainage system in E
ast Broadw
ay which discharges to M
ahoney Brook (S
ee Figure 4)
c) Attach a detailed m
ap(s) indicating the site location and location of the outfall to the receiving water
1 For multiple discharges num
ber the discharges sequentialJy 2 For indirect dischargers indicate the location of the discharge to the indirect conveyance and the discharge to surface w
ater T
he map should also include the location and distance to the nearest sanitary sew
er as well as the locus of nearby sensitive receptors (based on U
SGS topographical
mapping) such as surface w
aters drinking water supplies and w
etland areas d) Provide the state w
ater quality classification of the receiving water
e) Provide the reported or calculated seven day- ten year low flow
(7QlO
) of the receiving water Jcfs
Please attach any calculation sheets used to support stream flow
and dilution calculations See A
ttachment B
f) Is the receiving water a listed 303(d) w
ater quality impaired or lim
ited water Y
es 0 No rg
If yes for which polJutant(s) N
A
Is there a TM
DL
Yes 0
No rg If yes for w
hich pollutant(s) NA
Rem
ediation General Perm
it - Notice of Intent
6 Results of C
onsultation with Federal Services Please p
rovide the following information according to requirements of Par
lBA
and A
ppendices II and VII
a) Are any listed threatened or endangered species or designated critical habitat in proxim
ity to the discharge Yes 0
No rg
Has any consultation w
ith the federal services been completed Y
es 0 No rg
or is consultation underway Y
es 0 No rg
What w
ere the results of the consultation with the U
S Fish and Wildlife Service andor N
ational Marine Fisheries Service (check one) N
ot applicable
a nojeopardy opinion
or written concurrenceD
on a finding that the discharges are not likely to adversely affect any endangered species or critical habitat
b) Are any historic properties listed or eligible for listing on the N
ational Register of H
istoric Places located on the facilty or site or in proximity to the discharge
Yes D
No
Have any state or tribal historic preservation offcer been consulted in this determ
ination (Massachusetts only) Y
es O N
o
7 SU
DD
lemental inform
ation
Please provide any supplemental information Attach any analytical data used to support the application A
ttach any celtification(s) required by the general permit
Attachm
ent A - Figures
Figure I - Site Locus M
ap
Figure 2 - MassD
EP Site Scoring M
ap
Figure 3 - Aerial M
ap
Figure 4 - Proposed Soil Excavation A
rea Map
Figure 5 - T
reatment S
ystem Line D
iagram
Attachm
ent B - D
ilution factor Calculations
Attachment C - L
aboratory Analytical R
eport Groundw
ater
Rem
ediation General Perm
it - Notice of 1ntenl
=-
including the following
8 Signature Requirements
The N
otice ofIntent must be signed by the operator in accordance w
ith the signatory requirements of 40 C
FR Section 122
certification
J certif under penalty of law that this docum
ent and all attachments w
ere prepared under my direction or supervision in accordance w
ith a system
designed to assure that qualifed personnel properly gather and evaluate the information subm
itted Based on m
y inquiry of the person or persons who
manage the system
or those persons directly responsible for gathering the information I certif that t
he information submitted
is to the best of m
y
knowledge and belief true accurate and com
plete J certif that I am aw
are that there are signifcant penalties for submitting false inform
ation including
the possibilty of fine and imprisonm
ent for knowing violations
FacilitySite Name
Form
er Speedw
ay Service S
tation 181 East B
roadwav G
ardner MA
01440
Operator signature
Title
Michael 1 D
ziura Sf Env E
ngineer
Date
4150- q
Rem
ediation General Perm
it - Notice of Intent
-
D- 0
0 0
il (J tu
Bw
o(0 -I
NJW
gQb
J(JZc o c
rou a -10
0 J 6shy
a 0
I-tDC
aJ Qj
E aJshy
ro ro ro
~~~ ~~~~- -- - _ - -_ - ~~~ ~~~~ ~~~ - - _- _- -- -- p __(
MA DEP - Bureau of Waste Site CleanupSITE NME Site S aP 5 MiFlII Former Speeway Station _-II181 Eat Broaday b b d IS I i I GARDNER MA 0144 v ri) i P f f 1 me- 1 5ylmI I L shy J --I 423315n 715835e SiteLocation y o oCop1odQcn Ofof W-_ l
1 1 I
r
r
iBARBER HILL
A c
Cf1 f o s
0
5
Roads Uned Acss Divd Mar Roed Conntor Street Track 1 EPA Sola Source Aquilar FEMA 100yaar iloodplain 0 c Puc Watar SLo GrunSelaceNon Corrty 0
Bounars lOwn Couny DE Region Tian Powerln Ine Aqedut ApprOld Zona2 tNPA Sue Wster Supp Zone A bStZ F--shy--rle
8os Mat Sub SUeor Porenrial Inermtent Man lvo8 Ste Dfm Hyro1apy Wmer FeatllePLio Suleee Wat S H-- L otlMds FrslSaltN-ES WeIMd Habat L
Potentia Prdutiv AqlJlers ModHig Yield Proteoted Opn Space ACC nIL c= Non-Potential Drng Water Sollce AIea ModumHi Yo1d ll DEP Pormrd SoidWes1 FsiIi6s cnifud Verne Pools f0
1I2 KIWUmR$ MtL
January 30 2004 SCALE 1 15000
-
LE
GE
ND
APX PROPER BONDA
- APPROXOiSPO SIT BOUNDA
-GR
OU
ND
WA
TE F1 D
IRE
cnON
SCA
LE
30 60 FE
(APR
OX
CORPORATE ENVIRONMENTAL
)i
AD
VISO
RS
INC
SC
AS SH
OW
D
R B
Y K
HA
EL
DA
TE
10407
JOB
NO
2920-96
AERIAL MAP
FO
RM
ER
SP
EE
DW
AY
ST
AT
ION
FlGURE -3
181 EA
BR
OA
AY
GA
NE
R fo
age 1 ot 1Streamflow Statistics Report
Streamstats Ungaged Site Report Date Wed Dec 31 2008 124908 Site Location Massachusetts NAD83 Latitude 425545 (42 3316) NAD83 Longitude -719758 (-71 58 32) NAD27 Latitude 425545 (423316) NAD27 Longitude - 9763 (-71 58 34) Drainage Area 502 mi2
IPeak Flow Basin Characteristics 1100 Statewide Low Flow (S02 mi2)
Regression Equation Valid Rang
I Min II Max1 Value III Parameter Drainage Area (square miles) 161 149
Mean Basin Slope from 250K DEM (percent) 032 24
Stratified Drift per Stream Length (square mile per mile) 129
Massachusetts Region (dimensionless)
Streamflow Statistics
gO-Percent Prediction Interval Prediction Error
MaximumStatistic Flow (ft s) (percent) Minimum
I D50 IIII 11 1811 II 24511 993
I D60 II 35511 2011 II 03611 35111 2411 II 041 I 201I D70 24111 2611 II 03811 151I D75 11 2811 II 0911 3761I D80 981I D85 1 I 3211 II o6311
1 I 3711 II 0441 1 2 2911 D90 11 4611 II 02411 15511 D95I D98 04511 6011 II 01511 11
I D99 03411 6511 II ol1ll 1021
5011 II 02611 11I M7D2Y 1111 3311 II odl 3 541
I AUGD50
IIIIIIIIIIIIIIIIIIIIII 0311 7111 II 0088411 0981I M7Dl0Y
1010
12312008httpstreamstatsagscrusgsgovgisimgReportsFlowStatsReport3494 - 2008123112498
Dilution Factor Calculation Former Speedway Service Station 181 East Broadway Gardner Ma
DF=(Od+Os)Od
DF = Dilution factor
Od = Max flow rate of discharge in cubic feet per second Os = receiving water flow in cubic feet per seconds 7010 flow rate Mahoney Brook 7010 = min flow for seven consecutive days with a recurrence interval of 10 years
7010 flow based on data obtained from USGS Steamflow Statistics Report Data attached
067
Semivolatile Organic Compounds by GCMS - Quality Control
Analyte( s)
Batch 8051216 - SW846 3510C
Blank 8051216BLK1)
Prepared amp Analyzed 16May-
Acenaphthene
Acenaphthylene
Aniline
Anthracene
AzobenzenelDi phenyld iazi ne
Benzidine
Benzo (a) anthracene
Benzo (a) pyrene
Benzo (b) fiuoranthene
Benzo (g i) perylene
Benzo (k) fiuoranthene
Benzoic acid
Benzyl alcohol
Bis(2-ch loroethoxy) methane
Bis(2-ch loroethyl)ether
Bis(2-ch loroi sopropyl)ether
Bis(2ethylhexyl) phthalate
Bromophenyl phenyl ether
Butyl benzyl phthalate
Carbazole
Ch loro-3-methyl phenol
Chloroaniline
Chloronaphthalene
Chlorophenol
Chlorophenyl phenyl ether
Chrysene
Dibenzo (a h) anthracene
Dibenzofuran
Dichlorobenzene
Dichlorobenzene
14- Dichlorobenzene
3 - Dichlorobenzidine
24-Dichlorophenol
Diethyl phthalate
Dimethyl phthalate
24- Dimethylphenol
Din-butyl phthalate
Dinitro-2-methylphenol
Dinitrophenol
Dinitrotoluene
Dinitrotoluene
Di-noctyl phthalate
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopehtadiene
Hexachloroethane
Indeno (1 cd) pyrene
Spike Source REC RPD
Result Flag Units RDL Level Result REC Limits RPD Limit
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gl
BRL gI
BRL gl
BRL gl
BRL gl
BRL gI
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gll
BRL gl
BRL gll
BRL gl
BRL gl
BRL gI
BRL gI
BRL gI
BRL gl
BRL gI
BRL gI
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gI
BRL gI
BRL gl
This laboratory report is IlOt valid without all authorized sigllature 011 the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page t4 of25
Volatie Organic Compounds - Quality Control
p (
Spike Source REC RPD
RDL Level Result REC Limits RPD Limit Analyte(s) Result Flag Units
Batch 8051244 - SW846 5030 Water MS
Matrix S ike Du 8051244-MSD1 Source SA78629shy
Prepared 16-May-08 Analyzed 17-May-BRL 106 251
Vinyl chloride 21 gl 20
101 70- 130 Surrogate 4-Bromofluorobenzene 50 gl 50
70- 13049 gl 50 111 70- 130
Surrogate Toluene-Surrogate 1 Dichloroethane- 55 gl 50
50 70- 130494 glSurrogate Dibromofluoromethane
Microextractable Organic Compounds - Quality Control
Spike Source REC RPD
Flag Units RDL Level Result REC Limits RPD Limit Analyte(s) Result
Batch 8051105 - SW846 3510C
Blank 8051105-BLK
Prepared amp Analyzed 15-May-
BRL gl 01001 Dibromoethane (ED B)
LCS 8051105-BS1
Prepared amp Analyzed 15-Mayshy50- 1500770 gl 0100 100
licate 8051105-DUP1 Source SA7B583shy
Prepared amp Analyzed 15-May-
BRL gl 0100 BRL
1 Dibromoethane (EDB)
1 Dibromoethane (EDB)
This laborntOlY report is not valid without an authorized signature 011 the cover page
Page 13 of2S Reportable Detection Limit BRL = Below Reporting Limit
Sam le Identification Client Pro ect Matrix Collection DateTime ReceivedMWshy
2920-96- Ground Water 13-May-081030 14-May-SA 78602shy
CAS No Analyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Volatile Organic Compounds
Volatile Or anic Com ounds b GCMS
Prepared by method SW846 5030 Water MS
123-91- Dioxane BRL 1-91 200 EPA 624 16-May-08 17-May-08 8051244
994-05-8 Ter-amyl methyl ether BRL 1-911 20
755- Tert-Butanoll butyl alcohol BRL 1-91 200
67-B4- Acetone BRL 1-91 400
71-43- Benzene BRL 1-91 20
75-27-4 Bromodichloromethane BRL 1-91 20
75-25- Bromoform BRL 1-91 20
74-83- Bromomethane BRL 1-91 40
78-93- Butanone (MEK) BRL 1-91 200
56-23- Carbon tetrachloride BRL 1-91 20
108-90- Chlorobenzene BRL 1-91 20
75-00- Chloroethane BRL 1-91 40
676- Chloroform BRL 1-91 20
74-87- Chloromethane BRL 1-91 40
124-48- Dibromochloromethane BRL 1-91 20
95-50- Dichlorobenzene BRL 1-911 20
541-73- Dichlorobenzene BRL 1-91 20
106-46- Dichlorobenzene BRL 1-91 20
75-34- 1- Dichloroethane BRL 1-91 20
107-06- Dichloroethane BRL 1-91 20
75-35-4 1- Dichloroethene BRL 1-91 20
156-59 cis- Dichloroethene BRL 1-91 20
156-60- trans- Dichloroethene BRL 1-91 20
78-87- 2- Dichloropropane BRL 1-91 20
10061-01-5 cis- Dichloropropene BRL 1-91 20
10061-02-B trans- Dichloropropene BRL 1-91 20
100-41-4 Ethylbenzene 411 1-911 20
591-78-B BRL 200Hexanone (MBK) 1-91
1634-04 -4 Methyl tert-butyl ether BRL 1-91 20
108-10- Methyl- pentanone (MIBK) BRL 1-91 200
75-09- Methylene chloride BRL 1-91 200
100-42- Styrene BRL 1-91 20
79-34- 1 Tetrachloroethane BRL 1-91 20
127- 18-4 T etrachloroethene BRL 1-91 20
108-88- Toluene BRL 1-91 20
71-55 1- Trichloroethane BRL 1-91 20
79-00- 2- Trichloroethane BRL 1-91 20
79-01-B Trichloroethene BRL 1-91 20
759-4 Trichlorofluoromethane (Freon 11) BRL 1-91 20
75-01-4 Vinyl chloride BRL 1-91 20
179601-23-1 m Xylene 390 1-91 40
95-47 Xylene 82 1-91 20
Surrogate recoveries 460-00- Bromofluorobenzene 70- 130
2037-26- Toluene- 100 70- 130
17060-07-0 1 Dichloroethane- 111 70- 130
1868-53- Dibromofluoromethane 70- 130
Microextractable Organic Compounds
106-93-4 1 Dibromoethane (EDB) BRL 1-91 0100 EPA 504 15-May- 15-May-08 8051105
Semivolatile Organic Compounds by GCMS
This laboratory report is not valid without all autllOrized signature 011 the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page 5 of 25
Sam le Identification Client Pro ect Matrix Collection DateTime Received
MWshy2920-96- Ground Water 13-May-081030 14-May-
SA 78602shy
CAS No Analyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Semivolatie Organic Compounds by GCMS
Semi volatile Or anic Com ounds b EPA 625
Prepared by method SW846 3510C 50 EPA 625 16-May- 19-May-08 805121683-32- Acenaphthene BRL IJgl
208-96-8 Acenaphthylene BRL IJgl 50
62-53- BRL IJgll 50Aniline
120- 12- Anthracene BRL 1J91 50
103-33- AzobenzenefDiphenyldiazine BRL IJgl 50
92-87 - Benzidine BRL IJgl 50
56-55- Benzo (a) anthracene BRL 1J91 50
50-32 - Benzo (a) pyrene IJglBRL 50
205-99- Benzo (b) fluoranthene BRL IJgl 50
191-24- Benzo (g i) perylene BRL IJgl 50
50207-08- Benzo (k) fluoranthene BRL IJgl
65-85 Benzoic acid BRL 1J91 50
100-51-6 Benzyl alcohol 1J91BRL 50
50111-91- Bis(2-chloroethoxy)methane BRL 1J91
111-4-4 Bis(2-chloroethyl)ether BRL IJgl 50
501 08-60- Bis(2-chloroisopropyl)ether BRL IJgl
117-81- Bis(2-ethylhexyl)phthalate BRL 1J91 50
101-55- Bromophenyl phenyl ether BRL IJgl 50
5085-68- Butyl benzyl phthalate BRL IJgl
5086-74- Carbazole BRL IJgl
5059-50- C hloro-3-methylphenol BRL IJgl
106-47- Chloroaniline BRL IJgl 50
91-58- Chloronaphthalene IJglBRL 50
5095-57 - Chlorophenol BRL 1J91
507005-72- Chlorophenyl phenyl ether BRL IJgl
216-01- Chrysene tJ91BRL 50
5053-70- Dibenzo (a h) anthracene BRL IJgl
50132-64- Dibenzofuran BRL IJgl
95-50- Dichlorobenzene IJglBRL 50
541-73- 13- Dichlorobenzene BRL IJgl 50
106-46- Dichlorobenzene 1J91BRL 50
5091-94- 3 - Dichlorobenzidine BRL IJgl
120-83- Dichlorophenol BRL IJgl 50
84-66- Diethyl phthalate BRL IJgl 50
131-11- Dimethyl phthalate BRL IJgll 50
105-67- Dimethylphenol BRL 1J91 50
5084-74- Di-n- butyl phthalate BRL 1J91
534-52 - Dinitro-2-methylphenol BRL IJgl 50
51-28- Dinitrophenol IJglBRL 50
50121-14- Dinitrotoluene BRL 1J91
606-20- Dinitrotoluene IJglBRL 50
50117-84-0 Di-n-octyl phthalate BRL IJgl
206-44-0 Fluoranthene 1J91BRL 50
BRL 50
50 86-73- Fluorene IJgi
118-74- Hexachlorobenzene BRL 1J91
87-68- Hexachlorobutadiene 1J91BRL 50
5077-47-4 Hexachlorocyclopentadiene BRL IJgl
67-72- Hexachloroethane IJglBRL 50
50193-39- Indeno (1 3-cd) pyrene BRL IJgl
5078-59- Isophorone BRL IJgl
Tfls laboratory report is not valid without all authorized signature 011 the coverpage
Page 6 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Sam le Identification Client Pro ect Matrix Collection DateTime ReceivedMWshy
2920-96- Ground Water I3-May-081030 14-May-SA 78602shy
CAS No Analyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Semivolatile Organic Compounds by GCMS
Semi volatile Or anic Com ounds b EPA 625
Prepared by method SW846 3510C
91-57 -6 Methylnaphthalene 367 1-91 50 EPA 625 16-May- 19-May-08 8051216
95-48- Methylphenol BRL 1-91 50
108-39-4 3 amp 4-Methylphenol BRL I-gl 100 106-44shy91-20- Naphthalene 247 1-91 50
88-74-4 Nitroaniline BRL 1-91 50
99-09- Nitroaniline BRL 1-91 50
100-01-6 Nitroaniline BRL 1-91 50
98-95- Nitrobenzene BRL 1-91 50
88-75- Nitrophenol BRL 1-91 50
100-02- Nitrophenol BRL 1-91 50
62-75- Nitrosodimethylamine BRL 1-91 50
621-64- N- Nitrosodi-n-propylamine BRL 1-91 50
86-30-6 Nitrosodiphenylamine BRL 1-91 50
87 -86- Pentachlorophenol BRL 1-91 50
85-0- Phenanthrene BRL 1-91 50
108-95- Phenol BRL 1-91 50
129-00-0 Pyrene BRL 1-91 50
110-86- Pyridine BRL 1-91 50
120-82- 4- Trichlorobenzene BRL 1-91 50
95-95- 5- Trichlorophenol BRL 1-91 50
88-06- 6- T richlorophenol BRL 1-91 50
Surrogate recoveries
321-60- Fluorobipheny 30- 130
367- 12- Fuorophenol 15- 110
4165-60- Nitrobenzene- 30- 130
4165-62- Pheno- 15- 110
1718-51- Terpheny-d4 30- 130
118- 79- 6- Tribromophenol 15- 110
Semivolatile Organic Compounds by GC
Pol chlorinated Bi hen ls b EPA 608
Prepared by method SW846 3510C
12674- 11-2 Aroclor- 1016 BRL 1-91 0650 EPA 608 15- May- 16-May-08 8051106
11104-28-2 Aroclor-1221 BRL IJgl 0650
11141-16-5 Aroclor- 1232 BRL 1-91 0650
53469-21-9 Aroclor- 1242 BRL 1-91 0650
12672-29-6 Aroclor- 1248 BRL 1-91 0650
11097-69-1 Aroclor- 1254 BRL 1-91 0650
11096-82-5 Aroclor -1260 BRL 1-91 0650
37324-23-5 Aroclor-1262 BRL 1-91 0650
11100-14-4 Aroclor-1268 BRL IJgl 0650
Surrogate recoveries
2051-24- Decachlorobipheny (Sr) 105 30- 150
10386-84-2 4 DB-Octafluorobiphenyl (Sr) 30- 150
Extractable Petroleum Hydrocarbons
mgl EPA 1664 Rev A 15-May- 19-May-08 8051102Non-polar material (SGT- HEM)
Soluble Metals by EPA 2006000 Series Metbods
Field Filtered NA EPA 200 73005A 15- May- 15-May-08 8051192Filtration
Soluble Metals by EPA 200 Series Methods
7440-22-4 Silver BRL mgl 0002 EPA 200 21-May- 27- May-08 8051249
This laboratory report is IlOt mlid without (II authorized signature on the cover page
Reportble Detection Limit BRL = Below Reporting Limit Page 7 of 25
Sam le Identification MW-
Client Pro ect 2920-96shy
Matrix Ground Water
Collection DateTime 13-May-08 1030
Received 14-May-
SA 78602shy
CAS No A nalyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Soluble Metals by EPA 200 Series Methods
7440-38shy Arsenic 0468 mg1 0040 EPA 200 21-Mayshy 21-May-08 80511 50
7440-43shy Cadmium BRL mg1 0002 EPA 200 21-May-088051249
7440-47shy Chromium BRL mg1 0050 EPA 200 21-May-088051150
7440-50-8 Copper BRL mg1 0050
7439-89-6 Iron 184 mg1 0150
7439-97-6 Mercury BRL mg1 00020 EPA 245 17470A 21-May-088051152
7440-02-0 Nickel BRL mg1 0050 EPA 200 21-May-088051150
7439-92shy Lead 0011 mg1 0002 EPA 200 21-May-088051249
7440-36-0 Antimony 0003 mg1 0002
7782-49shy Selenium BRL mg1 0150 EPA 200 21-May-08 8051150
7440-66-6 Zinc 0186 mgl 0050
General Chemistry Parameters
Filtration Completed NA Varies 14-Mayshy 14-May-08 8051095
18540-29-9 Hexavalent Chromium (soluble) BRL HT2 mg1 125 SM3500CrDI796A 14-Mayshy 14-May-08 8051094 R01 2013 2016
57-12shy Cyanide (total) BRL mg1 0100 EPA 3354 19-Mayshy 19-May-088051374
7782-50shy Total Residual Chlorine BRL CIHT mg1 500 Hach 8167 14-Mayshy 14-May-08 8051049 R01 1900 2001
Total Suspended Solids 580 mg1 25 SM2540D 16-Mayshy 16-May-08 8051275
This lahomtOlY report is not valid without an authorized signature on the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page 8 of 25
Volatie Organic Compounds - Quality Control
Analyte( s)
Batch 8051244 - SW846 5030 Water MS
Blank 8051244-BLK1
Prepared 16-May-08 Analyzed 17-May-
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromochloromethane
1 Dichlorobenzene
1 Dichlorobenzene
1 Dichlorobenzene
1-Dichloroethane
1 Dichloroethane
1 1-Dichloroethene
cis- Dichloroethene
trans- 1 Dichloroethene
1 Dichloropropane
cis- 1 Dichloropropene
trans- 1 Dichloropropene
Ethylbenzene
Hexanone (MBK)
Methyl tert-butyl ether
Methyl- pentanone (MIBK)
Methylene chloride
Styrene
2- Tetrachloroethane
Tetrachloroethene
Toluene
1- Trichloroethane
2- Trichloroethane
Trichloroethene
Trichlorofluoromethane (Freon 11)
Vinyl chloride
p-Xylene
Xylene
Surrogate 4-Bromofluorobenzene Surrogate Toluene-
Surrogate 1 Dichloroethane-Surrogate Dibromofluoromethane
LCS B051244-BS1
Prepared 16-May-08 Analyzed 17 -May-
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Spike Source REC RPD
Result Flag Units RDL Level Result REC Limits RPD Limit
BRL gl 20
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl 10
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gll
BRL gi
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl 10
BRL gll
BRL gll 10
BRL gl 10
BRL gll
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
41 gl 50 70- 130 49 gl 50 70- 130 59 gl 50 119 70- 130 52 gl 50 105 70- 130
QC2 jgl 20 70- 130
18 jgl 20 70- 130
192 jgl 20 35- 155
18 jgl 20 45- 169
19 jgl 20 242
This laboratOlY repol1 is lot valid without 011 authorized sigllature 011 the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page 9 of 25
Volatie Organic Compounds - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051244 - SW846 5030 Water MS
LC5 8051244B51
Prepared 16-May-08 Analyzed 17-May-
Butanone (MEK) 10 QC2 gl 20 70- 130
Carbon tetrachloride 204 gl 20 102 70- 140
Chlorobenzene 18 gl 20 70- 130
Chloroethane 164 gl 20 14-230
Chloroform 18 gll 20 51- 138
Chloromethane 21 gl 20 106 273
Dibromochloromethane 18 gl 20 53- 149
1 Dichlorobenzene 20 gl 20 104 18- 190
1 Dichlorobenzene 19 gl 20 59- 156
1 A-Dichlorobenzene 18 gl 20 18- 190
1- Dichloroethane 19 gl 20 59- 155
1 Dichloroethane 19 gl 20 49- 155
1-Dichloroethene 16 gl 20 70- 130
cis- 1 Dichloroethene 17 gl 20 70- 130
trans- 1 Dichloroethene 16 gll 20 54- 156
1 Dichloropropane 18 gl 20 210
cis- Dichloropropene 17 gl 20 227
trans- 1 Dichloropropene 17 gl 20 17- 183
Ethylbenzene 19 gl 20 37- 162
Hexanone (MBK) 124 QC2 gl 20 70- 130
Methyl tert-butyl ether 19 gl 20 70- 130
Methylshy pentanone (MIBK) 17 gl 20 70- 130
Methylene chloride 16 gl 20 221
Styrene 17 gl 20 70- 130
1 Tetrachloroethane 194 gl 20 46- 157
Tetrachloroethene 15 gl 20 64- 148
Toluene 18 gl 20 70- 130
1- Trichloroethane 20 gl 20 100 52- 162
2- Trichloroethane 18 gl 20 52- 150
Trichloroethene 17 gl 20 71- 157
Trichlorofluoromethane (Freon 11) 19 gl 20 17- 181
Vinyl chloride 21 gl 20 106 251
p-Xylene 39 gl 40 70- 130
Xylene 20 gl 20 102 70- 130
Surrogate 4-Bromofluorobenzene Surrogate Toluene-
Surrogate 1 Dichloroethane-Surrogate Dibromofluoromethane
52 49 56
49
gl
gl
gl
gl
50 50 50
50
105
112 100
70- 130 70- 130 70- 130 70- 130
LC5 DUD (8051244-B5D1
Prepared 16-May-08 Analyzed 17-May-
Acetone QC2 gl 20 70- 130
Benzene 18 gl 20 70- 130
Bromodichloromethane 18 gl 200 35- 155
Bromoform 17 gl 20 45- 169
Bromomethane 18 gl 20 242
Butanone (MEK) 11 QC2 1-91 20 70- 130
Carbon tetrachloride 20 gl 20 100 70- 140
Chlorobenzene 17 gl 20 70- 130
Chloroethane 15 1-91 20 14-230
Chloroform 18 1-91 20 51- 138
This laboratory report is aot valid without a1 authorized sig1ature 01 the cover page
Reportble Detection Limit BRL = Below Reporting Limit Page 10 of25
Volatie Organic Compounds - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051244 - SW846 5030 Water MS
LCS Dup 18051244-BSD1
Prepared 16-May-08 Analyzed 17-May-
Chloromethane 18 1-91 20 273
Dibromochloromethane 174 1-91 20 53- 149
Dichlorobenzene 20 1-91 20 100 18- 190
Dichlorobenzene 18 1-91 20 59- 156
Dichlorobenzene 18 1-91 20 18- 190
Dichloroethane 18 1-91 20 59- 155
Dichloroethane 19 1-91 20 49- 155
Dichloroethene 16 1-91 20 70- 130
cis- Dichloroethene 16 1-91 20 70- 130
trans- Dichloroethene 15 1-91 20 54- 156
Dichloropropane 17 1-91 20 210
cis- Dichloropropene 164 IJgl 20 227
trans- 1 Dichloropropene 164 I-gl 20 17- 183
Etlwlbenzene 18 IJgl 20 37- 162
Hexanone (MBK) 124 QC2 IJgl 20 70- 130
Methyl tert-butyl ether 184 1J91 20 70- 130
Methyl- pentanone (MIBK) 17 IJgl 20 70- 130
Methylene chloride 16 IJgl 20 221
Styrene 16 IJgl 20 70- 130
2- Tetrachloroethane 19 IJgl 20 46- 157
Tetrachloroethene 15 IJgl 20 64- 148
Toluene 17 IJgl 20 70- 130
1- Trichloroethane 19 1-91 20 52- 162
2- Trichloroethane 16 IJgl 20 52- 150
Trichloroethene 15 IJgl 20 71- 157
Trichlorofluoromethane (Freon 11) 17 IJgl 20 17- 181
Vinyl chloride 19 IJglI 20 251
p-Xylene 37 1J91 40 70- 130
Xylene 20 IJgl 20 100 70- 130
Surrogate 4-Bromofluorobenzene 51 IJgl 50 104 70- 130
Surrogate Toluene- 4B gl 50 70- 130
Surrogate 1 0ichloroethane- 53 IJgl 50 106 70- 130 Surrogate Oibromofluoromethane 50 1J9i 50 102 70- 130
Matrix S ike B051244-MS1 Source SA7B629shy
Prepared 16-May-08 Analyzed 17-May-
Benzene 18 20 BRL 70- 130IJgl
Bromodichloromethane 19 IJgl 20 BRL 35- 155
Bromoform 18 IJgl 20 BRL 45- 169
Bromomethane 16 IJgl 20 BRL 242
Carbon tetrachloride 21 IJgl 20 BRL 106 70- 140
Chlorobenzene 18 IJgl 20 BRL 70- 130
Chloroethane 16 IJgl 20 BRL 14-230
Chloroform 18 IJgl 20 BRL 51- 138
Chloromethane 19 IJgl 20 BRL 273
Dibromochloromethane 17 IJgl 20 BRL 53- 149
1 Dichlorobenzene 22 IJgl 20 BRL 112 18- 190
1 Dichlorobenzene 22 IJgl 20 BRL 110 59-156
1 Dichlorobenzene 21 IJgl 20 BRL 109 18- 190
1- Dichloroethane 19 IJgl 20 BRL 59- 155
1 Dichloroethane 18 IJgl 20 BRL 49- 155
This laboratory report is 110t mUd without an authorized signature on the covel page
Reportble Detection Limit BRL = Below Reporting Limit Page It of25
Volatile Organic Compounds - Quality Control
p
Spike Source REC RPD
Result REC imits RPD LimitAnalyte(s) Result Flag Units RDL Level
Batch 8051244 - SW846 5030 Water MS
Matrix ike S051244-MS1 Source SA7B629shy
Prepared 16-May-08 Analyzed 17-Mayshy
17 20 BRL 70- 130 1- Dichloroethene IJgl
16 20 BRL 54- 156trans- 1 Dichloroethene IJgl
21020 BRL1 Dichloropropane 17 1J91
cis- 1 Dichloropropene 17 IJgl 20 BRL 227
17- 183trans- 1 Dichloropropene 184 1J91 20 BRL
20 20 BRL 103 37- 162Ethylbenzene IJgl
15 20 BRL 221Methylene chloride IJgl
20 BRL 46- 1572- Tetrachloroethane 19 1J91
20 BRL 64- 148Tetrachloroethene 18 1J91
BRL 70- 130Toluene 18 1J91 20
105 52-1621- Trichloroethane 211 IJgl 20 BRL
18 20 BRL 52- 1502- Trichloroethane IJgl
17 20 BRL 71- 157Trichloroethene 1J91
20 BRL 17- 181Trichloroluoromethane (Freon 11) 194 IJgl
20 BRL 103 251Vinyl chloride 20 IJgl
102 70- 130Surrogate 4-Bromofluorobenzene 50 IJgl 50 50 70- 130Surrogate Toluene- 49 1J91
56 50 112 70- 130Surrogate 1 Dichloroethane- IJgl
50 100 70- 130Surrogate Dibromofluoromethane 50 IJgl
Matrix S ike Du S051244-MSD1 Source SA7S629shy
Prepared 16-May-08 Analyzed 17-Mayshy
18 20 BRL 70- 130Benzene IJgl
18 20 BRL 35- 155Bromodichloromethane IJgl
17 20 BRL 45- 169Bromoform IJgl
20 BRL 242Bromomethane 17 IJgl
20 BRL 103 70- 140Carbon tetrachloride 20 IJgl
18 20 BRL 70- 130Chlorobenzene 1J91
14-230Chloroethane 16 IJgl 20 BRL
20 51- 138Chloroform 184 IJgl BRL
Chloromethane 19 1J91 20 BRL 273
18 20 BRL 53- 149Dibromochloromethane 1J91
20 BRL 117 18- 190Dichlorobenzene 234 IJgl
20 BRL 112 59- 156Dichlorobenzene 22 IJgl
BRL 108 18- 190Dichlorobenzene 21 1J91 20
20 59- 1551 Dichloroethane 19 IJgl BRL
18 20 BRL 49- 155Dichloroethane IJgl
16 20 BRL 70- 130Dichloroethene IJgl
20 BRL 54- 156trans- Dichloroethene 154 1J91
20 BRL 210Dichloropropane 17 IJgl
0420 BRL 227cis- Dichloropropene 17 IJgl
17- 183trans- Dichloropropene 17 1J91 20 BRL
BRL 37- 162Ethylbenzene 20 1J91 20 102
Methylene chloride 15 IJgl 20 BRL 221
20 BRL 46- 1572- Tetrachloroethane 192 IJgl
20 BRL 64- 148 04Tetrachloroethene 18 IJgl
BRL 70- 130Toluene 184 1J91 20
52- 1621- Trichloroethane 20 IJgl 20 BRL 104
17 20 BRL 52- 1502- Trichloroethane IJgl
17 20 BRL 71- 157Trichloroethene IJgl
20 BRL 17-181Trichlorofluoromethane (Freon 11) 19 IJgl
This laboratory report is IIOt valid without all authorized sigllllture 011 the cover page
Page 12 of25 Reportble Detection Limit BRL = Below Reporting Limit
Semivolatile Organic Compounds by GCMS - Quality Control
Analyte(s)
Batch 8051216 - SW846 3510C
Blank 8051216-BLK1
Prepared amp Analyzed 16-May-
Isophorone
Methylnaphthalene
Methylphenol
3 amp 4-Methylphenol
Naphthalene
Nitroaniline
Nitroaniline
Nitroaniline
Nitrobenzene
Nitrophenol
Nitrophenol
Nitrosodimethylamine
N- N itrosodi-n-pro pyla mine
N itrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Pyridine
1 24-Trichlorobenzene
24 5- Trichlorophenol
246- Trichlorophenol
Surrogate 2-Fuorobipheny Surrogate 2-Fuoropheno Surrogate Nitrobenzene-Surrogate PhenoshySurrogate Terpheny-d4 Surrogate 6- Tribromopheno
LCS B051216-BS1
Prepared amp Analyzed 16-May-
Acenaphthene
Acenaphthylene
Aniline
Anthracene
AzobenzenelDi phenyld lazine
Benzidine
Benzo (a) anthracene
Benzo (a) pyrene
Benzo (b) fluoranthene
Benzo (g i) perylene
Benzo (k) fluoranthene
Benzoic acid
Benzyl alcohol
B is(2-chloroethoxy)methane
B i s (2-ch loroethyl)eth e r
Bis(2-ch loroisopropyl) ether
B is(2-ethy Ih exyl) phtha late
Bromophenyl phenyl ether
Butyl benzyl phthalate
Carbazole
Spike Source REC RPD
Result Flag Units RDL Level Result REC Limits RPD Limit
BRL gl
BRL gl
BRL gl
BRL gl 10
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gll
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
370 gl 50 30- 130 40 gl 50 15- 110 39 gl 50 30- 130 43 gl 50 15- 110 36 gl 50 30- 130 40 gl 50 15- 110
41 gl 50 40- 140
43 gI 50 40- 140
41 gl 50 40- 140
38 gl 50 40- 140
45 gl 50 40- 140
49 gl 50 153
41 gl 50 40- 140
43 gl 50 40- 140
41 gl 50 40- 140
41 gll 50 40- 140
45 gl 50 40- 140
32 gl 50 12- 149
41 gl 50 40- 140
39 gl 50 40- 140
384 gl 50 40- 140
47 gl 50 40- 140
47 gl 50 40- 140
40 gl 50 40- 140
47 gI 50 40- 140
56 gI 50 112 200
This laboratory report is lIot valid witllOut a1l authorized sigllature 011 the coverpage
Reportble Detection Limit BRL = Below Reporting Limit Page 15 of25
Semivolatile Organic Compounds by GCMS - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051216 - SW846 3510C
LCS 8051216-BS1
Prepared amp Analyzed 16-Mayshy
50 30- 1304 -C hloro-3-methylphenol 42 IJgl
40- 140Chloroaniline 39 IJgl 50
Chloronaphthalene 37 IJgl 50 40- 140
Chlorophenol 37 IJgl 50 30- 130
50 40- 140
40- 140
Chlorophenyl phenyl ether 45 IJgl
Chrysene 43 IJgl 50
Dibenzo (a h) anthracene 43 IJgl 50 40- 140
Dibenzofuran IJgl38 50 40- 140
50 40- 1401 Dichlorobenzene 35 IJgl
40- 1401 Dichlorobenzene 264 IJgl 50
40- 1401 Dichlorobenzene 434 IJgl 50
58 50 116 40- 1403 - Dichlorobenzidine IJgl
50 30- 130
40- 140 24-Dichlorophenol 38 IJgl
Diethyl phthalate 484 IJgl 50
50 40- 140Dimethyl phthalate 464 IJgl
Dlmethylphenol 39 IJgl 50 30- 130
DI-n-butyl phthalate 44 IJgll 50 40- 140
30- 130 6-Di nitro- 2-methylphenol 38 1J91 50
30- 130Dinltrophenol 36 1J91 50
42 50 40- 14024-Dlnitrotoluene 1J91
Dlnitrotoluene 1J9141 50 40- 140
Di-n-octyl phthalate 52 IJgl 50 104 40- 140
40- 140Fluoranthene 40 IJgl 50
Fluorene 41 IJgl 50 40- 140
39 50 40- 140Hexachlorobenzene IJgl
50 40- 140Hexachlorobutadiene 40 IJgl
40- 140Hexach lorocyclopentad iene 294 IJgl 50
40 50 40- 140Hexachloroethane IJgl
42 50 40-140Indeno (1 3-cd) pyrene IJgl
50 40- 140Isophorone 40 IJgl
40- 140Methylnaphthalene 394 IJgl 50
40- 140Methylphenol 39 IJgl 50
40 10 50 40- 1403 amp 4-Methylphenol IJgl
37 50 40-140Naphthalene IJgl
50 40-140Nitroaniline 39 IJgl
Nitroaniline 51 IJgl 50 102 40- 140
48 50 40- 140Nltroaniline 1J91
50 40- 140Nitrobenzene 40 IJgl
30- 130Nitrophenol 36 IJgl 50
40 IJgl 50 30- 130Nitrophenol 40- 140Nitrosodimethylamine 32 1J91 50
50 40-140N- N itrosodi-n-propyla mine 46 IJgl
40- 140N itrosodi phenyla ml ne 44 IJgl 50
41 IJgl 50 30- 130Pentachlorophenol 40- 140Phenanthrene 38 IJgl 50
50 30- 130Phenol 38 IJgl
40- 140Pyrene 424 1J91 50
40- 140Pyridine 294 1J91 50
40- 14024- Trichlorobenzene 364 IJgl 50
This laboratory report is not mlid without an authorized signature 011 the cover page
Page 16 of25 Reportble Detection Limit BRL = Below Reporting Limit
Semivolatie Organic Compounds by GCMS - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
BMch 8051216 - SW846 3510C
LC5 8051216-851
Prepared amp Analyzed 16-Mayshy
24 5- Trichlorophenol 404 gl 50 30- 130
246- Trichlorophenol 42 gl 50 30- 130
Surrogate 2-Fluorobiphenyl 29 gl 50 30- 130
Surrogate 2-Fluorophenot 27 gl 50 15- 110
Surrogate Nitrobenzene- 30 gl 50 30- 130
Surrogate Phenol- 29 gl 50 15- 110
Surrogate Terpheny-d4 30 gl 50 30- 130
Surrogate 6- Tribromopheno 324 gl 50 15- 110
This laboratory report is lIot valid without all authorized sigllature 011 tlle cover page
Reportble Detection Limit BRL = Below Reporting Limit Page 17 of25
Semivolatie Organic Compounds by GC - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051106 - SW846 3510C
Blank S051106-BLK1
Prepared amp Analyzed 15-Mayshy
Aroclor- 1016 BRL gI 0200
Aroclor- 1016 (2C) BRL gI 0200
Aroclor- 1221 BRL gI 0200
Aroclor- 1221 (2C) BRL gI 0200
Aroclor- 1232 BRL gI 0200
Aroclor- 1232 (2Cj BRL gI 0200
Aroclor- 1242 BRL gI 0200
Aroclor-1242 (2C) BRL gI 0200
Aroclor- 1248 BRL gI 0200
Aroclor- 1248 (2C) BRL gI 0200
Aroclor- 1254 BRL gI 0200
Aroclor- 1254(2Cj BRL gI 0200
Aroclor- 1260 BRL gI 0200
Aroclor- 1260 (2C) BRL gI 0200
Aroclor- 1262 BRL gI 0200
Aroclor- 1262 (2C) BRL gI 0200
Aroclor-1268 BRL gI 0200
Aroclor- 1268 (2C) BRL gI 0200
Surrogate Decachlorobiphenyl (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0231 0224 0194 0191
gI
gI
gI
gI
0200 0200 0200 0200
116 112
30- 150 30- 150 30- 150 30- 150
LC5 8051106-B51
Prepared 15-May-08 Analyzed 16-May-08
Aroclor- 1016 265 gI 0200 250 106 50- 114
Aroclor- 1 016 (2C) 240 gI 0200 250 50- 114
Aroclor- 1260 0269 gI 0200 250 107 40- 127
Aroclor-1260 (2Cj 270 gI 0200 250 108 40- 127
Surrogate Decachlorobiphenyl (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0225 0224 0188 0183
gI
gI
gI
gI
0200 0200 0200 0200
113 112
30- 150 30- 150 30- 150 30- 150
LC5 DUD rS051106-B5D1
Prepared 15-May-08 Analyzed 16-Mayshy
Aroclor- 1016 262 gl 0200 250 105 50- 114
Aroclor-1 016 (2Cj 241 gI 0200 250 50- 114
Aroclor- 1260 277 gI 0200 250 111 40- 127
Aroclor- 1260(2Cj 0260 gI 0200 250 104 40- 127
Surrogate Decachlorobipheny (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0238 0218 0189 0181
gI
gI
gI
gI
0200 0200 0200 0200
119 109
30- 150 30- 150 30- 150 30- 150
This laboratory report is lot valid without (II authorized sigllature 01 the cover page
Page 18 of25 Reportable Detection Limit BRL = Below Reporting Limit
Extractable Petroleum Hydrocarbons - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051102 - SW846 3510C
Blank 8051102-BLK1
Prepared 15-May-08 Analyzed 19-Mayshy
Non-polar material (SGT- HEM) BRL m91
LC8 8051102-B81
Prepared 15-May-08 Analyzed 19-Mayshy
Non-polar material (SGT- HEM) 184 m91 21 81 904
This laboratory report is not valid without an authorized signature 011 the cover page
Page 19 of25 Reportable Detection Limit BRL = Below Reporting Limit
Soluble Metals by EPA 200 Series Methods - Quality Control
Analyte(s) Result Flag Units RDL
Spike
Level
Source
Result REC
REC
Limits RPD
RPD
Limit
Batch 8051150 - EPA 200 Series
Blank 8051150-BLK1
Prepared amp Analyzed 21-May-
Iron
Zinc
Selenium
Nickel
Chromium
Copper
Arsenic
BRL
BRL
BRL
BRL
BRL
BRL
BRL
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0150
0050
0150
0050
0050
0050
0040
LCS 8051150-BS1
Prepared amp Analyzed 21-May-
Selenium
Zinc
Iron
Nickel
Chromium
Arsenic
Copper
123
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0150
0050
0150
0050
0050
0040
0050
103
105
101
100
85- 115
85- 115
85- 115
85- 115
85- 115
85-115
85- 115
licate B051150-DUP1 Source SA7B602shy
Prepared amp Analyzed 21-May-
Iron
Zinc
Selenium
Nickel
Copper
Chromium
Arsenic
17
0162
BRL
0015
0017
BRL
0450
QR8
mgl
mgl
mgl
mgl
mgl
mgl
mgi
0150
0050
0150
0050
0050
0050
0040
184
0186
BRL
0014
0023
BRL
0468
Matrix S ike 8051150-MS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Iron
Selenium
Nickel
Zinc
Copper
Chromium
Arsenic
19 QM2 mgl
mgll
mgl
mgl
mgl
mgl
mgl
0150
0150
0050
0050
0050
0050
0040
125
184
BRL
0014
0186
0023
BRL
0468
104
105
102
70- 130
70- 130
70-130
70- 130
70- 130
70-130
70- 130
Post S ike 8051150-PS1 Source SA78602shy
Prepared amp Analyzed 21-May-
Zinc
Iron
Selenium
Nickel
Copper
Arsenic
Chromium
18 QM2
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0050
0150
0150
0050
0050
0040
0050
0186
184
BRL
0014
0023
0468
BRL
104
104
101
85- 115
85- 115
85- 115
85-115
85-115
85- 115
85-115
Batch 8051152 - EPA200SW7000 Series
Blank B051152-BLK1
Prepared amp Analyzed 21-May-
Mercury BRL mgl 00020
This laboratory report is IIOt valid witllOut all authorized sigllature 011 the coverpage
Page 20 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Soluble Metals by EPA 200 Series Methods - Quality Control
Analyte(s) Result Flag Units RDL
Spike
Level
Source
Result REC
REC
Limits RPD
RPD
Limit
Batch 8051152 - EPA200SW7000 Series
LCS B051152-BS1
Prepared amp Analyzed 21-May-
Mercury 00576 m91 00020 00500 115 85- 115
licate B051152-DUP1 Source SA78602-01
Prepared amp Analyzed 21-May-
Mercury BRL m91 00020 BRL
Matrix S ike 8051152-MS1 Source SA78602shy
Prepared amp Analyzed 21-May-
Mercury 00632 OM m91 00020 00500 BRL 126 75- 125
Post S ike 8051152-PS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Mercury 00624 OC1 m91 00020 00500 BRL 125 85- 115
Batch 8051249 - 2008No digestion
Blank 8051249-BLK1
Prepared amp Analyzed 21-May-
Lead
Antimony
Cadmium
Silver
BRL
BRL
BRL
BRL
m91
m91
m91
m91
0002
0002
0002
0002
LCS B051249-BS1
Prepared amp Analyzed 21-May-
Antimony
Lead
Silver
Cadmium
143
145 OC2
m91
m91
m91
m91
0050
0050
0050
0040
103
115
107
116
85- 115
85- 115
85- 115
85- 115
licate 8051249-DUP1 Source SA7B602shy
Prepared amp Analyzed 21- May-
Lead
Antimony
Cadmium
Silver
0009
0002
00005
00002
ORB
m91
m91
m91
m91
0002
0002
0002
0002
0011
0003
00005
00003
Matrix S ike 8051249-MS1 Source SA78602shy
Prepared amp Analyzed 21- May-
Lead
Antimony
Cadmium
Silver
142
m91
m91
m91
m91
0050
0050
0040
0050
0011
0003
00005
00003
111
101
114
102
70- 130
70-130
70c130
70- 130
Post S ike 8051249-PS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Antimony
Cadmium
Silver
38
OC2
m91
m91
m91
0050
0040
0050
125
0003
00005
00003
110
121
109
85- 115
85- 115
85- 115
This laboratory report is flOt valid IVithout all authorized signature 011 the cOIer page
Reportable Detection Limit BRL Below Reporting Limit Page 21 of 25
General Chemistry Parameters - Quality Control
Spike Source REC RPD
Analyte( s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051049 - General Preparation
Blank S051 049-BLK1
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
Blank S051049-BLK2
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
Blank S051 049-BLK3
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
LCS S051049-BS1
Prepared amp Analyzed 14-May-
Total Residual Chlorine 046 mgl 020 0500 90- 110
LCS S051049-BS2
Prepared amp Analyzed 14-May-
Total Residual Chlorine 047 mgl 020 0500 90- 110
LCS S051049-BS3
Prepared amp Analyzed 14-May-
Total Residual Chlorine 054 mgl 020 0500 108 90-110
licate B051049-DUP1 Source SA7S544shy
Prepared amp Analyzed 14-May-
Total Residual Chlorine 012 mgl 020 010
licate S051049-DUP2 Source SA7S602-01
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020 BRL
Matrix S ike 8051049-MS1 Source SA78544-01
Prepared amp Analyzed 14-May-
Total Residual Chlorine 065 mgl 020 0500 010 110 80- 120
Matrix S ike 8051049-MS2 Source SA7B602shy
Prepared amp Analyzed 14-May-
Total Residual Chlorine mgl 500 125 BRL 108 80- 120
Reference 8051 049-SRM1
Prepared amp Analyzed 14-May-
Total Residual Chlorine 100 mgl 020 0967 103 85-115
Batch 8051094 - General Preparation
Blank 8051094-BLK1
Prepared amp Analyzed 14 May-
Hexavalent Chromium (soluble) BRL mgl 005
Blank 8051 094-BLK2
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) BRL mgl 005
LCS 8051094-BS1
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) 054 mgl 005 90- 110
licate 8051094-DUP1 Source SA78602-01
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) BRL mgl 125 BRL
Thi laboratory report is not valid without all authorized sigllature 011 the cover page
Page 22 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Page 6
PAR
AM
ET
ER
B
elieve B
elieve of
Type of
Absent
Present Sam
ples Sam
ple (e
(l min-
grab)
imum
)
25 1
1 Trichloroethane
GR
AB
26 1
2 Trichloroethane
GR
A
27 Trichloroethylene
GR
AB
28 Vinyl C
hloride G
RA
B
29 Acetone
GR
A
30 14 D
ioxane G
RA
B
31 Total Phenols
GR
AB
32 Pentachlorophenol
GR
AB
33 Total Phthalates 6
GR
AB
(phthalate esthers)
34 Bis (2-E
thylhexyl) G
RA
B
Phthalate (D
ishy(ethylhexyl) P
hthalate)
35 Total G
roup 1 G
RA
P
olycyclic Arom
atic H
ydrocarbons (PA
H)
a Benzo(a) A
nthracene G
RA
B
b Benzo(a) P
yrene G
RA
c Benzo(b )F
luoranthene G
RA
B
d Benzo(k) F
luoranthene G
RA
e Chrysene
GR
AB
The slim
of iijdividual phthalate compounds
Rem
ediation General Perm
it - Notice of Intent
Analytical
Minim
um L
evel M
aximum
daily value A
vg daiJy Value
Method Used
(ML) ofT est
(method )
Method
concentration m
ass concentration
mass
(ugI) (ugI)
(kgday) (ugl)
(kgday)
5030 20
5030 20
5030 20
5030 ~20
5030 400
5030 200
625 50
625 50
625 All phthalates are
BD
L see lab report
625 50
625 A
ll Group I P A
Hs
are BD
L
625 50
625 50
625 50
625 50
625 50
g
PAR
AM
ET
ER
B
elieve B
elieve of
Type of
Analytical
Minim
um
Maxim
um daily value
Average daily value
Absent
Present Sam
ples Sam
ple (e M
ethod Used
Level (M
L) of
(lmin -
grab) (m
ethod ) T
est Method
concentration m
ass concentration
mass
imum
) (ug1)
(ugl) (kgday)
(ugl) (kgday)
f Dibenzo(a
GR
AB
625
-(50
anthracene
Indeno(I 23-cd) G
RA
B
625 -(50
Pyrene
36 Total G
roup II G
RA
B
625 247
Polycyclic A
romatiC
H
ydrocarbons (pAR
)
h Acenaphthene
GR
AB
625
-(10
i Acenaphthylene
GR
A
625 -(50
j Anthracene
GR
A
625 -(50
k Benzo(ghi)
Perylene G
RA
B
625 -(50
I Fluoranthene G
RA
B
625 -(50
m F
luorene G
RA
B
625 -(50
n Naphthalene-
GR
AB
625
247
o Phenanthrene
GR
AB
625
-(50
p Pyrene
GR
AB
625
-(50
37 Total
POlychlorinated
GR
AB
608
065 -(0065
Biphenyls (PC
Bs)
38 Antim
ony G
RA
B
200 03
4Eshy
39 Arsenic
GR
AB
200
468
40 Cadm
ium
GR
AB
200
-( 0
41 Chrom
ium II
(1) G
RA
B
calculated calculated
-(5
42 Chrom
ium V
I G
RA
7196A
-( 125
NO
TE
S (1) Chrom
ium m
= T
otal Chrom
ium - H
exavalent Chrom
ium A
ccording to lab personnel the trivalent chromium
is calculated to be greater or equal to 5 ugI but less than 125 ugl Total
Chrom
ium w
as -(5 ugI and the Hexavalent C
hromium
was less than 125 ugl
Rem
ediation General Perm
it - Notice of Intent
--------
--------
-------
--------
---
PAR
AM
ET
ER
B
elieve B
elieve of
Type of
Analytical
Minim
um
Maxim
um daily value
Avg daily value
Absent
Present Sam
ples Sam
ple (e M
ethod L
evel (ML
) of grab)
Used
Test M
ethod concentration
mass
concentration m
ass(1 m
inshy
imum
) (m
ethod ) (ug1)
(ug1) (kgday)
(ug1) (kgday)
43 Copper
GR
A
200 (5
44 Lead G
RA
200
0001
45 Mercury
GR
A
7470A
(020
46 Nickel
GR
AB
200
(5
GR
AB
200
( 1547 Selenium
48 Silver G
RA
B
200 (0
49 Zinc
GR
A
200 18
0025
50 Iron G
RA
B
200 400
25
Other (describe)
c For discharges where m
etals are believed present please fill out the following
If yes which m
etals A
rsenic and Iron Step
I Do any of the m
etals in the influent have a reasonable potential to exceed the
etIluent limits in A
ppendix II (i the limits set at zero to five dilutions) Y
rg N D
Step 2 For any m
etals which have reasonable potential to exceed the A
ppendix III limits
Look up the lim
it calculated at the corresponding dilution factor in
calculate the dilution factor (DF) using the form
ula in Part I A 3 c) (step 2) of the N
O
Appendix IV
Do any of the m
etals in the influent have the potential to instructions or as determ
ined by the State prior to the submission of this N
OI
exceed the corresponding effuent lim
its in Appendix IV
(i is the
What is the dilution factor for applicable m
etals in1uent concentration above the lim
it set at the calculated dilution M
etals A
rsenic and Iron factor)
yrgND
If Y
es list which m
etals A
rsenic and Iron
DF
Rem
ediation General Pem
lit - Notice of Intent
4 Treatm
ent system inform
ation Please describe the treatment system
using separate sheets as necessary including
a) A description of the treatm
ent system including a schem
atic of the proposed or existing treatment system
S
ee Figures 4 and 5
Frac tank Air stripper
Oilw
ater separator Equalization tanks
Bag filter rg
GA
C filter rg
b) Identity each applicable
treatment unit (check alJ
that apply)
Chlorination
Dechlorination
Other (please describe)
c) Proposed average and maxim
um flow
rates (gallons per minute) for the discharge and the design flow
rate(s) (gallons per minute) ofthe treatm
ent system
Average flow
rate of discharge 15 G
PM
Maxim
um flow
rate oftreatment system
0 G
PM
Design flow
rate of treatment system
0 G
PM
d) A description of chem
ical additives being used or planned to be used (attach MSD
S sheets) Not A
pplicable
5 Receiving surface water(s) Please provide information about the receiving water (s) using separate sheets as necessary including
Identity the discharge pathway
I Direct
I Within facility
I Stonn drain rg I R
iverbrook I W
etlands _ I Other (describe)
Provide a narrative description ofthe discharge pathway including the nam
e(s) of the receiving waters
Discharge to catchbasin and stonnw
ater drainage system in E
ast Broadw
ay which discharges to M
ahoney Brook (S
ee Figure 4)
c) Attach a detailed m
ap(s) indicating the site location and location of the outfall to the receiving water
1 For multiple discharges num
ber the discharges sequentialJy 2 For indirect dischargers indicate the location of the discharge to the indirect conveyance and the discharge to surface w
ater T
he map should also include the location and distance to the nearest sanitary sew
er as well as the locus of nearby sensitive receptors (based on U
SGS topographical
mapping) such as surface w
aters drinking water supplies and w
etland areas d) Provide the state w
ater quality classification of the receiving water
e) Provide the reported or calculated seven day- ten year low flow
(7QlO
) of the receiving water Jcfs
Please attach any calculation sheets used to support stream flow
and dilution calculations See A
ttachment B
f) Is the receiving water a listed 303(d) w
ater quality impaired or lim
ited water Y
es 0 No rg
If yes for which polJutant(s) N
A
Is there a TM
DL
Yes 0
No rg If yes for w
hich pollutant(s) NA
Rem
ediation General Perm
it - Notice of Intent
6 Results of C
onsultation with Federal Services Please p
rovide the following information according to requirements of Par
lBA
and A
ppendices II and VII
a) Are any listed threatened or endangered species or designated critical habitat in proxim
ity to the discharge Yes 0
No rg
Has any consultation w
ith the federal services been completed Y
es 0 No rg
or is consultation underway Y
es 0 No rg
What w
ere the results of the consultation with the U
S Fish and Wildlife Service andor N
ational Marine Fisheries Service (check one) N
ot applicable
a nojeopardy opinion
or written concurrenceD
on a finding that the discharges are not likely to adversely affect any endangered species or critical habitat
b) Are any historic properties listed or eligible for listing on the N
ational Register of H
istoric Places located on the facilty or site or in proximity to the discharge
Yes D
No
Have any state or tribal historic preservation offcer been consulted in this determ
ination (Massachusetts only) Y
es O N
o
7 SU
DD
lemental inform
ation
Please provide any supplemental information Attach any analytical data used to support the application A
ttach any celtification(s) required by the general permit
Attachm
ent A - Figures
Figure I - Site Locus M
ap
Figure 2 - MassD
EP Site Scoring M
ap
Figure 3 - Aerial M
ap
Figure 4 - Proposed Soil Excavation A
rea Map
Figure 5 - T
reatment S
ystem Line D
iagram
Attachm
ent B - D
ilution factor Calculations
Attachment C - L
aboratory Analytical R
eport Groundw
ater
Rem
ediation General Perm
it - Notice of 1ntenl
=-
including the following
8 Signature Requirements
The N
otice ofIntent must be signed by the operator in accordance w
ith the signatory requirements of 40 C
FR Section 122
certification
J certif under penalty of law that this docum
ent and all attachments w
ere prepared under my direction or supervision in accordance w
ith a system
designed to assure that qualifed personnel properly gather and evaluate the information subm
itted Based on m
y inquiry of the person or persons who
manage the system
or those persons directly responsible for gathering the information I certif that t
he information submitted
is to the best of m
y
knowledge and belief true accurate and com
plete J certif that I am aw
are that there are signifcant penalties for submitting false inform
ation including
the possibilty of fine and imprisonm
ent for knowing violations
FacilitySite Name
Form
er Speedw
ay Service S
tation 181 East B
roadwav G
ardner MA
01440
Operator signature
Title
Michael 1 D
ziura Sf Env E
ngineer
Date
4150- q
Rem
ediation General Perm
it - Notice of Intent
-
D- 0
0 0
il (J tu
Bw
o(0 -I
NJW
gQb
J(JZc o c
rou a -10
0 J 6shy
a 0
I-tDC
aJ Qj
E aJshy
ro ro ro
~~~ ~~~~- -- - _ - -_ - ~~~ ~~~~ ~~~ - - _- _- -- -- p __(
MA DEP - Bureau of Waste Site CleanupSITE NME Site S aP 5 MiFlII Former Speeway Station _-II181 Eat Broaday b b d IS I i I GARDNER MA 0144 v ri) i P f f 1 me- 1 5ylmI I L shy J --I 423315n 715835e SiteLocation y o oCop1odQcn Ofof W-_ l
1 1 I
r
r
iBARBER HILL
A c
Cf1 f o s
0
5
Roads Uned Acss Divd Mar Roed Conntor Street Track 1 EPA Sola Source Aquilar FEMA 100yaar iloodplain 0 c Puc Watar SLo GrunSelaceNon Corrty 0
Bounars lOwn Couny DE Region Tian Powerln Ine Aqedut ApprOld Zona2 tNPA Sue Wster Supp Zone A bStZ F--shy--rle
8os Mat Sub SUeor Porenrial Inermtent Man lvo8 Ste Dfm Hyro1apy Wmer FeatllePLio Suleee Wat S H-- L otlMds FrslSaltN-ES WeIMd Habat L
Potentia Prdutiv AqlJlers ModHig Yield Proteoted Opn Space ACC nIL c= Non-Potential Drng Water Sollce AIea ModumHi Yo1d ll DEP Pormrd SoidWes1 FsiIi6s cnifud Verne Pools f0
1I2 KIWUmR$ MtL
January 30 2004 SCALE 1 15000
-
LE
GE
ND
APX PROPER BONDA
- APPROXOiSPO SIT BOUNDA
-GR
OU
ND
WA
TE F1 D
IRE
cnON
SCA
LE
30 60 FE
(APR
OX
CORPORATE ENVIRONMENTAL
)i
AD
VISO
RS
INC
SC
AS SH
OW
D
R B
Y K
HA
EL
DA
TE
10407
JOB
NO
2920-96
AERIAL MAP
FO
RM
ER
SP
EE
DW
AY
ST
AT
ION
FlGURE -3
181 EA
BR
OA
AY
GA
NE
R fo
age 1 ot 1Streamflow Statistics Report
Streamstats Ungaged Site Report Date Wed Dec 31 2008 124908 Site Location Massachusetts NAD83 Latitude 425545 (42 3316) NAD83 Longitude -719758 (-71 58 32) NAD27 Latitude 425545 (423316) NAD27 Longitude - 9763 (-71 58 34) Drainage Area 502 mi2
IPeak Flow Basin Characteristics 1100 Statewide Low Flow (S02 mi2)
Regression Equation Valid Rang
I Min II Max1 Value III Parameter Drainage Area (square miles) 161 149
Mean Basin Slope from 250K DEM (percent) 032 24
Stratified Drift per Stream Length (square mile per mile) 129
Massachusetts Region (dimensionless)
Streamflow Statistics
gO-Percent Prediction Interval Prediction Error
MaximumStatistic Flow (ft s) (percent) Minimum
I D50 IIII 11 1811 II 24511 993
I D60 II 35511 2011 II 03611 35111 2411 II 041 I 201I D70 24111 2611 II 03811 151I D75 11 2811 II 0911 3761I D80 981I D85 1 I 3211 II o6311
1 I 3711 II 0441 1 2 2911 D90 11 4611 II 02411 15511 D95I D98 04511 6011 II 01511 11
I D99 03411 6511 II ol1ll 1021
5011 II 02611 11I M7D2Y 1111 3311 II odl 3 541
I AUGD50
IIIIIIIIIIIIIIIIIIIIII 0311 7111 II 0088411 0981I M7Dl0Y
1010
12312008httpstreamstatsagscrusgsgovgisimgReportsFlowStatsReport3494 - 2008123112498
Dilution Factor Calculation Former Speedway Service Station 181 East Broadway Gardner Ma
DF=(Od+Os)Od
DF = Dilution factor
Od = Max flow rate of discharge in cubic feet per second Os = receiving water flow in cubic feet per seconds 7010 flow rate Mahoney Brook 7010 = min flow for seven consecutive days with a recurrence interval of 10 years
7010 flow based on data obtained from USGS Steamflow Statistics Report Data attached
067
Semivolatile Organic Compounds by GCMS - Quality Control
Analyte( s)
Batch 8051216 - SW846 3510C
Blank 8051216BLK1)
Prepared amp Analyzed 16May-
Acenaphthene
Acenaphthylene
Aniline
Anthracene
AzobenzenelDi phenyld iazi ne
Benzidine
Benzo (a) anthracene
Benzo (a) pyrene
Benzo (b) fiuoranthene
Benzo (g i) perylene
Benzo (k) fiuoranthene
Benzoic acid
Benzyl alcohol
Bis(2-ch loroethoxy) methane
Bis(2-ch loroethyl)ether
Bis(2-ch loroi sopropyl)ether
Bis(2ethylhexyl) phthalate
Bromophenyl phenyl ether
Butyl benzyl phthalate
Carbazole
Ch loro-3-methyl phenol
Chloroaniline
Chloronaphthalene
Chlorophenol
Chlorophenyl phenyl ether
Chrysene
Dibenzo (a h) anthracene
Dibenzofuran
Dichlorobenzene
Dichlorobenzene
14- Dichlorobenzene
3 - Dichlorobenzidine
24-Dichlorophenol
Diethyl phthalate
Dimethyl phthalate
24- Dimethylphenol
Din-butyl phthalate
Dinitro-2-methylphenol
Dinitrophenol
Dinitrotoluene
Dinitrotoluene
Di-noctyl phthalate
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopehtadiene
Hexachloroethane
Indeno (1 cd) pyrene
Spike Source REC RPD
Result Flag Units RDL Level Result REC Limits RPD Limit
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gl
BRL gI
BRL gl
BRL gl
BRL gl
BRL gI
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gll
BRL gl
BRL gll
BRL gl
BRL gl
BRL gI
BRL gI
BRL gI
BRL gl
BRL gI
BRL gI
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gI
BRL gI
BRL gl
This laboratory report is IlOt valid without all authorized sigllature 011 the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page t4 of25
Volatie Organic Compounds - Quality Control
p (
Spike Source REC RPD
RDL Level Result REC Limits RPD Limit Analyte(s) Result Flag Units
Batch 8051244 - SW846 5030 Water MS
Matrix S ike Du 8051244-MSD1 Source SA78629shy
Prepared 16-May-08 Analyzed 17-May-BRL 106 251
Vinyl chloride 21 gl 20
101 70- 130 Surrogate 4-Bromofluorobenzene 50 gl 50
70- 13049 gl 50 111 70- 130
Surrogate Toluene-Surrogate 1 Dichloroethane- 55 gl 50
50 70- 130494 glSurrogate Dibromofluoromethane
Microextractable Organic Compounds - Quality Control
Spike Source REC RPD
Flag Units RDL Level Result REC Limits RPD Limit Analyte(s) Result
Batch 8051105 - SW846 3510C
Blank 8051105-BLK
Prepared amp Analyzed 15-May-
BRL gl 01001 Dibromoethane (ED B)
LCS 8051105-BS1
Prepared amp Analyzed 15-Mayshy50- 1500770 gl 0100 100
licate 8051105-DUP1 Source SA7B583shy
Prepared amp Analyzed 15-May-
BRL gl 0100 BRL
1 Dibromoethane (EDB)
1 Dibromoethane (EDB)
This laborntOlY report is not valid without an authorized signature 011 the cover page
Page 13 of2S Reportable Detection Limit BRL = Below Reporting Limit
Sam le Identification Client Pro ect Matrix Collection DateTime ReceivedMWshy
2920-96- Ground Water 13-May-081030 14-May-SA 78602shy
CAS No Analyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Volatile Organic Compounds
Volatile Or anic Com ounds b GCMS
Prepared by method SW846 5030 Water MS
123-91- Dioxane BRL 1-91 200 EPA 624 16-May-08 17-May-08 8051244
994-05-8 Ter-amyl methyl ether BRL 1-911 20
755- Tert-Butanoll butyl alcohol BRL 1-91 200
67-B4- Acetone BRL 1-91 400
71-43- Benzene BRL 1-91 20
75-27-4 Bromodichloromethane BRL 1-91 20
75-25- Bromoform BRL 1-91 20
74-83- Bromomethane BRL 1-91 40
78-93- Butanone (MEK) BRL 1-91 200
56-23- Carbon tetrachloride BRL 1-91 20
108-90- Chlorobenzene BRL 1-91 20
75-00- Chloroethane BRL 1-91 40
676- Chloroform BRL 1-91 20
74-87- Chloromethane BRL 1-91 40
124-48- Dibromochloromethane BRL 1-91 20
95-50- Dichlorobenzene BRL 1-911 20
541-73- Dichlorobenzene BRL 1-91 20
106-46- Dichlorobenzene BRL 1-91 20
75-34- 1- Dichloroethane BRL 1-91 20
107-06- Dichloroethane BRL 1-91 20
75-35-4 1- Dichloroethene BRL 1-91 20
156-59 cis- Dichloroethene BRL 1-91 20
156-60- trans- Dichloroethene BRL 1-91 20
78-87- 2- Dichloropropane BRL 1-91 20
10061-01-5 cis- Dichloropropene BRL 1-91 20
10061-02-B trans- Dichloropropene BRL 1-91 20
100-41-4 Ethylbenzene 411 1-911 20
591-78-B BRL 200Hexanone (MBK) 1-91
1634-04 -4 Methyl tert-butyl ether BRL 1-91 20
108-10- Methyl- pentanone (MIBK) BRL 1-91 200
75-09- Methylene chloride BRL 1-91 200
100-42- Styrene BRL 1-91 20
79-34- 1 Tetrachloroethane BRL 1-91 20
127- 18-4 T etrachloroethene BRL 1-91 20
108-88- Toluene BRL 1-91 20
71-55 1- Trichloroethane BRL 1-91 20
79-00- 2- Trichloroethane BRL 1-91 20
79-01-B Trichloroethene BRL 1-91 20
759-4 Trichlorofluoromethane (Freon 11) BRL 1-91 20
75-01-4 Vinyl chloride BRL 1-91 20
179601-23-1 m Xylene 390 1-91 40
95-47 Xylene 82 1-91 20
Surrogate recoveries 460-00- Bromofluorobenzene 70- 130
2037-26- Toluene- 100 70- 130
17060-07-0 1 Dichloroethane- 111 70- 130
1868-53- Dibromofluoromethane 70- 130
Microextractable Organic Compounds
106-93-4 1 Dibromoethane (EDB) BRL 1-91 0100 EPA 504 15-May- 15-May-08 8051105
Semivolatile Organic Compounds by GCMS
This laboratory report is not valid without all autllOrized signature 011 the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page 5 of 25
Sam le Identification Client Pro ect Matrix Collection DateTime Received
MWshy2920-96- Ground Water 13-May-081030 14-May-
SA 78602shy
CAS No Analyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Semivolatie Organic Compounds by GCMS
Semi volatile Or anic Com ounds b EPA 625
Prepared by method SW846 3510C 50 EPA 625 16-May- 19-May-08 805121683-32- Acenaphthene BRL IJgl
208-96-8 Acenaphthylene BRL IJgl 50
62-53- BRL IJgll 50Aniline
120- 12- Anthracene BRL 1J91 50
103-33- AzobenzenefDiphenyldiazine BRL IJgl 50
92-87 - Benzidine BRL IJgl 50
56-55- Benzo (a) anthracene BRL 1J91 50
50-32 - Benzo (a) pyrene IJglBRL 50
205-99- Benzo (b) fluoranthene BRL IJgl 50
191-24- Benzo (g i) perylene BRL IJgl 50
50207-08- Benzo (k) fluoranthene BRL IJgl
65-85 Benzoic acid BRL 1J91 50
100-51-6 Benzyl alcohol 1J91BRL 50
50111-91- Bis(2-chloroethoxy)methane BRL 1J91
111-4-4 Bis(2-chloroethyl)ether BRL IJgl 50
501 08-60- Bis(2-chloroisopropyl)ether BRL IJgl
117-81- Bis(2-ethylhexyl)phthalate BRL 1J91 50
101-55- Bromophenyl phenyl ether BRL IJgl 50
5085-68- Butyl benzyl phthalate BRL IJgl
5086-74- Carbazole BRL IJgl
5059-50- C hloro-3-methylphenol BRL IJgl
106-47- Chloroaniline BRL IJgl 50
91-58- Chloronaphthalene IJglBRL 50
5095-57 - Chlorophenol BRL 1J91
507005-72- Chlorophenyl phenyl ether BRL IJgl
216-01- Chrysene tJ91BRL 50
5053-70- Dibenzo (a h) anthracene BRL IJgl
50132-64- Dibenzofuran BRL IJgl
95-50- Dichlorobenzene IJglBRL 50
541-73- 13- Dichlorobenzene BRL IJgl 50
106-46- Dichlorobenzene 1J91BRL 50
5091-94- 3 - Dichlorobenzidine BRL IJgl
120-83- Dichlorophenol BRL IJgl 50
84-66- Diethyl phthalate BRL IJgl 50
131-11- Dimethyl phthalate BRL IJgll 50
105-67- Dimethylphenol BRL 1J91 50
5084-74- Di-n- butyl phthalate BRL 1J91
534-52 - Dinitro-2-methylphenol BRL IJgl 50
51-28- Dinitrophenol IJglBRL 50
50121-14- Dinitrotoluene BRL 1J91
606-20- Dinitrotoluene IJglBRL 50
50117-84-0 Di-n-octyl phthalate BRL IJgl
206-44-0 Fluoranthene 1J91BRL 50
BRL 50
50 86-73- Fluorene IJgi
118-74- Hexachlorobenzene BRL 1J91
87-68- Hexachlorobutadiene 1J91BRL 50
5077-47-4 Hexachlorocyclopentadiene BRL IJgl
67-72- Hexachloroethane IJglBRL 50
50193-39- Indeno (1 3-cd) pyrene BRL IJgl
5078-59- Isophorone BRL IJgl
Tfls laboratory report is not valid without all authorized signature 011 the coverpage
Page 6 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Sam le Identification Client Pro ect Matrix Collection DateTime ReceivedMWshy
2920-96- Ground Water I3-May-081030 14-May-SA 78602shy
CAS No Analyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Semivolatile Organic Compounds by GCMS
Semi volatile Or anic Com ounds b EPA 625
Prepared by method SW846 3510C
91-57 -6 Methylnaphthalene 367 1-91 50 EPA 625 16-May- 19-May-08 8051216
95-48- Methylphenol BRL 1-91 50
108-39-4 3 amp 4-Methylphenol BRL I-gl 100 106-44shy91-20- Naphthalene 247 1-91 50
88-74-4 Nitroaniline BRL 1-91 50
99-09- Nitroaniline BRL 1-91 50
100-01-6 Nitroaniline BRL 1-91 50
98-95- Nitrobenzene BRL 1-91 50
88-75- Nitrophenol BRL 1-91 50
100-02- Nitrophenol BRL 1-91 50
62-75- Nitrosodimethylamine BRL 1-91 50
621-64- N- Nitrosodi-n-propylamine BRL 1-91 50
86-30-6 Nitrosodiphenylamine BRL 1-91 50
87 -86- Pentachlorophenol BRL 1-91 50
85-0- Phenanthrene BRL 1-91 50
108-95- Phenol BRL 1-91 50
129-00-0 Pyrene BRL 1-91 50
110-86- Pyridine BRL 1-91 50
120-82- 4- Trichlorobenzene BRL 1-91 50
95-95- 5- Trichlorophenol BRL 1-91 50
88-06- 6- T richlorophenol BRL 1-91 50
Surrogate recoveries
321-60- Fluorobipheny 30- 130
367- 12- Fuorophenol 15- 110
4165-60- Nitrobenzene- 30- 130
4165-62- Pheno- 15- 110
1718-51- Terpheny-d4 30- 130
118- 79- 6- Tribromophenol 15- 110
Semivolatile Organic Compounds by GC
Pol chlorinated Bi hen ls b EPA 608
Prepared by method SW846 3510C
12674- 11-2 Aroclor- 1016 BRL 1-91 0650 EPA 608 15- May- 16-May-08 8051106
11104-28-2 Aroclor-1221 BRL IJgl 0650
11141-16-5 Aroclor- 1232 BRL 1-91 0650
53469-21-9 Aroclor- 1242 BRL 1-91 0650
12672-29-6 Aroclor- 1248 BRL 1-91 0650
11097-69-1 Aroclor- 1254 BRL 1-91 0650
11096-82-5 Aroclor -1260 BRL 1-91 0650
37324-23-5 Aroclor-1262 BRL 1-91 0650
11100-14-4 Aroclor-1268 BRL IJgl 0650
Surrogate recoveries
2051-24- Decachlorobipheny (Sr) 105 30- 150
10386-84-2 4 DB-Octafluorobiphenyl (Sr) 30- 150
Extractable Petroleum Hydrocarbons
mgl EPA 1664 Rev A 15-May- 19-May-08 8051102Non-polar material (SGT- HEM)
Soluble Metals by EPA 2006000 Series Metbods
Field Filtered NA EPA 200 73005A 15- May- 15-May-08 8051192Filtration
Soluble Metals by EPA 200 Series Methods
7440-22-4 Silver BRL mgl 0002 EPA 200 21-May- 27- May-08 8051249
This laboratory report is IlOt mlid without (II authorized signature on the cover page
Reportble Detection Limit BRL = Below Reporting Limit Page 7 of 25
Sam le Identification MW-
Client Pro ect 2920-96shy
Matrix Ground Water
Collection DateTime 13-May-08 1030
Received 14-May-
SA 78602shy
CAS No A nalyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Soluble Metals by EPA 200 Series Methods
7440-38shy Arsenic 0468 mg1 0040 EPA 200 21-Mayshy 21-May-08 80511 50
7440-43shy Cadmium BRL mg1 0002 EPA 200 21-May-088051249
7440-47shy Chromium BRL mg1 0050 EPA 200 21-May-088051150
7440-50-8 Copper BRL mg1 0050
7439-89-6 Iron 184 mg1 0150
7439-97-6 Mercury BRL mg1 00020 EPA 245 17470A 21-May-088051152
7440-02-0 Nickel BRL mg1 0050 EPA 200 21-May-088051150
7439-92shy Lead 0011 mg1 0002 EPA 200 21-May-088051249
7440-36-0 Antimony 0003 mg1 0002
7782-49shy Selenium BRL mg1 0150 EPA 200 21-May-08 8051150
7440-66-6 Zinc 0186 mgl 0050
General Chemistry Parameters
Filtration Completed NA Varies 14-Mayshy 14-May-08 8051095
18540-29-9 Hexavalent Chromium (soluble) BRL HT2 mg1 125 SM3500CrDI796A 14-Mayshy 14-May-08 8051094 R01 2013 2016
57-12shy Cyanide (total) BRL mg1 0100 EPA 3354 19-Mayshy 19-May-088051374
7782-50shy Total Residual Chlorine BRL CIHT mg1 500 Hach 8167 14-Mayshy 14-May-08 8051049 R01 1900 2001
Total Suspended Solids 580 mg1 25 SM2540D 16-Mayshy 16-May-08 8051275
This lahomtOlY report is not valid without an authorized signature on the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page 8 of 25
Volatie Organic Compounds - Quality Control
Analyte( s)
Batch 8051244 - SW846 5030 Water MS
Blank 8051244-BLK1
Prepared 16-May-08 Analyzed 17-May-
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromochloromethane
1 Dichlorobenzene
1 Dichlorobenzene
1 Dichlorobenzene
1-Dichloroethane
1 Dichloroethane
1 1-Dichloroethene
cis- Dichloroethene
trans- 1 Dichloroethene
1 Dichloropropane
cis- 1 Dichloropropene
trans- 1 Dichloropropene
Ethylbenzene
Hexanone (MBK)
Methyl tert-butyl ether
Methyl- pentanone (MIBK)
Methylene chloride
Styrene
2- Tetrachloroethane
Tetrachloroethene
Toluene
1- Trichloroethane
2- Trichloroethane
Trichloroethene
Trichlorofluoromethane (Freon 11)
Vinyl chloride
p-Xylene
Xylene
Surrogate 4-Bromofluorobenzene Surrogate Toluene-
Surrogate 1 Dichloroethane-Surrogate Dibromofluoromethane
LCS B051244-BS1
Prepared 16-May-08 Analyzed 17 -May-
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Spike Source REC RPD
Result Flag Units RDL Level Result REC Limits RPD Limit
BRL gl 20
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl 10
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gll
BRL gi
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl 10
BRL gll
BRL gll 10
BRL gl 10
BRL gll
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
41 gl 50 70- 130 49 gl 50 70- 130 59 gl 50 119 70- 130 52 gl 50 105 70- 130
QC2 jgl 20 70- 130
18 jgl 20 70- 130
192 jgl 20 35- 155
18 jgl 20 45- 169
19 jgl 20 242
This laboratOlY repol1 is lot valid without 011 authorized sigllature 011 the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page 9 of 25
Volatie Organic Compounds - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051244 - SW846 5030 Water MS
LC5 8051244B51
Prepared 16-May-08 Analyzed 17-May-
Butanone (MEK) 10 QC2 gl 20 70- 130
Carbon tetrachloride 204 gl 20 102 70- 140
Chlorobenzene 18 gl 20 70- 130
Chloroethane 164 gl 20 14-230
Chloroform 18 gll 20 51- 138
Chloromethane 21 gl 20 106 273
Dibromochloromethane 18 gl 20 53- 149
1 Dichlorobenzene 20 gl 20 104 18- 190
1 Dichlorobenzene 19 gl 20 59- 156
1 A-Dichlorobenzene 18 gl 20 18- 190
1- Dichloroethane 19 gl 20 59- 155
1 Dichloroethane 19 gl 20 49- 155
1-Dichloroethene 16 gl 20 70- 130
cis- 1 Dichloroethene 17 gl 20 70- 130
trans- 1 Dichloroethene 16 gll 20 54- 156
1 Dichloropropane 18 gl 20 210
cis- Dichloropropene 17 gl 20 227
trans- 1 Dichloropropene 17 gl 20 17- 183
Ethylbenzene 19 gl 20 37- 162
Hexanone (MBK) 124 QC2 gl 20 70- 130
Methyl tert-butyl ether 19 gl 20 70- 130
Methylshy pentanone (MIBK) 17 gl 20 70- 130
Methylene chloride 16 gl 20 221
Styrene 17 gl 20 70- 130
1 Tetrachloroethane 194 gl 20 46- 157
Tetrachloroethene 15 gl 20 64- 148
Toluene 18 gl 20 70- 130
1- Trichloroethane 20 gl 20 100 52- 162
2- Trichloroethane 18 gl 20 52- 150
Trichloroethene 17 gl 20 71- 157
Trichlorofluoromethane (Freon 11) 19 gl 20 17- 181
Vinyl chloride 21 gl 20 106 251
p-Xylene 39 gl 40 70- 130
Xylene 20 gl 20 102 70- 130
Surrogate 4-Bromofluorobenzene Surrogate Toluene-
Surrogate 1 Dichloroethane-Surrogate Dibromofluoromethane
52 49 56
49
gl
gl
gl
gl
50 50 50
50
105
112 100
70- 130 70- 130 70- 130 70- 130
LC5 DUD (8051244-B5D1
Prepared 16-May-08 Analyzed 17-May-
Acetone QC2 gl 20 70- 130
Benzene 18 gl 20 70- 130
Bromodichloromethane 18 gl 200 35- 155
Bromoform 17 gl 20 45- 169
Bromomethane 18 gl 20 242
Butanone (MEK) 11 QC2 1-91 20 70- 130
Carbon tetrachloride 20 gl 20 100 70- 140
Chlorobenzene 17 gl 20 70- 130
Chloroethane 15 1-91 20 14-230
Chloroform 18 1-91 20 51- 138
This laboratory report is aot valid without a1 authorized sig1ature 01 the cover page
Reportble Detection Limit BRL = Below Reporting Limit Page 10 of25
Volatie Organic Compounds - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051244 - SW846 5030 Water MS
LCS Dup 18051244-BSD1
Prepared 16-May-08 Analyzed 17-May-
Chloromethane 18 1-91 20 273
Dibromochloromethane 174 1-91 20 53- 149
Dichlorobenzene 20 1-91 20 100 18- 190
Dichlorobenzene 18 1-91 20 59- 156
Dichlorobenzene 18 1-91 20 18- 190
Dichloroethane 18 1-91 20 59- 155
Dichloroethane 19 1-91 20 49- 155
Dichloroethene 16 1-91 20 70- 130
cis- Dichloroethene 16 1-91 20 70- 130
trans- Dichloroethene 15 1-91 20 54- 156
Dichloropropane 17 1-91 20 210
cis- Dichloropropene 164 IJgl 20 227
trans- 1 Dichloropropene 164 I-gl 20 17- 183
Etlwlbenzene 18 IJgl 20 37- 162
Hexanone (MBK) 124 QC2 IJgl 20 70- 130
Methyl tert-butyl ether 184 1J91 20 70- 130
Methyl- pentanone (MIBK) 17 IJgl 20 70- 130
Methylene chloride 16 IJgl 20 221
Styrene 16 IJgl 20 70- 130
2- Tetrachloroethane 19 IJgl 20 46- 157
Tetrachloroethene 15 IJgl 20 64- 148
Toluene 17 IJgl 20 70- 130
1- Trichloroethane 19 1-91 20 52- 162
2- Trichloroethane 16 IJgl 20 52- 150
Trichloroethene 15 IJgl 20 71- 157
Trichlorofluoromethane (Freon 11) 17 IJgl 20 17- 181
Vinyl chloride 19 IJglI 20 251
p-Xylene 37 1J91 40 70- 130
Xylene 20 IJgl 20 100 70- 130
Surrogate 4-Bromofluorobenzene 51 IJgl 50 104 70- 130
Surrogate Toluene- 4B gl 50 70- 130
Surrogate 1 0ichloroethane- 53 IJgl 50 106 70- 130 Surrogate Oibromofluoromethane 50 1J9i 50 102 70- 130
Matrix S ike B051244-MS1 Source SA7B629shy
Prepared 16-May-08 Analyzed 17-May-
Benzene 18 20 BRL 70- 130IJgl
Bromodichloromethane 19 IJgl 20 BRL 35- 155
Bromoform 18 IJgl 20 BRL 45- 169
Bromomethane 16 IJgl 20 BRL 242
Carbon tetrachloride 21 IJgl 20 BRL 106 70- 140
Chlorobenzene 18 IJgl 20 BRL 70- 130
Chloroethane 16 IJgl 20 BRL 14-230
Chloroform 18 IJgl 20 BRL 51- 138
Chloromethane 19 IJgl 20 BRL 273
Dibromochloromethane 17 IJgl 20 BRL 53- 149
1 Dichlorobenzene 22 IJgl 20 BRL 112 18- 190
1 Dichlorobenzene 22 IJgl 20 BRL 110 59-156
1 Dichlorobenzene 21 IJgl 20 BRL 109 18- 190
1- Dichloroethane 19 IJgl 20 BRL 59- 155
1 Dichloroethane 18 IJgl 20 BRL 49- 155
This laboratory report is 110t mUd without an authorized signature on the covel page
Reportble Detection Limit BRL = Below Reporting Limit Page It of25
Volatile Organic Compounds - Quality Control
p
Spike Source REC RPD
Result REC imits RPD LimitAnalyte(s) Result Flag Units RDL Level
Batch 8051244 - SW846 5030 Water MS
Matrix ike S051244-MS1 Source SA7B629shy
Prepared 16-May-08 Analyzed 17-Mayshy
17 20 BRL 70- 130 1- Dichloroethene IJgl
16 20 BRL 54- 156trans- 1 Dichloroethene IJgl
21020 BRL1 Dichloropropane 17 1J91
cis- 1 Dichloropropene 17 IJgl 20 BRL 227
17- 183trans- 1 Dichloropropene 184 1J91 20 BRL
20 20 BRL 103 37- 162Ethylbenzene IJgl
15 20 BRL 221Methylene chloride IJgl
20 BRL 46- 1572- Tetrachloroethane 19 1J91
20 BRL 64- 148Tetrachloroethene 18 1J91
BRL 70- 130Toluene 18 1J91 20
105 52-1621- Trichloroethane 211 IJgl 20 BRL
18 20 BRL 52- 1502- Trichloroethane IJgl
17 20 BRL 71- 157Trichloroethene 1J91
20 BRL 17- 181Trichloroluoromethane (Freon 11) 194 IJgl
20 BRL 103 251Vinyl chloride 20 IJgl
102 70- 130Surrogate 4-Bromofluorobenzene 50 IJgl 50 50 70- 130Surrogate Toluene- 49 1J91
56 50 112 70- 130Surrogate 1 Dichloroethane- IJgl
50 100 70- 130Surrogate Dibromofluoromethane 50 IJgl
Matrix S ike Du S051244-MSD1 Source SA7S629shy
Prepared 16-May-08 Analyzed 17-Mayshy
18 20 BRL 70- 130Benzene IJgl
18 20 BRL 35- 155Bromodichloromethane IJgl
17 20 BRL 45- 169Bromoform IJgl
20 BRL 242Bromomethane 17 IJgl
20 BRL 103 70- 140Carbon tetrachloride 20 IJgl
18 20 BRL 70- 130Chlorobenzene 1J91
14-230Chloroethane 16 IJgl 20 BRL
20 51- 138Chloroform 184 IJgl BRL
Chloromethane 19 1J91 20 BRL 273
18 20 BRL 53- 149Dibromochloromethane 1J91
20 BRL 117 18- 190Dichlorobenzene 234 IJgl
20 BRL 112 59- 156Dichlorobenzene 22 IJgl
BRL 108 18- 190Dichlorobenzene 21 1J91 20
20 59- 1551 Dichloroethane 19 IJgl BRL
18 20 BRL 49- 155Dichloroethane IJgl
16 20 BRL 70- 130Dichloroethene IJgl
20 BRL 54- 156trans- Dichloroethene 154 1J91
20 BRL 210Dichloropropane 17 IJgl
0420 BRL 227cis- Dichloropropene 17 IJgl
17- 183trans- Dichloropropene 17 1J91 20 BRL
BRL 37- 162Ethylbenzene 20 1J91 20 102
Methylene chloride 15 IJgl 20 BRL 221
20 BRL 46- 1572- Tetrachloroethane 192 IJgl
20 BRL 64- 148 04Tetrachloroethene 18 IJgl
BRL 70- 130Toluene 184 1J91 20
52- 1621- Trichloroethane 20 IJgl 20 BRL 104
17 20 BRL 52- 1502- Trichloroethane IJgl
17 20 BRL 71- 157Trichloroethene IJgl
20 BRL 17-181Trichlorofluoromethane (Freon 11) 19 IJgl
This laboratory report is IIOt valid without all authorized sigllllture 011 the cover page
Page 12 of25 Reportble Detection Limit BRL = Below Reporting Limit
Semivolatile Organic Compounds by GCMS - Quality Control
Analyte(s)
Batch 8051216 - SW846 3510C
Blank 8051216-BLK1
Prepared amp Analyzed 16-May-
Isophorone
Methylnaphthalene
Methylphenol
3 amp 4-Methylphenol
Naphthalene
Nitroaniline
Nitroaniline
Nitroaniline
Nitrobenzene
Nitrophenol
Nitrophenol
Nitrosodimethylamine
N- N itrosodi-n-pro pyla mine
N itrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Pyridine
1 24-Trichlorobenzene
24 5- Trichlorophenol
246- Trichlorophenol
Surrogate 2-Fuorobipheny Surrogate 2-Fuoropheno Surrogate Nitrobenzene-Surrogate PhenoshySurrogate Terpheny-d4 Surrogate 6- Tribromopheno
LCS B051216-BS1
Prepared amp Analyzed 16-May-
Acenaphthene
Acenaphthylene
Aniline
Anthracene
AzobenzenelDi phenyld lazine
Benzidine
Benzo (a) anthracene
Benzo (a) pyrene
Benzo (b) fluoranthene
Benzo (g i) perylene
Benzo (k) fluoranthene
Benzoic acid
Benzyl alcohol
B is(2-chloroethoxy)methane
B i s (2-ch loroethyl)eth e r
Bis(2-ch loroisopropyl) ether
B is(2-ethy Ih exyl) phtha late
Bromophenyl phenyl ether
Butyl benzyl phthalate
Carbazole
Spike Source REC RPD
Result Flag Units RDL Level Result REC Limits RPD Limit
BRL gl
BRL gl
BRL gl
BRL gl 10
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gll
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
370 gl 50 30- 130 40 gl 50 15- 110 39 gl 50 30- 130 43 gl 50 15- 110 36 gl 50 30- 130 40 gl 50 15- 110
41 gl 50 40- 140
43 gI 50 40- 140
41 gl 50 40- 140
38 gl 50 40- 140
45 gl 50 40- 140
49 gl 50 153
41 gl 50 40- 140
43 gl 50 40- 140
41 gl 50 40- 140
41 gll 50 40- 140
45 gl 50 40- 140
32 gl 50 12- 149
41 gl 50 40- 140
39 gl 50 40- 140
384 gl 50 40- 140
47 gl 50 40- 140
47 gl 50 40- 140
40 gl 50 40- 140
47 gI 50 40- 140
56 gI 50 112 200
This laboratory report is lIot valid witllOut a1l authorized sigllature 011 the coverpage
Reportble Detection Limit BRL = Below Reporting Limit Page 15 of25
Semivolatile Organic Compounds by GCMS - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051216 - SW846 3510C
LCS 8051216-BS1
Prepared amp Analyzed 16-Mayshy
50 30- 1304 -C hloro-3-methylphenol 42 IJgl
40- 140Chloroaniline 39 IJgl 50
Chloronaphthalene 37 IJgl 50 40- 140
Chlorophenol 37 IJgl 50 30- 130
50 40- 140
40- 140
Chlorophenyl phenyl ether 45 IJgl
Chrysene 43 IJgl 50
Dibenzo (a h) anthracene 43 IJgl 50 40- 140
Dibenzofuran IJgl38 50 40- 140
50 40- 1401 Dichlorobenzene 35 IJgl
40- 1401 Dichlorobenzene 264 IJgl 50
40- 1401 Dichlorobenzene 434 IJgl 50
58 50 116 40- 1403 - Dichlorobenzidine IJgl
50 30- 130
40- 140 24-Dichlorophenol 38 IJgl
Diethyl phthalate 484 IJgl 50
50 40- 140Dimethyl phthalate 464 IJgl
Dlmethylphenol 39 IJgl 50 30- 130
DI-n-butyl phthalate 44 IJgll 50 40- 140
30- 130 6-Di nitro- 2-methylphenol 38 1J91 50
30- 130Dinltrophenol 36 1J91 50
42 50 40- 14024-Dlnitrotoluene 1J91
Dlnitrotoluene 1J9141 50 40- 140
Di-n-octyl phthalate 52 IJgl 50 104 40- 140
40- 140Fluoranthene 40 IJgl 50
Fluorene 41 IJgl 50 40- 140
39 50 40- 140Hexachlorobenzene IJgl
50 40- 140Hexachlorobutadiene 40 IJgl
40- 140Hexach lorocyclopentad iene 294 IJgl 50
40 50 40- 140Hexachloroethane IJgl
42 50 40-140Indeno (1 3-cd) pyrene IJgl
50 40- 140Isophorone 40 IJgl
40- 140Methylnaphthalene 394 IJgl 50
40- 140Methylphenol 39 IJgl 50
40 10 50 40- 1403 amp 4-Methylphenol IJgl
37 50 40-140Naphthalene IJgl
50 40-140Nitroaniline 39 IJgl
Nitroaniline 51 IJgl 50 102 40- 140
48 50 40- 140Nltroaniline 1J91
50 40- 140Nitrobenzene 40 IJgl
30- 130Nitrophenol 36 IJgl 50
40 IJgl 50 30- 130Nitrophenol 40- 140Nitrosodimethylamine 32 1J91 50
50 40-140N- N itrosodi-n-propyla mine 46 IJgl
40- 140N itrosodi phenyla ml ne 44 IJgl 50
41 IJgl 50 30- 130Pentachlorophenol 40- 140Phenanthrene 38 IJgl 50
50 30- 130Phenol 38 IJgl
40- 140Pyrene 424 1J91 50
40- 140Pyridine 294 1J91 50
40- 14024- Trichlorobenzene 364 IJgl 50
This laboratory report is not mlid without an authorized signature 011 the cover page
Page 16 of25 Reportble Detection Limit BRL = Below Reporting Limit
Semivolatie Organic Compounds by GCMS - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
BMch 8051216 - SW846 3510C
LC5 8051216-851
Prepared amp Analyzed 16-Mayshy
24 5- Trichlorophenol 404 gl 50 30- 130
246- Trichlorophenol 42 gl 50 30- 130
Surrogate 2-Fluorobiphenyl 29 gl 50 30- 130
Surrogate 2-Fluorophenot 27 gl 50 15- 110
Surrogate Nitrobenzene- 30 gl 50 30- 130
Surrogate Phenol- 29 gl 50 15- 110
Surrogate Terpheny-d4 30 gl 50 30- 130
Surrogate 6- Tribromopheno 324 gl 50 15- 110
This laboratory report is lIot valid without all authorized sigllature 011 tlle cover page
Reportble Detection Limit BRL = Below Reporting Limit Page 17 of25
Semivolatie Organic Compounds by GC - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051106 - SW846 3510C
Blank S051106-BLK1
Prepared amp Analyzed 15-Mayshy
Aroclor- 1016 BRL gI 0200
Aroclor- 1016 (2C) BRL gI 0200
Aroclor- 1221 BRL gI 0200
Aroclor- 1221 (2C) BRL gI 0200
Aroclor- 1232 BRL gI 0200
Aroclor- 1232 (2Cj BRL gI 0200
Aroclor- 1242 BRL gI 0200
Aroclor-1242 (2C) BRL gI 0200
Aroclor- 1248 BRL gI 0200
Aroclor- 1248 (2C) BRL gI 0200
Aroclor- 1254 BRL gI 0200
Aroclor- 1254(2Cj BRL gI 0200
Aroclor- 1260 BRL gI 0200
Aroclor- 1260 (2C) BRL gI 0200
Aroclor- 1262 BRL gI 0200
Aroclor- 1262 (2C) BRL gI 0200
Aroclor-1268 BRL gI 0200
Aroclor- 1268 (2C) BRL gI 0200
Surrogate Decachlorobiphenyl (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0231 0224 0194 0191
gI
gI
gI
gI
0200 0200 0200 0200
116 112
30- 150 30- 150 30- 150 30- 150
LC5 8051106-B51
Prepared 15-May-08 Analyzed 16-May-08
Aroclor- 1016 265 gI 0200 250 106 50- 114
Aroclor- 1 016 (2C) 240 gI 0200 250 50- 114
Aroclor- 1260 0269 gI 0200 250 107 40- 127
Aroclor-1260 (2Cj 270 gI 0200 250 108 40- 127
Surrogate Decachlorobiphenyl (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0225 0224 0188 0183
gI
gI
gI
gI
0200 0200 0200 0200
113 112
30- 150 30- 150 30- 150 30- 150
LC5 DUD rS051106-B5D1
Prepared 15-May-08 Analyzed 16-Mayshy
Aroclor- 1016 262 gl 0200 250 105 50- 114
Aroclor-1 016 (2Cj 241 gI 0200 250 50- 114
Aroclor- 1260 277 gI 0200 250 111 40- 127
Aroclor- 1260(2Cj 0260 gI 0200 250 104 40- 127
Surrogate Decachlorobipheny (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0238 0218 0189 0181
gI
gI
gI
gI
0200 0200 0200 0200
119 109
30- 150 30- 150 30- 150 30- 150
This laboratory report is lot valid without (II authorized sigllature 01 the cover page
Page 18 of25 Reportable Detection Limit BRL = Below Reporting Limit
Extractable Petroleum Hydrocarbons - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051102 - SW846 3510C
Blank 8051102-BLK1
Prepared 15-May-08 Analyzed 19-Mayshy
Non-polar material (SGT- HEM) BRL m91
LC8 8051102-B81
Prepared 15-May-08 Analyzed 19-Mayshy
Non-polar material (SGT- HEM) 184 m91 21 81 904
This laboratory report is not valid without an authorized signature 011 the cover page
Page 19 of25 Reportable Detection Limit BRL = Below Reporting Limit
Soluble Metals by EPA 200 Series Methods - Quality Control
Analyte(s) Result Flag Units RDL
Spike
Level
Source
Result REC
REC
Limits RPD
RPD
Limit
Batch 8051150 - EPA 200 Series
Blank 8051150-BLK1
Prepared amp Analyzed 21-May-
Iron
Zinc
Selenium
Nickel
Chromium
Copper
Arsenic
BRL
BRL
BRL
BRL
BRL
BRL
BRL
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0150
0050
0150
0050
0050
0050
0040
LCS 8051150-BS1
Prepared amp Analyzed 21-May-
Selenium
Zinc
Iron
Nickel
Chromium
Arsenic
Copper
123
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0150
0050
0150
0050
0050
0040
0050
103
105
101
100
85- 115
85- 115
85- 115
85- 115
85- 115
85-115
85- 115
licate B051150-DUP1 Source SA7B602shy
Prepared amp Analyzed 21-May-
Iron
Zinc
Selenium
Nickel
Copper
Chromium
Arsenic
17
0162
BRL
0015
0017
BRL
0450
QR8
mgl
mgl
mgl
mgl
mgl
mgl
mgi
0150
0050
0150
0050
0050
0050
0040
184
0186
BRL
0014
0023
BRL
0468
Matrix S ike 8051150-MS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Iron
Selenium
Nickel
Zinc
Copper
Chromium
Arsenic
19 QM2 mgl
mgll
mgl
mgl
mgl
mgl
mgl
0150
0150
0050
0050
0050
0050
0040
125
184
BRL
0014
0186
0023
BRL
0468
104
105
102
70- 130
70- 130
70-130
70- 130
70- 130
70-130
70- 130
Post S ike 8051150-PS1 Source SA78602shy
Prepared amp Analyzed 21-May-
Zinc
Iron
Selenium
Nickel
Copper
Arsenic
Chromium
18 QM2
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0050
0150
0150
0050
0050
0040
0050
0186
184
BRL
0014
0023
0468
BRL
104
104
101
85- 115
85- 115
85- 115
85-115
85-115
85- 115
85-115
Batch 8051152 - EPA200SW7000 Series
Blank B051152-BLK1
Prepared amp Analyzed 21-May-
Mercury BRL mgl 00020
This laboratory report is IIOt valid witllOut all authorized sigllature 011 the coverpage
Page 20 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Soluble Metals by EPA 200 Series Methods - Quality Control
Analyte(s) Result Flag Units RDL
Spike
Level
Source
Result REC
REC
Limits RPD
RPD
Limit
Batch 8051152 - EPA200SW7000 Series
LCS B051152-BS1
Prepared amp Analyzed 21-May-
Mercury 00576 m91 00020 00500 115 85- 115
licate B051152-DUP1 Source SA78602-01
Prepared amp Analyzed 21-May-
Mercury BRL m91 00020 BRL
Matrix S ike 8051152-MS1 Source SA78602shy
Prepared amp Analyzed 21-May-
Mercury 00632 OM m91 00020 00500 BRL 126 75- 125
Post S ike 8051152-PS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Mercury 00624 OC1 m91 00020 00500 BRL 125 85- 115
Batch 8051249 - 2008No digestion
Blank 8051249-BLK1
Prepared amp Analyzed 21-May-
Lead
Antimony
Cadmium
Silver
BRL
BRL
BRL
BRL
m91
m91
m91
m91
0002
0002
0002
0002
LCS B051249-BS1
Prepared amp Analyzed 21-May-
Antimony
Lead
Silver
Cadmium
143
145 OC2
m91
m91
m91
m91
0050
0050
0050
0040
103
115
107
116
85- 115
85- 115
85- 115
85- 115
licate 8051249-DUP1 Source SA7B602shy
Prepared amp Analyzed 21- May-
Lead
Antimony
Cadmium
Silver
0009
0002
00005
00002
ORB
m91
m91
m91
m91
0002
0002
0002
0002
0011
0003
00005
00003
Matrix S ike 8051249-MS1 Source SA78602shy
Prepared amp Analyzed 21- May-
Lead
Antimony
Cadmium
Silver
142
m91
m91
m91
m91
0050
0050
0040
0050
0011
0003
00005
00003
111
101
114
102
70- 130
70-130
70c130
70- 130
Post S ike 8051249-PS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Antimony
Cadmium
Silver
38
OC2
m91
m91
m91
0050
0040
0050
125
0003
00005
00003
110
121
109
85- 115
85- 115
85- 115
This laboratory report is flOt valid IVithout all authorized signature 011 the cOIer page
Reportable Detection Limit BRL Below Reporting Limit Page 21 of 25
General Chemistry Parameters - Quality Control
Spike Source REC RPD
Analyte( s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051049 - General Preparation
Blank S051 049-BLK1
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
Blank S051049-BLK2
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
Blank S051 049-BLK3
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
LCS S051049-BS1
Prepared amp Analyzed 14-May-
Total Residual Chlorine 046 mgl 020 0500 90- 110
LCS S051049-BS2
Prepared amp Analyzed 14-May-
Total Residual Chlorine 047 mgl 020 0500 90- 110
LCS S051049-BS3
Prepared amp Analyzed 14-May-
Total Residual Chlorine 054 mgl 020 0500 108 90-110
licate B051049-DUP1 Source SA7S544shy
Prepared amp Analyzed 14-May-
Total Residual Chlorine 012 mgl 020 010
licate S051049-DUP2 Source SA7S602-01
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020 BRL
Matrix S ike 8051049-MS1 Source SA78544-01
Prepared amp Analyzed 14-May-
Total Residual Chlorine 065 mgl 020 0500 010 110 80- 120
Matrix S ike 8051049-MS2 Source SA7B602shy
Prepared amp Analyzed 14-May-
Total Residual Chlorine mgl 500 125 BRL 108 80- 120
Reference 8051 049-SRM1
Prepared amp Analyzed 14-May-
Total Residual Chlorine 100 mgl 020 0967 103 85-115
Batch 8051094 - General Preparation
Blank 8051094-BLK1
Prepared amp Analyzed 14 May-
Hexavalent Chromium (soluble) BRL mgl 005
Blank 8051 094-BLK2
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) BRL mgl 005
LCS 8051094-BS1
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) 054 mgl 005 90- 110
licate 8051094-DUP1 Source SA78602-01
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) BRL mgl 125 BRL
Thi laboratory report is not valid without all authorized sigllature 011 the cover page
Page 22 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Page 7
g
PAR
AM
ET
ER
B
elieve B
elieve of
Type of
Analytical
Minim
um
Maxim
um daily value
Average daily value
Absent
Present Sam
ples Sam
ple (e M
ethod Used
Level (M
L) of
(lmin -
grab) (m
ethod ) T
est Method
concentration m
ass concentration
mass
imum
) (ug1)
(ugl) (kgday)
(ugl) (kgday)
f Dibenzo(a
GR
AB
625
-(50
anthracene
Indeno(I 23-cd) G
RA
B
625 -(50
Pyrene
36 Total G
roup II G
RA
B
625 247
Polycyclic A
romatiC
H
ydrocarbons (pAR
)
h Acenaphthene
GR
AB
625
-(10
i Acenaphthylene
GR
A
625 -(50
j Anthracene
GR
A
625 -(50
k Benzo(ghi)
Perylene G
RA
B
625 -(50
I Fluoranthene G
RA
B
625 -(50
m F
luorene G
RA
B
625 -(50
n Naphthalene-
GR
AB
625
247
o Phenanthrene
GR
AB
625
-(50
p Pyrene
GR
AB
625
-(50
37 Total
POlychlorinated
GR
AB
608
065 -(0065
Biphenyls (PC
Bs)
38 Antim
ony G
RA
B
200 03
4Eshy
39 Arsenic
GR
AB
200
468
40 Cadm
ium
GR
AB
200
-( 0
41 Chrom
ium II
(1) G
RA
B
calculated calculated
-(5
42 Chrom
ium V
I G
RA
7196A
-( 125
NO
TE
S (1) Chrom
ium m
= T
otal Chrom
ium - H
exavalent Chrom
ium A
ccording to lab personnel the trivalent chromium
is calculated to be greater or equal to 5 ugI but less than 125 ugl Total
Chrom
ium w
as -(5 ugI and the Hexavalent C
hromium
was less than 125 ugl
Rem
ediation General Perm
it - Notice of Intent
--------
--------
-------
--------
---
PAR
AM
ET
ER
B
elieve B
elieve of
Type of
Analytical
Minim
um
Maxim
um daily value
Avg daily value
Absent
Present Sam
ples Sam
ple (e M
ethod L
evel (ML
) of grab)
Used
Test M
ethod concentration
mass
concentration m
ass(1 m
inshy
imum
) (m
ethod ) (ug1)
(ug1) (kgday)
(ug1) (kgday)
43 Copper
GR
A
200 (5
44 Lead G
RA
200
0001
45 Mercury
GR
A
7470A
(020
46 Nickel
GR
AB
200
(5
GR
AB
200
( 1547 Selenium
48 Silver G
RA
B
200 (0
49 Zinc
GR
A
200 18
0025
50 Iron G
RA
B
200 400
25
Other (describe)
c For discharges where m
etals are believed present please fill out the following
If yes which m
etals A
rsenic and Iron Step
I Do any of the m
etals in the influent have a reasonable potential to exceed the
etIluent limits in A
ppendix II (i the limits set at zero to five dilutions) Y
rg N D
Step 2 For any m
etals which have reasonable potential to exceed the A
ppendix III limits
Look up the lim
it calculated at the corresponding dilution factor in
calculate the dilution factor (DF) using the form
ula in Part I A 3 c) (step 2) of the N
O
Appendix IV
Do any of the m
etals in the influent have the potential to instructions or as determ
ined by the State prior to the submission of this N
OI
exceed the corresponding effuent lim
its in Appendix IV
(i is the
What is the dilution factor for applicable m
etals in1uent concentration above the lim
it set at the calculated dilution M
etals A
rsenic and Iron factor)
yrgND
If Y
es list which m
etals A
rsenic and Iron
DF
Rem
ediation General Pem
lit - Notice of Intent
4 Treatm
ent system inform
ation Please describe the treatment system
using separate sheets as necessary including
a) A description of the treatm
ent system including a schem
atic of the proposed or existing treatment system
S
ee Figures 4 and 5
Frac tank Air stripper
Oilw
ater separator Equalization tanks
Bag filter rg
GA
C filter rg
b) Identity each applicable
treatment unit (check alJ
that apply)
Chlorination
Dechlorination
Other (please describe)
c) Proposed average and maxim
um flow
rates (gallons per minute) for the discharge and the design flow
rate(s) (gallons per minute) ofthe treatm
ent system
Average flow
rate of discharge 15 G
PM
Maxim
um flow
rate oftreatment system
0 G
PM
Design flow
rate of treatment system
0 G
PM
d) A description of chem
ical additives being used or planned to be used (attach MSD
S sheets) Not A
pplicable
5 Receiving surface water(s) Please provide information about the receiving water (s) using separate sheets as necessary including
Identity the discharge pathway
I Direct
I Within facility
I Stonn drain rg I R
iverbrook I W
etlands _ I Other (describe)
Provide a narrative description ofthe discharge pathway including the nam
e(s) of the receiving waters
Discharge to catchbasin and stonnw
ater drainage system in E
ast Broadw
ay which discharges to M
ahoney Brook (S
ee Figure 4)
c) Attach a detailed m
ap(s) indicating the site location and location of the outfall to the receiving water
1 For multiple discharges num
ber the discharges sequentialJy 2 For indirect dischargers indicate the location of the discharge to the indirect conveyance and the discharge to surface w
ater T
he map should also include the location and distance to the nearest sanitary sew
er as well as the locus of nearby sensitive receptors (based on U
SGS topographical
mapping) such as surface w
aters drinking water supplies and w
etland areas d) Provide the state w
ater quality classification of the receiving water
e) Provide the reported or calculated seven day- ten year low flow
(7QlO
) of the receiving water Jcfs
Please attach any calculation sheets used to support stream flow
and dilution calculations See A
ttachment B
f) Is the receiving water a listed 303(d) w
ater quality impaired or lim
ited water Y
es 0 No rg
If yes for which polJutant(s) N
A
Is there a TM
DL
Yes 0
No rg If yes for w
hich pollutant(s) NA
Rem
ediation General Perm
it - Notice of Intent
6 Results of C
onsultation with Federal Services Please p
rovide the following information according to requirements of Par
lBA
and A
ppendices II and VII
a) Are any listed threatened or endangered species or designated critical habitat in proxim
ity to the discharge Yes 0
No rg
Has any consultation w
ith the federal services been completed Y
es 0 No rg
or is consultation underway Y
es 0 No rg
What w
ere the results of the consultation with the U
S Fish and Wildlife Service andor N
ational Marine Fisheries Service (check one) N
ot applicable
a nojeopardy opinion
or written concurrenceD
on a finding that the discharges are not likely to adversely affect any endangered species or critical habitat
b) Are any historic properties listed or eligible for listing on the N
ational Register of H
istoric Places located on the facilty or site or in proximity to the discharge
Yes D
No
Have any state or tribal historic preservation offcer been consulted in this determ
ination (Massachusetts only) Y
es O N
o
7 SU
DD
lemental inform
ation
Please provide any supplemental information Attach any analytical data used to support the application A
ttach any celtification(s) required by the general permit
Attachm
ent A - Figures
Figure I - Site Locus M
ap
Figure 2 - MassD
EP Site Scoring M
ap
Figure 3 - Aerial M
ap
Figure 4 - Proposed Soil Excavation A
rea Map
Figure 5 - T
reatment S
ystem Line D
iagram
Attachm
ent B - D
ilution factor Calculations
Attachment C - L
aboratory Analytical R
eport Groundw
ater
Rem
ediation General Perm
it - Notice of 1ntenl
=-
including the following
8 Signature Requirements
The N
otice ofIntent must be signed by the operator in accordance w
ith the signatory requirements of 40 C
FR Section 122
certification
J certif under penalty of law that this docum
ent and all attachments w
ere prepared under my direction or supervision in accordance w
ith a system
designed to assure that qualifed personnel properly gather and evaluate the information subm
itted Based on m
y inquiry of the person or persons who
manage the system
or those persons directly responsible for gathering the information I certif that t
he information submitted
is to the best of m
y
knowledge and belief true accurate and com
plete J certif that I am aw
are that there are signifcant penalties for submitting false inform
ation including
the possibilty of fine and imprisonm
ent for knowing violations
FacilitySite Name
Form
er Speedw
ay Service S
tation 181 East B
roadwav G
ardner MA
01440
Operator signature
Title
Michael 1 D
ziura Sf Env E
ngineer
Date
4150- q
Rem
ediation General Perm
it - Notice of Intent
-
D- 0
0 0
il (J tu
Bw
o(0 -I
NJW
gQb
J(JZc o c
rou a -10
0 J 6shy
a 0
I-tDC
aJ Qj
E aJshy
ro ro ro
~~~ ~~~~- -- - _ - -_ - ~~~ ~~~~ ~~~ - - _- _- -- -- p __(
MA DEP - Bureau of Waste Site CleanupSITE NME Site S aP 5 MiFlII Former Speeway Station _-II181 Eat Broaday b b d IS I i I GARDNER MA 0144 v ri) i P f f 1 me- 1 5ylmI I L shy J --I 423315n 715835e SiteLocation y o oCop1odQcn Ofof W-_ l
1 1 I
r
r
iBARBER HILL
A c
Cf1 f o s
0
5
Roads Uned Acss Divd Mar Roed Conntor Street Track 1 EPA Sola Source Aquilar FEMA 100yaar iloodplain 0 c Puc Watar SLo GrunSelaceNon Corrty 0
Bounars lOwn Couny DE Region Tian Powerln Ine Aqedut ApprOld Zona2 tNPA Sue Wster Supp Zone A bStZ F--shy--rle
8os Mat Sub SUeor Porenrial Inermtent Man lvo8 Ste Dfm Hyro1apy Wmer FeatllePLio Suleee Wat S H-- L otlMds FrslSaltN-ES WeIMd Habat L
Potentia Prdutiv AqlJlers ModHig Yield Proteoted Opn Space ACC nIL c= Non-Potential Drng Water Sollce AIea ModumHi Yo1d ll DEP Pormrd SoidWes1 FsiIi6s cnifud Verne Pools f0
1I2 KIWUmR$ MtL
January 30 2004 SCALE 1 15000
-
LE
GE
ND
APX PROPER BONDA
- APPROXOiSPO SIT BOUNDA
-GR
OU
ND
WA
TE F1 D
IRE
cnON
SCA
LE
30 60 FE
(APR
OX
CORPORATE ENVIRONMENTAL
)i
AD
VISO
RS
INC
SC
AS SH
OW
D
R B
Y K
HA
EL
DA
TE
10407
JOB
NO
2920-96
AERIAL MAP
FO
RM
ER
SP
EE
DW
AY
ST
AT
ION
FlGURE -3
181 EA
BR
OA
AY
GA
NE
R fo
age 1 ot 1Streamflow Statistics Report
Streamstats Ungaged Site Report Date Wed Dec 31 2008 124908 Site Location Massachusetts NAD83 Latitude 425545 (42 3316) NAD83 Longitude -719758 (-71 58 32) NAD27 Latitude 425545 (423316) NAD27 Longitude - 9763 (-71 58 34) Drainage Area 502 mi2
IPeak Flow Basin Characteristics 1100 Statewide Low Flow (S02 mi2)
Regression Equation Valid Rang
I Min II Max1 Value III Parameter Drainage Area (square miles) 161 149
Mean Basin Slope from 250K DEM (percent) 032 24
Stratified Drift per Stream Length (square mile per mile) 129
Massachusetts Region (dimensionless)
Streamflow Statistics
gO-Percent Prediction Interval Prediction Error
MaximumStatistic Flow (ft s) (percent) Minimum
I D50 IIII 11 1811 II 24511 993
I D60 II 35511 2011 II 03611 35111 2411 II 041 I 201I D70 24111 2611 II 03811 151I D75 11 2811 II 0911 3761I D80 981I D85 1 I 3211 II o6311
1 I 3711 II 0441 1 2 2911 D90 11 4611 II 02411 15511 D95I D98 04511 6011 II 01511 11
I D99 03411 6511 II ol1ll 1021
5011 II 02611 11I M7D2Y 1111 3311 II odl 3 541
I AUGD50
IIIIIIIIIIIIIIIIIIIIII 0311 7111 II 0088411 0981I M7Dl0Y
1010
12312008httpstreamstatsagscrusgsgovgisimgReportsFlowStatsReport3494 - 2008123112498
Dilution Factor Calculation Former Speedway Service Station 181 East Broadway Gardner Ma
DF=(Od+Os)Od
DF = Dilution factor
Od = Max flow rate of discharge in cubic feet per second Os = receiving water flow in cubic feet per seconds 7010 flow rate Mahoney Brook 7010 = min flow for seven consecutive days with a recurrence interval of 10 years
7010 flow based on data obtained from USGS Steamflow Statistics Report Data attached
067
Semivolatile Organic Compounds by GCMS - Quality Control
Analyte( s)
Batch 8051216 - SW846 3510C
Blank 8051216BLK1)
Prepared amp Analyzed 16May-
Acenaphthene
Acenaphthylene
Aniline
Anthracene
AzobenzenelDi phenyld iazi ne
Benzidine
Benzo (a) anthracene
Benzo (a) pyrene
Benzo (b) fiuoranthene
Benzo (g i) perylene
Benzo (k) fiuoranthene
Benzoic acid
Benzyl alcohol
Bis(2-ch loroethoxy) methane
Bis(2-ch loroethyl)ether
Bis(2-ch loroi sopropyl)ether
Bis(2ethylhexyl) phthalate
Bromophenyl phenyl ether
Butyl benzyl phthalate
Carbazole
Ch loro-3-methyl phenol
Chloroaniline
Chloronaphthalene
Chlorophenol
Chlorophenyl phenyl ether
Chrysene
Dibenzo (a h) anthracene
Dibenzofuran
Dichlorobenzene
Dichlorobenzene
14- Dichlorobenzene
3 - Dichlorobenzidine
24-Dichlorophenol
Diethyl phthalate
Dimethyl phthalate
24- Dimethylphenol
Din-butyl phthalate
Dinitro-2-methylphenol
Dinitrophenol
Dinitrotoluene
Dinitrotoluene
Di-noctyl phthalate
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopehtadiene
Hexachloroethane
Indeno (1 cd) pyrene
Spike Source REC RPD
Result Flag Units RDL Level Result REC Limits RPD Limit
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gl
BRL gI
BRL gl
BRL gl
BRL gl
BRL gI
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gll
BRL gl
BRL gll
BRL gl
BRL gl
BRL gI
BRL gI
BRL gI
BRL gl
BRL gI
BRL gI
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gI
BRL gI
BRL gl
This laboratory report is IlOt valid without all authorized sigllature 011 the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page t4 of25
Volatie Organic Compounds - Quality Control
p (
Spike Source REC RPD
RDL Level Result REC Limits RPD Limit Analyte(s) Result Flag Units
Batch 8051244 - SW846 5030 Water MS
Matrix S ike Du 8051244-MSD1 Source SA78629shy
Prepared 16-May-08 Analyzed 17-May-BRL 106 251
Vinyl chloride 21 gl 20
101 70- 130 Surrogate 4-Bromofluorobenzene 50 gl 50
70- 13049 gl 50 111 70- 130
Surrogate Toluene-Surrogate 1 Dichloroethane- 55 gl 50
50 70- 130494 glSurrogate Dibromofluoromethane
Microextractable Organic Compounds - Quality Control
Spike Source REC RPD
Flag Units RDL Level Result REC Limits RPD Limit Analyte(s) Result
Batch 8051105 - SW846 3510C
Blank 8051105-BLK
Prepared amp Analyzed 15-May-
BRL gl 01001 Dibromoethane (ED B)
LCS 8051105-BS1
Prepared amp Analyzed 15-Mayshy50- 1500770 gl 0100 100
licate 8051105-DUP1 Source SA7B583shy
Prepared amp Analyzed 15-May-
BRL gl 0100 BRL
1 Dibromoethane (EDB)
1 Dibromoethane (EDB)
This laborntOlY report is not valid without an authorized signature 011 the cover page
Page 13 of2S Reportable Detection Limit BRL = Below Reporting Limit
Sam le Identification Client Pro ect Matrix Collection DateTime ReceivedMWshy
2920-96- Ground Water 13-May-081030 14-May-SA 78602shy
CAS No Analyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Volatile Organic Compounds
Volatile Or anic Com ounds b GCMS
Prepared by method SW846 5030 Water MS
123-91- Dioxane BRL 1-91 200 EPA 624 16-May-08 17-May-08 8051244
994-05-8 Ter-amyl methyl ether BRL 1-911 20
755- Tert-Butanoll butyl alcohol BRL 1-91 200
67-B4- Acetone BRL 1-91 400
71-43- Benzene BRL 1-91 20
75-27-4 Bromodichloromethane BRL 1-91 20
75-25- Bromoform BRL 1-91 20
74-83- Bromomethane BRL 1-91 40
78-93- Butanone (MEK) BRL 1-91 200
56-23- Carbon tetrachloride BRL 1-91 20
108-90- Chlorobenzene BRL 1-91 20
75-00- Chloroethane BRL 1-91 40
676- Chloroform BRL 1-91 20
74-87- Chloromethane BRL 1-91 40
124-48- Dibromochloromethane BRL 1-91 20
95-50- Dichlorobenzene BRL 1-911 20
541-73- Dichlorobenzene BRL 1-91 20
106-46- Dichlorobenzene BRL 1-91 20
75-34- 1- Dichloroethane BRL 1-91 20
107-06- Dichloroethane BRL 1-91 20
75-35-4 1- Dichloroethene BRL 1-91 20
156-59 cis- Dichloroethene BRL 1-91 20
156-60- trans- Dichloroethene BRL 1-91 20
78-87- 2- Dichloropropane BRL 1-91 20
10061-01-5 cis- Dichloropropene BRL 1-91 20
10061-02-B trans- Dichloropropene BRL 1-91 20
100-41-4 Ethylbenzene 411 1-911 20
591-78-B BRL 200Hexanone (MBK) 1-91
1634-04 -4 Methyl tert-butyl ether BRL 1-91 20
108-10- Methyl- pentanone (MIBK) BRL 1-91 200
75-09- Methylene chloride BRL 1-91 200
100-42- Styrene BRL 1-91 20
79-34- 1 Tetrachloroethane BRL 1-91 20
127- 18-4 T etrachloroethene BRL 1-91 20
108-88- Toluene BRL 1-91 20
71-55 1- Trichloroethane BRL 1-91 20
79-00- 2- Trichloroethane BRL 1-91 20
79-01-B Trichloroethene BRL 1-91 20
759-4 Trichlorofluoromethane (Freon 11) BRL 1-91 20
75-01-4 Vinyl chloride BRL 1-91 20
179601-23-1 m Xylene 390 1-91 40
95-47 Xylene 82 1-91 20
Surrogate recoveries 460-00- Bromofluorobenzene 70- 130
2037-26- Toluene- 100 70- 130
17060-07-0 1 Dichloroethane- 111 70- 130
1868-53- Dibromofluoromethane 70- 130
Microextractable Organic Compounds
106-93-4 1 Dibromoethane (EDB) BRL 1-91 0100 EPA 504 15-May- 15-May-08 8051105
Semivolatile Organic Compounds by GCMS
This laboratory report is not valid without all autllOrized signature 011 the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page 5 of 25
Sam le Identification Client Pro ect Matrix Collection DateTime Received
MWshy2920-96- Ground Water 13-May-081030 14-May-
SA 78602shy
CAS No Analyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Semivolatie Organic Compounds by GCMS
Semi volatile Or anic Com ounds b EPA 625
Prepared by method SW846 3510C 50 EPA 625 16-May- 19-May-08 805121683-32- Acenaphthene BRL IJgl
208-96-8 Acenaphthylene BRL IJgl 50
62-53- BRL IJgll 50Aniline
120- 12- Anthracene BRL 1J91 50
103-33- AzobenzenefDiphenyldiazine BRL IJgl 50
92-87 - Benzidine BRL IJgl 50
56-55- Benzo (a) anthracene BRL 1J91 50
50-32 - Benzo (a) pyrene IJglBRL 50
205-99- Benzo (b) fluoranthene BRL IJgl 50
191-24- Benzo (g i) perylene BRL IJgl 50
50207-08- Benzo (k) fluoranthene BRL IJgl
65-85 Benzoic acid BRL 1J91 50
100-51-6 Benzyl alcohol 1J91BRL 50
50111-91- Bis(2-chloroethoxy)methane BRL 1J91
111-4-4 Bis(2-chloroethyl)ether BRL IJgl 50
501 08-60- Bis(2-chloroisopropyl)ether BRL IJgl
117-81- Bis(2-ethylhexyl)phthalate BRL 1J91 50
101-55- Bromophenyl phenyl ether BRL IJgl 50
5085-68- Butyl benzyl phthalate BRL IJgl
5086-74- Carbazole BRL IJgl
5059-50- C hloro-3-methylphenol BRL IJgl
106-47- Chloroaniline BRL IJgl 50
91-58- Chloronaphthalene IJglBRL 50
5095-57 - Chlorophenol BRL 1J91
507005-72- Chlorophenyl phenyl ether BRL IJgl
216-01- Chrysene tJ91BRL 50
5053-70- Dibenzo (a h) anthracene BRL IJgl
50132-64- Dibenzofuran BRL IJgl
95-50- Dichlorobenzene IJglBRL 50
541-73- 13- Dichlorobenzene BRL IJgl 50
106-46- Dichlorobenzene 1J91BRL 50
5091-94- 3 - Dichlorobenzidine BRL IJgl
120-83- Dichlorophenol BRL IJgl 50
84-66- Diethyl phthalate BRL IJgl 50
131-11- Dimethyl phthalate BRL IJgll 50
105-67- Dimethylphenol BRL 1J91 50
5084-74- Di-n- butyl phthalate BRL 1J91
534-52 - Dinitro-2-methylphenol BRL IJgl 50
51-28- Dinitrophenol IJglBRL 50
50121-14- Dinitrotoluene BRL 1J91
606-20- Dinitrotoluene IJglBRL 50
50117-84-0 Di-n-octyl phthalate BRL IJgl
206-44-0 Fluoranthene 1J91BRL 50
BRL 50
50 86-73- Fluorene IJgi
118-74- Hexachlorobenzene BRL 1J91
87-68- Hexachlorobutadiene 1J91BRL 50
5077-47-4 Hexachlorocyclopentadiene BRL IJgl
67-72- Hexachloroethane IJglBRL 50
50193-39- Indeno (1 3-cd) pyrene BRL IJgl
5078-59- Isophorone BRL IJgl
Tfls laboratory report is not valid without all authorized signature 011 the coverpage
Page 6 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Sam le Identification Client Pro ect Matrix Collection DateTime ReceivedMWshy
2920-96- Ground Water I3-May-081030 14-May-SA 78602shy
CAS No Analyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Semivolatile Organic Compounds by GCMS
Semi volatile Or anic Com ounds b EPA 625
Prepared by method SW846 3510C
91-57 -6 Methylnaphthalene 367 1-91 50 EPA 625 16-May- 19-May-08 8051216
95-48- Methylphenol BRL 1-91 50
108-39-4 3 amp 4-Methylphenol BRL I-gl 100 106-44shy91-20- Naphthalene 247 1-91 50
88-74-4 Nitroaniline BRL 1-91 50
99-09- Nitroaniline BRL 1-91 50
100-01-6 Nitroaniline BRL 1-91 50
98-95- Nitrobenzene BRL 1-91 50
88-75- Nitrophenol BRL 1-91 50
100-02- Nitrophenol BRL 1-91 50
62-75- Nitrosodimethylamine BRL 1-91 50
621-64- N- Nitrosodi-n-propylamine BRL 1-91 50
86-30-6 Nitrosodiphenylamine BRL 1-91 50
87 -86- Pentachlorophenol BRL 1-91 50
85-0- Phenanthrene BRL 1-91 50
108-95- Phenol BRL 1-91 50
129-00-0 Pyrene BRL 1-91 50
110-86- Pyridine BRL 1-91 50
120-82- 4- Trichlorobenzene BRL 1-91 50
95-95- 5- Trichlorophenol BRL 1-91 50
88-06- 6- T richlorophenol BRL 1-91 50
Surrogate recoveries
321-60- Fluorobipheny 30- 130
367- 12- Fuorophenol 15- 110
4165-60- Nitrobenzene- 30- 130
4165-62- Pheno- 15- 110
1718-51- Terpheny-d4 30- 130
118- 79- 6- Tribromophenol 15- 110
Semivolatile Organic Compounds by GC
Pol chlorinated Bi hen ls b EPA 608
Prepared by method SW846 3510C
12674- 11-2 Aroclor- 1016 BRL 1-91 0650 EPA 608 15- May- 16-May-08 8051106
11104-28-2 Aroclor-1221 BRL IJgl 0650
11141-16-5 Aroclor- 1232 BRL 1-91 0650
53469-21-9 Aroclor- 1242 BRL 1-91 0650
12672-29-6 Aroclor- 1248 BRL 1-91 0650
11097-69-1 Aroclor- 1254 BRL 1-91 0650
11096-82-5 Aroclor -1260 BRL 1-91 0650
37324-23-5 Aroclor-1262 BRL 1-91 0650
11100-14-4 Aroclor-1268 BRL IJgl 0650
Surrogate recoveries
2051-24- Decachlorobipheny (Sr) 105 30- 150
10386-84-2 4 DB-Octafluorobiphenyl (Sr) 30- 150
Extractable Petroleum Hydrocarbons
mgl EPA 1664 Rev A 15-May- 19-May-08 8051102Non-polar material (SGT- HEM)
Soluble Metals by EPA 2006000 Series Metbods
Field Filtered NA EPA 200 73005A 15- May- 15-May-08 8051192Filtration
Soluble Metals by EPA 200 Series Methods
7440-22-4 Silver BRL mgl 0002 EPA 200 21-May- 27- May-08 8051249
This laboratory report is IlOt mlid without (II authorized signature on the cover page
Reportble Detection Limit BRL = Below Reporting Limit Page 7 of 25
Sam le Identification MW-
Client Pro ect 2920-96shy
Matrix Ground Water
Collection DateTime 13-May-08 1030
Received 14-May-
SA 78602shy
CAS No A nalyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Soluble Metals by EPA 200 Series Methods
7440-38shy Arsenic 0468 mg1 0040 EPA 200 21-Mayshy 21-May-08 80511 50
7440-43shy Cadmium BRL mg1 0002 EPA 200 21-May-088051249
7440-47shy Chromium BRL mg1 0050 EPA 200 21-May-088051150
7440-50-8 Copper BRL mg1 0050
7439-89-6 Iron 184 mg1 0150
7439-97-6 Mercury BRL mg1 00020 EPA 245 17470A 21-May-088051152
7440-02-0 Nickel BRL mg1 0050 EPA 200 21-May-088051150
7439-92shy Lead 0011 mg1 0002 EPA 200 21-May-088051249
7440-36-0 Antimony 0003 mg1 0002
7782-49shy Selenium BRL mg1 0150 EPA 200 21-May-08 8051150
7440-66-6 Zinc 0186 mgl 0050
General Chemistry Parameters
Filtration Completed NA Varies 14-Mayshy 14-May-08 8051095
18540-29-9 Hexavalent Chromium (soluble) BRL HT2 mg1 125 SM3500CrDI796A 14-Mayshy 14-May-08 8051094 R01 2013 2016
57-12shy Cyanide (total) BRL mg1 0100 EPA 3354 19-Mayshy 19-May-088051374
7782-50shy Total Residual Chlorine BRL CIHT mg1 500 Hach 8167 14-Mayshy 14-May-08 8051049 R01 1900 2001
Total Suspended Solids 580 mg1 25 SM2540D 16-Mayshy 16-May-08 8051275
This lahomtOlY report is not valid without an authorized signature on the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page 8 of 25
Volatie Organic Compounds - Quality Control
Analyte( s)
Batch 8051244 - SW846 5030 Water MS
Blank 8051244-BLK1
Prepared 16-May-08 Analyzed 17-May-
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromochloromethane
1 Dichlorobenzene
1 Dichlorobenzene
1 Dichlorobenzene
1-Dichloroethane
1 Dichloroethane
1 1-Dichloroethene
cis- Dichloroethene
trans- 1 Dichloroethene
1 Dichloropropane
cis- 1 Dichloropropene
trans- 1 Dichloropropene
Ethylbenzene
Hexanone (MBK)
Methyl tert-butyl ether
Methyl- pentanone (MIBK)
Methylene chloride
Styrene
2- Tetrachloroethane
Tetrachloroethene
Toluene
1- Trichloroethane
2- Trichloroethane
Trichloroethene
Trichlorofluoromethane (Freon 11)
Vinyl chloride
p-Xylene
Xylene
Surrogate 4-Bromofluorobenzene Surrogate Toluene-
Surrogate 1 Dichloroethane-Surrogate Dibromofluoromethane
LCS B051244-BS1
Prepared 16-May-08 Analyzed 17 -May-
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Spike Source REC RPD
Result Flag Units RDL Level Result REC Limits RPD Limit
BRL gl 20
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl 10
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gll
BRL gi
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl 10
BRL gll
BRL gll 10
BRL gl 10
BRL gll
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
41 gl 50 70- 130 49 gl 50 70- 130 59 gl 50 119 70- 130 52 gl 50 105 70- 130
QC2 jgl 20 70- 130
18 jgl 20 70- 130
192 jgl 20 35- 155
18 jgl 20 45- 169
19 jgl 20 242
This laboratOlY repol1 is lot valid without 011 authorized sigllature 011 the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page 9 of 25
Volatie Organic Compounds - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051244 - SW846 5030 Water MS
LC5 8051244B51
Prepared 16-May-08 Analyzed 17-May-
Butanone (MEK) 10 QC2 gl 20 70- 130
Carbon tetrachloride 204 gl 20 102 70- 140
Chlorobenzene 18 gl 20 70- 130
Chloroethane 164 gl 20 14-230
Chloroform 18 gll 20 51- 138
Chloromethane 21 gl 20 106 273
Dibromochloromethane 18 gl 20 53- 149
1 Dichlorobenzene 20 gl 20 104 18- 190
1 Dichlorobenzene 19 gl 20 59- 156
1 A-Dichlorobenzene 18 gl 20 18- 190
1- Dichloroethane 19 gl 20 59- 155
1 Dichloroethane 19 gl 20 49- 155
1-Dichloroethene 16 gl 20 70- 130
cis- 1 Dichloroethene 17 gl 20 70- 130
trans- 1 Dichloroethene 16 gll 20 54- 156
1 Dichloropropane 18 gl 20 210
cis- Dichloropropene 17 gl 20 227
trans- 1 Dichloropropene 17 gl 20 17- 183
Ethylbenzene 19 gl 20 37- 162
Hexanone (MBK) 124 QC2 gl 20 70- 130
Methyl tert-butyl ether 19 gl 20 70- 130
Methylshy pentanone (MIBK) 17 gl 20 70- 130
Methylene chloride 16 gl 20 221
Styrene 17 gl 20 70- 130
1 Tetrachloroethane 194 gl 20 46- 157
Tetrachloroethene 15 gl 20 64- 148
Toluene 18 gl 20 70- 130
1- Trichloroethane 20 gl 20 100 52- 162
2- Trichloroethane 18 gl 20 52- 150
Trichloroethene 17 gl 20 71- 157
Trichlorofluoromethane (Freon 11) 19 gl 20 17- 181
Vinyl chloride 21 gl 20 106 251
p-Xylene 39 gl 40 70- 130
Xylene 20 gl 20 102 70- 130
Surrogate 4-Bromofluorobenzene Surrogate Toluene-
Surrogate 1 Dichloroethane-Surrogate Dibromofluoromethane
52 49 56
49
gl
gl
gl
gl
50 50 50
50
105
112 100
70- 130 70- 130 70- 130 70- 130
LC5 DUD (8051244-B5D1
Prepared 16-May-08 Analyzed 17-May-
Acetone QC2 gl 20 70- 130
Benzene 18 gl 20 70- 130
Bromodichloromethane 18 gl 200 35- 155
Bromoform 17 gl 20 45- 169
Bromomethane 18 gl 20 242
Butanone (MEK) 11 QC2 1-91 20 70- 130
Carbon tetrachloride 20 gl 20 100 70- 140
Chlorobenzene 17 gl 20 70- 130
Chloroethane 15 1-91 20 14-230
Chloroform 18 1-91 20 51- 138
This laboratory report is aot valid without a1 authorized sig1ature 01 the cover page
Reportble Detection Limit BRL = Below Reporting Limit Page 10 of25
Volatie Organic Compounds - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051244 - SW846 5030 Water MS
LCS Dup 18051244-BSD1
Prepared 16-May-08 Analyzed 17-May-
Chloromethane 18 1-91 20 273
Dibromochloromethane 174 1-91 20 53- 149
Dichlorobenzene 20 1-91 20 100 18- 190
Dichlorobenzene 18 1-91 20 59- 156
Dichlorobenzene 18 1-91 20 18- 190
Dichloroethane 18 1-91 20 59- 155
Dichloroethane 19 1-91 20 49- 155
Dichloroethene 16 1-91 20 70- 130
cis- Dichloroethene 16 1-91 20 70- 130
trans- Dichloroethene 15 1-91 20 54- 156
Dichloropropane 17 1-91 20 210
cis- Dichloropropene 164 IJgl 20 227
trans- 1 Dichloropropene 164 I-gl 20 17- 183
Etlwlbenzene 18 IJgl 20 37- 162
Hexanone (MBK) 124 QC2 IJgl 20 70- 130
Methyl tert-butyl ether 184 1J91 20 70- 130
Methyl- pentanone (MIBK) 17 IJgl 20 70- 130
Methylene chloride 16 IJgl 20 221
Styrene 16 IJgl 20 70- 130
2- Tetrachloroethane 19 IJgl 20 46- 157
Tetrachloroethene 15 IJgl 20 64- 148
Toluene 17 IJgl 20 70- 130
1- Trichloroethane 19 1-91 20 52- 162
2- Trichloroethane 16 IJgl 20 52- 150
Trichloroethene 15 IJgl 20 71- 157
Trichlorofluoromethane (Freon 11) 17 IJgl 20 17- 181
Vinyl chloride 19 IJglI 20 251
p-Xylene 37 1J91 40 70- 130
Xylene 20 IJgl 20 100 70- 130
Surrogate 4-Bromofluorobenzene 51 IJgl 50 104 70- 130
Surrogate Toluene- 4B gl 50 70- 130
Surrogate 1 0ichloroethane- 53 IJgl 50 106 70- 130 Surrogate Oibromofluoromethane 50 1J9i 50 102 70- 130
Matrix S ike B051244-MS1 Source SA7B629shy
Prepared 16-May-08 Analyzed 17-May-
Benzene 18 20 BRL 70- 130IJgl
Bromodichloromethane 19 IJgl 20 BRL 35- 155
Bromoform 18 IJgl 20 BRL 45- 169
Bromomethane 16 IJgl 20 BRL 242
Carbon tetrachloride 21 IJgl 20 BRL 106 70- 140
Chlorobenzene 18 IJgl 20 BRL 70- 130
Chloroethane 16 IJgl 20 BRL 14-230
Chloroform 18 IJgl 20 BRL 51- 138
Chloromethane 19 IJgl 20 BRL 273
Dibromochloromethane 17 IJgl 20 BRL 53- 149
1 Dichlorobenzene 22 IJgl 20 BRL 112 18- 190
1 Dichlorobenzene 22 IJgl 20 BRL 110 59-156
1 Dichlorobenzene 21 IJgl 20 BRL 109 18- 190
1- Dichloroethane 19 IJgl 20 BRL 59- 155
1 Dichloroethane 18 IJgl 20 BRL 49- 155
This laboratory report is 110t mUd without an authorized signature on the covel page
Reportble Detection Limit BRL = Below Reporting Limit Page It of25
Volatile Organic Compounds - Quality Control
p
Spike Source REC RPD
Result REC imits RPD LimitAnalyte(s) Result Flag Units RDL Level
Batch 8051244 - SW846 5030 Water MS
Matrix ike S051244-MS1 Source SA7B629shy
Prepared 16-May-08 Analyzed 17-Mayshy
17 20 BRL 70- 130 1- Dichloroethene IJgl
16 20 BRL 54- 156trans- 1 Dichloroethene IJgl
21020 BRL1 Dichloropropane 17 1J91
cis- 1 Dichloropropene 17 IJgl 20 BRL 227
17- 183trans- 1 Dichloropropene 184 1J91 20 BRL
20 20 BRL 103 37- 162Ethylbenzene IJgl
15 20 BRL 221Methylene chloride IJgl
20 BRL 46- 1572- Tetrachloroethane 19 1J91
20 BRL 64- 148Tetrachloroethene 18 1J91
BRL 70- 130Toluene 18 1J91 20
105 52-1621- Trichloroethane 211 IJgl 20 BRL
18 20 BRL 52- 1502- Trichloroethane IJgl
17 20 BRL 71- 157Trichloroethene 1J91
20 BRL 17- 181Trichloroluoromethane (Freon 11) 194 IJgl
20 BRL 103 251Vinyl chloride 20 IJgl
102 70- 130Surrogate 4-Bromofluorobenzene 50 IJgl 50 50 70- 130Surrogate Toluene- 49 1J91
56 50 112 70- 130Surrogate 1 Dichloroethane- IJgl
50 100 70- 130Surrogate Dibromofluoromethane 50 IJgl
Matrix S ike Du S051244-MSD1 Source SA7S629shy
Prepared 16-May-08 Analyzed 17-Mayshy
18 20 BRL 70- 130Benzene IJgl
18 20 BRL 35- 155Bromodichloromethane IJgl
17 20 BRL 45- 169Bromoform IJgl
20 BRL 242Bromomethane 17 IJgl
20 BRL 103 70- 140Carbon tetrachloride 20 IJgl
18 20 BRL 70- 130Chlorobenzene 1J91
14-230Chloroethane 16 IJgl 20 BRL
20 51- 138Chloroform 184 IJgl BRL
Chloromethane 19 1J91 20 BRL 273
18 20 BRL 53- 149Dibromochloromethane 1J91
20 BRL 117 18- 190Dichlorobenzene 234 IJgl
20 BRL 112 59- 156Dichlorobenzene 22 IJgl
BRL 108 18- 190Dichlorobenzene 21 1J91 20
20 59- 1551 Dichloroethane 19 IJgl BRL
18 20 BRL 49- 155Dichloroethane IJgl
16 20 BRL 70- 130Dichloroethene IJgl
20 BRL 54- 156trans- Dichloroethene 154 1J91
20 BRL 210Dichloropropane 17 IJgl
0420 BRL 227cis- Dichloropropene 17 IJgl
17- 183trans- Dichloropropene 17 1J91 20 BRL
BRL 37- 162Ethylbenzene 20 1J91 20 102
Methylene chloride 15 IJgl 20 BRL 221
20 BRL 46- 1572- Tetrachloroethane 192 IJgl
20 BRL 64- 148 04Tetrachloroethene 18 IJgl
BRL 70- 130Toluene 184 1J91 20
52- 1621- Trichloroethane 20 IJgl 20 BRL 104
17 20 BRL 52- 1502- Trichloroethane IJgl
17 20 BRL 71- 157Trichloroethene IJgl
20 BRL 17-181Trichlorofluoromethane (Freon 11) 19 IJgl
This laboratory report is IIOt valid without all authorized sigllllture 011 the cover page
Page 12 of25 Reportble Detection Limit BRL = Below Reporting Limit
Semivolatile Organic Compounds by GCMS - Quality Control
Analyte(s)
Batch 8051216 - SW846 3510C
Blank 8051216-BLK1
Prepared amp Analyzed 16-May-
Isophorone
Methylnaphthalene
Methylphenol
3 amp 4-Methylphenol
Naphthalene
Nitroaniline
Nitroaniline
Nitroaniline
Nitrobenzene
Nitrophenol
Nitrophenol
Nitrosodimethylamine
N- N itrosodi-n-pro pyla mine
N itrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Pyridine
1 24-Trichlorobenzene
24 5- Trichlorophenol
246- Trichlorophenol
Surrogate 2-Fuorobipheny Surrogate 2-Fuoropheno Surrogate Nitrobenzene-Surrogate PhenoshySurrogate Terpheny-d4 Surrogate 6- Tribromopheno
LCS B051216-BS1
Prepared amp Analyzed 16-May-
Acenaphthene
Acenaphthylene
Aniline
Anthracene
AzobenzenelDi phenyld lazine
Benzidine
Benzo (a) anthracene
Benzo (a) pyrene
Benzo (b) fluoranthene
Benzo (g i) perylene
Benzo (k) fluoranthene
Benzoic acid
Benzyl alcohol
B is(2-chloroethoxy)methane
B i s (2-ch loroethyl)eth e r
Bis(2-ch loroisopropyl) ether
B is(2-ethy Ih exyl) phtha late
Bromophenyl phenyl ether
Butyl benzyl phthalate
Carbazole
Spike Source REC RPD
Result Flag Units RDL Level Result REC Limits RPD Limit
BRL gl
BRL gl
BRL gl
BRL gl 10
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gll
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
370 gl 50 30- 130 40 gl 50 15- 110 39 gl 50 30- 130 43 gl 50 15- 110 36 gl 50 30- 130 40 gl 50 15- 110
41 gl 50 40- 140
43 gI 50 40- 140
41 gl 50 40- 140
38 gl 50 40- 140
45 gl 50 40- 140
49 gl 50 153
41 gl 50 40- 140
43 gl 50 40- 140
41 gl 50 40- 140
41 gll 50 40- 140
45 gl 50 40- 140
32 gl 50 12- 149
41 gl 50 40- 140
39 gl 50 40- 140
384 gl 50 40- 140
47 gl 50 40- 140
47 gl 50 40- 140
40 gl 50 40- 140
47 gI 50 40- 140
56 gI 50 112 200
This laboratory report is lIot valid witllOut a1l authorized sigllature 011 the coverpage
Reportble Detection Limit BRL = Below Reporting Limit Page 15 of25
Semivolatile Organic Compounds by GCMS - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051216 - SW846 3510C
LCS 8051216-BS1
Prepared amp Analyzed 16-Mayshy
50 30- 1304 -C hloro-3-methylphenol 42 IJgl
40- 140Chloroaniline 39 IJgl 50
Chloronaphthalene 37 IJgl 50 40- 140
Chlorophenol 37 IJgl 50 30- 130
50 40- 140
40- 140
Chlorophenyl phenyl ether 45 IJgl
Chrysene 43 IJgl 50
Dibenzo (a h) anthracene 43 IJgl 50 40- 140
Dibenzofuran IJgl38 50 40- 140
50 40- 1401 Dichlorobenzene 35 IJgl
40- 1401 Dichlorobenzene 264 IJgl 50
40- 1401 Dichlorobenzene 434 IJgl 50
58 50 116 40- 1403 - Dichlorobenzidine IJgl
50 30- 130
40- 140 24-Dichlorophenol 38 IJgl
Diethyl phthalate 484 IJgl 50
50 40- 140Dimethyl phthalate 464 IJgl
Dlmethylphenol 39 IJgl 50 30- 130
DI-n-butyl phthalate 44 IJgll 50 40- 140
30- 130 6-Di nitro- 2-methylphenol 38 1J91 50
30- 130Dinltrophenol 36 1J91 50
42 50 40- 14024-Dlnitrotoluene 1J91
Dlnitrotoluene 1J9141 50 40- 140
Di-n-octyl phthalate 52 IJgl 50 104 40- 140
40- 140Fluoranthene 40 IJgl 50
Fluorene 41 IJgl 50 40- 140
39 50 40- 140Hexachlorobenzene IJgl
50 40- 140Hexachlorobutadiene 40 IJgl
40- 140Hexach lorocyclopentad iene 294 IJgl 50
40 50 40- 140Hexachloroethane IJgl
42 50 40-140Indeno (1 3-cd) pyrene IJgl
50 40- 140Isophorone 40 IJgl
40- 140Methylnaphthalene 394 IJgl 50
40- 140Methylphenol 39 IJgl 50
40 10 50 40- 1403 amp 4-Methylphenol IJgl
37 50 40-140Naphthalene IJgl
50 40-140Nitroaniline 39 IJgl
Nitroaniline 51 IJgl 50 102 40- 140
48 50 40- 140Nltroaniline 1J91
50 40- 140Nitrobenzene 40 IJgl
30- 130Nitrophenol 36 IJgl 50
40 IJgl 50 30- 130Nitrophenol 40- 140Nitrosodimethylamine 32 1J91 50
50 40-140N- N itrosodi-n-propyla mine 46 IJgl
40- 140N itrosodi phenyla ml ne 44 IJgl 50
41 IJgl 50 30- 130Pentachlorophenol 40- 140Phenanthrene 38 IJgl 50
50 30- 130Phenol 38 IJgl
40- 140Pyrene 424 1J91 50
40- 140Pyridine 294 1J91 50
40- 14024- Trichlorobenzene 364 IJgl 50
This laboratory report is not mlid without an authorized signature 011 the cover page
Page 16 of25 Reportble Detection Limit BRL = Below Reporting Limit
Semivolatie Organic Compounds by GCMS - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
BMch 8051216 - SW846 3510C
LC5 8051216-851
Prepared amp Analyzed 16-Mayshy
24 5- Trichlorophenol 404 gl 50 30- 130
246- Trichlorophenol 42 gl 50 30- 130
Surrogate 2-Fluorobiphenyl 29 gl 50 30- 130
Surrogate 2-Fluorophenot 27 gl 50 15- 110
Surrogate Nitrobenzene- 30 gl 50 30- 130
Surrogate Phenol- 29 gl 50 15- 110
Surrogate Terpheny-d4 30 gl 50 30- 130
Surrogate 6- Tribromopheno 324 gl 50 15- 110
This laboratory report is lIot valid without all authorized sigllature 011 tlle cover page
Reportble Detection Limit BRL = Below Reporting Limit Page 17 of25
Semivolatie Organic Compounds by GC - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051106 - SW846 3510C
Blank S051106-BLK1
Prepared amp Analyzed 15-Mayshy
Aroclor- 1016 BRL gI 0200
Aroclor- 1016 (2C) BRL gI 0200
Aroclor- 1221 BRL gI 0200
Aroclor- 1221 (2C) BRL gI 0200
Aroclor- 1232 BRL gI 0200
Aroclor- 1232 (2Cj BRL gI 0200
Aroclor- 1242 BRL gI 0200
Aroclor-1242 (2C) BRL gI 0200
Aroclor- 1248 BRL gI 0200
Aroclor- 1248 (2C) BRL gI 0200
Aroclor- 1254 BRL gI 0200
Aroclor- 1254(2Cj BRL gI 0200
Aroclor- 1260 BRL gI 0200
Aroclor- 1260 (2C) BRL gI 0200
Aroclor- 1262 BRL gI 0200
Aroclor- 1262 (2C) BRL gI 0200
Aroclor-1268 BRL gI 0200
Aroclor- 1268 (2C) BRL gI 0200
Surrogate Decachlorobiphenyl (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0231 0224 0194 0191
gI
gI
gI
gI
0200 0200 0200 0200
116 112
30- 150 30- 150 30- 150 30- 150
LC5 8051106-B51
Prepared 15-May-08 Analyzed 16-May-08
Aroclor- 1016 265 gI 0200 250 106 50- 114
Aroclor- 1 016 (2C) 240 gI 0200 250 50- 114
Aroclor- 1260 0269 gI 0200 250 107 40- 127
Aroclor-1260 (2Cj 270 gI 0200 250 108 40- 127
Surrogate Decachlorobiphenyl (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0225 0224 0188 0183
gI
gI
gI
gI
0200 0200 0200 0200
113 112
30- 150 30- 150 30- 150 30- 150
LC5 DUD rS051106-B5D1
Prepared 15-May-08 Analyzed 16-Mayshy
Aroclor- 1016 262 gl 0200 250 105 50- 114
Aroclor-1 016 (2Cj 241 gI 0200 250 50- 114
Aroclor- 1260 277 gI 0200 250 111 40- 127
Aroclor- 1260(2Cj 0260 gI 0200 250 104 40- 127
Surrogate Decachlorobipheny (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0238 0218 0189 0181
gI
gI
gI
gI
0200 0200 0200 0200
119 109
30- 150 30- 150 30- 150 30- 150
This laboratory report is lot valid without (II authorized sigllature 01 the cover page
Page 18 of25 Reportable Detection Limit BRL = Below Reporting Limit
Extractable Petroleum Hydrocarbons - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051102 - SW846 3510C
Blank 8051102-BLK1
Prepared 15-May-08 Analyzed 19-Mayshy
Non-polar material (SGT- HEM) BRL m91
LC8 8051102-B81
Prepared 15-May-08 Analyzed 19-Mayshy
Non-polar material (SGT- HEM) 184 m91 21 81 904
This laboratory report is not valid without an authorized signature 011 the cover page
Page 19 of25 Reportable Detection Limit BRL = Below Reporting Limit
Soluble Metals by EPA 200 Series Methods - Quality Control
Analyte(s) Result Flag Units RDL
Spike
Level
Source
Result REC
REC
Limits RPD
RPD
Limit
Batch 8051150 - EPA 200 Series
Blank 8051150-BLK1
Prepared amp Analyzed 21-May-
Iron
Zinc
Selenium
Nickel
Chromium
Copper
Arsenic
BRL
BRL
BRL
BRL
BRL
BRL
BRL
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0150
0050
0150
0050
0050
0050
0040
LCS 8051150-BS1
Prepared amp Analyzed 21-May-
Selenium
Zinc
Iron
Nickel
Chromium
Arsenic
Copper
123
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0150
0050
0150
0050
0050
0040
0050
103
105
101
100
85- 115
85- 115
85- 115
85- 115
85- 115
85-115
85- 115
licate B051150-DUP1 Source SA7B602shy
Prepared amp Analyzed 21-May-
Iron
Zinc
Selenium
Nickel
Copper
Chromium
Arsenic
17
0162
BRL
0015
0017
BRL
0450
QR8
mgl
mgl
mgl
mgl
mgl
mgl
mgi
0150
0050
0150
0050
0050
0050
0040
184
0186
BRL
0014
0023
BRL
0468
Matrix S ike 8051150-MS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Iron
Selenium
Nickel
Zinc
Copper
Chromium
Arsenic
19 QM2 mgl
mgll
mgl
mgl
mgl
mgl
mgl
0150
0150
0050
0050
0050
0050
0040
125
184
BRL
0014
0186
0023
BRL
0468
104
105
102
70- 130
70- 130
70-130
70- 130
70- 130
70-130
70- 130
Post S ike 8051150-PS1 Source SA78602shy
Prepared amp Analyzed 21-May-
Zinc
Iron
Selenium
Nickel
Copper
Arsenic
Chromium
18 QM2
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0050
0150
0150
0050
0050
0040
0050
0186
184
BRL
0014
0023
0468
BRL
104
104
101
85- 115
85- 115
85- 115
85-115
85-115
85- 115
85-115
Batch 8051152 - EPA200SW7000 Series
Blank B051152-BLK1
Prepared amp Analyzed 21-May-
Mercury BRL mgl 00020
This laboratory report is IIOt valid witllOut all authorized sigllature 011 the coverpage
Page 20 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Soluble Metals by EPA 200 Series Methods - Quality Control
Analyte(s) Result Flag Units RDL
Spike
Level
Source
Result REC
REC
Limits RPD
RPD
Limit
Batch 8051152 - EPA200SW7000 Series
LCS B051152-BS1
Prepared amp Analyzed 21-May-
Mercury 00576 m91 00020 00500 115 85- 115
licate B051152-DUP1 Source SA78602-01
Prepared amp Analyzed 21-May-
Mercury BRL m91 00020 BRL
Matrix S ike 8051152-MS1 Source SA78602shy
Prepared amp Analyzed 21-May-
Mercury 00632 OM m91 00020 00500 BRL 126 75- 125
Post S ike 8051152-PS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Mercury 00624 OC1 m91 00020 00500 BRL 125 85- 115
Batch 8051249 - 2008No digestion
Blank 8051249-BLK1
Prepared amp Analyzed 21-May-
Lead
Antimony
Cadmium
Silver
BRL
BRL
BRL
BRL
m91
m91
m91
m91
0002
0002
0002
0002
LCS B051249-BS1
Prepared amp Analyzed 21-May-
Antimony
Lead
Silver
Cadmium
143
145 OC2
m91
m91
m91
m91
0050
0050
0050
0040
103
115
107
116
85- 115
85- 115
85- 115
85- 115
licate 8051249-DUP1 Source SA7B602shy
Prepared amp Analyzed 21- May-
Lead
Antimony
Cadmium
Silver
0009
0002
00005
00002
ORB
m91
m91
m91
m91
0002
0002
0002
0002
0011
0003
00005
00003
Matrix S ike 8051249-MS1 Source SA78602shy
Prepared amp Analyzed 21- May-
Lead
Antimony
Cadmium
Silver
142
m91
m91
m91
m91
0050
0050
0040
0050
0011
0003
00005
00003
111
101
114
102
70- 130
70-130
70c130
70- 130
Post S ike 8051249-PS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Antimony
Cadmium
Silver
38
OC2
m91
m91
m91
0050
0040
0050
125
0003
00005
00003
110
121
109
85- 115
85- 115
85- 115
This laboratory report is flOt valid IVithout all authorized signature 011 the cOIer page
Reportable Detection Limit BRL Below Reporting Limit Page 21 of 25
General Chemistry Parameters - Quality Control
Spike Source REC RPD
Analyte( s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051049 - General Preparation
Blank S051 049-BLK1
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
Blank S051049-BLK2
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
Blank S051 049-BLK3
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
LCS S051049-BS1
Prepared amp Analyzed 14-May-
Total Residual Chlorine 046 mgl 020 0500 90- 110
LCS S051049-BS2
Prepared amp Analyzed 14-May-
Total Residual Chlorine 047 mgl 020 0500 90- 110
LCS S051049-BS3
Prepared amp Analyzed 14-May-
Total Residual Chlorine 054 mgl 020 0500 108 90-110
licate B051049-DUP1 Source SA7S544shy
Prepared amp Analyzed 14-May-
Total Residual Chlorine 012 mgl 020 010
licate S051049-DUP2 Source SA7S602-01
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020 BRL
Matrix S ike 8051049-MS1 Source SA78544-01
Prepared amp Analyzed 14-May-
Total Residual Chlorine 065 mgl 020 0500 010 110 80- 120
Matrix S ike 8051049-MS2 Source SA7B602shy
Prepared amp Analyzed 14-May-
Total Residual Chlorine mgl 500 125 BRL 108 80- 120
Reference 8051 049-SRM1
Prepared amp Analyzed 14-May-
Total Residual Chlorine 100 mgl 020 0967 103 85-115
Batch 8051094 - General Preparation
Blank 8051094-BLK1
Prepared amp Analyzed 14 May-
Hexavalent Chromium (soluble) BRL mgl 005
Blank 8051 094-BLK2
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) BRL mgl 005
LCS 8051094-BS1
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) 054 mgl 005 90- 110
licate 8051094-DUP1 Source SA78602-01
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) BRL mgl 125 BRL
Thi laboratory report is not valid without all authorized sigllature 011 the cover page
Page 22 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Page 8
--------
--------
-------
--------
---
PAR
AM
ET
ER
B
elieve B
elieve of
Type of
Analytical
Minim
um
Maxim
um daily value
Avg daily value
Absent
Present Sam
ples Sam
ple (e M
ethod L
evel (ML
) of grab)
Used
Test M
ethod concentration
mass
concentration m
ass(1 m
inshy
imum
) (m
ethod ) (ug1)
(ug1) (kgday)
(ug1) (kgday)
43 Copper
GR
A
200 (5
44 Lead G
RA
200
0001
45 Mercury
GR
A
7470A
(020
46 Nickel
GR
AB
200
(5
GR
AB
200
( 1547 Selenium
48 Silver G
RA
B
200 (0
49 Zinc
GR
A
200 18
0025
50 Iron G
RA
B
200 400
25
Other (describe)
c For discharges where m
etals are believed present please fill out the following
If yes which m
etals A
rsenic and Iron Step
I Do any of the m
etals in the influent have a reasonable potential to exceed the
etIluent limits in A
ppendix II (i the limits set at zero to five dilutions) Y
rg N D
Step 2 For any m
etals which have reasonable potential to exceed the A
ppendix III limits
Look up the lim
it calculated at the corresponding dilution factor in
calculate the dilution factor (DF) using the form
ula in Part I A 3 c) (step 2) of the N
O
Appendix IV
Do any of the m
etals in the influent have the potential to instructions or as determ
ined by the State prior to the submission of this N
OI
exceed the corresponding effuent lim
its in Appendix IV
(i is the
What is the dilution factor for applicable m
etals in1uent concentration above the lim
it set at the calculated dilution M
etals A
rsenic and Iron factor)
yrgND
If Y
es list which m
etals A
rsenic and Iron
DF
Rem
ediation General Pem
lit - Notice of Intent
4 Treatm
ent system inform
ation Please describe the treatment system
using separate sheets as necessary including
a) A description of the treatm
ent system including a schem
atic of the proposed or existing treatment system
S
ee Figures 4 and 5
Frac tank Air stripper
Oilw
ater separator Equalization tanks
Bag filter rg
GA
C filter rg
b) Identity each applicable
treatment unit (check alJ
that apply)
Chlorination
Dechlorination
Other (please describe)
c) Proposed average and maxim
um flow
rates (gallons per minute) for the discharge and the design flow
rate(s) (gallons per minute) ofthe treatm
ent system
Average flow
rate of discharge 15 G
PM
Maxim
um flow
rate oftreatment system
0 G
PM
Design flow
rate of treatment system
0 G
PM
d) A description of chem
ical additives being used or planned to be used (attach MSD
S sheets) Not A
pplicable
5 Receiving surface water(s) Please provide information about the receiving water (s) using separate sheets as necessary including
Identity the discharge pathway
I Direct
I Within facility
I Stonn drain rg I R
iverbrook I W
etlands _ I Other (describe)
Provide a narrative description ofthe discharge pathway including the nam
e(s) of the receiving waters
Discharge to catchbasin and stonnw
ater drainage system in E
ast Broadw
ay which discharges to M
ahoney Brook (S
ee Figure 4)
c) Attach a detailed m
ap(s) indicating the site location and location of the outfall to the receiving water
1 For multiple discharges num
ber the discharges sequentialJy 2 For indirect dischargers indicate the location of the discharge to the indirect conveyance and the discharge to surface w
ater T
he map should also include the location and distance to the nearest sanitary sew
er as well as the locus of nearby sensitive receptors (based on U
SGS topographical
mapping) such as surface w
aters drinking water supplies and w
etland areas d) Provide the state w
ater quality classification of the receiving water
e) Provide the reported or calculated seven day- ten year low flow
(7QlO
) of the receiving water Jcfs
Please attach any calculation sheets used to support stream flow
and dilution calculations See A
ttachment B
f) Is the receiving water a listed 303(d) w
ater quality impaired or lim
ited water Y
es 0 No rg
If yes for which polJutant(s) N
A
Is there a TM
DL
Yes 0
No rg If yes for w
hich pollutant(s) NA
Rem
ediation General Perm
it - Notice of Intent
6 Results of C
onsultation with Federal Services Please p
rovide the following information according to requirements of Par
lBA
and A
ppendices II and VII
a) Are any listed threatened or endangered species or designated critical habitat in proxim
ity to the discharge Yes 0
No rg
Has any consultation w
ith the federal services been completed Y
es 0 No rg
or is consultation underway Y
es 0 No rg
What w
ere the results of the consultation with the U
S Fish and Wildlife Service andor N
ational Marine Fisheries Service (check one) N
ot applicable
a nojeopardy opinion
or written concurrenceD
on a finding that the discharges are not likely to adversely affect any endangered species or critical habitat
b) Are any historic properties listed or eligible for listing on the N
ational Register of H
istoric Places located on the facilty or site or in proximity to the discharge
Yes D
No
Have any state or tribal historic preservation offcer been consulted in this determ
ination (Massachusetts only) Y
es O N
o
7 SU
DD
lemental inform
ation
Please provide any supplemental information Attach any analytical data used to support the application A
ttach any celtification(s) required by the general permit
Attachm
ent A - Figures
Figure I - Site Locus M
ap
Figure 2 - MassD
EP Site Scoring M
ap
Figure 3 - Aerial M
ap
Figure 4 - Proposed Soil Excavation A
rea Map
Figure 5 - T
reatment S
ystem Line D
iagram
Attachm
ent B - D
ilution factor Calculations
Attachment C - L
aboratory Analytical R
eport Groundw
ater
Rem
ediation General Perm
it - Notice of 1ntenl
=-
including the following
8 Signature Requirements
The N
otice ofIntent must be signed by the operator in accordance w
ith the signatory requirements of 40 C
FR Section 122
certification
J certif under penalty of law that this docum
ent and all attachments w
ere prepared under my direction or supervision in accordance w
ith a system
designed to assure that qualifed personnel properly gather and evaluate the information subm
itted Based on m
y inquiry of the person or persons who
manage the system
or those persons directly responsible for gathering the information I certif that t
he information submitted
is to the best of m
y
knowledge and belief true accurate and com
plete J certif that I am aw
are that there are signifcant penalties for submitting false inform
ation including
the possibilty of fine and imprisonm
ent for knowing violations
FacilitySite Name
Form
er Speedw
ay Service S
tation 181 East B
roadwav G
ardner MA
01440
Operator signature
Title
Michael 1 D
ziura Sf Env E
ngineer
Date
4150- q
Rem
ediation General Perm
it - Notice of Intent
-
D- 0
0 0
il (J tu
Bw
o(0 -I
NJW
gQb
J(JZc o c
rou a -10
0 J 6shy
a 0
I-tDC
aJ Qj
E aJshy
ro ro ro
~~~ ~~~~- -- - _ - -_ - ~~~ ~~~~ ~~~ - - _- _- -- -- p __(
MA DEP - Bureau of Waste Site CleanupSITE NME Site S aP 5 MiFlII Former Speeway Station _-II181 Eat Broaday b b d IS I i I GARDNER MA 0144 v ri) i P f f 1 me- 1 5ylmI I L shy J --I 423315n 715835e SiteLocation y o oCop1odQcn Ofof W-_ l
1 1 I
r
r
iBARBER HILL
A c
Cf1 f o s
0
5
Roads Uned Acss Divd Mar Roed Conntor Street Track 1 EPA Sola Source Aquilar FEMA 100yaar iloodplain 0 c Puc Watar SLo GrunSelaceNon Corrty 0
Bounars lOwn Couny DE Region Tian Powerln Ine Aqedut ApprOld Zona2 tNPA Sue Wster Supp Zone A bStZ F--shy--rle
8os Mat Sub SUeor Porenrial Inermtent Man lvo8 Ste Dfm Hyro1apy Wmer FeatllePLio Suleee Wat S H-- L otlMds FrslSaltN-ES WeIMd Habat L
Potentia Prdutiv AqlJlers ModHig Yield Proteoted Opn Space ACC nIL c= Non-Potential Drng Water Sollce AIea ModumHi Yo1d ll DEP Pormrd SoidWes1 FsiIi6s cnifud Verne Pools f0
1I2 KIWUmR$ MtL
January 30 2004 SCALE 1 15000
-
LE
GE
ND
APX PROPER BONDA
- APPROXOiSPO SIT BOUNDA
-GR
OU
ND
WA
TE F1 D
IRE
cnON
SCA
LE
30 60 FE
(APR
OX
CORPORATE ENVIRONMENTAL
)i
AD
VISO
RS
INC
SC
AS SH
OW
D
R B
Y K
HA
EL
DA
TE
10407
JOB
NO
2920-96
AERIAL MAP
FO
RM
ER
SP
EE
DW
AY
ST
AT
ION
FlGURE -3
181 EA
BR
OA
AY
GA
NE
R fo
age 1 ot 1Streamflow Statistics Report
Streamstats Ungaged Site Report Date Wed Dec 31 2008 124908 Site Location Massachusetts NAD83 Latitude 425545 (42 3316) NAD83 Longitude -719758 (-71 58 32) NAD27 Latitude 425545 (423316) NAD27 Longitude - 9763 (-71 58 34) Drainage Area 502 mi2
IPeak Flow Basin Characteristics 1100 Statewide Low Flow (S02 mi2)
Regression Equation Valid Rang
I Min II Max1 Value III Parameter Drainage Area (square miles) 161 149
Mean Basin Slope from 250K DEM (percent) 032 24
Stratified Drift per Stream Length (square mile per mile) 129
Massachusetts Region (dimensionless)
Streamflow Statistics
gO-Percent Prediction Interval Prediction Error
MaximumStatistic Flow (ft s) (percent) Minimum
I D50 IIII 11 1811 II 24511 993
I D60 II 35511 2011 II 03611 35111 2411 II 041 I 201I D70 24111 2611 II 03811 151I D75 11 2811 II 0911 3761I D80 981I D85 1 I 3211 II o6311
1 I 3711 II 0441 1 2 2911 D90 11 4611 II 02411 15511 D95I D98 04511 6011 II 01511 11
I D99 03411 6511 II ol1ll 1021
5011 II 02611 11I M7D2Y 1111 3311 II odl 3 541
I AUGD50
IIIIIIIIIIIIIIIIIIIIII 0311 7111 II 0088411 0981I M7Dl0Y
1010
12312008httpstreamstatsagscrusgsgovgisimgReportsFlowStatsReport3494 - 2008123112498
Dilution Factor Calculation Former Speedway Service Station 181 East Broadway Gardner Ma
DF=(Od+Os)Od
DF = Dilution factor
Od = Max flow rate of discharge in cubic feet per second Os = receiving water flow in cubic feet per seconds 7010 flow rate Mahoney Brook 7010 = min flow for seven consecutive days with a recurrence interval of 10 years
7010 flow based on data obtained from USGS Steamflow Statistics Report Data attached
067
Semivolatile Organic Compounds by GCMS - Quality Control
Analyte( s)
Batch 8051216 - SW846 3510C
Blank 8051216BLK1)
Prepared amp Analyzed 16May-
Acenaphthene
Acenaphthylene
Aniline
Anthracene
AzobenzenelDi phenyld iazi ne
Benzidine
Benzo (a) anthracene
Benzo (a) pyrene
Benzo (b) fiuoranthene
Benzo (g i) perylene
Benzo (k) fiuoranthene
Benzoic acid
Benzyl alcohol
Bis(2-ch loroethoxy) methane
Bis(2-ch loroethyl)ether
Bis(2-ch loroi sopropyl)ether
Bis(2ethylhexyl) phthalate
Bromophenyl phenyl ether
Butyl benzyl phthalate
Carbazole
Ch loro-3-methyl phenol
Chloroaniline
Chloronaphthalene
Chlorophenol
Chlorophenyl phenyl ether
Chrysene
Dibenzo (a h) anthracene
Dibenzofuran
Dichlorobenzene
Dichlorobenzene
14- Dichlorobenzene
3 - Dichlorobenzidine
24-Dichlorophenol
Diethyl phthalate
Dimethyl phthalate
24- Dimethylphenol
Din-butyl phthalate
Dinitro-2-methylphenol
Dinitrophenol
Dinitrotoluene
Dinitrotoluene
Di-noctyl phthalate
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopehtadiene
Hexachloroethane
Indeno (1 cd) pyrene
Spike Source REC RPD
Result Flag Units RDL Level Result REC Limits RPD Limit
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gl
BRL gI
BRL gl
BRL gl
BRL gl
BRL gI
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gll
BRL gl
BRL gll
BRL gl
BRL gl
BRL gI
BRL gI
BRL gI
BRL gl
BRL gI
BRL gI
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gI
BRL gI
BRL gl
This laboratory report is IlOt valid without all authorized sigllature 011 the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page t4 of25
Volatie Organic Compounds - Quality Control
p (
Spike Source REC RPD
RDL Level Result REC Limits RPD Limit Analyte(s) Result Flag Units
Batch 8051244 - SW846 5030 Water MS
Matrix S ike Du 8051244-MSD1 Source SA78629shy
Prepared 16-May-08 Analyzed 17-May-BRL 106 251
Vinyl chloride 21 gl 20
101 70- 130 Surrogate 4-Bromofluorobenzene 50 gl 50
70- 13049 gl 50 111 70- 130
Surrogate Toluene-Surrogate 1 Dichloroethane- 55 gl 50
50 70- 130494 glSurrogate Dibromofluoromethane
Microextractable Organic Compounds - Quality Control
Spike Source REC RPD
Flag Units RDL Level Result REC Limits RPD Limit Analyte(s) Result
Batch 8051105 - SW846 3510C
Blank 8051105-BLK
Prepared amp Analyzed 15-May-
BRL gl 01001 Dibromoethane (ED B)
LCS 8051105-BS1
Prepared amp Analyzed 15-Mayshy50- 1500770 gl 0100 100
licate 8051105-DUP1 Source SA7B583shy
Prepared amp Analyzed 15-May-
BRL gl 0100 BRL
1 Dibromoethane (EDB)
1 Dibromoethane (EDB)
This laborntOlY report is not valid without an authorized signature 011 the cover page
Page 13 of2S Reportable Detection Limit BRL = Below Reporting Limit
Sam le Identification Client Pro ect Matrix Collection DateTime ReceivedMWshy
2920-96- Ground Water 13-May-081030 14-May-SA 78602shy
CAS No Analyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Volatile Organic Compounds
Volatile Or anic Com ounds b GCMS
Prepared by method SW846 5030 Water MS
123-91- Dioxane BRL 1-91 200 EPA 624 16-May-08 17-May-08 8051244
994-05-8 Ter-amyl methyl ether BRL 1-911 20
755- Tert-Butanoll butyl alcohol BRL 1-91 200
67-B4- Acetone BRL 1-91 400
71-43- Benzene BRL 1-91 20
75-27-4 Bromodichloromethane BRL 1-91 20
75-25- Bromoform BRL 1-91 20
74-83- Bromomethane BRL 1-91 40
78-93- Butanone (MEK) BRL 1-91 200
56-23- Carbon tetrachloride BRL 1-91 20
108-90- Chlorobenzene BRL 1-91 20
75-00- Chloroethane BRL 1-91 40
676- Chloroform BRL 1-91 20
74-87- Chloromethane BRL 1-91 40
124-48- Dibromochloromethane BRL 1-91 20
95-50- Dichlorobenzene BRL 1-911 20
541-73- Dichlorobenzene BRL 1-91 20
106-46- Dichlorobenzene BRL 1-91 20
75-34- 1- Dichloroethane BRL 1-91 20
107-06- Dichloroethane BRL 1-91 20
75-35-4 1- Dichloroethene BRL 1-91 20
156-59 cis- Dichloroethene BRL 1-91 20
156-60- trans- Dichloroethene BRL 1-91 20
78-87- 2- Dichloropropane BRL 1-91 20
10061-01-5 cis- Dichloropropene BRL 1-91 20
10061-02-B trans- Dichloropropene BRL 1-91 20
100-41-4 Ethylbenzene 411 1-911 20
591-78-B BRL 200Hexanone (MBK) 1-91
1634-04 -4 Methyl tert-butyl ether BRL 1-91 20
108-10- Methyl- pentanone (MIBK) BRL 1-91 200
75-09- Methylene chloride BRL 1-91 200
100-42- Styrene BRL 1-91 20
79-34- 1 Tetrachloroethane BRL 1-91 20
127- 18-4 T etrachloroethene BRL 1-91 20
108-88- Toluene BRL 1-91 20
71-55 1- Trichloroethane BRL 1-91 20
79-00- 2- Trichloroethane BRL 1-91 20
79-01-B Trichloroethene BRL 1-91 20
759-4 Trichlorofluoromethane (Freon 11) BRL 1-91 20
75-01-4 Vinyl chloride BRL 1-91 20
179601-23-1 m Xylene 390 1-91 40
95-47 Xylene 82 1-91 20
Surrogate recoveries 460-00- Bromofluorobenzene 70- 130
2037-26- Toluene- 100 70- 130
17060-07-0 1 Dichloroethane- 111 70- 130
1868-53- Dibromofluoromethane 70- 130
Microextractable Organic Compounds
106-93-4 1 Dibromoethane (EDB) BRL 1-91 0100 EPA 504 15-May- 15-May-08 8051105
Semivolatile Organic Compounds by GCMS
This laboratory report is not valid without all autllOrized signature 011 the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page 5 of 25
Sam le Identification Client Pro ect Matrix Collection DateTime Received
MWshy2920-96- Ground Water 13-May-081030 14-May-
SA 78602shy
CAS No Analyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Semivolatie Organic Compounds by GCMS
Semi volatile Or anic Com ounds b EPA 625
Prepared by method SW846 3510C 50 EPA 625 16-May- 19-May-08 805121683-32- Acenaphthene BRL IJgl
208-96-8 Acenaphthylene BRL IJgl 50
62-53- BRL IJgll 50Aniline
120- 12- Anthracene BRL 1J91 50
103-33- AzobenzenefDiphenyldiazine BRL IJgl 50
92-87 - Benzidine BRL IJgl 50
56-55- Benzo (a) anthracene BRL 1J91 50
50-32 - Benzo (a) pyrene IJglBRL 50
205-99- Benzo (b) fluoranthene BRL IJgl 50
191-24- Benzo (g i) perylene BRL IJgl 50
50207-08- Benzo (k) fluoranthene BRL IJgl
65-85 Benzoic acid BRL 1J91 50
100-51-6 Benzyl alcohol 1J91BRL 50
50111-91- Bis(2-chloroethoxy)methane BRL 1J91
111-4-4 Bis(2-chloroethyl)ether BRL IJgl 50
501 08-60- Bis(2-chloroisopropyl)ether BRL IJgl
117-81- Bis(2-ethylhexyl)phthalate BRL 1J91 50
101-55- Bromophenyl phenyl ether BRL IJgl 50
5085-68- Butyl benzyl phthalate BRL IJgl
5086-74- Carbazole BRL IJgl
5059-50- C hloro-3-methylphenol BRL IJgl
106-47- Chloroaniline BRL IJgl 50
91-58- Chloronaphthalene IJglBRL 50
5095-57 - Chlorophenol BRL 1J91
507005-72- Chlorophenyl phenyl ether BRL IJgl
216-01- Chrysene tJ91BRL 50
5053-70- Dibenzo (a h) anthracene BRL IJgl
50132-64- Dibenzofuran BRL IJgl
95-50- Dichlorobenzene IJglBRL 50
541-73- 13- Dichlorobenzene BRL IJgl 50
106-46- Dichlorobenzene 1J91BRL 50
5091-94- 3 - Dichlorobenzidine BRL IJgl
120-83- Dichlorophenol BRL IJgl 50
84-66- Diethyl phthalate BRL IJgl 50
131-11- Dimethyl phthalate BRL IJgll 50
105-67- Dimethylphenol BRL 1J91 50
5084-74- Di-n- butyl phthalate BRL 1J91
534-52 - Dinitro-2-methylphenol BRL IJgl 50
51-28- Dinitrophenol IJglBRL 50
50121-14- Dinitrotoluene BRL 1J91
606-20- Dinitrotoluene IJglBRL 50
50117-84-0 Di-n-octyl phthalate BRL IJgl
206-44-0 Fluoranthene 1J91BRL 50
BRL 50
50 86-73- Fluorene IJgi
118-74- Hexachlorobenzene BRL 1J91
87-68- Hexachlorobutadiene 1J91BRL 50
5077-47-4 Hexachlorocyclopentadiene BRL IJgl
67-72- Hexachloroethane IJglBRL 50
50193-39- Indeno (1 3-cd) pyrene BRL IJgl
5078-59- Isophorone BRL IJgl
Tfls laboratory report is not valid without all authorized signature 011 the coverpage
Page 6 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Sam le Identification Client Pro ect Matrix Collection DateTime ReceivedMWshy
2920-96- Ground Water I3-May-081030 14-May-SA 78602shy
CAS No Analyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Semivolatile Organic Compounds by GCMS
Semi volatile Or anic Com ounds b EPA 625
Prepared by method SW846 3510C
91-57 -6 Methylnaphthalene 367 1-91 50 EPA 625 16-May- 19-May-08 8051216
95-48- Methylphenol BRL 1-91 50
108-39-4 3 amp 4-Methylphenol BRL I-gl 100 106-44shy91-20- Naphthalene 247 1-91 50
88-74-4 Nitroaniline BRL 1-91 50
99-09- Nitroaniline BRL 1-91 50
100-01-6 Nitroaniline BRL 1-91 50
98-95- Nitrobenzene BRL 1-91 50
88-75- Nitrophenol BRL 1-91 50
100-02- Nitrophenol BRL 1-91 50
62-75- Nitrosodimethylamine BRL 1-91 50
621-64- N- Nitrosodi-n-propylamine BRL 1-91 50
86-30-6 Nitrosodiphenylamine BRL 1-91 50
87 -86- Pentachlorophenol BRL 1-91 50
85-0- Phenanthrene BRL 1-91 50
108-95- Phenol BRL 1-91 50
129-00-0 Pyrene BRL 1-91 50
110-86- Pyridine BRL 1-91 50
120-82- 4- Trichlorobenzene BRL 1-91 50
95-95- 5- Trichlorophenol BRL 1-91 50
88-06- 6- T richlorophenol BRL 1-91 50
Surrogate recoveries
321-60- Fluorobipheny 30- 130
367- 12- Fuorophenol 15- 110
4165-60- Nitrobenzene- 30- 130
4165-62- Pheno- 15- 110
1718-51- Terpheny-d4 30- 130
118- 79- 6- Tribromophenol 15- 110
Semivolatile Organic Compounds by GC
Pol chlorinated Bi hen ls b EPA 608
Prepared by method SW846 3510C
12674- 11-2 Aroclor- 1016 BRL 1-91 0650 EPA 608 15- May- 16-May-08 8051106
11104-28-2 Aroclor-1221 BRL IJgl 0650
11141-16-5 Aroclor- 1232 BRL 1-91 0650
53469-21-9 Aroclor- 1242 BRL 1-91 0650
12672-29-6 Aroclor- 1248 BRL 1-91 0650
11097-69-1 Aroclor- 1254 BRL 1-91 0650
11096-82-5 Aroclor -1260 BRL 1-91 0650
37324-23-5 Aroclor-1262 BRL 1-91 0650
11100-14-4 Aroclor-1268 BRL IJgl 0650
Surrogate recoveries
2051-24- Decachlorobipheny (Sr) 105 30- 150
10386-84-2 4 DB-Octafluorobiphenyl (Sr) 30- 150
Extractable Petroleum Hydrocarbons
mgl EPA 1664 Rev A 15-May- 19-May-08 8051102Non-polar material (SGT- HEM)
Soluble Metals by EPA 2006000 Series Metbods
Field Filtered NA EPA 200 73005A 15- May- 15-May-08 8051192Filtration
Soluble Metals by EPA 200 Series Methods
7440-22-4 Silver BRL mgl 0002 EPA 200 21-May- 27- May-08 8051249
This laboratory report is IlOt mlid without (II authorized signature on the cover page
Reportble Detection Limit BRL = Below Reporting Limit Page 7 of 25
Sam le Identification MW-
Client Pro ect 2920-96shy
Matrix Ground Water
Collection DateTime 13-May-08 1030
Received 14-May-
SA 78602shy
CAS No A nalyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Soluble Metals by EPA 200 Series Methods
7440-38shy Arsenic 0468 mg1 0040 EPA 200 21-Mayshy 21-May-08 80511 50
7440-43shy Cadmium BRL mg1 0002 EPA 200 21-May-088051249
7440-47shy Chromium BRL mg1 0050 EPA 200 21-May-088051150
7440-50-8 Copper BRL mg1 0050
7439-89-6 Iron 184 mg1 0150
7439-97-6 Mercury BRL mg1 00020 EPA 245 17470A 21-May-088051152
7440-02-0 Nickel BRL mg1 0050 EPA 200 21-May-088051150
7439-92shy Lead 0011 mg1 0002 EPA 200 21-May-088051249
7440-36-0 Antimony 0003 mg1 0002
7782-49shy Selenium BRL mg1 0150 EPA 200 21-May-08 8051150
7440-66-6 Zinc 0186 mgl 0050
General Chemistry Parameters
Filtration Completed NA Varies 14-Mayshy 14-May-08 8051095
18540-29-9 Hexavalent Chromium (soluble) BRL HT2 mg1 125 SM3500CrDI796A 14-Mayshy 14-May-08 8051094 R01 2013 2016
57-12shy Cyanide (total) BRL mg1 0100 EPA 3354 19-Mayshy 19-May-088051374
7782-50shy Total Residual Chlorine BRL CIHT mg1 500 Hach 8167 14-Mayshy 14-May-08 8051049 R01 1900 2001
Total Suspended Solids 580 mg1 25 SM2540D 16-Mayshy 16-May-08 8051275
This lahomtOlY report is not valid without an authorized signature on the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page 8 of 25
Volatie Organic Compounds - Quality Control
Analyte( s)
Batch 8051244 - SW846 5030 Water MS
Blank 8051244-BLK1
Prepared 16-May-08 Analyzed 17-May-
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromochloromethane
1 Dichlorobenzene
1 Dichlorobenzene
1 Dichlorobenzene
1-Dichloroethane
1 Dichloroethane
1 1-Dichloroethene
cis- Dichloroethene
trans- 1 Dichloroethene
1 Dichloropropane
cis- 1 Dichloropropene
trans- 1 Dichloropropene
Ethylbenzene
Hexanone (MBK)
Methyl tert-butyl ether
Methyl- pentanone (MIBK)
Methylene chloride
Styrene
2- Tetrachloroethane
Tetrachloroethene
Toluene
1- Trichloroethane
2- Trichloroethane
Trichloroethene
Trichlorofluoromethane (Freon 11)
Vinyl chloride
p-Xylene
Xylene
Surrogate 4-Bromofluorobenzene Surrogate Toluene-
Surrogate 1 Dichloroethane-Surrogate Dibromofluoromethane
LCS B051244-BS1
Prepared 16-May-08 Analyzed 17 -May-
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Spike Source REC RPD
Result Flag Units RDL Level Result REC Limits RPD Limit
BRL gl 20
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl 10
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gll
BRL gi
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl 10
BRL gll
BRL gll 10
BRL gl 10
BRL gll
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
41 gl 50 70- 130 49 gl 50 70- 130 59 gl 50 119 70- 130 52 gl 50 105 70- 130
QC2 jgl 20 70- 130
18 jgl 20 70- 130
192 jgl 20 35- 155
18 jgl 20 45- 169
19 jgl 20 242
This laboratOlY repol1 is lot valid without 011 authorized sigllature 011 the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page 9 of 25
Volatie Organic Compounds - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051244 - SW846 5030 Water MS
LC5 8051244B51
Prepared 16-May-08 Analyzed 17-May-
Butanone (MEK) 10 QC2 gl 20 70- 130
Carbon tetrachloride 204 gl 20 102 70- 140
Chlorobenzene 18 gl 20 70- 130
Chloroethane 164 gl 20 14-230
Chloroform 18 gll 20 51- 138
Chloromethane 21 gl 20 106 273
Dibromochloromethane 18 gl 20 53- 149
1 Dichlorobenzene 20 gl 20 104 18- 190
1 Dichlorobenzene 19 gl 20 59- 156
1 A-Dichlorobenzene 18 gl 20 18- 190
1- Dichloroethane 19 gl 20 59- 155
1 Dichloroethane 19 gl 20 49- 155
1-Dichloroethene 16 gl 20 70- 130
cis- 1 Dichloroethene 17 gl 20 70- 130
trans- 1 Dichloroethene 16 gll 20 54- 156
1 Dichloropropane 18 gl 20 210
cis- Dichloropropene 17 gl 20 227
trans- 1 Dichloropropene 17 gl 20 17- 183
Ethylbenzene 19 gl 20 37- 162
Hexanone (MBK) 124 QC2 gl 20 70- 130
Methyl tert-butyl ether 19 gl 20 70- 130
Methylshy pentanone (MIBK) 17 gl 20 70- 130
Methylene chloride 16 gl 20 221
Styrene 17 gl 20 70- 130
1 Tetrachloroethane 194 gl 20 46- 157
Tetrachloroethene 15 gl 20 64- 148
Toluene 18 gl 20 70- 130
1- Trichloroethane 20 gl 20 100 52- 162
2- Trichloroethane 18 gl 20 52- 150
Trichloroethene 17 gl 20 71- 157
Trichlorofluoromethane (Freon 11) 19 gl 20 17- 181
Vinyl chloride 21 gl 20 106 251
p-Xylene 39 gl 40 70- 130
Xylene 20 gl 20 102 70- 130
Surrogate 4-Bromofluorobenzene Surrogate Toluene-
Surrogate 1 Dichloroethane-Surrogate Dibromofluoromethane
52 49 56
49
gl
gl
gl
gl
50 50 50
50
105
112 100
70- 130 70- 130 70- 130 70- 130
LC5 DUD (8051244-B5D1
Prepared 16-May-08 Analyzed 17-May-
Acetone QC2 gl 20 70- 130
Benzene 18 gl 20 70- 130
Bromodichloromethane 18 gl 200 35- 155
Bromoform 17 gl 20 45- 169
Bromomethane 18 gl 20 242
Butanone (MEK) 11 QC2 1-91 20 70- 130
Carbon tetrachloride 20 gl 20 100 70- 140
Chlorobenzene 17 gl 20 70- 130
Chloroethane 15 1-91 20 14-230
Chloroform 18 1-91 20 51- 138
This laboratory report is aot valid without a1 authorized sig1ature 01 the cover page
Reportble Detection Limit BRL = Below Reporting Limit Page 10 of25
Volatie Organic Compounds - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051244 - SW846 5030 Water MS
LCS Dup 18051244-BSD1
Prepared 16-May-08 Analyzed 17-May-
Chloromethane 18 1-91 20 273
Dibromochloromethane 174 1-91 20 53- 149
Dichlorobenzene 20 1-91 20 100 18- 190
Dichlorobenzene 18 1-91 20 59- 156
Dichlorobenzene 18 1-91 20 18- 190
Dichloroethane 18 1-91 20 59- 155
Dichloroethane 19 1-91 20 49- 155
Dichloroethene 16 1-91 20 70- 130
cis- Dichloroethene 16 1-91 20 70- 130
trans- Dichloroethene 15 1-91 20 54- 156
Dichloropropane 17 1-91 20 210
cis- Dichloropropene 164 IJgl 20 227
trans- 1 Dichloropropene 164 I-gl 20 17- 183
Etlwlbenzene 18 IJgl 20 37- 162
Hexanone (MBK) 124 QC2 IJgl 20 70- 130
Methyl tert-butyl ether 184 1J91 20 70- 130
Methyl- pentanone (MIBK) 17 IJgl 20 70- 130
Methylene chloride 16 IJgl 20 221
Styrene 16 IJgl 20 70- 130
2- Tetrachloroethane 19 IJgl 20 46- 157
Tetrachloroethene 15 IJgl 20 64- 148
Toluene 17 IJgl 20 70- 130
1- Trichloroethane 19 1-91 20 52- 162
2- Trichloroethane 16 IJgl 20 52- 150
Trichloroethene 15 IJgl 20 71- 157
Trichlorofluoromethane (Freon 11) 17 IJgl 20 17- 181
Vinyl chloride 19 IJglI 20 251
p-Xylene 37 1J91 40 70- 130
Xylene 20 IJgl 20 100 70- 130
Surrogate 4-Bromofluorobenzene 51 IJgl 50 104 70- 130
Surrogate Toluene- 4B gl 50 70- 130
Surrogate 1 0ichloroethane- 53 IJgl 50 106 70- 130 Surrogate Oibromofluoromethane 50 1J9i 50 102 70- 130
Matrix S ike B051244-MS1 Source SA7B629shy
Prepared 16-May-08 Analyzed 17-May-
Benzene 18 20 BRL 70- 130IJgl
Bromodichloromethane 19 IJgl 20 BRL 35- 155
Bromoform 18 IJgl 20 BRL 45- 169
Bromomethane 16 IJgl 20 BRL 242
Carbon tetrachloride 21 IJgl 20 BRL 106 70- 140
Chlorobenzene 18 IJgl 20 BRL 70- 130
Chloroethane 16 IJgl 20 BRL 14-230
Chloroform 18 IJgl 20 BRL 51- 138
Chloromethane 19 IJgl 20 BRL 273
Dibromochloromethane 17 IJgl 20 BRL 53- 149
1 Dichlorobenzene 22 IJgl 20 BRL 112 18- 190
1 Dichlorobenzene 22 IJgl 20 BRL 110 59-156
1 Dichlorobenzene 21 IJgl 20 BRL 109 18- 190
1- Dichloroethane 19 IJgl 20 BRL 59- 155
1 Dichloroethane 18 IJgl 20 BRL 49- 155
This laboratory report is 110t mUd without an authorized signature on the covel page
Reportble Detection Limit BRL = Below Reporting Limit Page It of25
Volatile Organic Compounds - Quality Control
p
Spike Source REC RPD
Result REC imits RPD LimitAnalyte(s) Result Flag Units RDL Level
Batch 8051244 - SW846 5030 Water MS
Matrix ike S051244-MS1 Source SA7B629shy
Prepared 16-May-08 Analyzed 17-Mayshy
17 20 BRL 70- 130 1- Dichloroethene IJgl
16 20 BRL 54- 156trans- 1 Dichloroethene IJgl
21020 BRL1 Dichloropropane 17 1J91
cis- 1 Dichloropropene 17 IJgl 20 BRL 227
17- 183trans- 1 Dichloropropene 184 1J91 20 BRL
20 20 BRL 103 37- 162Ethylbenzene IJgl
15 20 BRL 221Methylene chloride IJgl
20 BRL 46- 1572- Tetrachloroethane 19 1J91
20 BRL 64- 148Tetrachloroethene 18 1J91
BRL 70- 130Toluene 18 1J91 20
105 52-1621- Trichloroethane 211 IJgl 20 BRL
18 20 BRL 52- 1502- Trichloroethane IJgl
17 20 BRL 71- 157Trichloroethene 1J91
20 BRL 17- 181Trichloroluoromethane (Freon 11) 194 IJgl
20 BRL 103 251Vinyl chloride 20 IJgl
102 70- 130Surrogate 4-Bromofluorobenzene 50 IJgl 50 50 70- 130Surrogate Toluene- 49 1J91
56 50 112 70- 130Surrogate 1 Dichloroethane- IJgl
50 100 70- 130Surrogate Dibromofluoromethane 50 IJgl
Matrix S ike Du S051244-MSD1 Source SA7S629shy
Prepared 16-May-08 Analyzed 17-Mayshy
18 20 BRL 70- 130Benzene IJgl
18 20 BRL 35- 155Bromodichloromethane IJgl
17 20 BRL 45- 169Bromoform IJgl
20 BRL 242Bromomethane 17 IJgl
20 BRL 103 70- 140Carbon tetrachloride 20 IJgl
18 20 BRL 70- 130Chlorobenzene 1J91
14-230Chloroethane 16 IJgl 20 BRL
20 51- 138Chloroform 184 IJgl BRL
Chloromethane 19 1J91 20 BRL 273
18 20 BRL 53- 149Dibromochloromethane 1J91
20 BRL 117 18- 190Dichlorobenzene 234 IJgl
20 BRL 112 59- 156Dichlorobenzene 22 IJgl
BRL 108 18- 190Dichlorobenzene 21 1J91 20
20 59- 1551 Dichloroethane 19 IJgl BRL
18 20 BRL 49- 155Dichloroethane IJgl
16 20 BRL 70- 130Dichloroethene IJgl
20 BRL 54- 156trans- Dichloroethene 154 1J91
20 BRL 210Dichloropropane 17 IJgl
0420 BRL 227cis- Dichloropropene 17 IJgl
17- 183trans- Dichloropropene 17 1J91 20 BRL
BRL 37- 162Ethylbenzene 20 1J91 20 102
Methylene chloride 15 IJgl 20 BRL 221
20 BRL 46- 1572- Tetrachloroethane 192 IJgl
20 BRL 64- 148 04Tetrachloroethene 18 IJgl
BRL 70- 130Toluene 184 1J91 20
52- 1621- Trichloroethane 20 IJgl 20 BRL 104
17 20 BRL 52- 1502- Trichloroethane IJgl
17 20 BRL 71- 157Trichloroethene IJgl
20 BRL 17-181Trichlorofluoromethane (Freon 11) 19 IJgl
This laboratory report is IIOt valid without all authorized sigllllture 011 the cover page
Page 12 of25 Reportble Detection Limit BRL = Below Reporting Limit
Semivolatile Organic Compounds by GCMS - Quality Control
Analyte(s)
Batch 8051216 - SW846 3510C
Blank 8051216-BLK1
Prepared amp Analyzed 16-May-
Isophorone
Methylnaphthalene
Methylphenol
3 amp 4-Methylphenol
Naphthalene
Nitroaniline
Nitroaniline
Nitroaniline
Nitrobenzene
Nitrophenol
Nitrophenol
Nitrosodimethylamine
N- N itrosodi-n-pro pyla mine
N itrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Pyridine
1 24-Trichlorobenzene
24 5- Trichlorophenol
246- Trichlorophenol
Surrogate 2-Fuorobipheny Surrogate 2-Fuoropheno Surrogate Nitrobenzene-Surrogate PhenoshySurrogate Terpheny-d4 Surrogate 6- Tribromopheno
LCS B051216-BS1
Prepared amp Analyzed 16-May-
Acenaphthene
Acenaphthylene
Aniline
Anthracene
AzobenzenelDi phenyld lazine
Benzidine
Benzo (a) anthracene
Benzo (a) pyrene
Benzo (b) fluoranthene
Benzo (g i) perylene
Benzo (k) fluoranthene
Benzoic acid
Benzyl alcohol
B is(2-chloroethoxy)methane
B i s (2-ch loroethyl)eth e r
Bis(2-ch loroisopropyl) ether
B is(2-ethy Ih exyl) phtha late
Bromophenyl phenyl ether
Butyl benzyl phthalate
Carbazole
Spike Source REC RPD
Result Flag Units RDL Level Result REC Limits RPD Limit
BRL gl
BRL gl
BRL gl
BRL gl 10
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gll
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
370 gl 50 30- 130 40 gl 50 15- 110 39 gl 50 30- 130 43 gl 50 15- 110 36 gl 50 30- 130 40 gl 50 15- 110
41 gl 50 40- 140
43 gI 50 40- 140
41 gl 50 40- 140
38 gl 50 40- 140
45 gl 50 40- 140
49 gl 50 153
41 gl 50 40- 140
43 gl 50 40- 140
41 gl 50 40- 140
41 gll 50 40- 140
45 gl 50 40- 140
32 gl 50 12- 149
41 gl 50 40- 140
39 gl 50 40- 140
384 gl 50 40- 140
47 gl 50 40- 140
47 gl 50 40- 140
40 gl 50 40- 140
47 gI 50 40- 140
56 gI 50 112 200
This laboratory report is lIot valid witllOut a1l authorized sigllature 011 the coverpage
Reportble Detection Limit BRL = Below Reporting Limit Page 15 of25
Semivolatile Organic Compounds by GCMS - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051216 - SW846 3510C
LCS 8051216-BS1
Prepared amp Analyzed 16-Mayshy
50 30- 1304 -C hloro-3-methylphenol 42 IJgl
40- 140Chloroaniline 39 IJgl 50
Chloronaphthalene 37 IJgl 50 40- 140
Chlorophenol 37 IJgl 50 30- 130
50 40- 140
40- 140
Chlorophenyl phenyl ether 45 IJgl
Chrysene 43 IJgl 50
Dibenzo (a h) anthracene 43 IJgl 50 40- 140
Dibenzofuran IJgl38 50 40- 140
50 40- 1401 Dichlorobenzene 35 IJgl
40- 1401 Dichlorobenzene 264 IJgl 50
40- 1401 Dichlorobenzene 434 IJgl 50
58 50 116 40- 1403 - Dichlorobenzidine IJgl
50 30- 130
40- 140 24-Dichlorophenol 38 IJgl
Diethyl phthalate 484 IJgl 50
50 40- 140Dimethyl phthalate 464 IJgl
Dlmethylphenol 39 IJgl 50 30- 130
DI-n-butyl phthalate 44 IJgll 50 40- 140
30- 130 6-Di nitro- 2-methylphenol 38 1J91 50
30- 130Dinltrophenol 36 1J91 50
42 50 40- 14024-Dlnitrotoluene 1J91
Dlnitrotoluene 1J9141 50 40- 140
Di-n-octyl phthalate 52 IJgl 50 104 40- 140
40- 140Fluoranthene 40 IJgl 50
Fluorene 41 IJgl 50 40- 140
39 50 40- 140Hexachlorobenzene IJgl
50 40- 140Hexachlorobutadiene 40 IJgl
40- 140Hexach lorocyclopentad iene 294 IJgl 50
40 50 40- 140Hexachloroethane IJgl
42 50 40-140Indeno (1 3-cd) pyrene IJgl
50 40- 140Isophorone 40 IJgl
40- 140Methylnaphthalene 394 IJgl 50
40- 140Methylphenol 39 IJgl 50
40 10 50 40- 1403 amp 4-Methylphenol IJgl
37 50 40-140Naphthalene IJgl
50 40-140Nitroaniline 39 IJgl
Nitroaniline 51 IJgl 50 102 40- 140
48 50 40- 140Nltroaniline 1J91
50 40- 140Nitrobenzene 40 IJgl
30- 130Nitrophenol 36 IJgl 50
40 IJgl 50 30- 130Nitrophenol 40- 140Nitrosodimethylamine 32 1J91 50
50 40-140N- N itrosodi-n-propyla mine 46 IJgl
40- 140N itrosodi phenyla ml ne 44 IJgl 50
41 IJgl 50 30- 130Pentachlorophenol 40- 140Phenanthrene 38 IJgl 50
50 30- 130Phenol 38 IJgl
40- 140Pyrene 424 1J91 50
40- 140Pyridine 294 1J91 50
40- 14024- Trichlorobenzene 364 IJgl 50
This laboratory report is not mlid without an authorized signature 011 the cover page
Page 16 of25 Reportble Detection Limit BRL = Below Reporting Limit
Semivolatie Organic Compounds by GCMS - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
BMch 8051216 - SW846 3510C
LC5 8051216-851
Prepared amp Analyzed 16-Mayshy
24 5- Trichlorophenol 404 gl 50 30- 130
246- Trichlorophenol 42 gl 50 30- 130
Surrogate 2-Fluorobiphenyl 29 gl 50 30- 130
Surrogate 2-Fluorophenot 27 gl 50 15- 110
Surrogate Nitrobenzene- 30 gl 50 30- 130
Surrogate Phenol- 29 gl 50 15- 110
Surrogate Terpheny-d4 30 gl 50 30- 130
Surrogate 6- Tribromopheno 324 gl 50 15- 110
This laboratory report is lIot valid without all authorized sigllature 011 tlle cover page
Reportble Detection Limit BRL = Below Reporting Limit Page 17 of25
Semivolatie Organic Compounds by GC - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051106 - SW846 3510C
Blank S051106-BLK1
Prepared amp Analyzed 15-Mayshy
Aroclor- 1016 BRL gI 0200
Aroclor- 1016 (2C) BRL gI 0200
Aroclor- 1221 BRL gI 0200
Aroclor- 1221 (2C) BRL gI 0200
Aroclor- 1232 BRL gI 0200
Aroclor- 1232 (2Cj BRL gI 0200
Aroclor- 1242 BRL gI 0200
Aroclor-1242 (2C) BRL gI 0200
Aroclor- 1248 BRL gI 0200
Aroclor- 1248 (2C) BRL gI 0200
Aroclor- 1254 BRL gI 0200
Aroclor- 1254(2Cj BRL gI 0200
Aroclor- 1260 BRL gI 0200
Aroclor- 1260 (2C) BRL gI 0200
Aroclor- 1262 BRL gI 0200
Aroclor- 1262 (2C) BRL gI 0200
Aroclor-1268 BRL gI 0200
Aroclor- 1268 (2C) BRL gI 0200
Surrogate Decachlorobiphenyl (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0231 0224 0194 0191
gI
gI
gI
gI
0200 0200 0200 0200
116 112
30- 150 30- 150 30- 150 30- 150
LC5 8051106-B51
Prepared 15-May-08 Analyzed 16-May-08
Aroclor- 1016 265 gI 0200 250 106 50- 114
Aroclor- 1 016 (2C) 240 gI 0200 250 50- 114
Aroclor- 1260 0269 gI 0200 250 107 40- 127
Aroclor-1260 (2Cj 270 gI 0200 250 108 40- 127
Surrogate Decachlorobiphenyl (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0225 0224 0188 0183
gI
gI
gI
gI
0200 0200 0200 0200
113 112
30- 150 30- 150 30- 150 30- 150
LC5 DUD rS051106-B5D1
Prepared 15-May-08 Analyzed 16-Mayshy
Aroclor- 1016 262 gl 0200 250 105 50- 114
Aroclor-1 016 (2Cj 241 gI 0200 250 50- 114
Aroclor- 1260 277 gI 0200 250 111 40- 127
Aroclor- 1260(2Cj 0260 gI 0200 250 104 40- 127
Surrogate Decachlorobipheny (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0238 0218 0189 0181
gI
gI
gI
gI
0200 0200 0200 0200
119 109
30- 150 30- 150 30- 150 30- 150
This laboratory report is lot valid without (II authorized sigllature 01 the cover page
Page 18 of25 Reportable Detection Limit BRL = Below Reporting Limit
Extractable Petroleum Hydrocarbons - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051102 - SW846 3510C
Blank 8051102-BLK1
Prepared 15-May-08 Analyzed 19-Mayshy
Non-polar material (SGT- HEM) BRL m91
LC8 8051102-B81
Prepared 15-May-08 Analyzed 19-Mayshy
Non-polar material (SGT- HEM) 184 m91 21 81 904
This laboratory report is not valid without an authorized signature 011 the cover page
Page 19 of25 Reportable Detection Limit BRL = Below Reporting Limit
Soluble Metals by EPA 200 Series Methods - Quality Control
Analyte(s) Result Flag Units RDL
Spike
Level
Source
Result REC
REC
Limits RPD
RPD
Limit
Batch 8051150 - EPA 200 Series
Blank 8051150-BLK1
Prepared amp Analyzed 21-May-
Iron
Zinc
Selenium
Nickel
Chromium
Copper
Arsenic
BRL
BRL
BRL
BRL
BRL
BRL
BRL
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0150
0050
0150
0050
0050
0050
0040
LCS 8051150-BS1
Prepared amp Analyzed 21-May-
Selenium
Zinc
Iron
Nickel
Chromium
Arsenic
Copper
123
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0150
0050
0150
0050
0050
0040
0050
103
105
101
100
85- 115
85- 115
85- 115
85- 115
85- 115
85-115
85- 115
licate B051150-DUP1 Source SA7B602shy
Prepared amp Analyzed 21-May-
Iron
Zinc
Selenium
Nickel
Copper
Chromium
Arsenic
17
0162
BRL
0015
0017
BRL
0450
QR8
mgl
mgl
mgl
mgl
mgl
mgl
mgi
0150
0050
0150
0050
0050
0050
0040
184
0186
BRL
0014
0023
BRL
0468
Matrix S ike 8051150-MS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Iron
Selenium
Nickel
Zinc
Copper
Chromium
Arsenic
19 QM2 mgl
mgll
mgl
mgl
mgl
mgl
mgl
0150
0150
0050
0050
0050
0050
0040
125
184
BRL
0014
0186
0023
BRL
0468
104
105
102
70- 130
70- 130
70-130
70- 130
70- 130
70-130
70- 130
Post S ike 8051150-PS1 Source SA78602shy
Prepared amp Analyzed 21-May-
Zinc
Iron
Selenium
Nickel
Copper
Arsenic
Chromium
18 QM2
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0050
0150
0150
0050
0050
0040
0050
0186
184
BRL
0014
0023
0468
BRL
104
104
101
85- 115
85- 115
85- 115
85-115
85-115
85- 115
85-115
Batch 8051152 - EPA200SW7000 Series
Blank B051152-BLK1
Prepared amp Analyzed 21-May-
Mercury BRL mgl 00020
This laboratory report is IIOt valid witllOut all authorized sigllature 011 the coverpage
Page 20 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Soluble Metals by EPA 200 Series Methods - Quality Control
Analyte(s) Result Flag Units RDL
Spike
Level
Source
Result REC
REC
Limits RPD
RPD
Limit
Batch 8051152 - EPA200SW7000 Series
LCS B051152-BS1
Prepared amp Analyzed 21-May-
Mercury 00576 m91 00020 00500 115 85- 115
licate B051152-DUP1 Source SA78602-01
Prepared amp Analyzed 21-May-
Mercury BRL m91 00020 BRL
Matrix S ike 8051152-MS1 Source SA78602shy
Prepared amp Analyzed 21-May-
Mercury 00632 OM m91 00020 00500 BRL 126 75- 125
Post S ike 8051152-PS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Mercury 00624 OC1 m91 00020 00500 BRL 125 85- 115
Batch 8051249 - 2008No digestion
Blank 8051249-BLK1
Prepared amp Analyzed 21-May-
Lead
Antimony
Cadmium
Silver
BRL
BRL
BRL
BRL
m91
m91
m91
m91
0002
0002
0002
0002
LCS B051249-BS1
Prepared amp Analyzed 21-May-
Antimony
Lead
Silver
Cadmium
143
145 OC2
m91
m91
m91
m91
0050
0050
0050
0040
103
115
107
116
85- 115
85- 115
85- 115
85- 115
licate 8051249-DUP1 Source SA7B602shy
Prepared amp Analyzed 21- May-
Lead
Antimony
Cadmium
Silver
0009
0002
00005
00002
ORB
m91
m91
m91
m91
0002
0002
0002
0002
0011
0003
00005
00003
Matrix S ike 8051249-MS1 Source SA78602shy
Prepared amp Analyzed 21- May-
Lead
Antimony
Cadmium
Silver
142
m91
m91
m91
m91
0050
0050
0040
0050
0011
0003
00005
00003
111
101
114
102
70- 130
70-130
70c130
70- 130
Post S ike 8051249-PS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Antimony
Cadmium
Silver
38
OC2
m91
m91
m91
0050
0040
0050
125
0003
00005
00003
110
121
109
85- 115
85- 115
85- 115
This laboratory report is flOt valid IVithout all authorized signature 011 the cOIer page
Reportable Detection Limit BRL Below Reporting Limit Page 21 of 25
General Chemistry Parameters - Quality Control
Spike Source REC RPD
Analyte( s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051049 - General Preparation
Blank S051 049-BLK1
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
Blank S051049-BLK2
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
Blank S051 049-BLK3
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
LCS S051049-BS1
Prepared amp Analyzed 14-May-
Total Residual Chlorine 046 mgl 020 0500 90- 110
LCS S051049-BS2
Prepared amp Analyzed 14-May-
Total Residual Chlorine 047 mgl 020 0500 90- 110
LCS S051049-BS3
Prepared amp Analyzed 14-May-
Total Residual Chlorine 054 mgl 020 0500 108 90-110
licate B051049-DUP1 Source SA7S544shy
Prepared amp Analyzed 14-May-
Total Residual Chlorine 012 mgl 020 010
licate S051049-DUP2 Source SA7S602-01
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020 BRL
Matrix S ike 8051049-MS1 Source SA78544-01
Prepared amp Analyzed 14-May-
Total Residual Chlorine 065 mgl 020 0500 010 110 80- 120
Matrix S ike 8051049-MS2 Source SA7B602shy
Prepared amp Analyzed 14-May-
Total Residual Chlorine mgl 500 125 BRL 108 80- 120
Reference 8051 049-SRM1
Prepared amp Analyzed 14-May-
Total Residual Chlorine 100 mgl 020 0967 103 85-115
Batch 8051094 - General Preparation
Blank 8051094-BLK1
Prepared amp Analyzed 14 May-
Hexavalent Chromium (soluble) BRL mgl 005
Blank 8051 094-BLK2
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) BRL mgl 005
LCS 8051094-BS1
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) 054 mgl 005 90- 110
licate 8051094-DUP1 Source SA78602-01
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) BRL mgl 125 BRL
Thi laboratory report is not valid without all authorized sigllature 011 the cover page
Page 22 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Page 9
4 Treatm
ent system inform
ation Please describe the treatment system
using separate sheets as necessary including
a) A description of the treatm
ent system including a schem
atic of the proposed or existing treatment system
S
ee Figures 4 and 5
Frac tank Air stripper
Oilw
ater separator Equalization tanks
Bag filter rg
GA
C filter rg
b) Identity each applicable
treatment unit (check alJ
that apply)
Chlorination
Dechlorination
Other (please describe)
c) Proposed average and maxim
um flow
rates (gallons per minute) for the discharge and the design flow
rate(s) (gallons per minute) ofthe treatm
ent system
Average flow
rate of discharge 15 G
PM
Maxim
um flow
rate oftreatment system
0 G
PM
Design flow
rate of treatment system
0 G
PM
d) A description of chem
ical additives being used or planned to be used (attach MSD
S sheets) Not A
pplicable
5 Receiving surface water(s) Please provide information about the receiving water (s) using separate sheets as necessary including
Identity the discharge pathway
I Direct
I Within facility
I Stonn drain rg I R
iverbrook I W
etlands _ I Other (describe)
Provide a narrative description ofthe discharge pathway including the nam
e(s) of the receiving waters
Discharge to catchbasin and stonnw
ater drainage system in E
ast Broadw
ay which discharges to M
ahoney Brook (S
ee Figure 4)
c) Attach a detailed m
ap(s) indicating the site location and location of the outfall to the receiving water
1 For multiple discharges num
ber the discharges sequentialJy 2 For indirect dischargers indicate the location of the discharge to the indirect conveyance and the discharge to surface w
ater T
he map should also include the location and distance to the nearest sanitary sew
er as well as the locus of nearby sensitive receptors (based on U
SGS topographical
mapping) such as surface w
aters drinking water supplies and w
etland areas d) Provide the state w
ater quality classification of the receiving water
e) Provide the reported or calculated seven day- ten year low flow
(7QlO
) of the receiving water Jcfs
Please attach any calculation sheets used to support stream flow
and dilution calculations See A
ttachment B
f) Is the receiving water a listed 303(d) w
ater quality impaired or lim
ited water Y
es 0 No rg
If yes for which polJutant(s) N
A
Is there a TM
DL
Yes 0
No rg If yes for w
hich pollutant(s) NA
Rem
ediation General Perm
it - Notice of Intent
6 Results of C
onsultation with Federal Services Please p
rovide the following information according to requirements of Par
lBA
and A
ppendices II and VII
a) Are any listed threatened or endangered species or designated critical habitat in proxim
ity to the discharge Yes 0
No rg
Has any consultation w
ith the federal services been completed Y
es 0 No rg
or is consultation underway Y
es 0 No rg
What w
ere the results of the consultation with the U
S Fish and Wildlife Service andor N
ational Marine Fisheries Service (check one) N
ot applicable
a nojeopardy opinion
or written concurrenceD
on a finding that the discharges are not likely to adversely affect any endangered species or critical habitat
b) Are any historic properties listed or eligible for listing on the N
ational Register of H
istoric Places located on the facilty or site or in proximity to the discharge
Yes D
No
Have any state or tribal historic preservation offcer been consulted in this determ
ination (Massachusetts only) Y
es O N
o
7 SU
DD
lemental inform
ation
Please provide any supplemental information Attach any analytical data used to support the application A
ttach any celtification(s) required by the general permit
Attachm
ent A - Figures
Figure I - Site Locus M
ap
Figure 2 - MassD
EP Site Scoring M
ap
Figure 3 - Aerial M
ap
Figure 4 - Proposed Soil Excavation A
rea Map
Figure 5 - T
reatment S
ystem Line D
iagram
Attachm
ent B - D
ilution factor Calculations
Attachment C - L
aboratory Analytical R
eport Groundw
ater
Rem
ediation General Perm
it - Notice of 1ntenl
=-
including the following
8 Signature Requirements
The N
otice ofIntent must be signed by the operator in accordance w
ith the signatory requirements of 40 C
FR Section 122
certification
J certif under penalty of law that this docum
ent and all attachments w
ere prepared under my direction or supervision in accordance w
ith a system
designed to assure that qualifed personnel properly gather and evaluate the information subm
itted Based on m
y inquiry of the person or persons who
manage the system
or those persons directly responsible for gathering the information I certif that t
he information submitted
is to the best of m
y
knowledge and belief true accurate and com
plete J certif that I am aw
are that there are signifcant penalties for submitting false inform
ation including
the possibilty of fine and imprisonm
ent for knowing violations
FacilitySite Name
Form
er Speedw
ay Service S
tation 181 East B
roadwav G
ardner MA
01440
Operator signature
Title
Michael 1 D
ziura Sf Env E
ngineer
Date
4150- q
Rem
ediation General Perm
it - Notice of Intent
-
D- 0
0 0
il (J tu
Bw
o(0 -I
NJW
gQb
J(JZc o c
rou a -10
0 J 6shy
a 0
I-tDC
aJ Qj
E aJshy
ro ro ro
~~~ ~~~~- -- - _ - -_ - ~~~ ~~~~ ~~~ - - _- _- -- -- p __(
MA DEP - Bureau of Waste Site CleanupSITE NME Site S aP 5 MiFlII Former Speeway Station _-II181 Eat Broaday b b d IS I i I GARDNER MA 0144 v ri) i P f f 1 me- 1 5ylmI I L shy J --I 423315n 715835e SiteLocation y o oCop1odQcn Ofof W-_ l
1 1 I
r
r
iBARBER HILL
A c
Cf1 f o s
0
5
Roads Uned Acss Divd Mar Roed Conntor Street Track 1 EPA Sola Source Aquilar FEMA 100yaar iloodplain 0 c Puc Watar SLo GrunSelaceNon Corrty 0
Bounars lOwn Couny DE Region Tian Powerln Ine Aqedut ApprOld Zona2 tNPA Sue Wster Supp Zone A bStZ F--shy--rle
8os Mat Sub SUeor Porenrial Inermtent Man lvo8 Ste Dfm Hyro1apy Wmer FeatllePLio Suleee Wat S H-- L otlMds FrslSaltN-ES WeIMd Habat L
Potentia Prdutiv AqlJlers ModHig Yield Proteoted Opn Space ACC nIL c= Non-Potential Drng Water Sollce AIea ModumHi Yo1d ll DEP Pormrd SoidWes1 FsiIi6s cnifud Verne Pools f0
1I2 KIWUmR$ MtL
January 30 2004 SCALE 1 15000
-
LE
GE
ND
APX PROPER BONDA
- APPROXOiSPO SIT BOUNDA
-GR
OU
ND
WA
TE F1 D
IRE
cnON
SCA
LE
30 60 FE
(APR
OX
CORPORATE ENVIRONMENTAL
)i
AD
VISO
RS
INC
SC
AS SH
OW
D
R B
Y K
HA
EL
DA
TE
10407
JOB
NO
2920-96
AERIAL MAP
FO
RM
ER
SP
EE
DW
AY
ST
AT
ION
FlGURE -3
181 EA
BR
OA
AY
GA
NE
R fo
age 1 ot 1Streamflow Statistics Report
Streamstats Ungaged Site Report Date Wed Dec 31 2008 124908 Site Location Massachusetts NAD83 Latitude 425545 (42 3316) NAD83 Longitude -719758 (-71 58 32) NAD27 Latitude 425545 (423316) NAD27 Longitude - 9763 (-71 58 34) Drainage Area 502 mi2
IPeak Flow Basin Characteristics 1100 Statewide Low Flow (S02 mi2)
Regression Equation Valid Rang
I Min II Max1 Value III Parameter Drainage Area (square miles) 161 149
Mean Basin Slope from 250K DEM (percent) 032 24
Stratified Drift per Stream Length (square mile per mile) 129
Massachusetts Region (dimensionless)
Streamflow Statistics
gO-Percent Prediction Interval Prediction Error
MaximumStatistic Flow (ft s) (percent) Minimum
I D50 IIII 11 1811 II 24511 993
I D60 II 35511 2011 II 03611 35111 2411 II 041 I 201I D70 24111 2611 II 03811 151I D75 11 2811 II 0911 3761I D80 981I D85 1 I 3211 II o6311
1 I 3711 II 0441 1 2 2911 D90 11 4611 II 02411 15511 D95I D98 04511 6011 II 01511 11
I D99 03411 6511 II ol1ll 1021
5011 II 02611 11I M7D2Y 1111 3311 II odl 3 541
I AUGD50
IIIIIIIIIIIIIIIIIIIIII 0311 7111 II 0088411 0981I M7Dl0Y
1010
12312008httpstreamstatsagscrusgsgovgisimgReportsFlowStatsReport3494 - 2008123112498
Dilution Factor Calculation Former Speedway Service Station 181 East Broadway Gardner Ma
DF=(Od+Os)Od
DF = Dilution factor
Od = Max flow rate of discharge in cubic feet per second Os = receiving water flow in cubic feet per seconds 7010 flow rate Mahoney Brook 7010 = min flow for seven consecutive days with a recurrence interval of 10 years
7010 flow based on data obtained from USGS Steamflow Statistics Report Data attached
067
Semivolatile Organic Compounds by GCMS - Quality Control
Analyte( s)
Batch 8051216 - SW846 3510C
Blank 8051216BLK1)
Prepared amp Analyzed 16May-
Acenaphthene
Acenaphthylene
Aniline
Anthracene
AzobenzenelDi phenyld iazi ne
Benzidine
Benzo (a) anthracene
Benzo (a) pyrene
Benzo (b) fiuoranthene
Benzo (g i) perylene
Benzo (k) fiuoranthene
Benzoic acid
Benzyl alcohol
Bis(2-ch loroethoxy) methane
Bis(2-ch loroethyl)ether
Bis(2-ch loroi sopropyl)ether
Bis(2ethylhexyl) phthalate
Bromophenyl phenyl ether
Butyl benzyl phthalate
Carbazole
Ch loro-3-methyl phenol
Chloroaniline
Chloronaphthalene
Chlorophenol
Chlorophenyl phenyl ether
Chrysene
Dibenzo (a h) anthracene
Dibenzofuran
Dichlorobenzene
Dichlorobenzene
14- Dichlorobenzene
3 - Dichlorobenzidine
24-Dichlorophenol
Diethyl phthalate
Dimethyl phthalate
24- Dimethylphenol
Din-butyl phthalate
Dinitro-2-methylphenol
Dinitrophenol
Dinitrotoluene
Dinitrotoluene
Di-noctyl phthalate
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopehtadiene
Hexachloroethane
Indeno (1 cd) pyrene
Spike Source REC RPD
Result Flag Units RDL Level Result REC Limits RPD Limit
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gl
BRL gI
BRL gl
BRL gl
BRL gl
BRL gI
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gll
BRL gl
BRL gll
BRL gl
BRL gl
BRL gI
BRL gI
BRL gI
BRL gl
BRL gI
BRL gI
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gI
BRL gI
BRL gl
This laboratory report is IlOt valid without all authorized sigllature 011 the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page t4 of25
Volatie Organic Compounds - Quality Control
p (
Spike Source REC RPD
RDL Level Result REC Limits RPD Limit Analyte(s) Result Flag Units
Batch 8051244 - SW846 5030 Water MS
Matrix S ike Du 8051244-MSD1 Source SA78629shy
Prepared 16-May-08 Analyzed 17-May-BRL 106 251
Vinyl chloride 21 gl 20
101 70- 130 Surrogate 4-Bromofluorobenzene 50 gl 50
70- 13049 gl 50 111 70- 130
Surrogate Toluene-Surrogate 1 Dichloroethane- 55 gl 50
50 70- 130494 glSurrogate Dibromofluoromethane
Microextractable Organic Compounds - Quality Control
Spike Source REC RPD
Flag Units RDL Level Result REC Limits RPD Limit Analyte(s) Result
Batch 8051105 - SW846 3510C
Blank 8051105-BLK
Prepared amp Analyzed 15-May-
BRL gl 01001 Dibromoethane (ED B)
LCS 8051105-BS1
Prepared amp Analyzed 15-Mayshy50- 1500770 gl 0100 100
licate 8051105-DUP1 Source SA7B583shy
Prepared amp Analyzed 15-May-
BRL gl 0100 BRL
1 Dibromoethane (EDB)
1 Dibromoethane (EDB)
This laborntOlY report is not valid without an authorized signature 011 the cover page
Page 13 of2S Reportable Detection Limit BRL = Below Reporting Limit
Sam le Identification Client Pro ect Matrix Collection DateTime ReceivedMWshy
2920-96- Ground Water 13-May-081030 14-May-SA 78602shy
CAS No Analyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Volatile Organic Compounds
Volatile Or anic Com ounds b GCMS
Prepared by method SW846 5030 Water MS
123-91- Dioxane BRL 1-91 200 EPA 624 16-May-08 17-May-08 8051244
994-05-8 Ter-amyl methyl ether BRL 1-911 20
755- Tert-Butanoll butyl alcohol BRL 1-91 200
67-B4- Acetone BRL 1-91 400
71-43- Benzene BRL 1-91 20
75-27-4 Bromodichloromethane BRL 1-91 20
75-25- Bromoform BRL 1-91 20
74-83- Bromomethane BRL 1-91 40
78-93- Butanone (MEK) BRL 1-91 200
56-23- Carbon tetrachloride BRL 1-91 20
108-90- Chlorobenzene BRL 1-91 20
75-00- Chloroethane BRL 1-91 40
676- Chloroform BRL 1-91 20
74-87- Chloromethane BRL 1-91 40
124-48- Dibromochloromethane BRL 1-91 20
95-50- Dichlorobenzene BRL 1-911 20
541-73- Dichlorobenzene BRL 1-91 20
106-46- Dichlorobenzene BRL 1-91 20
75-34- 1- Dichloroethane BRL 1-91 20
107-06- Dichloroethane BRL 1-91 20
75-35-4 1- Dichloroethene BRL 1-91 20
156-59 cis- Dichloroethene BRL 1-91 20
156-60- trans- Dichloroethene BRL 1-91 20
78-87- 2- Dichloropropane BRL 1-91 20
10061-01-5 cis- Dichloropropene BRL 1-91 20
10061-02-B trans- Dichloropropene BRL 1-91 20
100-41-4 Ethylbenzene 411 1-911 20
591-78-B BRL 200Hexanone (MBK) 1-91
1634-04 -4 Methyl tert-butyl ether BRL 1-91 20
108-10- Methyl- pentanone (MIBK) BRL 1-91 200
75-09- Methylene chloride BRL 1-91 200
100-42- Styrene BRL 1-91 20
79-34- 1 Tetrachloroethane BRL 1-91 20
127- 18-4 T etrachloroethene BRL 1-91 20
108-88- Toluene BRL 1-91 20
71-55 1- Trichloroethane BRL 1-91 20
79-00- 2- Trichloroethane BRL 1-91 20
79-01-B Trichloroethene BRL 1-91 20
759-4 Trichlorofluoromethane (Freon 11) BRL 1-91 20
75-01-4 Vinyl chloride BRL 1-91 20
179601-23-1 m Xylene 390 1-91 40
95-47 Xylene 82 1-91 20
Surrogate recoveries 460-00- Bromofluorobenzene 70- 130
2037-26- Toluene- 100 70- 130
17060-07-0 1 Dichloroethane- 111 70- 130
1868-53- Dibromofluoromethane 70- 130
Microextractable Organic Compounds
106-93-4 1 Dibromoethane (EDB) BRL 1-91 0100 EPA 504 15-May- 15-May-08 8051105
Semivolatile Organic Compounds by GCMS
This laboratory report is not valid without all autllOrized signature 011 the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page 5 of 25
Sam le Identification Client Pro ect Matrix Collection DateTime Received
MWshy2920-96- Ground Water 13-May-081030 14-May-
SA 78602shy
CAS No Analyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Semivolatie Organic Compounds by GCMS
Semi volatile Or anic Com ounds b EPA 625
Prepared by method SW846 3510C 50 EPA 625 16-May- 19-May-08 805121683-32- Acenaphthene BRL IJgl
208-96-8 Acenaphthylene BRL IJgl 50
62-53- BRL IJgll 50Aniline
120- 12- Anthracene BRL 1J91 50
103-33- AzobenzenefDiphenyldiazine BRL IJgl 50
92-87 - Benzidine BRL IJgl 50
56-55- Benzo (a) anthracene BRL 1J91 50
50-32 - Benzo (a) pyrene IJglBRL 50
205-99- Benzo (b) fluoranthene BRL IJgl 50
191-24- Benzo (g i) perylene BRL IJgl 50
50207-08- Benzo (k) fluoranthene BRL IJgl
65-85 Benzoic acid BRL 1J91 50
100-51-6 Benzyl alcohol 1J91BRL 50
50111-91- Bis(2-chloroethoxy)methane BRL 1J91
111-4-4 Bis(2-chloroethyl)ether BRL IJgl 50
501 08-60- Bis(2-chloroisopropyl)ether BRL IJgl
117-81- Bis(2-ethylhexyl)phthalate BRL 1J91 50
101-55- Bromophenyl phenyl ether BRL IJgl 50
5085-68- Butyl benzyl phthalate BRL IJgl
5086-74- Carbazole BRL IJgl
5059-50- C hloro-3-methylphenol BRL IJgl
106-47- Chloroaniline BRL IJgl 50
91-58- Chloronaphthalene IJglBRL 50
5095-57 - Chlorophenol BRL 1J91
507005-72- Chlorophenyl phenyl ether BRL IJgl
216-01- Chrysene tJ91BRL 50
5053-70- Dibenzo (a h) anthracene BRL IJgl
50132-64- Dibenzofuran BRL IJgl
95-50- Dichlorobenzene IJglBRL 50
541-73- 13- Dichlorobenzene BRL IJgl 50
106-46- Dichlorobenzene 1J91BRL 50
5091-94- 3 - Dichlorobenzidine BRL IJgl
120-83- Dichlorophenol BRL IJgl 50
84-66- Diethyl phthalate BRL IJgl 50
131-11- Dimethyl phthalate BRL IJgll 50
105-67- Dimethylphenol BRL 1J91 50
5084-74- Di-n- butyl phthalate BRL 1J91
534-52 - Dinitro-2-methylphenol BRL IJgl 50
51-28- Dinitrophenol IJglBRL 50
50121-14- Dinitrotoluene BRL 1J91
606-20- Dinitrotoluene IJglBRL 50
50117-84-0 Di-n-octyl phthalate BRL IJgl
206-44-0 Fluoranthene 1J91BRL 50
BRL 50
50 86-73- Fluorene IJgi
118-74- Hexachlorobenzene BRL 1J91
87-68- Hexachlorobutadiene 1J91BRL 50
5077-47-4 Hexachlorocyclopentadiene BRL IJgl
67-72- Hexachloroethane IJglBRL 50
50193-39- Indeno (1 3-cd) pyrene BRL IJgl
5078-59- Isophorone BRL IJgl
Tfls laboratory report is not valid without all authorized signature 011 the coverpage
Page 6 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Sam le Identification Client Pro ect Matrix Collection DateTime ReceivedMWshy
2920-96- Ground Water I3-May-081030 14-May-SA 78602shy
CAS No Analyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Semivolatile Organic Compounds by GCMS
Semi volatile Or anic Com ounds b EPA 625
Prepared by method SW846 3510C
91-57 -6 Methylnaphthalene 367 1-91 50 EPA 625 16-May- 19-May-08 8051216
95-48- Methylphenol BRL 1-91 50
108-39-4 3 amp 4-Methylphenol BRL I-gl 100 106-44shy91-20- Naphthalene 247 1-91 50
88-74-4 Nitroaniline BRL 1-91 50
99-09- Nitroaniline BRL 1-91 50
100-01-6 Nitroaniline BRL 1-91 50
98-95- Nitrobenzene BRL 1-91 50
88-75- Nitrophenol BRL 1-91 50
100-02- Nitrophenol BRL 1-91 50
62-75- Nitrosodimethylamine BRL 1-91 50
621-64- N- Nitrosodi-n-propylamine BRL 1-91 50
86-30-6 Nitrosodiphenylamine BRL 1-91 50
87 -86- Pentachlorophenol BRL 1-91 50
85-0- Phenanthrene BRL 1-91 50
108-95- Phenol BRL 1-91 50
129-00-0 Pyrene BRL 1-91 50
110-86- Pyridine BRL 1-91 50
120-82- 4- Trichlorobenzene BRL 1-91 50
95-95- 5- Trichlorophenol BRL 1-91 50
88-06- 6- T richlorophenol BRL 1-91 50
Surrogate recoveries
321-60- Fluorobipheny 30- 130
367- 12- Fuorophenol 15- 110
4165-60- Nitrobenzene- 30- 130
4165-62- Pheno- 15- 110
1718-51- Terpheny-d4 30- 130
118- 79- 6- Tribromophenol 15- 110
Semivolatile Organic Compounds by GC
Pol chlorinated Bi hen ls b EPA 608
Prepared by method SW846 3510C
12674- 11-2 Aroclor- 1016 BRL 1-91 0650 EPA 608 15- May- 16-May-08 8051106
11104-28-2 Aroclor-1221 BRL IJgl 0650
11141-16-5 Aroclor- 1232 BRL 1-91 0650
53469-21-9 Aroclor- 1242 BRL 1-91 0650
12672-29-6 Aroclor- 1248 BRL 1-91 0650
11097-69-1 Aroclor- 1254 BRL 1-91 0650
11096-82-5 Aroclor -1260 BRL 1-91 0650
37324-23-5 Aroclor-1262 BRL 1-91 0650
11100-14-4 Aroclor-1268 BRL IJgl 0650
Surrogate recoveries
2051-24- Decachlorobipheny (Sr) 105 30- 150
10386-84-2 4 DB-Octafluorobiphenyl (Sr) 30- 150
Extractable Petroleum Hydrocarbons
mgl EPA 1664 Rev A 15-May- 19-May-08 8051102Non-polar material (SGT- HEM)
Soluble Metals by EPA 2006000 Series Metbods
Field Filtered NA EPA 200 73005A 15- May- 15-May-08 8051192Filtration
Soluble Metals by EPA 200 Series Methods
7440-22-4 Silver BRL mgl 0002 EPA 200 21-May- 27- May-08 8051249
This laboratory report is IlOt mlid without (II authorized signature on the cover page
Reportble Detection Limit BRL = Below Reporting Limit Page 7 of 25
Sam le Identification MW-
Client Pro ect 2920-96shy
Matrix Ground Water
Collection DateTime 13-May-08 1030
Received 14-May-
SA 78602shy
CAS No A nalyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Soluble Metals by EPA 200 Series Methods
7440-38shy Arsenic 0468 mg1 0040 EPA 200 21-Mayshy 21-May-08 80511 50
7440-43shy Cadmium BRL mg1 0002 EPA 200 21-May-088051249
7440-47shy Chromium BRL mg1 0050 EPA 200 21-May-088051150
7440-50-8 Copper BRL mg1 0050
7439-89-6 Iron 184 mg1 0150
7439-97-6 Mercury BRL mg1 00020 EPA 245 17470A 21-May-088051152
7440-02-0 Nickel BRL mg1 0050 EPA 200 21-May-088051150
7439-92shy Lead 0011 mg1 0002 EPA 200 21-May-088051249
7440-36-0 Antimony 0003 mg1 0002
7782-49shy Selenium BRL mg1 0150 EPA 200 21-May-08 8051150
7440-66-6 Zinc 0186 mgl 0050
General Chemistry Parameters
Filtration Completed NA Varies 14-Mayshy 14-May-08 8051095
18540-29-9 Hexavalent Chromium (soluble) BRL HT2 mg1 125 SM3500CrDI796A 14-Mayshy 14-May-08 8051094 R01 2013 2016
57-12shy Cyanide (total) BRL mg1 0100 EPA 3354 19-Mayshy 19-May-088051374
7782-50shy Total Residual Chlorine BRL CIHT mg1 500 Hach 8167 14-Mayshy 14-May-08 8051049 R01 1900 2001
Total Suspended Solids 580 mg1 25 SM2540D 16-Mayshy 16-May-08 8051275
This lahomtOlY report is not valid without an authorized signature on the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page 8 of 25
Volatie Organic Compounds - Quality Control
Analyte( s)
Batch 8051244 - SW846 5030 Water MS
Blank 8051244-BLK1
Prepared 16-May-08 Analyzed 17-May-
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromochloromethane
1 Dichlorobenzene
1 Dichlorobenzene
1 Dichlorobenzene
1-Dichloroethane
1 Dichloroethane
1 1-Dichloroethene
cis- Dichloroethene
trans- 1 Dichloroethene
1 Dichloropropane
cis- 1 Dichloropropene
trans- 1 Dichloropropene
Ethylbenzene
Hexanone (MBK)
Methyl tert-butyl ether
Methyl- pentanone (MIBK)
Methylene chloride
Styrene
2- Tetrachloroethane
Tetrachloroethene
Toluene
1- Trichloroethane
2- Trichloroethane
Trichloroethene
Trichlorofluoromethane (Freon 11)
Vinyl chloride
p-Xylene
Xylene
Surrogate 4-Bromofluorobenzene Surrogate Toluene-
Surrogate 1 Dichloroethane-Surrogate Dibromofluoromethane
LCS B051244-BS1
Prepared 16-May-08 Analyzed 17 -May-
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Spike Source REC RPD
Result Flag Units RDL Level Result REC Limits RPD Limit
BRL gl 20
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl 10
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gll
BRL gi
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl 10
BRL gll
BRL gll 10
BRL gl 10
BRL gll
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
41 gl 50 70- 130 49 gl 50 70- 130 59 gl 50 119 70- 130 52 gl 50 105 70- 130
QC2 jgl 20 70- 130
18 jgl 20 70- 130
192 jgl 20 35- 155
18 jgl 20 45- 169
19 jgl 20 242
This laboratOlY repol1 is lot valid without 011 authorized sigllature 011 the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page 9 of 25
Volatie Organic Compounds - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051244 - SW846 5030 Water MS
LC5 8051244B51
Prepared 16-May-08 Analyzed 17-May-
Butanone (MEK) 10 QC2 gl 20 70- 130
Carbon tetrachloride 204 gl 20 102 70- 140
Chlorobenzene 18 gl 20 70- 130
Chloroethane 164 gl 20 14-230
Chloroform 18 gll 20 51- 138
Chloromethane 21 gl 20 106 273
Dibromochloromethane 18 gl 20 53- 149
1 Dichlorobenzene 20 gl 20 104 18- 190
1 Dichlorobenzene 19 gl 20 59- 156
1 A-Dichlorobenzene 18 gl 20 18- 190
1- Dichloroethane 19 gl 20 59- 155
1 Dichloroethane 19 gl 20 49- 155
1-Dichloroethene 16 gl 20 70- 130
cis- 1 Dichloroethene 17 gl 20 70- 130
trans- 1 Dichloroethene 16 gll 20 54- 156
1 Dichloropropane 18 gl 20 210
cis- Dichloropropene 17 gl 20 227
trans- 1 Dichloropropene 17 gl 20 17- 183
Ethylbenzene 19 gl 20 37- 162
Hexanone (MBK) 124 QC2 gl 20 70- 130
Methyl tert-butyl ether 19 gl 20 70- 130
Methylshy pentanone (MIBK) 17 gl 20 70- 130
Methylene chloride 16 gl 20 221
Styrene 17 gl 20 70- 130
1 Tetrachloroethane 194 gl 20 46- 157
Tetrachloroethene 15 gl 20 64- 148
Toluene 18 gl 20 70- 130
1- Trichloroethane 20 gl 20 100 52- 162
2- Trichloroethane 18 gl 20 52- 150
Trichloroethene 17 gl 20 71- 157
Trichlorofluoromethane (Freon 11) 19 gl 20 17- 181
Vinyl chloride 21 gl 20 106 251
p-Xylene 39 gl 40 70- 130
Xylene 20 gl 20 102 70- 130
Surrogate 4-Bromofluorobenzene Surrogate Toluene-
Surrogate 1 Dichloroethane-Surrogate Dibromofluoromethane
52 49 56
49
gl
gl
gl
gl
50 50 50
50
105
112 100
70- 130 70- 130 70- 130 70- 130
LC5 DUD (8051244-B5D1
Prepared 16-May-08 Analyzed 17-May-
Acetone QC2 gl 20 70- 130
Benzene 18 gl 20 70- 130
Bromodichloromethane 18 gl 200 35- 155
Bromoform 17 gl 20 45- 169
Bromomethane 18 gl 20 242
Butanone (MEK) 11 QC2 1-91 20 70- 130
Carbon tetrachloride 20 gl 20 100 70- 140
Chlorobenzene 17 gl 20 70- 130
Chloroethane 15 1-91 20 14-230
Chloroform 18 1-91 20 51- 138
This laboratory report is aot valid without a1 authorized sig1ature 01 the cover page
Reportble Detection Limit BRL = Below Reporting Limit Page 10 of25
Volatie Organic Compounds - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051244 - SW846 5030 Water MS
LCS Dup 18051244-BSD1
Prepared 16-May-08 Analyzed 17-May-
Chloromethane 18 1-91 20 273
Dibromochloromethane 174 1-91 20 53- 149
Dichlorobenzene 20 1-91 20 100 18- 190
Dichlorobenzene 18 1-91 20 59- 156
Dichlorobenzene 18 1-91 20 18- 190
Dichloroethane 18 1-91 20 59- 155
Dichloroethane 19 1-91 20 49- 155
Dichloroethene 16 1-91 20 70- 130
cis- Dichloroethene 16 1-91 20 70- 130
trans- Dichloroethene 15 1-91 20 54- 156
Dichloropropane 17 1-91 20 210
cis- Dichloropropene 164 IJgl 20 227
trans- 1 Dichloropropene 164 I-gl 20 17- 183
Etlwlbenzene 18 IJgl 20 37- 162
Hexanone (MBK) 124 QC2 IJgl 20 70- 130
Methyl tert-butyl ether 184 1J91 20 70- 130
Methyl- pentanone (MIBK) 17 IJgl 20 70- 130
Methylene chloride 16 IJgl 20 221
Styrene 16 IJgl 20 70- 130
2- Tetrachloroethane 19 IJgl 20 46- 157
Tetrachloroethene 15 IJgl 20 64- 148
Toluene 17 IJgl 20 70- 130
1- Trichloroethane 19 1-91 20 52- 162
2- Trichloroethane 16 IJgl 20 52- 150
Trichloroethene 15 IJgl 20 71- 157
Trichlorofluoromethane (Freon 11) 17 IJgl 20 17- 181
Vinyl chloride 19 IJglI 20 251
p-Xylene 37 1J91 40 70- 130
Xylene 20 IJgl 20 100 70- 130
Surrogate 4-Bromofluorobenzene 51 IJgl 50 104 70- 130
Surrogate Toluene- 4B gl 50 70- 130
Surrogate 1 0ichloroethane- 53 IJgl 50 106 70- 130 Surrogate Oibromofluoromethane 50 1J9i 50 102 70- 130
Matrix S ike B051244-MS1 Source SA7B629shy
Prepared 16-May-08 Analyzed 17-May-
Benzene 18 20 BRL 70- 130IJgl
Bromodichloromethane 19 IJgl 20 BRL 35- 155
Bromoform 18 IJgl 20 BRL 45- 169
Bromomethane 16 IJgl 20 BRL 242
Carbon tetrachloride 21 IJgl 20 BRL 106 70- 140
Chlorobenzene 18 IJgl 20 BRL 70- 130
Chloroethane 16 IJgl 20 BRL 14-230
Chloroform 18 IJgl 20 BRL 51- 138
Chloromethane 19 IJgl 20 BRL 273
Dibromochloromethane 17 IJgl 20 BRL 53- 149
1 Dichlorobenzene 22 IJgl 20 BRL 112 18- 190
1 Dichlorobenzene 22 IJgl 20 BRL 110 59-156
1 Dichlorobenzene 21 IJgl 20 BRL 109 18- 190
1- Dichloroethane 19 IJgl 20 BRL 59- 155
1 Dichloroethane 18 IJgl 20 BRL 49- 155
This laboratory report is 110t mUd without an authorized signature on the covel page
Reportble Detection Limit BRL = Below Reporting Limit Page It of25
Volatile Organic Compounds - Quality Control
p
Spike Source REC RPD
Result REC imits RPD LimitAnalyte(s) Result Flag Units RDL Level
Batch 8051244 - SW846 5030 Water MS
Matrix ike S051244-MS1 Source SA7B629shy
Prepared 16-May-08 Analyzed 17-Mayshy
17 20 BRL 70- 130 1- Dichloroethene IJgl
16 20 BRL 54- 156trans- 1 Dichloroethene IJgl
21020 BRL1 Dichloropropane 17 1J91
cis- 1 Dichloropropene 17 IJgl 20 BRL 227
17- 183trans- 1 Dichloropropene 184 1J91 20 BRL
20 20 BRL 103 37- 162Ethylbenzene IJgl
15 20 BRL 221Methylene chloride IJgl
20 BRL 46- 1572- Tetrachloroethane 19 1J91
20 BRL 64- 148Tetrachloroethene 18 1J91
BRL 70- 130Toluene 18 1J91 20
105 52-1621- Trichloroethane 211 IJgl 20 BRL
18 20 BRL 52- 1502- Trichloroethane IJgl
17 20 BRL 71- 157Trichloroethene 1J91
20 BRL 17- 181Trichloroluoromethane (Freon 11) 194 IJgl
20 BRL 103 251Vinyl chloride 20 IJgl
102 70- 130Surrogate 4-Bromofluorobenzene 50 IJgl 50 50 70- 130Surrogate Toluene- 49 1J91
56 50 112 70- 130Surrogate 1 Dichloroethane- IJgl
50 100 70- 130Surrogate Dibromofluoromethane 50 IJgl
Matrix S ike Du S051244-MSD1 Source SA7S629shy
Prepared 16-May-08 Analyzed 17-Mayshy
18 20 BRL 70- 130Benzene IJgl
18 20 BRL 35- 155Bromodichloromethane IJgl
17 20 BRL 45- 169Bromoform IJgl
20 BRL 242Bromomethane 17 IJgl
20 BRL 103 70- 140Carbon tetrachloride 20 IJgl
18 20 BRL 70- 130Chlorobenzene 1J91
14-230Chloroethane 16 IJgl 20 BRL
20 51- 138Chloroform 184 IJgl BRL
Chloromethane 19 1J91 20 BRL 273
18 20 BRL 53- 149Dibromochloromethane 1J91
20 BRL 117 18- 190Dichlorobenzene 234 IJgl
20 BRL 112 59- 156Dichlorobenzene 22 IJgl
BRL 108 18- 190Dichlorobenzene 21 1J91 20
20 59- 1551 Dichloroethane 19 IJgl BRL
18 20 BRL 49- 155Dichloroethane IJgl
16 20 BRL 70- 130Dichloroethene IJgl
20 BRL 54- 156trans- Dichloroethene 154 1J91
20 BRL 210Dichloropropane 17 IJgl
0420 BRL 227cis- Dichloropropene 17 IJgl
17- 183trans- Dichloropropene 17 1J91 20 BRL
BRL 37- 162Ethylbenzene 20 1J91 20 102
Methylene chloride 15 IJgl 20 BRL 221
20 BRL 46- 1572- Tetrachloroethane 192 IJgl
20 BRL 64- 148 04Tetrachloroethene 18 IJgl
BRL 70- 130Toluene 184 1J91 20
52- 1621- Trichloroethane 20 IJgl 20 BRL 104
17 20 BRL 52- 1502- Trichloroethane IJgl
17 20 BRL 71- 157Trichloroethene IJgl
20 BRL 17-181Trichlorofluoromethane (Freon 11) 19 IJgl
This laboratory report is IIOt valid without all authorized sigllllture 011 the cover page
Page 12 of25 Reportble Detection Limit BRL = Below Reporting Limit
Semivolatile Organic Compounds by GCMS - Quality Control
Analyte(s)
Batch 8051216 - SW846 3510C
Blank 8051216-BLK1
Prepared amp Analyzed 16-May-
Isophorone
Methylnaphthalene
Methylphenol
3 amp 4-Methylphenol
Naphthalene
Nitroaniline
Nitroaniline
Nitroaniline
Nitrobenzene
Nitrophenol
Nitrophenol
Nitrosodimethylamine
N- N itrosodi-n-pro pyla mine
N itrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Pyridine
1 24-Trichlorobenzene
24 5- Trichlorophenol
246- Trichlorophenol
Surrogate 2-Fuorobipheny Surrogate 2-Fuoropheno Surrogate Nitrobenzene-Surrogate PhenoshySurrogate Terpheny-d4 Surrogate 6- Tribromopheno
LCS B051216-BS1
Prepared amp Analyzed 16-May-
Acenaphthene
Acenaphthylene
Aniline
Anthracene
AzobenzenelDi phenyld lazine
Benzidine
Benzo (a) anthracene
Benzo (a) pyrene
Benzo (b) fluoranthene
Benzo (g i) perylene
Benzo (k) fluoranthene
Benzoic acid
Benzyl alcohol
B is(2-chloroethoxy)methane
B i s (2-ch loroethyl)eth e r
Bis(2-ch loroisopropyl) ether
B is(2-ethy Ih exyl) phtha late
Bromophenyl phenyl ether
Butyl benzyl phthalate
Carbazole
Spike Source REC RPD
Result Flag Units RDL Level Result REC Limits RPD Limit
BRL gl
BRL gl
BRL gl
BRL gl 10
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gll
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
370 gl 50 30- 130 40 gl 50 15- 110 39 gl 50 30- 130 43 gl 50 15- 110 36 gl 50 30- 130 40 gl 50 15- 110
41 gl 50 40- 140
43 gI 50 40- 140
41 gl 50 40- 140
38 gl 50 40- 140
45 gl 50 40- 140
49 gl 50 153
41 gl 50 40- 140
43 gl 50 40- 140
41 gl 50 40- 140
41 gll 50 40- 140
45 gl 50 40- 140
32 gl 50 12- 149
41 gl 50 40- 140
39 gl 50 40- 140
384 gl 50 40- 140
47 gl 50 40- 140
47 gl 50 40- 140
40 gl 50 40- 140
47 gI 50 40- 140
56 gI 50 112 200
This laboratory report is lIot valid witllOut a1l authorized sigllature 011 the coverpage
Reportble Detection Limit BRL = Below Reporting Limit Page 15 of25
Semivolatile Organic Compounds by GCMS - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051216 - SW846 3510C
LCS 8051216-BS1
Prepared amp Analyzed 16-Mayshy
50 30- 1304 -C hloro-3-methylphenol 42 IJgl
40- 140Chloroaniline 39 IJgl 50
Chloronaphthalene 37 IJgl 50 40- 140
Chlorophenol 37 IJgl 50 30- 130
50 40- 140
40- 140
Chlorophenyl phenyl ether 45 IJgl
Chrysene 43 IJgl 50
Dibenzo (a h) anthracene 43 IJgl 50 40- 140
Dibenzofuran IJgl38 50 40- 140
50 40- 1401 Dichlorobenzene 35 IJgl
40- 1401 Dichlorobenzene 264 IJgl 50
40- 1401 Dichlorobenzene 434 IJgl 50
58 50 116 40- 1403 - Dichlorobenzidine IJgl
50 30- 130
40- 140 24-Dichlorophenol 38 IJgl
Diethyl phthalate 484 IJgl 50
50 40- 140Dimethyl phthalate 464 IJgl
Dlmethylphenol 39 IJgl 50 30- 130
DI-n-butyl phthalate 44 IJgll 50 40- 140
30- 130 6-Di nitro- 2-methylphenol 38 1J91 50
30- 130Dinltrophenol 36 1J91 50
42 50 40- 14024-Dlnitrotoluene 1J91
Dlnitrotoluene 1J9141 50 40- 140
Di-n-octyl phthalate 52 IJgl 50 104 40- 140
40- 140Fluoranthene 40 IJgl 50
Fluorene 41 IJgl 50 40- 140
39 50 40- 140Hexachlorobenzene IJgl
50 40- 140Hexachlorobutadiene 40 IJgl
40- 140Hexach lorocyclopentad iene 294 IJgl 50
40 50 40- 140Hexachloroethane IJgl
42 50 40-140Indeno (1 3-cd) pyrene IJgl
50 40- 140Isophorone 40 IJgl
40- 140Methylnaphthalene 394 IJgl 50
40- 140Methylphenol 39 IJgl 50
40 10 50 40- 1403 amp 4-Methylphenol IJgl
37 50 40-140Naphthalene IJgl
50 40-140Nitroaniline 39 IJgl
Nitroaniline 51 IJgl 50 102 40- 140
48 50 40- 140Nltroaniline 1J91
50 40- 140Nitrobenzene 40 IJgl
30- 130Nitrophenol 36 IJgl 50
40 IJgl 50 30- 130Nitrophenol 40- 140Nitrosodimethylamine 32 1J91 50
50 40-140N- N itrosodi-n-propyla mine 46 IJgl
40- 140N itrosodi phenyla ml ne 44 IJgl 50
41 IJgl 50 30- 130Pentachlorophenol 40- 140Phenanthrene 38 IJgl 50
50 30- 130Phenol 38 IJgl
40- 140Pyrene 424 1J91 50
40- 140Pyridine 294 1J91 50
40- 14024- Trichlorobenzene 364 IJgl 50
This laboratory report is not mlid without an authorized signature 011 the cover page
Page 16 of25 Reportble Detection Limit BRL = Below Reporting Limit
Semivolatie Organic Compounds by GCMS - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
BMch 8051216 - SW846 3510C
LC5 8051216-851
Prepared amp Analyzed 16-Mayshy
24 5- Trichlorophenol 404 gl 50 30- 130
246- Trichlorophenol 42 gl 50 30- 130
Surrogate 2-Fluorobiphenyl 29 gl 50 30- 130
Surrogate 2-Fluorophenot 27 gl 50 15- 110
Surrogate Nitrobenzene- 30 gl 50 30- 130
Surrogate Phenol- 29 gl 50 15- 110
Surrogate Terpheny-d4 30 gl 50 30- 130
Surrogate 6- Tribromopheno 324 gl 50 15- 110
This laboratory report is lIot valid without all authorized sigllature 011 tlle cover page
Reportble Detection Limit BRL = Below Reporting Limit Page 17 of25
Semivolatie Organic Compounds by GC - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051106 - SW846 3510C
Blank S051106-BLK1
Prepared amp Analyzed 15-Mayshy
Aroclor- 1016 BRL gI 0200
Aroclor- 1016 (2C) BRL gI 0200
Aroclor- 1221 BRL gI 0200
Aroclor- 1221 (2C) BRL gI 0200
Aroclor- 1232 BRL gI 0200
Aroclor- 1232 (2Cj BRL gI 0200
Aroclor- 1242 BRL gI 0200
Aroclor-1242 (2C) BRL gI 0200
Aroclor- 1248 BRL gI 0200
Aroclor- 1248 (2C) BRL gI 0200
Aroclor- 1254 BRL gI 0200
Aroclor- 1254(2Cj BRL gI 0200
Aroclor- 1260 BRL gI 0200
Aroclor- 1260 (2C) BRL gI 0200
Aroclor- 1262 BRL gI 0200
Aroclor- 1262 (2C) BRL gI 0200
Aroclor-1268 BRL gI 0200
Aroclor- 1268 (2C) BRL gI 0200
Surrogate Decachlorobiphenyl (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0231 0224 0194 0191
gI
gI
gI
gI
0200 0200 0200 0200
116 112
30- 150 30- 150 30- 150 30- 150
LC5 8051106-B51
Prepared 15-May-08 Analyzed 16-May-08
Aroclor- 1016 265 gI 0200 250 106 50- 114
Aroclor- 1 016 (2C) 240 gI 0200 250 50- 114
Aroclor- 1260 0269 gI 0200 250 107 40- 127
Aroclor-1260 (2Cj 270 gI 0200 250 108 40- 127
Surrogate Decachlorobiphenyl (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0225 0224 0188 0183
gI
gI
gI
gI
0200 0200 0200 0200
113 112
30- 150 30- 150 30- 150 30- 150
LC5 DUD rS051106-B5D1
Prepared 15-May-08 Analyzed 16-Mayshy
Aroclor- 1016 262 gl 0200 250 105 50- 114
Aroclor-1 016 (2Cj 241 gI 0200 250 50- 114
Aroclor- 1260 277 gI 0200 250 111 40- 127
Aroclor- 1260(2Cj 0260 gI 0200 250 104 40- 127
Surrogate Decachlorobipheny (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0238 0218 0189 0181
gI
gI
gI
gI
0200 0200 0200 0200
119 109
30- 150 30- 150 30- 150 30- 150
This laboratory report is lot valid without (II authorized sigllature 01 the cover page
Page 18 of25 Reportable Detection Limit BRL = Below Reporting Limit
Extractable Petroleum Hydrocarbons - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051102 - SW846 3510C
Blank 8051102-BLK1
Prepared 15-May-08 Analyzed 19-Mayshy
Non-polar material (SGT- HEM) BRL m91
LC8 8051102-B81
Prepared 15-May-08 Analyzed 19-Mayshy
Non-polar material (SGT- HEM) 184 m91 21 81 904
This laboratory report is not valid without an authorized signature 011 the cover page
Page 19 of25 Reportable Detection Limit BRL = Below Reporting Limit
Soluble Metals by EPA 200 Series Methods - Quality Control
Analyte(s) Result Flag Units RDL
Spike
Level
Source
Result REC
REC
Limits RPD
RPD
Limit
Batch 8051150 - EPA 200 Series
Blank 8051150-BLK1
Prepared amp Analyzed 21-May-
Iron
Zinc
Selenium
Nickel
Chromium
Copper
Arsenic
BRL
BRL
BRL
BRL
BRL
BRL
BRL
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0150
0050
0150
0050
0050
0050
0040
LCS 8051150-BS1
Prepared amp Analyzed 21-May-
Selenium
Zinc
Iron
Nickel
Chromium
Arsenic
Copper
123
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0150
0050
0150
0050
0050
0040
0050
103
105
101
100
85- 115
85- 115
85- 115
85- 115
85- 115
85-115
85- 115
licate B051150-DUP1 Source SA7B602shy
Prepared amp Analyzed 21-May-
Iron
Zinc
Selenium
Nickel
Copper
Chromium
Arsenic
17
0162
BRL
0015
0017
BRL
0450
QR8
mgl
mgl
mgl
mgl
mgl
mgl
mgi
0150
0050
0150
0050
0050
0050
0040
184
0186
BRL
0014
0023
BRL
0468
Matrix S ike 8051150-MS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Iron
Selenium
Nickel
Zinc
Copper
Chromium
Arsenic
19 QM2 mgl
mgll
mgl
mgl
mgl
mgl
mgl
0150
0150
0050
0050
0050
0050
0040
125
184
BRL
0014
0186
0023
BRL
0468
104
105
102
70- 130
70- 130
70-130
70- 130
70- 130
70-130
70- 130
Post S ike 8051150-PS1 Source SA78602shy
Prepared amp Analyzed 21-May-
Zinc
Iron
Selenium
Nickel
Copper
Arsenic
Chromium
18 QM2
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0050
0150
0150
0050
0050
0040
0050
0186
184
BRL
0014
0023
0468
BRL
104
104
101
85- 115
85- 115
85- 115
85-115
85-115
85- 115
85-115
Batch 8051152 - EPA200SW7000 Series
Blank B051152-BLK1
Prepared amp Analyzed 21-May-
Mercury BRL mgl 00020
This laboratory report is IIOt valid witllOut all authorized sigllature 011 the coverpage
Page 20 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Soluble Metals by EPA 200 Series Methods - Quality Control
Analyte(s) Result Flag Units RDL
Spike
Level
Source
Result REC
REC
Limits RPD
RPD
Limit
Batch 8051152 - EPA200SW7000 Series
LCS B051152-BS1
Prepared amp Analyzed 21-May-
Mercury 00576 m91 00020 00500 115 85- 115
licate B051152-DUP1 Source SA78602-01
Prepared amp Analyzed 21-May-
Mercury BRL m91 00020 BRL
Matrix S ike 8051152-MS1 Source SA78602shy
Prepared amp Analyzed 21-May-
Mercury 00632 OM m91 00020 00500 BRL 126 75- 125
Post S ike 8051152-PS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Mercury 00624 OC1 m91 00020 00500 BRL 125 85- 115
Batch 8051249 - 2008No digestion
Blank 8051249-BLK1
Prepared amp Analyzed 21-May-
Lead
Antimony
Cadmium
Silver
BRL
BRL
BRL
BRL
m91
m91
m91
m91
0002
0002
0002
0002
LCS B051249-BS1
Prepared amp Analyzed 21-May-
Antimony
Lead
Silver
Cadmium
143
145 OC2
m91
m91
m91
m91
0050
0050
0050
0040
103
115
107
116
85- 115
85- 115
85- 115
85- 115
licate 8051249-DUP1 Source SA7B602shy
Prepared amp Analyzed 21- May-
Lead
Antimony
Cadmium
Silver
0009
0002
00005
00002
ORB
m91
m91
m91
m91
0002
0002
0002
0002
0011
0003
00005
00003
Matrix S ike 8051249-MS1 Source SA78602shy
Prepared amp Analyzed 21- May-
Lead
Antimony
Cadmium
Silver
142
m91
m91
m91
m91
0050
0050
0040
0050
0011
0003
00005
00003
111
101
114
102
70- 130
70-130
70c130
70- 130
Post S ike 8051249-PS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Antimony
Cadmium
Silver
38
OC2
m91
m91
m91
0050
0040
0050
125
0003
00005
00003
110
121
109
85- 115
85- 115
85- 115
This laboratory report is flOt valid IVithout all authorized signature 011 the cOIer page
Reportable Detection Limit BRL Below Reporting Limit Page 21 of 25
General Chemistry Parameters - Quality Control
Spike Source REC RPD
Analyte( s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051049 - General Preparation
Blank S051 049-BLK1
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
Blank S051049-BLK2
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
Blank S051 049-BLK3
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
LCS S051049-BS1
Prepared amp Analyzed 14-May-
Total Residual Chlorine 046 mgl 020 0500 90- 110
LCS S051049-BS2
Prepared amp Analyzed 14-May-
Total Residual Chlorine 047 mgl 020 0500 90- 110
LCS S051049-BS3
Prepared amp Analyzed 14-May-
Total Residual Chlorine 054 mgl 020 0500 108 90-110
licate B051049-DUP1 Source SA7S544shy
Prepared amp Analyzed 14-May-
Total Residual Chlorine 012 mgl 020 010
licate S051049-DUP2 Source SA7S602-01
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020 BRL
Matrix S ike 8051049-MS1 Source SA78544-01
Prepared amp Analyzed 14-May-
Total Residual Chlorine 065 mgl 020 0500 010 110 80- 120
Matrix S ike 8051049-MS2 Source SA7B602shy
Prepared amp Analyzed 14-May-
Total Residual Chlorine mgl 500 125 BRL 108 80- 120
Reference 8051 049-SRM1
Prepared amp Analyzed 14-May-
Total Residual Chlorine 100 mgl 020 0967 103 85-115
Batch 8051094 - General Preparation
Blank 8051094-BLK1
Prepared amp Analyzed 14 May-
Hexavalent Chromium (soluble) BRL mgl 005
Blank 8051 094-BLK2
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) BRL mgl 005
LCS 8051094-BS1
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) 054 mgl 005 90- 110
licate 8051094-DUP1 Source SA78602-01
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) BRL mgl 125 BRL
Thi laboratory report is not valid without all authorized sigllature 011 the cover page
Page 22 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Page 10
6 Results of C
onsultation with Federal Services Please p
rovide the following information according to requirements of Par
lBA
and A
ppendices II and VII
a) Are any listed threatened or endangered species or designated critical habitat in proxim
ity to the discharge Yes 0
No rg
Has any consultation w
ith the federal services been completed Y
es 0 No rg
or is consultation underway Y
es 0 No rg
What w
ere the results of the consultation with the U
S Fish and Wildlife Service andor N
ational Marine Fisheries Service (check one) N
ot applicable
a nojeopardy opinion
or written concurrenceD
on a finding that the discharges are not likely to adversely affect any endangered species or critical habitat
b) Are any historic properties listed or eligible for listing on the N
ational Register of H
istoric Places located on the facilty or site or in proximity to the discharge
Yes D
No
Have any state or tribal historic preservation offcer been consulted in this determ
ination (Massachusetts only) Y
es O N
o
7 SU
DD
lemental inform
ation
Please provide any supplemental information Attach any analytical data used to support the application A
ttach any celtification(s) required by the general permit
Attachm
ent A - Figures
Figure I - Site Locus M
ap
Figure 2 - MassD
EP Site Scoring M
ap
Figure 3 - Aerial M
ap
Figure 4 - Proposed Soil Excavation A
rea Map
Figure 5 - T
reatment S
ystem Line D
iagram
Attachm
ent B - D
ilution factor Calculations
Attachment C - L
aboratory Analytical R
eport Groundw
ater
Rem
ediation General Perm
it - Notice of 1ntenl
=-
including the following
8 Signature Requirements
The N
otice ofIntent must be signed by the operator in accordance w
ith the signatory requirements of 40 C
FR Section 122
certification
J certif under penalty of law that this docum
ent and all attachments w
ere prepared under my direction or supervision in accordance w
ith a system
designed to assure that qualifed personnel properly gather and evaluate the information subm
itted Based on m
y inquiry of the person or persons who
manage the system
or those persons directly responsible for gathering the information I certif that t
he information submitted
is to the best of m
y
knowledge and belief true accurate and com
plete J certif that I am aw
are that there are signifcant penalties for submitting false inform
ation including
the possibilty of fine and imprisonm
ent for knowing violations
FacilitySite Name
Form
er Speedw
ay Service S
tation 181 East B
roadwav G
ardner MA
01440
Operator signature
Title
Michael 1 D
ziura Sf Env E
ngineer
Date
4150- q
Rem
ediation General Perm
it - Notice of Intent
-
D- 0
0 0
il (J tu
Bw
o(0 -I
NJW
gQb
J(JZc o c
rou a -10
0 J 6shy
a 0
I-tDC
aJ Qj
E aJshy
ro ro ro
~~~ ~~~~- -- - _ - -_ - ~~~ ~~~~ ~~~ - - _- _- -- -- p __(
MA DEP - Bureau of Waste Site CleanupSITE NME Site S aP 5 MiFlII Former Speeway Station _-II181 Eat Broaday b b d IS I i I GARDNER MA 0144 v ri) i P f f 1 me- 1 5ylmI I L shy J --I 423315n 715835e SiteLocation y o oCop1odQcn Ofof W-_ l
1 1 I
r
r
iBARBER HILL
A c
Cf1 f o s
0
5
Roads Uned Acss Divd Mar Roed Conntor Street Track 1 EPA Sola Source Aquilar FEMA 100yaar iloodplain 0 c Puc Watar SLo GrunSelaceNon Corrty 0
Bounars lOwn Couny DE Region Tian Powerln Ine Aqedut ApprOld Zona2 tNPA Sue Wster Supp Zone A bStZ F--shy--rle
8os Mat Sub SUeor Porenrial Inermtent Man lvo8 Ste Dfm Hyro1apy Wmer FeatllePLio Suleee Wat S H-- L otlMds FrslSaltN-ES WeIMd Habat L
Potentia Prdutiv AqlJlers ModHig Yield Proteoted Opn Space ACC nIL c= Non-Potential Drng Water Sollce AIea ModumHi Yo1d ll DEP Pormrd SoidWes1 FsiIi6s cnifud Verne Pools f0
1I2 KIWUmR$ MtL
January 30 2004 SCALE 1 15000
-
LE
GE
ND
APX PROPER BONDA
- APPROXOiSPO SIT BOUNDA
-GR
OU
ND
WA
TE F1 D
IRE
cnON
SCA
LE
30 60 FE
(APR
OX
CORPORATE ENVIRONMENTAL
)i
AD
VISO
RS
INC
SC
AS SH
OW
D
R B
Y K
HA
EL
DA
TE
10407
JOB
NO
2920-96
AERIAL MAP
FO
RM
ER
SP
EE
DW
AY
ST
AT
ION
FlGURE -3
181 EA
BR
OA
AY
GA
NE
R fo
age 1 ot 1Streamflow Statistics Report
Streamstats Ungaged Site Report Date Wed Dec 31 2008 124908 Site Location Massachusetts NAD83 Latitude 425545 (42 3316) NAD83 Longitude -719758 (-71 58 32) NAD27 Latitude 425545 (423316) NAD27 Longitude - 9763 (-71 58 34) Drainage Area 502 mi2
IPeak Flow Basin Characteristics 1100 Statewide Low Flow (S02 mi2)
Regression Equation Valid Rang
I Min II Max1 Value III Parameter Drainage Area (square miles) 161 149
Mean Basin Slope from 250K DEM (percent) 032 24
Stratified Drift per Stream Length (square mile per mile) 129
Massachusetts Region (dimensionless)
Streamflow Statistics
gO-Percent Prediction Interval Prediction Error
MaximumStatistic Flow (ft s) (percent) Minimum
I D50 IIII 11 1811 II 24511 993
I D60 II 35511 2011 II 03611 35111 2411 II 041 I 201I D70 24111 2611 II 03811 151I D75 11 2811 II 0911 3761I D80 981I D85 1 I 3211 II o6311
1 I 3711 II 0441 1 2 2911 D90 11 4611 II 02411 15511 D95I D98 04511 6011 II 01511 11
I D99 03411 6511 II ol1ll 1021
5011 II 02611 11I M7D2Y 1111 3311 II odl 3 541
I AUGD50
IIIIIIIIIIIIIIIIIIIIII 0311 7111 II 0088411 0981I M7Dl0Y
1010
12312008httpstreamstatsagscrusgsgovgisimgReportsFlowStatsReport3494 - 2008123112498
Dilution Factor Calculation Former Speedway Service Station 181 East Broadway Gardner Ma
DF=(Od+Os)Od
DF = Dilution factor
Od = Max flow rate of discharge in cubic feet per second Os = receiving water flow in cubic feet per seconds 7010 flow rate Mahoney Brook 7010 = min flow for seven consecutive days with a recurrence interval of 10 years
7010 flow based on data obtained from USGS Steamflow Statistics Report Data attached
067
Semivolatile Organic Compounds by GCMS - Quality Control
Analyte( s)
Batch 8051216 - SW846 3510C
Blank 8051216BLK1)
Prepared amp Analyzed 16May-
Acenaphthene
Acenaphthylene
Aniline
Anthracene
AzobenzenelDi phenyld iazi ne
Benzidine
Benzo (a) anthracene
Benzo (a) pyrene
Benzo (b) fiuoranthene
Benzo (g i) perylene
Benzo (k) fiuoranthene
Benzoic acid
Benzyl alcohol
Bis(2-ch loroethoxy) methane
Bis(2-ch loroethyl)ether
Bis(2-ch loroi sopropyl)ether
Bis(2ethylhexyl) phthalate
Bromophenyl phenyl ether
Butyl benzyl phthalate
Carbazole
Ch loro-3-methyl phenol
Chloroaniline
Chloronaphthalene
Chlorophenol
Chlorophenyl phenyl ether
Chrysene
Dibenzo (a h) anthracene
Dibenzofuran
Dichlorobenzene
Dichlorobenzene
14- Dichlorobenzene
3 - Dichlorobenzidine
24-Dichlorophenol
Diethyl phthalate
Dimethyl phthalate
24- Dimethylphenol
Din-butyl phthalate
Dinitro-2-methylphenol
Dinitrophenol
Dinitrotoluene
Dinitrotoluene
Di-noctyl phthalate
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopehtadiene
Hexachloroethane
Indeno (1 cd) pyrene
Spike Source REC RPD
Result Flag Units RDL Level Result REC Limits RPD Limit
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gl
BRL gI
BRL gl
BRL gl
BRL gl
BRL gI
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gll
BRL gl
BRL gll
BRL gl
BRL gl
BRL gI
BRL gI
BRL gI
BRL gl
BRL gI
BRL gI
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gI
BRL gI
BRL gl
This laboratory report is IlOt valid without all authorized sigllature 011 the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page t4 of25
Volatie Organic Compounds - Quality Control
p (
Spike Source REC RPD
RDL Level Result REC Limits RPD Limit Analyte(s) Result Flag Units
Batch 8051244 - SW846 5030 Water MS
Matrix S ike Du 8051244-MSD1 Source SA78629shy
Prepared 16-May-08 Analyzed 17-May-BRL 106 251
Vinyl chloride 21 gl 20
101 70- 130 Surrogate 4-Bromofluorobenzene 50 gl 50
70- 13049 gl 50 111 70- 130
Surrogate Toluene-Surrogate 1 Dichloroethane- 55 gl 50
50 70- 130494 glSurrogate Dibromofluoromethane
Microextractable Organic Compounds - Quality Control
Spike Source REC RPD
Flag Units RDL Level Result REC Limits RPD Limit Analyte(s) Result
Batch 8051105 - SW846 3510C
Blank 8051105-BLK
Prepared amp Analyzed 15-May-
BRL gl 01001 Dibromoethane (ED B)
LCS 8051105-BS1
Prepared amp Analyzed 15-Mayshy50- 1500770 gl 0100 100
licate 8051105-DUP1 Source SA7B583shy
Prepared amp Analyzed 15-May-
BRL gl 0100 BRL
1 Dibromoethane (EDB)
1 Dibromoethane (EDB)
This laborntOlY report is not valid without an authorized signature 011 the cover page
Page 13 of2S Reportable Detection Limit BRL = Below Reporting Limit
Sam le Identification Client Pro ect Matrix Collection DateTime ReceivedMWshy
2920-96- Ground Water 13-May-081030 14-May-SA 78602shy
CAS No Analyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Volatile Organic Compounds
Volatile Or anic Com ounds b GCMS
Prepared by method SW846 5030 Water MS
123-91- Dioxane BRL 1-91 200 EPA 624 16-May-08 17-May-08 8051244
994-05-8 Ter-amyl methyl ether BRL 1-911 20
755- Tert-Butanoll butyl alcohol BRL 1-91 200
67-B4- Acetone BRL 1-91 400
71-43- Benzene BRL 1-91 20
75-27-4 Bromodichloromethane BRL 1-91 20
75-25- Bromoform BRL 1-91 20
74-83- Bromomethane BRL 1-91 40
78-93- Butanone (MEK) BRL 1-91 200
56-23- Carbon tetrachloride BRL 1-91 20
108-90- Chlorobenzene BRL 1-91 20
75-00- Chloroethane BRL 1-91 40
676- Chloroform BRL 1-91 20
74-87- Chloromethane BRL 1-91 40
124-48- Dibromochloromethane BRL 1-91 20
95-50- Dichlorobenzene BRL 1-911 20
541-73- Dichlorobenzene BRL 1-91 20
106-46- Dichlorobenzene BRL 1-91 20
75-34- 1- Dichloroethane BRL 1-91 20
107-06- Dichloroethane BRL 1-91 20
75-35-4 1- Dichloroethene BRL 1-91 20
156-59 cis- Dichloroethene BRL 1-91 20
156-60- trans- Dichloroethene BRL 1-91 20
78-87- 2- Dichloropropane BRL 1-91 20
10061-01-5 cis- Dichloropropene BRL 1-91 20
10061-02-B trans- Dichloropropene BRL 1-91 20
100-41-4 Ethylbenzene 411 1-911 20
591-78-B BRL 200Hexanone (MBK) 1-91
1634-04 -4 Methyl tert-butyl ether BRL 1-91 20
108-10- Methyl- pentanone (MIBK) BRL 1-91 200
75-09- Methylene chloride BRL 1-91 200
100-42- Styrene BRL 1-91 20
79-34- 1 Tetrachloroethane BRL 1-91 20
127- 18-4 T etrachloroethene BRL 1-91 20
108-88- Toluene BRL 1-91 20
71-55 1- Trichloroethane BRL 1-91 20
79-00- 2- Trichloroethane BRL 1-91 20
79-01-B Trichloroethene BRL 1-91 20
759-4 Trichlorofluoromethane (Freon 11) BRL 1-91 20
75-01-4 Vinyl chloride BRL 1-91 20
179601-23-1 m Xylene 390 1-91 40
95-47 Xylene 82 1-91 20
Surrogate recoveries 460-00- Bromofluorobenzene 70- 130
2037-26- Toluene- 100 70- 130
17060-07-0 1 Dichloroethane- 111 70- 130
1868-53- Dibromofluoromethane 70- 130
Microextractable Organic Compounds
106-93-4 1 Dibromoethane (EDB) BRL 1-91 0100 EPA 504 15-May- 15-May-08 8051105
Semivolatile Organic Compounds by GCMS
This laboratory report is not valid without all autllOrized signature 011 the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page 5 of 25
Sam le Identification Client Pro ect Matrix Collection DateTime Received
MWshy2920-96- Ground Water 13-May-081030 14-May-
SA 78602shy
CAS No Analyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Semivolatie Organic Compounds by GCMS
Semi volatile Or anic Com ounds b EPA 625
Prepared by method SW846 3510C 50 EPA 625 16-May- 19-May-08 805121683-32- Acenaphthene BRL IJgl
208-96-8 Acenaphthylene BRL IJgl 50
62-53- BRL IJgll 50Aniline
120- 12- Anthracene BRL 1J91 50
103-33- AzobenzenefDiphenyldiazine BRL IJgl 50
92-87 - Benzidine BRL IJgl 50
56-55- Benzo (a) anthracene BRL 1J91 50
50-32 - Benzo (a) pyrene IJglBRL 50
205-99- Benzo (b) fluoranthene BRL IJgl 50
191-24- Benzo (g i) perylene BRL IJgl 50
50207-08- Benzo (k) fluoranthene BRL IJgl
65-85 Benzoic acid BRL 1J91 50
100-51-6 Benzyl alcohol 1J91BRL 50
50111-91- Bis(2-chloroethoxy)methane BRL 1J91
111-4-4 Bis(2-chloroethyl)ether BRL IJgl 50
501 08-60- Bis(2-chloroisopropyl)ether BRL IJgl
117-81- Bis(2-ethylhexyl)phthalate BRL 1J91 50
101-55- Bromophenyl phenyl ether BRL IJgl 50
5085-68- Butyl benzyl phthalate BRL IJgl
5086-74- Carbazole BRL IJgl
5059-50- C hloro-3-methylphenol BRL IJgl
106-47- Chloroaniline BRL IJgl 50
91-58- Chloronaphthalene IJglBRL 50
5095-57 - Chlorophenol BRL 1J91
507005-72- Chlorophenyl phenyl ether BRL IJgl
216-01- Chrysene tJ91BRL 50
5053-70- Dibenzo (a h) anthracene BRL IJgl
50132-64- Dibenzofuran BRL IJgl
95-50- Dichlorobenzene IJglBRL 50
541-73- 13- Dichlorobenzene BRL IJgl 50
106-46- Dichlorobenzene 1J91BRL 50
5091-94- 3 - Dichlorobenzidine BRL IJgl
120-83- Dichlorophenol BRL IJgl 50
84-66- Diethyl phthalate BRL IJgl 50
131-11- Dimethyl phthalate BRL IJgll 50
105-67- Dimethylphenol BRL 1J91 50
5084-74- Di-n- butyl phthalate BRL 1J91
534-52 - Dinitro-2-methylphenol BRL IJgl 50
51-28- Dinitrophenol IJglBRL 50
50121-14- Dinitrotoluene BRL 1J91
606-20- Dinitrotoluene IJglBRL 50
50117-84-0 Di-n-octyl phthalate BRL IJgl
206-44-0 Fluoranthene 1J91BRL 50
BRL 50
50 86-73- Fluorene IJgi
118-74- Hexachlorobenzene BRL 1J91
87-68- Hexachlorobutadiene 1J91BRL 50
5077-47-4 Hexachlorocyclopentadiene BRL IJgl
67-72- Hexachloroethane IJglBRL 50
50193-39- Indeno (1 3-cd) pyrene BRL IJgl
5078-59- Isophorone BRL IJgl
Tfls laboratory report is not valid without all authorized signature 011 the coverpage
Page 6 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Sam le Identification Client Pro ect Matrix Collection DateTime ReceivedMWshy
2920-96- Ground Water I3-May-081030 14-May-SA 78602shy
CAS No Analyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Semivolatile Organic Compounds by GCMS
Semi volatile Or anic Com ounds b EPA 625
Prepared by method SW846 3510C
91-57 -6 Methylnaphthalene 367 1-91 50 EPA 625 16-May- 19-May-08 8051216
95-48- Methylphenol BRL 1-91 50
108-39-4 3 amp 4-Methylphenol BRL I-gl 100 106-44shy91-20- Naphthalene 247 1-91 50
88-74-4 Nitroaniline BRL 1-91 50
99-09- Nitroaniline BRL 1-91 50
100-01-6 Nitroaniline BRL 1-91 50
98-95- Nitrobenzene BRL 1-91 50
88-75- Nitrophenol BRL 1-91 50
100-02- Nitrophenol BRL 1-91 50
62-75- Nitrosodimethylamine BRL 1-91 50
621-64- N- Nitrosodi-n-propylamine BRL 1-91 50
86-30-6 Nitrosodiphenylamine BRL 1-91 50
87 -86- Pentachlorophenol BRL 1-91 50
85-0- Phenanthrene BRL 1-91 50
108-95- Phenol BRL 1-91 50
129-00-0 Pyrene BRL 1-91 50
110-86- Pyridine BRL 1-91 50
120-82- 4- Trichlorobenzene BRL 1-91 50
95-95- 5- Trichlorophenol BRL 1-91 50
88-06- 6- T richlorophenol BRL 1-91 50
Surrogate recoveries
321-60- Fluorobipheny 30- 130
367- 12- Fuorophenol 15- 110
4165-60- Nitrobenzene- 30- 130
4165-62- Pheno- 15- 110
1718-51- Terpheny-d4 30- 130
118- 79- 6- Tribromophenol 15- 110
Semivolatile Organic Compounds by GC
Pol chlorinated Bi hen ls b EPA 608
Prepared by method SW846 3510C
12674- 11-2 Aroclor- 1016 BRL 1-91 0650 EPA 608 15- May- 16-May-08 8051106
11104-28-2 Aroclor-1221 BRL IJgl 0650
11141-16-5 Aroclor- 1232 BRL 1-91 0650
53469-21-9 Aroclor- 1242 BRL 1-91 0650
12672-29-6 Aroclor- 1248 BRL 1-91 0650
11097-69-1 Aroclor- 1254 BRL 1-91 0650
11096-82-5 Aroclor -1260 BRL 1-91 0650
37324-23-5 Aroclor-1262 BRL 1-91 0650
11100-14-4 Aroclor-1268 BRL IJgl 0650
Surrogate recoveries
2051-24- Decachlorobipheny (Sr) 105 30- 150
10386-84-2 4 DB-Octafluorobiphenyl (Sr) 30- 150
Extractable Petroleum Hydrocarbons
mgl EPA 1664 Rev A 15-May- 19-May-08 8051102Non-polar material (SGT- HEM)
Soluble Metals by EPA 2006000 Series Metbods
Field Filtered NA EPA 200 73005A 15- May- 15-May-08 8051192Filtration
Soluble Metals by EPA 200 Series Methods
7440-22-4 Silver BRL mgl 0002 EPA 200 21-May- 27- May-08 8051249
This laboratory report is IlOt mlid without (II authorized signature on the cover page
Reportble Detection Limit BRL = Below Reporting Limit Page 7 of 25
Sam le Identification MW-
Client Pro ect 2920-96shy
Matrix Ground Water
Collection DateTime 13-May-08 1030
Received 14-May-
SA 78602shy
CAS No A nalyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Soluble Metals by EPA 200 Series Methods
7440-38shy Arsenic 0468 mg1 0040 EPA 200 21-Mayshy 21-May-08 80511 50
7440-43shy Cadmium BRL mg1 0002 EPA 200 21-May-088051249
7440-47shy Chromium BRL mg1 0050 EPA 200 21-May-088051150
7440-50-8 Copper BRL mg1 0050
7439-89-6 Iron 184 mg1 0150
7439-97-6 Mercury BRL mg1 00020 EPA 245 17470A 21-May-088051152
7440-02-0 Nickel BRL mg1 0050 EPA 200 21-May-088051150
7439-92shy Lead 0011 mg1 0002 EPA 200 21-May-088051249
7440-36-0 Antimony 0003 mg1 0002
7782-49shy Selenium BRL mg1 0150 EPA 200 21-May-08 8051150
7440-66-6 Zinc 0186 mgl 0050
General Chemistry Parameters
Filtration Completed NA Varies 14-Mayshy 14-May-08 8051095
18540-29-9 Hexavalent Chromium (soluble) BRL HT2 mg1 125 SM3500CrDI796A 14-Mayshy 14-May-08 8051094 R01 2013 2016
57-12shy Cyanide (total) BRL mg1 0100 EPA 3354 19-Mayshy 19-May-088051374
7782-50shy Total Residual Chlorine BRL CIHT mg1 500 Hach 8167 14-Mayshy 14-May-08 8051049 R01 1900 2001
Total Suspended Solids 580 mg1 25 SM2540D 16-Mayshy 16-May-08 8051275
This lahomtOlY report is not valid without an authorized signature on the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page 8 of 25
Volatie Organic Compounds - Quality Control
Analyte( s)
Batch 8051244 - SW846 5030 Water MS
Blank 8051244-BLK1
Prepared 16-May-08 Analyzed 17-May-
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromochloromethane
1 Dichlorobenzene
1 Dichlorobenzene
1 Dichlorobenzene
1-Dichloroethane
1 Dichloroethane
1 1-Dichloroethene
cis- Dichloroethene
trans- 1 Dichloroethene
1 Dichloropropane
cis- 1 Dichloropropene
trans- 1 Dichloropropene
Ethylbenzene
Hexanone (MBK)
Methyl tert-butyl ether
Methyl- pentanone (MIBK)
Methylene chloride
Styrene
2- Tetrachloroethane
Tetrachloroethene
Toluene
1- Trichloroethane
2- Trichloroethane
Trichloroethene
Trichlorofluoromethane (Freon 11)
Vinyl chloride
p-Xylene
Xylene
Surrogate 4-Bromofluorobenzene Surrogate Toluene-
Surrogate 1 Dichloroethane-Surrogate Dibromofluoromethane
LCS B051244-BS1
Prepared 16-May-08 Analyzed 17 -May-
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Spike Source REC RPD
Result Flag Units RDL Level Result REC Limits RPD Limit
BRL gl 20
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl 10
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gll
BRL gi
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl 10
BRL gll
BRL gll 10
BRL gl 10
BRL gll
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
41 gl 50 70- 130 49 gl 50 70- 130 59 gl 50 119 70- 130 52 gl 50 105 70- 130
QC2 jgl 20 70- 130
18 jgl 20 70- 130
192 jgl 20 35- 155
18 jgl 20 45- 169
19 jgl 20 242
This laboratOlY repol1 is lot valid without 011 authorized sigllature 011 the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page 9 of 25
Volatie Organic Compounds - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051244 - SW846 5030 Water MS
LC5 8051244B51
Prepared 16-May-08 Analyzed 17-May-
Butanone (MEK) 10 QC2 gl 20 70- 130
Carbon tetrachloride 204 gl 20 102 70- 140
Chlorobenzene 18 gl 20 70- 130
Chloroethane 164 gl 20 14-230
Chloroform 18 gll 20 51- 138
Chloromethane 21 gl 20 106 273
Dibromochloromethane 18 gl 20 53- 149
1 Dichlorobenzene 20 gl 20 104 18- 190
1 Dichlorobenzene 19 gl 20 59- 156
1 A-Dichlorobenzene 18 gl 20 18- 190
1- Dichloroethane 19 gl 20 59- 155
1 Dichloroethane 19 gl 20 49- 155
1-Dichloroethene 16 gl 20 70- 130
cis- 1 Dichloroethene 17 gl 20 70- 130
trans- 1 Dichloroethene 16 gll 20 54- 156
1 Dichloropropane 18 gl 20 210
cis- Dichloropropene 17 gl 20 227
trans- 1 Dichloropropene 17 gl 20 17- 183
Ethylbenzene 19 gl 20 37- 162
Hexanone (MBK) 124 QC2 gl 20 70- 130
Methyl tert-butyl ether 19 gl 20 70- 130
Methylshy pentanone (MIBK) 17 gl 20 70- 130
Methylene chloride 16 gl 20 221
Styrene 17 gl 20 70- 130
1 Tetrachloroethane 194 gl 20 46- 157
Tetrachloroethene 15 gl 20 64- 148
Toluene 18 gl 20 70- 130
1- Trichloroethane 20 gl 20 100 52- 162
2- Trichloroethane 18 gl 20 52- 150
Trichloroethene 17 gl 20 71- 157
Trichlorofluoromethane (Freon 11) 19 gl 20 17- 181
Vinyl chloride 21 gl 20 106 251
p-Xylene 39 gl 40 70- 130
Xylene 20 gl 20 102 70- 130
Surrogate 4-Bromofluorobenzene Surrogate Toluene-
Surrogate 1 Dichloroethane-Surrogate Dibromofluoromethane
52 49 56
49
gl
gl
gl
gl
50 50 50
50
105
112 100
70- 130 70- 130 70- 130 70- 130
LC5 DUD (8051244-B5D1
Prepared 16-May-08 Analyzed 17-May-
Acetone QC2 gl 20 70- 130
Benzene 18 gl 20 70- 130
Bromodichloromethane 18 gl 200 35- 155
Bromoform 17 gl 20 45- 169
Bromomethane 18 gl 20 242
Butanone (MEK) 11 QC2 1-91 20 70- 130
Carbon tetrachloride 20 gl 20 100 70- 140
Chlorobenzene 17 gl 20 70- 130
Chloroethane 15 1-91 20 14-230
Chloroform 18 1-91 20 51- 138
This laboratory report is aot valid without a1 authorized sig1ature 01 the cover page
Reportble Detection Limit BRL = Below Reporting Limit Page 10 of25
Volatie Organic Compounds - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051244 - SW846 5030 Water MS
LCS Dup 18051244-BSD1
Prepared 16-May-08 Analyzed 17-May-
Chloromethane 18 1-91 20 273
Dibromochloromethane 174 1-91 20 53- 149
Dichlorobenzene 20 1-91 20 100 18- 190
Dichlorobenzene 18 1-91 20 59- 156
Dichlorobenzene 18 1-91 20 18- 190
Dichloroethane 18 1-91 20 59- 155
Dichloroethane 19 1-91 20 49- 155
Dichloroethene 16 1-91 20 70- 130
cis- Dichloroethene 16 1-91 20 70- 130
trans- Dichloroethene 15 1-91 20 54- 156
Dichloropropane 17 1-91 20 210
cis- Dichloropropene 164 IJgl 20 227
trans- 1 Dichloropropene 164 I-gl 20 17- 183
Etlwlbenzene 18 IJgl 20 37- 162
Hexanone (MBK) 124 QC2 IJgl 20 70- 130
Methyl tert-butyl ether 184 1J91 20 70- 130
Methyl- pentanone (MIBK) 17 IJgl 20 70- 130
Methylene chloride 16 IJgl 20 221
Styrene 16 IJgl 20 70- 130
2- Tetrachloroethane 19 IJgl 20 46- 157
Tetrachloroethene 15 IJgl 20 64- 148
Toluene 17 IJgl 20 70- 130
1- Trichloroethane 19 1-91 20 52- 162
2- Trichloroethane 16 IJgl 20 52- 150
Trichloroethene 15 IJgl 20 71- 157
Trichlorofluoromethane (Freon 11) 17 IJgl 20 17- 181
Vinyl chloride 19 IJglI 20 251
p-Xylene 37 1J91 40 70- 130
Xylene 20 IJgl 20 100 70- 130
Surrogate 4-Bromofluorobenzene 51 IJgl 50 104 70- 130
Surrogate Toluene- 4B gl 50 70- 130
Surrogate 1 0ichloroethane- 53 IJgl 50 106 70- 130 Surrogate Oibromofluoromethane 50 1J9i 50 102 70- 130
Matrix S ike B051244-MS1 Source SA7B629shy
Prepared 16-May-08 Analyzed 17-May-
Benzene 18 20 BRL 70- 130IJgl
Bromodichloromethane 19 IJgl 20 BRL 35- 155
Bromoform 18 IJgl 20 BRL 45- 169
Bromomethane 16 IJgl 20 BRL 242
Carbon tetrachloride 21 IJgl 20 BRL 106 70- 140
Chlorobenzene 18 IJgl 20 BRL 70- 130
Chloroethane 16 IJgl 20 BRL 14-230
Chloroform 18 IJgl 20 BRL 51- 138
Chloromethane 19 IJgl 20 BRL 273
Dibromochloromethane 17 IJgl 20 BRL 53- 149
1 Dichlorobenzene 22 IJgl 20 BRL 112 18- 190
1 Dichlorobenzene 22 IJgl 20 BRL 110 59-156
1 Dichlorobenzene 21 IJgl 20 BRL 109 18- 190
1- Dichloroethane 19 IJgl 20 BRL 59- 155
1 Dichloroethane 18 IJgl 20 BRL 49- 155
This laboratory report is 110t mUd without an authorized signature on the covel page
Reportble Detection Limit BRL = Below Reporting Limit Page It of25
Volatile Organic Compounds - Quality Control
p
Spike Source REC RPD
Result REC imits RPD LimitAnalyte(s) Result Flag Units RDL Level
Batch 8051244 - SW846 5030 Water MS
Matrix ike S051244-MS1 Source SA7B629shy
Prepared 16-May-08 Analyzed 17-Mayshy
17 20 BRL 70- 130 1- Dichloroethene IJgl
16 20 BRL 54- 156trans- 1 Dichloroethene IJgl
21020 BRL1 Dichloropropane 17 1J91
cis- 1 Dichloropropene 17 IJgl 20 BRL 227
17- 183trans- 1 Dichloropropene 184 1J91 20 BRL
20 20 BRL 103 37- 162Ethylbenzene IJgl
15 20 BRL 221Methylene chloride IJgl
20 BRL 46- 1572- Tetrachloroethane 19 1J91
20 BRL 64- 148Tetrachloroethene 18 1J91
BRL 70- 130Toluene 18 1J91 20
105 52-1621- Trichloroethane 211 IJgl 20 BRL
18 20 BRL 52- 1502- Trichloroethane IJgl
17 20 BRL 71- 157Trichloroethene 1J91
20 BRL 17- 181Trichloroluoromethane (Freon 11) 194 IJgl
20 BRL 103 251Vinyl chloride 20 IJgl
102 70- 130Surrogate 4-Bromofluorobenzene 50 IJgl 50 50 70- 130Surrogate Toluene- 49 1J91
56 50 112 70- 130Surrogate 1 Dichloroethane- IJgl
50 100 70- 130Surrogate Dibromofluoromethane 50 IJgl
Matrix S ike Du S051244-MSD1 Source SA7S629shy
Prepared 16-May-08 Analyzed 17-Mayshy
18 20 BRL 70- 130Benzene IJgl
18 20 BRL 35- 155Bromodichloromethane IJgl
17 20 BRL 45- 169Bromoform IJgl
20 BRL 242Bromomethane 17 IJgl
20 BRL 103 70- 140Carbon tetrachloride 20 IJgl
18 20 BRL 70- 130Chlorobenzene 1J91
14-230Chloroethane 16 IJgl 20 BRL
20 51- 138Chloroform 184 IJgl BRL
Chloromethane 19 1J91 20 BRL 273
18 20 BRL 53- 149Dibromochloromethane 1J91
20 BRL 117 18- 190Dichlorobenzene 234 IJgl
20 BRL 112 59- 156Dichlorobenzene 22 IJgl
BRL 108 18- 190Dichlorobenzene 21 1J91 20
20 59- 1551 Dichloroethane 19 IJgl BRL
18 20 BRL 49- 155Dichloroethane IJgl
16 20 BRL 70- 130Dichloroethene IJgl
20 BRL 54- 156trans- Dichloroethene 154 1J91
20 BRL 210Dichloropropane 17 IJgl
0420 BRL 227cis- Dichloropropene 17 IJgl
17- 183trans- Dichloropropene 17 1J91 20 BRL
BRL 37- 162Ethylbenzene 20 1J91 20 102
Methylene chloride 15 IJgl 20 BRL 221
20 BRL 46- 1572- Tetrachloroethane 192 IJgl
20 BRL 64- 148 04Tetrachloroethene 18 IJgl
BRL 70- 130Toluene 184 1J91 20
52- 1621- Trichloroethane 20 IJgl 20 BRL 104
17 20 BRL 52- 1502- Trichloroethane IJgl
17 20 BRL 71- 157Trichloroethene IJgl
20 BRL 17-181Trichlorofluoromethane (Freon 11) 19 IJgl
This laboratory report is IIOt valid without all authorized sigllllture 011 the cover page
Page 12 of25 Reportble Detection Limit BRL = Below Reporting Limit
Semivolatile Organic Compounds by GCMS - Quality Control
Analyte(s)
Batch 8051216 - SW846 3510C
Blank 8051216-BLK1
Prepared amp Analyzed 16-May-
Isophorone
Methylnaphthalene
Methylphenol
3 amp 4-Methylphenol
Naphthalene
Nitroaniline
Nitroaniline
Nitroaniline
Nitrobenzene
Nitrophenol
Nitrophenol
Nitrosodimethylamine
N- N itrosodi-n-pro pyla mine
N itrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Pyridine
1 24-Trichlorobenzene
24 5- Trichlorophenol
246- Trichlorophenol
Surrogate 2-Fuorobipheny Surrogate 2-Fuoropheno Surrogate Nitrobenzene-Surrogate PhenoshySurrogate Terpheny-d4 Surrogate 6- Tribromopheno
LCS B051216-BS1
Prepared amp Analyzed 16-May-
Acenaphthene
Acenaphthylene
Aniline
Anthracene
AzobenzenelDi phenyld lazine
Benzidine
Benzo (a) anthracene
Benzo (a) pyrene
Benzo (b) fluoranthene
Benzo (g i) perylene
Benzo (k) fluoranthene
Benzoic acid
Benzyl alcohol
B is(2-chloroethoxy)methane
B i s (2-ch loroethyl)eth e r
Bis(2-ch loroisopropyl) ether
B is(2-ethy Ih exyl) phtha late
Bromophenyl phenyl ether
Butyl benzyl phthalate
Carbazole
Spike Source REC RPD
Result Flag Units RDL Level Result REC Limits RPD Limit
BRL gl
BRL gl
BRL gl
BRL gl 10
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gll
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
370 gl 50 30- 130 40 gl 50 15- 110 39 gl 50 30- 130 43 gl 50 15- 110 36 gl 50 30- 130 40 gl 50 15- 110
41 gl 50 40- 140
43 gI 50 40- 140
41 gl 50 40- 140
38 gl 50 40- 140
45 gl 50 40- 140
49 gl 50 153
41 gl 50 40- 140
43 gl 50 40- 140
41 gl 50 40- 140
41 gll 50 40- 140
45 gl 50 40- 140
32 gl 50 12- 149
41 gl 50 40- 140
39 gl 50 40- 140
384 gl 50 40- 140
47 gl 50 40- 140
47 gl 50 40- 140
40 gl 50 40- 140
47 gI 50 40- 140
56 gI 50 112 200
This laboratory report is lIot valid witllOut a1l authorized sigllature 011 the coverpage
Reportble Detection Limit BRL = Below Reporting Limit Page 15 of25
Semivolatile Organic Compounds by GCMS - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051216 - SW846 3510C
LCS 8051216-BS1
Prepared amp Analyzed 16-Mayshy
50 30- 1304 -C hloro-3-methylphenol 42 IJgl
40- 140Chloroaniline 39 IJgl 50
Chloronaphthalene 37 IJgl 50 40- 140
Chlorophenol 37 IJgl 50 30- 130
50 40- 140
40- 140
Chlorophenyl phenyl ether 45 IJgl
Chrysene 43 IJgl 50
Dibenzo (a h) anthracene 43 IJgl 50 40- 140
Dibenzofuran IJgl38 50 40- 140
50 40- 1401 Dichlorobenzene 35 IJgl
40- 1401 Dichlorobenzene 264 IJgl 50
40- 1401 Dichlorobenzene 434 IJgl 50
58 50 116 40- 1403 - Dichlorobenzidine IJgl
50 30- 130
40- 140 24-Dichlorophenol 38 IJgl
Diethyl phthalate 484 IJgl 50
50 40- 140Dimethyl phthalate 464 IJgl
Dlmethylphenol 39 IJgl 50 30- 130
DI-n-butyl phthalate 44 IJgll 50 40- 140
30- 130 6-Di nitro- 2-methylphenol 38 1J91 50
30- 130Dinltrophenol 36 1J91 50
42 50 40- 14024-Dlnitrotoluene 1J91
Dlnitrotoluene 1J9141 50 40- 140
Di-n-octyl phthalate 52 IJgl 50 104 40- 140
40- 140Fluoranthene 40 IJgl 50
Fluorene 41 IJgl 50 40- 140
39 50 40- 140Hexachlorobenzene IJgl
50 40- 140Hexachlorobutadiene 40 IJgl
40- 140Hexach lorocyclopentad iene 294 IJgl 50
40 50 40- 140Hexachloroethane IJgl
42 50 40-140Indeno (1 3-cd) pyrene IJgl
50 40- 140Isophorone 40 IJgl
40- 140Methylnaphthalene 394 IJgl 50
40- 140Methylphenol 39 IJgl 50
40 10 50 40- 1403 amp 4-Methylphenol IJgl
37 50 40-140Naphthalene IJgl
50 40-140Nitroaniline 39 IJgl
Nitroaniline 51 IJgl 50 102 40- 140
48 50 40- 140Nltroaniline 1J91
50 40- 140Nitrobenzene 40 IJgl
30- 130Nitrophenol 36 IJgl 50
40 IJgl 50 30- 130Nitrophenol 40- 140Nitrosodimethylamine 32 1J91 50
50 40-140N- N itrosodi-n-propyla mine 46 IJgl
40- 140N itrosodi phenyla ml ne 44 IJgl 50
41 IJgl 50 30- 130Pentachlorophenol 40- 140Phenanthrene 38 IJgl 50
50 30- 130Phenol 38 IJgl
40- 140Pyrene 424 1J91 50
40- 140Pyridine 294 1J91 50
40- 14024- Trichlorobenzene 364 IJgl 50
This laboratory report is not mlid without an authorized signature 011 the cover page
Page 16 of25 Reportble Detection Limit BRL = Below Reporting Limit
Semivolatie Organic Compounds by GCMS - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
BMch 8051216 - SW846 3510C
LC5 8051216-851
Prepared amp Analyzed 16-Mayshy
24 5- Trichlorophenol 404 gl 50 30- 130
246- Trichlorophenol 42 gl 50 30- 130
Surrogate 2-Fluorobiphenyl 29 gl 50 30- 130
Surrogate 2-Fluorophenot 27 gl 50 15- 110
Surrogate Nitrobenzene- 30 gl 50 30- 130
Surrogate Phenol- 29 gl 50 15- 110
Surrogate Terpheny-d4 30 gl 50 30- 130
Surrogate 6- Tribromopheno 324 gl 50 15- 110
This laboratory report is lIot valid without all authorized sigllature 011 tlle cover page
Reportble Detection Limit BRL = Below Reporting Limit Page 17 of25
Semivolatie Organic Compounds by GC - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051106 - SW846 3510C
Blank S051106-BLK1
Prepared amp Analyzed 15-Mayshy
Aroclor- 1016 BRL gI 0200
Aroclor- 1016 (2C) BRL gI 0200
Aroclor- 1221 BRL gI 0200
Aroclor- 1221 (2C) BRL gI 0200
Aroclor- 1232 BRL gI 0200
Aroclor- 1232 (2Cj BRL gI 0200
Aroclor- 1242 BRL gI 0200
Aroclor-1242 (2C) BRL gI 0200
Aroclor- 1248 BRL gI 0200
Aroclor- 1248 (2C) BRL gI 0200
Aroclor- 1254 BRL gI 0200
Aroclor- 1254(2Cj BRL gI 0200
Aroclor- 1260 BRL gI 0200
Aroclor- 1260 (2C) BRL gI 0200
Aroclor- 1262 BRL gI 0200
Aroclor- 1262 (2C) BRL gI 0200
Aroclor-1268 BRL gI 0200
Aroclor- 1268 (2C) BRL gI 0200
Surrogate Decachlorobiphenyl (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0231 0224 0194 0191
gI
gI
gI
gI
0200 0200 0200 0200
116 112
30- 150 30- 150 30- 150 30- 150
LC5 8051106-B51
Prepared 15-May-08 Analyzed 16-May-08
Aroclor- 1016 265 gI 0200 250 106 50- 114
Aroclor- 1 016 (2C) 240 gI 0200 250 50- 114
Aroclor- 1260 0269 gI 0200 250 107 40- 127
Aroclor-1260 (2Cj 270 gI 0200 250 108 40- 127
Surrogate Decachlorobiphenyl (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0225 0224 0188 0183
gI
gI
gI
gI
0200 0200 0200 0200
113 112
30- 150 30- 150 30- 150 30- 150
LC5 DUD rS051106-B5D1
Prepared 15-May-08 Analyzed 16-Mayshy
Aroclor- 1016 262 gl 0200 250 105 50- 114
Aroclor-1 016 (2Cj 241 gI 0200 250 50- 114
Aroclor- 1260 277 gI 0200 250 111 40- 127
Aroclor- 1260(2Cj 0260 gI 0200 250 104 40- 127
Surrogate Decachlorobipheny (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0238 0218 0189 0181
gI
gI
gI
gI
0200 0200 0200 0200
119 109
30- 150 30- 150 30- 150 30- 150
This laboratory report is lot valid without (II authorized sigllature 01 the cover page
Page 18 of25 Reportable Detection Limit BRL = Below Reporting Limit
Extractable Petroleum Hydrocarbons - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051102 - SW846 3510C
Blank 8051102-BLK1
Prepared 15-May-08 Analyzed 19-Mayshy
Non-polar material (SGT- HEM) BRL m91
LC8 8051102-B81
Prepared 15-May-08 Analyzed 19-Mayshy
Non-polar material (SGT- HEM) 184 m91 21 81 904
This laboratory report is not valid without an authorized signature 011 the cover page
Page 19 of25 Reportable Detection Limit BRL = Below Reporting Limit
Soluble Metals by EPA 200 Series Methods - Quality Control
Analyte(s) Result Flag Units RDL
Spike
Level
Source
Result REC
REC
Limits RPD
RPD
Limit
Batch 8051150 - EPA 200 Series
Blank 8051150-BLK1
Prepared amp Analyzed 21-May-
Iron
Zinc
Selenium
Nickel
Chromium
Copper
Arsenic
BRL
BRL
BRL
BRL
BRL
BRL
BRL
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0150
0050
0150
0050
0050
0050
0040
LCS 8051150-BS1
Prepared amp Analyzed 21-May-
Selenium
Zinc
Iron
Nickel
Chromium
Arsenic
Copper
123
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0150
0050
0150
0050
0050
0040
0050
103
105
101
100
85- 115
85- 115
85- 115
85- 115
85- 115
85-115
85- 115
licate B051150-DUP1 Source SA7B602shy
Prepared amp Analyzed 21-May-
Iron
Zinc
Selenium
Nickel
Copper
Chromium
Arsenic
17
0162
BRL
0015
0017
BRL
0450
QR8
mgl
mgl
mgl
mgl
mgl
mgl
mgi
0150
0050
0150
0050
0050
0050
0040
184
0186
BRL
0014
0023
BRL
0468
Matrix S ike 8051150-MS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Iron
Selenium
Nickel
Zinc
Copper
Chromium
Arsenic
19 QM2 mgl
mgll
mgl
mgl
mgl
mgl
mgl
0150
0150
0050
0050
0050
0050
0040
125
184
BRL
0014
0186
0023
BRL
0468
104
105
102
70- 130
70- 130
70-130
70- 130
70- 130
70-130
70- 130
Post S ike 8051150-PS1 Source SA78602shy
Prepared amp Analyzed 21-May-
Zinc
Iron
Selenium
Nickel
Copper
Arsenic
Chromium
18 QM2
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0050
0150
0150
0050
0050
0040
0050
0186
184
BRL
0014
0023
0468
BRL
104
104
101
85- 115
85- 115
85- 115
85-115
85-115
85- 115
85-115
Batch 8051152 - EPA200SW7000 Series
Blank B051152-BLK1
Prepared amp Analyzed 21-May-
Mercury BRL mgl 00020
This laboratory report is IIOt valid witllOut all authorized sigllature 011 the coverpage
Page 20 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Soluble Metals by EPA 200 Series Methods - Quality Control
Analyte(s) Result Flag Units RDL
Spike
Level
Source
Result REC
REC
Limits RPD
RPD
Limit
Batch 8051152 - EPA200SW7000 Series
LCS B051152-BS1
Prepared amp Analyzed 21-May-
Mercury 00576 m91 00020 00500 115 85- 115
licate B051152-DUP1 Source SA78602-01
Prepared amp Analyzed 21-May-
Mercury BRL m91 00020 BRL
Matrix S ike 8051152-MS1 Source SA78602shy
Prepared amp Analyzed 21-May-
Mercury 00632 OM m91 00020 00500 BRL 126 75- 125
Post S ike 8051152-PS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Mercury 00624 OC1 m91 00020 00500 BRL 125 85- 115
Batch 8051249 - 2008No digestion
Blank 8051249-BLK1
Prepared amp Analyzed 21-May-
Lead
Antimony
Cadmium
Silver
BRL
BRL
BRL
BRL
m91
m91
m91
m91
0002
0002
0002
0002
LCS B051249-BS1
Prepared amp Analyzed 21-May-
Antimony
Lead
Silver
Cadmium
143
145 OC2
m91
m91
m91
m91
0050
0050
0050
0040
103
115
107
116
85- 115
85- 115
85- 115
85- 115
licate 8051249-DUP1 Source SA7B602shy
Prepared amp Analyzed 21- May-
Lead
Antimony
Cadmium
Silver
0009
0002
00005
00002
ORB
m91
m91
m91
m91
0002
0002
0002
0002
0011
0003
00005
00003
Matrix S ike 8051249-MS1 Source SA78602shy
Prepared amp Analyzed 21- May-
Lead
Antimony
Cadmium
Silver
142
m91
m91
m91
m91
0050
0050
0040
0050
0011
0003
00005
00003
111
101
114
102
70- 130
70-130
70c130
70- 130
Post S ike 8051249-PS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Antimony
Cadmium
Silver
38
OC2
m91
m91
m91
0050
0040
0050
125
0003
00005
00003
110
121
109
85- 115
85- 115
85- 115
This laboratory report is flOt valid IVithout all authorized signature 011 the cOIer page
Reportable Detection Limit BRL Below Reporting Limit Page 21 of 25
General Chemistry Parameters - Quality Control
Spike Source REC RPD
Analyte( s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051049 - General Preparation
Blank S051 049-BLK1
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
Blank S051049-BLK2
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
Blank S051 049-BLK3
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
LCS S051049-BS1
Prepared amp Analyzed 14-May-
Total Residual Chlorine 046 mgl 020 0500 90- 110
LCS S051049-BS2
Prepared amp Analyzed 14-May-
Total Residual Chlorine 047 mgl 020 0500 90- 110
LCS S051049-BS3
Prepared amp Analyzed 14-May-
Total Residual Chlorine 054 mgl 020 0500 108 90-110
licate B051049-DUP1 Source SA7S544shy
Prepared amp Analyzed 14-May-
Total Residual Chlorine 012 mgl 020 010
licate S051049-DUP2 Source SA7S602-01
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020 BRL
Matrix S ike 8051049-MS1 Source SA78544-01
Prepared amp Analyzed 14-May-
Total Residual Chlorine 065 mgl 020 0500 010 110 80- 120
Matrix S ike 8051049-MS2 Source SA7B602shy
Prepared amp Analyzed 14-May-
Total Residual Chlorine mgl 500 125 BRL 108 80- 120
Reference 8051 049-SRM1
Prepared amp Analyzed 14-May-
Total Residual Chlorine 100 mgl 020 0967 103 85-115
Batch 8051094 - General Preparation
Blank 8051094-BLK1
Prepared amp Analyzed 14 May-
Hexavalent Chromium (soluble) BRL mgl 005
Blank 8051 094-BLK2
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) BRL mgl 005
LCS 8051094-BS1
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) 054 mgl 005 90- 110
licate 8051094-DUP1 Source SA78602-01
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) BRL mgl 125 BRL
Thi laboratory report is not valid without all authorized sigllature 011 the cover page
Page 22 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Page 11
=-
including the following
8 Signature Requirements
The N
otice ofIntent must be signed by the operator in accordance w
ith the signatory requirements of 40 C
FR Section 122
certification
J certif under penalty of law that this docum
ent and all attachments w
ere prepared under my direction or supervision in accordance w
ith a system
designed to assure that qualifed personnel properly gather and evaluate the information subm
itted Based on m
y inquiry of the person or persons who
manage the system
or those persons directly responsible for gathering the information I certif that t
he information submitted
is to the best of m
y
knowledge and belief true accurate and com
plete J certif that I am aw
are that there are signifcant penalties for submitting false inform
ation including
the possibilty of fine and imprisonm
ent for knowing violations
FacilitySite Name
Form
er Speedw
ay Service S
tation 181 East B
roadwav G
ardner MA
01440
Operator signature
Title
Michael 1 D
ziura Sf Env E
ngineer
Date
4150- q
Rem
ediation General Perm
it - Notice of Intent
-
D- 0
0 0
il (J tu
Bw
o(0 -I
NJW
gQb
J(JZc o c
rou a -10
0 J 6shy
a 0
I-tDC
aJ Qj
E aJshy
ro ro ro
~~~ ~~~~- -- - _ - -_ - ~~~ ~~~~ ~~~ - - _- _- -- -- p __(
MA DEP - Bureau of Waste Site CleanupSITE NME Site S aP 5 MiFlII Former Speeway Station _-II181 Eat Broaday b b d IS I i I GARDNER MA 0144 v ri) i P f f 1 me- 1 5ylmI I L shy J --I 423315n 715835e SiteLocation y o oCop1odQcn Ofof W-_ l
1 1 I
r
r
iBARBER HILL
A c
Cf1 f o s
0
5
Roads Uned Acss Divd Mar Roed Conntor Street Track 1 EPA Sola Source Aquilar FEMA 100yaar iloodplain 0 c Puc Watar SLo GrunSelaceNon Corrty 0
Bounars lOwn Couny DE Region Tian Powerln Ine Aqedut ApprOld Zona2 tNPA Sue Wster Supp Zone A bStZ F--shy--rle
8os Mat Sub SUeor Porenrial Inermtent Man lvo8 Ste Dfm Hyro1apy Wmer FeatllePLio Suleee Wat S H-- L otlMds FrslSaltN-ES WeIMd Habat L
Potentia Prdutiv AqlJlers ModHig Yield Proteoted Opn Space ACC nIL c= Non-Potential Drng Water Sollce AIea ModumHi Yo1d ll DEP Pormrd SoidWes1 FsiIi6s cnifud Verne Pools f0
1I2 KIWUmR$ MtL
January 30 2004 SCALE 1 15000
-
LE
GE
ND
APX PROPER BONDA
- APPROXOiSPO SIT BOUNDA
-GR
OU
ND
WA
TE F1 D
IRE
cnON
SCA
LE
30 60 FE
(APR
OX
CORPORATE ENVIRONMENTAL
)i
AD
VISO
RS
INC
SC
AS SH
OW
D
R B
Y K
HA
EL
DA
TE
10407
JOB
NO
2920-96
AERIAL MAP
FO
RM
ER
SP
EE
DW
AY
ST
AT
ION
FlGURE -3
181 EA
BR
OA
AY
GA
NE
R fo
age 1 ot 1Streamflow Statistics Report
Streamstats Ungaged Site Report Date Wed Dec 31 2008 124908 Site Location Massachusetts NAD83 Latitude 425545 (42 3316) NAD83 Longitude -719758 (-71 58 32) NAD27 Latitude 425545 (423316) NAD27 Longitude - 9763 (-71 58 34) Drainage Area 502 mi2
IPeak Flow Basin Characteristics 1100 Statewide Low Flow (S02 mi2)
Regression Equation Valid Rang
I Min II Max1 Value III Parameter Drainage Area (square miles) 161 149
Mean Basin Slope from 250K DEM (percent) 032 24
Stratified Drift per Stream Length (square mile per mile) 129
Massachusetts Region (dimensionless)
Streamflow Statistics
gO-Percent Prediction Interval Prediction Error
MaximumStatistic Flow (ft s) (percent) Minimum
I D50 IIII 11 1811 II 24511 993
I D60 II 35511 2011 II 03611 35111 2411 II 041 I 201I D70 24111 2611 II 03811 151I D75 11 2811 II 0911 3761I D80 981I D85 1 I 3211 II o6311
1 I 3711 II 0441 1 2 2911 D90 11 4611 II 02411 15511 D95I D98 04511 6011 II 01511 11
I D99 03411 6511 II ol1ll 1021
5011 II 02611 11I M7D2Y 1111 3311 II odl 3 541
I AUGD50
IIIIIIIIIIIIIIIIIIIIII 0311 7111 II 0088411 0981I M7Dl0Y
1010
12312008httpstreamstatsagscrusgsgovgisimgReportsFlowStatsReport3494 - 2008123112498
Dilution Factor Calculation Former Speedway Service Station 181 East Broadway Gardner Ma
DF=(Od+Os)Od
DF = Dilution factor
Od = Max flow rate of discharge in cubic feet per second Os = receiving water flow in cubic feet per seconds 7010 flow rate Mahoney Brook 7010 = min flow for seven consecutive days with a recurrence interval of 10 years
7010 flow based on data obtained from USGS Steamflow Statistics Report Data attached
067
Semivolatile Organic Compounds by GCMS - Quality Control
Analyte( s)
Batch 8051216 - SW846 3510C
Blank 8051216BLK1)
Prepared amp Analyzed 16May-
Acenaphthene
Acenaphthylene
Aniline
Anthracene
AzobenzenelDi phenyld iazi ne
Benzidine
Benzo (a) anthracene
Benzo (a) pyrene
Benzo (b) fiuoranthene
Benzo (g i) perylene
Benzo (k) fiuoranthene
Benzoic acid
Benzyl alcohol
Bis(2-ch loroethoxy) methane
Bis(2-ch loroethyl)ether
Bis(2-ch loroi sopropyl)ether
Bis(2ethylhexyl) phthalate
Bromophenyl phenyl ether
Butyl benzyl phthalate
Carbazole
Ch loro-3-methyl phenol
Chloroaniline
Chloronaphthalene
Chlorophenol
Chlorophenyl phenyl ether
Chrysene
Dibenzo (a h) anthracene
Dibenzofuran
Dichlorobenzene
Dichlorobenzene
14- Dichlorobenzene
3 - Dichlorobenzidine
24-Dichlorophenol
Diethyl phthalate
Dimethyl phthalate
24- Dimethylphenol
Din-butyl phthalate
Dinitro-2-methylphenol
Dinitrophenol
Dinitrotoluene
Dinitrotoluene
Di-noctyl phthalate
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopehtadiene
Hexachloroethane
Indeno (1 cd) pyrene
Spike Source REC RPD
Result Flag Units RDL Level Result REC Limits RPD Limit
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gl
BRL gI
BRL gl
BRL gl
BRL gl
BRL gI
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gll
BRL gl
BRL gll
BRL gl
BRL gl
BRL gI
BRL gI
BRL gI
BRL gl
BRL gI
BRL gI
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gI
BRL gI
BRL gl
This laboratory report is IlOt valid without all authorized sigllature 011 the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page t4 of25
Volatie Organic Compounds - Quality Control
p (
Spike Source REC RPD
RDL Level Result REC Limits RPD Limit Analyte(s) Result Flag Units
Batch 8051244 - SW846 5030 Water MS
Matrix S ike Du 8051244-MSD1 Source SA78629shy
Prepared 16-May-08 Analyzed 17-May-BRL 106 251
Vinyl chloride 21 gl 20
101 70- 130 Surrogate 4-Bromofluorobenzene 50 gl 50
70- 13049 gl 50 111 70- 130
Surrogate Toluene-Surrogate 1 Dichloroethane- 55 gl 50
50 70- 130494 glSurrogate Dibromofluoromethane
Microextractable Organic Compounds - Quality Control
Spike Source REC RPD
Flag Units RDL Level Result REC Limits RPD Limit Analyte(s) Result
Batch 8051105 - SW846 3510C
Blank 8051105-BLK
Prepared amp Analyzed 15-May-
BRL gl 01001 Dibromoethane (ED B)
LCS 8051105-BS1
Prepared amp Analyzed 15-Mayshy50- 1500770 gl 0100 100
licate 8051105-DUP1 Source SA7B583shy
Prepared amp Analyzed 15-May-
BRL gl 0100 BRL
1 Dibromoethane (EDB)
1 Dibromoethane (EDB)
This laborntOlY report is not valid without an authorized signature 011 the cover page
Page 13 of2S Reportable Detection Limit BRL = Below Reporting Limit
Sam le Identification Client Pro ect Matrix Collection DateTime ReceivedMWshy
2920-96- Ground Water 13-May-081030 14-May-SA 78602shy
CAS No Analyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Volatile Organic Compounds
Volatile Or anic Com ounds b GCMS
Prepared by method SW846 5030 Water MS
123-91- Dioxane BRL 1-91 200 EPA 624 16-May-08 17-May-08 8051244
994-05-8 Ter-amyl methyl ether BRL 1-911 20
755- Tert-Butanoll butyl alcohol BRL 1-91 200
67-B4- Acetone BRL 1-91 400
71-43- Benzene BRL 1-91 20
75-27-4 Bromodichloromethane BRL 1-91 20
75-25- Bromoform BRL 1-91 20
74-83- Bromomethane BRL 1-91 40
78-93- Butanone (MEK) BRL 1-91 200
56-23- Carbon tetrachloride BRL 1-91 20
108-90- Chlorobenzene BRL 1-91 20
75-00- Chloroethane BRL 1-91 40
676- Chloroform BRL 1-91 20
74-87- Chloromethane BRL 1-91 40
124-48- Dibromochloromethane BRL 1-91 20
95-50- Dichlorobenzene BRL 1-911 20
541-73- Dichlorobenzene BRL 1-91 20
106-46- Dichlorobenzene BRL 1-91 20
75-34- 1- Dichloroethane BRL 1-91 20
107-06- Dichloroethane BRL 1-91 20
75-35-4 1- Dichloroethene BRL 1-91 20
156-59 cis- Dichloroethene BRL 1-91 20
156-60- trans- Dichloroethene BRL 1-91 20
78-87- 2- Dichloropropane BRL 1-91 20
10061-01-5 cis- Dichloropropene BRL 1-91 20
10061-02-B trans- Dichloropropene BRL 1-91 20
100-41-4 Ethylbenzene 411 1-911 20
591-78-B BRL 200Hexanone (MBK) 1-91
1634-04 -4 Methyl tert-butyl ether BRL 1-91 20
108-10- Methyl- pentanone (MIBK) BRL 1-91 200
75-09- Methylene chloride BRL 1-91 200
100-42- Styrene BRL 1-91 20
79-34- 1 Tetrachloroethane BRL 1-91 20
127- 18-4 T etrachloroethene BRL 1-91 20
108-88- Toluene BRL 1-91 20
71-55 1- Trichloroethane BRL 1-91 20
79-00- 2- Trichloroethane BRL 1-91 20
79-01-B Trichloroethene BRL 1-91 20
759-4 Trichlorofluoromethane (Freon 11) BRL 1-91 20
75-01-4 Vinyl chloride BRL 1-91 20
179601-23-1 m Xylene 390 1-91 40
95-47 Xylene 82 1-91 20
Surrogate recoveries 460-00- Bromofluorobenzene 70- 130
2037-26- Toluene- 100 70- 130
17060-07-0 1 Dichloroethane- 111 70- 130
1868-53- Dibromofluoromethane 70- 130
Microextractable Organic Compounds
106-93-4 1 Dibromoethane (EDB) BRL 1-91 0100 EPA 504 15-May- 15-May-08 8051105
Semivolatile Organic Compounds by GCMS
This laboratory report is not valid without all autllOrized signature 011 the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page 5 of 25
Sam le Identification Client Pro ect Matrix Collection DateTime Received
MWshy2920-96- Ground Water 13-May-081030 14-May-
SA 78602shy
CAS No Analyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Semivolatie Organic Compounds by GCMS
Semi volatile Or anic Com ounds b EPA 625
Prepared by method SW846 3510C 50 EPA 625 16-May- 19-May-08 805121683-32- Acenaphthene BRL IJgl
208-96-8 Acenaphthylene BRL IJgl 50
62-53- BRL IJgll 50Aniline
120- 12- Anthracene BRL 1J91 50
103-33- AzobenzenefDiphenyldiazine BRL IJgl 50
92-87 - Benzidine BRL IJgl 50
56-55- Benzo (a) anthracene BRL 1J91 50
50-32 - Benzo (a) pyrene IJglBRL 50
205-99- Benzo (b) fluoranthene BRL IJgl 50
191-24- Benzo (g i) perylene BRL IJgl 50
50207-08- Benzo (k) fluoranthene BRL IJgl
65-85 Benzoic acid BRL 1J91 50
100-51-6 Benzyl alcohol 1J91BRL 50
50111-91- Bis(2-chloroethoxy)methane BRL 1J91
111-4-4 Bis(2-chloroethyl)ether BRL IJgl 50
501 08-60- Bis(2-chloroisopropyl)ether BRL IJgl
117-81- Bis(2-ethylhexyl)phthalate BRL 1J91 50
101-55- Bromophenyl phenyl ether BRL IJgl 50
5085-68- Butyl benzyl phthalate BRL IJgl
5086-74- Carbazole BRL IJgl
5059-50- C hloro-3-methylphenol BRL IJgl
106-47- Chloroaniline BRL IJgl 50
91-58- Chloronaphthalene IJglBRL 50
5095-57 - Chlorophenol BRL 1J91
507005-72- Chlorophenyl phenyl ether BRL IJgl
216-01- Chrysene tJ91BRL 50
5053-70- Dibenzo (a h) anthracene BRL IJgl
50132-64- Dibenzofuran BRL IJgl
95-50- Dichlorobenzene IJglBRL 50
541-73- 13- Dichlorobenzene BRL IJgl 50
106-46- Dichlorobenzene 1J91BRL 50
5091-94- 3 - Dichlorobenzidine BRL IJgl
120-83- Dichlorophenol BRL IJgl 50
84-66- Diethyl phthalate BRL IJgl 50
131-11- Dimethyl phthalate BRL IJgll 50
105-67- Dimethylphenol BRL 1J91 50
5084-74- Di-n- butyl phthalate BRL 1J91
534-52 - Dinitro-2-methylphenol BRL IJgl 50
51-28- Dinitrophenol IJglBRL 50
50121-14- Dinitrotoluene BRL 1J91
606-20- Dinitrotoluene IJglBRL 50
50117-84-0 Di-n-octyl phthalate BRL IJgl
206-44-0 Fluoranthene 1J91BRL 50
BRL 50
50 86-73- Fluorene IJgi
118-74- Hexachlorobenzene BRL 1J91
87-68- Hexachlorobutadiene 1J91BRL 50
5077-47-4 Hexachlorocyclopentadiene BRL IJgl
67-72- Hexachloroethane IJglBRL 50
50193-39- Indeno (1 3-cd) pyrene BRL IJgl
5078-59- Isophorone BRL IJgl
Tfls laboratory report is not valid without all authorized signature 011 the coverpage
Page 6 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Sam le Identification Client Pro ect Matrix Collection DateTime ReceivedMWshy
2920-96- Ground Water I3-May-081030 14-May-SA 78602shy
CAS No Analyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Semivolatile Organic Compounds by GCMS
Semi volatile Or anic Com ounds b EPA 625
Prepared by method SW846 3510C
91-57 -6 Methylnaphthalene 367 1-91 50 EPA 625 16-May- 19-May-08 8051216
95-48- Methylphenol BRL 1-91 50
108-39-4 3 amp 4-Methylphenol BRL I-gl 100 106-44shy91-20- Naphthalene 247 1-91 50
88-74-4 Nitroaniline BRL 1-91 50
99-09- Nitroaniline BRL 1-91 50
100-01-6 Nitroaniline BRL 1-91 50
98-95- Nitrobenzene BRL 1-91 50
88-75- Nitrophenol BRL 1-91 50
100-02- Nitrophenol BRL 1-91 50
62-75- Nitrosodimethylamine BRL 1-91 50
621-64- N- Nitrosodi-n-propylamine BRL 1-91 50
86-30-6 Nitrosodiphenylamine BRL 1-91 50
87 -86- Pentachlorophenol BRL 1-91 50
85-0- Phenanthrene BRL 1-91 50
108-95- Phenol BRL 1-91 50
129-00-0 Pyrene BRL 1-91 50
110-86- Pyridine BRL 1-91 50
120-82- 4- Trichlorobenzene BRL 1-91 50
95-95- 5- Trichlorophenol BRL 1-91 50
88-06- 6- T richlorophenol BRL 1-91 50
Surrogate recoveries
321-60- Fluorobipheny 30- 130
367- 12- Fuorophenol 15- 110
4165-60- Nitrobenzene- 30- 130
4165-62- Pheno- 15- 110
1718-51- Terpheny-d4 30- 130
118- 79- 6- Tribromophenol 15- 110
Semivolatile Organic Compounds by GC
Pol chlorinated Bi hen ls b EPA 608
Prepared by method SW846 3510C
12674- 11-2 Aroclor- 1016 BRL 1-91 0650 EPA 608 15- May- 16-May-08 8051106
11104-28-2 Aroclor-1221 BRL IJgl 0650
11141-16-5 Aroclor- 1232 BRL 1-91 0650
53469-21-9 Aroclor- 1242 BRL 1-91 0650
12672-29-6 Aroclor- 1248 BRL 1-91 0650
11097-69-1 Aroclor- 1254 BRL 1-91 0650
11096-82-5 Aroclor -1260 BRL 1-91 0650
37324-23-5 Aroclor-1262 BRL 1-91 0650
11100-14-4 Aroclor-1268 BRL IJgl 0650
Surrogate recoveries
2051-24- Decachlorobipheny (Sr) 105 30- 150
10386-84-2 4 DB-Octafluorobiphenyl (Sr) 30- 150
Extractable Petroleum Hydrocarbons
mgl EPA 1664 Rev A 15-May- 19-May-08 8051102Non-polar material (SGT- HEM)
Soluble Metals by EPA 2006000 Series Metbods
Field Filtered NA EPA 200 73005A 15- May- 15-May-08 8051192Filtration
Soluble Metals by EPA 200 Series Methods
7440-22-4 Silver BRL mgl 0002 EPA 200 21-May- 27- May-08 8051249
This laboratory report is IlOt mlid without (II authorized signature on the cover page
Reportble Detection Limit BRL = Below Reporting Limit Page 7 of 25
Sam le Identification MW-
Client Pro ect 2920-96shy
Matrix Ground Water
Collection DateTime 13-May-08 1030
Received 14-May-
SA 78602shy
CAS No A nalyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Soluble Metals by EPA 200 Series Methods
7440-38shy Arsenic 0468 mg1 0040 EPA 200 21-Mayshy 21-May-08 80511 50
7440-43shy Cadmium BRL mg1 0002 EPA 200 21-May-088051249
7440-47shy Chromium BRL mg1 0050 EPA 200 21-May-088051150
7440-50-8 Copper BRL mg1 0050
7439-89-6 Iron 184 mg1 0150
7439-97-6 Mercury BRL mg1 00020 EPA 245 17470A 21-May-088051152
7440-02-0 Nickel BRL mg1 0050 EPA 200 21-May-088051150
7439-92shy Lead 0011 mg1 0002 EPA 200 21-May-088051249
7440-36-0 Antimony 0003 mg1 0002
7782-49shy Selenium BRL mg1 0150 EPA 200 21-May-08 8051150
7440-66-6 Zinc 0186 mgl 0050
General Chemistry Parameters
Filtration Completed NA Varies 14-Mayshy 14-May-08 8051095
18540-29-9 Hexavalent Chromium (soluble) BRL HT2 mg1 125 SM3500CrDI796A 14-Mayshy 14-May-08 8051094 R01 2013 2016
57-12shy Cyanide (total) BRL mg1 0100 EPA 3354 19-Mayshy 19-May-088051374
7782-50shy Total Residual Chlorine BRL CIHT mg1 500 Hach 8167 14-Mayshy 14-May-08 8051049 R01 1900 2001
Total Suspended Solids 580 mg1 25 SM2540D 16-Mayshy 16-May-08 8051275
This lahomtOlY report is not valid without an authorized signature on the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page 8 of 25
Volatie Organic Compounds - Quality Control
Analyte( s)
Batch 8051244 - SW846 5030 Water MS
Blank 8051244-BLK1
Prepared 16-May-08 Analyzed 17-May-
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromochloromethane
1 Dichlorobenzene
1 Dichlorobenzene
1 Dichlorobenzene
1-Dichloroethane
1 Dichloroethane
1 1-Dichloroethene
cis- Dichloroethene
trans- 1 Dichloroethene
1 Dichloropropane
cis- 1 Dichloropropene
trans- 1 Dichloropropene
Ethylbenzene
Hexanone (MBK)
Methyl tert-butyl ether
Methyl- pentanone (MIBK)
Methylene chloride
Styrene
2- Tetrachloroethane
Tetrachloroethene
Toluene
1- Trichloroethane
2- Trichloroethane
Trichloroethene
Trichlorofluoromethane (Freon 11)
Vinyl chloride
p-Xylene
Xylene
Surrogate 4-Bromofluorobenzene Surrogate Toluene-
Surrogate 1 Dichloroethane-Surrogate Dibromofluoromethane
LCS B051244-BS1
Prepared 16-May-08 Analyzed 17 -May-
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Spike Source REC RPD
Result Flag Units RDL Level Result REC Limits RPD Limit
BRL gl 20
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl 10
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gll
BRL gi
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl 10
BRL gll
BRL gll 10
BRL gl 10
BRL gll
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
41 gl 50 70- 130 49 gl 50 70- 130 59 gl 50 119 70- 130 52 gl 50 105 70- 130
QC2 jgl 20 70- 130
18 jgl 20 70- 130
192 jgl 20 35- 155
18 jgl 20 45- 169
19 jgl 20 242
This laboratOlY repol1 is lot valid without 011 authorized sigllature 011 the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page 9 of 25
Volatie Organic Compounds - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051244 - SW846 5030 Water MS
LC5 8051244B51
Prepared 16-May-08 Analyzed 17-May-
Butanone (MEK) 10 QC2 gl 20 70- 130
Carbon tetrachloride 204 gl 20 102 70- 140
Chlorobenzene 18 gl 20 70- 130
Chloroethane 164 gl 20 14-230
Chloroform 18 gll 20 51- 138
Chloromethane 21 gl 20 106 273
Dibromochloromethane 18 gl 20 53- 149
1 Dichlorobenzene 20 gl 20 104 18- 190
1 Dichlorobenzene 19 gl 20 59- 156
1 A-Dichlorobenzene 18 gl 20 18- 190
1- Dichloroethane 19 gl 20 59- 155
1 Dichloroethane 19 gl 20 49- 155
1-Dichloroethene 16 gl 20 70- 130
cis- 1 Dichloroethene 17 gl 20 70- 130
trans- 1 Dichloroethene 16 gll 20 54- 156
1 Dichloropropane 18 gl 20 210
cis- Dichloropropene 17 gl 20 227
trans- 1 Dichloropropene 17 gl 20 17- 183
Ethylbenzene 19 gl 20 37- 162
Hexanone (MBK) 124 QC2 gl 20 70- 130
Methyl tert-butyl ether 19 gl 20 70- 130
Methylshy pentanone (MIBK) 17 gl 20 70- 130
Methylene chloride 16 gl 20 221
Styrene 17 gl 20 70- 130
1 Tetrachloroethane 194 gl 20 46- 157
Tetrachloroethene 15 gl 20 64- 148
Toluene 18 gl 20 70- 130
1- Trichloroethane 20 gl 20 100 52- 162
2- Trichloroethane 18 gl 20 52- 150
Trichloroethene 17 gl 20 71- 157
Trichlorofluoromethane (Freon 11) 19 gl 20 17- 181
Vinyl chloride 21 gl 20 106 251
p-Xylene 39 gl 40 70- 130
Xylene 20 gl 20 102 70- 130
Surrogate 4-Bromofluorobenzene Surrogate Toluene-
Surrogate 1 Dichloroethane-Surrogate Dibromofluoromethane
52 49 56
49
gl
gl
gl
gl
50 50 50
50
105
112 100
70- 130 70- 130 70- 130 70- 130
LC5 DUD (8051244-B5D1
Prepared 16-May-08 Analyzed 17-May-
Acetone QC2 gl 20 70- 130
Benzene 18 gl 20 70- 130
Bromodichloromethane 18 gl 200 35- 155
Bromoform 17 gl 20 45- 169
Bromomethane 18 gl 20 242
Butanone (MEK) 11 QC2 1-91 20 70- 130
Carbon tetrachloride 20 gl 20 100 70- 140
Chlorobenzene 17 gl 20 70- 130
Chloroethane 15 1-91 20 14-230
Chloroform 18 1-91 20 51- 138
This laboratory report is aot valid without a1 authorized sig1ature 01 the cover page
Reportble Detection Limit BRL = Below Reporting Limit Page 10 of25
Volatie Organic Compounds - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051244 - SW846 5030 Water MS
LCS Dup 18051244-BSD1
Prepared 16-May-08 Analyzed 17-May-
Chloromethane 18 1-91 20 273
Dibromochloromethane 174 1-91 20 53- 149
Dichlorobenzene 20 1-91 20 100 18- 190
Dichlorobenzene 18 1-91 20 59- 156
Dichlorobenzene 18 1-91 20 18- 190
Dichloroethane 18 1-91 20 59- 155
Dichloroethane 19 1-91 20 49- 155
Dichloroethene 16 1-91 20 70- 130
cis- Dichloroethene 16 1-91 20 70- 130
trans- Dichloroethene 15 1-91 20 54- 156
Dichloropropane 17 1-91 20 210
cis- Dichloropropene 164 IJgl 20 227
trans- 1 Dichloropropene 164 I-gl 20 17- 183
Etlwlbenzene 18 IJgl 20 37- 162
Hexanone (MBK) 124 QC2 IJgl 20 70- 130
Methyl tert-butyl ether 184 1J91 20 70- 130
Methyl- pentanone (MIBK) 17 IJgl 20 70- 130
Methylene chloride 16 IJgl 20 221
Styrene 16 IJgl 20 70- 130
2- Tetrachloroethane 19 IJgl 20 46- 157
Tetrachloroethene 15 IJgl 20 64- 148
Toluene 17 IJgl 20 70- 130
1- Trichloroethane 19 1-91 20 52- 162
2- Trichloroethane 16 IJgl 20 52- 150
Trichloroethene 15 IJgl 20 71- 157
Trichlorofluoromethane (Freon 11) 17 IJgl 20 17- 181
Vinyl chloride 19 IJglI 20 251
p-Xylene 37 1J91 40 70- 130
Xylene 20 IJgl 20 100 70- 130
Surrogate 4-Bromofluorobenzene 51 IJgl 50 104 70- 130
Surrogate Toluene- 4B gl 50 70- 130
Surrogate 1 0ichloroethane- 53 IJgl 50 106 70- 130 Surrogate Oibromofluoromethane 50 1J9i 50 102 70- 130
Matrix S ike B051244-MS1 Source SA7B629shy
Prepared 16-May-08 Analyzed 17-May-
Benzene 18 20 BRL 70- 130IJgl
Bromodichloromethane 19 IJgl 20 BRL 35- 155
Bromoform 18 IJgl 20 BRL 45- 169
Bromomethane 16 IJgl 20 BRL 242
Carbon tetrachloride 21 IJgl 20 BRL 106 70- 140
Chlorobenzene 18 IJgl 20 BRL 70- 130
Chloroethane 16 IJgl 20 BRL 14-230
Chloroform 18 IJgl 20 BRL 51- 138
Chloromethane 19 IJgl 20 BRL 273
Dibromochloromethane 17 IJgl 20 BRL 53- 149
1 Dichlorobenzene 22 IJgl 20 BRL 112 18- 190
1 Dichlorobenzene 22 IJgl 20 BRL 110 59-156
1 Dichlorobenzene 21 IJgl 20 BRL 109 18- 190
1- Dichloroethane 19 IJgl 20 BRL 59- 155
1 Dichloroethane 18 IJgl 20 BRL 49- 155
This laboratory report is 110t mUd without an authorized signature on the covel page
Reportble Detection Limit BRL = Below Reporting Limit Page It of25
Volatile Organic Compounds - Quality Control
p
Spike Source REC RPD
Result REC imits RPD LimitAnalyte(s) Result Flag Units RDL Level
Batch 8051244 - SW846 5030 Water MS
Matrix ike S051244-MS1 Source SA7B629shy
Prepared 16-May-08 Analyzed 17-Mayshy
17 20 BRL 70- 130 1- Dichloroethene IJgl
16 20 BRL 54- 156trans- 1 Dichloroethene IJgl
21020 BRL1 Dichloropropane 17 1J91
cis- 1 Dichloropropene 17 IJgl 20 BRL 227
17- 183trans- 1 Dichloropropene 184 1J91 20 BRL
20 20 BRL 103 37- 162Ethylbenzene IJgl
15 20 BRL 221Methylene chloride IJgl
20 BRL 46- 1572- Tetrachloroethane 19 1J91
20 BRL 64- 148Tetrachloroethene 18 1J91
BRL 70- 130Toluene 18 1J91 20
105 52-1621- Trichloroethane 211 IJgl 20 BRL
18 20 BRL 52- 1502- Trichloroethane IJgl
17 20 BRL 71- 157Trichloroethene 1J91
20 BRL 17- 181Trichloroluoromethane (Freon 11) 194 IJgl
20 BRL 103 251Vinyl chloride 20 IJgl
102 70- 130Surrogate 4-Bromofluorobenzene 50 IJgl 50 50 70- 130Surrogate Toluene- 49 1J91
56 50 112 70- 130Surrogate 1 Dichloroethane- IJgl
50 100 70- 130Surrogate Dibromofluoromethane 50 IJgl
Matrix S ike Du S051244-MSD1 Source SA7S629shy
Prepared 16-May-08 Analyzed 17-Mayshy
18 20 BRL 70- 130Benzene IJgl
18 20 BRL 35- 155Bromodichloromethane IJgl
17 20 BRL 45- 169Bromoform IJgl
20 BRL 242Bromomethane 17 IJgl
20 BRL 103 70- 140Carbon tetrachloride 20 IJgl
18 20 BRL 70- 130Chlorobenzene 1J91
14-230Chloroethane 16 IJgl 20 BRL
20 51- 138Chloroform 184 IJgl BRL
Chloromethane 19 1J91 20 BRL 273
18 20 BRL 53- 149Dibromochloromethane 1J91
20 BRL 117 18- 190Dichlorobenzene 234 IJgl
20 BRL 112 59- 156Dichlorobenzene 22 IJgl
BRL 108 18- 190Dichlorobenzene 21 1J91 20
20 59- 1551 Dichloroethane 19 IJgl BRL
18 20 BRL 49- 155Dichloroethane IJgl
16 20 BRL 70- 130Dichloroethene IJgl
20 BRL 54- 156trans- Dichloroethene 154 1J91
20 BRL 210Dichloropropane 17 IJgl
0420 BRL 227cis- Dichloropropene 17 IJgl
17- 183trans- Dichloropropene 17 1J91 20 BRL
BRL 37- 162Ethylbenzene 20 1J91 20 102
Methylene chloride 15 IJgl 20 BRL 221
20 BRL 46- 1572- Tetrachloroethane 192 IJgl
20 BRL 64- 148 04Tetrachloroethene 18 IJgl
BRL 70- 130Toluene 184 1J91 20
52- 1621- Trichloroethane 20 IJgl 20 BRL 104
17 20 BRL 52- 1502- Trichloroethane IJgl
17 20 BRL 71- 157Trichloroethene IJgl
20 BRL 17-181Trichlorofluoromethane (Freon 11) 19 IJgl
This laboratory report is IIOt valid without all authorized sigllllture 011 the cover page
Page 12 of25 Reportble Detection Limit BRL = Below Reporting Limit
Semivolatile Organic Compounds by GCMS - Quality Control
Analyte(s)
Batch 8051216 - SW846 3510C
Blank 8051216-BLK1
Prepared amp Analyzed 16-May-
Isophorone
Methylnaphthalene
Methylphenol
3 amp 4-Methylphenol
Naphthalene
Nitroaniline
Nitroaniline
Nitroaniline
Nitrobenzene
Nitrophenol
Nitrophenol
Nitrosodimethylamine
N- N itrosodi-n-pro pyla mine
N itrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Pyridine
1 24-Trichlorobenzene
24 5- Trichlorophenol
246- Trichlorophenol
Surrogate 2-Fuorobipheny Surrogate 2-Fuoropheno Surrogate Nitrobenzene-Surrogate PhenoshySurrogate Terpheny-d4 Surrogate 6- Tribromopheno
LCS B051216-BS1
Prepared amp Analyzed 16-May-
Acenaphthene
Acenaphthylene
Aniline
Anthracene
AzobenzenelDi phenyld lazine
Benzidine
Benzo (a) anthracene
Benzo (a) pyrene
Benzo (b) fluoranthene
Benzo (g i) perylene
Benzo (k) fluoranthene
Benzoic acid
Benzyl alcohol
B is(2-chloroethoxy)methane
B i s (2-ch loroethyl)eth e r
Bis(2-ch loroisopropyl) ether
B is(2-ethy Ih exyl) phtha late
Bromophenyl phenyl ether
Butyl benzyl phthalate
Carbazole
Spike Source REC RPD
Result Flag Units RDL Level Result REC Limits RPD Limit
BRL gl
BRL gl
BRL gl
BRL gl 10
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gll
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
370 gl 50 30- 130 40 gl 50 15- 110 39 gl 50 30- 130 43 gl 50 15- 110 36 gl 50 30- 130 40 gl 50 15- 110
41 gl 50 40- 140
43 gI 50 40- 140
41 gl 50 40- 140
38 gl 50 40- 140
45 gl 50 40- 140
49 gl 50 153
41 gl 50 40- 140
43 gl 50 40- 140
41 gl 50 40- 140
41 gll 50 40- 140
45 gl 50 40- 140
32 gl 50 12- 149
41 gl 50 40- 140
39 gl 50 40- 140
384 gl 50 40- 140
47 gl 50 40- 140
47 gl 50 40- 140
40 gl 50 40- 140
47 gI 50 40- 140
56 gI 50 112 200
This laboratory report is lIot valid witllOut a1l authorized sigllature 011 the coverpage
Reportble Detection Limit BRL = Below Reporting Limit Page 15 of25
Semivolatile Organic Compounds by GCMS - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051216 - SW846 3510C
LCS 8051216-BS1
Prepared amp Analyzed 16-Mayshy
50 30- 1304 -C hloro-3-methylphenol 42 IJgl
40- 140Chloroaniline 39 IJgl 50
Chloronaphthalene 37 IJgl 50 40- 140
Chlorophenol 37 IJgl 50 30- 130
50 40- 140
40- 140
Chlorophenyl phenyl ether 45 IJgl
Chrysene 43 IJgl 50
Dibenzo (a h) anthracene 43 IJgl 50 40- 140
Dibenzofuran IJgl38 50 40- 140
50 40- 1401 Dichlorobenzene 35 IJgl
40- 1401 Dichlorobenzene 264 IJgl 50
40- 1401 Dichlorobenzene 434 IJgl 50
58 50 116 40- 1403 - Dichlorobenzidine IJgl
50 30- 130
40- 140 24-Dichlorophenol 38 IJgl
Diethyl phthalate 484 IJgl 50
50 40- 140Dimethyl phthalate 464 IJgl
Dlmethylphenol 39 IJgl 50 30- 130
DI-n-butyl phthalate 44 IJgll 50 40- 140
30- 130 6-Di nitro- 2-methylphenol 38 1J91 50
30- 130Dinltrophenol 36 1J91 50
42 50 40- 14024-Dlnitrotoluene 1J91
Dlnitrotoluene 1J9141 50 40- 140
Di-n-octyl phthalate 52 IJgl 50 104 40- 140
40- 140Fluoranthene 40 IJgl 50
Fluorene 41 IJgl 50 40- 140
39 50 40- 140Hexachlorobenzene IJgl
50 40- 140Hexachlorobutadiene 40 IJgl
40- 140Hexach lorocyclopentad iene 294 IJgl 50
40 50 40- 140Hexachloroethane IJgl
42 50 40-140Indeno (1 3-cd) pyrene IJgl
50 40- 140Isophorone 40 IJgl
40- 140Methylnaphthalene 394 IJgl 50
40- 140Methylphenol 39 IJgl 50
40 10 50 40- 1403 amp 4-Methylphenol IJgl
37 50 40-140Naphthalene IJgl
50 40-140Nitroaniline 39 IJgl
Nitroaniline 51 IJgl 50 102 40- 140
48 50 40- 140Nltroaniline 1J91
50 40- 140Nitrobenzene 40 IJgl
30- 130Nitrophenol 36 IJgl 50
40 IJgl 50 30- 130Nitrophenol 40- 140Nitrosodimethylamine 32 1J91 50
50 40-140N- N itrosodi-n-propyla mine 46 IJgl
40- 140N itrosodi phenyla ml ne 44 IJgl 50
41 IJgl 50 30- 130Pentachlorophenol 40- 140Phenanthrene 38 IJgl 50
50 30- 130Phenol 38 IJgl
40- 140Pyrene 424 1J91 50
40- 140Pyridine 294 1J91 50
40- 14024- Trichlorobenzene 364 IJgl 50
This laboratory report is not mlid without an authorized signature 011 the cover page
Page 16 of25 Reportble Detection Limit BRL = Below Reporting Limit
Semivolatie Organic Compounds by GCMS - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
BMch 8051216 - SW846 3510C
LC5 8051216-851
Prepared amp Analyzed 16-Mayshy
24 5- Trichlorophenol 404 gl 50 30- 130
246- Trichlorophenol 42 gl 50 30- 130
Surrogate 2-Fluorobiphenyl 29 gl 50 30- 130
Surrogate 2-Fluorophenot 27 gl 50 15- 110
Surrogate Nitrobenzene- 30 gl 50 30- 130
Surrogate Phenol- 29 gl 50 15- 110
Surrogate Terpheny-d4 30 gl 50 30- 130
Surrogate 6- Tribromopheno 324 gl 50 15- 110
This laboratory report is lIot valid without all authorized sigllature 011 tlle cover page
Reportble Detection Limit BRL = Below Reporting Limit Page 17 of25
Semivolatie Organic Compounds by GC - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051106 - SW846 3510C
Blank S051106-BLK1
Prepared amp Analyzed 15-Mayshy
Aroclor- 1016 BRL gI 0200
Aroclor- 1016 (2C) BRL gI 0200
Aroclor- 1221 BRL gI 0200
Aroclor- 1221 (2C) BRL gI 0200
Aroclor- 1232 BRL gI 0200
Aroclor- 1232 (2Cj BRL gI 0200
Aroclor- 1242 BRL gI 0200
Aroclor-1242 (2C) BRL gI 0200
Aroclor- 1248 BRL gI 0200
Aroclor- 1248 (2C) BRL gI 0200
Aroclor- 1254 BRL gI 0200
Aroclor- 1254(2Cj BRL gI 0200
Aroclor- 1260 BRL gI 0200
Aroclor- 1260 (2C) BRL gI 0200
Aroclor- 1262 BRL gI 0200
Aroclor- 1262 (2C) BRL gI 0200
Aroclor-1268 BRL gI 0200
Aroclor- 1268 (2C) BRL gI 0200
Surrogate Decachlorobiphenyl (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0231 0224 0194 0191
gI
gI
gI
gI
0200 0200 0200 0200
116 112
30- 150 30- 150 30- 150 30- 150
LC5 8051106-B51
Prepared 15-May-08 Analyzed 16-May-08
Aroclor- 1016 265 gI 0200 250 106 50- 114
Aroclor- 1 016 (2C) 240 gI 0200 250 50- 114
Aroclor- 1260 0269 gI 0200 250 107 40- 127
Aroclor-1260 (2Cj 270 gI 0200 250 108 40- 127
Surrogate Decachlorobiphenyl (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0225 0224 0188 0183
gI
gI
gI
gI
0200 0200 0200 0200
113 112
30- 150 30- 150 30- 150 30- 150
LC5 DUD rS051106-B5D1
Prepared 15-May-08 Analyzed 16-Mayshy
Aroclor- 1016 262 gl 0200 250 105 50- 114
Aroclor-1 016 (2Cj 241 gI 0200 250 50- 114
Aroclor- 1260 277 gI 0200 250 111 40- 127
Aroclor- 1260(2Cj 0260 gI 0200 250 104 40- 127
Surrogate Decachlorobipheny (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0238 0218 0189 0181
gI
gI
gI
gI
0200 0200 0200 0200
119 109
30- 150 30- 150 30- 150 30- 150
This laboratory report is lot valid without (II authorized sigllature 01 the cover page
Page 18 of25 Reportable Detection Limit BRL = Below Reporting Limit
Extractable Petroleum Hydrocarbons - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051102 - SW846 3510C
Blank 8051102-BLK1
Prepared 15-May-08 Analyzed 19-Mayshy
Non-polar material (SGT- HEM) BRL m91
LC8 8051102-B81
Prepared 15-May-08 Analyzed 19-Mayshy
Non-polar material (SGT- HEM) 184 m91 21 81 904
This laboratory report is not valid without an authorized signature 011 the cover page
Page 19 of25 Reportable Detection Limit BRL = Below Reporting Limit
Soluble Metals by EPA 200 Series Methods - Quality Control
Analyte(s) Result Flag Units RDL
Spike
Level
Source
Result REC
REC
Limits RPD
RPD
Limit
Batch 8051150 - EPA 200 Series
Blank 8051150-BLK1
Prepared amp Analyzed 21-May-
Iron
Zinc
Selenium
Nickel
Chromium
Copper
Arsenic
BRL
BRL
BRL
BRL
BRL
BRL
BRL
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0150
0050
0150
0050
0050
0050
0040
LCS 8051150-BS1
Prepared amp Analyzed 21-May-
Selenium
Zinc
Iron
Nickel
Chromium
Arsenic
Copper
123
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0150
0050
0150
0050
0050
0040
0050
103
105
101
100
85- 115
85- 115
85- 115
85- 115
85- 115
85-115
85- 115
licate B051150-DUP1 Source SA7B602shy
Prepared amp Analyzed 21-May-
Iron
Zinc
Selenium
Nickel
Copper
Chromium
Arsenic
17
0162
BRL
0015
0017
BRL
0450
QR8
mgl
mgl
mgl
mgl
mgl
mgl
mgi
0150
0050
0150
0050
0050
0050
0040
184
0186
BRL
0014
0023
BRL
0468
Matrix S ike 8051150-MS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Iron
Selenium
Nickel
Zinc
Copper
Chromium
Arsenic
19 QM2 mgl
mgll
mgl
mgl
mgl
mgl
mgl
0150
0150
0050
0050
0050
0050
0040
125
184
BRL
0014
0186
0023
BRL
0468
104
105
102
70- 130
70- 130
70-130
70- 130
70- 130
70-130
70- 130
Post S ike 8051150-PS1 Source SA78602shy
Prepared amp Analyzed 21-May-
Zinc
Iron
Selenium
Nickel
Copper
Arsenic
Chromium
18 QM2
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0050
0150
0150
0050
0050
0040
0050
0186
184
BRL
0014
0023
0468
BRL
104
104
101
85- 115
85- 115
85- 115
85-115
85-115
85- 115
85-115
Batch 8051152 - EPA200SW7000 Series
Blank B051152-BLK1
Prepared amp Analyzed 21-May-
Mercury BRL mgl 00020
This laboratory report is IIOt valid witllOut all authorized sigllature 011 the coverpage
Page 20 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Soluble Metals by EPA 200 Series Methods - Quality Control
Analyte(s) Result Flag Units RDL
Spike
Level
Source
Result REC
REC
Limits RPD
RPD
Limit
Batch 8051152 - EPA200SW7000 Series
LCS B051152-BS1
Prepared amp Analyzed 21-May-
Mercury 00576 m91 00020 00500 115 85- 115
licate B051152-DUP1 Source SA78602-01
Prepared amp Analyzed 21-May-
Mercury BRL m91 00020 BRL
Matrix S ike 8051152-MS1 Source SA78602shy
Prepared amp Analyzed 21-May-
Mercury 00632 OM m91 00020 00500 BRL 126 75- 125
Post S ike 8051152-PS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Mercury 00624 OC1 m91 00020 00500 BRL 125 85- 115
Batch 8051249 - 2008No digestion
Blank 8051249-BLK1
Prepared amp Analyzed 21-May-
Lead
Antimony
Cadmium
Silver
BRL
BRL
BRL
BRL
m91
m91
m91
m91
0002
0002
0002
0002
LCS B051249-BS1
Prepared amp Analyzed 21-May-
Antimony
Lead
Silver
Cadmium
143
145 OC2
m91
m91
m91
m91
0050
0050
0050
0040
103
115
107
116
85- 115
85- 115
85- 115
85- 115
licate 8051249-DUP1 Source SA7B602shy
Prepared amp Analyzed 21- May-
Lead
Antimony
Cadmium
Silver
0009
0002
00005
00002
ORB
m91
m91
m91
m91
0002
0002
0002
0002
0011
0003
00005
00003
Matrix S ike 8051249-MS1 Source SA78602shy
Prepared amp Analyzed 21- May-
Lead
Antimony
Cadmium
Silver
142
m91
m91
m91
m91
0050
0050
0040
0050
0011
0003
00005
00003
111
101
114
102
70- 130
70-130
70c130
70- 130
Post S ike 8051249-PS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Antimony
Cadmium
Silver
38
OC2
m91
m91
m91
0050
0040
0050
125
0003
00005
00003
110
121
109
85- 115
85- 115
85- 115
This laboratory report is flOt valid IVithout all authorized signature 011 the cOIer page
Reportable Detection Limit BRL Below Reporting Limit Page 21 of 25
General Chemistry Parameters - Quality Control
Spike Source REC RPD
Analyte( s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051049 - General Preparation
Blank S051 049-BLK1
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
Blank S051049-BLK2
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
Blank S051 049-BLK3
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
LCS S051049-BS1
Prepared amp Analyzed 14-May-
Total Residual Chlorine 046 mgl 020 0500 90- 110
LCS S051049-BS2
Prepared amp Analyzed 14-May-
Total Residual Chlorine 047 mgl 020 0500 90- 110
LCS S051049-BS3
Prepared amp Analyzed 14-May-
Total Residual Chlorine 054 mgl 020 0500 108 90-110
licate B051049-DUP1 Source SA7S544shy
Prepared amp Analyzed 14-May-
Total Residual Chlorine 012 mgl 020 010
licate S051049-DUP2 Source SA7S602-01
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020 BRL
Matrix S ike 8051049-MS1 Source SA78544-01
Prepared amp Analyzed 14-May-
Total Residual Chlorine 065 mgl 020 0500 010 110 80- 120
Matrix S ike 8051049-MS2 Source SA7B602shy
Prepared amp Analyzed 14-May-
Total Residual Chlorine mgl 500 125 BRL 108 80- 120
Reference 8051 049-SRM1
Prepared amp Analyzed 14-May-
Total Residual Chlorine 100 mgl 020 0967 103 85-115
Batch 8051094 - General Preparation
Blank 8051094-BLK1
Prepared amp Analyzed 14 May-
Hexavalent Chromium (soluble) BRL mgl 005
Blank 8051 094-BLK2
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) BRL mgl 005
LCS 8051094-BS1
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) 054 mgl 005 90- 110
licate 8051094-DUP1 Source SA78602-01
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) BRL mgl 125 BRL
Thi laboratory report is not valid without all authorized sigllature 011 the cover page
Page 22 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Page 12
-
D- 0
0 0
il (J tu
Bw
o(0 -I
NJW
gQb
J(JZc o c
rou a -10
0 J 6shy
a 0
I-tDC
aJ Qj
E aJshy
ro ro ro
~~~ ~~~~- -- - _ - -_ - ~~~ ~~~~ ~~~ - - _- _- -- -- p __(
MA DEP - Bureau of Waste Site CleanupSITE NME Site S aP 5 MiFlII Former Speeway Station _-II181 Eat Broaday b b d IS I i I GARDNER MA 0144 v ri) i P f f 1 me- 1 5ylmI I L shy J --I 423315n 715835e SiteLocation y o oCop1odQcn Ofof W-_ l
1 1 I
r
r
iBARBER HILL
A c
Cf1 f o s
0
5
Roads Uned Acss Divd Mar Roed Conntor Street Track 1 EPA Sola Source Aquilar FEMA 100yaar iloodplain 0 c Puc Watar SLo GrunSelaceNon Corrty 0
Bounars lOwn Couny DE Region Tian Powerln Ine Aqedut ApprOld Zona2 tNPA Sue Wster Supp Zone A bStZ F--shy--rle
8os Mat Sub SUeor Porenrial Inermtent Man lvo8 Ste Dfm Hyro1apy Wmer FeatllePLio Suleee Wat S H-- L otlMds FrslSaltN-ES WeIMd Habat L
Potentia Prdutiv AqlJlers ModHig Yield Proteoted Opn Space ACC nIL c= Non-Potential Drng Water Sollce AIea ModumHi Yo1d ll DEP Pormrd SoidWes1 FsiIi6s cnifud Verne Pools f0
1I2 KIWUmR$ MtL
January 30 2004 SCALE 1 15000
-
LE
GE
ND
APX PROPER BONDA
- APPROXOiSPO SIT BOUNDA
-GR
OU
ND
WA
TE F1 D
IRE
cnON
SCA
LE
30 60 FE
(APR
OX
CORPORATE ENVIRONMENTAL
)i
AD
VISO
RS
INC
SC
AS SH
OW
D
R B
Y K
HA
EL
DA
TE
10407
JOB
NO
2920-96
AERIAL MAP
FO
RM
ER
SP
EE
DW
AY
ST
AT
ION
FlGURE -3
181 EA
BR
OA
AY
GA
NE
R fo
age 1 ot 1Streamflow Statistics Report
Streamstats Ungaged Site Report Date Wed Dec 31 2008 124908 Site Location Massachusetts NAD83 Latitude 425545 (42 3316) NAD83 Longitude -719758 (-71 58 32) NAD27 Latitude 425545 (423316) NAD27 Longitude - 9763 (-71 58 34) Drainage Area 502 mi2
IPeak Flow Basin Characteristics 1100 Statewide Low Flow (S02 mi2)
Regression Equation Valid Rang
I Min II Max1 Value III Parameter Drainage Area (square miles) 161 149
Mean Basin Slope from 250K DEM (percent) 032 24
Stratified Drift per Stream Length (square mile per mile) 129
Massachusetts Region (dimensionless)
Streamflow Statistics
gO-Percent Prediction Interval Prediction Error
MaximumStatistic Flow (ft s) (percent) Minimum
I D50 IIII 11 1811 II 24511 993
I D60 II 35511 2011 II 03611 35111 2411 II 041 I 201I D70 24111 2611 II 03811 151I D75 11 2811 II 0911 3761I D80 981I D85 1 I 3211 II o6311
1 I 3711 II 0441 1 2 2911 D90 11 4611 II 02411 15511 D95I D98 04511 6011 II 01511 11
I D99 03411 6511 II ol1ll 1021
5011 II 02611 11I M7D2Y 1111 3311 II odl 3 541
I AUGD50
IIIIIIIIIIIIIIIIIIIIII 0311 7111 II 0088411 0981I M7Dl0Y
1010
12312008httpstreamstatsagscrusgsgovgisimgReportsFlowStatsReport3494 - 2008123112498
Dilution Factor Calculation Former Speedway Service Station 181 East Broadway Gardner Ma
DF=(Od+Os)Od
DF = Dilution factor
Od = Max flow rate of discharge in cubic feet per second Os = receiving water flow in cubic feet per seconds 7010 flow rate Mahoney Brook 7010 = min flow for seven consecutive days with a recurrence interval of 10 years
7010 flow based on data obtained from USGS Steamflow Statistics Report Data attached
067
Semivolatile Organic Compounds by GCMS - Quality Control
Analyte( s)
Batch 8051216 - SW846 3510C
Blank 8051216BLK1)
Prepared amp Analyzed 16May-
Acenaphthene
Acenaphthylene
Aniline
Anthracene
AzobenzenelDi phenyld iazi ne
Benzidine
Benzo (a) anthracene
Benzo (a) pyrene
Benzo (b) fiuoranthene
Benzo (g i) perylene
Benzo (k) fiuoranthene
Benzoic acid
Benzyl alcohol
Bis(2-ch loroethoxy) methane
Bis(2-ch loroethyl)ether
Bis(2-ch loroi sopropyl)ether
Bis(2ethylhexyl) phthalate
Bromophenyl phenyl ether
Butyl benzyl phthalate
Carbazole
Ch loro-3-methyl phenol
Chloroaniline
Chloronaphthalene
Chlorophenol
Chlorophenyl phenyl ether
Chrysene
Dibenzo (a h) anthracene
Dibenzofuran
Dichlorobenzene
Dichlorobenzene
14- Dichlorobenzene
3 - Dichlorobenzidine
24-Dichlorophenol
Diethyl phthalate
Dimethyl phthalate
24- Dimethylphenol
Din-butyl phthalate
Dinitro-2-methylphenol
Dinitrophenol
Dinitrotoluene
Dinitrotoluene
Di-noctyl phthalate
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopehtadiene
Hexachloroethane
Indeno (1 cd) pyrene
Spike Source REC RPD
Result Flag Units RDL Level Result REC Limits RPD Limit
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gl
BRL gI
BRL gl
BRL gl
BRL gl
BRL gI
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gll
BRL gl
BRL gll
BRL gl
BRL gl
BRL gI
BRL gI
BRL gI
BRL gl
BRL gI
BRL gI
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gI
BRL gI
BRL gl
This laboratory report is IlOt valid without all authorized sigllature 011 the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page t4 of25
Volatie Organic Compounds - Quality Control
p (
Spike Source REC RPD
RDL Level Result REC Limits RPD Limit Analyte(s) Result Flag Units
Batch 8051244 - SW846 5030 Water MS
Matrix S ike Du 8051244-MSD1 Source SA78629shy
Prepared 16-May-08 Analyzed 17-May-BRL 106 251
Vinyl chloride 21 gl 20
101 70- 130 Surrogate 4-Bromofluorobenzene 50 gl 50
70- 13049 gl 50 111 70- 130
Surrogate Toluene-Surrogate 1 Dichloroethane- 55 gl 50
50 70- 130494 glSurrogate Dibromofluoromethane
Microextractable Organic Compounds - Quality Control
Spike Source REC RPD
Flag Units RDL Level Result REC Limits RPD Limit Analyte(s) Result
Batch 8051105 - SW846 3510C
Blank 8051105-BLK
Prepared amp Analyzed 15-May-
BRL gl 01001 Dibromoethane (ED B)
LCS 8051105-BS1
Prepared amp Analyzed 15-Mayshy50- 1500770 gl 0100 100
licate 8051105-DUP1 Source SA7B583shy
Prepared amp Analyzed 15-May-
BRL gl 0100 BRL
1 Dibromoethane (EDB)
1 Dibromoethane (EDB)
This laborntOlY report is not valid without an authorized signature 011 the cover page
Page 13 of2S Reportable Detection Limit BRL = Below Reporting Limit
Sam le Identification Client Pro ect Matrix Collection DateTime ReceivedMWshy
2920-96- Ground Water 13-May-081030 14-May-SA 78602shy
CAS No Analyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Volatile Organic Compounds
Volatile Or anic Com ounds b GCMS
Prepared by method SW846 5030 Water MS
123-91- Dioxane BRL 1-91 200 EPA 624 16-May-08 17-May-08 8051244
994-05-8 Ter-amyl methyl ether BRL 1-911 20
755- Tert-Butanoll butyl alcohol BRL 1-91 200
67-B4- Acetone BRL 1-91 400
71-43- Benzene BRL 1-91 20
75-27-4 Bromodichloromethane BRL 1-91 20
75-25- Bromoform BRL 1-91 20
74-83- Bromomethane BRL 1-91 40
78-93- Butanone (MEK) BRL 1-91 200
56-23- Carbon tetrachloride BRL 1-91 20
108-90- Chlorobenzene BRL 1-91 20
75-00- Chloroethane BRL 1-91 40
676- Chloroform BRL 1-91 20
74-87- Chloromethane BRL 1-91 40
124-48- Dibromochloromethane BRL 1-91 20
95-50- Dichlorobenzene BRL 1-911 20
541-73- Dichlorobenzene BRL 1-91 20
106-46- Dichlorobenzene BRL 1-91 20
75-34- 1- Dichloroethane BRL 1-91 20
107-06- Dichloroethane BRL 1-91 20
75-35-4 1- Dichloroethene BRL 1-91 20
156-59 cis- Dichloroethene BRL 1-91 20
156-60- trans- Dichloroethene BRL 1-91 20
78-87- 2- Dichloropropane BRL 1-91 20
10061-01-5 cis- Dichloropropene BRL 1-91 20
10061-02-B trans- Dichloropropene BRL 1-91 20
100-41-4 Ethylbenzene 411 1-911 20
591-78-B BRL 200Hexanone (MBK) 1-91
1634-04 -4 Methyl tert-butyl ether BRL 1-91 20
108-10- Methyl- pentanone (MIBK) BRL 1-91 200
75-09- Methylene chloride BRL 1-91 200
100-42- Styrene BRL 1-91 20
79-34- 1 Tetrachloroethane BRL 1-91 20
127- 18-4 T etrachloroethene BRL 1-91 20
108-88- Toluene BRL 1-91 20
71-55 1- Trichloroethane BRL 1-91 20
79-00- 2- Trichloroethane BRL 1-91 20
79-01-B Trichloroethene BRL 1-91 20
759-4 Trichlorofluoromethane (Freon 11) BRL 1-91 20
75-01-4 Vinyl chloride BRL 1-91 20
179601-23-1 m Xylene 390 1-91 40
95-47 Xylene 82 1-91 20
Surrogate recoveries 460-00- Bromofluorobenzene 70- 130
2037-26- Toluene- 100 70- 130
17060-07-0 1 Dichloroethane- 111 70- 130
1868-53- Dibromofluoromethane 70- 130
Microextractable Organic Compounds
106-93-4 1 Dibromoethane (EDB) BRL 1-91 0100 EPA 504 15-May- 15-May-08 8051105
Semivolatile Organic Compounds by GCMS
This laboratory report is not valid without all autllOrized signature 011 the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page 5 of 25
Sam le Identification Client Pro ect Matrix Collection DateTime Received
MWshy2920-96- Ground Water 13-May-081030 14-May-
SA 78602shy
CAS No Analyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Semivolatie Organic Compounds by GCMS
Semi volatile Or anic Com ounds b EPA 625
Prepared by method SW846 3510C 50 EPA 625 16-May- 19-May-08 805121683-32- Acenaphthene BRL IJgl
208-96-8 Acenaphthylene BRL IJgl 50
62-53- BRL IJgll 50Aniline
120- 12- Anthracene BRL 1J91 50
103-33- AzobenzenefDiphenyldiazine BRL IJgl 50
92-87 - Benzidine BRL IJgl 50
56-55- Benzo (a) anthracene BRL 1J91 50
50-32 - Benzo (a) pyrene IJglBRL 50
205-99- Benzo (b) fluoranthene BRL IJgl 50
191-24- Benzo (g i) perylene BRL IJgl 50
50207-08- Benzo (k) fluoranthene BRL IJgl
65-85 Benzoic acid BRL 1J91 50
100-51-6 Benzyl alcohol 1J91BRL 50
50111-91- Bis(2-chloroethoxy)methane BRL 1J91
111-4-4 Bis(2-chloroethyl)ether BRL IJgl 50
501 08-60- Bis(2-chloroisopropyl)ether BRL IJgl
117-81- Bis(2-ethylhexyl)phthalate BRL 1J91 50
101-55- Bromophenyl phenyl ether BRL IJgl 50
5085-68- Butyl benzyl phthalate BRL IJgl
5086-74- Carbazole BRL IJgl
5059-50- C hloro-3-methylphenol BRL IJgl
106-47- Chloroaniline BRL IJgl 50
91-58- Chloronaphthalene IJglBRL 50
5095-57 - Chlorophenol BRL 1J91
507005-72- Chlorophenyl phenyl ether BRL IJgl
216-01- Chrysene tJ91BRL 50
5053-70- Dibenzo (a h) anthracene BRL IJgl
50132-64- Dibenzofuran BRL IJgl
95-50- Dichlorobenzene IJglBRL 50
541-73- 13- Dichlorobenzene BRL IJgl 50
106-46- Dichlorobenzene 1J91BRL 50
5091-94- 3 - Dichlorobenzidine BRL IJgl
120-83- Dichlorophenol BRL IJgl 50
84-66- Diethyl phthalate BRL IJgl 50
131-11- Dimethyl phthalate BRL IJgll 50
105-67- Dimethylphenol BRL 1J91 50
5084-74- Di-n- butyl phthalate BRL 1J91
534-52 - Dinitro-2-methylphenol BRL IJgl 50
51-28- Dinitrophenol IJglBRL 50
50121-14- Dinitrotoluene BRL 1J91
606-20- Dinitrotoluene IJglBRL 50
50117-84-0 Di-n-octyl phthalate BRL IJgl
206-44-0 Fluoranthene 1J91BRL 50
BRL 50
50 86-73- Fluorene IJgi
118-74- Hexachlorobenzene BRL 1J91
87-68- Hexachlorobutadiene 1J91BRL 50
5077-47-4 Hexachlorocyclopentadiene BRL IJgl
67-72- Hexachloroethane IJglBRL 50
50193-39- Indeno (1 3-cd) pyrene BRL IJgl
5078-59- Isophorone BRL IJgl
Tfls laboratory report is not valid without all authorized signature 011 the coverpage
Page 6 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Sam le Identification Client Pro ect Matrix Collection DateTime ReceivedMWshy
2920-96- Ground Water I3-May-081030 14-May-SA 78602shy
CAS No Analyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Semivolatile Organic Compounds by GCMS
Semi volatile Or anic Com ounds b EPA 625
Prepared by method SW846 3510C
91-57 -6 Methylnaphthalene 367 1-91 50 EPA 625 16-May- 19-May-08 8051216
95-48- Methylphenol BRL 1-91 50
108-39-4 3 amp 4-Methylphenol BRL I-gl 100 106-44shy91-20- Naphthalene 247 1-91 50
88-74-4 Nitroaniline BRL 1-91 50
99-09- Nitroaniline BRL 1-91 50
100-01-6 Nitroaniline BRL 1-91 50
98-95- Nitrobenzene BRL 1-91 50
88-75- Nitrophenol BRL 1-91 50
100-02- Nitrophenol BRL 1-91 50
62-75- Nitrosodimethylamine BRL 1-91 50
621-64- N- Nitrosodi-n-propylamine BRL 1-91 50
86-30-6 Nitrosodiphenylamine BRL 1-91 50
87 -86- Pentachlorophenol BRL 1-91 50
85-0- Phenanthrene BRL 1-91 50
108-95- Phenol BRL 1-91 50
129-00-0 Pyrene BRL 1-91 50
110-86- Pyridine BRL 1-91 50
120-82- 4- Trichlorobenzene BRL 1-91 50
95-95- 5- Trichlorophenol BRL 1-91 50
88-06- 6- T richlorophenol BRL 1-91 50
Surrogate recoveries
321-60- Fluorobipheny 30- 130
367- 12- Fuorophenol 15- 110
4165-60- Nitrobenzene- 30- 130
4165-62- Pheno- 15- 110
1718-51- Terpheny-d4 30- 130
118- 79- 6- Tribromophenol 15- 110
Semivolatile Organic Compounds by GC
Pol chlorinated Bi hen ls b EPA 608
Prepared by method SW846 3510C
12674- 11-2 Aroclor- 1016 BRL 1-91 0650 EPA 608 15- May- 16-May-08 8051106
11104-28-2 Aroclor-1221 BRL IJgl 0650
11141-16-5 Aroclor- 1232 BRL 1-91 0650
53469-21-9 Aroclor- 1242 BRL 1-91 0650
12672-29-6 Aroclor- 1248 BRL 1-91 0650
11097-69-1 Aroclor- 1254 BRL 1-91 0650
11096-82-5 Aroclor -1260 BRL 1-91 0650
37324-23-5 Aroclor-1262 BRL 1-91 0650
11100-14-4 Aroclor-1268 BRL IJgl 0650
Surrogate recoveries
2051-24- Decachlorobipheny (Sr) 105 30- 150
10386-84-2 4 DB-Octafluorobiphenyl (Sr) 30- 150
Extractable Petroleum Hydrocarbons
mgl EPA 1664 Rev A 15-May- 19-May-08 8051102Non-polar material (SGT- HEM)
Soluble Metals by EPA 2006000 Series Metbods
Field Filtered NA EPA 200 73005A 15- May- 15-May-08 8051192Filtration
Soluble Metals by EPA 200 Series Methods
7440-22-4 Silver BRL mgl 0002 EPA 200 21-May- 27- May-08 8051249
This laboratory report is IlOt mlid without (II authorized signature on the cover page
Reportble Detection Limit BRL = Below Reporting Limit Page 7 of 25
Sam le Identification MW-
Client Pro ect 2920-96shy
Matrix Ground Water
Collection DateTime 13-May-08 1030
Received 14-May-
SA 78602shy
CAS No A nalyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Soluble Metals by EPA 200 Series Methods
7440-38shy Arsenic 0468 mg1 0040 EPA 200 21-Mayshy 21-May-08 80511 50
7440-43shy Cadmium BRL mg1 0002 EPA 200 21-May-088051249
7440-47shy Chromium BRL mg1 0050 EPA 200 21-May-088051150
7440-50-8 Copper BRL mg1 0050
7439-89-6 Iron 184 mg1 0150
7439-97-6 Mercury BRL mg1 00020 EPA 245 17470A 21-May-088051152
7440-02-0 Nickel BRL mg1 0050 EPA 200 21-May-088051150
7439-92shy Lead 0011 mg1 0002 EPA 200 21-May-088051249
7440-36-0 Antimony 0003 mg1 0002
7782-49shy Selenium BRL mg1 0150 EPA 200 21-May-08 8051150
7440-66-6 Zinc 0186 mgl 0050
General Chemistry Parameters
Filtration Completed NA Varies 14-Mayshy 14-May-08 8051095
18540-29-9 Hexavalent Chromium (soluble) BRL HT2 mg1 125 SM3500CrDI796A 14-Mayshy 14-May-08 8051094 R01 2013 2016
57-12shy Cyanide (total) BRL mg1 0100 EPA 3354 19-Mayshy 19-May-088051374
7782-50shy Total Residual Chlorine BRL CIHT mg1 500 Hach 8167 14-Mayshy 14-May-08 8051049 R01 1900 2001
Total Suspended Solids 580 mg1 25 SM2540D 16-Mayshy 16-May-08 8051275
This lahomtOlY report is not valid without an authorized signature on the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page 8 of 25
Volatie Organic Compounds - Quality Control
Analyte( s)
Batch 8051244 - SW846 5030 Water MS
Blank 8051244-BLK1
Prepared 16-May-08 Analyzed 17-May-
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromochloromethane
1 Dichlorobenzene
1 Dichlorobenzene
1 Dichlorobenzene
1-Dichloroethane
1 Dichloroethane
1 1-Dichloroethene
cis- Dichloroethene
trans- 1 Dichloroethene
1 Dichloropropane
cis- 1 Dichloropropene
trans- 1 Dichloropropene
Ethylbenzene
Hexanone (MBK)
Methyl tert-butyl ether
Methyl- pentanone (MIBK)
Methylene chloride
Styrene
2- Tetrachloroethane
Tetrachloroethene
Toluene
1- Trichloroethane
2- Trichloroethane
Trichloroethene
Trichlorofluoromethane (Freon 11)
Vinyl chloride
p-Xylene
Xylene
Surrogate 4-Bromofluorobenzene Surrogate Toluene-
Surrogate 1 Dichloroethane-Surrogate Dibromofluoromethane
LCS B051244-BS1
Prepared 16-May-08 Analyzed 17 -May-
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Spike Source REC RPD
Result Flag Units RDL Level Result REC Limits RPD Limit
BRL gl 20
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl 10
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gll
BRL gi
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl 10
BRL gll
BRL gll 10
BRL gl 10
BRL gll
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
41 gl 50 70- 130 49 gl 50 70- 130 59 gl 50 119 70- 130 52 gl 50 105 70- 130
QC2 jgl 20 70- 130
18 jgl 20 70- 130
192 jgl 20 35- 155
18 jgl 20 45- 169
19 jgl 20 242
This laboratOlY repol1 is lot valid without 011 authorized sigllature 011 the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page 9 of 25
Volatie Organic Compounds - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051244 - SW846 5030 Water MS
LC5 8051244B51
Prepared 16-May-08 Analyzed 17-May-
Butanone (MEK) 10 QC2 gl 20 70- 130
Carbon tetrachloride 204 gl 20 102 70- 140
Chlorobenzene 18 gl 20 70- 130
Chloroethane 164 gl 20 14-230
Chloroform 18 gll 20 51- 138
Chloromethane 21 gl 20 106 273
Dibromochloromethane 18 gl 20 53- 149
1 Dichlorobenzene 20 gl 20 104 18- 190
1 Dichlorobenzene 19 gl 20 59- 156
1 A-Dichlorobenzene 18 gl 20 18- 190
1- Dichloroethane 19 gl 20 59- 155
1 Dichloroethane 19 gl 20 49- 155
1-Dichloroethene 16 gl 20 70- 130
cis- 1 Dichloroethene 17 gl 20 70- 130
trans- 1 Dichloroethene 16 gll 20 54- 156
1 Dichloropropane 18 gl 20 210
cis- Dichloropropene 17 gl 20 227
trans- 1 Dichloropropene 17 gl 20 17- 183
Ethylbenzene 19 gl 20 37- 162
Hexanone (MBK) 124 QC2 gl 20 70- 130
Methyl tert-butyl ether 19 gl 20 70- 130
Methylshy pentanone (MIBK) 17 gl 20 70- 130
Methylene chloride 16 gl 20 221
Styrene 17 gl 20 70- 130
1 Tetrachloroethane 194 gl 20 46- 157
Tetrachloroethene 15 gl 20 64- 148
Toluene 18 gl 20 70- 130
1- Trichloroethane 20 gl 20 100 52- 162
2- Trichloroethane 18 gl 20 52- 150
Trichloroethene 17 gl 20 71- 157
Trichlorofluoromethane (Freon 11) 19 gl 20 17- 181
Vinyl chloride 21 gl 20 106 251
p-Xylene 39 gl 40 70- 130
Xylene 20 gl 20 102 70- 130
Surrogate 4-Bromofluorobenzene Surrogate Toluene-
Surrogate 1 Dichloroethane-Surrogate Dibromofluoromethane
52 49 56
49
gl
gl
gl
gl
50 50 50
50
105
112 100
70- 130 70- 130 70- 130 70- 130
LC5 DUD (8051244-B5D1
Prepared 16-May-08 Analyzed 17-May-
Acetone QC2 gl 20 70- 130
Benzene 18 gl 20 70- 130
Bromodichloromethane 18 gl 200 35- 155
Bromoform 17 gl 20 45- 169
Bromomethane 18 gl 20 242
Butanone (MEK) 11 QC2 1-91 20 70- 130
Carbon tetrachloride 20 gl 20 100 70- 140
Chlorobenzene 17 gl 20 70- 130
Chloroethane 15 1-91 20 14-230
Chloroform 18 1-91 20 51- 138
This laboratory report is aot valid without a1 authorized sig1ature 01 the cover page
Reportble Detection Limit BRL = Below Reporting Limit Page 10 of25
Volatie Organic Compounds - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051244 - SW846 5030 Water MS
LCS Dup 18051244-BSD1
Prepared 16-May-08 Analyzed 17-May-
Chloromethane 18 1-91 20 273
Dibromochloromethane 174 1-91 20 53- 149
Dichlorobenzene 20 1-91 20 100 18- 190
Dichlorobenzene 18 1-91 20 59- 156
Dichlorobenzene 18 1-91 20 18- 190
Dichloroethane 18 1-91 20 59- 155
Dichloroethane 19 1-91 20 49- 155
Dichloroethene 16 1-91 20 70- 130
cis- Dichloroethene 16 1-91 20 70- 130
trans- Dichloroethene 15 1-91 20 54- 156
Dichloropropane 17 1-91 20 210
cis- Dichloropropene 164 IJgl 20 227
trans- 1 Dichloropropene 164 I-gl 20 17- 183
Etlwlbenzene 18 IJgl 20 37- 162
Hexanone (MBK) 124 QC2 IJgl 20 70- 130
Methyl tert-butyl ether 184 1J91 20 70- 130
Methyl- pentanone (MIBK) 17 IJgl 20 70- 130
Methylene chloride 16 IJgl 20 221
Styrene 16 IJgl 20 70- 130
2- Tetrachloroethane 19 IJgl 20 46- 157
Tetrachloroethene 15 IJgl 20 64- 148
Toluene 17 IJgl 20 70- 130
1- Trichloroethane 19 1-91 20 52- 162
2- Trichloroethane 16 IJgl 20 52- 150
Trichloroethene 15 IJgl 20 71- 157
Trichlorofluoromethane (Freon 11) 17 IJgl 20 17- 181
Vinyl chloride 19 IJglI 20 251
p-Xylene 37 1J91 40 70- 130
Xylene 20 IJgl 20 100 70- 130
Surrogate 4-Bromofluorobenzene 51 IJgl 50 104 70- 130
Surrogate Toluene- 4B gl 50 70- 130
Surrogate 1 0ichloroethane- 53 IJgl 50 106 70- 130 Surrogate Oibromofluoromethane 50 1J9i 50 102 70- 130
Matrix S ike B051244-MS1 Source SA7B629shy
Prepared 16-May-08 Analyzed 17-May-
Benzene 18 20 BRL 70- 130IJgl
Bromodichloromethane 19 IJgl 20 BRL 35- 155
Bromoform 18 IJgl 20 BRL 45- 169
Bromomethane 16 IJgl 20 BRL 242
Carbon tetrachloride 21 IJgl 20 BRL 106 70- 140
Chlorobenzene 18 IJgl 20 BRL 70- 130
Chloroethane 16 IJgl 20 BRL 14-230
Chloroform 18 IJgl 20 BRL 51- 138
Chloromethane 19 IJgl 20 BRL 273
Dibromochloromethane 17 IJgl 20 BRL 53- 149
1 Dichlorobenzene 22 IJgl 20 BRL 112 18- 190
1 Dichlorobenzene 22 IJgl 20 BRL 110 59-156
1 Dichlorobenzene 21 IJgl 20 BRL 109 18- 190
1- Dichloroethane 19 IJgl 20 BRL 59- 155
1 Dichloroethane 18 IJgl 20 BRL 49- 155
This laboratory report is 110t mUd without an authorized signature on the covel page
Reportble Detection Limit BRL = Below Reporting Limit Page It of25
Volatile Organic Compounds - Quality Control
p
Spike Source REC RPD
Result REC imits RPD LimitAnalyte(s) Result Flag Units RDL Level
Batch 8051244 - SW846 5030 Water MS
Matrix ike S051244-MS1 Source SA7B629shy
Prepared 16-May-08 Analyzed 17-Mayshy
17 20 BRL 70- 130 1- Dichloroethene IJgl
16 20 BRL 54- 156trans- 1 Dichloroethene IJgl
21020 BRL1 Dichloropropane 17 1J91
cis- 1 Dichloropropene 17 IJgl 20 BRL 227
17- 183trans- 1 Dichloropropene 184 1J91 20 BRL
20 20 BRL 103 37- 162Ethylbenzene IJgl
15 20 BRL 221Methylene chloride IJgl
20 BRL 46- 1572- Tetrachloroethane 19 1J91
20 BRL 64- 148Tetrachloroethene 18 1J91
BRL 70- 130Toluene 18 1J91 20
105 52-1621- Trichloroethane 211 IJgl 20 BRL
18 20 BRL 52- 1502- Trichloroethane IJgl
17 20 BRL 71- 157Trichloroethene 1J91
20 BRL 17- 181Trichloroluoromethane (Freon 11) 194 IJgl
20 BRL 103 251Vinyl chloride 20 IJgl
102 70- 130Surrogate 4-Bromofluorobenzene 50 IJgl 50 50 70- 130Surrogate Toluene- 49 1J91
56 50 112 70- 130Surrogate 1 Dichloroethane- IJgl
50 100 70- 130Surrogate Dibromofluoromethane 50 IJgl
Matrix S ike Du S051244-MSD1 Source SA7S629shy
Prepared 16-May-08 Analyzed 17-Mayshy
18 20 BRL 70- 130Benzene IJgl
18 20 BRL 35- 155Bromodichloromethane IJgl
17 20 BRL 45- 169Bromoform IJgl
20 BRL 242Bromomethane 17 IJgl
20 BRL 103 70- 140Carbon tetrachloride 20 IJgl
18 20 BRL 70- 130Chlorobenzene 1J91
14-230Chloroethane 16 IJgl 20 BRL
20 51- 138Chloroform 184 IJgl BRL
Chloromethane 19 1J91 20 BRL 273
18 20 BRL 53- 149Dibromochloromethane 1J91
20 BRL 117 18- 190Dichlorobenzene 234 IJgl
20 BRL 112 59- 156Dichlorobenzene 22 IJgl
BRL 108 18- 190Dichlorobenzene 21 1J91 20
20 59- 1551 Dichloroethane 19 IJgl BRL
18 20 BRL 49- 155Dichloroethane IJgl
16 20 BRL 70- 130Dichloroethene IJgl
20 BRL 54- 156trans- Dichloroethene 154 1J91
20 BRL 210Dichloropropane 17 IJgl
0420 BRL 227cis- Dichloropropene 17 IJgl
17- 183trans- Dichloropropene 17 1J91 20 BRL
BRL 37- 162Ethylbenzene 20 1J91 20 102
Methylene chloride 15 IJgl 20 BRL 221
20 BRL 46- 1572- Tetrachloroethane 192 IJgl
20 BRL 64- 148 04Tetrachloroethene 18 IJgl
BRL 70- 130Toluene 184 1J91 20
52- 1621- Trichloroethane 20 IJgl 20 BRL 104
17 20 BRL 52- 1502- Trichloroethane IJgl
17 20 BRL 71- 157Trichloroethene IJgl
20 BRL 17-181Trichlorofluoromethane (Freon 11) 19 IJgl
This laboratory report is IIOt valid without all authorized sigllllture 011 the cover page
Page 12 of25 Reportble Detection Limit BRL = Below Reporting Limit
Semivolatile Organic Compounds by GCMS - Quality Control
Analyte(s)
Batch 8051216 - SW846 3510C
Blank 8051216-BLK1
Prepared amp Analyzed 16-May-
Isophorone
Methylnaphthalene
Methylphenol
3 amp 4-Methylphenol
Naphthalene
Nitroaniline
Nitroaniline
Nitroaniline
Nitrobenzene
Nitrophenol
Nitrophenol
Nitrosodimethylamine
N- N itrosodi-n-pro pyla mine
N itrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Pyridine
1 24-Trichlorobenzene
24 5- Trichlorophenol
246- Trichlorophenol
Surrogate 2-Fuorobipheny Surrogate 2-Fuoropheno Surrogate Nitrobenzene-Surrogate PhenoshySurrogate Terpheny-d4 Surrogate 6- Tribromopheno
LCS B051216-BS1
Prepared amp Analyzed 16-May-
Acenaphthene
Acenaphthylene
Aniline
Anthracene
AzobenzenelDi phenyld lazine
Benzidine
Benzo (a) anthracene
Benzo (a) pyrene
Benzo (b) fluoranthene
Benzo (g i) perylene
Benzo (k) fluoranthene
Benzoic acid
Benzyl alcohol
B is(2-chloroethoxy)methane
B i s (2-ch loroethyl)eth e r
Bis(2-ch loroisopropyl) ether
B is(2-ethy Ih exyl) phtha late
Bromophenyl phenyl ether
Butyl benzyl phthalate
Carbazole
Spike Source REC RPD
Result Flag Units RDL Level Result REC Limits RPD Limit
BRL gl
BRL gl
BRL gl
BRL gl 10
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gll
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
370 gl 50 30- 130 40 gl 50 15- 110 39 gl 50 30- 130 43 gl 50 15- 110 36 gl 50 30- 130 40 gl 50 15- 110
41 gl 50 40- 140
43 gI 50 40- 140
41 gl 50 40- 140
38 gl 50 40- 140
45 gl 50 40- 140
49 gl 50 153
41 gl 50 40- 140
43 gl 50 40- 140
41 gl 50 40- 140
41 gll 50 40- 140
45 gl 50 40- 140
32 gl 50 12- 149
41 gl 50 40- 140
39 gl 50 40- 140
384 gl 50 40- 140
47 gl 50 40- 140
47 gl 50 40- 140
40 gl 50 40- 140
47 gI 50 40- 140
56 gI 50 112 200
This laboratory report is lIot valid witllOut a1l authorized sigllature 011 the coverpage
Reportble Detection Limit BRL = Below Reporting Limit Page 15 of25
Semivolatile Organic Compounds by GCMS - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051216 - SW846 3510C
LCS 8051216-BS1
Prepared amp Analyzed 16-Mayshy
50 30- 1304 -C hloro-3-methylphenol 42 IJgl
40- 140Chloroaniline 39 IJgl 50
Chloronaphthalene 37 IJgl 50 40- 140
Chlorophenol 37 IJgl 50 30- 130
50 40- 140
40- 140
Chlorophenyl phenyl ether 45 IJgl
Chrysene 43 IJgl 50
Dibenzo (a h) anthracene 43 IJgl 50 40- 140
Dibenzofuran IJgl38 50 40- 140
50 40- 1401 Dichlorobenzene 35 IJgl
40- 1401 Dichlorobenzene 264 IJgl 50
40- 1401 Dichlorobenzene 434 IJgl 50
58 50 116 40- 1403 - Dichlorobenzidine IJgl
50 30- 130
40- 140 24-Dichlorophenol 38 IJgl
Diethyl phthalate 484 IJgl 50
50 40- 140Dimethyl phthalate 464 IJgl
Dlmethylphenol 39 IJgl 50 30- 130
DI-n-butyl phthalate 44 IJgll 50 40- 140
30- 130 6-Di nitro- 2-methylphenol 38 1J91 50
30- 130Dinltrophenol 36 1J91 50
42 50 40- 14024-Dlnitrotoluene 1J91
Dlnitrotoluene 1J9141 50 40- 140
Di-n-octyl phthalate 52 IJgl 50 104 40- 140
40- 140Fluoranthene 40 IJgl 50
Fluorene 41 IJgl 50 40- 140
39 50 40- 140Hexachlorobenzene IJgl
50 40- 140Hexachlorobutadiene 40 IJgl
40- 140Hexach lorocyclopentad iene 294 IJgl 50
40 50 40- 140Hexachloroethane IJgl
42 50 40-140Indeno (1 3-cd) pyrene IJgl
50 40- 140Isophorone 40 IJgl
40- 140Methylnaphthalene 394 IJgl 50
40- 140Methylphenol 39 IJgl 50
40 10 50 40- 1403 amp 4-Methylphenol IJgl
37 50 40-140Naphthalene IJgl
50 40-140Nitroaniline 39 IJgl
Nitroaniline 51 IJgl 50 102 40- 140
48 50 40- 140Nltroaniline 1J91
50 40- 140Nitrobenzene 40 IJgl
30- 130Nitrophenol 36 IJgl 50
40 IJgl 50 30- 130Nitrophenol 40- 140Nitrosodimethylamine 32 1J91 50
50 40-140N- N itrosodi-n-propyla mine 46 IJgl
40- 140N itrosodi phenyla ml ne 44 IJgl 50
41 IJgl 50 30- 130Pentachlorophenol 40- 140Phenanthrene 38 IJgl 50
50 30- 130Phenol 38 IJgl
40- 140Pyrene 424 1J91 50
40- 140Pyridine 294 1J91 50
40- 14024- Trichlorobenzene 364 IJgl 50
This laboratory report is not mlid without an authorized signature 011 the cover page
Page 16 of25 Reportble Detection Limit BRL = Below Reporting Limit
Semivolatie Organic Compounds by GCMS - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
BMch 8051216 - SW846 3510C
LC5 8051216-851
Prepared amp Analyzed 16-Mayshy
24 5- Trichlorophenol 404 gl 50 30- 130
246- Trichlorophenol 42 gl 50 30- 130
Surrogate 2-Fluorobiphenyl 29 gl 50 30- 130
Surrogate 2-Fluorophenot 27 gl 50 15- 110
Surrogate Nitrobenzene- 30 gl 50 30- 130
Surrogate Phenol- 29 gl 50 15- 110
Surrogate Terpheny-d4 30 gl 50 30- 130
Surrogate 6- Tribromopheno 324 gl 50 15- 110
This laboratory report is lIot valid without all authorized sigllature 011 tlle cover page
Reportble Detection Limit BRL = Below Reporting Limit Page 17 of25
Semivolatie Organic Compounds by GC - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051106 - SW846 3510C
Blank S051106-BLK1
Prepared amp Analyzed 15-Mayshy
Aroclor- 1016 BRL gI 0200
Aroclor- 1016 (2C) BRL gI 0200
Aroclor- 1221 BRL gI 0200
Aroclor- 1221 (2C) BRL gI 0200
Aroclor- 1232 BRL gI 0200
Aroclor- 1232 (2Cj BRL gI 0200
Aroclor- 1242 BRL gI 0200
Aroclor-1242 (2C) BRL gI 0200
Aroclor- 1248 BRL gI 0200
Aroclor- 1248 (2C) BRL gI 0200
Aroclor- 1254 BRL gI 0200
Aroclor- 1254(2Cj BRL gI 0200
Aroclor- 1260 BRL gI 0200
Aroclor- 1260 (2C) BRL gI 0200
Aroclor- 1262 BRL gI 0200
Aroclor- 1262 (2C) BRL gI 0200
Aroclor-1268 BRL gI 0200
Aroclor- 1268 (2C) BRL gI 0200
Surrogate Decachlorobiphenyl (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0231 0224 0194 0191
gI
gI
gI
gI
0200 0200 0200 0200
116 112
30- 150 30- 150 30- 150 30- 150
LC5 8051106-B51
Prepared 15-May-08 Analyzed 16-May-08
Aroclor- 1016 265 gI 0200 250 106 50- 114
Aroclor- 1 016 (2C) 240 gI 0200 250 50- 114
Aroclor- 1260 0269 gI 0200 250 107 40- 127
Aroclor-1260 (2Cj 270 gI 0200 250 108 40- 127
Surrogate Decachlorobiphenyl (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0225 0224 0188 0183
gI
gI
gI
gI
0200 0200 0200 0200
113 112
30- 150 30- 150 30- 150 30- 150
LC5 DUD rS051106-B5D1
Prepared 15-May-08 Analyzed 16-Mayshy
Aroclor- 1016 262 gl 0200 250 105 50- 114
Aroclor-1 016 (2Cj 241 gI 0200 250 50- 114
Aroclor- 1260 277 gI 0200 250 111 40- 127
Aroclor- 1260(2Cj 0260 gI 0200 250 104 40- 127
Surrogate Decachlorobipheny (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0238 0218 0189 0181
gI
gI
gI
gI
0200 0200 0200 0200
119 109
30- 150 30- 150 30- 150 30- 150
This laboratory report is lot valid without (II authorized sigllature 01 the cover page
Page 18 of25 Reportable Detection Limit BRL = Below Reporting Limit
Extractable Petroleum Hydrocarbons - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051102 - SW846 3510C
Blank 8051102-BLK1
Prepared 15-May-08 Analyzed 19-Mayshy
Non-polar material (SGT- HEM) BRL m91
LC8 8051102-B81
Prepared 15-May-08 Analyzed 19-Mayshy
Non-polar material (SGT- HEM) 184 m91 21 81 904
This laboratory report is not valid without an authorized signature 011 the cover page
Page 19 of25 Reportable Detection Limit BRL = Below Reporting Limit
Soluble Metals by EPA 200 Series Methods - Quality Control
Analyte(s) Result Flag Units RDL
Spike
Level
Source
Result REC
REC
Limits RPD
RPD
Limit
Batch 8051150 - EPA 200 Series
Blank 8051150-BLK1
Prepared amp Analyzed 21-May-
Iron
Zinc
Selenium
Nickel
Chromium
Copper
Arsenic
BRL
BRL
BRL
BRL
BRL
BRL
BRL
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0150
0050
0150
0050
0050
0050
0040
LCS 8051150-BS1
Prepared amp Analyzed 21-May-
Selenium
Zinc
Iron
Nickel
Chromium
Arsenic
Copper
123
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0150
0050
0150
0050
0050
0040
0050
103
105
101
100
85- 115
85- 115
85- 115
85- 115
85- 115
85-115
85- 115
licate B051150-DUP1 Source SA7B602shy
Prepared amp Analyzed 21-May-
Iron
Zinc
Selenium
Nickel
Copper
Chromium
Arsenic
17
0162
BRL
0015
0017
BRL
0450
QR8
mgl
mgl
mgl
mgl
mgl
mgl
mgi
0150
0050
0150
0050
0050
0050
0040
184
0186
BRL
0014
0023
BRL
0468
Matrix S ike 8051150-MS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Iron
Selenium
Nickel
Zinc
Copper
Chromium
Arsenic
19 QM2 mgl
mgll
mgl
mgl
mgl
mgl
mgl
0150
0150
0050
0050
0050
0050
0040
125
184
BRL
0014
0186
0023
BRL
0468
104
105
102
70- 130
70- 130
70-130
70- 130
70- 130
70-130
70- 130
Post S ike 8051150-PS1 Source SA78602shy
Prepared amp Analyzed 21-May-
Zinc
Iron
Selenium
Nickel
Copper
Arsenic
Chromium
18 QM2
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0050
0150
0150
0050
0050
0040
0050
0186
184
BRL
0014
0023
0468
BRL
104
104
101
85- 115
85- 115
85- 115
85-115
85-115
85- 115
85-115
Batch 8051152 - EPA200SW7000 Series
Blank B051152-BLK1
Prepared amp Analyzed 21-May-
Mercury BRL mgl 00020
This laboratory report is IIOt valid witllOut all authorized sigllature 011 the coverpage
Page 20 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Soluble Metals by EPA 200 Series Methods - Quality Control
Analyte(s) Result Flag Units RDL
Spike
Level
Source
Result REC
REC
Limits RPD
RPD
Limit
Batch 8051152 - EPA200SW7000 Series
LCS B051152-BS1
Prepared amp Analyzed 21-May-
Mercury 00576 m91 00020 00500 115 85- 115
licate B051152-DUP1 Source SA78602-01
Prepared amp Analyzed 21-May-
Mercury BRL m91 00020 BRL
Matrix S ike 8051152-MS1 Source SA78602shy
Prepared amp Analyzed 21-May-
Mercury 00632 OM m91 00020 00500 BRL 126 75- 125
Post S ike 8051152-PS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Mercury 00624 OC1 m91 00020 00500 BRL 125 85- 115
Batch 8051249 - 2008No digestion
Blank 8051249-BLK1
Prepared amp Analyzed 21-May-
Lead
Antimony
Cadmium
Silver
BRL
BRL
BRL
BRL
m91
m91
m91
m91
0002
0002
0002
0002
LCS B051249-BS1
Prepared amp Analyzed 21-May-
Antimony
Lead
Silver
Cadmium
143
145 OC2
m91
m91
m91
m91
0050
0050
0050
0040
103
115
107
116
85- 115
85- 115
85- 115
85- 115
licate 8051249-DUP1 Source SA7B602shy
Prepared amp Analyzed 21- May-
Lead
Antimony
Cadmium
Silver
0009
0002
00005
00002
ORB
m91
m91
m91
m91
0002
0002
0002
0002
0011
0003
00005
00003
Matrix S ike 8051249-MS1 Source SA78602shy
Prepared amp Analyzed 21- May-
Lead
Antimony
Cadmium
Silver
142
m91
m91
m91
m91
0050
0050
0040
0050
0011
0003
00005
00003
111
101
114
102
70- 130
70-130
70c130
70- 130
Post S ike 8051249-PS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Antimony
Cadmium
Silver
38
OC2
m91
m91
m91
0050
0040
0050
125
0003
00005
00003
110
121
109
85- 115
85- 115
85- 115
This laboratory report is flOt valid IVithout all authorized signature 011 the cOIer page
Reportable Detection Limit BRL Below Reporting Limit Page 21 of 25
General Chemistry Parameters - Quality Control
Spike Source REC RPD
Analyte( s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051049 - General Preparation
Blank S051 049-BLK1
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
Blank S051049-BLK2
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
Blank S051 049-BLK3
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
LCS S051049-BS1
Prepared amp Analyzed 14-May-
Total Residual Chlorine 046 mgl 020 0500 90- 110
LCS S051049-BS2
Prepared amp Analyzed 14-May-
Total Residual Chlorine 047 mgl 020 0500 90- 110
LCS S051049-BS3
Prepared amp Analyzed 14-May-
Total Residual Chlorine 054 mgl 020 0500 108 90-110
licate B051049-DUP1 Source SA7S544shy
Prepared amp Analyzed 14-May-
Total Residual Chlorine 012 mgl 020 010
licate S051049-DUP2 Source SA7S602-01
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020 BRL
Matrix S ike 8051049-MS1 Source SA78544-01
Prepared amp Analyzed 14-May-
Total Residual Chlorine 065 mgl 020 0500 010 110 80- 120
Matrix S ike 8051049-MS2 Source SA7B602shy
Prepared amp Analyzed 14-May-
Total Residual Chlorine mgl 500 125 BRL 108 80- 120
Reference 8051 049-SRM1
Prepared amp Analyzed 14-May-
Total Residual Chlorine 100 mgl 020 0967 103 85-115
Batch 8051094 - General Preparation
Blank 8051094-BLK1
Prepared amp Analyzed 14 May-
Hexavalent Chromium (soluble) BRL mgl 005
Blank 8051 094-BLK2
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) BRL mgl 005
LCS 8051094-BS1
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) 054 mgl 005 90- 110
licate 8051094-DUP1 Source SA78602-01
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) BRL mgl 125 BRL
Thi laboratory report is not valid without all authorized sigllature 011 the cover page
Page 22 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Page 13
~~~ ~~~~- -- - _ - -_ - ~~~ ~~~~ ~~~ - - _- _- -- -- p __(
MA DEP - Bureau of Waste Site CleanupSITE NME Site S aP 5 MiFlII Former Speeway Station _-II181 Eat Broaday b b d IS I i I GARDNER MA 0144 v ri) i P f f 1 me- 1 5ylmI I L shy J --I 423315n 715835e SiteLocation y o oCop1odQcn Ofof W-_ l
1 1 I
r
r
iBARBER HILL
A c
Cf1 f o s
0
5
Roads Uned Acss Divd Mar Roed Conntor Street Track 1 EPA Sola Source Aquilar FEMA 100yaar iloodplain 0 c Puc Watar SLo GrunSelaceNon Corrty 0
Bounars lOwn Couny DE Region Tian Powerln Ine Aqedut ApprOld Zona2 tNPA Sue Wster Supp Zone A bStZ F--shy--rle
8os Mat Sub SUeor Porenrial Inermtent Man lvo8 Ste Dfm Hyro1apy Wmer FeatllePLio Suleee Wat S H-- L otlMds FrslSaltN-ES WeIMd Habat L
Potentia Prdutiv AqlJlers ModHig Yield Proteoted Opn Space ACC nIL c= Non-Potential Drng Water Sollce AIea ModumHi Yo1d ll DEP Pormrd SoidWes1 FsiIi6s cnifud Verne Pools f0
1I2 KIWUmR$ MtL
January 30 2004 SCALE 1 15000
-
LE
GE
ND
APX PROPER BONDA
- APPROXOiSPO SIT BOUNDA
-GR
OU
ND
WA
TE F1 D
IRE
cnON
SCA
LE
30 60 FE
(APR
OX
CORPORATE ENVIRONMENTAL
)i
AD
VISO
RS
INC
SC
AS SH
OW
D
R B
Y K
HA
EL
DA
TE
10407
JOB
NO
2920-96
AERIAL MAP
FO
RM
ER
SP
EE
DW
AY
ST
AT
ION
FlGURE -3
181 EA
BR
OA
AY
GA
NE
R fo
age 1 ot 1Streamflow Statistics Report
Streamstats Ungaged Site Report Date Wed Dec 31 2008 124908 Site Location Massachusetts NAD83 Latitude 425545 (42 3316) NAD83 Longitude -719758 (-71 58 32) NAD27 Latitude 425545 (423316) NAD27 Longitude - 9763 (-71 58 34) Drainage Area 502 mi2
IPeak Flow Basin Characteristics 1100 Statewide Low Flow (S02 mi2)
Regression Equation Valid Rang
I Min II Max1 Value III Parameter Drainage Area (square miles) 161 149
Mean Basin Slope from 250K DEM (percent) 032 24
Stratified Drift per Stream Length (square mile per mile) 129
Massachusetts Region (dimensionless)
Streamflow Statistics
gO-Percent Prediction Interval Prediction Error
MaximumStatistic Flow (ft s) (percent) Minimum
I D50 IIII 11 1811 II 24511 993
I D60 II 35511 2011 II 03611 35111 2411 II 041 I 201I D70 24111 2611 II 03811 151I D75 11 2811 II 0911 3761I D80 981I D85 1 I 3211 II o6311
1 I 3711 II 0441 1 2 2911 D90 11 4611 II 02411 15511 D95I D98 04511 6011 II 01511 11
I D99 03411 6511 II ol1ll 1021
5011 II 02611 11I M7D2Y 1111 3311 II odl 3 541
I AUGD50
IIIIIIIIIIIIIIIIIIIIII 0311 7111 II 0088411 0981I M7Dl0Y
1010
12312008httpstreamstatsagscrusgsgovgisimgReportsFlowStatsReport3494 - 2008123112498
Dilution Factor Calculation Former Speedway Service Station 181 East Broadway Gardner Ma
DF=(Od+Os)Od
DF = Dilution factor
Od = Max flow rate of discharge in cubic feet per second Os = receiving water flow in cubic feet per seconds 7010 flow rate Mahoney Brook 7010 = min flow for seven consecutive days with a recurrence interval of 10 years
7010 flow based on data obtained from USGS Steamflow Statistics Report Data attached
067
Semivolatile Organic Compounds by GCMS - Quality Control
Analyte( s)
Batch 8051216 - SW846 3510C
Blank 8051216BLK1)
Prepared amp Analyzed 16May-
Acenaphthene
Acenaphthylene
Aniline
Anthracene
AzobenzenelDi phenyld iazi ne
Benzidine
Benzo (a) anthracene
Benzo (a) pyrene
Benzo (b) fiuoranthene
Benzo (g i) perylene
Benzo (k) fiuoranthene
Benzoic acid
Benzyl alcohol
Bis(2-ch loroethoxy) methane
Bis(2-ch loroethyl)ether
Bis(2-ch loroi sopropyl)ether
Bis(2ethylhexyl) phthalate
Bromophenyl phenyl ether
Butyl benzyl phthalate
Carbazole
Ch loro-3-methyl phenol
Chloroaniline
Chloronaphthalene
Chlorophenol
Chlorophenyl phenyl ether
Chrysene
Dibenzo (a h) anthracene
Dibenzofuran
Dichlorobenzene
Dichlorobenzene
14- Dichlorobenzene
3 - Dichlorobenzidine
24-Dichlorophenol
Diethyl phthalate
Dimethyl phthalate
24- Dimethylphenol
Din-butyl phthalate
Dinitro-2-methylphenol
Dinitrophenol
Dinitrotoluene
Dinitrotoluene
Di-noctyl phthalate
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopehtadiene
Hexachloroethane
Indeno (1 cd) pyrene
Spike Source REC RPD
Result Flag Units RDL Level Result REC Limits RPD Limit
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gl
BRL gI
BRL gl
BRL gl
BRL gl
BRL gI
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gll
BRL gl
BRL gll
BRL gl
BRL gl
BRL gI
BRL gI
BRL gI
BRL gl
BRL gI
BRL gI
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gI
BRL gI
BRL gl
This laboratory report is IlOt valid without all authorized sigllature 011 the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page t4 of25
Volatie Organic Compounds - Quality Control
p (
Spike Source REC RPD
RDL Level Result REC Limits RPD Limit Analyte(s) Result Flag Units
Batch 8051244 - SW846 5030 Water MS
Matrix S ike Du 8051244-MSD1 Source SA78629shy
Prepared 16-May-08 Analyzed 17-May-BRL 106 251
Vinyl chloride 21 gl 20
101 70- 130 Surrogate 4-Bromofluorobenzene 50 gl 50
70- 13049 gl 50 111 70- 130
Surrogate Toluene-Surrogate 1 Dichloroethane- 55 gl 50
50 70- 130494 glSurrogate Dibromofluoromethane
Microextractable Organic Compounds - Quality Control
Spike Source REC RPD
Flag Units RDL Level Result REC Limits RPD Limit Analyte(s) Result
Batch 8051105 - SW846 3510C
Blank 8051105-BLK
Prepared amp Analyzed 15-May-
BRL gl 01001 Dibromoethane (ED B)
LCS 8051105-BS1
Prepared amp Analyzed 15-Mayshy50- 1500770 gl 0100 100
licate 8051105-DUP1 Source SA7B583shy
Prepared amp Analyzed 15-May-
BRL gl 0100 BRL
1 Dibromoethane (EDB)
1 Dibromoethane (EDB)
This laborntOlY report is not valid without an authorized signature 011 the cover page
Page 13 of2S Reportable Detection Limit BRL = Below Reporting Limit
Sam le Identification Client Pro ect Matrix Collection DateTime ReceivedMWshy
2920-96- Ground Water 13-May-081030 14-May-SA 78602shy
CAS No Analyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Volatile Organic Compounds
Volatile Or anic Com ounds b GCMS
Prepared by method SW846 5030 Water MS
123-91- Dioxane BRL 1-91 200 EPA 624 16-May-08 17-May-08 8051244
994-05-8 Ter-amyl methyl ether BRL 1-911 20
755- Tert-Butanoll butyl alcohol BRL 1-91 200
67-B4- Acetone BRL 1-91 400
71-43- Benzene BRL 1-91 20
75-27-4 Bromodichloromethane BRL 1-91 20
75-25- Bromoform BRL 1-91 20
74-83- Bromomethane BRL 1-91 40
78-93- Butanone (MEK) BRL 1-91 200
56-23- Carbon tetrachloride BRL 1-91 20
108-90- Chlorobenzene BRL 1-91 20
75-00- Chloroethane BRL 1-91 40
676- Chloroform BRL 1-91 20
74-87- Chloromethane BRL 1-91 40
124-48- Dibromochloromethane BRL 1-91 20
95-50- Dichlorobenzene BRL 1-911 20
541-73- Dichlorobenzene BRL 1-91 20
106-46- Dichlorobenzene BRL 1-91 20
75-34- 1- Dichloroethane BRL 1-91 20
107-06- Dichloroethane BRL 1-91 20
75-35-4 1- Dichloroethene BRL 1-91 20
156-59 cis- Dichloroethene BRL 1-91 20
156-60- trans- Dichloroethene BRL 1-91 20
78-87- 2- Dichloropropane BRL 1-91 20
10061-01-5 cis- Dichloropropene BRL 1-91 20
10061-02-B trans- Dichloropropene BRL 1-91 20
100-41-4 Ethylbenzene 411 1-911 20
591-78-B BRL 200Hexanone (MBK) 1-91
1634-04 -4 Methyl tert-butyl ether BRL 1-91 20
108-10- Methyl- pentanone (MIBK) BRL 1-91 200
75-09- Methylene chloride BRL 1-91 200
100-42- Styrene BRL 1-91 20
79-34- 1 Tetrachloroethane BRL 1-91 20
127- 18-4 T etrachloroethene BRL 1-91 20
108-88- Toluene BRL 1-91 20
71-55 1- Trichloroethane BRL 1-91 20
79-00- 2- Trichloroethane BRL 1-91 20
79-01-B Trichloroethene BRL 1-91 20
759-4 Trichlorofluoromethane (Freon 11) BRL 1-91 20
75-01-4 Vinyl chloride BRL 1-91 20
179601-23-1 m Xylene 390 1-91 40
95-47 Xylene 82 1-91 20
Surrogate recoveries 460-00- Bromofluorobenzene 70- 130
2037-26- Toluene- 100 70- 130
17060-07-0 1 Dichloroethane- 111 70- 130
1868-53- Dibromofluoromethane 70- 130
Microextractable Organic Compounds
106-93-4 1 Dibromoethane (EDB) BRL 1-91 0100 EPA 504 15-May- 15-May-08 8051105
Semivolatile Organic Compounds by GCMS
This laboratory report is not valid without all autllOrized signature 011 the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page 5 of 25
Sam le Identification Client Pro ect Matrix Collection DateTime Received
MWshy2920-96- Ground Water 13-May-081030 14-May-
SA 78602shy
CAS No Analyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Semivolatie Organic Compounds by GCMS
Semi volatile Or anic Com ounds b EPA 625
Prepared by method SW846 3510C 50 EPA 625 16-May- 19-May-08 805121683-32- Acenaphthene BRL IJgl
208-96-8 Acenaphthylene BRL IJgl 50
62-53- BRL IJgll 50Aniline
120- 12- Anthracene BRL 1J91 50
103-33- AzobenzenefDiphenyldiazine BRL IJgl 50
92-87 - Benzidine BRL IJgl 50
56-55- Benzo (a) anthracene BRL 1J91 50
50-32 - Benzo (a) pyrene IJglBRL 50
205-99- Benzo (b) fluoranthene BRL IJgl 50
191-24- Benzo (g i) perylene BRL IJgl 50
50207-08- Benzo (k) fluoranthene BRL IJgl
65-85 Benzoic acid BRL 1J91 50
100-51-6 Benzyl alcohol 1J91BRL 50
50111-91- Bis(2-chloroethoxy)methane BRL 1J91
111-4-4 Bis(2-chloroethyl)ether BRL IJgl 50
501 08-60- Bis(2-chloroisopropyl)ether BRL IJgl
117-81- Bis(2-ethylhexyl)phthalate BRL 1J91 50
101-55- Bromophenyl phenyl ether BRL IJgl 50
5085-68- Butyl benzyl phthalate BRL IJgl
5086-74- Carbazole BRL IJgl
5059-50- C hloro-3-methylphenol BRL IJgl
106-47- Chloroaniline BRL IJgl 50
91-58- Chloronaphthalene IJglBRL 50
5095-57 - Chlorophenol BRL 1J91
507005-72- Chlorophenyl phenyl ether BRL IJgl
216-01- Chrysene tJ91BRL 50
5053-70- Dibenzo (a h) anthracene BRL IJgl
50132-64- Dibenzofuran BRL IJgl
95-50- Dichlorobenzene IJglBRL 50
541-73- 13- Dichlorobenzene BRL IJgl 50
106-46- Dichlorobenzene 1J91BRL 50
5091-94- 3 - Dichlorobenzidine BRL IJgl
120-83- Dichlorophenol BRL IJgl 50
84-66- Diethyl phthalate BRL IJgl 50
131-11- Dimethyl phthalate BRL IJgll 50
105-67- Dimethylphenol BRL 1J91 50
5084-74- Di-n- butyl phthalate BRL 1J91
534-52 - Dinitro-2-methylphenol BRL IJgl 50
51-28- Dinitrophenol IJglBRL 50
50121-14- Dinitrotoluene BRL 1J91
606-20- Dinitrotoluene IJglBRL 50
50117-84-0 Di-n-octyl phthalate BRL IJgl
206-44-0 Fluoranthene 1J91BRL 50
BRL 50
50 86-73- Fluorene IJgi
118-74- Hexachlorobenzene BRL 1J91
87-68- Hexachlorobutadiene 1J91BRL 50
5077-47-4 Hexachlorocyclopentadiene BRL IJgl
67-72- Hexachloroethane IJglBRL 50
50193-39- Indeno (1 3-cd) pyrene BRL IJgl
5078-59- Isophorone BRL IJgl
Tfls laboratory report is not valid without all authorized signature 011 the coverpage
Page 6 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Sam le Identification Client Pro ect Matrix Collection DateTime ReceivedMWshy
2920-96- Ground Water I3-May-081030 14-May-SA 78602shy
CAS No Analyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Semivolatile Organic Compounds by GCMS
Semi volatile Or anic Com ounds b EPA 625
Prepared by method SW846 3510C
91-57 -6 Methylnaphthalene 367 1-91 50 EPA 625 16-May- 19-May-08 8051216
95-48- Methylphenol BRL 1-91 50
108-39-4 3 amp 4-Methylphenol BRL I-gl 100 106-44shy91-20- Naphthalene 247 1-91 50
88-74-4 Nitroaniline BRL 1-91 50
99-09- Nitroaniline BRL 1-91 50
100-01-6 Nitroaniline BRL 1-91 50
98-95- Nitrobenzene BRL 1-91 50
88-75- Nitrophenol BRL 1-91 50
100-02- Nitrophenol BRL 1-91 50
62-75- Nitrosodimethylamine BRL 1-91 50
621-64- N- Nitrosodi-n-propylamine BRL 1-91 50
86-30-6 Nitrosodiphenylamine BRL 1-91 50
87 -86- Pentachlorophenol BRL 1-91 50
85-0- Phenanthrene BRL 1-91 50
108-95- Phenol BRL 1-91 50
129-00-0 Pyrene BRL 1-91 50
110-86- Pyridine BRL 1-91 50
120-82- 4- Trichlorobenzene BRL 1-91 50
95-95- 5- Trichlorophenol BRL 1-91 50
88-06- 6- T richlorophenol BRL 1-91 50
Surrogate recoveries
321-60- Fluorobipheny 30- 130
367- 12- Fuorophenol 15- 110
4165-60- Nitrobenzene- 30- 130
4165-62- Pheno- 15- 110
1718-51- Terpheny-d4 30- 130
118- 79- 6- Tribromophenol 15- 110
Semivolatile Organic Compounds by GC
Pol chlorinated Bi hen ls b EPA 608
Prepared by method SW846 3510C
12674- 11-2 Aroclor- 1016 BRL 1-91 0650 EPA 608 15- May- 16-May-08 8051106
11104-28-2 Aroclor-1221 BRL IJgl 0650
11141-16-5 Aroclor- 1232 BRL 1-91 0650
53469-21-9 Aroclor- 1242 BRL 1-91 0650
12672-29-6 Aroclor- 1248 BRL 1-91 0650
11097-69-1 Aroclor- 1254 BRL 1-91 0650
11096-82-5 Aroclor -1260 BRL 1-91 0650
37324-23-5 Aroclor-1262 BRL 1-91 0650
11100-14-4 Aroclor-1268 BRL IJgl 0650
Surrogate recoveries
2051-24- Decachlorobipheny (Sr) 105 30- 150
10386-84-2 4 DB-Octafluorobiphenyl (Sr) 30- 150
Extractable Petroleum Hydrocarbons
mgl EPA 1664 Rev A 15-May- 19-May-08 8051102Non-polar material (SGT- HEM)
Soluble Metals by EPA 2006000 Series Metbods
Field Filtered NA EPA 200 73005A 15- May- 15-May-08 8051192Filtration
Soluble Metals by EPA 200 Series Methods
7440-22-4 Silver BRL mgl 0002 EPA 200 21-May- 27- May-08 8051249
This laboratory report is IlOt mlid without (II authorized signature on the cover page
Reportble Detection Limit BRL = Below Reporting Limit Page 7 of 25
Sam le Identification MW-
Client Pro ect 2920-96shy
Matrix Ground Water
Collection DateTime 13-May-08 1030
Received 14-May-
SA 78602shy
CAS No A nalyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Soluble Metals by EPA 200 Series Methods
7440-38shy Arsenic 0468 mg1 0040 EPA 200 21-Mayshy 21-May-08 80511 50
7440-43shy Cadmium BRL mg1 0002 EPA 200 21-May-088051249
7440-47shy Chromium BRL mg1 0050 EPA 200 21-May-088051150
7440-50-8 Copper BRL mg1 0050
7439-89-6 Iron 184 mg1 0150
7439-97-6 Mercury BRL mg1 00020 EPA 245 17470A 21-May-088051152
7440-02-0 Nickel BRL mg1 0050 EPA 200 21-May-088051150
7439-92shy Lead 0011 mg1 0002 EPA 200 21-May-088051249
7440-36-0 Antimony 0003 mg1 0002
7782-49shy Selenium BRL mg1 0150 EPA 200 21-May-08 8051150
7440-66-6 Zinc 0186 mgl 0050
General Chemistry Parameters
Filtration Completed NA Varies 14-Mayshy 14-May-08 8051095
18540-29-9 Hexavalent Chromium (soluble) BRL HT2 mg1 125 SM3500CrDI796A 14-Mayshy 14-May-08 8051094 R01 2013 2016
57-12shy Cyanide (total) BRL mg1 0100 EPA 3354 19-Mayshy 19-May-088051374
7782-50shy Total Residual Chlorine BRL CIHT mg1 500 Hach 8167 14-Mayshy 14-May-08 8051049 R01 1900 2001
Total Suspended Solids 580 mg1 25 SM2540D 16-Mayshy 16-May-08 8051275
This lahomtOlY report is not valid without an authorized signature on the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page 8 of 25
Volatie Organic Compounds - Quality Control
Analyte( s)
Batch 8051244 - SW846 5030 Water MS
Blank 8051244-BLK1
Prepared 16-May-08 Analyzed 17-May-
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromochloromethane
1 Dichlorobenzene
1 Dichlorobenzene
1 Dichlorobenzene
1-Dichloroethane
1 Dichloroethane
1 1-Dichloroethene
cis- Dichloroethene
trans- 1 Dichloroethene
1 Dichloropropane
cis- 1 Dichloropropene
trans- 1 Dichloropropene
Ethylbenzene
Hexanone (MBK)
Methyl tert-butyl ether
Methyl- pentanone (MIBK)
Methylene chloride
Styrene
2- Tetrachloroethane
Tetrachloroethene
Toluene
1- Trichloroethane
2- Trichloroethane
Trichloroethene
Trichlorofluoromethane (Freon 11)
Vinyl chloride
p-Xylene
Xylene
Surrogate 4-Bromofluorobenzene Surrogate Toluene-
Surrogate 1 Dichloroethane-Surrogate Dibromofluoromethane
LCS B051244-BS1
Prepared 16-May-08 Analyzed 17 -May-
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Spike Source REC RPD
Result Flag Units RDL Level Result REC Limits RPD Limit
BRL gl 20
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl 10
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gll
BRL gi
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl 10
BRL gll
BRL gll 10
BRL gl 10
BRL gll
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
41 gl 50 70- 130 49 gl 50 70- 130 59 gl 50 119 70- 130 52 gl 50 105 70- 130
QC2 jgl 20 70- 130
18 jgl 20 70- 130
192 jgl 20 35- 155
18 jgl 20 45- 169
19 jgl 20 242
This laboratOlY repol1 is lot valid without 011 authorized sigllature 011 the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page 9 of 25
Volatie Organic Compounds - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051244 - SW846 5030 Water MS
LC5 8051244B51
Prepared 16-May-08 Analyzed 17-May-
Butanone (MEK) 10 QC2 gl 20 70- 130
Carbon tetrachloride 204 gl 20 102 70- 140
Chlorobenzene 18 gl 20 70- 130
Chloroethane 164 gl 20 14-230
Chloroform 18 gll 20 51- 138
Chloromethane 21 gl 20 106 273
Dibromochloromethane 18 gl 20 53- 149
1 Dichlorobenzene 20 gl 20 104 18- 190
1 Dichlorobenzene 19 gl 20 59- 156
1 A-Dichlorobenzene 18 gl 20 18- 190
1- Dichloroethane 19 gl 20 59- 155
1 Dichloroethane 19 gl 20 49- 155
1-Dichloroethene 16 gl 20 70- 130
cis- 1 Dichloroethene 17 gl 20 70- 130
trans- 1 Dichloroethene 16 gll 20 54- 156
1 Dichloropropane 18 gl 20 210
cis- Dichloropropene 17 gl 20 227
trans- 1 Dichloropropene 17 gl 20 17- 183
Ethylbenzene 19 gl 20 37- 162
Hexanone (MBK) 124 QC2 gl 20 70- 130
Methyl tert-butyl ether 19 gl 20 70- 130
Methylshy pentanone (MIBK) 17 gl 20 70- 130
Methylene chloride 16 gl 20 221
Styrene 17 gl 20 70- 130
1 Tetrachloroethane 194 gl 20 46- 157
Tetrachloroethene 15 gl 20 64- 148
Toluene 18 gl 20 70- 130
1- Trichloroethane 20 gl 20 100 52- 162
2- Trichloroethane 18 gl 20 52- 150
Trichloroethene 17 gl 20 71- 157
Trichlorofluoromethane (Freon 11) 19 gl 20 17- 181
Vinyl chloride 21 gl 20 106 251
p-Xylene 39 gl 40 70- 130
Xylene 20 gl 20 102 70- 130
Surrogate 4-Bromofluorobenzene Surrogate Toluene-
Surrogate 1 Dichloroethane-Surrogate Dibromofluoromethane
52 49 56
49
gl
gl
gl
gl
50 50 50
50
105
112 100
70- 130 70- 130 70- 130 70- 130
LC5 DUD (8051244-B5D1
Prepared 16-May-08 Analyzed 17-May-
Acetone QC2 gl 20 70- 130
Benzene 18 gl 20 70- 130
Bromodichloromethane 18 gl 200 35- 155
Bromoform 17 gl 20 45- 169
Bromomethane 18 gl 20 242
Butanone (MEK) 11 QC2 1-91 20 70- 130
Carbon tetrachloride 20 gl 20 100 70- 140
Chlorobenzene 17 gl 20 70- 130
Chloroethane 15 1-91 20 14-230
Chloroform 18 1-91 20 51- 138
This laboratory report is aot valid without a1 authorized sig1ature 01 the cover page
Reportble Detection Limit BRL = Below Reporting Limit Page 10 of25
Volatie Organic Compounds - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051244 - SW846 5030 Water MS
LCS Dup 18051244-BSD1
Prepared 16-May-08 Analyzed 17-May-
Chloromethane 18 1-91 20 273
Dibromochloromethane 174 1-91 20 53- 149
Dichlorobenzene 20 1-91 20 100 18- 190
Dichlorobenzene 18 1-91 20 59- 156
Dichlorobenzene 18 1-91 20 18- 190
Dichloroethane 18 1-91 20 59- 155
Dichloroethane 19 1-91 20 49- 155
Dichloroethene 16 1-91 20 70- 130
cis- Dichloroethene 16 1-91 20 70- 130
trans- Dichloroethene 15 1-91 20 54- 156
Dichloropropane 17 1-91 20 210
cis- Dichloropropene 164 IJgl 20 227
trans- 1 Dichloropropene 164 I-gl 20 17- 183
Etlwlbenzene 18 IJgl 20 37- 162
Hexanone (MBK) 124 QC2 IJgl 20 70- 130
Methyl tert-butyl ether 184 1J91 20 70- 130
Methyl- pentanone (MIBK) 17 IJgl 20 70- 130
Methylene chloride 16 IJgl 20 221
Styrene 16 IJgl 20 70- 130
2- Tetrachloroethane 19 IJgl 20 46- 157
Tetrachloroethene 15 IJgl 20 64- 148
Toluene 17 IJgl 20 70- 130
1- Trichloroethane 19 1-91 20 52- 162
2- Trichloroethane 16 IJgl 20 52- 150
Trichloroethene 15 IJgl 20 71- 157
Trichlorofluoromethane (Freon 11) 17 IJgl 20 17- 181
Vinyl chloride 19 IJglI 20 251
p-Xylene 37 1J91 40 70- 130
Xylene 20 IJgl 20 100 70- 130
Surrogate 4-Bromofluorobenzene 51 IJgl 50 104 70- 130
Surrogate Toluene- 4B gl 50 70- 130
Surrogate 1 0ichloroethane- 53 IJgl 50 106 70- 130 Surrogate Oibromofluoromethane 50 1J9i 50 102 70- 130
Matrix S ike B051244-MS1 Source SA7B629shy
Prepared 16-May-08 Analyzed 17-May-
Benzene 18 20 BRL 70- 130IJgl
Bromodichloromethane 19 IJgl 20 BRL 35- 155
Bromoform 18 IJgl 20 BRL 45- 169
Bromomethane 16 IJgl 20 BRL 242
Carbon tetrachloride 21 IJgl 20 BRL 106 70- 140
Chlorobenzene 18 IJgl 20 BRL 70- 130
Chloroethane 16 IJgl 20 BRL 14-230
Chloroform 18 IJgl 20 BRL 51- 138
Chloromethane 19 IJgl 20 BRL 273
Dibromochloromethane 17 IJgl 20 BRL 53- 149
1 Dichlorobenzene 22 IJgl 20 BRL 112 18- 190
1 Dichlorobenzene 22 IJgl 20 BRL 110 59-156
1 Dichlorobenzene 21 IJgl 20 BRL 109 18- 190
1- Dichloroethane 19 IJgl 20 BRL 59- 155
1 Dichloroethane 18 IJgl 20 BRL 49- 155
This laboratory report is 110t mUd without an authorized signature on the covel page
Reportble Detection Limit BRL = Below Reporting Limit Page It of25
Volatile Organic Compounds - Quality Control
p
Spike Source REC RPD
Result REC imits RPD LimitAnalyte(s) Result Flag Units RDL Level
Batch 8051244 - SW846 5030 Water MS
Matrix ike S051244-MS1 Source SA7B629shy
Prepared 16-May-08 Analyzed 17-Mayshy
17 20 BRL 70- 130 1- Dichloroethene IJgl
16 20 BRL 54- 156trans- 1 Dichloroethene IJgl
21020 BRL1 Dichloropropane 17 1J91
cis- 1 Dichloropropene 17 IJgl 20 BRL 227
17- 183trans- 1 Dichloropropene 184 1J91 20 BRL
20 20 BRL 103 37- 162Ethylbenzene IJgl
15 20 BRL 221Methylene chloride IJgl
20 BRL 46- 1572- Tetrachloroethane 19 1J91
20 BRL 64- 148Tetrachloroethene 18 1J91
BRL 70- 130Toluene 18 1J91 20
105 52-1621- Trichloroethane 211 IJgl 20 BRL
18 20 BRL 52- 1502- Trichloroethane IJgl
17 20 BRL 71- 157Trichloroethene 1J91
20 BRL 17- 181Trichloroluoromethane (Freon 11) 194 IJgl
20 BRL 103 251Vinyl chloride 20 IJgl
102 70- 130Surrogate 4-Bromofluorobenzene 50 IJgl 50 50 70- 130Surrogate Toluene- 49 1J91
56 50 112 70- 130Surrogate 1 Dichloroethane- IJgl
50 100 70- 130Surrogate Dibromofluoromethane 50 IJgl
Matrix S ike Du S051244-MSD1 Source SA7S629shy
Prepared 16-May-08 Analyzed 17-Mayshy
18 20 BRL 70- 130Benzene IJgl
18 20 BRL 35- 155Bromodichloromethane IJgl
17 20 BRL 45- 169Bromoform IJgl
20 BRL 242Bromomethane 17 IJgl
20 BRL 103 70- 140Carbon tetrachloride 20 IJgl
18 20 BRL 70- 130Chlorobenzene 1J91
14-230Chloroethane 16 IJgl 20 BRL
20 51- 138Chloroform 184 IJgl BRL
Chloromethane 19 1J91 20 BRL 273
18 20 BRL 53- 149Dibromochloromethane 1J91
20 BRL 117 18- 190Dichlorobenzene 234 IJgl
20 BRL 112 59- 156Dichlorobenzene 22 IJgl
BRL 108 18- 190Dichlorobenzene 21 1J91 20
20 59- 1551 Dichloroethane 19 IJgl BRL
18 20 BRL 49- 155Dichloroethane IJgl
16 20 BRL 70- 130Dichloroethene IJgl
20 BRL 54- 156trans- Dichloroethene 154 1J91
20 BRL 210Dichloropropane 17 IJgl
0420 BRL 227cis- Dichloropropene 17 IJgl
17- 183trans- Dichloropropene 17 1J91 20 BRL
BRL 37- 162Ethylbenzene 20 1J91 20 102
Methylene chloride 15 IJgl 20 BRL 221
20 BRL 46- 1572- Tetrachloroethane 192 IJgl
20 BRL 64- 148 04Tetrachloroethene 18 IJgl
BRL 70- 130Toluene 184 1J91 20
52- 1621- Trichloroethane 20 IJgl 20 BRL 104
17 20 BRL 52- 1502- Trichloroethane IJgl
17 20 BRL 71- 157Trichloroethene IJgl
20 BRL 17-181Trichlorofluoromethane (Freon 11) 19 IJgl
This laboratory report is IIOt valid without all authorized sigllllture 011 the cover page
Page 12 of25 Reportble Detection Limit BRL = Below Reporting Limit
Semivolatile Organic Compounds by GCMS - Quality Control
Analyte(s)
Batch 8051216 - SW846 3510C
Blank 8051216-BLK1
Prepared amp Analyzed 16-May-
Isophorone
Methylnaphthalene
Methylphenol
3 amp 4-Methylphenol
Naphthalene
Nitroaniline
Nitroaniline
Nitroaniline
Nitrobenzene
Nitrophenol
Nitrophenol
Nitrosodimethylamine
N- N itrosodi-n-pro pyla mine
N itrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Pyridine
1 24-Trichlorobenzene
24 5- Trichlorophenol
246- Trichlorophenol
Surrogate 2-Fuorobipheny Surrogate 2-Fuoropheno Surrogate Nitrobenzene-Surrogate PhenoshySurrogate Terpheny-d4 Surrogate 6- Tribromopheno
LCS B051216-BS1
Prepared amp Analyzed 16-May-
Acenaphthene
Acenaphthylene
Aniline
Anthracene
AzobenzenelDi phenyld lazine
Benzidine
Benzo (a) anthracene
Benzo (a) pyrene
Benzo (b) fluoranthene
Benzo (g i) perylene
Benzo (k) fluoranthene
Benzoic acid
Benzyl alcohol
B is(2-chloroethoxy)methane
B i s (2-ch loroethyl)eth e r
Bis(2-ch loroisopropyl) ether
B is(2-ethy Ih exyl) phtha late
Bromophenyl phenyl ether
Butyl benzyl phthalate
Carbazole
Spike Source REC RPD
Result Flag Units RDL Level Result REC Limits RPD Limit
BRL gl
BRL gl
BRL gl
BRL gl 10
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gll
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
370 gl 50 30- 130 40 gl 50 15- 110 39 gl 50 30- 130 43 gl 50 15- 110 36 gl 50 30- 130 40 gl 50 15- 110
41 gl 50 40- 140
43 gI 50 40- 140
41 gl 50 40- 140
38 gl 50 40- 140
45 gl 50 40- 140
49 gl 50 153
41 gl 50 40- 140
43 gl 50 40- 140
41 gl 50 40- 140
41 gll 50 40- 140
45 gl 50 40- 140
32 gl 50 12- 149
41 gl 50 40- 140
39 gl 50 40- 140
384 gl 50 40- 140
47 gl 50 40- 140
47 gl 50 40- 140
40 gl 50 40- 140
47 gI 50 40- 140
56 gI 50 112 200
This laboratory report is lIot valid witllOut a1l authorized sigllature 011 the coverpage
Reportble Detection Limit BRL = Below Reporting Limit Page 15 of25
Semivolatile Organic Compounds by GCMS - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051216 - SW846 3510C
LCS 8051216-BS1
Prepared amp Analyzed 16-Mayshy
50 30- 1304 -C hloro-3-methylphenol 42 IJgl
40- 140Chloroaniline 39 IJgl 50
Chloronaphthalene 37 IJgl 50 40- 140
Chlorophenol 37 IJgl 50 30- 130
50 40- 140
40- 140
Chlorophenyl phenyl ether 45 IJgl
Chrysene 43 IJgl 50
Dibenzo (a h) anthracene 43 IJgl 50 40- 140
Dibenzofuran IJgl38 50 40- 140
50 40- 1401 Dichlorobenzene 35 IJgl
40- 1401 Dichlorobenzene 264 IJgl 50
40- 1401 Dichlorobenzene 434 IJgl 50
58 50 116 40- 1403 - Dichlorobenzidine IJgl
50 30- 130
40- 140 24-Dichlorophenol 38 IJgl
Diethyl phthalate 484 IJgl 50
50 40- 140Dimethyl phthalate 464 IJgl
Dlmethylphenol 39 IJgl 50 30- 130
DI-n-butyl phthalate 44 IJgll 50 40- 140
30- 130 6-Di nitro- 2-methylphenol 38 1J91 50
30- 130Dinltrophenol 36 1J91 50
42 50 40- 14024-Dlnitrotoluene 1J91
Dlnitrotoluene 1J9141 50 40- 140
Di-n-octyl phthalate 52 IJgl 50 104 40- 140
40- 140Fluoranthene 40 IJgl 50
Fluorene 41 IJgl 50 40- 140
39 50 40- 140Hexachlorobenzene IJgl
50 40- 140Hexachlorobutadiene 40 IJgl
40- 140Hexach lorocyclopentad iene 294 IJgl 50
40 50 40- 140Hexachloroethane IJgl
42 50 40-140Indeno (1 3-cd) pyrene IJgl
50 40- 140Isophorone 40 IJgl
40- 140Methylnaphthalene 394 IJgl 50
40- 140Methylphenol 39 IJgl 50
40 10 50 40- 1403 amp 4-Methylphenol IJgl
37 50 40-140Naphthalene IJgl
50 40-140Nitroaniline 39 IJgl
Nitroaniline 51 IJgl 50 102 40- 140
48 50 40- 140Nltroaniline 1J91
50 40- 140Nitrobenzene 40 IJgl
30- 130Nitrophenol 36 IJgl 50
40 IJgl 50 30- 130Nitrophenol 40- 140Nitrosodimethylamine 32 1J91 50
50 40-140N- N itrosodi-n-propyla mine 46 IJgl
40- 140N itrosodi phenyla ml ne 44 IJgl 50
41 IJgl 50 30- 130Pentachlorophenol 40- 140Phenanthrene 38 IJgl 50
50 30- 130Phenol 38 IJgl
40- 140Pyrene 424 1J91 50
40- 140Pyridine 294 1J91 50
40- 14024- Trichlorobenzene 364 IJgl 50
This laboratory report is not mlid without an authorized signature 011 the cover page
Page 16 of25 Reportble Detection Limit BRL = Below Reporting Limit
Semivolatie Organic Compounds by GCMS - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
BMch 8051216 - SW846 3510C
LC5 8051216-851
Prepared amp Analyzed 16-Mayshy
24 5- Trichlorophenol 404 gl 50 30- 130
246- Trichlorophenol 42 gl 50 30- 130
Surrogate 2-Fluorobiphenyl 29 gl 50 30- 130
Surrogate 2-Fluorophenot 27 gl 50 15- 110
Surrogate Nitrobenzene- 30 gl 50 30- 130
Surrogate Phenol- 29 gl 50 15- 110
Surrogate Terpheny-d4 30 gl 50 30- 130
Surrogate 6- Tribromopheno 324 gl 50 15- 110
This laboratory report is lIot valid without all authorized sigllature 011 tlle cover page
Reportble Detection Limit BRL = Below Reporting Limit Page 17 of25
Semivolatie Organic Compounds by GC - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051106 - SW846 3510C
Blank S051106-BLK1
Prepared amp Analyzed 15-Mayshy
Aroclor- 1016 BRL gI 0200
Aroclor- 1016 (2C) BRL gI 0200
Aroclor- 1221 BRL gI 0200
Aroclor- 1221 (2C) BRL gI 0200
Aroclor- 1232 BRL gI 0200
Aroclor- 1232 (2Cj BRL gI 0200
Aroclor- 1242 BRL gI 0200
Aroclor-1242 (2C) BRL gI 0200
Aroclor- 1248 BRL gI 0200
Aroclor- 1248 (2C) BRL gI 0200
Aroclor- 1254 BRL gI 0200
Aroclor- 1254(2Cj BRL gI 0200
Aroclor- 1260 BRL gI 0200
Aroclor- 1260 (2C) BRL gI 0200
Aroclor- 1262 BRL gI 0200
Aroclor- 1262 (2C) BRL gI 0200
Aroclor-1268 BRL gI 0200
Aroclor- 1268 (2C) BRL gI 0200
Surrogate Decachlorobiphenyl (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0231 0224 0194 0191
gI
gI
gI
gI
0200 0200 0200 0200
116 112
30- 150 30- 150 30- 150 30- 150
LC5 8051106-B51
Prepared 15-May-08 Analyzed 16-May-08
Aroclor- 1016 265 gI 0200 250 106 50- 114
Aroclor- 1 016 (2C) 240 gI 0200 250 50- 114
Aroclor- 1260 0269 gI 0200 250 107 40- 127
Aroclor-1260 (2Cj 270 gI 0200 250 108 40- 127
Surrogate Decachlorobiphenyl (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0225 0224 0188 0183
gI
gI
gI
gI
0200 0200 0200 0200
113 112
30- 150 30- 150 30- 150 30- 150
LC5 DUD rS051106-B5D1
Prepared 15-May-08 Analyzed 16-Mayshy
Aroclor- 1016 262 gl 0200 250 105 50- 114
Aroclor-1 016 (2Cj 241 gI 0200 250 50- 114
Aroclor- 1260 277 gI 0200 250 111 40- 127
Aroclor- 1260(2Cj 0260 gI 0200 250 104 40- 127
Surrogate Decachlorobipheny (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0238 0218 0189 0181
gI
gI
gI
gI
0200 0200 0200 0200
119 109
30- 150 30- 150 30- 150 30- 150
This laboratory report is lot valid without (II authorized sigllature 01 the cover page
Page 18 of25 Reportable Detection Limit BRL = Below Reporting Limit
Extractable Petroleum Hydrocarbons - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051102 - SW846 3510C
Blank 8051102-BLK1
Prepared 15-May-08 Analyzed 19-Mayshy
Non-polar material (SGT- HEM) BRL m91
LC8 8051102-B81
Prepared 15-May-08 Analyzed 19-Mayshy
Non-polar material (SGT- HEM) 184 m91 21 81 904
This laboratory report is not valid without an authorized signature 011 the cover page
Page 19 of25 Reportable Detection Limit BRL = Below Reporting Limit
Soluble Metals by EPA 200 Series Methods - Quality Control
Analyte(s) Result Flag Units RDL
Spike
Level
Source
Result REC
REC
Limits RPD
RPD
Limit
Batch 8051150 - EPA 200 Series
Blank 8051150-BLK1
Prepared amp Analyzed 21-May-
Iron
Zinc
Selenium
Nickel
Chromium
Copper
Arsenic
BRL
BRL
BRL
BRL
BRL
BRL
BRL
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0150
0050
0150
0050
0050
0050
0040
LCS 8051150-BS1
Prepared amp Analyzed 21-May-
Selenium
Zinc
Iron
Nickel
Chromium
Arsenic
Copper
123
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0150
0050
0150
0050
0050
0040
0050
103
105
101
100
85- 115
85- 115
85- 115
85- 115
85- 115
85-115
85- 115
licate B051150-DUP1 Source SA7B602shy
Prepared amp Analyzed 21-May-
Iron
Zinc
Selenium
Nickel
Copper
Chromium
Arsenic
17
0162
BRL
0015
0017
BRL
0450
QR8
mgl
mgl
mgl
mgl
mgl
mgl
mgi
0150
0050
0150
0050
0050
0050
0040
184
0186
BRL
0014
0023
BRL
0468
Matrix S ike 8051150-MS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Iron
Selenium
Nickel
Zinc
Copper
Chromium
Arsenic
19 QM2 mgl
mgll
mgl
mgl
mgl
mgl
mgl
0150
0150
0050
0050
0050
0050
0040
125
184
BRL
0014
0186
0023
BRL
0468
104
105
102
70- 130
70- 130
70-130
70- 130
70- 130
70-130
70- 130
Post S ike 8051150-PS1 Source SA78602shy
Prepared amp Analyzed 21-May-
Zinc
Iron
Selenium
Nickel
Copper
Arsenic
Chromium
18 QM2
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0050
0150
0150
0050
0050
0040
0050
0186
184
BRL
0014
0023
0468
BRL
104
104
101
85- 115
85- 115
85- 115
85-115
85-115
85- 115
85-115
Batch 8051152 - EPA200SW7000 Series
Blank B051152-BLK1
Prepared amp Analyzed 21-May-
Mercury BRL mgl 00020
This laboratory report is IIOt valid witllOut all authorized sigllature 011 the coverpage
Page 20 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Soluble Metals by EPA 200 Series Methods - Quality Control
Analyte(s) Result Flag Units RDL
Spike
Level
Source
Result REC
REC
Limits RPD
RPD
Limit
Batch 8051152 - EPA200SW7000 Series
LCS B051152-BS1
Prepared amp Analyzed 21-May-
Mercury 00576 m91 00020 00500 115 85- 115
licate B051152-DUP1 Source SA78602-01
Prepared amp Analyzed 21-May-
Mercury BRL m91 00020 BRL
Matrix S ike 8051152-MS1 Source SA78602shy
Prepared amp Analyzed 21-May-
Mercury 00632 OM m91 00020 00500 BRL 126 75- 125
Post S ike 8051152-PS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Mercury 00624 OC1 m91 00020 00500 BRL 125 85- 115
Batch 8051249 - 2008No digestion
Blank 8051249-BLK1
Prepared amp Analyzed 21-May-
Lead
Antimony
Cadmium
Silver
BRL
BRL
BRL
BRL
m91
m91
m91
m91
0002
0002
0002
0002
LCS B051249-BS1
Prepared amp Analyzed 21-May-
Antimony
Lead
Silver
Cadmium
143
145 OC2
m91
m91
m91
m91
0050
0050
0050
0040
103
115
107
116
85- 115
85- 115
85- 115
85- 115
licate 8051249-DUP1 Source SA7B602shy
Prepared amp Analyzed 21- May-
Lead
Antimony
Cadmium
Silver
0009
0002
00005
00002
ORB
m91
m91
m91
m91
0002
0002
0002
0002
0011
0003
00005
00003
Matrix S ike 8051249-MS1 Source SA78602shy
Prepared amp Analyzed 21- May-
Lead
Antimony
Cadmium
Silver
142
m91
m91
m91
m91
0050
0050
0040
0050
0011
0003
00005
00003
111
101
114
102
70- 130
70-130
70c130
70- 130
Post S ike 8051249-PS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Antimony
Cadmium
Silver
38
OC2
m91
m91
m91
0050
0040
0050
125
0003
00005
00003
110
121
109
85- 115
85- 115
85- 115
This laboratory report is flOt valid IVithout all authorized signature 011 the cOIer page
Reportable Detection Limit BRL Below Reporting Limit Page 21 of 25
General Chemistry Parameters - Quality Control
Spike Source REC RPD
Analyte( s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051049 - General Preparation
Blank S051 049-BLK1
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
Blank S051049-BLK2
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
Blank S051 049-BLK3
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
LCS S051049-BS1
Prepared amp Analyzed 14-May-
Total Residual Chlorine 046 mgl 020 0500 90- 110
LCS S051049-BS2
Prepared amp Analyzed 14-May-
Total Residual Chlorine 047 mgl 020 0500 90- 110
LCS S051049-BS3
Prepared amp Analyzed 14-May-
Total Residual Chlorine 054 mgl 020 0500 108 90-110
licate B051049-DUP1 Source SA7S544shy
Prepared amp Analyzed 14-May-
Total Residual Chlorine 012 mgl 020 010
licate S051049-DUP2 Source SA7S602-01
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020 BRL
Matrix S ike 8051049-MS1 Source SA78544-01
Prepared amp Analyzed 14-May-
Total Residual Chlorine 065 mgl 020 0500 010 110 80- 120
Matrix S ike 8051049-MS2 Source SA7B602shy
Prepared amp Analyzed 14-May-
Total Residual Chlorine mgl 500 125 BRL 108 80- 120
Reference 8051 049-SRM1
Prepared amp Analyzed 14-May-
Total Residual Chlorine 100 mgl 020 0967 103 85-115
Batch 8051094 - General Preparation
Blank 8051094-BLK1
Prepared amp Analyzed 14 May-
Hexavalent Chromium (soluble) BRL mgl 005
Blank 8051 094-BLK2
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) BRL mgl 005
LCS 8051094-BS1
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) 054 mgl 005 90- 110
licate 8051094-DUP1 Source SA78602-01
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) BRL mgl 125 BRL
Thi laboratory report is not valid without all authorized sigllature 011 the cover page
Page 22 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Page 14
-
LE
GE
ND
APX PROPER BONDA
- APPROXOiSPO SIT BOUNDA
-GR
OU
ND
WA
TE F1 D
IRE
cnON
SCA
LE
30 60 FE
(APR
OX
CORPORATE ENVIRONMENTAL
)i
AD
VISO
RS
INC
SC
AS SH
OW
D
R B
Y K
HA
EL
DA
TE
10407
JOB
NO
2920-96
AERIAL MAP
FO
RM
ER
SP
EE
DW
AY
ST
AT
ION
FlGURE -3
181 EA
BR
OA
AY
GA
NE
R fo
age 1 ot 1Streamflow Statistics Report
Streamstats Ungaged Site Report Date Wed Dec 31 2008 124908 Site Location Massachusetts NAD83 Latitude 425545 (42 3316) NAD83 Longitude -719758 (-71 58 32) NAD27 Latitude 425545 (423316) NAD27 Longitude - 9763 (-71 58 34) Drainage Area 502 mi2
IPeak Flow Basin Characteristics 1100 Statewide Low Flow (S02 mi2)
Regression Equation Valid Rang
I Min II Max1 Value III Parameter Drainage Area (square miles) 161 149
Mean Basin Slope from 250K DEM (percent) 032 24
Stratified Drift per Stream Length (square mile per mile) 129
Massachusetts Region (dimensionless)
Streamflow Statistics
gO-Percent Prediction Interval Prediction Error
MaximumStatistic Flow (ft s) (percent) Minimum
I D50 IIII 11 1811 II 24511 993
I D60 II 35511 2011 II 03611 35111 2411 II 041 I 201I D70 24111 2611 II 03811 151I D75 11 2811 II 0911 3761I D80 981I D85 1 I 3211 II o6311
1 I 3711 II 0441 1 2 2911 D90 11 4611 II 02411 15511 D95I D98 04511 6011 II 01511 11
I D99 03411 6511 II ol1ll 1021
5011 II 02611 11I M7D2Y 1111 3311 II odl 3 541
I AUGD50
IIIIIIIIIIIIIIIIIIIIII 0311 7111 II 0088411 0981I M7Dl0Y
1010
12312008httpstreamstatsagscrusgsgovgisimgReportsFlowStatsReport3494 - 2008123112498
Dilution Factor Calculation Former Speedway Service Station 181 East Broadway Gardner Ma
DF=(Od+Os)Od
DF = Dilution factor
Od = Max flow rate of discharge in cubic feet per second Os = receiving water flow in cubic feet per seconds 7010 flow rate Mahoney Brook 7010 = min flow for seven consecutive days with a recurrence interval of 10 years
7010 flow based on data obtained from USGS Steamflow Statistics Report Data attached
067
Semivolatile Organic Compounds by GCMS - Quality Control
Analyte( s)
Batch 8051216 - SW846 3510C
Blank 8051216BLK1)
Prepared amp Analyzed 16May-
Acenaphthene
Acenaphthylene
Aniline
Anthracene
AzobenzenelDi phenyld iazi ne
Benzidine
Benzo (a) anthracene
Benzo (a) pyrene
Benzo (b) fiuoranthene
Benzo (g i) perylene
Benzo (k) fiuoranthene
Benzoic acid
Benzyl alcohol
Bis(2-ch loroethoxy) methane
Bis(2-ch loroethyl)ether
Bis(2-ch loroi sopropyl)ether
Bis(2ethylhexyl) phthalate
Bromophenyl phenyl ether
Butyl benzyl phthalate
Carbazole
Ch loro-3-methyl phenol
Chloroaniline
Chloronaphthalene
Chlorophenol
Chlorophenyl phenyl ether
Chrysene
Dibenzo (a h) anthracene
Dibenzofuran
Dichlorobenzene
Dichlorobenzene
14- Dichlorobenzene
3 - Dichlorobenzidine
24-Dichlorophenol
Diethyl phthalate
Dimethyl phthalate
24- Dimethylphenol
Din-butyl phthalate
Dinitro-2-methylphenol
Dinitrophenol
Dinitrotoluene
Dinitrotoluene
Di-noctyl phthalate
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopehtadiene
Hexachloroethane
Indeno (1 cd) pyrene
Spike Source REC RPD
Result Flag Units RDL Level Result REC Limits RPD Limit
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gl
BRL gI
BRL gl
BRL gl
BRL gl
BRL gI
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gll
BRL gl
BRL gll
BRL gl
BRL gl
BRL gI
BRL gI
BRL gI
BRL gl
BRL gI
BRL gI
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gI
BRL gI
BRL gl
This laboratory report is IlOt valid without all authorized sigllature 011 the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page t4 of25
Volatie Organic Compounds - Quality Control
p (
Spike Source REC RPD
RDL Level Result REC Limits RPD Limit Analyte(s) Result Flag Units
Batch 8051244 - SW846 5030 Water MS
Matrix S ike Du 8051244-MSD1 Source SA78629shy
Prepared 16-May-08 Analyzed 17-May-BRL 106 251
Vinyl chloride 21 gl 20
101 70- 130 Surrogate 4-Bromofluorobenzene 50 gl 50
70- 13049 gl 50 111 70- 130
Surrogate Toluene-Surrogate 1 Dichloroethane- 55 gl 50
50 70- 130494 glSurrogate Dibromofluoromethane
Microextractable Organic Compounds - Quality Control
Spike Source REC RPD
Flag Units RDL Level Result REC Limits RPD Limit Analyte(s) Result
Batch 8051105 - SW846 3510C
Blank 8051105-BLK
Prepared amp Analyzed 15-May-
BRL gl 01001 Dibromoethane (ED B)
LCS 8051105-BS1
Prepared amp Analyzed 15-Mayshy50- 1500770 gl 0100 100
licate 8051105-DUP1 Source SA7B583shy
Prepared amp Analyzed 15-May-
BRL gl 0100 BRL
1 Dibromoethane (EDB)
1 Dibromoethane (EDB)
This laborntOlY report is not valid without an authorized signature 011 the cover page
Page 13 of2S Reportable Detection Limit BRL = Below Reporting Limit
Sam le Identification Client Pro ect Matrix Collection DateTime ReceivedMWshy
2920-96- Ground Water 13-May-081030 14-May-SA 78602shy
CAS No Analyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Volatile Organic Compounds
Volatile Or anic Com ounds b GCMS
Prepared by method SW846 5030 Water MS
123-91- Dioxane BRL 1-91 200 EPA 624 16-May-08 17-May-08 8051244
994-05-8 Ter-amyl methyl ether BRL 1-911 20
755- Tert-Butanoll butyl alcohol BRL 1-91 200
67-B4- Acetone BRL 1-91 400
71-43- Benzene BRL 1-91 20
75-27-4 Bromodichloromethane BRL 1-91 20
75-25- Bromoform BRL 1-91 20
74-83- Bromomethane BRL 1-91 40
78-93- Butanone (MEK) BRL 1-91 200
56-23- Carbon tetrachloride BRL 1-91 20
108-90- Chlorobenzene BRL 1-91 20
75-00- Chloroethane BRL 1-91 40
676- Chloroform BRL 1-91 20
74-87- Chloromethane BRL 1-91 40
124-48- Dibromochloromethane BRL 1-91 20
95-50- Dichlorobenzene BRL 1-911 20
541-73- Dichlorobenzene BRL 1-91 20
106-46- Dichlorobenzene BRL 1-91 20
75-34- 1- Dichloroethane BRL 1-91 20
107-06- Dichloroethane BRL 1-91 20
75-35-4 1- Dichloroethene BRL 1-91 20
156-59 cis- Dichloroethene BRL 1-91 20
156-60- trans- Dichloroethene BRL 1-91 20
78-87- 2- Dichloropropane BRL 1-91 20
10061-01-5 cis- Dichloropropene BRL 1-91 20
10061-02-B trans- Dichloropropene BRL 1-91 20
100-41-4 Ethylbenzene 411 1-911 20
591-78-B BRL 200Hexanone (MBK) 1-91
1634-04 -4 Methyl tert-butyl ether BRL 1-91 20
108-10- Methyl- pentanone (MIBK) BRL 1-91 200
75-09- Methylene chloride BRL 1-91 200
100-42- Styrene BRL 1-91 20
79-34- 1 Tetrachloroethane BRL 1-91 20
127- 18-4 T etrachloroethene BRL 1-91 20
108-88- Toluene BRL 1-91 20
71-55 1- Trichloroethane BRL 1-91 20
79-00- 2- Trichloroethane BRL 1-91 20
79-01-B Trichloroethene BRL 1-91 20
759-4 Trichlorofluoromethane (Freon 11) BRL 1-91 20
75-01-4 Vinyl chloride BRL 1-91 20
179601-23-1 m Xylene 390 1-91 40
95-47 Xylene 82 1-91 20
Surrogate recoveries 460-00- Bromofluorobenzene 70- 130
2037-26- Toluene- 100 70- 130
17060-07-0 1 Dichloroethane- 111 70- 130
1868-53- Dibromofluoromethane 70- 130
Microextractable Organic Compounds
106-93-4 1 Dibromoethane (EDB) BRL 1-91 0100 EPA 504 15-May- 15-May-08 8051105
Semivolatile Organic Compounds by GCMS
This laboratory report is not valid without all autllOrized signature 011 the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page 5 of 25
Sam le Identification Client Pro ect Matrix Collection DateTime Received
MWshy2920-96- Ground Water 13-May-081030 14-May-
SA 78602shy
CAS No Analyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Semivolatie Organic Compounds by GCMS
Semi volatile Or anic Com ounds b EPA 625
Prepared by method SW846 3510C 50 EPA 625 16-May- 19-May-08 805121683-32- Acenaphthene BRL IJgl
208-96-8 Acenaphthylene BRL IJgl 50
62-53- BRL IJgll 50Aniline
120- 12- Anthracene BRL 1J91 50
103-33- AzobenzenefDiphenyldiazine BRL IJgl 50
92-87 - Benzidine BRL IJgl 50
56-55- Benzo (a) anthracene BRL 1J91 50
50-32 - Benzo (a) pyrene IJglBRL 50
205-99- Benzo (b) fluoranthene BRL IJgl 50
191-24- Benzo (g i) perylene BRL IJgl 50
50207-08- Benzo (k) fluoranthene BRL IJgl
65-85 Benzoic acid BRL 1J91 50
100-51-6 Benzyl alcohol 1J91BRL 50
50111-91- Bis(2-chloroethoxy)methane BRL 1J91
111-4-4 Bis(2-chloroethyl)ether BRL IJgl 50
501 08-60- Bis(2-chloroisopropyl)ether BRL IJgl
117-81- Bis(2-ethylhexyl)phthalate BRL 1J91 50
101-55- Bromophenyl phenyl ether BRL IJgl 50
5085-68- Butyl benzyl phthalate BRL IJgl
5086-74- Carbazole BRL IJgl
5059-50- C hloro-3-methylphenol BRL IJgl
106-47- Chloroaniline BRL IJgl 50
91-58- Chloronaphthalene IJglBRL 50
5095-57 - Chlorophenol BRL 1J91
507005-72- Chlorophenyl phenyl ether BRL IJgl
216-01- Chrysene tJ91BRL 50
5053-70- Dibenzo (a h) anthracene BRL IJgl
50132-64- Dibenzofuran BRL IJgl
95-50- Dichlorobenzene IJglBRL 50
541-73- 13- Dichlorobenzene BRL IJgl 50
106-46- Dichlorobenzene 1J91BRL 50
5091-94- 3 - Dichlorobenzidine BRL IJgl
120-83- Dichlorophenol BRL IJgl 50
84-66- Diethyl phthalate BRL IJgl 50
131-11- Dimethyl phthalate BRL IJgll 50
105-67- Dimethylphenol BRL 1J91 50
5084-74- Di-n- butyl phthalate BRL 1J91
534-52 - Dinitro-2-methylphenol BRL IJgl 50
51-28- Dinitrophenol IJglBRL 50
50121-14- Dinitrotoluene BRL 1J91
606-20- Dinitrotoluene IJglBRL 50
50117-84-0 Di-n-octyl phthalate BRL IJgl
206-44-0 Fluoranthene 1J91BRL 50
BRL 50
50 86-73- Fluorene IJgi
118-74- Hexachlorobenzene BRL 1J91
87-68- Hexachlorobutadiene 1J91BRL 50
5077-47-4 Hexachlorocyclopentadiene BRL IJgl
67-72- Hexachloroethane IJglBRL 50
50193-39- Indeno (1 3-cd) pyrene BRL IJgl
5078-59- Isophorone BRL IJgl
Tfls laboratory report is not valid without all authorized signature 011 the coverpage
Page 6 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Sam le Identification Client Pro ect Matrix Collection DateTime ReceivedMWshy
2920-96- Ground Water I3-May-081030 14-May-SA 78602shy
CAS No Analyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Semivolatile Organic Compounds by GCMS
Semi volatile Or anic Com ounds b EPA 625
Prepared by method SW846 3510C
91-57 -6 Methylnaphthalene 367 1-91 50 EPA 625 16-May- 19-May-08 8051216
95-48- Methylphenol BRL 1-91 50
108-39-4 3 amp 4-Methylphenol BRL I-gl 100 106-44shy91-20- Naphthalene 247 1-91 50
88-74-4 Nitroaniline BRL 1-91 50
99-09- Nitroaniline BRL 1-91 50
100-01-6 Nitroaniline BRL 1-91 50
98-95- Nitrobenzene BRL 1-91 50
88-75- Nitrophenol BRL 1-91 50
100-02- Nitrophenol BRL 1-91 50
62-75- Nitrosodimethylamine BRL 1-91 50
621-64- N- Nitrosodi-n-propylamine BRL 1-91 50
86-30-6 Nitrosodiphenylamine BRL 1-91 50
87 -86- Pentachlorophenol BRL 1-91 50
85-0- Phenanthrene BRL 1-91 50
108-95- Phenol BRL 1-91 50
129-00-0 Pyrene BRL 1-91 50
110-86- Pyridine BRL 1-91 50
120-82- 4- Trichlorobenzene BRL 1-91 50
95-95- 5- Trichlorophenol BRL 1-91 50
88-06- 6- T richlorophenol BRL 1-91 50
Surrogate recoveries
321-60- Fluorobipheny 30- 130
367- 12- Fuorophenol 15- 110
4165-60- Nitrobenzene- 30- 130
4165-62- Pheno- 15- 110
1718-51- Terpheny-d4 30- 130
118- 79- 6- Tribromophenol 15- 110
Semivolatile Organic Compounds by GC
Pol chlorinated Bi hen ls b EPA 608
Prepared by method SW846 3510C
12674- 11-2 Aroclor- 1016 BRL 1-91 0650 EPA 608 15- May- 16-May-08 8051106
11104-28-2 Aroclor-1221 BRL IJgl 0650
11141-16-5 Aroclor- 1232 BRL 1-91 0650
53469-21-9 Aroclor- 1242 BRL 1-91 0650
12672-29-6 Aroclor- 1248 BRL 1-91 0650
11097-69-1 Aroclor- 1254 BRL 1-91 0650
11096-82-5 Aroclor -1260 BRL 1-91 0650
37324-23-5 Aroclor-1262 BRL 1-91 0650
11100-14-4 Aroclor-1268 BRL IJgl 0650
Surrogate recoveries
2051-24- Decachlorobipheny (Sr) 105 30- 150
10386-84-2 4 DB-Octafluorobiphenyl (Sr) 30- 150
Extractable Petroleum Hydrocarbons
mgl EPA 1664 Rev A 15-May- 19-May-08 8051102Non-polar material (SGT- HEM)
Soluble Metals by EPA 2006000 Series Metbods
Field Filtered NA EPA 200 73005A 15- May- 15-May-08 8051192Filtration
Soluble Metals by EPA 200 Series Methods
7440-22-4 Silver BRL mgl 0002 EPA 200 21-May- 27- May-08 8051249
This laboratory report is IlOt mlid without (II authorized signature on the cover page
Reportble Detection Limit BRL = Below Reporting Limit Page 7 of 25
Sam le Identification MW-
Client Pro ect 2920-96shy
Matrix Ground Water
Collection DateTime 13-May-08 1030
Received 14-May-
SA 78602shy
CAS No A nalyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Soluble Metals by EPA 200 Series Methods
7440-38shy Arsenic 0468 mg1 0040 EPA 200 21-Mayshy 21-May-08 80511 50
7440-43shy Cadmium BRL mg1 0002 EPA 200 21-May-088051249
7440-47shy Chromium BRL mg1 0050 EPA 200 21-May-088051150
7440-50-8 Copper BRL mg1 0050
7439-89-6 Iron 184 mg1 0150
7439-97-6 Mercury BRL mg1 00020 EPA 245 17470A 21-May-088051152
7440-02-0 Nickel BRL mg1 0050 EPA 200 21-May-088051150
7439-92shy Lead 0011 mg1 0002 EPA 200 21-May-088051249
7440-36-0 Antimony 0003 mg1 0002
7782-49shy Selenium BRL mg1 0150 EPA 200 21-May-08 8051150
7440-66-6 Zinc 0186 mgl 0050
General Chemistry Parameters
Filtration Completed NA Varies 14-Mayshy 14-May-08 8051095
18540-29-9 Hexavalent Chromium (soluble) BRL HT2 mg1 125 SM3500CrDI796A 14-Mayshy 14-May-08 8051094 R01 2013 2016
57-12shy Cyanide (total) BRL mg1 0100 EPA 3354 19-Mayshy 19-May-088051374
7782-50shy Total Residual Chlorine BRL CIHT mg1 500 Hach 8167 14-Mayshy 14-May-08 8051049 R01 1900 2001
Total Suspended Solids 580 mg1 25 SM2540D 16-Mayshy 16-May-08 8051275
This lahomtOlY report is not valid without an authorized signature on the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page 8 of 25
Volatie Organic Compounds - Quality Control
Analyte( s)
Batch 8051244 - SW846 5030 Water MS
Blank 8051244-BLK1
Prepared 16-May-08 Analyzed 17-May-
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromochloromethane
1 Dichlorobenzene
1 Dichlorobenzene
1 Dichlorobenzene
1-Dichloroethane
1 Dichloroethane
1 1-Dichloroethene
cis- Dichloroethene
trans- 1 Dichloroethene
1 Dichloropropane
cis- 1 Dichloropropene
trans- 1 Dichloropropene
Ethylbenzene
Hexanone (MBK)
Methyl tert-butyl ether
Methyl- pentanone (MIBK)
Methylene chloride
Styrene
2- Tetrachloroethane
Tetrachloroethene
Toluene
1- Trichloroethane
2- Trichloroethane
Trichloroethene
Trichlorofluoromethane (Freon 11)
Vinyl chloride
p-Xylene
Xylene
Surrogate 4-Bromofluorobenzene Surrogate Toluene-
Surrogate 1 Dichloroethane-Surrogate Dibromofluoromethane
LCS B051244-BS1
Prepared 16-May-08 Analyzed 17 -May-
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Spike Source REC RPD
Result Flag Units RDL Level Result REC Limits RPD Limit
BRL gl 20
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl 10
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gll
BRL gi
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl 10
BRL gll
BRL gll 10
BRL gl 10
BRL gll
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
41 gl 50 70- 130 49 gl 50 70- 130 59 gl 50 119 70- 130 52 gl 50 105 70- 130
QC2 jgl 20 70- 130
18 jgl 20 70- 130
192 jgl 20 35- 155
18 jgl 20 45- 169
19 jgl 20 242
This laboratOlY repol1 is lot valid without 011 authorized sigllature 011 the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page 9 of 25
Volatie Organic Compounds - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051244 - SW846 5030 Water MS
LC5 8051244B51
Prepared 16-May-08 Analyzed 17-May-
Butanone (MEK) 10 QC2 gl 20 70- 130
Carbon tetrachloride 204 gl 20 102 70- 140
Chlorobenzene 18 gl 20 70- 130
Chloroethane 164 gl 20 14-230
Chloroform 18 gll 20 51- 138
Chloromethane 21 gl 20 106 273
Dibromochloromethane 18 gl 20 53- 149
1 Dichlorobenzene 20 gl 20 104 18- 190
1 Dichlorobenzene 19 gl 20 59- 156
1 A-Dichlorobenzene 18 gl 20 18- 190
1- Dichloroethane 19 gl 20 59- 155
1 Dichloroethane 19 gl 20 49- 155
1-Dichloroethene 16 gl 20 70- 130
cis- 1 Dichloroethene 17 gl 20 70- 130
trans- 1 Dichloroethene 16 gll 20 54- 156
1 Dichloropropane 18 gl 20 210
cis- Dichloropropene 17 gl 20 227
trans- 1 Dichloropropene 17 gl 20 17- 183
Ethylbenzene 19 gl 20 37- 162
Hexanone (MBK) 124 QC2 gl 20 70- 130
Methyl tert-butyl ether 19 gl 20 70- 130
Methylshy pentanone (MIBK) 17 gl 20 70- 130
Methylene chloride 16 gl 20 221
Styrene 17 gl 20 70- 130
1 Tetrachloroethane 194 gl 20 46- 157
Tetrachloroethene 15 gl 20 64- 148
Toluene 18 gl 20 70- 130
1- Trichloroethane 20 gl 20 100 52- 162
2- Trichloroethane 18 gl 20 52- 150
Trichloroethene 17 gl 20 71- 157
Trichlorofluoromethane (Freon 11) 19 gl 20 17- 181
Vinyl chloride 21 gl 20 106 251
p-Xylene 39 gl 40 70- 130
Xylene 20 gl 20 102 70- 130
Surrogate 4-Bromofluorobenzene Surrogate Toluene-
Surrogate 1 Dichloroethane-Surrogate Dibromofluoromethane
52 49 56
49
gl
gl
gl
gl
50 50 50
50
105
112 100
70- 130 70- 130 70- 130 70- 130
LC5 DUD (8051244-B5D1
Prepared 16-May-08 Analyzed 17-May-
Acetone QC2 gl 20 70- 130
Benzene 18 gl 20 70- 130
Bromodichloromethane 18 gl 200 35- 155
Bromoform 17 gl 20 45- 169
Bromomethane 18 gl 20 242
Butanone (MEK) 11 QC2 1-91 20 70- 130
Carbon tetrachloride 20 gl 20 100 70- 140
Chlorobenzene 17 gl 20 70- 130
Chloroethane 15 1-91 20 14-230
Chloroform 18 1-91 20 51- 138
This laboratory report is aot valid without a1 authorized sig1ature 01 the cover page
Reportble Detection Limit BRL = Below Reporting Limit Page 10 of25
Volatie Organic Compounds - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051244 - SW846 5030 Water MS
LCS Dup 18051244-BSD1
Prepared 16-May-08 Analyzed 17-May-
Chloromethane 18 1-91 20 273
Dibromochloromethane 174 1-91 20 53- 149
Dichlorobenzene 20 1-91 20 100 18- 190
Dichlorobenzene 18 1-91 20 59- 156
Dichlorobenzene 18 1-91 20 18- 190
Dichloroethane 18 1-91 20 59- 155
Dichloroethane 19 1-91 20 49- 155
Dichloroethene 16 1-91 20 70- 130
cis- Dichloroethene 16 1-91 20 70- 130
trans- Dichloroethene 15 1-91 20 54- 156
Dichloropropane 17 1-91 20 210
cis- Dichloropropene 164 IJgl 20 227
trans- 1 Dichloropropene 164 I-gl 20 17- 183
Etlwlbenzene 18 IJgl 20 37- 162
Hexanone (MBK) 124 QC2 IJgl 20 70- 130
Methyl tert-butyl ether 184 1J91 20 70- 130
Methyl- pentanone (MIBK) 17 IJgl 20 70- 130
Methylene chloride 16 IJgl 20 221
Styrene 16 IJgl 20 70- 130
2- Tetrachloroethane 19 IJgl 20 46- 157
Tetrachloroethene 15 IJgl 20 64- 148
Toluene 17 IJgl 20 70- 130
1- Trichloroethane 19 1-91 20 52- 162
2- Trichloroethane 16 IJgl 20 52- 150
Trichloroethene 15 IJgl 20 71- 157
Trichlorofluoromethane (Freon 11) 17 IJgl 20 17- 181
Vinyl chloride 19 IJglI 20 251
p-Xylene 37 1J91 40 70- 130
Xylene 20 IJgl 20 100 70- 130
Surrogate 4-Bromofluorobenzene 51 IJgl 50 104 70- 130
Surrogate Toluene- 4B gl 50 70- 130
Surrogate 1 0ichloroethane- 53 IJgl 50 106 70- 130 Surrogate Oibromofluoromethane 50 1J9i 50 102 70- 130
Matrix S ike B051244-MS1 Source SA7B629shy
Prepared 16-May-08 Analyzed 17-May-
Benzene 18 20 BRL 70- 130IJgl
Bromodichloromethane 19 IJgl 20 BRL 35- 155
Bromoform 18 IJgl 20 BRL 45- 169
Bromomethane 16 IJgl 20 BRL 242
Carbon tetrachloride 21 IJgl 20 BRL 106 70- 140
Chlorobenzene 18 IJgl 20 BRL 70- 130
Chloroethane 16 IJgl 20 BRL 14-230
Chloroform 18 IJgl 20 BRL 51- 138
Chloromethane 19 IJgl 20 BRL 273
Dibromochloromethane 17 IJgl 20 BRL 53- 149
1 Dichlorobenzene 22 IJgl 20 BRL 112 18- 190
1 Dichlorobenzene 22 IJgl 20 BRL 110 59-156
1 Dichlorobenzene 21 IJgl 20 BRL 109 18- 190
1- Dichloroethane 19 IJgl 20 BRL 59- 155
1 Dichloroethane 18 IJgl 20 BRL 49- 155
This laboratory report is 110t mUd without an authorized signature on the covel page
Reportble Detection Limit BRL = Below Reporting Limit Page It of25
Volatile Organic Compounds - Quality Control
p
Spike Source REC RPD
Result REC imits RPD LimitAnalyte(s) Result Flag Units RDL Level
Batch 8051244 - SW846 5030 Water MS
Matrix ike S051244-MS1 Source SA7B629shy
Prepared 16-May-08 Analyzed 17-Mayshy
17 20 BRL 70- 130 1- Dichloroethene IJgl
16 20 BRL 54- 156trans- 1 Dichloroethene IJgl
21020 BRL1 Dichloropropane 17 1J91
cis- 1 Dichloropropene 17 IJgl 20 BRL 227
17- 183trans- 1 Dichloropropene 184 1J91 20 BRL
20 20 BRL 103 37- 162Ethylbenzene IJgl
15 20 BRL 221Methylene chloride IJgl
20 BRL 46- 1572- Tetrachloroethane 19 1J91
20 BRL 64- 148Tetrachloroethene 18 1J91
BRL 70- 130Toluene 18 1J91 20
105 52-1621- Trichloroethane 211 IJgl 20 BRL
18 20 BRL 52- 1502- Trichloroethane IJgl
17 20 BRL 71- 157Trichloroethene 1J91
20 BRL 17- 181Trichloroluoromethane (Freon 11) 194 IJgl
20 BRL 103 251Vinyl chloride 20 IJgl
102 70- 130Surrogate 4-Bromofluorobenzene 50 IJgl 50 50 70- 130Surrogate Toluene- 49 1J91
56 50 112 70- 130Surrogate 1 Dichloroethane- IJgl
50 100 70- 130Surrogate Dibromofluoromethane 50 IJgl
Matrix S ike Du S051244-MSD1 Source SA7S629shy
Prepared 16-May-08 Analyzed 17-Mayshy
18 20 BRL 70- 130Benzene IJgl
18 20 BRL 35- 155Bromodichloromethane IJgl
17 20 BRL 45- 169Bromoform IJgl
20 BRL 242Bromomethane 17 IJgl
20 BRL 103 70- 140Carbon tetrachloride 20 IJgl
18 20 BRL 70- 130Chlorobenzene 1J91
14-230Chloroethane 16 IJgl 20 BRL
20 51- 138Chloroform 184 IJgl BRL
Chloromethane 19 1J91 20 BRL 273
18 20 BRL 53- 149Dibromochloromethane 1J91
20 BRL 117 18- 190Dichlorobenzene 234 IJgl
20 BRL 112 59- 156Dichlorobenzene 22 IJgl
BRL 108 18- 190Dichlorobenzene 21 1J91 20
20 59- 1551 Dichloroethane 19 IJgl BRL
18 20 BRL 49- 155Dichloroethane IJgl
16 20 BRL 70- 130Dichloroethene IJgl
20 BRL 54- 156trans- Dichloroethene 154 1J91
20 BRL 210Dichloropropane 17 IJgl
0420 BRL 227cis- Dichloropropene 17 IJgl
17- 183trans- Dichloropropene 17 1J91 20 BRL
BRL 37- 162Ethylbenzene 20 1J91 20 102
Methylene chloride 15 IJgl 20 BRL 221
20 BRL 46- 1572- Tetrachloroethane 192 IJgl
20 BRL 64- 148 04Tetrachloroethene 18 IJgl
BRL 70- 130Toluene 184 1J91 20
52- 1621- Trichloroethane 20 IJgl 20 BRL 104
17 20 BRL 52- 1502- Trichloroethane IJgl
17 20 BRL 71- 157Trichloroethene IJgl
20 BRL 17-181Trichlorofluoromethane (Freon 11) 19 IJgl
This laboratory report is IIOt valid without all authorized sigllllture 011 the cover page
Page 12 of25 Reportble Detection Limit BRL = Below Reporting Limit
Semivolatile Organic Compounds by GCMS - Quality Control
Analyte(s)
Batch 8051216 - SW846 3510C
Blank 8051216-BLK1
Prepared amp Analyzed 16-May-
Isophorone
Methylnaphthalene
Methylphenol
3 amp 4-Methylphenol
Naphthalene
Nitroaniline
Nitroaniline
Nitroaniline
Nitrobenzene
Nitrophenol
Nitrophenol
Nitrosodimethylamine
N- N itrosodi-n-pro pyla mine
N itrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Pyridine
1 24-Trichlorobenzene
24 5- Trichlorophenol
246- Trichlorophenol
Surrogate 2-Fuorobipheny Surrogate 2-Fuoropheno Surrogate Nitrobenzene-Surrogate PhenoshySurrogate Terpheny-d4 Surrogate 6- Tribromopheno
LCS B051216-BS1
Prepared amp Analyzed 16-May-
Acenaphthene
Acenaphthylene
Aniline
Anthracene
AzobenzenelDi phenyld lazine
Benzidine
Benzo (a) anthracene
Benzo (a) pyrene
Benzo (b) fluoranthene
Benzo (g i) perylene
Benzo (k) fluoranthene
Benzoic acid
Benzyl alcohol
B is(2-chloroethoxy)methane
B i s (2-ch loroethyl)eth e r
Bis(2-ch loroisopropyl) ether
B is(2-ethy Ih exyl) phtha late
Bromophenyl phenyl ether
Butyl benzyl phthalate
Carbazole
Spike Source REC RPD
Result Flag Units RDL Level Result REC Limits RPD Limit
BRL gl
BRL gl
BRL gl
BRL gl 10
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gll
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
370 gl 50 30- 130 40 gl 50 15- 110 39 gl 50 30- 130 43 gl 50 15- 110 36 gl 50 30- 130 40 gl 50 15- 110
41 gl 50 40- 140
43 gI 50 40- 140
41 gl 50 40- 140
38 gl 50 40- 140
45 gl 50 40- 140
49 gl 50 153
41 gl 50 40- 140
43 gl 50 40- 140
41 gl 50 40- 140
41 gll 50 40- 140
45 gl 50 40- 140
32 gl 50 12- 149
41 gl 50 40- 140
39 gl 50 40- 140
384 gl 50 40- 140
47 gl 50 40- 140
47 gl 50 40- 140
40 gl 50 40- 140
47 gI 50 40- 140
56 gI 50 112 200
This laboratory report is lIot valid witllOut a1l authorized sigllature 011 the coverpage
Reportble Detection Limit BRL = Below Reporting Limit Page 15 of25
Semivolatile Organic Compounds by GCMS - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051216 - SW846 3510C
LCS 8051216-BS1
Prepared amp Analyzed 16-Mayshy
50 30- 1304 -C hloro-3-methylphenol 42 IJgl
40- 140Chloroaniline 39 IJgl 50
Chloronaphthalene 37 IJgl 50 40- 140
Chlorophenol 37 IJgl 50 30- 130
50 40- 140
40- 140
Chlorophenyl phenyl ether 45 IJgl
Chrysene 43 IJgl 50
Dibenzo (a h) anthracene 43 IJgl 50 40- 140
Dibenzofuran IJgl38 50 40- 140
50 40- 1401 Dichlorobenzene 35 IJgl
40- 1401 Dichlorobenzene 264 IJgl 50
40- 1401 Dichlorobenzene 434 IJgl 50
58 50 116 40- 1403 - Dichlorobenzidine IJgl
50 30- 130
40- 140 24-Dichlorophenol 38 IJgl
Diethyl phthalate 484 IJgl 50
50 40- 140Dimethyl phthalate 464 IJgl
Dlmethylphenol 39 IJgl 50 30- 130
DI-n-butyl phthalate 44 IJgll 50 40- 140
30- 130 6-Di nitro- 2-methylphenol 38 1J91 50
30- 130Dinltrophenol 36 1J91 50
42 50 40- 14024-Dlnitrotoluene 1J91
Dlnitrotoluene 1J9141 50 40- 140
Di-n-octyl phthalate 52 IJgl 50 104 40- 140
40- 140Fluoranthene 40 IJgl 50
Fluorene 41 IJgl 50 40- 140
39 50 40- 140Hexachlorobenzene IJgl
50 40- 140Hexachlorobutadiene 40 IJgl
40- 140Hexach lorocyclopentad iene 294 IJgl 50
40 50 40- 140Hexachloroethane IJgl
42 50 40-140Indeno (1 3-cd) pyrene IJgl
50 40- 140Isophorone 40 IJgl
40- 140Methylnaphthalene 394 IJgl 50
40- 140Methylphenol 39 IJgl 50
40 10 50 40- 1403 amp 4-Methylphenol IJgl
37 50 40-140Naphthalene IJgl
50 40-140Nitroaniline 39 IJgl
Nitroaniline 51 IJgl 50 102 40- 140
48 50 40- 140Nltroaniline 1J91
50 40- 140Nitrobenzene 40 IJgl
30- 130Nitrophenol 36 IJgl 50
40 IJgl 50 30- 130Nitrophenol 40- 140Nitrosodimethylamine 32 1J91 50
50 40-140N- N itrosodi-n-propyla mine 46 IJgl
40- 140N itrosodi phenyla ml ne 44 IJgl 50
41 IJgl 50 30- 130Pentachlorophenol 40- 140Phenanthrene 38 IJgl 50
50 30- 130Phenol 38 IJgl
40- 140Pyrene 424 1J91 50
40- 140Pyridine 294 1J91 50
40- 14024- Trichlorobenzene 364 IJgl 50
This laboratory report is not mlid without an authorized signature 011 the cover page
Page 16 of25 Reportble Detection Limit BRL = Below Reporting Limit
Semivolatie Organic Compounds by GCMS - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
BMch 8051216 - SW846 3510C
LC5 8051216-851
Prepared amp Analyzed 16-Mayshy
24 5- Trichlorophenol 404 gl 50 30- 130
246- Trichlorophenol 42 gl 50 30- 130
Surrogate 2-Fluorobiphenyl 29 gl 50 30- 130
Surrogate 2-Fluorophenot 27 gl 50 15- 110
Surrogate Nitrobenzene- 30 gl 50 30- 130
Surrogate Phenol- 29 gl 50 15- 110
Surrogate Terpheny-d4 30 gl 50 30- 130
Surrogate 6- Tribromopheno 324 gl 50 15- 110
This laboratory report is lIot valid without all authorized sigllature 011 tlle cover page
Reportble Detection Limit BRL = Below Reporting Limit Page 17 of25
Semivolatie Organic Compounds by GC - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051106 - SW846 3510C
Blank S051106-BLK1
Prepared amp Analyzed 15-Mayshy
Aroclor- 1016 BRL gI 0200
Aroclor- 1016 (2C) BRL gI 0200
Aroclor- 1221 BRL gI 0200
Aroclor- 1221 (2C) BRL gI 0200
Aroclor- 1232 BRL gI 0200
Aroclor- 1232 (2Cj BRL gI 0200
Aroclor- 1242 BRL gI 0200
Aroclor-1242 (2C) BRL gI 0200
Aroclor- 1248 BRL gI 0200
Aroclor- 1248 (2C) BRL gI 0200
Aroclor- 1254 BRL gI 0200
Aroclor- 1254(2Cj BRL gI 0200
Aroclor- 1260 BRL gI 0200
Aroclor- 1260 (2C) BRL gI 0200
Aroclor- 1262 BRL gI 0200
Aroclor- 1262 (2C) BRL gI 0200
Aroclor-1268 BRL gI 0200
Aroclor- 1268 (2C) BRL gI 0200
Surrogate Decachlorobiphenyl (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0231 0224 0194 0191
gI
gI
gI
gI
0200 0200 0200 0200
116 112
30- 150 30- 150 30- 150 30- 150
LC5 8051106-B51
Prepared 15-May-08 Analyzed 16-May-08
Aroclor- 1016 265 gI 0200 250 106 50- 114
Aroclor- 1 016 (2C) 240 gI 0200 250 50- 114
Aroclor- 1260 0269 gI 0200 250 107 40- 127
Aroclor-1260 (2Cj 270 gI 0200 250 108 40- 127
Surrogate Decachlorobiphenyl (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0225 0224 0188 0183
gI
gI
gI
gI
0200 0200 0200 0200
113 112
30- 150 30- 150 30- 150 30- 150
LC5 DUD rS051106-B5D1
Prepared 15-May-08 Analyzed 16-Mayshy
Aroclor- 1016 262 gl 0200 250 105 50- 114
Aroclor-1 016 (2Cj 241 gI 0200 250 50- 114
Aroclor- 1260 277 gI 0200 250 111 40- 127
Aroclor- 1260(2Cj 0260 gI 0200 250 104 40- 127
Surrogate Decachlorobipheny (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0238 0218 0189 0181
gI
gI
gI
gI
0200 0200 0200 0200
119 109
30- 150 30- 150 30- 150 30- 150
This laboratory report is lot valid without (II authorized sigllature 01 the cover page
Page 18 of25 Reportable Detection Limit BRL = Below Reporting Limit
Extractable Petroleum Hydrocarbons - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051102 - SW846 3510C
Blank 8051102-BLK1
Prepared 15-May-08 Analyzed 19-Mayshy
Non-polar material (SGT- HEM) BRL m91
LC8 8051102-B81
Prepared 15-May-08 Analyzed 19-Mayshy
Non-polar material (SGT- HEM) 184 m91 21 81 904
This laboratory report is not valid without an authorized signature 011 the cover page
Page 19 of25 Reportable Detection Limit BRL = Below Reporting Limit
Soluble Metals by EPA 200 Series Methods - Quality Control
Analyte(s) Result Flag Units RDL
Spike
Level
Source
Result REC
REC
Limits RPD
RPD
Limit
Batch 8051150 - EPA 200 Series
Blank 8051150-BLK1
Prepared amp Analyzed 21-May-
Iron
Zinc
Selenium
Nickel
Chromium
Copper
Arsenic
BRL
BRL
BRL
BRL
BRL
BRL
BRL
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0150
0050
0150
0050
0050
0050
0040
LCS 8051150-BS1
Prepared amp Analyzed 21-May-
Selenium
Zinc
Iron
Nickel
Chromium
Arsenic
Copper
123
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0150
0050
0150
0050
0050
0040
0050
103
105
101
100
85- 115
85- 115
85- 115
85- 115
85- 115
85-115
85- 115
licate B051150-DUP1 Source SA7B602shy
Prepared amp Analyzed 21-May-
Iron
Zinc
Selenium
Nickel
Copper
Chromium
Arsenic
17
0162
BRL
0015
0017
BRL
0450
QR8
mgl
mgl
mgl
mgl
mgl
mgl
mgi
0150
0050
0150
0050
0050
0050
0040
184
0186
BRL
0014
0023
BRL
0468
Matrix S ike 8051150-MS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Iron
Selenium
Nickel
Zinc
Copper
Chromium
Arsenic
19 QM2 mgl
mgll
mgl
mgl
mgl
mgl
mgl
0150
0150
0050
0050
0050
0050
0040
125
184
BRL
0014
0186
0023
BRL
0468
104
105
102
70- 130
70- 130
70-130
70- 130
70- 130
70-130
70- 130
Post S ike 8051150-PS1 Source SA78602shy
Prepared amp Analyzed 21-May-
Zinc
Iron
Selenium
Nickel
Copper
Arsenic
Chromium
18 QM2
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0050
0150
0150
0050
0050
0040
0050
0186
184
BRL
0014
0023
0468
BRL
104
104
101
85- 115
85- 115
85- 115
85-115
85-115
85- 115
85-115
Batch 8051152 - EPA200SW7000 Series
Blank B051152-BLK1
Prepared amp Analyzed 21-May-
Mercury BRL mgl 00020
This laboratory report is IIOt valid witllOut all authorized sigllature 011 the coverpage
Page 20 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Soluble Metals by EPA 200 Series Methods - Quality Control
Analyte(s) Result Flag Units RDL
Spike
Level
Source
Result REC
REC
Limits RPD
RPD
Limit
Batch 8051152 - EPA200SW7000 Series
LCS B051152-BS1
Prepared amp Analyzed 21-May-
Mercury 00576 m91 00020 00500 115 85- 115
licate B051152-DUP1 Source SA78602-01
Prepared amp Analyzed 21-May-
Mercury BRL m91 00020 BRL
Matrix S ike 8051152-MS1 Source SA78602shy
Prepared amp Analyzed 21-May-
Mercury 00632 OM m91 00020 00500 BRL 126 75- 125
Post S ike 8051152-PS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Mercury 00624 OC1 m91 00020 00500 BRL 125 85- 115
Batch 8051249 - 2008No digestion
Blank 8051249-BLK1
Prepared amp Analyzed 21-May-
Lead
Antimony
Cadmium
Silver
BRL
BRL
BRL
BRL
m91
m91
m91
m91
0002
0002
0002
0002
LCS B051249-BS1
Prepared amp Analyzed 21-May-
Antimony
Lead
Silver
Cadmium
143
145 OC2
m91
m91
m91
m91
0050
0050
0050
0040
103
115
107
116
85- 115
85- 115
85- 115
85- 115
licate 8051249-DUP1 Source SA7B602shy
Prepared amp Analyzed 21- May-
Lead
Antimony
Cadmium
Silver
0009
0002
00005
00002
ORB
m91
m91
m91
m91
0002
0002
0002
0002
0011
0003
00005
00003
Matrix S ike 8051249-MS1 Source SA78602shy
Prepared amp Analyzed 21- May-
Lead
Antimony
Cadmium
Silver
142
m91
m91
m91
m91
0050
0050
0040
0050
0011
0003
00005
00003
111
101
114
102
70- 130
70-130
70c130
70- 130
Post S ike 8051249-PS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Antimony
Cadmium
Silver
38
OC2
m91
m91
m91
0050
0040
0050
125
0003
00005
00003
110
121
109
85- 115
85- 115
85- 115
This laboratory report is flOt valid IVithout all authorized signature 011 the cOIer page
Reportable Detection Limit BRL Below Reporting Limit Page 21 of 25
General Chemistry Parameters - Quality Control
Spike Source REC RPD
Analyte( s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051049 - General Preparation
Blank S051 049-BLK1
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
Blank S051049-BLK2
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
Blank S051 049-BLK3
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
LCS S051049-BS1
Prepared amp Analyzed 14-May-
Total Residual Chlorine 046 mgl 020 0500 90- 110
LCS S051049-BS2
Prepared amp Analyzed 14-May-
Total Residual Chlorine 047 mgl 020 0500 90- 110
LCS S051049-BS3
Prepared amp Analyzed 14-May-
Total Residual Chlorine 054 mgl 020 0500 108 90-110
licate B051049-DUP1 Source SA7S544shy
Prepared amp Analyzed 14-May-
Total Residual Chlorine 012 mgl 020 010
licate S051049-DUP2 Source SA7S602-01
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020 BRL
Matrix S ike 8051049-MS1 Source SA78544-01
Prepared amp Analyzed 14-May-
Total Residual Chlorine 065 mgl 020 0500 010 110 80- 120
Matrix S ike 8051049-MS2 Source SA7B602shy
Prepared amp Analyzed 14-May-
Total Residual Chlorine mgl 500 125 BRL 108 80- 120
Reference 8051 049-SRM1
Prepared amp Analyzed 14-May-
Total Residual Chlorine 100 mgl 020 0967 103 85-115
Batch 8051094 - General Preparation
Blank 8051094-BLK1
Prepared amp Analyzed 14 May-
Hexavalent Chromium (soluble) BRL mgl 005
Blank 8051 094-BLK2
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) BRL mgl 005
LCS 8051094-BS1
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) 054 mgl 005 90- 110
licate 8051094-DUP1 Source SA78602-01
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) BRL mgl 125 BRL
Thi laboratory report is not valid without all authorized sigllature 011 the cover page
Page 22 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Page 15
age 1 ot 1Streamflow Statistics Report
Streamstats Ungaged Site Report Date Wed Dec 31 2008 124908 Site Location Massachusetts NAD83 Latitude 425545 (42 3316) NAD83 Longitude -719758 (-71 58 32) NAD27 Latitude 425545 (423316) NAD27 Longitude - 9763 (-71 58 34) Drainage Area 502 mi2
IPeak Flow Basin Characteristics 1100 Statewide Low Flow (S02 mi2)
Regression Equation Valid Rang
I Min II Max1 Value III Parameter Drainage Area (square miles) 161 149
Mean Basin Slope from 250K DEM (percent) 032 24
Stratified Drift per Stream Length (square mile per mile) 129
Massachusetts Region (dimensionless)
Streamflow Statistics
gO-Percent Prediction Interval Prediction Error
MaximumStatistic Flow (ft s) (percent) Minimum
I D50 IIII 11 1811 II 24511 993
I D60 II 35511 2011 II 03611 35111 2411 II 041 I 201I D70 24111 2611 II 03811 151I D75 11 2811 II 0911 3761I D80 981I D85 1 I 3211 II o6311
1 I 3711 II 0441 1 2 2911 D90 11 4611 II 02411 15511 D95I D98 04511 6011 II 01511 11
I D99 03411 6511 II ol1ll 1021
5011 II 02611 11I M7D2Y 1111 3311 II odl 3 541
I AUGD50
IIIIIIIIIIIIIIIIIIIIII 0311 7111 II 0088411 0981I M7Dl0Y
1010
12312008httpstreamstatsagscrusgsgovgisimgReportsFlowStatsReport3494 - 2008123112498
Dilution Factor Calculation Former Speedway Service Station 181 East Broadway Gardner Ma
DF=(Od+Os)Od
DF = Dilution factor
Od = Max flow rate of discharge in cubic feet per second Os = receiving water flow in cubic feet per seconds 7010 flow rate Mahoney Brook 7010 = min flow for seven consecutive days with a recurrence interval of 10 years
7010 flow based on data obtained from USGS Steamflow Statistics Report Data attached
067
Semivolatile Organic Compounds by GCMS - Quality Control
Analyte( s)
Batch 8051216 - SW846 3510C
Blank 8051216BLK1)
Prepared amp Analyzed 16May-
Acenaphthene
Acenaphthylene
Aniline
Anthracene
AzobenzenelDi phenyld iazi ne
Benzidine
Benzo (a) anthracene
Benzo (a) pyrene
Benzo (b) fiuoranthene
Benzo (g i) perylene
Benzo (k) fiuoranthene
Benzoic acid
Benzyl alcohol
Bis(2-ch loroethoxy) methane
Bis(2-ch loroethyl)ether
Bis(2-ch loroi sopropyl)ether
Bis(2ethylhexyl) phthalate
Bromophenyl phenyl ether
Butyl benzyl phthalate
Carbazole
Ch loro-3-methyl phenol
Chloroaniline
Chloronaphthalene
Chlorophenol
Chlorophenyl phenyl ether
Chrysene
Dibenzo (a h) anthracene
Dibenzofuran
Dichlorobenzene
Dichlorobenzene
14- Dichlorobenzene
3 - Dichlorobenzidine
24-Dichlorophenol
Diethyl phthalate
Dimethyl phthalate
24- Dimethylphenol
Din-butyl phthalate
Dinitro-2-methylphenol
Dinitrophenol
Dinitrotoluene
Dinitrotoluene
Di-noctyl phthalate
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopehtadiene
Hexachloroethane
Indeno (1 cd) pyrene
Spike Source REC RPD
Result Flag Units RDL Level Result REC Limits RPD Limit
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gl
BRL gI
BRL gl
BRL gl
BRL gl
BRL gI
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gll
BRL gl
BRL gll
BRL gl
BRL gl
BRL gI
BRL gI
BRL gI
BRL gl
BRL gI
BRL gI
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gI
BRL gI
BRL gl
This laboratory report is IlOt valid without all authorized sigllature 011 the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page t4 of25
Volatie Organic Compounds - Quality Control
p (
Spike Source REC RPD
RDL Level Result REC Limits RPD Limit Analyte(s) Result Flag Units
Batch 8051244 - SW846 5030 Water MS
Matrix S ike Du 8051244-MSD1 Source SA78629shy
Prepared 16-May-08 Analyzed 17-May-BRL 106 251
Vinyl chloride 21 gl 20
101 70- 130 Surrogate 4-Bromofluorobenzene 50 gl 50
70- 13049 gl 50 111 70- 130
Surrogate Toluene-Surrogate 1 Dichloroethane- 55 gl 50
50 70- 130494 glSurrogate Dibromofluoromethane
Microextractable Organic Compounds - Quality Control
Spike Source REC RPD
Flag Units RDL Level Result REC Limits RPD Limit Analyte(s) Result
Batch 8051105 - SW846 3510C
Blank 8051105-BLK
Prepared amp Analyzed 15-May-
BRL gl 01001 Dibromoethane (ED B)
LCS 8051105-BS1
Prepared amp Analyzed 15-Mayshy50- 1500770 gl 0100 100
licate 8051105-DUP1 Source SA7B583shy
Prepared amp Analyzed 15-May-
BRL gl 0100 BRL
1 Dibromoethane (EDB)
1 Dibromoethane (EDB)
This laborntOlY report is not valid without an authorized signature 011 the cover page
Page 13 of2S Reportable Detection Limit BRL = Below Reporting Limit
Sam le Identification Client Pro ect Matrix Collection DateTime ReceivedMWshy
2920-96- Ground Water 13-May-081030 14-May-SA 78602shy
CAS No Analyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Volatile Organic Compounds
Volatile Or anic Com ounds b GCMS
Prepared by method SW846 5030 Water MS
123-91- Dioxane BRL 1-91 200 EPA 624 16-May-08 17-May-08 8051244
994-05-8 Ter-amyl methyl ether BRL 1-911 20
755- Tert-Butanoll butyl alcohol BRL 1-91 200
67-B4- Acetone BRL 1-91 400
71-43- Benzene BRL 1-91 20
75-27-4 Bromodichloromethane BRL 1-91 20
75-25- Bromoform BRL 1-91 20
74-83- Bromomethane BRL 1-91 40
78-93- Butanone (MEK) BRL 1-91 200
56-23- Carbon tetrachloride BRL 1-91 20
108-90- Chlorobenzene BRL 1-91 20
75-00- Chloroethane BRL 1-91 40
676- Chloroform BRL 1-91 20
74-87- Chloromethane BRL 1-91 40
124-48- Dibromochloromethane BRL 1-91 20
95-50- Dichlorobenzene BRL 1-911 20
541-73- Dichlorobenzene BRL 1-91 20
106-46- Dichlorobenzene BRL 1-91 20
75-34- 1- Dichloroethane BRL 1-91 20
107-06- Dichloroethane BRL 1-91 20
75-35-4 1- Dichloroethene BRL 1-91 20
156-59 cis- Dichloroethene BRL 1-91 20
156-60- trans- Dichloroethene BRL 1-91 20
78-87- 2- Dichloropropane BRL 1-91 20
10061-01-5 cis- Dichloropropene BRL 1-91 20
10061-02-B trans- Dichloropropene BRL 1-91 20
100-41-4 Ethylbenzene 411 1-911 20
591-78-B BRL 200Hexanone (MBK) 1-91
1634-04 -4 Methyl tert-butyl ether BRL 1-91 20
108-10- Methyl- pentanone (MIBK) BRL 1-91 200
75-09- Methylene chloride BRL 1-91 200
100-42- Styrene BRL 1-91 20
79-34- 1 Tetrachloroethane BRL 1-91 20
127- 18-4 T etrachloroethene BRL 1-91 20
108-88- Toluene BRL 1-91 20
71-55 1- Trichloroethane BRL 1-91 20
79-00- 2- Trichloroethane BRL 1-91 20
79-01-B Trichloroethene BRL 1-91 20
759-4 Trichlorofluoromethane (Freon 11) BRL 1-91 20
75-01-4 Vinyl chloride BRL 1-91 20
179601-23-1 m Xylene 390 1-91 40
95-47 Xylene 82 1-91 20
Surrogate recoveries 460-00- Bromofluorobenzene 70- 130
2037-26- Toluene- 100 70- 130
17060-07-0 1 Dichloroethane- 111 70- 130
1868-53- Dibromofluoromethane 70- 130
Microextractable Organic Compounds
106-93-4 1 Dibromoethane (EDB) BRL 1-91 0100 EPA 504 15-May- 15-May-08 8051105
Semivolatile Organic Compounds by GCMS
This laboratory report is not valid without all autllOrized signature 011 the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page 5 of 25
Sam le Identification Client Pro ect Matrix Collection DateTime Received
MWshy2920-96- Ground Water 13-May-081030 14-May-
SA 78602shy
CAS No Analyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Semivolatie Organic Compounds by GCMS
Semi volatile Or anic Com ounds b EPA 625
Prepared by method SW846 3510C 50 EPA 625 16-May- 19-May-08 805121683-32- Acenaphthene BRL IJgl
208-96-8 Acenaphthylene BRL IJgl 50
62-53- BRL IJgll 50Aniline
120- 12- Anthracene BRL 1J91 50
103-33- AzobenzenefDiphenyldiazine BRL IJgl 50
92-87 - Benzidine BRL IJgl 50
56-55- Benzo (a) anthracene BRL 1J91 50
50-32 - Benzo (a) pyrene IJglBRL 50
205-99- Benzo (b) fluoranthene BRL IJgl 50
191-24- Benzo (g i) perylene BRL IJgl 50
50207-08- Benzo (k) fluoranthene BRL IJgl
65-85 Benzoic acid BRL 1J91 50
100-51-6 Benzyl alcohol 1J91BRL 50
50111-91- Bis(2-chloroethoxy)methane BRL 1J91
111-4-4 Bis(2-chloroethyl)ether BRL IJgl 50
501 08-60- Bis(2-chloroisopropyl)ether BRL IJgl
117-81- Bis(2-ethylhexyl)phthalate BRL 1J91 50
101-55- Bromophenyl phenyl ether BRL IJgl 50
5085-68- Butyl benzyl phthalate BRL IJgl
5086-74- Carbazole BRL IJgl
5059-50- C hloro-3-methylphenol BRL IJgl
106-47- Chloroaniline BRL IJgl 50
91-58- Chloronaphthalene IJglBRL 50
5095-57 - Chlorophenol BRL 1J91
507005-72- Chlorophenyl phenyl ether BRL IJgl
216-01- Chrysene tJ91BRL 50
5053-70- Dibenzo (a h) anthracene BRL IJgl
50132-64- Dibenzofuran BRL IJgl
95-50- Dichlorobenzene IJglBRL 50
541-73- 13- Dichlorobenzene BRL IJgl 50
106-46- Dichlorobenzene 1J91BRL 50
5091-94- 3 - Dichlorobenzidine BRL IJgl
120-83- Dichlorophenol BRL IJgl 50
84-66- Diethyl phthalate BRL IJgl 50
131-11- Dimethyl phthalate BRL IJgll 50
105-67- Dimethylphenol BRL 1J91 50
5084-74- Di-n- butyl phthalate BRL 1J91
534-52 - Dinitro-2-methylphenol BRL IJgl 50
51-28- Dinitrophenol IJglBRL 50
50121-14- Dinitrotoluene BRL 1J91
606-20- Dinitrotoluene IJglBRL 50
50117-84-0 Di-n-octyl phthalate BRL IJgl
206-44-0 Fluoranthene 1J91BRL 50
BRL 50
50 86-73- Fluorene IJgi
118-74- Hexachlorobenzene BRL 1J91
87-68- Hexachlorobutadiene 1J91BRL 50
5077-47-4 Hexachlorocyclopentadiene BRL IJgl
67-72- Hexachloroethane IJglBRL 50
50193-39- Indeno (1 3-cd) pyrene BRL IJgl
5078-59- Isophorone BRL IJgl
Tfls laboratory report is not valid without all authorized signature 011 the coverpage
Page 6 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Sam le Identification Client Pro ect Matrix Collection DateTime ReceivedMWshy
2920-96- Ground Water I3-May-081030 14-May-SA 78602shy
CAS No Analyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Semivolatile Organic Compounds by GCMS
Semi volatile Or anic Com ounds b EPA 625
Prepared by method SW846 3510C
91-57 -6 Methylnaphthalene 367 1-91 50 EPA 625 16-May- 19-May-08 8051216
95-48- Methylphenol BRL 1-91 50
108-39-4 3 amp 4-Methylphenol BRL I-gl 100 106-44shy91-20- Naphthalene 247 1-91 50
88-74-4 Nitroaniline BRL 1-91 50
99-09- Nitroaniline BRL 1-91 50
100-01-6 Nitroaniline BRL 1-91 50
98-95- Nitrobenzene BRL 1-91 50
88-75- Nitrophenol BRL 1-91 50
100-02- Nitrophenol BRL 1-91 50
62-75- Nitrosodimethylamine BRL 1-91 50
621-64- N- Nitrosodi-n-propylamine BRL 1-91 50
86-30-6 Nitrosodiphenylamine BRL 1-91 50
87 -86- Pentachlorophenol BRL 1-91 50
85-0- Phenanthrene BRL 1-91 50
108-95- Phenol BRL 1-91 50
129-00-0 Pyrene BRL 1-91 50
110-86- Pyridine BRL 1-91 50
120-82- 4- Trichlorobenzene BRL 1-91 50
95-95- 5- Trichlorophenol BRL 1-91 50
88-06- 6- T richlorophenol BRL 1-91 50
Surrogate recoveries
321-60- Fluorobipheny 30- 130
367- 12- Fuorophenol 15- 110
4165-60- Nitrobenzene- 30- 130
4165-62- Pheno- 15- 110
1718-51- Terpheny-d4 30- 130
118- 79- 6- Tribromophenol 15- 110
Semivolatile Organic Compounds by GC
Pol chlorinated Bi hen ls b EPA 608
Prepared by method SW846 3510C
12674- 11-2 Aroclor- 1016 BRL 1-91 0650 EPA 608 15- May- 16-May-08 8051106
11104-28-2 Aroclor-1221 BRL IJgl 0650
11141-16-5 Aroclor- 1232 BRL 1-91 0650
53469-21-9 Aroclor- 1242 BRL 1-91 0650
12672-29-6 Aroclor- 1248 BRL 1-91 0650
11097-69-1 Aroclor- 1254 BRL 1-91 0650
11096-82-5 Aroclor -1260 BRL 1-91 0650
37324-23-5 Aroclor-1262 BRL 1-91 0650
11100-14-4 Aroclor-1268 BRL IJgl 0650
Surrogate recoveries
2051-24- Decachlorobipheny (Sr) 105 30- 150
10386-84-2 4 DB-Octafluorobiphenyl (Sr) 30- 150
Extractable Petroleum Hydrocarbons
mgl EPA 1664 Rev A 15-May- 19-May-08 8051102Non-polar material (SGT- HEM)
Soluble Metals by EPA 2006000 Series Metbods
Field Filtered NA EPA 200 73005A 15- May- 15-May-08 8051192Filtration
Soluble Metals by EPA 200 Series Methods
7440-22-4 Silver BRL mgl 0002 EPA 200 21-May- 27- May-08 8051249
This laboratory report is IlOt mlid without (II authorized signature on the cover page
Reportble Detection Limit BRL = Below Reporting Limit Page 7 of 25
Sam le Identification MW-
Client Pro ect 2920-96shy
Matrix Ground Water
Collection DateTime 13-May-08 1030
Received 14-May-
SA 78602shy
CAS No A nalyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Soluble Metals by EPA 200 Series Methods
7440-38shy Arsenic 0468 mg1 0040 EPA 200 21-Mayshy 21-May-08 80511 50
7440-43shy Cadmium BRL mg1 0002 EPA 200 21-May-088051249
7440-47shy Chromium BRL mg1 0050 EPA 200 21-May-088051150
7440-50-8 Copper BRL mg1 0050
7439-89-6 Iron 184 mg1 0150
7439-97-6 Mercury BRL mg1 00020 EPA 245 17470A 21-May-088051152
7440-02-0 Nickel BRL mg1 0050 EPA 200 21-May-088051150
7439-92shy Lead 0011 mg1 0002 EPA 200 21-May-088051249
7440-36-0 Antimony 0003 mg1 0002
7782-49shy Selenium BRL mg1 0150 EPA 200 21-May-08 8051150
7440-66-6 Zinc 0186 mgl 0050
General Chemistry Parameters
Filtration Completed NA Varies 14-Mayshy 14-May-08 8051095
18540-29-9 Hexavalent Chromium (soluble) BRL HT2 mg1 125 SM3500CrDI796A 14-Mayshy 14-May-08 8051094 R01 2013 2016
57-12shy Cyanide (total) BRL mg1 0100 EPA 3354 19-Mayshy 19-May-088051374
7782-50shy Total Residual Chlorine BRL CIHT mg1 500 Hach 8167 14-Mayshy 14-May-08 8051049 R01 1900 2001
Total Suspended Solids 580 mg1 25 SM2540D 16-Mayshy 16-May-08 8051275
This lahomtOlY report is not valid without an authorized signature on the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page 8 of 25
Volatie Organic Compounds - Quality Control
Analyte( s)
Batch 8051244 - SW846 5030 Water MS
Blank 8051244-BLK1
Prepared 16-May-08 Analyzed 17-May-
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromochloromethane
1 Dichlorobenzene
1 Dichlorobenzene
1 Dichlorobenzene
1-Dichloroethane
1 Dichloroethane
1 1-Dichloroethene
cis- Dichloroethene
trans- 1 Dichloroethene
1 Dichloropropane
cis- 1 Dichloropropene
trans- 1 Dichloropropene
Ethylbenzene
Hexanone (MBK)
Methyl tert-butyl ether
Methyl- pentanone (MIBK)
Methylene chloride
Styrene
2- Tetrachloroethane
Tetrachloroethene
Toluene
1- Trichloroethane
2- Trichloroethane
Trichloroethene
Trichlorofluoromethane (Freon 11)
Vinyl chloride
p-Xylene
Xylene
Surrogate 4-Bromofluorobenzene Surrogate Toluene-
Surrogate 1 Dichloroethane-Surrogate Dibromofluoromethane
LCS B051244-BS1
Prepared 16-May-08 Analyzed 17 -May-
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Spike Source REC RPD
Result Flag Units RDL Level Result REC Limits RPD Limit
BRL gl 20
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl 10
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gll
BRL gi
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl 10
BRL gll
BRL gll 10
BRL gl 10
BRL gll
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
41 gl 50 70- 130 49 gl 50 70- 130 59 gl 50 119 70- 130 52 gl 50 105 70- 130
QC2 jgl 20 70- 130
18 jgl 20 70- 130
192 jgl 20 35- 155
18 jgl 20 45- 169
19 jgl 20 242
This laboratOlY repol1 is lot valid without 011 authorized sigllature 011 the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page 9 of 25
Volatie Organic Compounds - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051244 - SW846 5030 Water MS
LC5 8051244B51
Prepared 16-May-08 Analyzed 17-May-
Butanone (MEK) 10 QC2 gl 20 70- 130
Carbon tetrachloride 204 gl 20 102 70- 140
Chlorobenzene 18 gl 20 70- 130
Chloroethane 164 gl 20 14-230
Chloroform 18 gll 20 51- 138
Chloromethane 21 gl 20 106 273
Dibromochloromethane 18 gl 20 53- 149
1 Dichlorobenzene 20 gl 20 104 18- 190
1 Dichlorobenzene 19 gl 20 59- 156
1 A-Dichlorobenzene 18 gl 20 18- 190
1- Dichloroethane 19 gl 20 59- 155
1 Dichloroethane 19 gl 20 49- 155
1-Dichloroethene 16 gl 20 70- 130
cis- 1 Dichloroethene 17 gl 20 70- 130
trans- 1 Dichloroethene 16 gll 20 54- 156
1 Dichloropropane 18 gl 20 210
cis- Dichloropropene 17 gl 20 227
trans- 1 Dichloropropene 17 gl 20 17- 183
Ethylbenzene 19 gl 20 37- 162
Hexanone (MBK) 124 QC2 gl 20 70- 130
Methyl tert-butyl ether 19 gl 20 70- 130
Methylshy pentanone (MIBK) 17 gl 20 70- 130
Methylene chloride 16 gl 20 221
Styrene 17 gl 20 70- 130
1 Tetrachloroethane 194 gl 20 46- 157
Tetrachloroethene 15 gl 20 64- 148
Toluene 18 gl 20 70- 130
1- Trichloroethane 20 gl 20 100 52- 162
2- Trichloroethane 18 gl 20 52- 150
Trichloroethene 17 gl 20 71- 157
Trichlorofluoromethane (Freon 11) 19 gl 20 17- 181
Vinyl chloride 21 gl 20 106 251
p-Xylene 39 gl 40 70- 130
Xylene 20 gl 20 102 70- 130
Surrogate 4-Bromofluorobenzene Surrogate Toluene-
Surrogate 1 Dichloroethane-Surrogate Dibromofluoromethane
52 49 56
49
gl
gl
gl
gl
50 50 50
50
105
112 100
70- 130 70- 130 70- 130 70- 130
LC5 DUD (8051244-B5D1
Prepared 16-May-08 Analyzed 17-May-
Acetone QC2 gl 20 70- 130
Benzene 18 gl 20 70- 130
Bromodichloromethane 18 gl 200 35- 155
Bromoform 17 gl 20 45- 169
Bromomethane 18 gl 20 242
Butanone (MEK) 11 QC2 1-91 20 70- 130
Carbon tetrachloride 20 gl 20 100 70- 140
Chlorobenzene 17 gl 20 70- 130
Chloroethane 15 1-91 20 14-230
Chloroform 18 1-91 20 51- 138
This laboratory report is aot valid without a1 authorized sig1ature 01 the cover page
Reportble Detection Limit BRL = Below Reporting Limit Page 10 of25
Volatie Organic Compounds - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051244 - SW846 5030 Water MS
LCS Dup 18051244-BSD1
Prepared 16-May-08 Analyzed 17-May-
Chloromethane 18 1-91 20 273
Dibromochloromethane 174 1-91 20 53- 149
Dichlorobenzene 20 1-91 20 100 18- 190
Dichlorobenzene 18 1-91 20 59- 156
Dichlorobenzene 18 1-91 20 18- 190
Dichloroethane 18 1-91 20 59- 155
Dichloroethane 19 1-91 20 49- 155
Dichloroethene 16 1-91 20 70- 130
cis- Dichloroethene 16 1-91 20 70- 130
trans- Dichloroethene 15 1-91 20 54- 156
Dichloropropane 17 1-91 20 210
cis- Dichloropropene 164 IJgl 20 227
trans- 1 Dichloropropene 164 I-gl 20 17- 183
Etlwlbenzene 18 IJgl 20 37- 162
Hexanone (MBK) 124 QC2 IJgl 20 70- 130
Methyl tert-butyl ether 184 1J91 20 70- 130
Methyl- pentanone (MIBK) 17 IJgl 20 70- 130
Methylene chloride 16 IJgl 20 221
Styrene 16 IJgl 20 70- 130
2- Tetrachloroethane 19 IJgl 20 46- 157
Tetrachloroethene 15 IJgl 20 64- 148
Toluene 17 IJgl 20 70- 130
1- Trichloroethane 19 1-91 20 52- 162
2- Trichloroethane 16 IJgl 20 52- 150
Trichloroethene 15 IJgl 20 71- 157
Trichlorofluoromethane (Freon 11) 17 IJgl 20 17- 181
Vinyl chloride 19 IJglI 20 251
p-Xylene 37 1J91 40 70- 130
Xylene 20 IJgl 20 100 70- 130
Surrogate 4-Bromofluorobenzene 51 IJgl 50 104 70- 130
Surrogate Toluene- 4B gl 50 70- 130
Surrogate 1 0ichloroethane- 53 IJgl 50 106 70- 130 Surrogate Oibromofluoromethane 50 1J9i 50 102 70- 130
Matrix S ike B051244-MS1 Source SA7B629shy
Prepared 16-May-08 Analyzed 17-May-
Benzene 18 20 BRL 70- 130IJgl
Bromodichloromethane 19 IJgl 20 BRL 35- 155
Bromoform 18 IJgl 20 BRL 45- 169
Bromomethane 16 IJgl 20 BRL 242
Carbon tetrachloride 21 IJgl 20 BRL 106 70- 140
Chlorobenzene 18 IJgl 20 BRL 70- 130
Chloroethane 16 IJgl 20 BRL 14-230
Chloroform 18 IJgl 20 BRL 51- 138
Chloromethane 19 IJgl 20 BRL 273
Dibromochloromethane 17 IJgl 20 BRL 53- 149
1 Dichlorobenzene 22 IJgl 20 BRL 112 18- 190
1 Dichlorobenzene 22 IJgl 20 BRL 110 59-156
1 Dichlorobenzene 21 IJgl 20 BRL 109 18- 190
1- Dichloroethane 19 IJgl 20 BRL 59- 155
1 Dichloroethane 18 IJgl 20 BRL 49- 155
This laboratory report is 110t mUd without an authorized signature on the covel page
Reportble Detection Limit BRL = Below Reporting Limit Page It of25
Volatile Organic Compounds - Quality Control
p
Spike Source REC RPD
Result REC imits RPD LimitAnalyte(s) Result Flag Units RDL Level
Batch 8051244 - SW846 5030 Water MS
Matrix ike S051244-MS1 Source SA7B629shy
Prepared 16-May-08 Analyzed 17-Mayshy
17 20 BRL 70- 130 1- Dichloroethene IJgl
16 20 BRL 54- 156trans- 1 Dichloroethene IJgl
21020 BRL1 Dichloropropane 17 1J91
cis- 1 Dichloropropene 17 IJgl 20 BRL 227
17- 183trans- 1 Dichloropropene 184 1J91 20 BRL
20 20 BRL 103 37- 162Ethylbenzene IJgl
15 20 BRL 221Methylene chloride IJgl
20 BRL 46- 1572- Tetrachloroethane 19 1J91
20 BRL 64- 148Tetrachloroethene 18 1J91
BRL 70- 130Toluene 18 1J91 20
105 52-1621- Trichloroethane 211 IJgl 20 BRL
18 20 BRL 52- 1502- Trichloroethane IJgl
17 20 BRL 71- 157Trichloroethene 1J91
20 BRL 17- 181Trichloroluoromethane (Freon 11) 194 IJgl
20 BRL 103 251Vinyl chloride 20 IJgl
102 70- 130Surrogate 4-Bromofluorobenzene 50 IJgl 50 50 70- 130Surrogate Toluene- 49 1J91
56 50 112 70- 130Surrogate 1 Dichloroethane- IJgl
50 100 70- 130Surrogate Dibromofluoromethane 50 IJgl
Matrix S ike Du S051244-MSD1 Source SA7S629shy
Prepared 16-May-08 Analyzed 17-Mayshy
18 20 BRL 70- 130Benzene IJgl
18 20 BRL 35- 155Bromodichloromethane IJgl
17 20 BRL 45- 169Bromoform IJgl
20 BRL 242Bromomethane 17 IJgl
20 BRL 103 70- 140Carbon tetrachloride 20 IJgl
18 20 BRL 70- 130Chlorobenzene 1J91
14-230Chloroethane 16 IJgl 20 BRL
20 51- 138Chloroform 184 IJgl BRL
Chloromethane 19 1J91 20 BRL 273
18 20 BRL 53- 149Dibromochloromethane 1J91
20 BRL 117 18- 190Dichlorobenzene 234 IJgl
20 BRL 112 59- 156Dichlorobenzene 22 IJgl
BRL 108 18- 190Dichlorobenzene 21 1J91 20
20 59- 1551 Dichloroethane 19 IJgl BRL
18 20 BRL 49- 155Dichloroethane IJgl
16 20 BRL 70- 130Dichloroethene IJgl
20 BRL 54- 156trans- Dichloroethene 154 1J91
20 BRL 210Dichloropropane 17 IJgl
0420 BRL 227cis- Dichloropropene 17 IJgl
17- 183trans- Dichloropropene 17 1J91 20 BRL
BRL 37- 162Ethylbenzene 20 1J91 20 102
Methylene chloride 15 IJgl 20 BRL 221
20 BRL 46- 1572- Tetrachloroethane 192 IJgl
20 BRL 64- 148 04Tetrachloroethene 18 IJgl
BRL 70- 130Toluene 184 1J91 20
52- 1621- Trichloroethane 20 IJgl 20 BRL 104
17 20 BRL 52- 1502- Trichloroethane IJgl
17 20 BRL 71- 157Trichloroethene IJgl
20 BRL 17-181Trichlorofluoromethane (Freon 11) 19 IJgl
This laboratory report is IIOt valid without all authorized sigllllture 011 the cover page
Page 12 of25 Reportble Detection Limit BRL = Below Reporting Limit
Semivolatile Organic Compounds by GCMS - Quality Control
Analyte(s)
Batch 8051216 - SW846 3510C
Blank 8051216-BLK1
Prepared amp Analyzed 16-May-
Isophorone
Methylnaphthalene
Methylphenol
3 amp 4-Methylphenol
Naphthalene
Nitroaniline
Nitroaniline
Nitroaniline
Nitrobenzene
Nitrophenol
Nitrophenol
Nitrosodimethylamine
N- N itrosodi-n-pro pyla mine
N itrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Pyridine
1 24-Trichlorobenzene
24 5- Trichlorophenol
246- Trichlorophenol
Surrogate 2-Fuorobipheny Surrogate 2-Fuoropheno Surrogate Nitrobenzene-Surrogate PhenoshySurrogate Terpheny-d4 Surrogate 6- Tribromopheno
LCS B051216-BS1
Prepared amp Analyzed 16-May-
Acenaphthene
Acenaphthylene
Aniline
Anthracene
AzobenzenelDi phenyld lazine
Benzidine
Benzo (a) anthracene
Benzo (a) pyrene
Benzo (b) fluoranthene
Benzo (g i) perylene
Benzo (k) fluoranthene
Benzoic acid
Benzyl alcohol
B is(2-chloroethoxy)methane
B i s (2-ch loroethyl)eth e r
Bis(2-ch loroisopropyl) ether
B is(2-ethy Ih exyl) phtha late
Bromophenyl phenyl ether
Butyl benzyl phthalate
Carbazole
Spike Source REC RPD
Result Flag Units RDL Level Result REC Limits RPD Limit
BRL gl
BRL gl
BRL gl
BRL gl 10
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gll
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
370 gl 50 30- 130 40 gl 50 15- 110 39 gl 50 30- 130 43 gl 50 15- 110 36 gl 50 30- 130 40 gl 50 15- 110
41 gl 50 40- 140
43 gI 50 40- 140
41 gl 50 40- 140
38 gl 50 40- 140
45 gl 50 40- 140
49 gl 50 153
41 gl 50 40- 140
43 gl 50 40- 140
41 gl 50 40- 140
41 gll 50 40- 140
45 gl 50 40- 140
32 gl 50 12- 149
41 gl 50 40- 140
39 gl 50 40- 140
384 gl 50 40- 140
47 gl 50 40- 140
47 gl 50 40- 140
40 gl 50 40- 140
47 gI 50 40- 140
56 gI 50 112 200
This laboratory report is lIot valid witllOut a1l authorized sigllature 011 the coverpage
Reportble Detection Limit BRL = Below Reporting Limit Page 15 of25
Semivolatile Organic Compounds by GCMS - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051216 - SW846 3510C
LCS 8051216-BS1
Prepared amp Analyzed 16-Mayshy
50 30- 1304 -C hloro-3-methylphenol 42 IJgl
40- 140Chloroaniline 39 IJgl 50
Chloronaphthalene 37 IJgl 50 40- 140
Chlorophenol 37 IJgl 50 30- 130
50 40- 140
40- 140
Chlorophenyl phenyl ether 45 IJgl
Chrysene 43 IJgl 50
Dibenzo (a h) anthracene 43 IJgl 50 40- 140
Dibenzofuran IJgl38 50 40- 140
50 40- 1401 Dichlorobenzene 35 IJgl
40- 1401 Dichlorobenzene 264 IJgl 50
40- 1401 Dichlorobenzene 434 IJgl 50
58 50 116 40- 1403 - Dichlorobenzidine IJgl
50 30- 130
40- 140 24-Dichlorophenol 38 IJgl
Diethyl phthalate 484 IJgl 50
50 40- 140Dimethyl phthalate 464 IJgl
Dlmethylphenol 39 IJgl 50 30- 130
DI-n-butyl phthalate 44 IJgll 50 40- 140
30- 130 6-Di nitro- 2-methylphenol 38 1J91 50
30- 130Dinltrophenol 36 1J91 50
42 50 40- 14024-Dlnitrotoluene 1J91
Dlnitrotoluene 1J9141 50 40- 140
Di-n-octyl phthalate 52 IJgl 50 104 40- 140
40- 140Fluoranthene 40 IJgl 50
Fluorene 41 IJgl 50 40- 140
39 50 40- 140Hexachlorobenzene IJgl
50 40- 140Hexachlorobutadiene 40 IJgl
40- 140Hexach lorocyclopentad iene 294 IJgl 50
40 50 40- 140Hexachloroethane IJgl
42 50 40-140Indeno (1 3-cd) pyrene IJgl
50 40- 140Isophorone 40 IJgl
40- 140Methylnaphthalene 394 IJgl 50
40- 140Methylphenol 39 IJgl 50
40 10 50 40- 1403 amp 4-Methylphenol IJgl
37 50 40-140Naphthalene IJgl
50 40-140Nitroaniline 39 IJgl
Nitroaniline 51 IJgl 50 102 40- 140
48 50 40- 140Nltroaniline 1J91
50 40- 140Nitrobenzene 40 IJgl
30- 130Nitrophenol 36 IJgl 50
40 IJgl 50 30- 130Nitrophenol 40- 140Nitrosodimethylamine 32 1J91 50
50 40-140N- N itrosodi-n-propyla mine 46 IJgl
40- 140N itrosodi phenyla ml ne 44 IJgl 50
41 IJgl 50 30- 130Pentachlorophenol 40- 140Phenanthrene 38 IJgl 50
50 30- 130Phenol 38 IJgl
40- 140Pyrene 424 1J91 50
40- 140Pyridine 294 1J91 50
40- 14024- Trichlorobenzene 364 IJgl 50
This laboratory report is not mlid without an authorized signature 011 the cover page
Page 16 of25 Reportble Detection Limit BRL = Below Reporting Limit
Semivolatie Organic Compounds by GCMS - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
BMch 8051216 - SW846 3510C
LC5 8051216-851
Prepared amp Analyzed 16-Mayshy
24 5- Trichlorophenol 404 gl 50 30- 130
246- Trichlorophenol 42 gl 50 30- 130
Surrogate 2-Fluorobiphenyl 29 gl 50 30- 130
Surrogate 2-Fluorophenot 27 gl 50 15- 110
Surrogate Nitrobenzene- 30 gl 50 30- 130
Surrogate Phenol- 29 gl 50 15- 110
Surrogate Terpheny-d4 30 gl 50 30- 130
Surrogate 6- Tribromopheno 324 gl 50 15- 110
This laboratory report is lIot valid without all authorized sigllature 011 tlle cover page
Reportble Detection Limit BRL = Below Reporting Limit Page 17 of25
Semivolatie Organic Compounds by GC - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051106 - SW846 3510C
Blank S051106-BLK1
Prepared amp Analyzed 15-Mayshy
Aroclor- 1016 BRL gI 0200
Aroclor- 1016 (2C) BRL gI 0200
Aroclor- 1221 BRL gI 0200
Aroclor- 1221 (2C) BRL gI 0200
Aroclor- 1232 BRL gI 0200
Aroclor- 1232 (2Cj BRL gI 0200
Aroclor- 1242 BRL gI 0200
Aroclor-1242 (2C) BRL gI 0200
Aroclor- 1248 BRL gI 0200
Aroclor- 1248 (2C) BRL gI 0200
Aroclor- 1254 BRL gI 0200
Aroclor- 1254(2Cj BRL gI 0200
Aroclor- 1260 BRL gI 0200
Aroclor- 1260 (2C) BRL gI 0200
Aroclor- 1262 BRL gI 0200
Aroclor- 1262 (2C) BRL gI 0200
Aroclor-1268 BRL gI 0200
Aroclor- 1268 (2C) BRL gI 0200
Surrogate Decachlorobiphenyl (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0231 0224 0194 0191
gI
gI
gI
gI
0200 0200 0200 0200
116 112
30- 150 30- 150 30- 150 30- 150
LC5 8051106-B51
Prepared 15-May-08 Analyzed 16-May-08
Aroclor- 1016 265 gI 0200 250 106 50- 114
Aroclor- 1 016 (2C) 240 gI 0200 250 50- 114
Aroclor- 1260 0269 gI 0200 250 107 40- 127
Aroclor-1260 (2Cj 270 gI 0200 250 108 40- 127
Surrogate Decachlorobiphenyl (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0225 0224 0188 0183
gI
gI
gI
gI
0200 0200 0200 0200
113 112
30- 150 30- 150 30- 150 30- 150
LC5 DUD rS051106-B5D1
Prepared 15-May-08 Analyzed 16-Mayshy
Aroclor- 1016 262 gl 0200 250 105 50- 114
Aroclor-1 016 (2Cj 241 gI 0200 250 50- 114
Aroclor- 1260 277 gI 0200 250 111 40- 127
Aroclor- 1260(2Cj 0260 gI 0200 250 104 40- 127
Surrogate Decachlorobipheny (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0238 0218 0189 0181
gI
gI
gI
gI
0200 0200 0200 0200
119 109
30- 150 30- 150 30- 150 30- 150
This laboratory report is lot valid without (II authorized sigllature 01 the cover page
Page 18 of25 Reportable Detection Limit BRL = Below Reporting Limit
Extractable Petroleum Hydrocarbons - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051102 - SW846 3510C
Blank 8051102-BLK1
Prepared 15-May-08 Analyzed 19-Mayshy
Non-polar material (SGT- HEM) BRL m91
LC8 8051102-B81
Prepared 15-May-08 Analyzed 19-Mayshy
Non-polar material (SGT- HEM) 184 m91 21 81 904
This laboratory report is not valid without an authorized signature 011 the cover page
Page 19 of25 Reportable Detection Limit BRL = Below Reporting Limit
Soluble Metals by EPA 200 Series Methods - Quality Control
Analyte(s) Result Flag Units RDL
Spike
Level
Source
Result REC
REC
Limits RPD
RPD
Limit
Batch 8051150 - EPA 200 Series
Blank 8051150-BLK1
Prepared amp Analyzed 21-May-
Iron
Zinc
Selenium
Nickel
Chromium
Copper
Arsenic
BRL
BRL
BRL
BRL
BRL
BRL
BRL
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0150
0050
0150
0050
0050
0050
0040
LCS 8051150-BS1
Prepared amp Analyzed 21-May-
Selenium
Zinc
Iron
Nickel
Chromium
Arsenic
Copper
123
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0150
0050
0150
0050
0050
0040
0050
103
105
101
100
85- 115
85- 115
85- 115
85- 115
85- 115
85-115
85- 115
licate B051150-DUP1 Source SA7B602shy
Prepared amp Analyzed 21-May-
Iron
Zinc
Selenium
Nickel
Copper
Chromium
Arsenic
17
0162
BRL
0015
0017
BRL
0450
QR8
mgl
mgl
mgl
mgl
mgl
mgl
mgi
0150
0050
0150
0050
0050
0050
0040
184
0186
BRL
0014
0023
BRL
0468
Matrix S ike 8051150-MS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Iron
Selenium
Nickel
Zinc
Copper
Chromium
Arsenic
19 QM2 mgl
mgll
mgl
mgl
mgl
mgl
mgl
0150
0150
0050
0050
0050
0050
0040
125
184
BRL
0014
0186
0023
BRL
0468
104
105
102
70- 130
70- 130
70-130
70- 130
70- 130
70-130
70- 130
Post S ike 8051150-PS1 Source SA78602shy
Prepared amp Analyzed 21-May-
Zinc
Iron
Selenium
Nickel
Copper
Arsenic
Chromium
18 QM2
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0050
0150
0150
0050
0050
0040
0050
0186
184
BRL
0014
0023
0468
BRL
104
104
101
85- 115
85- 115
85- 115
85-115
85-115
85- 115
85-115
Batch 8051152 - EPA200SW7000 Series
Blank B051152-BLK1
Prepared amp Analyzed 21-May-
Mercury BRL mgl 00020
This laboratory report is IIOt valid witllOut all authorized sigllature 011 the coverpage
Page 20 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Soluble Metals by EPA 200 Series Methods - Quality Control
Analyte(s) Result Flag Units RDL
Spike
Level
Source
Result REC
REC
Limits RPD
RPD
Limit
Batch 8051152 - EPA200SW7000 Series
LCS B051152-BS1
Prepared amp Analyzed 21-May-
Mercury 00576 m91 00020 00500 115 85- 115
licate B051152-DUP1 Source SA78602-01
Prepared amp Analyzed 21-May-
Mercury BRL m91 00020 BRL
Matrix S ike 8051152-MS1 Source SA78602shy
Prepared amp Analyzed 21-May-
Mercury 00632 OM m91 00020 00500 BRL 126 75- 125
Post S ike 8051152-PS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Mercury 00624 OC1 m91 00020 00500 BRL 125 85- 115
Batch 8051249 - 2008No digestion
Blank 8051249-BLK1
Prepared amp Analyzed 21-May-
Lead
Antimony
Cadmium
Silver
BRL
BRL
BRL
BRL
m91
m91
m91
m91
0002
0002
0002
0002
LCS B051249-BS1
Prepared amp Analyzed 21-May-
Antimony
Lead
Silver
Cadmium
143
145 OC2
m91
m91
m91
m91
0050
0050
0050
0040
103
115
107
116
85- 115
85- 115
85- 115
85- 115
licate 8051249-DUP1 Source SA7B602shy
Prepared amp Analyzed 21- May-
Lead
Antimony
Cadmium
Silver
0009
0002
00005
00002
ORB
m91
m91
m91
m91
0002
0002
0002
0002
0011
0003
00005
00003
Matrix S ike 8051249-MS1 Source SA78602shy
Prepared amp Analyzed 21- May-
Lead
Antimony
Cadmium
Silver
142
m91
m91
m91
m91
0050
0050
0040
0050
0011
0003
00005
00003
111
101
114
102
70- 130
70-130
70c130
70- 130
Post S ike 8051249-PS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Antimony
Cadmium
Silver
38
OC2
m91
m91
m91
0050
0040
0050
125
0003
00005
00003
110
121
109
85- 115
85- 115
85- 115
This laboratory report is flOt valid IVithout all authorized signature 011 the cOIer page
Reportable Detection Limit BRL Below Reporting Limit Page 21 of 25
General Chemistry Parameters - Quality Control
Spike Source REC RPD
Analyte( s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051049 - General Preparation
Blank S051 049-BLK1
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
Blank S051049-BLK2
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
Blank S051 049-BLK3
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
LCS S051049-BS1
Prepared amp Analyzed 14-May-
Total Residual Chlorine 046 mgl 020 0500 90- 110
LCS S051049-BS2
Prepared amp Analyzed 14-May-
Total Residual Chlorine 047 mgl 020 0500 90- 110
LCS S051049-BS3
Prepared amp Analyzed 14-May-
Total Residual Chlorine 054 mgl 020 0500 108 90-110
licate B051049-DUP1 Source SA7S544shy
Prepared amp Analyzed 14-May-
Total Residual Chlorine 012 mgl 020 010
licate S051049-DUP2 Source SA7S602-01
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020 BRL
Matrix S ike 8051049-MS1 Source SA78544-01
Prepared amp Analyzed 14-May-
Total Residual Chlorine 065 mgl 020 0500 010 110 80- 120
Matrix S ike 8051049-MS2 Source SA7B602shy
Prepared amp Analyzed 14-May-
Total Residual Chlorine mgl 500 125 BRL 108 80- 120
Reference 8051 049-SRM1
Prepared amp Analyzed 14-May-
Total Residual Chlorine 100 mgl 020 0967 103 85-115
Batch 8051094 - General Preparation
Blank 8051094-BLK1
Prepared amp Analyzed 14 May-
Hexavalent Chromium (soluble) BRL mgl 005
Blank 8051 094-BLK2
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) BRL mgl 005
LCS 8051094-BS1
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) 054 mgl 005 90- 110
licate 8051094-DUP1 Source SA78602-01
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) BRL mgl 125 BRL
Thi laboratory report is not valid without all authorized sigllature 011 the cover page
Page 22 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Page 16
Dilution Factor Calculation Former Speedway Service Station 181 East Broadway Gardner Ma
DF=(Od+Os)Od
DF = Dilution factor
Od = Max flow rate of discharge in cubic feet per second Os = receiving water flow in cubic feet per seconds 7010 flow rate Mahoney Brook 7010 = min flow for seven consecutive days with a recurrence interval of 10 years
7010 flow based on data obtained from USGS Steamflow Statistics Report Data attached
067
Semivolatile Organic Compounds by GCMS - Quality Control
Analyte( s)
Batch 8051216 - SW846 3510C
Blank 8051216BLK1)
Prepared amp Analyzed 16May-
Acenaphthene
Acenaphthylene
Aniline
Anthracene
AzobenzenelDi phenyld iazi ne
Benzidine
Benzo (a) anthracene
Benzo (a) pyrene
Benzo (b) fiuoranthene
Benzo (g i) perylene
Benzo (k) fiuoranthene
Benzoic acid
Benzyl alcohol
Bis(2-ch loroethoxy) methane
Bis(2-ch loroethyl)ether
Bis(2-ch loroi sopropyl)ether
Bis(2ethylhexyl) phthalate
Bromophenyl phenyl ether
Butyl benzyl phthalate
Carbazole
Ch loro-3-methyl phenol
Chloroaniline
Chloronaphthalene
Chlorophenol
Chlorophenyl phenyl ether
Chrysene
Dibenzo (a h) anthracene
Dibenzofuran
Dichlorobenzene
Dichlorobenzene
14- Dichlorobenzene
3 - Dichlorobenzidine
24-Dichlorophenol
Diethyl phthalate
Dimethyl phthalate
24- Dimethylphenol
Din-butyl phthalate
Dinitro-2-methylphenol
Dinitrophenol
Dinitrotoluene
Dinitrotoluene
Di-noctyl phthalate
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopehtadiene
Hexachloroethane
Indeno (1 cd) pyrene
Spike Source REC RPD
Result Flag Units RDL Level Result REC Limits RPD Limit
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gl
BRL gI
BRL gl
BRL gl
BRL gl
BRL gI
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gll
BRL gl
BRL gll
BRL gl
BRL gl
BRL gI
BRL gI
BRL gI
BRL gl
BRL gI
BRL gI
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gI
BRL gI
BRL gl
This laboratory report is IlOt valid without all authorized sigllature 011 the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page t4 of25
Volatie Organic Compounds - Quality Control
p (
Spike Source REC RPD
RDL Level Result REC Limits RPD Limit Analyte(s) Result Flag Units
Batch 8051244 - SW846 5030 Water MS
Matrix S ike Du 8051244-MSD1 Source SA78629shy
Prepared 16-May-08 Analyzed 17-May-BRL 106 251
Vinyl chloride 21 gl 20
101 70- 130 Surrogate 4-Bromofluorobenzene 50 gl 50
70- 13049 gl 50 111 70- 130
Surrogate Toluene-Surrogate 1 Dichloroethane- 55 gl 50
50 70- 130494 glSurrogate Dibromofluoromethane
Microextractable Organic Compounds - Quality Control
Spike Source REC RPD
Flag Units RDL Level Result REC Limits RPD Limit Analyte(s) Result
Batch 8051105 - SW846 3510C
Blank 8051105-BLK
Prepared amp Analyzed 15-May-
BRL gl 01001 Dibromoethane (ED B)
LCS 8051105-BS1
Prepared amp Analyzed 15-Mayshy50- 1500770 gl 0100 100
licate 8051105-DUP1 Source SA7B583shy
Prepared amp Analyzed 15-May-
BRL gl 0100 BRL
1 Dibromoethane (EDB)
1 Dibromoethane (EDB)
This laborntOlY report is not valid without an authorized signature 011 the cover page
Page 13 of2S Reportable Detection Limit BRL = Below Reporting Limit
Sam le Identification Client Pro ect Matrix Collection DateTime ReceivedMWshy
2920-96- Ground Water 13-May-081030 14-May-SA 78602shy
CAS No Analyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Volatile Organic Compounds
Volatile Or anic Com ounds b GCMS
Prepared by method SW846 5030 Water MS
123-91- Dioxane BRL 1-91 200 EPA 624 16-May-08 17-May-08 8051244
994-05-8 Ter-amyl methyl ether BRL 1-911 20
755- Tert-Butanoll butyl alcohol BRL 1-91 200
67-B4- Acetone BRL 1-91 400
71-43- Benzene BRL 1-91 20
75-27-4 Bromodichloromethane BRL 1-91 20
75-25- Bromoform BRL 1-91 20
74-83- Bromomethane BRL 1-91 40
78-93- Butanone (MEK) BRL 1-91 200
56-23- Carbon tetrachloride BRL 1-91 20
108-90- Chlorobenzene BRL 1-91 20
75-00- Chloroethane BRL 1-91 40
676- Chloroform BRL 1-91 20
74-87- Chloromethane BRL 1-91 40
124-48- Dibromochloromethane BRL 1-91 20
95-50- Dichlorobenzene BRL 1-911 20
541-73- Dichlorobenzene BRL 1-91 20
106-46- Dichlorobenzene BRL 1-91 20
75-34- 1- Dichloroethane BRL 1-91 20
107-06- Dichloroethane BRL 1-91 20
75-35-4 1- Dichloroethene BRL 1-91 20
156-59 cis- Dichloroethene BRL 1-91 20
156-60- trans- Dichloroethene BRL 1-91 20
78-87- 2- Dichloropropane BRL 1-91 20
10061-01-5 cis- Dichloropropene BRL 1-91 20
10061-02-B trans- Dichloropropene BRL 1-91 20
100-41-4 Ethylbenzene 411 1-911 20
591-78-B BRL 200Hexanone (MBK) 1-91
1634-04 -4 Methyl tert-butyl ether BRL 1-91 20
108-10- Methyl- pentanone (MIBK) BRL 1-91 200
75-09- Methylene chloride BRL 1-91 200
100-42- Styrene BRL 1-91 20
79-34- 1 Tetrachloroethane BRL 1-91 20
127- 18-4 T etrachloroethene BRL 1-91 20
108-88- Toluene BRL 1-91 20
71-55 1- Trichloroethane BRL 1-91 20
79-00- 2- Trichloroethane BRL 1-91 20
79-01-B Trichloroethene BRL 1-91 20
759-4 Trichlorofluoromethane (Freon 11) BRL 1-91 20
75-01-4 Vinyl chloride BRL 1-91 20
179601-23-1 m Xylene 390 1-91 40
95-47 Xylene 82 1-91 20
Surrogate recoveries 460-00- Bromofluorobenzene 70- 130
2037-26- Toluene- 100 70- 130
17060-07-0 1 Dichloroethane- 111 70- 130
1868-53- Dibromofluoromethane 70- 130
Microextractable Organic Compounds
106-93-4 1 Dibromoethane (EDB) BRL 1-91 0100 EPA 504 15-May- 15-May-08 8051105
Semivolatile Organic Compounds by GCMS
This laboratory report is not valid without all autllOrized signature 011 the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page 5 of 25
Sam le Identification Client Pro ect Matrix Collection DateTime Received
MWshy2920-96- Ground Water 13-May-081030 14-May-
SA 78602shy
CAS No Analyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Semivolatie Organic Compounds by GCMS
Semi volatile Or anic Com ounds b EPA 625
Prepared by method SW846 3510C 50 EPA 625 16-May- 19-May-08 805121683-32- Acenaphthene BRL IJgl
208-96-8 Acenaphthylene BRL IJgl 50
62-53- BRL IJgll 50Aniline
120- 12- Anthracene BRL 1J91 50
103-33- AzobenzenefDiphenyldiazine BRL IJgl 50
92-87 - Benzidine BRL IJgl 50
56-55- Benzo (a) anthracene BRL 1J91 50
50-32 - Benzo (a) pyrene IJglBRL 50
205-99- Benzo (b) fluoranthene BRL IJgl 50
191-24- Benzo (g i) perylene BRL IJgl 50
50207-08- Benzo (k) fluoranthene BRL IJgl
65-85 Benzoic acid BRL 1J91 50
100-51-6 Benzyl alcohol 1J91BRL 50
50111-91- Bis(2-chloroethoxy)methane BRL 1J91
111-4-4 Bis(2-chloroethyl)ether BRL IJgl 50
501 08-60- Bis(2-chloroisopropyl)ether BRL IJgl
117-81- Bis(2-ethylhexyl)phthalate BRL 1J91 50
101-55- Bromophenyl phenyl ether BRL IJgl 50
5085-68- Butyl benzyl phthalate BRL IJgl
5086-74- Carbazole BRL IJgl
5059-50- C hloro-3-methylphenol BRL IJgl
106-47- Chloroaniline BRL IJgl 50
91-58- Chloronaphthalene IJglBRL 50
5095-57 - Chlorophenol BRL 1J91
507005-72- Chlorophenyl phenyl ether BRL IJgl
216-01- Chrysene tJ91BRL 50
5053-70- Dibenzo (a h) anthracene BRL IJgl
50132-64- Dibenzofuran BRL IJgl
95-50- Dichlorobenzene IJglBRL 50
541-73- 13- Dichlorobenzene BRL IJgl 50
106-46- Dichlorobenzene 1J91BRL 50
5091-94- 3 - Dichlorobenzidine BRL IJgl
120-83- Dichlorophenol BRL IJgl 50
84-66- Diethyl phthalate BRL IJgl 50
131-11- Dimethyl phthalate BRL IJgll 50
105-67- Dimethylphenol BRL 1J91 50
5084-74- Di-n- butyl phthalate BRL 1J91
534-52 - Dinitro-2-methylphenol BRL IJgl 50
51-28- Dinitrophenol IJglBRL 50
50121-14- Dinitrotoluene BRL 1J91
606-20- Dinitrotoluene IJglBRL 50
50117-84-0 Di-n-octyl phthalate BRL IJgl
206-44-0 Fluoranthene 1J91BRL 50
BRL 50
50 86-73- Fluorene IJgi
118-74- Hexachlorobenzene BRL 1J91
87-68- Hexachlorobutadiene 1J91BRL 50
5077-47-4 Hexachlorocyclopentadiene BRL IJgl
67-72- Hexachloroethane IJglBRL 50
50193-39- Indeno (1 3-cd) pyrene BRL IJgl
5078-59- Isophorone BRL IJgl
Tfls laboratory report is not valid without all authorized signature 011 the coverpage
Page 6 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Sam le Identification Client Pro ect Matrix Collection DateTime ReceivedMWshy
2920-96- Ground Water I3-May-081030 14-May-SA 78602shy
CAS No Analyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Semivolatile Organic Compounds by GCMS
Semi volatile Or anic Com ounds b EPA 625
Prepared by method SW846 3510C
91-57 -6 Methylnaphthalene 367 1-91 50 EPA 625 16-May- 19-May-08 8051216
95-48- Methylphenol BRL 1-91 50
108-39-4 3 amp 4-Methylphenol BRL I-gl 100 106-44shy91-20- Naphthalene 247 1-91 50
88-74-4 Nitroaniline BRL 1-91 50
99-09- Nitroaniline BRL 1-91 50
100-01-6 Nitroaniline BRL 1-91 50
98-95- Nitrobenzene BRL 1-91 50
88-75- Nitrophenol BRL 1-91 50
100-02- Nitrophenol BRL 1-91 50
62-75- Nitrosodimethylamine BRL 1-91 50
621-64- N- Nitrosodi-n-propylamine BRL 1-91 50
86-30-6 Nitrosodiphenylamine BRL 1-91 50
87 -86- Pentachlorophenol BRL 1-91 50
85-0- Phenanthrene BRL 1-91 50
108-95- Phenol BRL 1-91 50
129-00-0 Pyrene BRL 1-91 50
110-86- Pyridine BRL 1-91 50
120-82- 4- Trichlorobenzene BRL 1-91 50
95-95- 5- Trichlorophenol BRL 1-91 50
88-06- 6- T richlorophenol BRL 1-91 50
Surrogate recoveries
321-60- Fluorobipheny 30- 130
367- 12- Fuorophenol 15- 110
4165-60- Nitrobenzene- 30- 130
4165-62- Pheno- 15- 110
1718-51- Terpheny-d4 30- 130
118- 79- 6- Tribromophenol 15- 110
Semivolatile Organic Compounds by GC
Pol chlorinated Bi hen ls b EPA 608
Prepared by method SW846 3510C
12674- 11-2 Aroclor- 1016 BRL 1-91 0650 EPA 608 15- May- 16-May-08 8051106
11104-28-2 Aroclor-1221 BRL IJgl 0650
11141-16-5 Aroclor- 1232 BRL 1-91 0650
53469-21-9 Aroclor- 1242 BRL 1-91 0650
12672-29-6 Aroclor- 1248 BRL 1-91 0650
11097-69-1 Aroclor- 1254 BRL 1-91 0650
11096-82-5 Aroclor -1260 BRL 1-91 0650
37324-23-5 Aroclor-1262 BRL 1-91 0650
11100-14-4 Aroclor-1268 BRL IJgl 0650
Surrogate recoveries
2051-24- Decachlorobipheny (Sr) 105 30- 150
10386-84-2 4 DB-Octafluorobiphenyl (Sr) 30- 150
Extractable Petroleum Hydrocarbons
mgl EPA 1664 Rev A 15-May- 19-May-08 8051102Non-polar material (SGT- HEM)
Soluble Metals by EPA 2006000 Series Metbods
Field Filtered NA EPA 200 73005A 15- May- 15-May-08 8051192Filtration
Soluble Metals by EPA 200 Series Methods
7440-22-4 Silver BRL mgl 0002 EPA 200 21-May- 27- May-08 8051249
This laboratory report is IlOt mlid without (II authorized signature on the cover page
Reportble Detection Limit BRL = Below Reporting Limit Page 7 of 25
Sam le Identification MW-
Client Pro ect 2920-96shy
Matrix Ground Water
Collection DateTime 13-May-08 1030
Received 14-May-
SA 78602shy
CAS No A nalyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Soluble Metals by EPA 200 Series Methods
7440-38shy Arsenic 0468 mg1 0040 EPA 200 21-Mayshy 21-May-08 80511 50
7440-43shy Cadmium BRL mg1 0002 EPA 200 21-May-088051249
7440-47shy Chromium BRL mg1 0050 EPA 200 21-May-088051150
7440-50-8 Copper BRL mg1 0050
7439-89-6 Iron 184 mg1 0150
7439-97-6 Mercury BRL mg1 00020 EPA 245 17470A 21-May-088051152
7440-02-0 Nickel BRL mg1 0050 EPA 200 21-May-088051150
7439-92shy Lead 0011 mg1 0002 EPA 200 21-May-088051249
7440-36-0 Antimony 0003 mg1 0002
7782-49shy Selenium BRL mg1 0150 EPA 200 21-May-08 8051150
7440-66-6 Zinc 0186 mgl 0050
General Chemistry Parameters
Filtration Completed NA Varies 14-Mayshy 14-May-08 8051095
18540-29-9 Hexavalent Chromium (soluble) BRL HT2 mg1 125 SM3500CrDI796A 14-Mayshy 14-May-08 8051094 R01 2013 2016
57-12shy Cyanide (total) BRL mg1 0100 EPA 3354 19-Mayshy 19-May-088051374
7782-50shy Total Residual Chlorine BRL CIHT mg1 500 Hach 8167 14-Mayshy 14-May-08 8051049 R01 1900 2001
Total Suspended Solids 580 mg1 25 SM2540D 16-Mayshy 16-May-08 8051275
This lahomtOlY report is not valid without an authorized signature on the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page 8 of 25
Volatie Organic Compounds - Quality Control
Analyte( s)
Batch 8051244 - SW846 5030 Water MS
Blank 8051244-BLK1
Prepared 16-May-08 Analyzed 17-May-
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromochloromethane
1 Dichlorobenzene
1 Dichlorobenzene
1 Dichlorobenzene
1-Dichloroethane
1 Dichloroethane
1 1-Dichloroethene
cis- Dichloroethene
trans- 1 Dichloroethene
1 Dichloropropane
cis- 1 Dichloropropene
trans- 1 Dichloropropene
Ethylbenzene
Hexanone (MBK)
Methyl tert-butyl ether
Methyl- pentanone (MIBK)
Methylene chloride
Styrene
2- Tetrachloroethane
Tetrachloroethene
Toluene
1- Trichloroethane
2- Trichloroethane
Trichloroethene
Trichlorofluoromethane (Freon 11)
Vinyl chloride
p-Xylene
Xylene
Surrogate 4-Bromofluorobenzene Surrogate Toluene-
Surrogate 1 Dichloroethane-Surrogate Dibromofluoromethane
LCS B051244-BS1
Prepared 16-May-08 Analyzed 17 -May-
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Spike Source REC RPD
Result Flag Units RDL Level Result REC Limits RPD Limit
BRL gl 20
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl 10
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gll
BRL gi
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl 10
BRL gll
BRL gll 10
BRL gl 10
BRL gll
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
41 gl 50 70- 130 49 gl 50 70- 130 59 gl 50 119 70- 130 52 gl 50 105 70- 130
QC2 jgl 20 70- 130
18 jgl 20 70- 130
192 jgl 20 35- 155
18 jgl 20 45- 169
19 jgl 20 242
This laboratOlY repol1 is lot valid without 011 authorized sigllature 011 the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page 9 of 25
Volatie Organic Compounds - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051244 - SW846 5030 Water MS
LC5 8051244B51
Prepared 16-May-08 Analyzed 17-May-
Butanone (MEK) 10 QC2 gl 20 70- 130
Carbon tetrachloride 204 gl 20 102 70- 140
Chlorobenzene 18 gl 20 70- 130
Chloroethane 164 gl 20 14-230
Chloroform 18 gll 20 51- 138
Chloromethane 21 gl 20 106 273
Dibromochloromethane 18 gl 20 53- 149
1 Dichlorobenzene 20 gl 20 104 18- 190
1 Dichlorobenzene 19 gl 20 59- 156
1 A-Dichlorobenzene 18 gl 20 18- 190
1- Dichloroethane 19 gl 20 59- 155
1 Dichloroethane 19 gl 20 49- 155
1-Dichloroethene 16 gl 20 70- 130
cis- 1 Dichloroethene 17 gl 20 70- 130
trans- 1 Dichloroethene 16 gll 20 54- 156
1 Dichloropropane 18 gl 20 210
cis- Dichloropropene 17 gl 20 227
trans- 1 Dichloropropene 17 gl 20 17- 183
Ethylbenzene 19 gl 20 37- 162
Hexanone (MBK) 124 QC2 gl 20 70- 130
Methyl tert-butyl ether 19 gl 20 70- 130
Methylshy pentanone (MIBK) 17 gl 20 70- 130
Methylene chloride 16 gl 20 221
Styrene 17 gl 20 70- 130
1 Tetrachloroethane 194 gl 20 46- 157
Tetrachloroethene 15 gl 20 64- 148
Toluene 18 gl 20 70- 130
1- Trichloroethane 20 gl 20 100 52- 162
2- Trichloroethane 18 gl 20 52- 150
Trichloroethene 17 gl 20 71- 157
Trichlorofluoromethane (Freon 11) 19 gl 20 17- 181
Vinyl chloride 21 gl 20 106 251
p-Xylene 39 gl 40 70- 130
Xylene 20 gl 20 102 70- 130
Surrogate 4-Bromofluorobenzene Surrogate Toluene-
Surrogate 1 Dichloroethane-Surrogate Dibromofluoromethane
52 49 56
49
gl
gl
gl
gl
50 50 50
50
105
112 100
70- 130 70- 130 70- 130 70- 130
LC5 DUD (8051244-B5D1
Prepared 16-May-08 Analyzed 17-May-
Acetone QC2 gl 20 70- 130
Benzene 18 gl 20 70- 130
Bromodichloromethane 18 gl 200 35- 155
Bromoform 17 gl 20 45- 169
Bromomethane 18 gl 20 242
Butanone (MEK) 11 QC2 1-91 20 70- 130
Carbon tetrachloride 20 gl 20 100 70- 140
Chlorobenzene 17 gl 20 70- 130
Chloroethane 15 1-91 20 14-230
Chloroform 18 1-91 20 51- 138
This laboratory report is aot valid without a1 authorized sig1ature 01 the cover page
Reportble Detection Limit BRL = Below Reporting Limit Page 10 of25
Volatie Organic Compounds - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051244 - SW846 5030 Water MS
LCS Dup 18051244-BSD1
Prepared 16-May-08 Analyzed 17-May-
Chloromethane 18 1-91 20 273
Dibromochloromethane 174 1-91 20 53- 149
Dichlorobenzene 20 1-91 20 100 18- 190
Dichlorobenzene 18 1-91 20 59- 156
Dichlorobenzene 18 1-91 20 18- 190
Dichloroethane 18 1-91 20 59- 155
Dichloroethane 19 1-91 20 49- 155
Dichloroethene 16 1-91 20 70- 130
cis- Dichloroethene 16 1-91 20 70- 130
trans- Dichloroethene 15 1-91 20 54- 156
Dichloropropane 17 1-91 20 210
cis- Dichloropropene 164 IJgl 20 227
trans- 1 Dichloropropene 164 I-gl 20 17- 183
Etlwlbenzene 18 IJgl 20 37- 162
Hexanone (MBK) 124 QC2 IJgl 20 70- 130
Methyl tert-butyl ether 184 1J91 20 70- 130
Methyl- pentanone (MIBK) 17 IJgl 20 70- 130
Methylene chloride 16 IJgl 20 221
Styrene 16 IJgl 20 70- 130
2- Tetrachloroethane 19 IJgl 20 46- 157
Tetrachloroethene 15 IJgl 20 64- 148
Toluene 17 IJgl 20 70- 130
1- Trichloroethane 19 1-91 20 52- 162
2- Trichloroethane 16 IJgl 20 52- 150
Trichloroethene 15 IJgl 20 71- 157
Trichlorofluoromethane (Freon 11) 17 IJgl 20 17- 181
Vinyl chloride 19 IJglI 20 251
p-Xylene 37 1J91 40 70- 130
Xylene 20 IJgl 20 100 70- 130
Surrogate 4-Bromofluorobenzene 51 IJgl 50 104 70- 130
Surrogate Toluene- 4B gl 50 70- 130
Surrogate 1 0ichloroethane- 53 IJgl 50 106 70- 130 Surrogate Oibromofluoromethane 50 1J9i 50 102 70- 130
Matrix S ike B051244-MS1 Source SA7B629shy
Prepared 16-May-08 Analyzed 17-May-
Benzene 18 20 BRL 70- 130IJgl
Bromodichloromethane 19 IJgl 20 BRL 35- 155
Bromoform 18 IJgl 20 BRL 45- 169
Bromomethane 16 IJgl 20 BRL 242
Carbon tetrachloride 21 IJgl 20 BRL 106 70- 140
Chlorobenzene 18 IJgl 20 BRL 70- 130
Chloroethane 16 IJgl 20 BRL 14-230
Chloroform 18 IJgl 20 BRL 51- 138
Chloromethane 19 IJgl 20 BRL 273
Dibromochloromethane 17 IJgl 20 BRL 53- 149
1 Dichlorobenzene 22 IJgl 20 BRL 112 18- 190
1 Dichlorobenzene 22 IJgl 20 BRL 110 59-156
1 Dichlorobenzene 21 IJgl 20 BRL 109 18- 190
1- Dichloroethane 19 IJgl 20 BRL 59- 155
1 Dichloroethane 18 IJgl 20 BRL 49- 155
This laboratory report is 110t mUd without an authorized signature on the covel page
Reportble Detection Limit BRL = Below Reporting Limit Page It of25
Volatile Organic Compounds - Quality Control
p
Spike Source REC RPD
Result REC imits RPD LimitAnalyte(s) Result Flag Units RDL Level
Batch 8051244 - SW846 5030 Water MS
Matrix ike S051244-MS1 Source SA7B629shy
Prepared 16-May-08 Analyzed 17-Mayshy
17 20 BRL 70- 130 1- Dichloroethene IJgl
16 20 BRL 54- 156trans- 1 Dichloroethene IJgl
21020 BRL1 Dichloropropane 17 1J91
cis- 1 Dichloropropene 17 IJgl 20 BRL 227
17- 183trans- 1 Dichloropropene 184 1J91 20 BRL
20 20 BRL 103 37- 162Ethylbenzene IJgl
15 20 BRL 221Methylene chloride IJgl
20 BRL 46- 1572- Tetrachloroethane 19 1J91
20 BRL 64- 148Tetrachloroethene 18 1J91
BRL 70- 130Toluene 18 1J91 20
105 52-1621- Trichloroethane 211 IJgl 20 BRL
18 20 BRL 52- 1502- Trichloroethane IJgl
17 20 BRL 71- 157Trichloroethene 1J91
20 BRL 17- 181Trichloroluoromethane (Freon 11) 194 IJgl
20 BRL 103 251Vinyl chloride 20 IJgl
102 70- 130Surrogate 4-Bromofluorobenzene 50 IJgl 50 50 70- 130Surrogate Toluene- 49 1J91
56 50 112 70- 130Surrogate 1 Dichloroethane- IJgl
50 100 70- 130Surrogate Dibromofluoromethane 50 IJgl
Matrix S ike Du S051244-MSD1 Source SA7S629shy
Prepared 16-May-08 Analyzed 17-Mayshy
18 20 BRL 70- 130Benzene IJgl
18 20 BRL 35- 155Bromodichloromethane IJgl
17 20 BRL 45- 169Bromoform IJgl
20 BRL 242Bromomethane 17 IJgl
20 BRL 103 70- 140Carbon tetrachloride 20 IJgl
18 20 BRL 70- 130Chlorobenzene 1J91
14-230Chloroethane 16 IJgl 20 BRL
20 51- 138Chloroform 184 IJgl BRL
Chloromethane 19 1J91 20 BRL 273
18 20 BRL 53- 149Dibromochloromethane 1J91
20 BRL 117 18- 190Dichlorobenzene 234 IJgl
20 BRL 112 59- 156Dichlorobenzene 22 IJgl
BRL 108 18- 190Dichlorobenzene 21 1J91 20
20 59- 1551 Dichloroethane 19 IJgl BRL
18 20 BRL 49- 155Dichloroethane IJgl
16 20 BRL 70- 130Dichloroethene IJgl
20 BRL 54- 156trans- Dichloroethene 154 1J91
20 BRL 210Dichloropropane 17 IJgl
0420 BRL 227cis- Dichloropropene 17 IJgl
17- 183trans- Dichloropropene 17 1J91 20 BRL
BRL 37- 162Ethylbenzene 20 1J91 20 102
Methylene chloride 15 IJgl 20 BRL 221
20 BRL 46- 1572- Tetrachloroethane 192 IJgl
20 BRL 64- 148 04Tetrachloroethene 18 IJgl
BRL 70- 130Toluene 184 1J91 20
52- 1621- Trichloroethane 20 IJgl 20 BRL 104
17 20 BRL 52- 1502- Trichloroethane IJgl
17 20 BRL 71- 157Trichloroethene IJgl
20 BRL 17-181Trichlorofluoromethane (Freon 11) 19 IJgl
This laboratory report is IIOt valid without all authorized sigllllture 011 the cover page
Page 12 of25 Reportble Detection Limit BRL = Below Reporting Limit
Semivolatile Organic Compounds by GCMS - Quality Control
Analyte(s)
Batch 8051216 - SW846 3510C
Blank 8051216-BLK1
Prepared amp Analyzed 16-May-
Isophorone
Methylnaphthalene
Methylphenol
3 amp 4-Methylphenol
Naphthalene
Nitroaniline
Nitroaniline
Nitroaniline
Nitrobenzene
Nitrophenol
Nitrophenol
Nitrosodimethylamine
N- N itrosodi-n-pro pyla mine
N itrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Pyridine
1 24-Trichlorobenzene
24 5- Trichlorophenol
246- Trichlorophenol
Surrogate 2-Fuorobipheny Surrogate 2-Fuoropheno Surrogate Nitrobenzene-Surrogate PhenoshySurrogate Terpheny-d4 Surrogate 6- Tribromopheno
LCS B051216-BS1
Prepared amp Analyzed 16-May-
Acenaphthene
Acenaphthylene
Aniline
Anthracene
AzobenzenelDi phenyld lazine
Benzidine
Benzo (a) anthracene
Benzo (a) pyrene
Benzo (b) fluoranthene
Benzo (g i) perylene
Benzo (k) fluoranthene
Benzoic acid
Benzyl alcohol
B is(2-chloroethoxy)methane
B i s (2-ch loroethyl)eth e r
Bis(2-ch loroisopropyl) ether
B is(2-ethy Ih exyl) phtha late
Bromophenyl phenyl ether
Butyl benzyl phthalate
Carbazole
Spike Source REC RPD
Result Flag Units RDL Level Result REC Limits RPD Limit
BRL gl
BRL gl
BRL gl
BRL gl 10
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gll
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
370 gl 50 30- 130 40 gl 50 15- 110 39 gl 50 30- 130 43 gl 50 15- 110 36 gl 50 30- 130 40 gl 50 15- 110
41 gl 50 40- 140
43 gI 50 40- 140
41 gl 50 40- 140
38 gl 50 40- 140
45 gl 50 40- 140
49 gl 50 153
41 gl 50 40- 140
43 gl 50 40- 140
41 gl 50 40- 140
41 gll 50 40- 140
45 gl 50 40- 140
32 gl 50 12- 149
41 gl 50 40- 140
39 gl 50 40- 140
384 gl 50 40- 140
47 gl 50 40- 140
47 gl 50 40- 140
40 gl 50 40- 140
47 gI 50 40- 140
56 gI 50 112 200
This laboratory report is lIot valid witllOut a1l authorized sigllature 011 the coverpage
Reportble Detection Limit BRL = Below Reporting Limit Page 15 of25
Semivolatile Organic Compounds by GCMS - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051216 - SW846 3510C
LCS 8051216-BS1
Prepared amp Analyzed 16-Mayshy
50 30- 1304 -C hloro-3-methylphenol 42 IJgl
40- 140Chloroaniline 39 IJgl 50
Chloronaphthalene 37 IJgl 50 40- 140
Chlorophenol 37 IJgl 50 30- 130
50 40- 140
40- 140
Chlorophenyl phenyl ether 45 IJgl
Chrysene 43 IJgl 50
Dibenzo (a h) anthracene 43 IJgl 50 40- 140
Dibenzofuran IJgl38 50 40- 140
50 40- 1401 Dichlorobenzene 35 IJgl
40- 1401 Dichlorobenzene 264 IJgl 50
40- 1401 Dichlorobenzene 434 IJgl 50
58 50 116 40- 1403 - Dichlorobenzidine IJgl
50 30- 130
40- 140 24-Dichlorophenol 38 IJgl
Diethyl phthalate 484 IJgl 50
50 40- 140Dimethyl phthalate 464 IJgl
Dlmethylphenol 39 IJgl 50 30- 130
DI-n-butyl phthalate 44 IJgll 50 40- 140
30- 130 6-Di nitro- 2-methylphenol 38 1J91 50
30- 130Dinltrophenol 36 1J91 50
42 50 40- 14024-Dlnitrotoluene 1J91
Dlnitrotoluene 1J9141 50 40- 140
Di-n-octyl phthalate 52 IJgl 50 104 40- 140
40- 140Fluoranthene 40 IJgl 50
Fluorene 41 IJgl 50 40- 140
39 50 40- 140Hexachlorobenzene IJgl
50 40- 140Hexachlorobutadiene 40 IJgl
40- 140Hexach lorocyclopentad iene 294 IJgl 50
40 50 40- 140Hexachloroethane IJgl
42 50 40-140Indeno (1 3-cd) pyrene IJgl
50 40- 140Isophorone 40 IJgl
40- 140Methylnaphthalene 394 IJgl 50
40- 140Methylphenol 39 IJgl 50
40 10 50 40- 1403 amp 4-Methylphenol IJgl
37 50 40-140Naphthalene IJgl
50 40-140Nitroaniline 39 IJgl
Nitroaniline 51 IJgl 50 102 40- 140
48 50 40- 140Nltroaniline 1J91
50 40- 140Nitrobenzene 40 IJgl
30- 130Nitrophenol 36 IJgl 50
40 IJgl 50 30- 130Nitrophenol 40- 140Nitrosodimethylamine 32 1J91 50
50 40-140N- N itrosodi-n-propyla mine 46 IJgl
40- 140N itrosodi phenyla ml ne 44 IJgl 50
41 IJgl 50 30- 130Pentachlorophenol 40- 140Phenanthrene 38 IJgl 50
50 30- 130Phenol 38 IJgl
40- 140Pyrene 424 1J91 50
40- 140Pyridine 294 1J91 50
40- 14024- Trichlorobenzene 364 IJgl 50
This laboratory report is not mlid without an authorized signature 011 the cover page
Page 16 of25 Reportble Detection Limit BRL = Below Reporting Limit
Semivolatie Organic Compounds by GCMS - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
BMch 8051216 - SW846 3510C
LC5 8051216-851
Prepared amp Analyzed 16-Mayshy
24 5- Trichlorophenol 404 gl 50 30- 130
246- Trichlorophenol 42 gl 50 30- 130
Surrogate 2-Fluorobiphenyl 29 gl 50 30- 130
Surrogate 2-Fluorophenot 27 gl 50 15- 110
Surrogate Nitrobenzene- 30 gl 50 30- 130
Surrogate Phenol- 29 gl 50 15- 110
Surrogate Terpheny-d4 30 gl 50 30- 130
Surrogate 6- Tribromopheno 324 gl 50 15- 110
This laboratory report is lIot valid without all authorized sigllature 011 tlle cover page
Reportble Detection Limit BRL = Below Reporting Limit Page 17 of25
Semivolatie Organic Compounds by GC - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051106 - SW846 3510C
Blank S051106-BLK1
Prepared amp Analyzed 15-Mayshy
Aroclor- 1016 BRL gI 0200
Aroclor- 1016 (2C) BRL gI 0200
Aroclor- 1221 BRL gI 0200
Aroclor- 1221 (2C) BRL gI 0200
Aroclor- 1232 BRL gI 0200
Aroclor- 1232 (2Cj BRL gI 0200
Aroclor- 1242 BRL gI 0200
Aroclor-1242 (2C) BRL gI 0200
Aroclor- 1248 BRL gI 0200
Aroclor- 1248 (2C) BRL gI 0200
Aroclor- 1254 BRL gI 0200
Aroclor- 1254(2Cj BRL gI 0200
Aroclor- 1260 BRL gI 0200
Aroclor- 1260 (2C) BRL gI 0200
Aroclor- 1262 BRL gI 0200
Aroclor- 1262 (2C) BRL gI 0200
Aroclor-1268 BRL gI 0200
Aroclor- 1268 (2C) BRL gI 0200
Surrogate Decachlorobiphenyl (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0231 0224 0194 0191
gI
gI
gI
gI
0200 0200 0200 0200
116 112
30- 150 30- 150 30- 150 30- 150
LC5 8051106-B51
Prepared 15-May-08 Analyzed 16-May-08
Aroclor- 1016 265 gI 0200 250 106 50- 114
Aroclor- 1 016 (2C) 240 gI 0200 250 50- 114
Aroclor- 1260 0269 gI 0200 250 107 40- 127
Aroclor-1260 (2Cj 270 gI 0200 250 108 40- 127
Surrogate Decachlorobiphenyl (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0225 0224 0188 0183
gI
gI
gI
gI
0200 0200 0200 0200
113 112
30- 150 30- 150 30- 150 30- 150
LC5 DUD rS051106-B5D1
Prepared 15-May-08 Analyzed 16-Mayshy
Aroclor- 1016 262 gl 0200 250 105 50- 114
Aroclor-1 016 (2Cj 241 gI 0200 250 50- 114
Aroclor- 1260 277 gI 0200 250 111 40- 127
Aroclor- 1260(2Cj 0260 gI 0200 250 104 40- 127
Surrogate Decachlorobipheny (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0238 0218 0189 0181
gI
gI
gI
gI
0200 0200 0200 0200
119 109
30- 150 30- 150 30- 150 30- 150
This laboratory report is lot valid without (II authorized sigllature 01 the cover page
Page 18 of25 Reportable Detection Limit BRL = Below Reporting Limit
Extractable Petroleum Hydrocarbons - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051102 - SW846 3510C
Blank 8051102-BLK1
Prepared 15-May-08 Analyzed 19-Mayshy
Non-polar material (SGT- HEM) BRL m91
LC8 8051102-B81
Prepared 15-May-08 Analyzed 19-Mayshy
Non-polar material (SGT- HEM) 184 m91 21 81 904
This laboratory report is not valid without an authorized signature 011 the cover page
Page 19 of25 Reportable Detection Limit BRL = Below Reporting Limit
Soluble Metals by EPA 200 Series Methods - Quality Control
Analyte(s) Result Flag Units RDL
Spike
Level
Source
Result REC
REC
Limits RPD
RPD
Limit
Batch 8051150 - EPA 200 Series
Blank 8051150-BLK1
Prepared amp Analyzed 21-May-
Iron
Zinc
Selenium
Nickel
Chromium
Copper
Arsenic
BRL
BRL
BRL
BRL
BRL
BRL
BRL
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0150
0050
0150
0050
0050
0050
0040
LCS 8051150-BS1
Prepared amp Analyzed 21-May-
Selenium
Zinc
Iron
Nickel
Chromium
Arsenic
Copper
123
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0150
0050
0150
0050
0050
0040
0050
103
105
101
100
85- 115
85- 115
85- 115
85- 115
85- 115
85-115
85- 115
licate B051150-DUP1 Source SA7B602shy
Prepared amp Analyzed 21-May-
Iron
Zinc
Selenium
Nickel
Copper
Chromium
Arsenic
17
0162
BRL
0015
0017
BRL
0450
QR8
mgl
mgl
mgl
mgl
mgl
mgl
mgi
0150
0050
0150
0050
0050
0050
0040
184
0186
BRL
0014
0023
BRL
0468
Matrix S ike 8051150-MS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Iron
Selenium
Nickel
Zinc
Copper
Chromium
Arsenic
19 QM2 mgl
mgll
mgl
mgl
mgl
mgl
mgl
0150
0150
0050
0050
0050
0050
0040
125
184
BRL
0014
0186
0023
BRL
0468
104
105
102
70- 130
70- 130
70-130
70- 130
70- 130
70-130
70- 130
Post S ike 8051150-PS1 Source SA78602shy
Prepared amp Analyzed 21-May-
Zinc
Iron
Selenium
Nickel
Copper
Arsenic
Chromium
18 QM2
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0050
0150
0150
0050
0050
0040
0050
0186
184
BRL
0014
0023
0468
BRL
104
104
101
85- 115
85- 115
85- 115
85-115
85-115
85- 115
85-115
Batch 8051152 - EPA200SW7000 Series
Blank B051152-BLK1
Prepared amp Analyzed 21-May-
Mercury BRL mgl 00020
This laboratory report is IIOt valid witllOut all authorized sigllature 011 the coverpage
Page 20 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Soluble Metals by EPA 200 Series Methods - Quality Control
Analyte(s) Result Flag Units RDL
Spike
Level
Source
Result REC
REC
Limits RPD
RPD
Limit
Batch 8051152 - EPA200SW7000 Series
LCS B051152-BS1
Prepared amp Analyzed 21-May-
Mercury 00576 m91 00020 00500 115 85- 115
licate B051152-DUP1 Source SA78602-01
Prepared amp Analyzed 21-May-
Mercury BRL m91 00020 BRL
Matrix S ike 8051152-MS1 Source SA78602shy
Prepared amp Analyzed 21-May-
Mercury 00632 OM m91 00020 00500 BRL 126 75- 125
Post S ike 8051152-PS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Mercury 00624 OC1 m91 00020 00500 BRL 125 85- 115
Batch 8051249 - 2008No digestion
Blank 8051249-BLK1
Prepared amp Analyzed 21-May-
Lead
Antimony
Cadmium
Silver
BRL
BRL
BRL
BRL
m91
m91
m91
m91
0002
0002
0002
0002
LCS B051249-BS1
Prepared amp Analyzed 21-May-
Antimony
Lead
Silver
Cadmium
143
145 OC2
m91
m91
m91
m91
0050
0050
0050
0040
103
115
107
116
85- 115
85- 115
85- 115
85- 115
licate 8051249-DUP1 Source SA7B602shy
Prepared amp Analyzed 21- May-
Lead
Antimony
Cadmium
Silver
0009
0002
00005
00002
ORB
m91
m91
m91
m91
0002
0002
0002
0002
0011
0003
00005
00003
Matrix S ike 8051249-MS1 Source SA78602shy
Prepared amp Analyzed 21- May-
Lead
Antimony
Cadmium
Silver
142
m91
m91
m91
m91
0050
0050
0040
0050
0011
0003
00005
00003
111
101
114
102
70- 130
70-130
70c130
70- 130
Post S ike 8051249-PS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Antimony
Cadmium
Silver
38
OC2
m91
m91
m91
0050
0040
0050
125
0003
00005
00003
110
121
109
85- 115
85- 115
85- 115
This laboratory report is flOt valid IVithout all authorized signature 011 the cOIer page
Reportable Detection Limit BRL Below Reporting Limit Page 21 of 25
General Chemistry Parameters - Quality Control
Spike Source REC RPD
Analyte( s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051049 - General Preparation
Blank S051 049-BLK1
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
Blank S051049-BLK2
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
Blank S051 049-BLK3
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
LCS S051049-BS1
Prepared amp Analyzed 14-May-
Total Residual Chlorine 046 mgl 020 0500 90- 110
LCS S051049-BS2
Prepared amp Analyzed 14-May-
Total Residual Chlorine 047 mgl 020 0500 90- 110
LCS S051049-BS3
Prepared amp Analyzed 14-May-
Total Residual Chlorine 054 mgl 020 0500 108 90-110
licate B051049-DUP1 Source SA7S544shy
Prepared amp Analyzed 14-May-
Total Residual Chlorine 012 mgl 020 010
licate S051049-DUP2 Source SA7S602-01
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020 BRL
Matrix S ike 8051049-MS1 Source SA78544-01
Prepared amp Analyzed 14-May-
Total Residual Chlorine 065 mgl 020 0500 010 110 80- 120
Matrix S ike 8051049-MS2 Source SA7B602shy
Prepared amp Analyzed 14-May-
Total Residual Chlorine mgl 500 125 BRL 108 80- 120
Reference 8051 049-SRM1
Prepared amp Analyzed 14-May-
Total Residual Chlorine 100 mgl 020 0967 103 85-115
Batch 8051094 - General Preparation
Blank 8051094-BLK1
Prepared amp Analyzed 14 May-
Hexavalent Chromium (soluble) BRL mgl 005
Blank 8051 094-BLK2
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) BRL mgl 005
LCS 8051094-BS1
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) 054 mgl 005 90- 110
licate 8051094-DUP1 Source SA78602-01
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) BRL mgl 125 BRL
Thi laboratory report is not valid without all authorized sigllature 011 the cover page
Page 22 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Page 17
Semivolatile Organic Compounds by GCMS - Quality Control
Analyte( s)
Batch 8051216 - SW846 3510C
Blank 8051216BLK1)
Prepared amp Analyzed 16May-
Acenaphthene
Acenaphthylene
Aniline
Anthracene
AzobenzenelDi phenyld iazi ne
Benzidine
Benzo (a) anthracene
Benzo (a) pyrene
Benzo (b) fiuoranthene
Benzo (g i) perylene
Benzo (k) fiuoranthene
Benzoic acid
Benzyl alcohol
Bis(2-ch loroethoxy) methane
Bis(2-ch loroethyl)ether
Bis(2-ch loroi sopropyl)ether
Bis(2ethylhexyl) phthalate
Bromophenyl phenyl ether
Butyl benzyl phthalate
Carbazole
Ch loro-3-methyl phenol
Chloroaniline
Chloronaphthalene
Chlorophenol
Chlorophenyl phenyl ether
Chrysene
Dibenzo (a h) anthracene
Dibenzofuran
Dichlorobenzene
Dichlorobenzene
14- Dichlorobenzene
3 - Dichlorobenzidine
24-Dichlorophenol
Diethyl phthalate
Dimethyl phthalate
24- Dimethylphenol
Din-butyl phthalate
Dinitro-2-methylphenol
Dinitrophenol
Dinitrotoluene
Dinitrotoluene
Di-noctyl phthalate
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopehtadiene
Hexachloroethane
Indeno (1 cd) pyrene
Spike Source REC RPD
Result Flag Units RDL Level Result REC Limits RPD Limit
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gI
BRL gl
BRL gI
BRL gl
BRL gl
BRL gl
BRL gI
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gll
BRL gl
BRL gll
BRL gl
BRL gl
BRL gI
BRL gI
BRL gI
BRL gl
BRL gI
BRL gI
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gI
BRL gI
BRL gl
This laboratory report is IlOt valid without all authorized sigllature 011 the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page t4 of25
Volatie Organic Compounds - Quality Control
p (
Spike Source REC RPD
RDL Level Result REC Limits RPD Limit Analyte(s) Result Flag Units
Batch 8051244 - SW846 5030 Water MS
Matrix S ike Du 8051244-MSD1 Source SA78629shy
Prepared 16-May-08 Analyzed 17-May-BRL 106 251
Vinyl chloride 21 gl 20
101 70- 130 Surrogate 4-Bromofluorobenzene 50 gl 50
70- 13049 gl 50 111 70- 130
Surrogate Toluene-Surrogate 1 Dichloroethane- 55 gl 50
50 70- 130494 glSurrogate Dibromofluoromethane
Microextractable Organic Compounds - Quality Control
Spike Source REC RPD
Flag Units RDL Level Result REC Limits RPD Limit Analyte(s) Result
Batch 8051105 - SW846 3510C
Blank 8051105-BLK
Prepared amp Analyzed 15-May-
BRL gl 01001 Dibromoethane (ED B)
LCS 8051105-BS1
Prepared amp Analyzed 15-Mayshy50- 1500770 gl 0100 100
licate 8051105-DUP1 Source SA7B583shy
Prepared amp Analyzed 15-May-
BRL gl 0100 BRL
1 Dibromoethane (EDB)
1 Dibromoethane (EDB)
This laborntOlY report is not valid without an authorized signature 011 the cover page
Page 13 of2S Reportable Detection Limit BRL = Below Reporting Limit
Sam le Identification Client Pro ect Matrix Collection DateTime ReceivedMWshy
2920-96- Ground Water 13-May-081030 14-May-SA 78602shy
CAS No Analyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Volatile Organic Compounds
Volatile Or anic Com ounds b GCMS
Prepared by method SW846 5030 Water MS
123-91- Dioxane BRL 1-91 200 EPA 624 16-May-08 17-May-08 8051244
994-05-8 Ter-amyl methyl ether BRL 1-911 20
755- Tert-Butanoll butyl alcohol BRL 1-91 200
67-B4- Acetone BRL 1-91 400
71-43- Benzene BRL 1-91 20
75-27-4 Bromodichloromethane BRL 1-91 20
75-25- Bromoform BRL 1-91 20
74-83- Bromomethane BRL 1-91 40
78-93- Butanone (MEK) BRL 1-91 200
56-23- Carbon tetrachloride BRL 1-91 20
108-90- Chlorobenzene BRL 1-91 20
75-00- Chloroethane BRL 1-91 40
676- Chloroform BRL 1-91 20
74-87- Chloromethane BRL 1-91 40
124-48- Dibromochloromethane BRL 1-91 20
95-50- Dichlorobenzene BRL 1-911 20
541-73- Dichlorobenzene BRL 1-91 20
106-46- Dichlorobenzene BRL 1-91 20
75-34- 1- Dichloroethane BRL 1-91 20
107-06- Dichloroethane BRL 1-91 20
75-35-4 1- Dichloroethene BRL 1-91 20
156-59 cis- Dichloroethene BRL 1-91 20
156-60- trans- Dichloroethene BRL 1-91 20
78-87- 2- Dichloropropane BRL 1-91 20
10061-01-5 cis- Dichloropropene BRL 1-91 20
10061-02-B trans- Dichloropropene BRL 1-91 20
100-41-4 Ethylbenzene 411 1-911 20
591-78-B BRL 200Hexanone (MBK) 1-91
1634-04 -4 Methyl tert-butyl ether BRL 1-91 20
108-10- Methyl- pentanone (MIBK) BRL 1-91 200
75-09- Methylene chloride BRL 1-91 200
100-42- Styrene BRL 1-91 20
79-34- 1 Tetrachloroethane BRL 1-91 20
127- 18-4 T etrachloroethene BRL 1-91 20
108-88- Toluene BRL 1-91 20
71-55 1- Trichloroethane BRL 1-91 20
79-00- 2- Trichloroethane BRL 1-91 20
79-01-B Trichloroethene BRL 1-91 20
759-4 Trichlorofluoromethane (Freon 11) BRL 1-91 20
75-01-4 Vinyl chloride BRL 1-91 20
179601-23-1 m Xylene 390 1-91 40
95-47 Xylene 82 1-91 20
Surrogate recoveries 460-00- Bromofluorobenzene 70- 130
2037-26- Toluene- 100 70- 130
17060-07-0 1 Dichloroethane- 111 70- 130
1868-53- Dibromofluoromethane 70- 130
Microextractable Organic Compounds
106-93-4 1 Dibromoethane (EDB) BRL 1-91 0100 EPA 504 15-May- 15-May-08 8051105
Semivolatile Organic Compounds by GCMS
This laboratory report is not valid without all autllOrized signature 011 the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page 5 of 25
Sam le Identification Client Pro ect Matrix Collection DateTime Received
MWshy2920-96- Ground Water 13-May-081030 14-May-
SA 78602shy
CAS No Analyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Semivolatie Organic Compounds by GCMS
Semi volatile Or anic Com ounds b EPA 625
Prepared by method SW846 3510C 50 EPA 625 16-May- 19-May-08 805121683-32- Acenaphthene BRL IJgl
208-96-8 Acenaphthylene BRL IJgl 50
62-53- BRL IJgll 50Aniline
120- 12- Anthracene BRL 1J91 50
103-33- AzobenzenefDiphenyldiazine BRL IJgl 50
92-87 - Benzidine BRL IJgl 50
56-55- Benzo (a) anthracene BRL 1J91 50
50-32 - Benzo (a) pyrene IJglBRL 50
205-99- Benzo (b) fluoranthene BRL IJgl 50
191-24- Benzo (g i) perylene BRL IJgl 50
50207-08- Benzo (k) fluoranthene BRL IJgl
65-85 Benzoic acid BRL 1J91 50
100-51-6 Benzyl alcohol 1J91BRL 50
50111-91- Bis(2-chloroethoxy)methane BRL 1J91
111-4-4 Bis(2-chloroethyl)ether BRL IJgl 50
501 08-60- Bis(2-chloroisopropyl)ether BRL IJgl
117-81- Bis(2-ethylhexyl)phthalate BRL 1J91 50
101-55- Bromophenyl phenyl ether BRL IJgl 50
5085-68- Butyl benzyl phthalate BRL IJgl
5086-74- Carbazole BRL IJgl
5059-50- C hloro-3-methylphenol BRL IJgl
106-47- Chloroaniline BRL IJgl 50
91-58- Chloronaphthalene IJglBRL 50
5095-57 - Chlorophenol BRL 1J91
507005-72- Chlorophenyl phenyl ether BRL IJgl
216-01- Chrysene tJ91BRL 50
5053-70- Dibenzo (a h) anthracene BRL IJgl
50132-64- Dibenzofuran BRL IJgl
95-50- Dichlorobenzene IJglBRL 50
541-73- 13- Dichlorobenzene BRL IJgl 50
106-46- Dichlorobenzene 1J91BRL 50
5091-94- 3 - Dichlorobenzidine BRL IJgl
120-83- Dichlorophenol BRL IJgl 50
84-66- Diethyl phthalate BRL IJgl 50
131-11- Dimethyl phthalate BRL IJgll 50
105-67- Dimethylphenol BRL 1J91 50
5084-74- Di-n- butyl phthalate BRL 1J91
534-52 - Dinitro-2-methylphenol BRL IJgl 50
51-28- Dinitrophenol IJglBRL 50
50121-14- Dinitrotoluene BRL 1J91
606-20- Dinitrotoluene IJglBRL 50
50117-84-0 Di-n-octyl phthalate BRL IJgl
206-44-0 Fluoranthene 1J91BRL 50
BRL 50
50 86-73- Fluorene IJgi
118-74- Hexachlorobenzene BRL 1J91
87-68- Hexachlorobutadiene 1J91BRL 50
5077-47-4 Hexachlorocyclopentadiene BRL IJgl
67-72- Hexachloroethane IJglBRL 50
50193-39- Indeno (1 3-cd) pyrene BRL IJgl
5078-59- Isophorone BRL IJgl
Tfls laboratory report is not valid without all authorized signature 011 the coverpage
Page 6 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Sam le Identification Client Pro ect Matrix Collection DateTime ReceivedMWshy
2920-96- Ground Water I3-May-081030 14-May-SA 78602shy
CAS No Analyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Semivolatile Organic Compounds by GCMS
Semi volatile Or anic Com ounds b EPA 625
Prepared by method SW846 3510C
91-57 -6 Methylnaphthalene 367 1-91 50 EPA 625 16-May- 19-May-08 8051216
95-48- Methylphenol BRL 1-91 50
108-39-4 3 amp 4-Methylphenol BRL I-gl 100 106-44shy91-20- Naphthalene 247 1-91 50
88-74-4 Nitroaniline BRL 1-91 50
99-09- Nitroaniline BRL 1-91 50
100-01-6 Nitroaniline BRL 1-91 50
98-95- Nitrobenzene BRL 1-91 50
88-75- Nitrophenol BRL 1-91 50
100-02- Nitrophenol BRL 1-91 50
62-75- Nitrosodimethylamine BRL 1-91 50
621-64- N- Nitrosodi-n-propylamine BRL 1-91 50
86-30-6 Nitrosodiphenylamine BRL 1-91 50
87 -86- Pentachlorophenol BRL 1-91 50
85-0- Phenanthrene BRL 1-91 50
108-95- Phenol BRL 1-91 50
129-00-0 Pyrene BRL 1-91 50
110-86- Pyridine BRL 1-91 50
120-82- 4- Trichlorobenzene BRL 1-91 50
95-95- 5- Trichlorophenol BRL 1-91 50
88-06- 6- T richlorophenol BRL 1-91 50
Surrogate recoveries
321-60- Fluorobipheny 30- 130
367- 12- Fuorophenol 15- 110
4165-60- Nitrobenzene- 30- 130
4165-62- Pheno- 15- 110
1718-51- Terpheny-d4 30- 130
118- 79- 6- Tribromophenol 15- 110
Semivolatile Organic Compounds by GC
Pol chlorinated Bi hen ls b EPA 608
Prepared by method SW846 3510C
12674- 11-2 Aroclor- 1016 BRL 1-91 0650 EPA 608 15- May- 16-May-08 8051106
11104-28-2 Aroclor-1221 BRL IJgl 0650
11141-16-5 Aroclor- 1232 BRL 1-91 0650
53469-21-9 Aroclor- 1242 BRL 1-91 0650
12672-29-6 Aroclor- 1248 BRL 1-91 0650
11097-69-1 Aroclor- 1254 BRL 1-91 0650
11096-82-5 Aroclor -1260 BRL 1-91 0650
37324-23-5 Aroclor-1262 BRL 1-91 0650
11100-14-4 Aroclor-1268 BRL IJgl 0650
Surrogate recoveries
2051-24- Decachlorobipheny (Sr) 105 30- 150
10386-84-2 4 DB-Octafluorobiphenyl (Sr) 30- 150
Extractable Petroleum Hydrocarbons
mgl EPA 1664 Rev A 15-May- 19-May-08 8051102Non-polar material (SGT- HEM)
Soluble Metals by EPA 2006000 Series Metbods
Field Filtered NA EPA 200 73005A 15- May- 15-May-08 8051192Filtration
Soluble Metals by EPA 200 Series Methods
7440-22-4 Silver BRL mgl 0002 EPA 200 21-May- 27- May-08 8051249
This laboratory report is IlOt mlid without (II authorized signature on the cover page
Reportble Detection Limit BRL = Below Reporting Limit Page 7 of 25
Sam le Identification MW-
Client Pro ect 2920-96shy
Matrix Ground Water
Collection DateTime 13-May-08 1030
Received 14-May-
SA 78602shy
CAS No A nalyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Soluble Metals by EPA 200 Series Methods
7440-38shy Arsenic 0468 mg1 0040 EPA 200 21-Mayshy 21-May-08 80511 50
7440-43shy Cadmium BRL mg1 0002 EPA 200 21-May-088051249
7440-47shy Chromium BRL mg1 0050 EPA 200 21-May-088051150
7440-50-8 Copper BRL mg1 0050
7439-89-6 Iron 184 mg1 0150
7439-97-6 Mercury BRL mg1 00020 EPA 245 17470A 21-May-088051152
7440-02-0 Nickel BRL mg1 0050 EPA 200 21-May-088051150
7439-92shy Lead 0011 mg1 0002 EPA 200 21-May-088051249
7440-36-0 Antimony 0003 mg1 0002
7782-49shy Selenium BRL mg1 0150 EPA 200 21-May-08 8051150
7440-66-6 Zinc 0186 mgl 0050
General Chemistry Parameters
Filtration Completed NA Varies 14-Mayshy 14-May-08 8051095
18540-29-9 Hexavalent Chromium (soluble) BRL HT2 mg1 125 SM3500CrDI796A 14-Mayshy 14-May-08 8051094 R01 2013 2016
57-12shy Cyanide (total) BRL mg1 0100 EPA 3354 19-Mayshy 19-May-088051374
7782-50shy Total Residual Chlorine BRL CIHT mg1 500 Hach 8167 14-Mayshy 14-May-08 8051049 R01 1900 2001
Total Suspended Solids 580 mg1 25 SM2540D 16-Mayshy 16-May-08 8051275
This lahomtOlY report is not valid without an authorized signature on the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page 8 of 25
Volatie Organic Compounds - Quality Control
Analyte( s)
Batch 8051244 - SW846 5030 Water MS
Blank 8051244-BLK1
Prepared 16-May-08 Analyzed 17-May-
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromochloromethane
1 Dichlorobenzene
1 Dichlorobenzene
1 Dichlorobenzene
1-Dichloroethane
1 Dichloroethane
1 1-Dichloroethene
cis- Dichloroethene
trans- 1 Dichloroethene
1 Dichloropropane
cis- 1 Dichloropropene
trans- 1 Dichloropropene
Ethylbenzene
Hexanone (MBK)
Methyl tert-butyl ether
Methyl- pentanone (MIBK)
Methylene chloride
Styrene
2- Tetrachloroethane
Tetrachloroethene
Toluene
1- Trichloroethane
2- Trichloroethane
Trichloroethene
Trichlorofluoromethane (Freon 11)
Vinyl chloride
p-Xylene
Xylene
Surrogate 4-Bromofluorobenzene Surrogate Toluene-
Surrogate 1 Dichloroethane-Surrogate Dibromofluoromethane
LCS B051244-BS1
Prepared 16-May-08 Analyzed 17 -May-
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Spike Source REC RPD
Result Flag Units RDL Level Result REC Limits RPD Limit
BRL gl 20
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl 10
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gll
BRL gi
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl 10
BRL gll
BRL gll 10
BRL gl 10
BRL gll
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
41 gl 50 70- 130 49 gl 50 70- 130 59 gl 50 119 70- 130 52 gl 50 105 70- 130
QC2 jgl 20 70- 130
18 jgl 20 70- 130
192 jgl 20 35- 155
18 jgl 20 45- 169
19 jgl 20 242
This laboratOlY repol1 is lot valid without 011 authorized sigllature 011 the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page 9 of 25
Volatie Organic Compounds - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051244 - SW846 5030 Water MS
LC5 8051244B51
Prepared 16-May-08 Analyzed 17-May-
Butanone (MEK) 10 QC2 gl 20 70- 130
Carbon tetrachloride 204 gl 20 102 70- 140
Chlorobenzene 18 gl 20 70- 130
Chloroethane 164 gl 20 14-230
Chloroform 18 gll 20 51- 138
Chloromethane 21 gl 20 106 273
Dibromochloromethane 18 gl 20 53- 149
1 Dichlorobenzene 20 gl 20 104 18- 190
1 Dichlorobenzene 19 gl 20 59- 156
1 A-Dichlorobenzene 18 gl 20 18- 190
1- Dichloroethane 19 gl 20 59- 155
1 Dichloroethane 19 gl 20 49- 155
1-Dichloroethene 16 gl 20 70- 130
cis- 1 Dichloroethene 17 gl 20 70- 130
trans- 1 Dichloroethene 16 gll 20 54- 156
1 Dichloropropane 18 gl 20 210
cis- Dichloropropene 17 gl 20 227
trans- 1 Dichloropropene 17 gl 20 17- 183
Ethylbenzene 19 gl 20 37- 162
Hexanone (MBK) 124 QC2 gl 20 70- 130
Methyl tert-butyl ether 19 gl 20 70- 130
Methylshy pentanone (MIBK) 17 gl 20 70- 130
Methylene chloride 16 gl 20 221
Styrene 17 gl 20 70- 130
1 Tetrachloroethane 194 gl 20 46- 157
Tetrachloroethene 15 gl 20 64- 148
Toluene 18 gl 20 70- 130
1- Trichloroethane 20 gl 20 100 52- 162
2- Trichloroethane 18 gl 20 52- 150
Trichloroethene 17 gl 20 71- 157
Trichlorofluoromethane (Freon 11) 19 gl 20 17- 181
Vinyl chloride 21 gl 20 106 251
p-Xylene 39 gl 40 70- 130
Xylene 20 gl 20 102 70- 130
Surrogate 4-Bromofluorobenzene Surrogate Toluene-
Surrogate 1 Dichloroethane-Surrogate Dibromofluoromethane
52 49 56
49
gl
gl
gl
gl
50 50 50
50
105
112 100
70- 130 70- 130 70- 130 70- 130
LC5 DUD (8051244-B5D1
Prepared 16-May-08 Analyzed 17-May-
Acetone QC2 gl 20 70- 130
Benzene 18 gl 20 70- 130
Bromodichloromethane 18 gl 200 35- 155
Bromoform 17 gl 20 45- 169
Bromomethane 18 gl 20 242
Butanone (MEK) 11 QC2 1-91 20 70- 130
Carbon tetrachloride 20 gl 20 100 70- 140
Chlorobenzene 17 gl 20 70- 130
Chloroethane 15 1-91 20 14-230
Chloroform 18 1-91 20 51- 138
This laboratory report is aot valid without a1 authorized sig1ature 01 the cover page
Reportble Detection Limit BRL = Below Reporting Limit Page 10 of25
Volatie Organic Compounds - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051244 - SW846 5030 Water MS
LCS Dup 18051244-BSD1
Prepared 16-May-08 Analyzed 17-May-
Chloromethane 18 1-91 20 273
Dibromochloromethane 174 1-91 20 53- 149
Dichlorobenzene 20 1-91 20 100 18- 190
Dichlorobenzene 18 1-91 20 59- 156
Dichlorobenzene 18 1-91 20 18- 190
Dichloroethane 18 1-91 20 59- 155
Dichloroethane 19 1-91 20 49- 155
Dichloroethene 16 1-91 20 70- 130
cis- Dichloroethene 16 1-91 20 70- 130
trans- Dichloroethene 15 1-91 20 54- 156
Dichloropropane 17 1-91 20 210
cis- Dichloropropene 164 IJgl 20 227
trans- 1 Dichloropropene 164 I-gl 20 17- 183
Etlwlbenzene 18 IJgl 20 37- 162
Hexanone (MBK) 124 QC2 IJgl 20 70- 130
Methyl tert-butyl ether 184 1J91 20 70- 130
Methyl- pentanone (MIBK) 17 IJgl 20 70- 130
Methylene chloride 16 IJgl 20 221
Styrene 16 IJgl 20 70- 130
2- Tetrachloroethane 19 IJgl 20 46- 157
Tetrachloroethene 15 IJgl 20 64- 148
Toluene 17 IJgl 20 70- 130
1- Trichloroethane 19 1-91 20 52- 162
2- Trichloroethane 16 IJgl 20 52- 150
Trichloroethene 15 IJgl 20 71- 157
Trichlorofluoromethane (Freon 11) 17 IJgl 20 17- 181
Vinyl chloride 19 IJglI 20 251
p-Xylene 37 1J91 40 70- 130
Xylene 20 IJgl 20 100 70- 130
Surrogate 4-Bromofluorobenzene 51 IJgl 50 104 70- 130
Surrogate Toluene- 4B gl 50 70- 130
Surrogate 1 0ichloroethane- 53 IJgl 50 106 70- 130 Surrogate Oibromofluoromethane 50 1J9i 50 102 70- 130
Matrix S ike B051244-MS1 Source SA7B629shy
Prepared 16-May-08 Analyzed 17-May-
Benzene 18 20 BRL 70- 130IJgl
Bromodichloromethane 19 IJgl 20 BRL 35- 155
Bromoform 18 IJgl 20 BRL 45- 169
Bromomethane 16 IJgl 20 BRL 242
Carbon tetrachloride 21 IJgl 20 BRL 106 70- 140
Chlorobenzene 18 IJgl 20 BRL 70- 130
Chloroethane 16 IJgl 20 BRL 14-230
Chloroform 18 IJgl 20 BRL 51- 138
Chloromethane 19 IJgl 20 BRL 273
Dibromochloromethane 17 IJgl 20 BRL 53- 149
1 Dichlorobenzene 22 IJgl 20 BRL 112 18- 190
1 Dichlorobenzene 22 IJgl 20 BRL 110 59-156
1 Dichlorobenzene 21 IJgl 20 BRL 109 18- 190
1- Dichloroethane 19 IJgl 20 BRL 59- 155
1 Dichloroethane 18 IJgl 20 BRL 49- 155
This laboratory report is 110t mUd without an authorized signature on the covel page
Reportble Detection Limit BRL = Below Reporting Limit Page It of25
Volatile Organic Compounds - Quality Control
p
Spike Source REC RPD
Result REC imits RPD LimitAnalyte(s) Result Flag Units RDL Level
Batch 8051244 - SW846 5030 Water MS
Matrix ike S051244-MS1 Source SA7B629shy
Prepared 16-May-08 Analyzed 17-Mayshy
17 20 BRL 70- 130 1- Dichloroethene IJgl
16 20 BRL 54- 156trans- 1 Dichloroethene IJgl
21020 BRL1 Dichloropropane 17 1J91
cis- 1 Dichloropropene 17 IJgl 20 BRL 227
17- 183trans- 1 Dichloropropene 184 1J91 20 BRL
20 20 BRL 103 37- 162Ethylbenzene IJgl
15 20 BRL 221Methylene chloride IJgl
20 BRL 46- 1572- Tetrachloroethane 19 1J91
20 BRL 64- 148Tetrachloroethene 18 1J91
BRL 70- 130Toluene 18 1J91 20
105 52-1621- Trichloroethane 211 IJgl 20 BRL
18 20 BRL 52- 1502- Trichloroethane IJgl
17 20 BRL 71- 157Trichloroethene 1J91
20 BRL 17- 181Trichloroluoromethane (Freon 11) 194 IJgl
20 BRL 103 251Vinyl chloride 20 IJgl
102 70- 130Surrogate 4-Bromofluorobenzene 50 IJgl 50 50 70- 130Surrogate Toluene- 49 1J91
56 50 112 70- 130Surrogate 1 Dichloroethane- IJgl
50 100 70- 130Surrogate Dibromofluoromethane 50 IJgl
Matrix S ike Du S051244-MSD1 Source SA7S629shy
Prepared 16-May-08 Analyzed 17-Mayshy
18 20 BRL 70- 130Benzene IJgl
18 20 BRL 35- 155Bromodichloromethane IJgl
17 20 BRL 45- 169Bromoform IJgl
20 BRL 242Bromomethane 17 IJgl
20 BRL 103 70- 140Carbon tetrachloride 20 IJgl
18 20 BRL 70- 130Chlorobenzene 1J91
14-230Chloroethane 16 IJgl 20 BRL
20 51- 138Chloroform 184 IJgl BRL
Chloromethane 19 1J91 20 BRL 273
18 20 BRL 53- 149Dibromochloromethane 1J91
20 BRL 117 18- 190Dichlorobenzene 234 IJgl
20 BRL 112 59- 156Dichlorobenzene 22 IJgl
BRL 108 18- 190Dichlorobenzene 21 1J91 20
20 59- 1551 Dichloroethane 19 IJgl BRL
18 20 BRL 49- 155Dichloroethane IJgl
16 20 BRL 70- 130Dichloroethene IJgl
20 BRL 54- 156trans- Dichloroethene 154 1J91
20 BRL 210Dichloropropane 17 IJgl
0420 BRL 227cis- Dichloropropene 17 IJgl
17- 183trans- Dichloropropene 17 1J91 20 BRL
BRL 37- 162Ethylbenzene 20 1J91 20 102
Methylene chloride 15 IJgl 20 BRL 221
20 BRL 46- 1572- Tetrachloroethane 192 IJgl
20 BRL 64- 148 04Tetrachloroethene 18 IJgl
BRL 70- 130Toluene 184 1J91 20
52- 1621- Trichloroethane 20 IJgl 20 BRL 104
17 20 BRL 52- 1502- Trichloroethane IJgl
17 20 BRL 71- 157Trichloroethene IJgl
20 BRL 17-181Trichlorofluoromethane (Freon 11) 19 IJgl
This laboratory report is IIOt valid without all authorized sigllllture 011 the cover page
Page 12 of25 Reportble Detection Limit BRL = Below Reporting Limit
Semivolatile Organic Compounds by GCMS - Quality Control
Analyte(s)
Batch 8051216 - SW846 3510C
Blank 8051216-BLK1
Prepared amp Analyzed 16-May-
Isophorone
Methylnaphthalene
Methylphenol
3 amp 4-Methylphenol
Naphthalene
Nitroaniline
Nitroaniline
Nitroaniline
Nitrobenzene
Nitrophenol
Nitrophenol
Nitrosodimethylamine
N- N itrosodi-n-pro pyla mine
N itrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Pyridine
1 24-Trichlorobenzene
24 5- Trichlorophenol
246- Trichlorophenol
Surrogate 2-Fuorobipheny Surrogate 2-Fuoropheno Surrogate Nitrobenzene-Surrogate PhenoshySurrogate Terpheny-d4 Surrogate 6- Tribromopheno
LCS B051216-BS1
Prepared amp Analyzed 16-May-
Acenaphthene
Acenaphthylene
Aniline
Anthracene
AzobenzenelDi phenyld lazine
Benzidine
Benzo (a) anthracene
Benzo (a) pyrene
Benzo (b) fluoranthene
Benzo (g i) perylene
Benzo (k) fluoranthene
Benzoic acid
Benzyl alcohol
B is(2-chloroethoxy)methane
B i s (2-ch loroethyl)eth e r
Bis(2-ch loroisopropyl) ether
B is(2-ethy Ih exyl) phtha late
Bromophenyl phenyl ether
Butyl benzyl phthalate
Carbazole
Spike Source REC RPD
Result Flag Units RDL Level Result REC Limits RPD Limit
BRL gl
BRL gl
BRL gl
BRL gl 10
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gll
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
370 gl 50 30- 130 40 gl 50 15- 110 39 gl 50 30- 130 43 gl 50 15- 110 36 gl 50 30- 130 40 gl 50 15- 110
41 gl 50 40- 140
43 gI 50 40- 140
41 gl 50 40- 140
38 gl 50 40- 140
45 gl 50 40- 140
49 gl 50 153
41 gl 50 40- 140
43 gl 50 40- 140
41 gl 50 40- 140
41 gll 50 40- 140
45 gl 50 40- 140
32 gl 50 12- 149
41 gl 50 40- 140
39 gl 50 40- 140
384 gl 50 40- 140
47 gl 50 40- 140
47 gl 50 40- 140
40 gl 50 40- 140
47 gI 50 40- 140
56 gI 50 112 200
This laboratory report is lIot valid witllOut a1l authorized sigllature 011 the coverpage
Reportble Detection Limit BRL = Below Reporting Limit Page 15 of25
Semivolatile Organic Compounds by GCMS - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051216 - SW846 3510C
LCS 8051216-BS1
Prepared amp Analyzed 16-Mayshy
50 30- 1304 -C hloro-3-methylphenol 42 IJgl
40- 140Chloroaniline 39 IJgl 50
Chloronaphthalene 37 IJgl 50 40- 140
Chlorophenol 37 IJgl 50 30- 130
50 40- 140
40- 140
Chlorophenyl phenyl ether 45 IJgl
Chrysene 43 IJgl 50
Dibenzo (a h) anthracene 43 IJgl 50 40- 140
Dibenzofuran IJgl38 50 40- 140
50 40- 1401 Dichlorobenzene 35 IJgl
40- 1401 Dichlorobenzene 264 IJgl 50
40- 1401 Dichlorobenzene 434 IJgl 50
58 50 116 40- 1403 - Dichlorobenzidine IJgl
50 30- 130
40- 140 24-Dichlorophenol 38 IJgl
Diethyl phthalate 484 IJgl 50
50 40- 140Dimethyl phthalate 464 IJgl
Dlmethylphenol 39 IJgl 50 30- 130
DI-n-butyl phthalate 44 IJgll 50 40- 140
30- 130 6-Di nitro- 2-methylphenol 38 1J91 50
30- 130Dinltrophenol 36 1J91 50
42 50 40- 14024-Dlnitrotoluene 1J91
Dlnitrotoluene 1J9141 50 40- 140
Di-n-octyl phthalate 52 IJgl 50 104 40- 140
40- 140Fluoranthene 40 IJgl 50
Fluorene 41 IJgl 50 40- 140
39 50 40- 140Hexachlorobenzene IJgl
50 40- 140Hexachlorobutadiene 40 IJgl
40- 140Hexach lorocyclopentad iene 294 IJgl 50
40 50 40- 140Hexachloroethane IJgl
42 50 40-140Indeno (1 3-cd) pyrene IJgl
50 40- 140Isophorone 40 IJgl
40- 140Methylnaphthalene 394 IJgl 50
40- 140Methylphenol 39 IJgl 50
40 10 50 40- 1403 amp 4-Methylphenol IJgl
37 50 40-140Naphthalene IJgl
50 40-140Nitroaniline 39 IJgl
Nitroaniline 51 IJgl 50 102 40- 140
48 50 40- 140Nltroaniline 1J91
50 40- 140Nitrobenzene 40 IJgl
30- 130Nitrophenol 36 IJgl 50
40 IJgl 50 30- 130Nitrophenol 40- 140Nitrosodimethylamine 32 1J91 50
50 40-140N- N itrosodi-n-propyla mine 46 IJgl
40- 140N itrosodi phenyla ml ne 44 IJgl 50
41 IJgl 50 30- 130Pentachlorophenol 40- 140Phenanthrene 38 IJgl 50
50 30- 130Phenol 38 IJgl
40- 140Pyrene 424 1J91 50
40- 140Pyridine 294 1J91 50
40- 14024- Trichlorobenzene 364 IJgl 50
This laboratory report is not mlid without an authorized signature 011 the cover page
Page 16 of25 Reportble Detection Limit BRL = Below Reporting Limit
Semivolatie Organic Compounds by GCMS - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
BMch 8051216 - SW846 3510C
LC5 8051216-851
Prepared amp Analyzed 16-Mayshy
24 5- Trichlorophenol 404 gl 50 30- 130
246- Trichlorophenol 42 gl 50 30- 130
Surrogate 2-Fluorobiphenyl 29 gl 50 30- 130
Surrogate 2-Fluorophenot 27 gl 50 15- 110
Surrogate Nitrobenzene- 30 gl 50 30- 130
Surrogate Phenol- 29 gl 50 15- 110
Surrogate Terpheny-d4 30 gl 50 30- 130
Surrogate 6- Tribromopheno 324 gl 50 15- 110
This laboratory report is lIot valid without all authorized sigllature 011 tlle cover page
Reportble Detection Limit BRL = Below Reporting Limit Page 17 of25
Semivolatie Organic Compounds by GC - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051106 - SW846 3510C
Blank S051106-BLK1
Prepared amp Analyzed 15-Mayshy
Aroclor- 1016 BRL gI 0200
Aroclor- 1016 (2C) BRL gI 0200
Aroclor- 1221 BRL gI 0200
Aroclor- 1221 (2C) BRL gI 0200
Aroclor- 1232 BRL gI 0200
Aroclor- 1232 (2Cj BRL gI 0200
Aroclor- 1242 BRL gI 0200
Aroclor-1242 (2C) BRL gI 0200
Aroclor- 1248 BRL gI 0200
Aroclor- 1248 (2C) BRL gI 0200
Aroclor- 1254 BRL gI 0200
Aroclor- 1254(2Cj BRL gI 0200
Aroclor- 1260 BRL gI 0200
Aroclor- 1260 (2C) BRL gI 0200
Aroclor- 1262 BRL gI 0200
Aroclor- 1262 (2C) BRL gI 0200
Aroclor-1268 BRL gI 0200
Aroclor- 1268 (2C) BRL gI 0200
Surrogate Decachlorobiphenyl (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0231 0224 0194 0191
gI
gI
gI
gI
0200 0200 0200 0200
116 112
30- 150 30- 150 30- 150 30- 150
LC5 8051106-B51
Prepared 15-May-08 Analyzed 16-May-08
Aroclor- 1016 265 gI 0200 250 106 50- 114
Aroclor- 1 016 (2C) 240 gI 0200 250 50- 114
Aroclor- 1260 0269 gI 0200 250 107 40- 127
Aroclor-1260 (2Cj 270 gI 0200 250 108 40- 127
Surrogate Decachlorobiphenyl (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0225 0224 0188 0183
gI
gI
gI
gI
0200 0200 0200 0200
113 112
30- 150 30- 150 30- 150 30- 150
LC5 DUD rS051106-B5D1
Prepared 15-May-08 Analyzed 16-Mayshy
Aroclor- 1016 262 gl 0200 250 105 50- 114
Aroclor-1 016 (2Cj 241 gI 0200 250 50- 114
Aroclor- 1260 277 gI 0200 250 111 40- 127
Aroclor- 1260(2Cj 0260 gI 0200 250 104 40- 127
Surrogate Decachlorobipheny (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0238 0218 0189 0181
gI
gI
gI
gI
0200 0200 0200 0200
119 109
30- 150 30- 150 30- 150 30- 150
This laboratory report is lot valid without (II authorized sigllature 01 the cover page
Page 18 of25 Reportable Detection Limit BRL = Below Reporting Limit
Extractable Petroleum Hydrocarbons - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051102 - SW846 3510C
Blank 8051102-BLK1
Prepared 15-May-08 Analyzed 19-Mayshy
Non-polar material (SGT- HEM) BRL m91
LC8 8051102-B81
Prepared 15-May-08 Analyzed 19-Mayshy
Non-polar material (SGT- HEM) 184 m91 21 81 904
This laboratory report is not valid without an authorized signature 011 the cover page
Page 19 of25 Reportable Detection Limit BRL = Below Reporting Limit
Soluble Metals by EPA 200 Series Methods - Quality Control
Analyte(s) Result Flag Units RDL
Spike
Level
Source
Result REC
REC
Limits RPD
RPD
Limit
Batch 8051150 - EPA 200 Series
Blank 8051150-BLK1
Prepared amp Analyzed 21-May-
Iron
Zinc
Selenium
Nickel
Chromium
Copper
Arsenic
BRL
BRL
BRL
BRL
BRL
BRL
BRL
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0150
0050
0150
0050
0050
0050
0040
LCS 8051150-BS1
Prepared amp Analyzed 21-May-
Selenium
Zinc
Iron
Nickel
Chromium
Arsenic
Copper
123
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0150
0050
0150
0050
0050
0040
0050
103
105
101
100
85- 115
85- 115
85- 115
85- 115
85- 115
85-115
85- 115
licate B051150-DUP1 Source SA7B602shy
Prepared amp Analyzed 21-May-
Iron
Zinc
Selenium
Nickel
Copper
Chromium
Arsenic
17
0162
BRL
0015
0017
BRL
0450
QR8
mgl
mgl
mgl
mgl
mgl
mgl
mgi
0150
0050
0150
0050
0050
0050
0040
184
0186
BRL
0014
0023
BRL
0468
Matrix S ike 8051150-MS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Iron
Selenium
Nickel
Zinc
Copper
Chromium
Arsenic
19 QM2 mgl
mgll
mgl
mgl
mgl
mgl
mgl
0150
0150
0050
0050
0050
0050
0040
125
184
BRL
0014
0186
0023
BRL
0468
104
105
102
70- 130
70- 130
70-130
70- 130
70- 130
70-130
70- 130
Post S ike 8051150-PS1 Source SA78602shy
Prepared amp Analyzed 21-May-
Zinc
Iron
Selenium
Nickel
Copper
Arsenic
Chromium
18 QM2
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0050
0150
0150
0050
0050
0040
0050
0186
184
BRL
0014
0023
0468
BRL
104
104
101
85- 115
85- 115
85- 115
85-115
85-115
85- 115
85-115
Batch 8051152 - EPA200SW7000 Series
Blank B051152-BLK1
Prepared amp Analyzed 21-May-
Mercury BRL mgl 00020
This laboratory report is IIOt valid witllOut all authorized sigllature 011 the coverpage
Page 20 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Soluble Metals by EPA 200 Series Methods - Quality Control
Analyte(s) Result Flag Units RDL
Spike
Level
Source
Result REC
REC
Limits RPD
RPD
Limit
Batch 8051152 - EPA200SW7000 Series
LCS B051152-BS1
Prepared amp Analyzed 21-May-
Mercury 00576 m91 00020 00500 115 85- 115
licate B051152-DUP1 Source SA78602-01
Prepared amp Analyzed 21-May-
Mercury BRL m91 00020 BRL
Matrix S ike 8051152-MS1 Source SA78602shy
Prepared amp Analyzed 21-May-
Mercury 00632 OM m91 00020 00500 BRL 126 75- 125
Post S ike 8051152-PS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Mercury 00624 OC1 m91 00020 00500 BRL 125 85- 115
Batch 8051249 - 2008No digestion
Blank 8051249-BLK1
Prepared amp Analyzed 21-May-
Lead
Antimony
Cadmium
Silver
BRL
BRL
BRL
BRL
m91
m91
m91
m91
0002
0002
0002
0002
LCS B051249-BS1
Prepared amp Analyzed 21-May-
Antimony
Lead
Silver
Cadmium
143
145 OC2
m91
m91
m91
m91
0050
0050
0050
0040
103
115
107
116
85- 115
85- 115
85- 115
85- 115
licate 8051249-DUP1 Source SA7B602shy
Prepared amp Analyzed 21- May-
Lead
Antimony
Cadmium
Silver
0009
0002
00005
00002
ORB
m91
m91
m91
m91
0002
0002
0002
0002
0011
0003
00005
00003
Matrix S ike 8051249-MS1 Source SA78602shy
Prepared amp Analyzed 21- May-
Lead
Antimony
Cadmium
Silver
142
m91
m91
m91
m91
0050
0050
0040
0050
0011
0003
00005
00003
111
101
114
102
70- 130
70-130
70c130
70- 130
Post S ike 8051249-PS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Antimony
Cadmium
Silver
38
OC2
m91
m91
m91
0050
0040
0050
125
0003
00005
00003
110
121
109
85- 115
85- 115
85- 115
This laboratory report is flOt valid IVithout all authorized signature 011 the cOIer page
Reportable Detection Limit BRL Below Reporting Limit Page 21 of 25
General Chemistry Parameters - Quality Control
Spike Source REC RPD
Analyte( s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051049 - General Preparation
Blank S051 049-BLK1
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
Blank S051049-BLK2
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
Blank S051 049-BLK3
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
LCS S051049-BS1
Prepared amp Analyzed 14-May-
Total Residual Chlorine 046 mgl 020 0500 90- 110
LCS S051049-BS2
Prepared amp Analyzed 14-May-
Total Residual Chlorine 047 mgl 020 0500 90- 110
LCS S051049-BS3
Prepared amp Analyzed 14-May-
Total Residual Chlorine 054 mgl 020 0500 108 90-110
licate B051049-DUP1 Source SA7S544shy
Prepared amp Analyzed 14-May-
Total Residual Chlorine 012 mgl 020 010
licate S051049-DUP2 Source SA7S602-01
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020 BRL
Matrix S ike 8051049-MS1 Source SA78544-01
Prepared amp Analyzed 14-May-
Total Residual Chlorine 065 mgl 020 0500 010 110 80- 120
Matrix S ike 8051049-MS2 Source SA7B602shy
Prepared amp Analyzed 14-May-
Total Residual Chlorine mgl 500 125 BRL 108 80- 120
Reference 8051 049-SRM1
Prepared amp Analyzed 14-May-
Total Residual Chlorine 100 mgl 020 0967 103 85-115
Batch 8051094 - General Preparation
Blank 8051094-BLK1
Prepared amp Analyzed 14 May-
Hexavalent Chromium (soluble) BRL mgl 005
Blank 8051 094-BLK2
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) BRL mgl 005
LCS 8051094-BS1
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) 054 mgl 005 90- 110
licate 8051094-DUP1 Source SA78602-01
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) BRL mgl 125 BRL
Thi laboratory report is not valid without all authorized sigllature 011 the cover page
Page 22 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Page 18
Volatie Organic Compounds - Quality Control
p (
Spike Source REC RPD
RDL Level Result REC Limits RPD Limit Analyte(s) Result Flag Units
Batch 8051244 - SW846 5030 Water MS
Matrix S ike Du 8051244-MSD1 Source SA78629shy
Prepared 16-May-08 Analyzed 17-May-BRL 106 251
Vinyl chloride 21 gl 20
101 70- 130 Surrogate 4-Bromofluorobenzene 50 gl 50
70- 13049 gl 50 111 70- 130
Surrogate Toluene-Surrogate 1 Dichloroethane- 55 gl 50
50 70- 130494 glSurrogate Dibromofluoromethane
Microextractable Organic Compounds - Quality Control
Spike Source REC RPD
Flag Units RDL Level Result REC Limits RPD Limit Analyte(s) Result
Batch 8051105 - SW846 3510C
Blank 8051105-BLK
Prepared amp Analyzed 15-May-
BRL gl 01001 Dibromoethane (ED B)
LCS 8051105-BS1
Prepared amp Analyzed 15-Mayshy50- 1500770 gl 0100 100
licate 8051105-DUP1 Source SA7B583shy
Prepared amp Analyzed 15-May-
BRL gl 0100 BRL
1 Dibromoethane (EDB)
1 Dibromoethane (EDB)
This laborntOlY report is not valid without an authorized signature 011 the cover page
Page 13 of2S Reportable Detection Limit BRL = Below Reporting Limit
Sam le Identification Client Pro ect Matrix Collection DateTime ReceivedMWshy
2920-96- Ground Water 13-May-081030 14-May-SA 78602shy
CAS No Analyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Volatile Organic Compounds
Volatile Or anic Com ounds b GCMS
Prepared by method SW846 5030 Water MS
123-91- Dioxane BRL 1-91 200 EPA 624 16-May-08 17-May-08 8051244
994-05-8 Ter-amyl methyl ether BRL 1-911 20
755- Tert-Butanoll butyl alcohol BRL 1-91 200
67-B4- Acetone BRL 1-91 400
71-43- Benzene BRL 1-91 20
75-27-4 Bromodichloromethane BRL 1-91 20
75-25- Bromoform BRL 1-91 20
74-83- Bromomethane BRL 1-91 40
78-93- Butanone (MEK) BRL 1-91 200
56-23- Carbon tetrachloride BRL 1-91 20
108-90- Chlorobenzene BRL 1-91 20
75-00- Chloroethane BRL 1-91 40
676- Chloroform BRL 1-91 20
74-87- Chloromethane BRL 1-91 40
124-48- Dibromochloromethane BRL 1-91 20
95-50- Dichlorobenzene BRL 1-911 20
541-73- Dichlorobenzene BRL 1-91 20
106-46- Dichlorobenzene BRL 1-91 20
75-34- 1- Dichloroethane BRL 1-91 20
107-06- Dichloroethane BRL 1-91 20
75-35-4 1- Dichloroethene BRL 1-91 20
156-59 cis- Dichloroethene BRL 1-91 20
156-60- trans- Dichloroethene BRL 1-91 20
78-87- 2- Dichloropropane BRL 1-91 20
10061-01-5 cis- Dichloropropene BRL 1-91 20
10061-02-B trans- Dichloropropene BRL 1-91 20
100-41-4 Ethylbenzene 411 1-911 20
591-78-B BRL 200Hexanone (MBK) 1-91
1634-04 -4 Methyl tert-butyl ether BRL 1-91 20
108-10- Methyl- pentanone (MIBK) BRL 1-91 200
75-09- Methylene chloride BRL 1-91 200
100-42- Styrene BRL 1-91 20
79-34- 1 Tetrachloroethane BRL 1-91 20
127- 18-4 T etrachloroethene BRL 1-91 20
108-88- Toluene BRL 1-91 20
71-55 1- Trichloroethane BRL 1-91 20
79-00- 2- Trichloroethane BRL 1-91 20
79-01-B Trichloroethene BRL 1-91 20
759-4 Trichlorofluoromethane (Freon 11) BRL 1-91 20
75-01-4 Vinyl chloride BRL 1-91 20
179601-23-1 m Xylene 390 1-91 40
95-47 Xylene 82 1-91 20
Surrogate recoveries 460-00- Bromofluorobenzene 70- 130
2037-26- Toluene- 100 70- 130
17060-07-0 1 Dichloroethane- 111 70- 130
1868-53- Dibromofluoromethane 70- 130
Microextractable Organic Compounds
106-93-4 1 Dibromoethane (EDB) BRL 1-91 0100 EPA 504 15-May- 15-May-08 8051105
Semivolatile Organic Compounds by GCMS
This laboratory report is not valid without all autllOrized signature 011 the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page 5 of 25
Sam le Identification Client Pro ect Matrix Collection DateTime Received
MWshy2920-96- Ground Water 13-May-081030 14-May-
SA 78602shy
CAS No Analyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Semivolatie Organic Compounds by GCMS
Semi volatile Or anic Com ounds b EPA 625
Prepared by method SW846 3510C 50 EPA 625 16-May- 19-May-08 805121683-32- Acenaphthene BRL IJgl
208-96-8 Acenaphthylene BRL IJgl 50
62-53- BRL IJgll 50Aniline
120- 12- Anthracene BRL 1J91 50
103-33- AzobenzenefDiphenyldiazine BRL IJgl 50
92-87 - Benzidine BRL IJgl 50
56-55- Benzo (a) anthracene BRL 1J91 50
50-32 - Benzo (a) pyrene IJglBRL 50
205-99- Benzo (b) fluoranthene BRL IJgl 50
191-24- Benzo (g i) perylene BRL IJgl 50
50207-08- Benzo (k) fluoranthene BRL IJgl
65-85 Benzoic acid BRL 1J91 50
100-51-6 Benzyl alcohol 1J91BRL 50
50111-91- Bis(2-chloroethoxy)methane BRL 1J91
111-4-4 Bis(2-chloroethyl)ether BRL IJgl 50
501 08-60- Bis(2-chloroisopropyl)ether BRL IJgl
117-81- Bis(2-ethylhexyl)phthalate BRL 1J91 50
101-55- Bromophenyl phenyl ether BRL IJgl 50
5085-68- Butyl benzyl phthalate BRL IJgl
5086-74- Carbazole BRL IJgl
5059-50- C hloro-3-methylphenol BRL IJgl
106-47- Chloroaniline BRL IJgl 50
91-58- Chloronaphthalene IJglBRL 50
5095-57 - Chlorophenol BRL 1J91
507005-72- Chlorophenyl phenyl ether BRL IJgl
216-01- Chrysene tJ91BRL 50
5053-70- Dibenzo (a h) anthracene BRL IJgl
50132-64- Dibenzofuran BRL IJgl
95-50- Dichlorobenzene IJglBRL 50
541-73- 13- Dichlorobenzene BRL IJgl 50
106-46- Dichlorobenzene 1J91BRL 50
5091-94- 3 - Dichlorobenzidine BRL IJgl
120-83- Dichlorophenol BRL IJgl 50
84-66- Diethyl phthalate BRL IJgl 50
131-11- Dimethyl phthalate BRL IJgll 50
105-67- Dimethylphenol BRL 1J91 50
5084-74- Di-n- butyl phthalate BRL 1J91
534-52 - Dinitro-2-methylphenol BRL IJgl 50
51-28- Dinitrophenol IJglBRL 50
50121-14- Dinitrotoluene BRL 1J91
606-20- Dinitrotoluene IJglBRL 50
50117-84-0 Di-n-octyl phthalate BRL IJgl
206-44-0 Fluoranthene 1J91BRL 50
BRL 50
50 86-73- Fluorene IJgi
118-74- Hexachlorobenzene BRL 1J91
87-68- Hexachlorobutadiene 1J91BRL 50
5077-47-4 Hexachlorocyclopentadiene BRL IJgl
67-72- Hexachloroethane IJglBRL 50
50193-39- Indeno (1 3-cd) pyrene BRL IJgl
5078-59- Isophorone BRL IJgl
Tfls laboratory report is not valid without all authorized signature 011 the coverpage
Page 6 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Sam le Identification Client Pro ect Matrix Collection DateTime ReceivedMWshy
2920-96- Ground Water I3-May-081030 14-May-SA 78602shy
CAS No Analyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Semivolatile Organic Compounds by GCMS
Semi volatile Or anic Com ounds b EPA 625
Prepared by method SW846 3510C
91-57 -6 Methylnaphthalene 367 1-91 50 EPA 625 16-May- 19-May-08 8051216
95-48- Methylphenol BRL 1-91 50
108-39-4 3 amp 4-Methylphenol BRL I-gl 100 106-44shy91-20- Naphthalene 247 1-91 50
88-74-4 Nitroaniline BRL 1-91 50
99-09- Nitroaniline BRL 1-91 50
100-01-6 Nitroaniline BRL 1-91 50
98-95- Nitrobenzene BRL 1-91 50
88-75- Nitrophenol BRL 1-91 50
100-02- Nitrophenol BRL 1-91 50
62-75- Nitrosodimethylamine BRL 1-91 50
621-64- N- Nitrosodi-n-propylamine BRL 1-91 50
86-30-6 Nitrosodiphenylamine BRL 1-91 50
87 -86- Pentachlorophenol BRL 1-91 50
85-0- Phenanthrene BRL 1-91 50
108-95- Phenol BRL 1-91 50
129-00-0 Pyrene BRL 1-91 50
110-86- Pyridine BRL 1-91 50
120-82- 4- Trichlorobenzene BRL 1-91 50
95-95- 5- Trichlorophenol BRL 1-91 50
88-06- 6- T richlorophenol BRL 1-91 50
Surrogate recoveries
321-60- Fluorobipheny 30- 130
367- 12- Fuorophenol 15- 110
4165-60- Nitrobenzene- 30- 130
4165-62- Pheno- 15- 110
1718-51- Terpheny-d4 30- 130
118- 79- 6- Tribromophenol 15- 110
Semivolatile Organic Compounds by GC
Pol chlorinated Bi hen ls b EPA 608
Prepared by method SW846 3510C
12674- 11-2 Aroclor- 1016 BRL 1-91 0650 EPA 608 15- May- 16-May-08 8051106
11104-28-2 Aroclor-1221 BRL IJgl 0650
11141-16-5 Aroclor- 1232 BRL 1-91 0650
53469-21-9 Aroclor- 1242 BRL 1-91 0650
12672-29-6 Aroclor- 1248 BRL 1-91 0650
11097-69-1 Aroclor- 1254 BRL 1-91 0650
11096-82-5 Aroclor -1260 BRL 1-91 0650
37324-23-5 Aroclor-1262 BRL 1-91 0650
11100-14-4 Aroclor-1268 BRL IJgl 0650
Surrogate recoveries
2051-24- Decachlorobipheny (Sr) 105 30- 150
10386-84-2 4 DB-Octafluorobiphenyl (Sr) 30- 150
Extractable Petroleum Hydrocarbons
mgl EPA 1664 Rev A 15-May- 19-May-08 8051102Non-polar material (SGT- HEM)
Soluble Metals by EPA 2006000 Series Metbods
Field Filtered NA EPA 200 73005A 15- May- 15-May-08 8051192Filtration
Soluble Metals by EPA 200 Series Methods
7440-22-4 Silver BRL mgl 0002 EPA 200 21-May- 27- May-08 8051249
This laboratory report is IlOt mlid without (II authorized signature on the cover page
Reportble Detection Limit BRL = Below Reporting Limit Page 7 of 25
Sam le Identification MW-
Client Pro ect 2920-96shy
Matrix Ground Water
Collection DateTime 13-May-08 1030
Received 14-May-
SA 78602shy
CAS No A nalyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Soluble Metals by EPA 200 Series Methods
7440-38shy Arsenic 0468 mg1 0040 EPA 200 21-Mayshy 21-May-08 80511 50
7440-43shy Cadmium BRL mg1 0002 EPA 200 21-May-088051249
7440-47shy Chromium BRL mg1 0050 EPA 200 21-May-088051150
7440-50-8 Copper BRL mg1 0050
7439-89-6 Iron 184 mg1 0150
7439-97-6 Mercury BRL mg1 00020 EPA 245 17470A 21-May-088051152
7440-02-0 Nickel BRL mg1 0050 EPA 200 21-May-088051150
7439-92shy Lead 0011 mg1 0002 EPA 200 21-May-088051249
7440-36-0 Antimony 0003 mg1 0002
7782-49shy Selenium BRL mg1 0150 EPA 200 21-May-08 8051150
7440-66-6 Zinc 0186 mgl 0050
General Chemistry Parameters
Filtration Completed NA Varies 14-Mayshy 14-May-08 8051095
18540-29-9 Hexavalent Chromium (soluble) BRL HT2 mg1 125 SM3500CrDI796A 14-Mayshy 14-May-08 8051094 R01 2013 2016
57-12shy Cyanide (total) BRL mg1 0100 EPA 3354 19-Mayshy 19-May-088051374
7782-50shy Total Residual Chlorine BRL CIHT mg1 500 Hach 8167 14-Mayshy 14-May-08 8051049 R01 1900 2001
Total Suspended Solids 580 mg1 25 SM2540D 16-Mayshy 16-May-08 8051275
This lahomtOlY report is not valid without an authorized signature on the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page 8 of 25
Volatie Organic Compounds - Quality Control
Analyte( s)
Batch 8051244 - SW846 5030 Water MS
Blank 8051244-BLK1
Prepared 16-May-08 Analyzed 17-May-
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromochloromethane
1 Dichlorobenzene
1 Dichlorobenzene
1 Dichlorobenzene
1-Dichloroethane
1 Dichloroethane
1 1-Dichloroethene
cis- Dichloroethene
trans- 1 Dichloroethene
1 Dichloropropane
cis- 1 Dichloropropene
trans- 1 Dichloropropene
Ethylbenzene
Hexanone (MBK)
Methyl tert-butyl ether
Methyl- pentanone (MIBK)
Methylene chloride
Styrene
2- Tetrachloroethane
Tetrachloroethene
Toluene
1- Trichloroethane
2- Trichloroethane
Trichloroethene
Trichlorofluoromethane (Freon 11)
Vinyl chloride
p-Xylene
Xylene
Surrogate 4-Bromofluorobenzene Surrogate Toluene-
Surrogate 1 Dichloroethane-Surrogate Dibromofluoromethane
LCS B051244-BS1
Prepared 16-May-08 Analyzed 17 -May-
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Spike Source REC RPD
Result Flag Units RDL Level Result REC Limits RPD Limit
BRL gl 20
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl 10
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gll
BRL gi
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl 10
BRL gll
BRL gll 10
BRL gl 10
BRL gll
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
41 gl 50 70- 130 49 gl 50 70- 130 59 gl 50 119 70- 130 52 gl 50 105 70- 130
QC2 jgl 20 70- 130
18 jgl 20 70- 130
192 jgl 20 35- 155
18 jgl 20 45- 169
19 jgl 20 242
This laboratOlY repol1 is lot valid without 011 authorized sigllature 011 the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page 9 of 25
Volatie Organic Compounds - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051244 - SW846 5030 Water MS
LC5 8051244B51
Prepared 16-May-08 Analyzed 17-May-
Butanone (MEK) 10 QC2 gl 20 70- 130
Carbon tetrachloride 204 gl 20 102 70- 140
Chlorobenzene 18 gl 20 70- 130
Chloroethane 164 gl 20 14-230
Chloroform 18 gll 20 51- 138
Chloromethane 21 gl 20 106 273
Dibromochloromethane 18 gl 20 53- 149
1 Dichlorobenzene 20 gl 20 104 18- 190
1 Dichlorobenzene 19 gl 20 59- 156
1 A-Dichlorobenzene 18 gl 20 18- 190
1- Dichloroethane 19 gl 20 59- 155
1 Dichloroethane 19 gl 20 49- 155
1-Dichloroethene 16 gl 20 70- 130
cis- 1 Dichloroethene 17 gl 20 70- 130
trans- 1 Dichloroethene 16 gll 20 54- 156
1 Dichloropropane 18 gl 20 210
cis- Dichloropropene 17 gl 20 227
trans- 1 Dichloropropene 17 gl 20 17- 183
Ethylbenzene 19 gl 20 37- 162
Hexanone (MBK) 124 QC2 gl 20 70- 130
Methyl tert-butyl ether 19 gl 20 70- 130
Methylshy pentanone (MIBK) 17 gl 20 70- 130
Methylene chloride 16 gl 20 221
Styrene 17 gl 20 70- 130
1 Tetrachloroethane 194 gl 20 46- 157
Tetrachloroethene 15 gl 20 64- 148
Toluene 18 gl 20 70- 130
1- Trichloroethane 20 gl 20 100 52- 162
2- Trichloroethane 18 gl 20 52- 150
Trichloroethene 17 gl 20 71- 157
Trichlorofluoromethane (Freon 11) 19 gl 20 17- 181
Vinyl chloride 21 gl 20 106 251
p-Xylene 39 gl 40 70- 130
Xylene 20 gl 20 102 70- 130
Surrogate 4-Bromofluorobenzene Surrogate Toluene-
Surrogate 1 Dichloroethane-Surrogate Dibromofluoromethane
52 49 56
49
gl
gl
gl
gl
50 50 50
50
105
112 100
70- 130 70- 130 70- 130 70- 130
LC5 DUD (8051244-B5D1
Prepared 16-May-08 Analyzed 17-May-
Acetone QC2 gl 20 70- 130
Benzene 18 gl 20 70- 130
Bromodichloromethane 18 gl 200 35- 155
Bromoform 17 gl 20 45- 169
Bromomethane 18 gl 20 242
Butanone (MEK) 11 QC2 1-91 20 70- 130
Carbon tetrachloride 20 gl 20 100 70- 140
Chlorobenzene 17 gl 20 70- 130
Chloroethane 15 1-91 20 14-230
Chloroform 18 1-91 20 51- 138
This laboratory report is aot valid without a1 authorized sig1ature 01 the cover page
Reportble Detection Limit BRL = Below Reporting Limit Page 10 of25
Volatie Organic Compounds - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051244 - SW846 5030 Water MS
LCS Dup 18051244-BSD1
Prepared 16-May-08 Analyzed 17-May-
Chloromethane 18 1-91 20 273
Dibromochloromethane 174 1-91 20 53- 149
Dichlorobenzene 20 1-91 20 100 18- 190
Dichlorobenzene 18 1-91 20 59- 156
Dichlorobenzene 18 1-91 20 18- 190
Dichloroethane 18 1-91 20 59- 155
Dichloroethane 19 1-91 20 49- 155
Dichloroethene 16 1-91 20 70- 130
cis- Dichloroethene 16 1-91 20 70- 130
trans- Dichloroethene 15 1-91 20 54- 156
Dichloropropane 17 1-91 20 210
cis- Dichloropropene 164 IJgl 20 227
trans- 1 Dichloropropene 164 I-gl 20 17- 183
Etlwlbenzene 18 IJgl 20 37- 162
Hexanone (MBK) 124 QC2 IJgl 20 70- 130
Methyl tert-butyl ether 184 1J91 20 70- 130
Methyl- pentanone (MIBK) 17 IJgl 20 70- 130
Methylene chloride 16 IJgl 20 221
Styrene 16 IJgl 20 70- 130
2- Tetrachloroethane 19 IJgl 20 46- 157
Tetrachloroethene 15 IJgl 20 64- 148
Toluene 17 IJgl 20 70- 130
1- Trichloroethane 19 1-91 20 52- 162
2- Trichloroethane 16 IJgl 20 52- 150
Trichloroethene 15 IJgl 20 71- 157
Trichlorofluoromethane (Freon 11) 17 IJgl 20 17- 181
Vinyl chloride 19 IJglI 20 251
p-Xylene 37 1J91 40 70- 130
Xylene 20 IJgl 20 100 70- 130
Surrogate 4-Bromofluorobenzene 51 IJgl 50 104 70- 130
Surrogate Toluene- 4B gl 50 70- 130
Surrogate 1 0ichloroethane- 53 IJgl 50 106 70- 130 Surrogate Oibromofluoromethane 50 1J9i 50 102 70- 130
Matrix S ike B051244-MS1 Source SA7B629shy
Prepared 16-May-08 Analyzed 17-May-
Benzene 18 20 BRL 70- 130IJgl
Bromodichloromethane 19 IJgl 20 BRL 35- 155
Bromoform 18 IJgl 20 BRL 45- 169
Bromomethane 16 IJgl 20 BRL 242
Carbon tetrachloride 21 IJgl 20 BRL 106 70- 140
Chlorobenzene 18 IJgl 20 BRL 70- 130
Chloroethane 16 IJgl 20 BRL 14-230
Chloroform 18 IJgl 20 BRL 51- 138
Chloromethane 19 IJgl 20 BRL 273
Dibromochloromethane 17 IJgl 20 BRL 53- 149
1 Dichlorobenzene 22 IJgl 20 BRL 112 18- 190
1 Dichlorobenzene 22 IJgl 20 BRL 110 59-156
1 Dichlorobenzene 21 IJgl 20 BRL 109 18- 190
1- Dichloroethane 19 IJgl 20 BRL 59- 155
1 Dichloroethane 18 IJgl 20 BRL 49- 155
This laboratory report is 110t mUd without an authorized signature on the covel page
Reportble Detection Limit BRL = Below Reporting Limit Page It of25
Volatile Organic Compounds - Quality Control
p
Spike Source REC RPD
Result REC imits RPD LimitAnalyte(s) Result Flag Units RDL Level
Batch 8051244 - SW846 5030 Water MS
Matrix ike S051244-MS1 Source SA7B629shy
Prepared 16-May-08 Analyzed 17-Mayshy
17 20 BRL 70- 130 1- Dichloroethene IJgl
16 20 BRL 54- 156trans- 1 Dichloroethene IJgl
21020 BRL1 Dichloropropane 17 1J91
cis- 1 Dichloropropene 17 IJgl 20 BRL 227
17- 183trans- 1 Dichloropropene 184 1J91 20 BRL
20 20 BRL 103 37- 162Ethylbenzene IJgl
15 20 BRL 221Methylene chloride IJgl
20 BRL 46- 1572- Tetrachloroethane 19 1J91
20 BRL 64- 148Tetrachloroethene 18 1J91
BRL 70- 130Toluene 18 1J91 20
105 52-1621- Trichloroethane 211 IJgl 20 BRL
18 20 BRL 52- 1502- Trichloroethane IJgl
17 20 BRL 71- 157Trichloroethene 1J91
20 BRL 17- 181Trichloroluoromethane (Freon 11) 194 IJgl
20 BRL 103 251Vinyl chloride 20 IJgl
102 70- 130Surrogate 4-Bromofluorobenzene 50 IJgl 50 50 70- 130Surrogate Toluene- 49 1J91
56 50 112 70- 130Surrogate 1 Dichloroethane- IJgl
50 100 70- 130Surrogate Dibromofluoromethane 50 IJgl
Matrix S ike Du S051244-MSD1 Source SA7S629shy
Prepared 16-May-08 Analyzed 17-Mayshy
18 20 BRL 70- 130Benzene IJgl
18 20 BRL 35- 155Bromodichloromethane IJgl
17 20 BRL 45- 169Bromoform IJgl
20 BRL 242Bromomethane 17 IJgl
20 BRL 103 70- 140Carbon tetrachloride 20 IJgl
18 20 BRL 70- 130Chlorobenzene 1J91
14-230Chloroethane 16 IJgl 20 BRL
20 51- 138Chloroform 184 IJgl BRL
Chloromethane 19 1J91 20 BRL 273
18 20 BRL 53- 149Dibromochloromethane 1J91
20 BRL 117 18- 190Dichlorobenzene 234 IJgl
20 BRL 112 59- 156Dichlorobenzene 22 IJgl
BRL 108 18- 190Dichlorobenzene 21 1J91 20
20 59- 1551 Dichloroethane 19 IJgl BRL
18 20 BRL 49- 155Dichloroethane IJgl
16 20 BRL 70- 130Dichloroethene IJgl
20 BRL 54- 156trans- Dichloroethene 154 1J91
20 BRL 210Dichloropropane 17 IJgl
0420 BRL 227cis- Dichloropropene 17 IJgl
17- 183trans- Dichloropropene 17 1J91 20 BRL
BRL 37- 162Ethylbenzene 20 1J91 20 102
Methylene chloride 15 IJgl 20 BRL 221
20 BRL 46- 1572- Tetrachloroethane 192 IJgl
20 BRL 64- 148 04Tetrachloroethene 18 IJgl
BRL 70- 130Toluene 184 1J91 20
52- 1621- Trichloroethane 20 IJgl 20 BRL 104
17 20 BRL 52- 1502- Trichloroethane IJgl
17 20 BRL 71- 157Trichloroethene IJgl
20 BRL 17-181Trichlorofluoromethane (Freon 11) 19 IJgl
This laboratory report is IIOt valid without all authorized sigllllture 011 the cover page
Page 12 of25 Reportble Detection Limit BRL = Below Reporting Limit
Semivolatile Organic Compounds by GCMS - Quality Control
Analyte(s)
Batch 8051216 - SW846 3510C
Blank 8051216-BLK1
Prepared amp Analyzed 16-May-
Isophorone
Methylnaphthalene
Methylphenol
3 amp 4-Methylphenol
Naphthalene
Nitroaniline
Nitroaniline
Nitroaniline
Nitrobenzene
Nitrophenol
Nitrophenol
Nitrosodimethylamine
N- N itrosodi-n-pro pyla mine
N itrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Pyridine
1 24-Trichlorobenzene
24 5- Trichlorophenol
246- Trichlorophenol
Surrogate 2-Fuorobipheny Surrogate 2-Fuoropheno Surrogate Nitrobenzene-Surrogate PhenoshySurrogate Terpheny-d4 Surrogate 6- Tribromopheno
LCS B051216-BS1
Prepared amp Analyzed 16-May-
Acenaphthene
Acenaphthylene
Aniline
Anthracene
AzobenzenelDi phenyld lazine
Benzidine
Benzo (a) anthracene
Benzo (a) pyrene
Benzo (b) fluoranthene
Benzo (g i) perylene
Benzo (k) fluoranthene
Benzoic acid
Benzyl alcohol
B is(2-chloroethoxy)methane
B i s (2-ch loroethyl)eth e r
Bis(2-ch loroisopropyl) ether
B is(2-ethy Ih exyl) phtha late
Bromophenyl phenyl ether
Butyl benzyl phthalate
Carbazole
Spike Source REC RPD
Result Flag Units RDL Level Result REC Limits RPD Limit
BRL gl
BRL gl
BRL gl
BRL gl 10
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gll
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
370 gl 50 30- 130 40 gl 50 15- 110 39 gl 50 30- 130 43 gl 50 15- 110 36 gl 50 30- 130 40 gl 50 15- 110
41 gl 50 40- 140
43 gI 50 40- 140
41 gl 50 40- 140
38 gl 50 40- 140
45 gl 50 40- 140
49 gl 50 153
41 gl 50 40- 140
43 gl 50 40- 140
41 gl 50 40- 140
41 gll 50 40- 140
45 gl 50 40- 140
32 gl 50 12- 149
41 gl 50 40- 140
39 gl 50 40- 140
384 gl 50 40- 140
47 gl 50 40- 140
47 gl 50 40- 140
40 gl 50 40- 140
47 gI 50 40- 140
56 gI 50 112 200
This laboratory report is lIot valid witllOut a1l authorized sigllature 011 the coverpage
Reportble Detection Limit BRL = Below Reporting Limit Page 15 of25
Semivolatile Organic Compounds by GCMS - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051216 - SW846 3510C
LCS 8051216-BS1
Prepared amp Analyzed 16-Mayshy
50 30- 1304 -C hloro-3-methylphenol 42 IJgl
40- 140Chloroaniline 39 IJgl 50
Chloronaphthalene 37 IJgl 50 40- 140
Chlorophenol 37 IJgl 50 30- 130
50 40- 140
40- 140
Chlorophenyl phenyl ether 45 IJgl
Chrysene 43 IJgl 50
Dibenzo (a h) anthracene 43 IJgl 50 40- 140
Dibenzofuran IJgl38 50 40- 140
50 40- 1401 Dichlorobenzene 35 IJgl
40- 1401 Dichlorobenzene 264 IJgl 50
40- 1401 Dichlorobenzene 434 IJgl 50
58 50 116 40- 1403 - Dichlorobenzidine IJgl
50 30- 130
40- 140 24-Dichlorophenol 38 IJgl
Diethyl phthalate 484 IJgl 50
50 40- 140Dimethyl phthalate 464 IJgl
Dlmethylphenol 39 IJgl 50 30- 130
DI-n-butyl phthalate 44 IJgll 50 40- 140
30- 130 6-Di nitro- 2-methylphenol 38 1J91 50
30- 130Dinltrophenol 36 1J91 50
42 50 40- 14024-Dlnitrotoluene 1J91
Dlnitrotoluene 1J9141 50 40- 140
Di-n-octyl phthalate 52 IJgl 50 104 40- 140
40- 140Fluoranthene 40 IJgl 50
Fluorene 41 IJgl 50 40- 140
39 50 40- 140Hexachlorobenzene IJgl
50 40- 140Hexachlorobutadiene 40 IJgl
40- 140Hexach lorocyclopentad iene 294 IJgl 50
40 50 40- 140Hexachloroethane IJgl
42 50 40-140Indeno (1 3-cd) pyrene IJgl
50 40- 140Isophorone 40 IJgl
40- 140Methylnaphthalene 394 IJgl 50
40- 140Methylphenol 39 IJgl 50
40 10 50 40- 1403 amp 4-Methylphenol IJgl
37 50 40-140Naphthalene IJgl
50 40-140Nitroaniline 39 IJgl
Nitroaniline 51 IJgl 50 102 40- 140
48 50 40- 140Nltroaniline 1J91
50 40- 140Nitrobenzene 40 IJgl
30- 130Nitrophenol 36 IJgl 50
40 IJgl 50 30- 130Nitrophenol 40- 140Nitrosodimethylamine 32 1J91 50
50 40-140N- N itrosodi-n-propyla mine 46 IJgl
40- 140N itrosodi phenyla ml ne 44 IJgl 50
41 IJgl 50 30- 130Pentachlorophenol 40- 140Phenanthrene 38 IJgl 50
50 30- 130Phenol 38 IJgl
40- 140Pyrene 424 1J91 50
40- 140Pyridine 294 1J91 50
40- 14024- Trichlorobenzene 364 IJgl 50
This laboratory report is not mlid without an authorized signature 011 the cover page
Page 16 of25 Reportble Detection Limit BRL = Below Reporting Limit
Semivolatie Organic Compounds by GCMS - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
BMch 8051216 - SW846 3510C
LC5 8051216-851
Prepared amp Analyzed 16-Mayshy
24 5- Trichlorophenol 404 gl 50 30- 130
246- Trichlorophenol 42 gl 50 30- 130
Surrogate 2-Fluorobiphenyl 29 gl 50 30- 130
Surrogate 2-Fluorophenot 27 gl 50 15- 110
Surrogate Nitrobenzene- 30 gl 50 30- 130
Surrogate Phenol- 29 gl 50 15- 110
Surrogate Terpheny-d4 30 gl 50 30- 130
Surrogate 6- Tribromopheno 324 gl 50 15- 110
This laboratory report is lIot valid without all authorized sigllature 011 tlle cover page
Reportble Detection Limit BRL = Below Reporting Limit Page 17 of25
Semivolatie Organic Compounds by GC - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051106 - SW846 3510C
Blank S051106-BLK1
Prepared amp Analyzed 15-Mayshy
Aroclor- 1016 BRL gI 0200
Aroclor- 1016 (2C) BRL gI 0200
Aroclor- 1221 BRL gI 0200
Aroclor- 1221 (2C) BRL gI 0200
Aroclor- 1232 BRL gI 0200
Aroclor- 1232 (2Cj BRL gI 0200
Aroclor- 1242 BRL gI 0200
Aroclor-1242 (2C) BRL gI 0200
Aroclor- 1248 BRL gI 0200
Aroclor- 1248 (2C) BRL gI 0200
Aroclor- 1254 BRL gI 0200
Aroclor- 1254(2Cj BRL gI 0200
Aroclor- 1260 BRL gI 0200
Aroclor- 1260 (2C) BRL gI 0200
Aroclor- 1262 BRL gI 0200
Aroclor- 1262 (2C) BRL gI 0200
Aroclor-1268 BRL gI 0200
Aroclor- 1268 (2C) BRL gI 0200
Surrogate Decachlorobiphenyl (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0231 0224 0194 0191
gI
gI
gI
gI
0200 0200 0200 0200
116 112
30- 150 30- 150 30- 150 30- 150
LC5 8051106-B51
Prepared 15-May-08 Analyzed 16-May-08
Aroclor- 1016 265 gI 0200 250 106 50- 114
Aroclor- 1 016 (2C) 240 gI 0200 250 50- 114
Aroclor- 1260 0269 gI 0200 250 107 40- 127
Aroclor-1260 (2Cj 270 gI 0200 250 108 40- 127
Surrogate Decachlorobiphenyl (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0225 0224 0188 0183
gI
gI
gI
gI
0200 0200 0200 0200
113 112
30- 150 30- 150 30- 150 30- 150
LC5 DUD rS051106-B5D1
Prepared 15-May-08 Analyzed 16-Mayshy
Aroclor- 1016 262 gl 0200 250 105 50- 114
Aroclor-1 016 (2Cj 241 gI 0200 250 50- 114
Aroclor- 1260 277 gI 0200 250 111 40- 127
Aroclor- 1260(2Cj 0260 gI 0200 250 104 40- 127
Surrogate Decachlorobipheny (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0238 0218 0189 0181
gI
gI
gI
gI
0200 0200 0200 0200
119 109
30- 150 30- 150 30- 150 30- 150
This laboratory report is lot valid without (II authorized sigllature 01 the cover page
Page 18 of25 Reportable Detection Limit BRL = Below Reporting Limit
Extractable Petroleum Hydrocarbons - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051102 - SW846 3510C
Blank 8051102-BLK1
Prepared 15-May-08 Analyzed 19-Mayshy
Non-polar material (SGT- HEM) BRL m91
LC8 8051102-B81
Prepared 15-May-08 Analyzed 19-Mayshy
Non-polar material (SGT- HEM) 184 m91 21 81 904
This laboratory report is not valid without an authorized signature 011 the cover page
Page 19 of25 Reportable Detection Limit BRL = Below Reporting Limit
Soluble Metals by EPA 200 Series Methods - Quality Control
Analyte(s) Result Flag Units RDL
Spike
Level
Source
Result REC
REC
Limits RPD
RPD
Limit
Batch 8051150 - EPA 200 Series
Blank 8051150-BLK1
Prepared amp Analyzed 21-May-
Iron
Zinc
Selenium
Nickel
Chromium
Copper
Arsenic
BRL
BRL
BRL
BRL
BRL
BRL
BRL
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0150
0050
0150
0050
0050
0050
0040
LCS 8051150-BS1
Prepared amp Analyzed 21-May-
Selenium
Zinc
Iron
Nickel
Chromium
Arsenic
Copper
123
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0150
0050
0150
0050
0050
0040
0050
103
105
101
100
85- 115
85- 115
85- 115
85- 115
85- 115
85-115
85- 115
licate B051150-DUP1 Source SA7B602shy
Prepared amp Analyzed 21-May-
Iron
Zinc
Selenium
Nickel
Copper
Chromium
Arsenic
17
0162
BRL
0015
0017
BRL
0450
QR8
mgl
mgl
mgl
mgl
mgl
mgl
mgi
0150
0050
0150
0050
0050
0050
0040
184
0186
BRL
0014
0023
BRL
0468
Matrix S ike 8051150-MS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Iron
Selenium
Nickel
Zinc
Copper
Chromium
Arsenic
19 QM2 mgl
mgll
mgl
mgl
mgl
mgl
mgl
0150
0150
0050
0050
0050
0050
0040
125
184
BRL
0014
0186
0023
BRL
0468
104
105
102
70- 130
70- 130
70-130
70- 130
70- 130
70-130
70- 130
Post S ike 8051150-PS1 Source SA78602shy
Prepared amp Analyzed 21-May-
Zinc
Iron
Selenium
Nickel
Copper
Arsenic
Chromium
18 QM2
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0050
0150
0150
0050
0050
0040
0050
0186
184
BRL
0014
0023
0468
BRL
104
104
101
85- 115
85- 115
85- 115
85-115
85-115
85- 115
85-115
Batch 8051152 - EPA200SW7000 Series
Blank B051152-BLK1
Prepared amp Analyzed 21-May-
Mercury BRL mgl 00020
This laboratory report is IIOt valid witllOut all authorized sigllature 011 the coverpage
Page 20 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Soluble Metals by EPA 200 Series Methods - Quality Control
Analyte(s) Result Flag Units RDL
Spike
Level
Source
Result REC
REC
Limits RPD
RPD
Limit
Batch 8051152 - EPA200SW7000 Series
LCS B051152-BS1
Prepared amp Analyzed 21-May-
Mercury 00576 m91 00020 00500 115 85- 115
licate B051152-DUP1 Source SA78602-01
Prepared amp Analyzed 21-May-
Mercury BRL m91 00020 BRL
Matrix S ike 8051152-MS1 Source SA78602shy
Prepared amp Analyzed 21-May-
Mercury 00632 OM m91 00020 00500 BRL 126 75- 125
Post S ike 8051152-PS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Mercury 00624 OC1 m91 00020 00500 BRL 125 85- 115
Batch 8051249 - 2008No digestion
Blank 8051249-BLK1
Prepared amp Analyzed 21-May-
Lead
Antimony
Cadmium
Silver
BRL
BRL
BRL
BRL
m91
m91
m91
m91
0002
0002
0002
0002
LCS B051249-BS1
Prepared amp Analyzed 21-May-
Antimony
Lead
Silver
Cadmium
143
145 OC2
m91
m91
m91
m91
0050
0050
0050
0040
103
115
107
116
85- 115
85- 115
85- 115
85- 115
licate 8051249-DUP1 Source SA7B602shy
Prepared amp Analyzed 21- May-
Lead
Antimony
Cadmium
Silver
0009
0002
00005
00002
ORB
m91
m91
m91
m91
0002
0002
0002
0002
0011
0003
00005
00003
Matrix S ike 8051249-MS1 Source SA78602shy
Prepared amp Analyzed 21- May-
Lead
Antimony
Cadmium
Silver
142
m91
m91
m91
m91
0050
0050
0040
0050
0011
0003
00005
00003
111
101
114
102
70- 130
70-130
70c130
70- 130
Post S ike 8051249-PS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Antimony
Cadmium
Silver
38
OC2
m91
m91
m91
0050
0040
0050
125
0003
00005
00003
110
121
109
85- 115
85- 115
85- 115
This laboratory report is flOt valid IVithout all authorized signature 011 the cOIer page
Reportable Detection Limit BRL Below Reporting Limit Page 21 of 25
General Chemistry Parameters - Quality Control
Spike Source REC RPD
Analyte( s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051049 - General Preparation
Blank S051 049-BLK1
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
Blank S051049-BLK2
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
Blank S051 049-BLK3
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
LCS S051049-BS1
Prepared amp Analyzed 14-May-
Total Residual Chlorine 046 mgl 020 0500 90- 110
LCS S051049-BS2
Prepared amp Analyzed 14-May-
Total Residual Chlorine 047 mgl 020 0500 90- 110
LCS S051049-BS3
Prepared amp Analyzed 14-May-
Total Residual Chlorine 054 mgl 020 0500 108 90-110
licate B051049-DUP1 Source SA7S544shy
Prepared amp Analyzed 14-May-
Total Residual Chlorine 012 mgl 020 010
licate S051049-DUP2 Source SA7S602-01
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020 BRL
Matrix S ike 8051049-MS1 Source SA78544-01
Prepared amp Analyzed 14-May-
Total Residual Chlorine 065 mgl 020 0500 010 110 80- 120
Matrix S ike 8051049-MS2 Source SA7B602shy
Prepared amp Analyzed 14-May-
Total Residual Chlorine mgl 500 125 BRL 108 80- 120
Reference 8051 049-SRM1
Prepared amp Analyzed 14-May-
Total Residual Chlorine 100 mgl 020 0967 103 85-115
Batch 8051094 - General Preparation
Blank 8051094-BLK1
Prepared amp Analyzed 14 May-
Hexavalent Chromium (soluble) BRL mgl 005
Blank 8051 094-BLK2
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) BRL mgl 005
LCS 8051094-BS1
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) 054 mgl 005 90- 110
licate 8051094-DUP1 Source SA78602-01
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) BRL mgl 125 BRL
Thi laboratory report is not valid without all authorized sigllature 011 the cover page
Page 22 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Page 19
Sam le Identification Client Pro ect Matrix Collection DateTime ReceivedMWshy
2920-96- Ground Water 13-May-081030 14-May-SA 78602shy
CAS No Analyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Volatile Organic Compounds
Volatile Or anic Com ounds b GCMS
Prepared by method SW846 5030 Water MS
123-91- Dioxane BRL 1-91 200 EPA 624 16-May-08 17-May-08 8051244
994-05-8 Ter-amyl methyl ether BRL 1-911 20
755- Tert-Butanoll butyl alcohol BRL 1-91 200
67-B4- Acetone BRL 1-91 400
71-43- Benzene BRL 1-91 20
75-27-4 Bromodichloromethane BRL 1-91 20
75-25- Bromoform BRL 1-91 20
74-83- Bromomethane BRL 1-91 40
78-93- Butanone (MEK) BRL 1-91 200
56-23- Carbon tetrachloride BRL 1-91 20
108-90- Chlorobenzene BRL 1-91 20
75-00- Chloroethane BRL 1-91 40
676- Chloroform BRL 1-91 20
74-87- Chloromethane BRL 1-91 40
124-48- Dibromochloromethane BRL 1-91 20
95-50- Dichlorobenzene BRL 1-911 20
541-73- Dichlorobenzene BRL 1-91 20
106-46- Dichlorobenzene BRL 1-91 20
75-34- 1- Dichloroethane BRL 1-91 20
107-06- Dichloroethane BRL 1-91 20
75-35-4 1- Dichloroethene BRL 1-91 20
156-59 cis- Dichloroethene BRL 1-91 20
156-60- trans- Dichloroethene BRL 1-91 20
78-87- 2- Dichloropropane BRL 1-91 20
10061-01-5 cis- Dichloropropene BRL 1-91 20
10061-02-B trans- Dichloropropene BRL 1-91 20
100-41-4 Ethylbenzene 411 1-911 20
591-78-B BRL 200Hexanone (MBK) 1-91
1634-04 -4 Methyl tert-butyl ether BRL 1-91 20
108-10- Methyl- pentanone (MIBK) BRL 1-91 200
75-09- Methylene chloride BRL 1-91 200
100-42- Styrene BRL 1-91 20
79-34- 1 Tetrachloroethane BRL 1-91 20
127- 18-4 T etrachloroethene BRL 1-91 20
108-88- Toluene BRL 1-91 20
71-55 1- Trichloroethane BRL 1-91 20
79-00- 2- Trichloroethane BRL 1-91 20
79-01-B Trichloroethene BRL 1-91 20
759-4 Trichlorofluoromethane (Freon 11) BRL 1-91 20
75-01-4 Vinyl chloride BRL 1-91 20
179601-23-1 m Xylene 390 1-91 40
95-47 Xylene 82 1-91 20
Surrogate recoveries 460-00- Bromofluorobenzene 70- 130
2037-26- Toluene- 100 70- 130
17060-07-0 1 Dichloroethane- 111 70- 130
1868-53- Dibromofluoromethane 70- 130
Microextractable Organic Compounds
106-93-4 1 Dibromoethane (EDB) BRL 1-91 0100 EPA 504 15-May- 15-May-08 8051105
Semivolatile Organic Compounds by GCMS
This laboratory report is not valid without all autllOrized signature 011 the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page 5 of 25
Sam le Identification Client Pro ect Matrix Collection DateTime Received
MWshy2920-96- Ground Water 13-May-081030 14-May-
SA 78602shy
CAS No Analyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Semivolatie Organic Compounds by GCMS
Semi volatile Or anic Com ounds b EPA 625
Prepared by method SW846 3510C 50 EPA 625 16-May- 19-May-08 805121683-32- Acenaphthene BRL IJgl
208-96-8 Acenaphthylene BRL IJgl 50
62-53- BRL IJgll 50Aniline
120- 12- Anthracene BRL 1J91 50
103-33- AzobenzenefDiphenyldiazine BRL IJgl 50
92-87 - Benzidine BRL IJgl 50
56-55- Benzo (a) anthracene BRL 1J91 50
50-32 - Benzo (a) pyrene IJglBRL 50
205-99- Benzo (b) fluoranthene BRL IJgl 50
191-24- Benzo (g i) perylene BRL IJgl 50
50207-08- Benzo (k) fluoranthene BRL IJgl
65-85 Benzoic acid BRL 1J91 50
100-51-6 Benzyl alcohol 1J91BRL 50
50111-91- Bis(2-chloroethoxy)methane BRL 1J91
111-4-4 Bis(2-chloroethyl)ether BRL IJgl 50
501 08-60- Bis(2-chloroisopropyl)ether BRL IJgl
117-81- Bis(2-ethylhexyl)phthalate BRL 1J91 50
101-55- Bromophenyl phenyl ether BRL IJgl 50
5085-68- Butyl benzyl phthalate BRL IJgl
5086-74- Carbazole BRL IJgl
5059-50- C hloro-3-methylphenol BRL IJgl
106-47- Chloroaniline BRL IJgl 50
91-58- Chloronaphthalene IJglBRL 50
5095-57 - Chlorophenol BRL 1J91
507005-72- Chlorophenyl phenyl ether BRL IJgl
216-01- Chrysene tJ91BRL 50
5053-70- Dibenzo (a h) anthracene BRL IJgl
50132-64- Dibenzofuran BRL IJgl
95-50- Dichlorobenzene IJglBRL 50
541-73- 13- Dichlorobenzene BRL IJgl 50
106-46- Dichlorobenzene 1J91BRL 50
5091-94- 3 - Dichlorobenzidine BRL IJgl
120-83- Dichlorophenol BRL IJgl 50
84-66- Diethyl phthalate BRL IJgl 50
131-11- Dimethyl phthalate BRL IJgll 50
105-67- Dimethylphenol BRL 1J91 50
5084-74- Di-n- butyl phthalate BRL 1J91
534-52 - Dinitro-2-methylphenol BRL IJgl 50
51-28- Dinitrophenol IJglBRL 50
50121-14- Dinitrotoluene BRL 1J91
606-20- Dinitrotoluene IJglBRL 50
50117-84-0 Di-n-octyl phthalate BRL IJgl
206-44-0 Fluoranthene 1J91BRL 50
BRL 50
50 86-73- Fluorene IJgi
118-74- Hexachlorobenzene BRL 1J91
87-68- Hexachlorobutadiene 1J91BRL 50
5077-47-4 Hexachlorocyclopentadiene BRL IJgl
67-72- Hexachloroethane IJglBRL 50
50193-39- Indeno (1 3-cd) pyrene BRL IJgl
5078-59- Isophorone BRL IJgl
Tfls laboratory report is not valid without all authorized signature 011 the coverpage
Page 6 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Sam le Identification Client Pro ect Matrix Collection DateTime ReceivedMWshy
2920-96- Ground Water I3-May-081030 14-May-SA 78602shy
CAS No Analyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Semivolatile Organic Compounds by GCMS
Semi volatile Or anic Com ounds b EPA 625
Prepared by method SW846 3510C
91-57 -6 Methylnaphthalene 367 1-91 50 EPA 625 16-May- 19-May-08 8051216
95-48- Methylphenol BRL 1-91 50
108-39-4 3 amp 4-Methylphenol BRL I-gl 100 106-44shy91-20- Naphthalene 247 1-91 50
88-74-4 Nitroaniline BRL 1-91 50
99-09- Nitroaniline BRL 1-91 50
100-01-6 Nitroaniline BRL 1-91 50
98-95- Nitrobenzene BRL 1-91 50
88-75- Nitrophenol BRL 1-91 50
100-02- Nitrophenol BRL 1-91 50
62-75- Nitrosodimethylamine BRL 1-91 50
621-64- N- Nitrosodi-n-propylamine BRL 1-91 50
86-30-6 Nitrosodiphenylamine BRL 1-91 50
87 -86- Pentachlorophenol BRL 1-91 50
85-0- Phenanthrene BRL 1-91 50
108-95- Phenol BRL 1-91 50
129-00-0 Pyrene BRL 1-91 50
110-86- Pyridine BRL 1-91 50
120-82- 4- Trichlorobenzene BRL 1-91 50
95-95- 5- Trichlorophenol BRL 1-91 50
88-06- 6- T richlorophenol BRL 1-91 50
Surrogate recoveries
321-60- Fluorobipheny 30- 130
367- 12- Fuorophenol 15- 110
4165-60- Nitrobenzene- 30- 130
4165-62- Pheno- 15- 110
1718-51- Terpheny-d4 30- 130
118- 79- 6- Tribromophenol 15- 110
Semivolatile Organic Compounds by GC
Pol chlorinated Bi hen ls b EPA 608
Prepared by method SW846 3510C
12674- 11-2 Aroclor- 1016 BRL 1-91 0650 EPA 608 15- May- 16-May-08 8051106
11104-28-2 Aroclor-1221 BRL IJgl 0650
11141-16-5 Aroclor- 1232 BRL 1-91 0650
53469-21-9 Aroclor- 1242 BRL 1-91 0650
12672-29-6 Aroclor- 1248 BRL 1-91 0650
11097-69-1 Aroclor- 1254 BRL 1-91 0650
11096-82-5 Aroclor -1260 BRL 1-91 0650
37324-23-5 Aroclor-1262 BRL 1-91 0650
11100-14-4 Aroclor-1268 BRL IJgl 0650
Surrogate recoveries
2051-24- Decachlorobipheny (Sr) 105 30- 150
10386-84-2 4 DB-Octafluorobiphenyl (Sr) 30- 150
Extractable Petroleum Hydrocarbons
mgl EPA 1664 Rev A 15-May- 19-May-08 8051102Non-polar material (SGT- HEM)
Soluble Metals by EPA 2006000 Series Metbods
Field Filtered NA EPA 200 73005A 15- May- 15-May-08 8051192Filtration
Soluble Metals by EPA 200 Series Methods
7440-22-4 Silver BRL mgl 0002 EPA 200 21-May- 27- May-08 8051249
This laboratory report is IlOt mlid without (II authorized signature on the cover page
Reportble Detection Limit BRL = Below Reporting Limit Page 7 of 25
Sam le Identification MW-
Client Pro ect 2920-96shy
Matrix Ground Water
Collection DateTime 13-May-08 1030
Received 14-May-
SA 78602shy
CAS No A nalyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Soluble Metals by EPA 200 Series Methods
7440-38shy Arsenic 0468 mg1 0040 EPA 200 21-Mayshy 21-May-08 80511 50
7440-43shy Cadmium BRL mg1 0002 EPA 200 21-May-088051249
7440-47shy Chromium BRL mg1 0050 EPA 200 21-May-088051150
7440-50-8 Copper BRL mg1 0050
7439-89-6 Iron 184 mg1 0150
7439-97-6 Mercury BRL mg1 00020 EPA 245 17470A 21-May-088051152
7440-02-0 Nickel BRL mg1 0050 EPA 200 21-May-088051150
7439-92shy Lead 0011 mg1 0002 EPA 200 21-May-088051249
7440-36-0 Antimony 0003 mg1 0002
7782-49shy Selenium BRL mg1 0150 EPA 200 21-May-08 8051150
7440-66-6 Zinc 0186 mgl 0050
General Chemistry Parameters
Filtration Completed NA Varies 14-Mayshy 14-May-08 8051095
18540-29-9 Hexavalent Chromium (soluble) BRL HT2 mg1 125 SM3500CrDI796A 14-Mayshy 14-May-08 8051094 R01 2013 2016
57-12shy Cyanide (total) BRL mg1 0100 EPA 3354 19-Mayshy 19-May-088051374
7782-50shy Total Residual Chlorine BRL CIHT mg1 500 Hach 8167 14-Mayshy 14-May-08 8051049 R01 1900 2001
Total Suspended Solids 580 mg1 25 SM2540D 16-Mayshy 16-May-08 8051275
This lahomtOlY report is not valid without an authorized signature on the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page 8 of 25
Volatie Organic Compounds - Quality Control
Analyte( s)
Batch 8051244 - SW846 5030 Water MS
Blank 8051244-BLK1
Prepared 16-May-08 Analyzed 17-May-
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromochloromethane
1 Dichlorobenzene
1 Dichlorobenzene
1 Dichlorobenzene
1-Dichloroethane
1 Dichloroethane
1 1-Dichloroethene
cis- Dichloroethene
trans- 1 Dichloroethene
1 Dichloropropane
cis- 1 Dichloropropene
trans- 1 Dichloropropene
Ethylbenzene
Hexanone (MBK)
Methyl tert-butyl ether
Methyl- pentanone (MIBK)
Methylene chloride
Styrene
2- Tetrachloroethane
Tetrachloroethene
Toluene
1- Trichloroethane
2- Trichloroethane
Trichloroethene
Trichlorofluoromethane (Freon 11)
Vinyl chloride
p-Xylene
Xylene
Surrogate 4-Bromofluorobenzene Surrogate Toluene-
Surrogate 1 Dichloroethane-Surrogate Dibromofluoromethane
LCS B051244-BS1
Prepared 16-May-08 Analyzed 17 -May-
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Spike Source REC RPD
Result Flag Units RDL Level Result REC Limits RPD Limit
BRL gl 20
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl 10
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gll
BRL gi
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl 10
BRL gll
BRL gll 10
BRL gl 10
BRL gll
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
41 gl 50 70- 130 49 gl 50 70- 130 59 gl 50 119 70- 130 52 gl 50 105 70- 130
QC2 jgl 20 70- 130
18 jgl 20 70- 130
192 jgl 20 35- 155
18 jgl 20 45- 169
19 jgl 20 242
This laboratOlY repol1 is lot valid without 011 authorized sigllature 011 the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page 9 of 25
Volatie Organic Compounds - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051244 - SW846 5030 Water MS
LC5 8051244B51
Prepared 16-May-08 Analyzed 17-May-
Butanone (MEK) 10 QC2 gl 20 70- 130
Carbon tetrachloride 204 gl 20 102 70- 140
Chlorobenzene 18 gl 20 70- 130
Chloroethane 164 gl 20 14-230
Chloroform 18 gll 20 51- 138
Chloromethane 21 gl 20 106 273
Dibromochloromethane 18 gl 20 53- 149
1 Dichlorobenzene 20 gl 20 104 18- 190
1 Dichlorobenzene 19 gl 20 59- 156
1 A-Dichlorobenzene 18 gl 20 18- 190
1- Dichloroethane 19 gl 20 59- 155
1 Dichloroethane 19 gl 20 49- 155
1-Dichloroethene 16 gl 20 70- 130
cis- 1 Dichloroethene 17 gl 20 70- 130
trans- 1 Dichloroethene 16 gll 20 54- 156
1 Dichloropropane 18 gl 20 210
cis- Dichloropropene 17 gl 20 227
trans- 1 Dichloropropene 17 gl 20 17- 183
Ethylbenzene 19 gl 20 37- 162
Hexanone (MBK) 124 QC2 gl 20 70- 130
Methyl tert-butyl ether 19 gl 20 70- 130
Methylshy pentanone (MIBK) 17 gl 20 70- 130
Methylene chloride 16 gl 20 221
Styrene 17 gl 20 70- 130
1 Tetrachloroethane 194 gl 20 46- 157
Tetrachloroethene 15 gl 20 64- 148
Toluene 18 gl 20 70- 130
1- Trichloroethane 20 gl 20 100 52- 162
2- Trichloroethane 18 gl 20 52- 150
Trichloroethene 17 gl 20 71- 157
Trichlorofluoromethane (Freon 11) 19 gl 20 17- 181
Vinyl chloride 21 gl 20 106 251
p-Xylene 39 gl 40 70- 130
Xylene 20 gl 20 102 70- 130
Surrogate 4-Bromofluorobenzene Surrogate Toluene-
Surrogate 1 Dichloroethane-Surrogate Dibromofluoromethane
52 49 56
49
gl
gl
gl
gl
50 50 50
50
105
112 100
70- 130 70- 130 70- 130 70- 130
LC5 DUD (8051244-B5D1
Prepared 16-May-08 Analyzed 17-May-
Acetone QC2 gl 20 70- 130
Benzene 18 gl 20 70- 130
Bromodichloromethane 18 gl 200 35- 155
Bromoform 17 gl 20 45- 169
Bromomethane 18 gl 20 242
Butanone (MEK) 11 QC2 1-91 20 70- 130
Carbon tetrachloride 20 gl 20 100 70- 140
Chlorobenzene 17 gl 20 70- 130
Chloroethane 15 1-91 20 14-230
Chloroform 18 1-91 20 51- 138
This laboratory report is aot valid without a1 authorized sig1ature 01 the cover page
Reportble Detection Limit BRL = Below Reporting Limit Page 10 of25
Volatie Organic Compounds - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051244 - SW846 5030 Water MS
LCS Dup 18051244-BSD1
Prepared 16-May-08 Analyzed 17-May-
Chloromethane 18 1-91 20 273
Dibromochloromethane 174 1-91 20 53- 149
Dichlorobenzene 20 1-91 20 100 18- 190
Dichlorobenzene 18 1-91 20 59- 156
Dichlorobenzene 18 1-91 20 18- 190
Dichloroethane 18 1-91 20 59- 155
Dichloroethane 19 1-91 20 49- 155
Dichloroethene 16 1-91 20 70- 130
cis- Dichloroethene 16 1-91 20 70- 130
trans- Dichloroethene 15 1-91 20 54- 156
Dichloropropane 17 1-91 20 210
cis- Dichloropropene 164 IJgl 20 227
trans- 1 Dichloropropene 164 I-gl 20 17- 183
Etlwlbenzene 18 IJgl 20 37- 162
Hexanone (MBK) 124 QC2 IJgl 20 70- 130
Methyl tert-butyl ether 184 1J91 20 70- 130
Methyl- pentanone (MIBK) 17 IJgl 20 70- 130
Methylene chloride 16 IJgl 20 221
Styrene 16 IJgl 20 70- 130
2- Tetrachloroethane 19 IJgl 20 46- 157
Tetrachloroethene 15 IJgl 20 64- 148
Toluene 17 IJgl 20 70- 130
1- Trichloroethane 19 1-91 20 52- 162
2- Trichloroethane 16 IJgl 20 52- 150
Trichloroethene 15 IJgl 20 71- 157
Trichlorofluoromethane (Freon 11) 17 IJgl 20 17- 181
Vinyl chloride 19 IJglI 20 251
p-Xylene 37 1J91 40 70- 130
Xylene 20 IJgl 20 100 70- 130
Surrogate 4-Bromofluorobenzene 51 IJgl 50 104 70- 130
Surrogate Toluene- 4B gl 50 70- 130
Surrogate 1 0ichloroethane- 53 IJgl 50 106 70- 130 Surrogate Oibromofluoromethane 50 1J9i 50 102 70- 130
Matrix S ike B051244-MS1 Source SA7B629shy
Prepared 16-May-08 Analyzed 17-May-
Benzene 18 20 BRL 70- 130IJgl
Bromodichloromethane 19 IJgl 20 BRL 35- 155
Bromoform 18 IJgl 20 BRL 45- 169
Bromomethane 16 IJgl 20 BRL 242
Carbon tetrachloride 21 IJgl 20 BRL 106 70- 140
Chlorobenzene 18 IJgl 20 BRL 70- 130
Chloroethane 16 IJgl 20 BRL 14-230
Chloroform 18 IJgl 20 BRL 51- 138
Chloromethane 19 IJgl 20 BRL 273
Dibromochloromethane 17 IJgl 20 BRL 53- 149
1 Dichlorobenzene 22 IJgl 20 BRL 112 18- 190
1 Dichlorobenzene 22 IJgl 20 BRL 110 59-156
1 Dichlorobenzene 21 IJgl 20 BRL 109 18- 190
1- Dichloroethane 19 IJgl 20 BRL 59- 155
1 Dichloroethane 18 IJgl 20 BRL 49- 155
This laboratory report is 110t mUd without an authorized signature on the covel page
Reportble Detection Limit BRL = Below Reporting Limit Page It of25
Volatile Organic Compounds - Quality Control
p
Spike Source REC RPD
Result REC imits RPD LimitAnalyte(s) Result Flag Units RDL Level
Batch 8051244 - SW846 5030 Water MS
Matrix ike S051244-MS1 Source SA7B629shy
Prepared 16-May-08 Analyzed 17-Mayshy
17 20 BRL 70- 130 1- Dichloroethene IJgl
16 20 BRL 54- 156trans- 1 Dichloroethene IJgl
21020 BRL1 Dichloropropane 17 1J91
cis- 1 Dichloropropene 17 IJgl 20 BRL 227
17- 183trans- 1 Dichloropropene 184 1J91 20 BRL
20 20 BRL 103 37- 162Ethylbenzene IJgl
15 20 BRL 221Methylene chloride IJgl
20 BRL 46- 1572- Tetrachloroethane 19 1J91
20 BRL 64- 148Tetrachloroethene 18 1J91
BRL 70- 130Toluene 18 1J91 20
105 52-1621- Trichloroethane 211 IJgl 20 BRL
18 20 BRL 52- 1502- Trichloroethane IJgl
17 20 BRL 71- 157Trichloroethene 1J91
20 BRL 17- 181Trichloroluoromethane (Freon 11) 194 IJgl
20 BRL 103 251Vinyl chloride 20 IJgl
102 70- 130Surrogate 4-Bromofluorobenzene 50 IJgl 50 50 70- 130Surrogate Toluene- 49 1J91
56 50 112 70- 130Surrogate 1 Dichloroethane- IJgl
50 100 70- 130Surrogate Dibromofluoromethane 50 IJgl
Matrix S ike Du S051244-MSD1 Source SA7S629shy
Prepared 16-May-08 Analyzed 17-Mayshy
18 20 BRL 70- 130Benzene IJgl
18 20 BRL 35- 155Bromodichloromethane IJgl
17 20 BRL 45- 169Bromoform IJgl
20 BRL 242Bromomethane 17 IJgl
20 BRL 103 70- 140Carbon tetrachloride 20 IJgl
18 20 BRL 70- 130Chlorobenzene 1J91
14-230Chloroethane 16 IJgl 20 BRL
20 51- 138Chloroform 184 IJgl BRL
Chloromethane 19 1J91 20 BRL 273
18 20 BRL 53- 149Dibromochloromethane 1J91
20 BRL 117 18- 190Dichlorobenzene 234 IJgl
20 BRL 112 59- 156Dichlorobenzene 22 IJgl
BRL 108 18- 190Dichlorobenzene 21 1J91 20
20 59- 1551 Dichloroethane 19 IJgl BRL
18 20 BRL 49- 155Dichloroethane IJgl
16 20 BRL 70- 130Dichloroethene IJgl
20 BRL 54- 156trans- Dichloroethene 154 1J91
20 BRL 210Dichloropropane 17 IJgl
0420 BRL 227cis- Dichloropropene 17 IJgl
17- 183trans- Dichloropropene 17 1J91 20 BRL
BRL 37- 162Ethylbenzene 20 1J91 20 102
Methylene chloride 15 IJgl 20 BRL 221
20 BRL 46- 1572- Tetrachloroethane 192 IJgl
20 BRL 64- 148 04Tetrachloroethene 18 IJgl
BRL 70- 130Toluene 184 1J91 20
52- 1621- Trichloroethane 20 IJgl 20 BRL 104
17 20 BRL 52- 1502- Trichloroethane IJgl
17 20 BRL 71- 157Trichloroethene IJgl
20 BRL 17-181Trichlorofluoromethane (Freon 11) 19 IJgl
This laboratory report is IIOt valid without all authorized sigllllture 011 the cover page
Page 12 of25 Reportble Detection Limit BRL = Below Reporting Limit
Semivolatile Organic Compounds by GCMS - Quality Control
Analyte(s)
Batch 8051216 - SW846 3510C
Blank 8051216-BLK1
Prepared amp Analyzed 16-May-
Isophorone
Methylnaphthalene
Methylphenol
3 amp 4-Methylphenol
Naphthalene
Nitroaniline
Nitroaniline
Nitroaniline
Nitrobenzene
Nitrophenol
Nitrophenol
Nitrosodimethylamine
N- N itrosodi-n-pro pyla mine
N itrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Pyridine
1 24-Trichlorobenzene
24 5- Trichlorophenol
246- Trichlorophenol
Surrogate 2-Fuorobipheny Surrogate 2-Fuoropheno Surrogate Nitrobenzene-Surrogate PhenoshySurrogate Terpheny-d4 Surrogate 6- Tribromopheno
LCS B051216-BS1
Prepared amp Analyzed 16-May-
Acenaphthene
Acenaphthylene
Aniline
Anthracene
AzobenzenelDi phenyld lazine
Benzidine
Benzo (a) anthracene
Benzo (a) pyrene
Benzo (b) fluoranthene
Benzo (g i) perylene
Benzo (k) fluoranthene
Benzoic acid
Benzyl alcohol
B is(2-chloroethoxy)methane
B i s (2-ch loroethyl)eth e r
Bis(2-ch loroisopropyl) ether
B is(2-ethy Ih exyl) phtha late
Bromophenyl phenyl ether
Butyl benzyl phthalate
Carbazole
Spike Source REC RPD
Result Flag Units RDL Level Result REC Limits RPD Limit
BRL gl
BRL gl
BRL gl
BRL gl 10
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gll
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
370 gl 50 30- 130 40 gl 50 15- 110 39 gl 50 30- 130 43 gl 50 15- 110 36 gl 50 30- 130 40 gl 50 15- 110
41 gl 50 40- 140
43 gI 50 40- 140
41 gl 50 40- 140
38 gl 50 40- 140
45 gl 50 40- 140
49 gl 50 153
41 gl 50 40- 140
43 gl 50 40- 140
41 gl 50 40- 140
41 gll 50 40- 140
45 gl 50 40- 140
32 gl 50 12- 149
41 gl 50 40- 140
39 gl 50 40- 140
384 gl 50 40- 140
47 gl 50 40- 140
47 gl 50 40- 140
40 gl 50 40- 140
47 gI 50 40- 140
56 gI 50 112 200
This laboratory report is lIot valid witllOut a1l authorized sigllature 011 the coverpage
Reportble Detection Limit BRL = Below Reporting Limit Page 15 of25
Semivolatile Organic Compounds by GCMS - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051216 - SW846 3510C
LCS 8051216-BS1
Prepared amp Analyzed 16-Mayshy
50 30- 1304 -C hloro-3-methylphenol 42 IJgl
40- 140Chloroaniline 39 IJgl 50
Chloronaphthalene 37 IJgl 50 40- 140
Chlorophenol 37 IJgl 50 30- 130
50 40- 140
40- 140
Chlorophenyl phenyl ether 45 IJgl
Chrysene 43 IJgl 50
Dibenzo (a h) anthracene 43 IJgl 50 40- 140
Dibenzofuran IJgl38 50 40- 140
50 40- 1401 Dichlorobenzene 35 IJgl
40- 1401 Dichlorobenzene 264 IJgl 50
40- 1401 Dichlorobenzene 434 IJgl 50
58 50 116 40- 1403 - Dichlorobenzidine IJgl
50 30- 130
40- 140 24-Dichlorophenol 38 IJgl
Diethyl phthalate 484 IJgl 50
50 40- 140Dimethyl phthalate 464 IJgl
Dlmethylphenol 39 IJgl 50 30- 130
DI-n-butyl phthalate 44 IJgll 50 40- 140
30- 130 6-Di nitro- 2-methylphenol 38 1J91 50
30- 130Dinltrophenol 36 1J91 50
42 50 40- 14024-Dlnitrotoluene 1J91
Dlnitrotoluene 1J9141 50 40- 140
Di-n-octyl phthalate 52 IJgl 50 104 40- 140
40- 140Fluoranthene 40 IJgl 50
Fluorene 41 IJgl 50 40- 140
39 50 40- 140Hexachlorobenzene IJgl
50 40- 140Hexachlorobutadiene 40 IJgl
40- 140Hexach lorocyclopentad iene 294 IJgl 50
40 50 40- 140Hexachloroethane IJgl
42 50 40-140Indeno (1 3-cd) pyrene IJgl
50 40- 140Isophorone 40 IJgl
40- 140Methylnaphthalene 394 IJgl 50
40- 140Methylphenol 39 IJgl 50
40 10 50 40- 1403 amp 4-Methylphenol IJgl
37 50 40-140Naphthalene IJgl
50 40-140Nitroaniline 39 IJgl
Nitroaniline 51 IJgl 50 102 40- 140
48 50 40- 140Nltroaniline 1J91
50 40- 140Nitrobenzene 40 IJgl
30- 130Nitrophenol 36 IJgl 50
40 IJgl 50 30- 130Nitrophenol 40- 140Nitrosodimethylamine 32 1J91 50
50 40-140N- N itrosodi-n-propyla mine 46 IJgl
40- 140N itrosodi phenyla ml ne 44 IJgl 50
41 IJgl 50 30- 130Pentachlorophenol 40- 140Phenanthrene 38 IJgl 50
50 30- 130Phenol 38 IJgl
40- 140Pyrene 424 1J91 50
40- 140Pyridine 294 1J91 50
40- 14024- Trichlorobenzene 364 IJgl 50
This laboratory report is not mlid without an authorized signature 011 the cover page
Page 16 of25 Reportble Detection Limit BRL = Below Reporting Limit
Semivolatie Organic Compounds by GCMS - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
BMch 8051216 - SW846 3510C
LC5 8051216-851
Prepared amp Analyzed 16-Mayshy
24 5- Trichlorophenol 404 gl 50 30- 130
246- Trichlorophenol 42 gl 50 30- 130
Surrogate 2-Fluorobiphenyl 29 gl 50 30- 130
Surrogate 2-Fluorophenot 27 gl 50 15- 110
Surrogate Nitrobenzene- 30 gl 50 30- 130
Surrogate Phenol- 29 gl 50 15- 110
Surrogate Terpheny-d4 30 gl 50 30- 130
Surrogate 6- Tribromopheno 324 gl 50 15- 110
This laboratory report is lIot valid without all authorized sigllature 011 tlle cover page
Reportble Detection Limit BRL = Below Reporting Limit Page 17 of25
Semivolatie Organic Compounds by GC - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051106 - SW846 3510C
Blank S051106-BLK1
Prepared amp Analyzed 15-Mayshy
Aroclor- 1016 BRL gI 0200
Aroclor- 1016 (2C) BRL gI 0200
Aroclor- 1221 BRL gI 0200
Aroclor- 1221 (2C) BRL gI 0200
Aroclor- 1232 BRL gI 0200
Aroclor- 1232 (2Cj BRL gI 0200
Aroclor- 1242 BRL gI 0200
Aroclor-1242 (2C) BRL gI 0200
Aroclor- 1248 BRL gI 0200
Aroclor- 1248 (2C) BRL gI 0200
Aroclor- 1254 BRL gI 0200
Aroclor- 1254(2Cj BRL gI 0200
Aroclor- 1260 BRL gI 0200
Aroclor- 1260 (2C) BRL gI 0200
Aroclor- 1262 BRL gI 0200
Aroclor- 1262 (2C) BRL gI 0200
Aroclor-1268 BRL gI 0200
Aroclor- 1268 (2C) BRL gI 0200
Surrogate Decachlorobiphenyl (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0231 0224 0194 0191
gI
gI
gI
gI
0200 0200 0200 0200
116 112
30- 150 30- 150 30- 150 30- 150
LC5 8051106-B51
Prepared 15-May-08 Analyzed 16-May-08
Aroclor- 1016 265 gI 0200 250 106 50- 114
Aroclor- 1 016 (2C) 240 gI 0200 250 50- 114
Aroclor- 1260 0269 gI 0200 250 107 40- 127
Aroclor-1260 (2Cj 270 gI 0200 250 108 40- 127
Surrogate Decachlorobiphenyl (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0225 0224 0188 0183
gI
gI
gI
gI
0200 0200 0200 0200
113 112
30- 150 30- 150 30- 150 30- 150
LC5 DUD rS051106-B5D1
Prepared 15-May-08 Analyzed 16-Mayshy
Aroclor- 1016 262 gl 0200 250 105 50- 114
Aroclor-1 016 (2Cj 241 gI 0200 250 50- 114
Aroclor- 1260 277 gI 0200 250 111 40- 127
Aroclor- 1260(2Cj 0260 gI 0200 250 104 40- 127
Surrogate Decachlorobipheny (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0238 0218 0189 0181
gI
gI
gI
gI
0200 0200 0200 0200
119 109
30- 150 30- 150 30- 150 30- 150
This laboratory report is lot valid without (II authorized sigllature 01 the cover page
Page 18 of25 Reportable Detection Limit BRL = Below Reporting Limit
Extractable Petroleum Hydrocarbons - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051102 - SW846 3510C
Blank 8051102-BLK1
Prepared 15-May-08 Analyzed 19-Mayshy
Non-polar material (SGT- HEM) BRL m91
LC8 8051102-B81
Prepared 15-May-08 Analyzed 19-Mayshy
Non-polar material (SGT- HEM) 184 m91 21 81 904
This laboratory report is not valid without an authorized signature 011 the cover page
Page 19 of25 Reportable Detection Limit BRL = Below Reporting Limit
Soluble Metals by EPA 200 Series Methods - Quality Control
Analyte(s) Result Flag Units RDL
Spike
Level
Source
Result REC
REC
Limits RPD
RPD
Limit
Batch 8051150 - EPA 200 Series
Blank 8051150-BLK1
Prepared amp Analyzed 21-May-
Iron
Zinc
Selenium
Nickel
Chromium
Copper
Arsenic
BRL
BRL
BRL
BRL
BRL
BRL
BRL
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0150
0050
0150
0050
0050
0050
0040
LCS 8051150-BS1
Prepared amp Analyzed 21-May-
Selenium
Zinc
Iron
Nickel
Chromium
Arsenic
Copper
123
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0150
0050
0150
0050
0050
0040
0050
103
105
101
100
85- 115
85- 115
85- 115
85- 115
85- 115
85-115
85- 115
licate B051150-DUP1 Source SA7B602shy
Prepared amp Analyzed 21-May-
Iron
Zinc
Selenium
Nickel
Copper
Chromium
Arsenic
17
0162
BRL
0015
0017
BRL
0450
QR8
mgl
mgl
mgl
mgl
mgl
mgl
mgi
0150
0050
0150
0050
0050
0050
0040
184
0186
BRL
0014
0023
BRL
0468
Matrix S ike 8051150-MS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Iron
Selenium
Nickel
Zinc
Copper
Chromium
Arsenic
19 QM2 mgl
mgll
mgl
mgl
mgl
mgl
mgl
0150
0150
0050
0050
0050
0050
0040
125
184
BRL
0014
0186
0023
BRL
0468
104
105
102
70- 130
70- 130
70-130
70- 130
70- 130
70-130
70- 130
Post S ike 8051150-PS1 Source SA78602shy
Prepared amp Analyzed 21-May-
Zinc
Iron
Selenium
Nickel
Copper
Arsenic
Chromium
18 QM2
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0050
0150
0150
0050
0050
0040
0050
0186
184
BRL
0014
0023
0468
BRL
104
104
101
85- 115
85- 115
85- 115
85-115
85-115
85- 115
85-115
Batch 8051152 - EPA200SW7000 Series
Blank B051152-BLK1
Prepared amp Analyzed 21-May-
Mercury BRL mgl 00020
This laboratory report is IIOt valid witllOut all authorized sigllature 011 the coverpage
Page 20 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Soluble Metals by EPA 200 Series Methods - Quality Control
Analyte(s) Result Flag Units RDL
Spike
Level
Source
Result REC
REC
Limits RPD
RPD
Limit
Batch 8051152 - EPA200SW7000 Series
LCS B051152-BS1
Prepared amp Analyzed 21-May-
Mercury 00576 m91 00020 00500 115 85- 115
licate B051152-DUP1 Source SA78602-01
Prepared amp Analyzed 21-May-
Mercury BRL m91 00020 BRL
Matrix S ike 8051152-MS1 Source SA78602shy
Prepared amp Analyzed 21-May-
Mercury 00632 OM m91 00020 00500 BRL 126 75- 125
Post S ike 8051152-PS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Mercury 00624 OC1 m91 00020 00500 BRL 125 85- 115
Batch 8051249 - 2008No digestion
Blank 8051249-BLK1
Prepared amp Analyzed 21-May-
Lead
Antimony
Cadmium
Silver
BRL
BRL
BRL
BRL
m91
m91
m91
m91
0002
0002
0002
0002
LCS B051249-BS1
Prepared amp Analyzed 21-May-
Antimony
Lead
Silver
Cadmium
143
145 OC2
m91
m91
m91
m91
0050
0050
0050
0040
103
115
107
116
85- 115
85- 115
85- 115
85- 115
licate 8051249-DUP1 Source SA7B602shy
Prepared amp Analyzed 21- May-
Lead
Antimony
Cadmium
Silver
0009
0002
00005
00002
ORB
m91
m91
m91
m91
0002
0002
0002
0002
0011
0003
00005
00003
Matrix S ike 8051249-MS1 Source SA78602shy
Prepared amp Analyzed 21- May-
Lead
Antimony
Cadmium
Silver
142
m91
m91
m91
m91
0050
0050
0040
0050
0011
0003
00005
00003
111
101
114
102
70- 130
70-130
70c130
70- 130
Post S ike 8051249-PS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Antimony
Cadmium
Silver
38
OC2
m91
m91
m91
0050
0040
0050
125
0003
00005
00003
110
121
109
85- 115
85- 115
85- 115
This laboratory report is flOt valid IVithout all authorized signature 011 the cOIer page
Reportable Detection Limit BRL Below Reporting Limit Page 21 of 25
General Chemistry Parameters - Quality Control
Spike Source REC RPD
Analyte( s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051049 - General Preparation
Blank S051 049-BLK1
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
Blank S051049-BLK2
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
Blank S051 049-BLK3
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
LCS S051049-BS1
Prepared amp Analyzed 14-May-
Total Residual Chlorine 046 mgl 020 0500 90- 110
LCS S051049-BS2
Prepared amp Analyzed 14-May-
Total Residual Chlorine 047 mgl 020 0500 90- 110
LCS S051049-BS3
Prepared amp Analyzed 14-May-
Total Residual Chlorine 054 mgl 020 0500 108 90-110
licate B051049-DUP1 Source SA7S544shy
Prepared amp Analyzed 14-May-
Total Residual Chlorine 012 mgl 020 010
licate S051049-DUP2 Source SA7S602-01
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020 BRL
Matrix S ike 8051049-MS1 Source SA78544-01
Prepared amp Analyzed 14-May-
Total Residual Chlorine 065 mgl 020 0500 010 110 80- 120
Matrix S ike 8051049-MS2 Source SA7B602shy
Prepared amp Analyzed 14-May-
Total Residual Chlorine mgl 500 125 BRL 108 80- 120
Reference 8051 049-SRM1
Prepared amp Analyzed 14-May-
Total Residual Chlorine 100 mgl 020 0967 103 85-115
Batch 8051094 - General Preparation
Blank 8051094-BLK1
Prepared amp Analyzed 14 May-
Hexavalent Chromium (soluble) BRL mgl 005
Blank 8051 094-BLK2
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) BRL mgl 005
LCS 8051094-BS1
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) 054 mgl 005 90- 110
licate 8051094-DUP1 Source SA78602-01
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) BRL mgl 125 BRL
Thi laboratory report is not valid without all authorized sigllature 011 the cover page
Page 22 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Page 20
Sam le Identification Client Pro ect Matrix Collection DateTime Received
MWshy2920-96- Ground Water 13-May-081030 14-May-
SA 78602shy
CAS No Analyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Semivolatie Organic Compounds by GCMS
Semi volatile Or anic Com ounds b EPA 625
Prepared by method SW846 3510C 50 EPA 625 16-May- 19-May-08 805121683-32- Acenaphthene BRL IJgl
208-96-8 Acenaphthylene BRL IJgl 50
62-53- BRL IJgll 50Aniline
120- 12- Anthracene BRL 1J91 50
103-33- AzobenzenefDiphenyldiazine BRL IJgl 50
92-87 - Benzidine BRL IJgl 50
56-55- Benzo (a) anthracene BRL 1J91 50
50-32 - Benzo (a) pyrene IJglBRL 50
205-99- Benzo (b) fluoranthene BRL IJgl 50
191-24- Benzo (g i) perylene BRL IJgl 50
50207-08- Benzo (k) fluoranthene BRL IJgl
65-85 Benzoic acid BRL 1J91 50
100-51-6 Benzyl alcohol 1J91BRL 50
50111-91- Bis(2-chloroethoxy)methane BRL 1J91
111-4-4 Bis(2-chloroethyl)ether BRL IJgl 50
501 08-60- Bis(2-chloroisopropyl)ether BRL IJgl
117-81- Bis(2-ethylhexyl)phthalate BRL 1J91 50
101-55- Bromophenyl phenyl ether BRL IJgl 50
5085-68- Butyl benzyl phthalate BRL IJgl
5086-74- Carbazole BRL IJgl
5059-50- C hloro-3-methylphenol BRL IJgl
106-47- Chloroaniline BRL IJgl 50
91-58- Chloronaphthalene IJglBRL 50
5095-57 - Chlorophenol BRL 1J91
507005-72- Chlorophenyl phenyl ether BRL IJgl
216-01- Chrysene tJ91BRL 50
5053-70- Dibenzo (a h) anthracene BRL IJgl
50132-64- Dibenzofuran BRL IJgl
95-50- Dichlorobenzene IJglBRL 50
541-73- 13- Dichlorobenzene BRL IJgl 50
106-46- Dichlorobenzene 1J91BRL 50
5091-94- 3 - Dichlorobenzidine BRL IJgl
120-83- Dichlorophenol BRL IJgl 50
84-66- Diethyl phthalate BRL IJgl 50
131-11- Dimethyl phthalate BRL IJgll 50
105-67- Dimethylphenol BRL 1J91 50
5084-74- Di-n- butyl phthalate BRL 1J91
534-52 - Dinitro-2-methylphenol BRL IJgl 50
51-28- Dinitrophenol IJglBRL 50
50121-14- Dinitrotoluene BRL 1J91
606-20- Dinitrotoluene IJglBRL 50
50117-84-0 Di-n-octyl phthalate BRL IJgl
206-44-0 Fluoranthene 1J91BRL 50
BRL 50
50 86-73- Fluorene IJgi
118-74- Hexachlorobenzene BRL 1J91
87-68- Hexachlorobutadiene 1J91BRL 50
5077-47-4 Hexachlorocyclopentadiene BRL IJgl
67-72- Hexachloroethane IJglBRL 50
50193-39- Indeno (1 3-cd) pyrene BRL IJgl
5078-59- Isophorone BRL IJgl
Tfls laboratory report is not valid without all authorized signature 011 the coverpage
Page 6 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Sam le Identification Client Pro ect Matrix Collection DateTime ReceivedMWshy
2920-96- Ground Water I3-May-081030 14-May-SA 78602shy
CAS No Analyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Semivolatile Organic Compounds by GCMS
Semi volatile Or anic Com ounds b EPA 625
Prepared by method SW846 3510C
91-57 -6 Methylnaphthalene 367 1-91 50 EPA 625 16-May- 19-May-08 8051216
95-48- Methylphenol BRL 1-91 50
108-39-4 3 amp 4-Methylphenol BRL I-gl 100 106-44shy91-20- Naphthalene 247 1-91 50
88-74-4 Nitroaniline BRL 1-91 50
99-09- Nitroaniline BRL 1-91 50
100-01-6 Nitroaniline BRL 1-91 50
98-95- Nitrobenzene BRL 1-91 50
88-75- Nitrophenol BRL 1-91 50
100-02- Nitrophenol BRL 1-91 50
62-75- Nitrosodimethylamine BRL 1-91 50
621-64- N- Nitrosodi-n-propylamine BRL 1-91 50
86-30-6 Nitrosodiphenylamine BRL 1-91 50
87 -86- Pentachlorophenol BRL 1-91 50
85-0- Phenanthrene BRL 1-91 50
108-95- Phenol BRL 1-91 50
129-00-0 Pyrene BRL 1-91 50
110-86- Pyridine BRL 1-91 50
120-82- 4- Trichlorobenzene BRL 1-91 50
95-95- 5- Trichlorophenol BRL 1-91 50
88-06- 6- T richlorophenol BRL 1-91 50
Surrogate recoveries
321-60- Fluorobipheny 30- 130
367- 12- Fuorophenol 15- 110
4165-60- Nitrobenzene- 30- 130
4165-62- Pheno- 15- 110
1718-51- Terpheny-d4 30- 130
118- 79- 6- Tribromophenol 15- 110
Semivolatile Organic Compounds by GC
Pol chlorinated Bi hen ls b EPA 608
Prepared by method SW846 3510C
12674- 11-2 Aroclor- 1016 BRL 1-91 0650 EPA 608 15- May- 16-May-08 8051106
11104-28-2 Aroclor-1221 BRL IJgl 0650
11141-16-5 Aroclor- 1232 BRL 1-91 0650
53469-21-9 Aroclor- 1242 BRL 1-91 0650
12672-29-6 Aroclor- 1248 BRL 1-91 0650
11097-69-1 Aroclor- 1254 BRL 1-91 0650
11096-82-5 Aroclor -1260 BRL 1-91 0650
37324-23-5 Aroclor-1262 BRL 1-91 0650
11100-14-4 Aroclor-1268 BRL IJgl 0650
Surrogate recoveries
2051-24- Decachlorobipheny (Sr) 105 30- 150
10386-84-2 4 DB-Octafluorobiphenyl (Sr) 30- 150
Extractable Petroleum Hydrocarbons
mgl EPA 1664 Rev A 15-May- 19-May-08 8051102Non-polar material (SGT- HEM)
Soluble Metals by EPA 2006000 Series Metbods
Field Filtered NA EPA 200 73005A 15- May- 15-May-08 8051192Filtration
Soluble Metals by EPA 200 Series Methods
7440-22-4 Silver BRL mgl 0002 EPA 200 21-May- 27- May-08 8051249
This laboratory report is IlOt mlid without (II authorized signature on the cover page
Reportble Detection Limit BRL = Below Reporting Limit Page 7 of 25
Sam le Identification MW-
Client Pro ect 2920-96shy
Matrix Ground Water
Collection DateTime 13-May-08 1030
Received 14-May-
SA 78602shy
CAS No A nalyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Soluble Metals by EPA 200 Series Methods
7440-38shy Arsenic 0468 mg1 0040 EPA 200 21-Mayshy 21-May-08 80511 50
7440-43shy Cadmium BRL mg1 0002 EPA 200 21-May-088051249
7440-47shy Chromium BRL mg1 0050 EPA 200 21-May-088051150
7440-50-8 Copper BRL mg1 0050
7439-89-6 Iron 184 mg1 0150
7439-97-6 Mercury BRL mg1 00020 EPA 245 17470A 21-May-088051152
7440-02-0 Nickel BRL mg1 0050 EPA 200 21-May-088051150
7439-92shy Lead 0011 mg1 0002 EPA 200 21-May-088051249
7440-36-0 Antimony 0003 mg1 0002
7782-49shy Selenium BRL mg1 0150 EPA 200 21-May-08 8051150
7440-66-6 Zinc 0186 mgl 0050
General Chemistry Parameters
Filtration Completed NA Varies 14-Mayshy 14-May-08 8051095
18540-29-9 Hexavalent Chromium (soluble) BRL HT2 mg1 125 SM3500CrDI796A 14-Mayshy 14-May-08 8051094 R01 2013 2016
57-12shy Cyanide (total) BRL mg1 0100 EPA 3354 19-Mayshy 19-May-088051374
7782-50shy Total Residual Chlorine BRL CIHT mg1 500 Hach 8167 14-Mayshy 14-May-08 8051049 R01 1900 2001
Total Suspended Solids 580 mg1 25 SM2540D 16-Mayshy 16-May-08 8051275
This lahomtOlY report is not valid without an authorized signature on the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page 8 of 25
Volatie Organic Compounds - Quality Control
Analyte( s)
Batch 8051244 - SW846 5030 Water MS
Blank 8051244-BLK1
Prepared 16-May-08 Analyzed 17-May-
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromochloromethane
1 Dichlorobenzene
1 Dichlorobenzene
1 Dichlorobenzene
1-Dichloroethane
1 Dichloroethane
1 1-Dichloroethene
cis- Dichloroethene
trans- 1 Dichloroethene
1 Dichloropropane
cis- 1 Dichloropropene
trans- 1 Dichloropropene
Ethylbenzene
Hexanone (MBK)
Methyl tert-butyl ether
Methyl- pentanone (MIBK)
Methylene chloride
Styrene
2- Tetrachloroethane
Tetrachloroethene
Toluene
1- Trichloroethane
2- Trichloroethane
Trichloroethene
Trichlorofluoromethane (Freon 11)
Vinyl chloride
p-Xylene
Xylene
Surrogate 4-Bromofluorobenzene Surrogate Toluene-
Surrogate 1 Dichloroethane-Surrogate Dibromofluoromethane
LCS B051244-BS1
Prepared 16-May-08 Analyzed 17 -May-
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Spike Source REC RPD
Result Flag Units RDL Level Result REC Limits RPD Limit
BRL gl 20
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl 10
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gll
BRL gi
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl 10
BRL gll
BRL gll 10
BRL gl 10
BRL gll
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
41 gl 50 70- 130 49 gl 50 70- 130 59 gl 50 119 70- 130 52 gl 50 105 70- 130
QC2 jgl 20 70- 130
18 jgl 20 70- 130
192 jgl 20 35- 155
18 jgl 20 45- 169
19 jgl 20 242
This laboratOlY repol1 is lot valid without 011 authorized sigllature 011 the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page 9 of 25
Volatie Organic Compounds - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051244 - SW846 5030 Water MS
LC5 8051244B51
Prepared 16-May-08 Analyzed 17-May-
Butanone (MEK) 10 QC2 gl 20 70- 130
Carbon tetrachloride 204 gl 20 102 70- 140
Chlorobenzene 18 gl 20 70- 130
Chloroethane 164 gl 20 14-230
Chloroform 18 gll 20 51- 138
Chloromethane 21 gl 20 106 273
Dibromochloromethane 18 gl 20 53- 149
1 Dichlorobenzene 20 gl 20 104 18- 190
1 Dichlorobenzene 19 gl 20 59- 156
1 A-Dichlorobenzene 18 gl 20 18- 190
1- Dichloroethane 19 gl 20 59- 155
1 Dichloroethane 19 gl 20 49- 155
1-Dichloroethene 16 gl 20 70- 130
cis- 1 Dichloroethene 17 gl 20 70- 130
trans- 1 Dichloroethene 16 gll 20 54- 156
1 Dichloropropane 18 gl 20 210
cis- Dichloropropene 17 gl 20 227
trans- 1 Dichloropropene 17 gl 20 17- 183
Ethylbenzene 19 gl 20 37- 162
Hexanone (MBK) 124 QC2 gl 20 70- 130
Methyl tert-butyl ether 19 gl 20 70- 130
Methylshy pentanone (MIBK) 17 gl 20 70- 130
Methylene chloride 16 gl 20 221
Styrene 17 gl 20 70- 130
1 Tetrachloroethane 194 gl 20 46- 157
Tetrachloroethene 15 gl 20 64- 148
Toluene 18 gl 20 70- 130
1- Trichloroethane 20 gl 20 100 52- 162
2- Trichloroethane 18 gl 20 52- 150
Trichloroethene 17 gl 20 71- 157
Trichlorofluoromethane (Freon 11) 19 gl 20 17- 181
Vinyl chloride 21 gl 20 106 251
p-Xylene 39 gl 40 70- 130
Xylene 20 gl 20 102 70- 130
Surrogate 4-Bromofluorobenzene Surrogate Toluene-
Surrogate 1 Dichloroethane-Surrogate Dibromofluoromethane
52 49 56
49
gl
gl
gl
gl
50 50 50
50
105
112 100
70- 130 70- 130 70- 130 70- 130
LC5 DUD (8051244-B5D1
Prepared 16-May-08 Analyzed 17-May-
Acetone QC2 gl 20 70- 130
Benzene 18 gl 20 70- 130
Bromodichloromethane 18 gl 200 35- 155
Bromoform 17 gl 20 45- 169
Bromomethane 18 gl 20 242
Butanone (MEK) 11 QC2 1-91 20 70- 130
Carbon tetrachloride 20 gl 20 100 70- 140
Chlorobenzene 17 gl 20 70- 130
Chloroethane 15 1-91 20 14-230
Chloroform 18 1-91 20 51- 138
This laboratory report is aot valid without a1 authorized sig1ature 01 the cover page
Reportble Detection Limit BRL = Below Reporting Limit Page 10 of25
Volatie Organic Compounds - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051244 - SW846 5030 Water MS
LCS Dup 18051244-BSD1
Prepared 16-May-08 Analyzed 17-May-
Chloromethane 18 1-91 20 273
Dibromochloromethane 174 1-91 20 53- 149
Dichlorobenzene 20 1-91 20 100 18- 190
Dichlorobenzene 18 1-91 20 59- 156
Dichlorobenzene 18 1-91 20 18- 190
Dichloroethane 18 1-91 20 59- 155
Dichloroethane 19 1-91 20 49- 155
Dichloroethene 16 1-91 20 70- 130
cis- Dichloroethene 16 1-91 20 70- 130
trans- Dichloroethene 15 1-91 20 54- 156
Dichloropropane 17 1-91 20 210
cis- Dichloropropene 164 IJgl 20 227
trans- 1 Dichloropropene 164 I-gl 20 17- 183
Etlwlbenzene 18 IJgl 20 37- 162
Hexanone (MBK) 124 QC2 IJgl 20 70- 130
Methyl tert-butyl ether 184 1J91 20 70- 130
Methyl- pentanone (MIBK) 17 IJgl 20 70- 130
Methylene chloride 16 IJgl 20 221
Styrene 16 IJgl 20 70- 130
2- Tetrachloroethane 19 IJgl 20 46- 157
Tetrachloroethene 15 IJgl 20 64- 148
Toluene 17 IJgl 20 70- 130
1- Trichloroethane 19 1-91 20 52- 162
2- Trichloroethane 16 IJgl 20 52- 150
Trichloroethene 15 IJgl 20 71- 157
Trichlorofluoromethane (Freon 11) 17 IJgl 20 17- 181
Vinyl chloride 19 IJglI 20 251
p-Xylene 37 1J91 40 70- 130
Xylene 20 IJgl 20 100 70- 130
Surrogate 4-Bromofluorobenzene 51 IJgl 50 104 70- 130
Surrogate Toluene- 4B gl 50 70- 130
Surrogate 1 0ichloroethane- 53 IJgl 50 106 70- 130 Surrogate Oibromofluoromethane 50 1J9i 50 102 70- 130
Matrix S ike B051244-MS1 Source SA7B629shy
Prepared 16-May-08 Analyzed 17-May-
Benzene 18 20 BRL 70- 130IJgl
Bromodichloromethane 19 IJgl 20 BRL 35- 155
Bromoform 18 IJgl 20 BRL 45- 169
Bromomethane 16 IJgl 20 BRL 242
Carbon tetrachloride 21 IJgl 20 BRL 106 70- 140
Chlorobenzene 18 IJgl 20 BRL 70- 130
Chloroethane 16 IJgl 20 BRL 14-230
Chloroform 18 IJgl 20 BRL 51- 138
Chloromethane 19 IJgl 20 BRL 273
Dibromochloromethane 17 IJgl 20 BRL 53- 149
1 Dichlorobenzene 22 IJgl 20 BRL 112 18- 190
1 Dichlorobenzene 22 IJgl 20 BRL 110 59-156
1 Dichlorobenzene 21 IJgl 20 BRL 109 18- 190
1- Dichloroethane 19 IJgl 20 BRL 59- 155
1 Dichloroethane 18 IJgl 20 BRL 49- 155
This laboratory report is 110t mUd without an authorized signature on the covel page
Reportble Detection Limit BRL = Below Reporting Limit Page It of25
Volatile Organic Compounds - Quality Control
p
Spike Source REC RPD
Result REC imits RPD LimitAnalyte(s) Result Flag Units RDL Level
Batch 8051244 - SW846 5030 Water MS
Matrix ike S051244-MS1 Source SA7B629shy
Prepared 16-May-08 Analyzed 17-Mayshy
17 20 BRL 70- 130 1- Dichloroethene IJgl
16 20 BRL 54- 156trans- 1 Dichloroethene IJgl
21020 BRL1 Dichloropropane 17 1J91
cis- 1 Dichloropropene 17 IJgl 20 BRL 227
17- 183trans- 1 Dichloropropene 184 1J91 20 BRL
20 20 BRL 103 37- 162Ethylbenzene IJgl
15 20 BRL 221Methylene chloride IJgl
20 BRL 46- 1572- Tetrachloroethane 19 1J91
20 BRL 64- 148Tetrachloroethene 18 1J91
BRL 70- 130Toluene 18 1J91 20
105 52-1621- Trichloroethane 211 IJgl 20 BRL
18 20 BRL 52- 1502- Trichloroethane IJgl
17 20 BRL 71- 157Trichloroethene 1J91
20 BRL 17- 181Trichloroluoromethane (Freon 11) 194 IJgl
20 BRL 103 251Vinyl chloride 20 IJgl
102 70- 130Surrogate 4-Bromofluorobenzene 50 IJgl 50 50 70- 130Surrogate Toluene- 49 1J91
56 50 112 70- 130Surrogate 1 Dichloroethane- IJgl
50 100 70- 130Surrogate Dibromofluoromethane 50 IJgl
Matrix S ike Du S051244-MSD1 Source SA7S629shy
Prepared 16-May-08 Analyzed 17-Mayshy
18 20 BRL 70- 130Benzene IJgl
18 20 BRL 35- 155Bromodichloromethane IJgl
17 20 BRL 45- 169Bromoform IJgl
20 BRL 242Bromomethane 17 IJgl
20 BRL 103 70- 140Carbon tetrachloride 20 IJgl
18 20 BRL 70- 130Chlorobenzene 1J91
14-230Chloroethane 16 IJgl 20 BRL
20 51- 138Chloroform 184 IJgl BRL
Chloromethane 19 1J91 20 BRL 273
18 20 BRL 53- 149Dibromochloromethane 1J91
20 BRL 117 18- 190Dichlorobenzene 234 IJgl
20 BRL 112 59- 156Dichlorobenzene 22 IJgl
BRL 108 18- 190Dichlorobenzene 21 1J91 20
20 59- 1551 Dichloroethane 19 IJgl BRL
18 20 BRL 49- 155Dichloroethane IJgl
16 20 BRL 70- 130Dichloroethene IJgl
20 BRL 54- 156trans- Dichloroethene 154 1J91
20 BRL 210Dichloropropane 17 IJgl
0420 BRL 227cis- Dichloropropene 17 IJgl
17- 183trans- Dichloropropene 17 1J91 20 BRL
BRL 37- 162Ethylbenzene 20 1J91 20 102
Methylene chloride 15 IJgl 20 BRL 221
20 BRL 46- 1572- Tetrachloroethane 192 IJgl
20 BRL 64- 148 04Tetrachloroethene 18 IJgl
BRL 70- 130Toluene 184 1J91 20
52- 1621- Trichloroethane 20 IJgl 20 BRL 104
17 20 BRL 52- 1502- Trichloroethane IJgl
17 20 BRL 71- 157Trichloroethene IJgl
20 BRL 17-181Trichlorofluoromethane (Freon 11) 19 IJgl
This laboratory report is IIOt valid without all authorized sigllllture 011 the cover page
Page 12 of25 Reportble Detection Limit BRL = Below Reporting Limit
Semivolatile Organic Compounds by GCMS - Quality Control
Analyte(s)
Batch 8051216 - SW846 3510C
Blank 8051216-BLK1
Prepared amp Analyzed 16-May-
Isophorone
Methylnaphthalene
Methylphenol
3 amp 4-Methylphenol
Naphthalene
Nitroaniline
Nitroaniline
Nitroaniline
Nitrobenzene
Nitrophenol
Nitrophenol
Nitrosodimethylamine
N- N itrosodi-n-pro pyla mine
N itrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Pyridine
1 24-Trichlorobenzene
24 5- Trichlorophenol
246- Trichlorophenol
Surrogate 2-Fuorobipheny Surrogate 2-Fuoropheno Surrogate Nitrobenzene-Surrogate PhenoshySurrogate Terpheny-d4 Surrogate 6- Tribromopheno
LCS B051216-BS1
Prepared amp Analyzed 16-May-
Acenaphthene
Acenaphthylene
Aniline
Anthracene
AzobenzenelDi phenyld lazine
Benzidine
Benzo (a) anthracene
Benzo (a) pyrene
Benzo (b) fluoranthene
Benzo (g i) perylene
Benzo (k) fluoranthene
Benzoic acid
Benzyl alcohol
B is(2-chloroethoxy)methane
B i s (2-ch loroethyl)eth e r
Bis(2-ch loroisopropyl) ether
B is(2-ethy Ih exyl) phtha late
Bromophenyl phenyl ether
Butyl benzyl phthalate
Carbazole
Spike Source REC RPD
Result Flag Units RDL Level Result REC Limits RPD Limit
BRL gl
BRL gl
BRL gl
BRL gl 10
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gll
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
370 gl 50 30- 130 40 gl 50 15- 110 39 gl 50 30- 130 43 gl 50 15- 110 36 gl 50 30- 130 40 gl 50 15- 110
41 gl 50 40- 140
43 gI 50 40- 140
41 gl 50 40- 140
38 gl 50 40- 140
45 gl 50 40- 140
49 gl 50 153
41 gl 50 40- 140
43 gl 50 40- 140
41 gl 50 40- 140
41 gll 50 40- 140
45 gl 50 40- 140
32 gl 50 12- 149
41 gl 50 40- 140
39 gl 50 40- 140
384 gl 50 40- 140
47 gl 50 40- 140
47 gl 50 40- 140
40 gl 50 40- 140
47 gI 50 40- 140
56 gI 50 112 200
This laboratory report is lIot valid witllOut a1l authorized sigllature 011 the coverpage
Reportble Detection Limit BRL = Below Reporting Limit Page 15 of25
Semivolatile Organic Compounds by GCMS - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051216 - SW846 3510C
LCS 8051216-BS1
Prepared amp Analyzed 16-Mayshy
50 30- 1304 -C hloro-3-methylphenol 42 IJgl
40- 140Chloroaniline 39 IJgl 50
Chloronaphthalene 37 IJgl 50 40- 140
Chlorophenol 37 IJgl 50 30- 130
50 40- 140
40- 140
Chlorophenyl phenyl ether 45 IJgl
Chrysene 43 IJgl 50
Dibenzo (a h) anthracene 43 IJgl 50 40- 140
Dibenzofuran IJgl38 50 40- 140
50 40- 1401 Dichlorobenzene 35 IJgl
40- 1401 Dichlorobenzene 264 IJgl 50
40- 1401 Dichlorobenzene 434 IJgl 50
58 50 116 40- 1403 - Dichlorobenzidine IJgl
50 30- 130
40- 140 24-Dichlorophenol 38 IJgl
Diethyl phthalate 484 IJgl 50
50 40- 140Dimethyl phthalate 464 IJgl
Dlmethylphenol 39 IJgl 50 30- 130
DI-n-butyl phthalate 44 IJgll 50 40- 140
30- 130 6-Di nitro- 2-methylphenol 38 1J91 50
30- 130Dinltrophenol 36 1J91 50
42 50 40- 14024-Dlnitrotoluene 1J91
Dlnitrotoluene 1J9141 50 40- 140
Di-n-octyl phthalate 52 IJgl 50 104 40- 140
40- 140Fluoranthene 40 IJgl 50
Fluorene 41 IJgl 50 40- 140
39 50 40- 140Hexachlorobenzene IJgl
50 40- 140Hexachlorobutadiene 40 IJgl
40- 140Hexach lorocyclopentad iene 294 IJgl 50
40 50 40- 140Hexachloroethane IJgl
42 50 40-140Indeno (1 3-cd) pyrene IJgl
50 40- 140Isophorone 40 IJgl
40- 140Methylnaphthalene 394 IJgl 50
40- 140Methylphenol 39 IJgl 50
40 10 50 40- 1403 amp 4-Methylphenol IJgl
37 50 40-140Naphthalene IJgl
50 40-140Nitroaniline 39 IJgl
Nitroaniline 51 IJgl 50 102 40- 140
48 50 40- 140Nltroaniline 1J91
50 40- 140Nitrobenzene 40 IJgl
30- 130Nitrophenol 36 IJgl 50
40 IJgl 50 30- 130Nitrophenol 40- 140Nitrosodimethylamine 32 1J91 50
50 40-140N- N itrosodi-n-propyla mine 46 IJgl
40- 140N itrosodi phenyla ml ne 44 IJgl 50
41 IJgl 50 30- 130Pentachlorophenol 40- 140Phenanthrene 38 IJgl 50
50 30- 130Phenol 38 IJgl
40- 140Pyrene 424 1J91 50
40- 140Pyridine 294 1J91 50
40- 14024- Trichlorobenzene 364 IJgl 50
This laboratory report is not mlid without an authorized signature 011 the cover page
Page 16 of25 Reportble Detection Limit BRL = Below Reporting Limit
Semivolatie Organic Compounds by GCMS - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
BMch 8051216 - SW846 3510C
LC5 8051216-851
Prepared amp Analyzed 16-Mayshy
24 5- Trichlorophenol 404 gl 50 30- 130
246- Trichlorophenol 42 gl 50 30- 130
Surrogate 2-Fluorobiphenyl 29 gl 50 30- 130
Surrogate 2-Fluorophenot 27 gl 50 15- 110
Surrogate Nitrobenzene- 30 gl 50 30- 130
Surrogate Phenol- 29 gl 50 15- 110
Surrogate Terpheny-d4 30 gl 50 30- 130
Surrogate 6- Tribromopheno 324 gl 50 15- 110
This laboratory report is lIot valid without all authorized sigllature 011 tlle cover page
Reportble Detection Limit BRL = Below Reporting Limit Page 17 of25
Semivolatie Organic Compounds by GC - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051106 - SW846 3510C
Blank S051106-BLK1
Prepared amp Analyzed 15-Mayshy
Aroclor- 1016 BRL gI 0200
Aroclor- 1016 (2C) BRL gI 0200
Aroclor- 1221 BRL gI 0200
Aroclor- 1221 (2C) BRL gI 0200
Aroclor- 1232 BRL gI 0200
Aroclor- 1232 (2Cj BRL gI 0200
Aroclor- 1242 BRL gI 0200
Aroclor-1242 (2C) BRL gI 0200
Aroclor- 1248 BRL gI 0200
Aroclor- 1248 (2C) BRL gI 0200
Aroclor- 1254 BRL gI 0200
Aroclor- 1254(2Cj BRL gI 0200
Aroclor- 1260 BRL gI 0200
Aroclor- 1260 (2C) BRL gI 0200
Aroclor- 1262 BRL gI 0200
Aroclor- 1262 (2C) BRL gI 0200
Aroclor-1268 BRL gI 0200
Aroclor- 1268 (2C) BRL gI 0200
Surrogate Decachlorobiphenyl (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0231 0224 0194 0191
gI
gI
gI
gI
0200 0200 0200 0200
116 112
30- 150 30- 150 30- 150 30- 150
LC5 8051106-B51
Prepared 15-May-08 Analyzed 16-May-08
Aroclor- 1016 265 gI 0200 250 106 50- 114
Aroclor- 1 016 (2C) 240 gI 0200 250 50- 114
Aroclor- 1260 0269 gI 0200 250 107 40- 127
Aroclor-1260 (2Cj 270 gI 0200 250 108 40- 127
Surrogate Decachlorobiphenyl (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0225 0224 0188 0183
gI
gI
gI
gI
0200 0200 0200 0200
113 112
30- 150 30- 150 30- 150 30- 150
LC5 DUD rS051106-B5D1
Prepared 15-May-08 Analyzed 16-Mayshy
Aroclor- 1016 262 gl 0200 250 105 50- 114
Aroclor-1 016 (2Cj 241 gI 0200 250 50- 114
Aroclor- 1260 277 gI 0200 250 111 40- 127
Aroclor- 1260(2Cj 0260 gI 0200 250 104 40- 127
Surrogate Decachlorobipheny (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0238 0218 0189 0181
gI
gI
gI
gI
0200 0200 0200 0200
119 109
30- 150 30- 150 30- 150 30- 150
This laboratory report is lot valid without (II authorized sigllature 01 the cover page
Page 18 of25 Reportable Detection Limit BRL = Below Reporting Limit
Extractable Petroleum Hydrocarbons - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051102 - SW846 3510C
Blank 8051102-BLK1
Prepared 15-May-08 Analyzed 19-Mayshy
Non-polar material (SGT- HEM) BRL m91
LC8 8051102-B81
Prepared 15-May-08 Analyzed 19-Mayshy
Non-polar material (SGT- HEM) 184 m91 21 81 904
This laboratory report is not valid without an authorized signature 011 the cover page
Page 19 of25 Reportable Detection Limit BRL = Below Reporting Limit
Soluble Metals by EPA 200 Series Methods - Quality Control
Analyte(s) Result Flag Units RDL
Spike
Level
Source
Result REC
REC
Limits RPD
RPD
Limit
Batch 8051150 - EPA 200 Series
Blank 8051150-BLK1
Prepared amp Analyzed 21-May-
Iron
Zinc
Selenium
Nickel
Chromium
Copper
Arsenic
BRL
BRL
BRL
BRL
BRL
BRL
BRL
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0150
0050
0150
0050
0050
0050
0040
LCS 8051150-BS1
Prepared amp Analyzed 21-May-
Selenium
Zinc
Iron
Nickel
Chromium
Arsenic
Copper
123
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0150
0050
0150
0050
0050
0040
0050
103
105
101
100
85- 115
85- 115
85- 115
85- 115
85- 115
85-115
85- 115
licate B051150-DUP1 Source SA7B602shy
Prepared amp Analyzed 21-May-
Iron
Zinc
Selenium
Nickel
Copper
Chromium
Arsenic
17
0162
BRL
0015
0017
BRL
0450
QR8
mgl
mgl
mgl
mgl
mgl
mgl
mgi
0150
0050
0150
0050
0050
0050
0040
184
0186
BRL
0014
0023
BRL
0468
Matrix S ike 8051150-MS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Iron
Selenium
Nickel
Zinc
Copper
Chromium
Arsenic
19 QM2 mgl
mgll
mgl
mgl
mgl
mgl
mgl
0150
0150
0050
0050
0050
0050
0040
125
184
BRL
0014
0186
0023
BRL
0468
104
105
102
70- 130
70- 130
70-130
70- 130
70- 130
70-130
70- 130
Post S ike 8051150-PS1 Source SA78602shy
Prepared amp Analyzed 21-May-
Zinc
Iron
Selenium
Nickel
Copper
Arsenic
Chromium
18 QM2
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0050
0150
0150
0050
0050
0040
0050
0186
184
BRL
0014
0023
0468
BRL
104
104
101
85- 115
85- 115
85- 115
85-115
85-115
85- 115
85-115
Batch 8051152 - EPA200SW7000 Series
Blank B051152-BLK1
Prepared amp Analyzed 21-May-
Mercury BRL mgl 00020
This laboratory report is IIOt valid witllOut all authorized sigllature 011 the coverpage
Page 20 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Soluble Metals by EPA 200 Series Methods - Quality Control
Analyte(s) Result Flag Units RDL
Spike
Level
Source
Result REC
REC
Limits RPD
RPD
Limit
Batch 8051152 - EPA200SW7000 Series
LCS B051152-BS1
Prepared amp Analyzed 21-May-
Mercury 00576 m91 00020 00500 115 85- 115
licate B051152-DUP1 Source SA78602-01
Prepared amp Analyzed 21-May-
Mercury BRL m91 00020 BRL
Matrix S ike 8051152-MS1 Source SA78602shy
Prepared amp Analyzed 21-May-
Mercury 00632 OM m91 00020 00500 BRL 126 75- 125
Post S ike 8051152-PS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Mercury 00624 OC1 m91 00020 00500 BRL 125 85- 115
Batch 8051249 - 2008No digestion
Blank 8051249-BLK1
Prepared amp Analyzed 21-May-
Lead
Antimony
Cadmium
Silver
BRL
BRL
BRL
BRL
m91
m91
m91
m91
0002
0002
0002
0002
LCS B051249-BS1
Prepared amp Analyzed 21-May-
Antimony
Lead
Silver
Cadmium
143
145 OC2
m91
m91
m91
m91
0050
0050
0050
0040
103
115
107
116
85- 115
85- 115
85- 115
85- 115
licate 8051249-DUP1 Source SA7B602shy
Prepared amp Analyzed 21- May-
Lead
Antimony
Cadmium
Silver
0009
0002
00005
00002
ORB
m91
m91
m91
m91
0002
0002
0002
0002
0011
0003
00005
00003
Matrix S ike 8051249-MS1 Source SA78602shy
Prepared amp Analyzed 21- May-
Lead
Antimony
Cadmium
Silver
142
m91
m91
m91
m91
0050
0050
0040
0050
0011
0003
00005
00003
111
101
114
102
70- 130
70-130
70c130
70- 130
Post S ike 8051249-PS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Antimony
Cadmium
Silver
38
OC2
m91
m91
m91
0050
0040
0050
125
0003
00005
00003
110
121
109
85- 115
85- 115
85- 115
This laboratory report is flOt valid IVithout all authorized signature 011 the cOIer page
Reportable Detection Limit BRL Below Reporting Limit Page 21 of 25
General Chemistry Parameters - Quality Control
Spike Source REC RPD
Analyte( s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051049 - General Preparation
Blank S051 049-BLK1
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
Blank S051049-BLK2
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
Blank S051 049-BLK3
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
LCS S051049-BS1
Prepared amp Analyzed 14-May-
Total Residual Chlorine 046 mgl 020 0500 90- 110
LCS S051049-BS2
Prepared amp Analyzed 14-May-
Total Residual Chlorine 047 mgl 020 0500 90- 110
LCS S051049-BS3
Prepared amp Analyzed 14-May-
Total Residual Chlorine 054 mgl 020 0500 108 90-110
licate B051049-DUP1 Source SA7S544shy
Prepared amp Analyzed 14-May-
Total Residual Chlorine 012 mgl 020 010
licate S051049-DUP2 Source SA7S602-01
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020 BRL
Matrix S ike 8051049-MS1 Source SA78544-01
Prepared amp Analyzed 14-May-
Total Residual Chlorine 065 mgl 020 0500 010 110 80- 120
Matrix S ike 8051049-MS2 Source SA7B602shy
Prepared amp Analyzed 14-May-
Total Residual Chlorine mgl 500 125 BRL 108 80- 120
Reference 8051 049-SRM1
Prepared amp Analyzed 14-May-
Total Residual Chlorine 100 mgl 020 0967 103 85-115
Batch 8051094 - General Preparation
Blank 8051094-BLK1
Prepared amp Analyzed 14 May-
Hexavalent Chromium (soluble) BRL mgl 005
Blank 8051 094-BLK2
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) BRL mgl 005
LCS 8051094-BS1
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) 054 mgl 005 90- 110
licate 8051094-DUP1 Source SA78602-01
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) BRL mgl 125 BRL
Thi laboratory report is not valid without all authorized sigllature 011 the cover page
Page 22 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Page 21
Sam le Identification Client Pro ect Matrix Collection DateTime ReceivedMWshy
2920-96- Ground Water I3-May-081030 14-May-SA 78602shy
CAS No Analyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Semivolatile Organic Compounds by GCMS
Semi volatile Or anic Com ounds b EPA 625
Prepared by method SW846 3510C
91-57 -6 Methylnaphthalene 367 1-91 50 EPA 625 16-May- 19-May-08 8051216
95-48- Methylphenol BRL 1-91 50
108-39-4 3 amp 4-Methylphenol BRL I-gl 100 106-44shy91-20- Naphthalene 247 1-91 50
88-74-4 Nitroaniline BRL 1-91 50
99-09- Nitroaniline BRL 1-91 50
100-01-6 Nitroaniline BRL 1-91 50
98-95- Nitrobenzene BRL 1-91 50
88-75- Nitrophenol BRL 1-91 50
100-02- Nitrophenol BRL 1-91 50
62-75- Nitrosodimethylamine BRL 1-91 50
621-64- N- Nitrosodi-n-propylamine BRL 1-91 50
86-30-6 Nitrosodiphenylamine BRL 1-91 50
87 -86- Pentachlorophenol BRL 1-91 50
85-0- Phenanthrene BRL 1-91 50
108-95- Phenol BRL 1-91 50
129-00-0 Pyrene BRL 1-91 50
110-86- Pyridine BRL 1-91 50
120-82- 4- Trichlorobenzene BRL 1-91 50
95-95- 5- Trichlorophenol BRL 1-91 50
88-06- 6- T richlorophenol BRL 1-91 50
Surrogate recoveries
321-60- Fluorobipheny 30- 130
367- 12- Fuorophenol 15- 110
4165-60- Nitrobenzene- 30- 130
4165-62- Pheno- 15- 110
1718-51- Terpheny-d4 30- 130
118- 79- 6- Tribromophenol 15- 110
Semivolatile Organic Compounds by GC
Pol chlorinated Bi hen ls b EPA 608
Prepared by method SW846 3510C
12674- 11-2 Aroclor- 1016 BRL 1-91 0650 EPA 608 15- May- 16-May-08 8051106
11104-28-2 Aroclor-1221 BRL IJgl 0650
11141-16-5 Aroclor- 1232 BRL 1-91 0650
53469-21-9 Aroclor- 1242 BRL 1-91 0650
12672-29-6 Aroclor- 1248 BRL 1-91 0650
11097-69-1 Aroclor- 1254 BRL 1-91 0650
11096-82-5 Aroclor -1260 BRL 1-91 0650
37324-23-5 Aroclor-1262 BRL 1-91 0650
11100-14-4 Aroclor-1268 BRL IJgl 0650
Surrogate recoveries
2051-24- Decachlorobipheny (Sr) 105 30- 150
10386-84-2 4 DB-Octafluorobiphenyl (Sr) 30- 150
Extractable Petroleum Hydrocarbons
mgl EPA 1664 Rev A 15-May- 19-May-08 8051102Non-polar material (SGT- HEM)
Soluble Metals by EPA 2006000 Series Metbods
Field Filtered NA EPA 200 73005A 15- May- 15-May-08 8051192Filtration
Soluble Metals by EPA 200 Series Methods
7440-22-4 Silver BRL mgl 0002 EPA 200 21-May- 27- May-08 8051249
This laboratory report is IlOt mlid without (II authorized signature on the cover page
Reportble Detection Limit BRL = Below Reporting Limit Page 7 of 25
Sam le Identification MW-
Client Pro ect 2920-96shy
Matrix Ground Water
Collection DateTime 13-May-08 1030
Received 14-May-
SA 78602shy
CAS No A nalyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Soluble Metals by EPA 200 Series Methods
7440-38shy Arsenic 0468 mg1 0040 EPA 200 21-Mayshy 21-May-08 80511 50
7440-43shy Cadmium BRL mg1 0002 EPA 200 21-May-088051249
7440-47shy Chromium BRL mg1 0050 EPA 200 21-May-088051150
7440-50-8 Copper BRL mg1 0050
7439-89-6 Iron 184 mg1 0150
7439-97-6 Mercury BRL mg1 00020 EPA 245 17470A 21-May-088051152
7440-02-0 Nickel BRL mg1 0050 EPA 200 21-May-088051150
7439-92shy Lead 0011 mg1 0002 EPA 200 21-May-088051249
7440-36-0 Antimony 0003 mg1 0002
7782-49shy Selenium BRL mg1 0150 EPA 200 21-May-08 8051150
7440-66-6 Zinc 0186 mgl 0050
General Chemistry Parameters
Filtration Completed NA Varies 14-Mayshy 14-May-08 8051095
18540-29-9 Hexavalent Chromium (soluble) BRL HT2 mg1 125 SM3500CrDI796A 14-Mayshy 14-May-08 8051094 R01 2013 2016
57-12shy Cyanide (total) BRL mg1 0100 EPA 3354 19-Mayshy 19-May-088051374
7782-50shy Total Residual Chlorine BRL CIHT mg1 500 Hach 8167 14-Mayshy 14-May-08 8051049 R01 1900 2001
Total Suspended Solids 580 mg1 25 SM2540D 16-Mayshy 16-May-08 8051275
This lahomtOlY report is not valid without an authorized signature on the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page 8 of 25
Volatie Organic Compounds - Quality Control
Analyte( s)
Batch 8051244 - SW846 5030 Water MS
Blank 8051244-BLK1
Prepared 16-May-08 Analyzed 17-May-
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromochloromethane
1 Dichlorobenzene
1 Dichlorobenzene
1 Dichlorobenzene
1-Dichloroethane
1 Dichloroethane
1 1-Dichloroethene
cis- Dichloroethene
trans- 1 Dichloroethene
1 Dichloropropane
cis- 1 Dichloropropene
trans- 1 Dichloropropene
Ethylbenzene
Hexanone (MBK)
Methyl tert-butyl ether
Methyl- pentanone (MIBK)
Methylene chloride
Styrene
2- Tetrachloroethane
Tetrachloroethene
Toluene
1- Trichloroethane
2- Trichloroethane
Trichloroethene
Trichlorofluoromethane (Freon 11)
Vinyl chloride
p-Xylene
Xylene
Surrogate 4-Bromofluorobenzene Surrogate Toluene-
Surrogate 1 Dichloroethane-Surrogate Dibromofluoromethane
LCS B051244-BS1
Prepared 16-May-08 Analyzed 17 -May-
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Spike Source REC RPD
Result Flag Units RDL Level Result REC Limits RPD Limit
BRL gl 20
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl 10
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gll
BRL gi
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl 10
BRL gll
BRL gll 10
BRL gl 10
BRL gll
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
41 gl 50 70- 130 49 gl 50 70- 130 59 gl 50 119 70- 130 52 gl 50 105 70- 130
QC2 jgl 20 70- 130
18 jgl 20 70- 130
192 jgl 20 35- 155
18 jgl 20 45- 169
19 jgl 20 242
This laboratOlY repol1 is lot valid without 011 authorized sigllature 011 the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page 9 of 25
Volatie Organic Compounds - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051244 - SW846 5030 Water MS
LC5 8051244B51
Prepared 16-May-08 Analyzed 17-May-
Butanone (MEK) 10 QC2 gl 20 70- 130
Carbon tetrachloride 204 gl 20 102 70- 140
Chlorobenzene 18 gl 20 70- 130
Chloroethane 164 gl 20 14-230
Chloroform 18 gll 20 51- 138
Chloromethane 21 gl 20 106 273
Dibromochloromethane 18 gl 20 53- 149
1 Dichlorobenzene 20 gl 20 104 18- 190
1 Dichlorobenzene 19 gl 20 59- 156
1 A-Dichlorobenzene 18 gl 20 18- 190
1- Dichloroethane 19 gl 20 59- 155
1 Dichloroethane 19 gl 20 49- 155
1-Dichloroethene 16 gl 20 70- 130
cis- 1 Dichloroethene 17 gl 20 70- 130
trans- 1 Dichloroethene 16 gll 20 54- 156
1 Dichloropropane 18 gl 20 210
cis- Dichloropropene 17 gl 20 227
trans- 1 Dichloropropene 17 gl 20 17- 183
Ethylbenzene 19 gl 20 37- 162
Hexanone (MBK) 124 QC2 gl 20 70- 130
Methyl tert-butyl ether 19 gl 20 70- 130
Methylshy pentanone (MIBK) 17 gl 20 70- 130
Methylene chloride 16 gl 20 221
Styrene 17 gl 20 70- 130
1 Tetrachloroethane 194 gl 20 46- 157
Tetrachloroethene 15 gl 20 64- 148
Toluene 18 gl 20 70- 130
1- Trichloroethane 20 gl 20 100 52- 162
2- Trichloroethane 18 gl 20 52- 150
Trichloroethene 17 gl 20 71- 157
Trichlorofluoromethane (Freon 11) 19 gl 20 17- 181
Vinyl chloride 21 gl 20 106 251
p-Xylene 39 gl 40 70- 130
Xylene 20 gl 20 102 70- 130
Surrogate 4-Bromofluorobenzene Surrogate Toluene-
Surrogate 1 Dichloroethane-Surrogate Dibromofluoromethane
52 49 56
49
gl
gl
gl
gl
50 50 50
50
105
112 100
70- 130 70- 130 70- 130 70- 130
LC5 DUD (8051244-B5D1
Prepared 16-May-08 Analyzed 17-May-
Acetone QC2 gl 20 70- 130
Benzene 18 gl 20 70- 130
Bromodichloromethane 18 gl 200 35- 155
Bromoform 17 gl 20 45- 169
Bromomethane 18 gl 20 242
Butanone (MEK) 11 QC2 1-91 20 70- 130
Carbon tetrachloride 20 gl 20 100 70- 140
Chlorobenzene 17 gl 20 70- 130
Chloroethane 15 1-91 20 14-230
Chloroform 18 1-91 20 51- 138
This laboratory report is aot valid without a1 authorized sig1ature 01 the cover page
Reportble Detection Limit BRL = Below Reporting Limit Page 10 of25
Volatie Organic Compounds - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051244 - SW846 5030 Water MS
LCS Dup 18051244-BSD1
Prepared 16-May-08 Analyzed 17-May-
Chloromethane 18 1-91 20 273
Dibromochloromethane 174 1-91 20 53- 149
Dichlorobenzene 20 1-91 20 100 18- 190
Dichlorobenzene 18 1-91 20 59- 156
Dichlorobenzene 18 1-91 20 18- 190
Dichloroethane 18 1-91 20 59- 155
Dichloroethane 19 1-91 20 49- 155
Dichloroethene 16 1-91 20 70- 130
cis- Dichloroethene 16 1-91 20 70- 130
trans- Dichloroethene 15 1-91 20 54- 156
Dichloropropane 17 1-91 20 210
cis- Dichloropropene 164 IJgl 20 227
trans- 1 Dichloropropene 164 I-gl 20 17- 183
Etlwlbenzene 18 IJgl 20 37- 162
Hexanone (MBK) 124 QC2 IJgl 20 70- 130
Methyl tert-butyl ether 184 1J91 20 70- 130
Methyl- pentanone (MIBK) 17 IJgl 20 70- 130
Methylene chloride 16 IJgl 20 221
Styrene 16 IJgl 20 70- 130
2- Tetrachloroethane 19 IJgl 20 46- 157
Tetrachloroethene 15 IJgl 20 64- 148
Toluene 17 IJgl 20 70- 130
1- Trichloroethane 19 1-91 20 52- 162
2- Trichloroethane 16 IJgl 20 52- 150
Trichloroethene 15 IJgl 20 71- 157
Trichlorofluoromethane (Freon 11) 17 IJgl 20 17- 181
Vinyl chloride 19 IJglI 20 251
p-Xylene 37 1J91 40 70- 130
Xylene 20 IJgl 20 100 70- 130
Surrogate 4-Bromofluorobenzene 51 IJgl 50 104 70- 130
Surrogate Toluene- 4B gl 50 70- 130
Surrogate 1 0ichloroethane- 53 IJgl 50 106 70- 130 Surrogate Oibromofluoromethane 50 1J9i 50 102 70- 130
Matrix S ike B051244-MS1 Source SA7B629shy
Prepared 16-May-08 Analyzed 17-May-
Benzene 18 20 BRL 70- 130IJgl
Bromodichloromethane 19 IJgl 20 BRL 35- 155
Bromoform 18 IJgl 20 BRL 45- 169
Bromomethane 16 IJgl 20 BRL 242
Carbon tetrachloride 21 IJgl 20 BRL 106 70- 140
Chlorobenzene 18 IJgl 20 BRL 70- 130
Chloroethane 16 IJgl 20 BRL 14-230
Chloroform 18 IJgl 20 BRL 51- 138
Chloromethane 19 IJgl 20 BRL 273
Dibromochloromethane 17 IJgl 20 BRL 53- 149
1 Dichlorobenzene 22 IJgl 20 BRL 112 18- 190
1 Dichlorobenzene 22 IJgl 20 BRL 110 59-156
1 Dichlorobenzene 21 IJgl 20 BRL 109 18- 190
1- Dichloroethane 19 IJgl 20 BRL 59- 155
1 Dichloroethane 18 IJgl 20 BRL 49- 155
This laboratory report is 110t mUd without an authorized signature on the covel page
Reportble Detection Limit BRL = Below Reporting Limit Page It of25
Volatile Organic Compounds - Quality Control
p
Spike Source REC RPD
Result REC imits RPD LimitAnalyte(s) Result Flag Units RDL Level
Batch 8051244 - SW846 5030 Water MS
Matrix ike S051244-MS1 Source SA7B629shy
Prepared 16-May-08 Analyzed 17-Mayshy
17 20 BRL 70- 130 1- Dichloroethene IJgl
16 20 BRL 54- 156trans- 1 Dichloroethene IJgl
21020 BRL1 Dichloropropane 17 1J91
cis- 1 Dichloropropene 17 IJgl 20 BRL 227
17- 183trans- 1 Dichloropropene 184 1J91 20 BRL
20 20 BRL 103 37- 162Ethylbenzene IJgl
15 20 BRL 221Methylene chloride IJgl
20 BRL 46- 1572- Tetrachloroethane 19 1J91
20 BRL 64- 148Tetrachloroethene 18 1J91
BRL 70- 130Toluene 18 1J91 20
105 52-1621- Trichloroethane 211 IJgl 20 BRL
18 20 BRL 52- 1502- Trichloroethane IJgl
17 20 BRL 71- 157Trichloroethene 1J91
20 BRL 17- 181Trichloroluoromethane (Freon 11) 194 IJgl
20 BRL 103 251Vinyl chloride 20 IJgl
102 70- 130Surrogate 4-Bromofluorobenzene 50 IJgl 50 50 70- 130Surrogate Toluene- 49 1J91
56 50 112 70- 130Surrogate 1 Dichloroethane- IJgl
50 100 70- 130Surrogate Dibromofluoromethane 50 IJgl
Matrix S ike Du S051244-MSD1 Source SA7S629shy
Prepared 16-May-08 Analyzed 17-Mayshy
18 20 BRL 70- 130Benzene IJgl
18 20 BRL 35- 155Bromodichloromethane IJgl
17 20 BRL 45- 169Bromoform IJgl
20 BRL 242Bromomethane 17 IJgl
20 BRL 103 70- 140Carbon tetrachloride 20 IJgl
18 20 BRL 70- 130Chlorobenzene 1J91
14-230Chloroethane 16 IJgl 20 BRL
20 51- 138Chloroform 184 IJgl BRL
Chloromethane 19 1J91 20 BRL 273
18 20 BRL 53- 149Dibromochloromethane 1J91
20 BRL 117 18- 190Dichlorobenzene 234 IJgl
20 BRL 112 59- 156Dichlorobenzene 22 IJgl
BRL 108 18- 190Dichlorobenzene 21 1J91 20
20 59- 1551 Dichloroethane 19 IJgl BRL
18 20 BRL 49- 155Dichloroethane IJgl
16 20 BRL 70- 130Dichloroethene IJgl
20 BRL 54- 156trans- Dichloroethene 154 1J91
20 BRL 210Dichloropropane 17 IJgl
0420 BRL 227cis- Dichloropropene 17 IJgl
17- 183trans- Dichloropropene 17 1J91 20 BRL
BRL 37- 162Ethylbenzene 20 1J91 20 102
Methylene chloride 15 IJgl 20 BRL 221
20 BRL 46- 1572- Tetrachloroethane 192 IJgl
20 BRL 64- 148 04Tetrachloroethene 18 IJgl
BRL 70- 130Toluene 184 1J91 20
52- 1621- Trichloroethane 20 IJgl 20 BRL 104
17 20 BRL 52- 1502- Trichloroethane IJgl
17 20 BRL 71- 157Trichloroethene IJgl
20 BRL 17-181Trichlorofluoromethane (Freon 11) 19 IJgl
This laboratory report is IIOt valid without all authorized sigllllture 011 the cover page
Page 12 of25 Reportble Detection Limit BRL = Below Reporting Limit
Semivolatile Organic Compounds by GCMS - Quality Control
Analyte(s)
Batch 8051216 - SW846 3510C
Blank 8051216-BLK1
Prepared amp Analyzed 16-May-
Isophorone
Methylnaphthalene
Methylphenol
3 amp 4-Methylphenol
Naphthalene
Nitroaniline
Nitroaniline
Nitroaniline
Nitrobenzene
Nitrophenol
Nitrophenol
Nitrosodimethylamine
N- N itrosodi-n-pro pyla mine
N itrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Pyridine
1 24-Trichlorobenzene
24 5- Trichlorophenol
246- Trichlorophenol
Surrogate 2-Fuorobipheny Surrogate 2-Fuoropheno Surrogate Nitrobenzene-Surrogate PhenoshySurrogate Terpheny-d4 Surrogate 6- Tribromopheno
LCS B051216-BS1
Prepared amp Analyzed 16-May-
Acenaphthene
Acenaphthylene
Aniline
Anthracene
AzobenzenelDi phenyld lazine
Benzidine
Benzo (a) anthracene
Benzo (a) pyrene
Benzo (b) fluoranthene
Benzo (g i) perylene
Benzo (k) fluoranthene
Benzoic acid
Benzyl alcohol
B is(2-chloroethoxy)methane
B i s (2-ch loroethyl)eth e r
Bis(2-ch loroisopropyl) ether
B is(2-ethy Ih exyl) phtha late
Bromophenyl phenyl ether
Butyl benzyl phthalate
Carbazole
Spike Source REC RPD
Result Flag Units RDL Level Result REC Limits RPD Limit
BRL gl
BRL gl
BRL gl
BRL gl 10
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gll
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
370 gl 50 30- 130 40 gl 50 15- 110 39 gl 50 30- 130 43 gl 50 15- 110 36 gl 50 30- 130 40 gl 50 15- 110
41 gl 50 40- 140
43 gI 50 40- 140
41 gl 50 40- 140
38 gl 50 40- 140
45 gl 50 40- 140
49 gl 50 153
41 gl 50 40- 140
43 gl 50 40- 140
41 gl 50 40- 140
41 gll 50 40- 140
45 gl 50 40- 140
32 gl 50 12- 149
41 gl 50 40- 140
39 gl 50 40- 140
384 gl 50 40- 140
47 gl 50 40- 140
47 gl 50 40- 140
40 gl 50 40- 140
47 gI 50 40- 140
56 gI 50 112 200
This laboratory report is lIot valid witllOut a1l authorized sigllature 011 the coverpage
Reportble Detection Limit BRL = Below Reporting Limit Page 15 of25
Semivolatile Organic Compounds by GCMS - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051216 - SW846 3510C
LCS 8051216-BS1
Prepared amp Analyzed 16-Mayshy
50 30- 1304 -C hloro-3-methylphenol 42 IJgl
40- 140Chloroaniline 39 IJgl 50
Chloronaphthalene 37 IJgl 50 40- 140
Chlorophenol 37 IJgl 50 30- 130
50 40- 140
40- 140
Chlorophenyl phenyl ether 45 IJgl
Chrysene 43 IJgl 50
Dibenzo (a h) anthracene 43 IJgl 50 40- 140
Dibenzofuran IJgl38 50 40- 140
50 40- 1401 Dichlorobenzene 35 IJgl
40- 1401 Dichlorobenzene 264 IJgl 50
40- 1401 Dichlorobenzene 434 IJgl 50
58 50 116 40- 1403 - Dichlorobenzidine IJgl
50 30- 130
40- 140 24-Dichlorophenol 38 IJgl
Diethyl phthalate 484 IJgl 50
50 40- 140Dimethyl phthalate 464 IJgl
Dlmethylphenol 39 IJgl 50 30- 130
DI-n-butyl phthalate 44 IJgll 50 40- 140
30- 130 6-Di nitro- 2-methylphenol 38 1J91 50
30- 130Dinltrophenol 36 1J91 50
42 50 40- 14024-Dlnitrotoluene 1J91
Dlnitrotoluene 1J9141 50 40- 140
Di-n-octyl phthalate 52 IJgl 50 104 40- 140
40- 140Fluoranthene 40 IJgl 50
Fluorene 41 IJgl 50 40- 140
39 50 40- 140Hexachlorobenzene IJgl
50 40- 140Hexachlorobutadiene 40 IJgl
40- 140Hexach lorocyclopentad iene 294 IJgl 50
40 50 40- 140Hexachloroethane IJgl
42 50 40-140Indeno (1 3-cd) pyrene IJgl
50 40- 140Isophorone 40 IJgl
40- 140Methylnaphthalene 394 IJgl 50
40- 140Methylphenol 39 IJgl 50
40 10 50 40- 1403 amp 4-Methylphenol IJgl
37 50 40-140Naphthalene IJgl
50 40-140Nitroaniline 39 IJgl
Nitroaniline 51 IJgl 50 102 40- 140
48 50 40- 140Nltroaniline 1J91
50 40- 140Nitrobenzene 40 IJgl
30- 130Nitrophenol 36 IJgl 50
40 IJgl 50 30- 130Nitrophenol 40- 140Nitrosodimethylamine 32 1J91 50
50 40-140N- N itrosodi-n-propyla mine 46 IJgl
40- 140N itrosodi phenyla ml ne 44 IJgl 50
41 IJgl 50 30- 130Pentachlorophenol 40- 140Phenanthrene 38 IJgl 50
50 30- 130Phenol 38 IJgl
40- 140Pyrene 424 1J91 50
40- 140Pyridine 294 1J91 50
40- 14024- Trichlorobenzene 364 IJgl 50
This laboratory report is not mlid without an authorized signature 011 the cover page
Page 16 of25 Reportble Detection Limit BRL = Below Reporting Limit
Semivolatie Organic Compounds by GCMS - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
BMch 8051216 - SW846 3510C
LC5 8051216-851
Prepared amp Analyzed 16-Mayshy
24 5- Trichlorophenol 404 gl 50 30- 130
246- Trichlorophenol 42 gl 50 30- 130
Surrogate 2-Fluorobiphenyl 29 gl 50 30- 130
Surrogate 2-Fluorophenot 27 gl 50 15- 110
Surrogate Nitrobenzene- 30 gl 50 30- 130
Surrogate Phenol- 29 gl 50 15- 110
Surrogate Terpheny-d4 30 gl 50 30- 130
Surrogate 6- Tribromopheno 324 gl 50 15- 110
This laboratory report is lIot valid without all authorized sigllature 011 tlle cover page
Reportble Detection Limit BRL = Below Reporting Limit Page 17 of25
Semivolatie Organic Compounds by GC - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051106 - SW846 3510C
Blank S051106-BLK1
Prepared amp Analyzed 15-Mayshy
Aroclor- 1016 BRL gI 0200
Aroclor- 1016 (2C) BRL gI 0200
Aroclor- 1221 BRL gI 0200
Aroclor- 1221 (2C) BRL gI 0200
Aroclor- 1232 BRL gI 0200
Aroclor- 1232 (2Cj BRL gI 0200
Aroclor- 1242 BRL gI 0200
Aroclor-1242 (2C) BRL gI 0200
Aroclor- 1248 BRL gI 0200
Aroclor- 1248 (2C) BRL gI 0200
Aroclor- 1254 BRL gI 0200
Aroclor- 1254(2Cj BRL gI 0200
Aroclor- 1260 BRL gI 0200
Aroclor- 1260 (2C) BRL gI 0200
Aroclor- 1262 BRL gI 0200
Aroclor- 1262 (2C) BRL gI 0200
Aroclor-1268 BRL gI 0200
Aroclor- 1268 (2C) BRL gI 0200
Surrogate Decachlorobiphenyl (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0231 0224 0194 0191
gI
gI
gI
gI
0200 0200 0200 0200
116 112
30- 150 30- 150 30- 150 30- 150
LC5 8051106-B51
Prepared 15-May-08 Analyzed 16-May-08
Aroclor- 1016 265 gI 0200 250 106 50- 114
Aroclor- 1 016 (2C) 240 gI 0200 250 50- 114
Aroclor- 1260 0269 gI 0200 250 107 40- 127
Aroclor-1260 (2Cj 270 gI 0200 250 108 40- 127
Surrogate Decachlorobiphenyl (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0225 0224 0188 0183
gI
gI
gI
gI
0200 0200 0200 0200
113 112
30- 150 30- 150 30- 150 30- 150
LC5 DUD rS051106-B5D1
Prepared 15-May-08 Analyzed 16-Mayshy
Aroclor- 1016 262 gl 0200 250 105 50- 114
Aroclor-1 016 (2Cj 241 gI 0200 250 50- 114
Aroclor- 1260 277 gI 0200 250 111 40- 127
Aroclor- 1260(2Cj 0260 gI 0200 250 104 40- 127
Surrogate Decachlorobipheny (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0238 0218 0189 0181
gI
gI
gI
gI
0200 0200 0200 0200
119 109
30- 150 30- 150 30- 150 30- 150
This laboratory report is lot valid without (II authorized sigllature 01 the cover page
Page 18 of25 Reportable Detection Limit BRL = Below Reporting Limit
Extractable Petroleum Hydrocarbons - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051102 - SW846 3510C
Blank 8051102-BLK1
Prepared 15-May-08 Analyzed 19-Mayshy
Non-polar material (SGT- HEM) BRL m91
LC8 8051102-B81
Prepared 15-May-08 Analyzed 19-Mayshy
Non-polar material (SGT- HEM) 184 m91 21 81 904
This laboratory report is not valid without an authorized signature 011 the cover page
Page 19 of25 Reportable Detection Limit BRL = Below Reporting Limit
Soluble Metals by EPA 200 Series Methods - Quality Control
Analyte(s) Result Flag Units RDL
Spike
Level
Source
Result REC
REC
Limits RPD
RPD
Limit
Batch 8051150 - EPA 200 Series
Blank 8051150-BLK1
Prepared amp Analyzed 21-May-
Iron
Zinc
Selenium
Nickel
Chromium
Copper
Arsenic
BRL
BRL
BRL
BRL
BRL
BRL
BRL
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0150
0050
0150
0050
0050
0050
0040
LCS 8051150-BS1
Prepared amp Analyzed 21-May-
Selenium
Zinc
Iron
Nickel
Chromium
Arsenic
Copper
123
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0150
0050
0150
0050
0050
0040
0050
103
105
101
100
85- 115
85- 115
85- 115
85- 115
85- 115
85-115
85- 115
licate B051150-DUP1 Source SA7B602shy
Prepared amp Analyzed 21-May-
Iron
Zinc
Selenium
Nickel
Copper
Chromium
Arsenic
17
0162
BRL
0015
0017
BRL
0450
QR8
mgl
mgl
mgl
mgl
mgl
mgl
mgi
0150
0050
0150
0050
0050
0050
0040
184
0186
BRL
0014
0023
BRL
0468
Matrix S ike 8051150-MS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Iron
Selenium
Nickel
Zinc
Copper
Chromium
Arsenic
19 QM2 mgl
mgll
mgl
mgl
mgl
mgl
mgl
0150
0150
0050
0050
0050
0050
0040
125
184
BRL
0014
0186
0023
BRL
0468
104
105
102
70- 130
70- 130
70-130
70- 130
70- 130
70-130
70- 130
Post S ike 8051150-PS1 Source SA78602shy
Prepared amp Analyzed 21-May-
Zinc
Iron
Selenium
Nickel
Copper
Arsenic
Chromium
18 QM2
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0050
0150
0150
0050
0050
0040
0050
0186
184
BRL
0014
0023
0468
BRL
104
104
101
85- 115
85- 115
85- 115
85-115
85-115
85- 115
85-115
Batch 8051152 - EPA200SW7000 Series
Blank B051152-BLK1
Prepared amp Analyzed 21-May-
Mercury BRL mgl 00020
This laboratory report is IIOt valid witllOut all authorized sigllature 011 the coverpage
Page 20 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Soluble Metals by EPA 200 Series Methods - Quality Control
Analyte(s) Result Flag Units RDL
Spike
Level
Source
Result REC
REC
Limits RPD
RPD
Limit
Batch 8051152 - EPA200SW7000 Series
LCS B051152-BS1
Prepared amp Analyzed 21-May-
Mercury 00576 m91 00020 00500 115 85- 115
licate B051152-DUP1 Source SA78602-01
Prepared amp Analyzed 21-May-
Mercury BRL m91 00020 BRL
Matrix S ike 8051152-MS1 Source SA78602shy
Prepared amp Analyzed 21-May-
Mercury 00632 OM m91 00020 00500 BRL 126 75- 125
Post S ike 8051152-PS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Mercury 00624 OC1 m91 00020 00500 BRL 125 85- 115
Batch 8051249 - 2008No digestion
Blank 8051249-BLK1
Prepared amp Analyzed 21-May-
Lead
Antimony
Cadmium
Silver
BRL
BRL
BRL
BRL
m91
m91
m91
m91
0002
0002
0002
0002
LCS B051249-BS1
Prepared amp Analyzed 21-May-
Antimony
Lead
Silver
Cadmium
143
145 OC2
m91
m91
m91
m91
0050
0050
0050
0040
103
115
107
116
85- 115
85- 115
85- 115
85- 115
licate 8051249-DUP1 Source SA7B602shy
Prepared amp Analyzed 21- May-
Lead
Antimony
Cadmium
Silver
0009
0002
00005
00002
ORB
m91
m91
m91
m91
0002
0002
0002
0002
0011
0003
00005
00003
Matrix S ike 8051249-MS1 Source SA78602shy
Prepared amp Analyzed 21- May-
Lead
Antimony
Cadmium
Silver
142
m91
m91
m91
m91
0050
0050
0040
0050
0011
0003
00005
00003
111
101
114
102
70- 130
70-130
70c130
70- 130
Post S ike 8051249-PS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Antimony
Cadmium
Silver
38
OC2
m91
m91
m91
0050
0040
0050
125
0003
00005
00003
110
121
109
85- 115
85- 115
85- 115
This laboratory report is flOt valid IVithout all authorized signature 011 the cOIer page
Reportable Detection Limit BRL Below Reporting Limit Page 21 of 25
General Chemistry Parameters - Quality Control
Spike Source REC RPD
Analyte( s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051049 - General Preparation
Blank S051 049-BLK1
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
Blank S051049-BLK2
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
Blank S051 049-BLK3
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
LCS S051049-BS1
Prepared amp Analyzed 14-May-
Total Residual Chlorine 046 mgl 020 0500 90- 110
LCS S051049-BS2
Prepared amp Analyzed 14-May-
Total Residual Chlorine 047 mgl 020 0500 90- 110
LCS S051049-BS3
Prepared amp Analyzed 14-May-
Total Residual Chlorine 054 mgl 020 0500 108 90-110
licate B051049-DUP1 Source SA7S544shy
Prepared amp Analyzed 14-May-
Total Residual Chlorine 012 mgl 020 010
licate S051049-DUP2 Source SA7S602-01
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020 BRL
Matrix S ike 8051049-MS1 Source SA78544-01
Prepared amp Analyzed 14-May-
Total Residual Chlorine 065 mgl 020 0500 010 110 80- 120
Matrix S ike 8051049-MS2 Source SA7B602shy
Prepared amp Analyzed 14-May-
Total Residual Chlorine mgl 500 125 BRL 108 80- 120
Reference 8051 049-SRM1
Prepared amp Analyzed 14-May-
Total Residual Chlorine 100 mgl 020 0967 103 85-115
Batch 8051094 - General Preparation
Blank 8051094-BLK1
Prepared amp Analyzed 14 May-
Hexavalent Chromium (soluble) BRL mgl 005
Blank 8051 094-BLK2
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) BRL mgl 005
LCS 8051094-BS1
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) 054 mgl 005 90- 110
licate 8051094-DUP1 Source SA78602-01
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) BRL mgl 125 BRL
Thi laboratory report is not valid without all authorized sigllature 011 the cover page
Page 22 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Page 22
Sam le Identification MW-
Client Pro ect 2920-96shy
Matrix Ground Water
Collection DateTime 13-May-08 1030
Received 14-May-
SA 78602shy
CAS No A nalyte(s) Result Flag Units RDL Dilution Method Ref Prepared Analyzed Batch Cert
Soluble Metals by EPA 200 Series Methods
7440-38shy Arsenic 0468 mg1 0040 EPA 200 21-Mayshy 21-May-08 80511 50
7440-43shy Cadmium BRL mg1 0002 EPA 200 21-May-088051249
7440-47shy Chromium BRL mg1 0050 EPA 200 21-May-088051150
7440-50-8 Copper BRL mg1 0050
7439-89-6 Iron 184 mg1 0150
7439-97-6 Mercury BRL mg1 00020 EPA 245 17470A 21-May-088051152
7440-02-0 Nickel BRL mg1 0050 EPA 200 21-May-088051150
7439-92shy Lead 0011 mg1 0002 EPA 200 21-May-088051249
7440-36-0 Antimony 0003 mg1 0002
7782-49shy Selenium BRL mg1 0150 EPA 200 21-May-08 8051150
7440-66-6 Zinc 0186 mgl 0050
General Chemistry Parameters
Filtration Completed NA Varies 14-Mayshy 14-May-08 8051095
18540-29-9 Hexavalent Chromium (soluble) BRL HT2 mg1 125 SM3500CrDI796A 14-Mayshy 14-May-08 8051094 R01 2013 2016
57-12shy Cyanide (total) BRL mg1 0100 EPA 3354 19-Mayshy 19-May-088051374
7782-50shy Total Residual Chlorine BRL CIHT mg1 500 Hach 8167 14-Mayshy 14-May-08 8051049 R01 1900 2001
Total Suspended Solids 580 mg1 25 SM2540D 16-Mayshy 16-May-08 8051275
This lahomtOlY report is not valid without an authorized signature on the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page 8 of 25
Volatie Organic Compounds - Quality Control
Analyte( s)
Batch 8051244 - SW846 5030 Water MS
Blank 8051244-BLK1
Prepared 16-May-08 Analyzed 17-May-
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromochloromethane
1 Dichlorobenzene
1 Dichlorobenzene
1 Dichlorobenzene
1-Dichloroethane
1 Dichloroethane
1 1-Dichloroethene
cis- Dichloroethene
trans- 1 Dichloroethene
1 Dichloropropane
cis- 1 Dichloropropene
trans- 1 Dichloropropene
Ethylbenzene
Hexanone (MBK)
Methyl tert-butyl ether
Methyl- pentanone (MIBK)
Methylene chloride
Styrene
2- Tetrachloroethane
Tetrachloroethene
Toluene
1- Trichloroethane
2- Trichloroethane
Trichloroethene
Trichlorofluoromethane (Freon 11)
Vinyl chloride
p-Xylene
Xylene
Surrogate 4-Bromofluorobenzene Surrogate Toluene-
Surrogate 1 Dichloroethane-Surrogate Dibromofluoromethane
LCS B051244-BS1
Prepared 16-May-08 Analyzed 17 -May-
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Spike Source REC RPD
Result Flag Units RDL Level Result REC Limits RPD Limit
BRL gl 20
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl 10
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gll
BRL gi
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl 10
BRL gll
BRL gll 10
BRL gl 10
BRL gll
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
41 gl 50 70- 130 49 gl 50 70- 130 59 gl 50 119 70- 130 52 gl 50 105 70- 130
QC2 jgl 20 70- 130
18 jgl 20 70- 130
192 jgl 20 35- 155
18 jgl 20 45- 169
19 jgl 20 242
This laboratOlY repol1 is lot valid without 011 authorized sigllature 011 the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page 9 of 25
Volatie Organic Compounds - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051244 - SW846 5030 Water MS
LC5 8051244B51
Prepared 16-May-08 Analyzed 17-May-
Butanone (MEK) 10 QC2 gl 20 70- 130
Carbon tetrachloride 204 gl 20 102 70- 140
Chlorobenzene 18 gl 20 70- 130
Chloroethane 164 gl 20 14-230
Chloroform 18 gll 20 51- 138
Chloromethane 21 gl 20 106 273
Dibromochloromethane 18 gl 20 53- 149
1 Dichlorobenzene 20 gl 20 104 18- 190
1 Dichlorobenzene 19 gl 20 59- 156
1 A-Dichlorobenzene 18 gl 20 18- 190
1- Dichloroethane 19 gl 20 59- 155
1 Dichloroethane 19 gl 20 49- 155
1-Dichloroethene 16 gl 20 70- 130
cis- 1 Dichloroethene 17 gl 20 70- 130
trans- 1 Dichloroethene 16 gll 20 54- 156
1 Dichloropropane 18 gl 20 210
cis- Dichloropropene 17 gl 20 227
trans- 1 Dichloropropene 17 gl 20 17- 183
Ethylbenzene 19 gl 20 37- 162
Hexanone (MBK) 124 QC2 gl 20 70- 130
Methyl tert-butyl ether 19 gl 20 70- 130
Methylshy pentanone (MIBK) 17 gl 20 70- 130
Methylene chloride 16 gl 20 221
Styrene 17 gl 20 70- 130
1 Tetrachloroethane 194 gl 20 46- 157
Tetrachloroethene 15 gl 20 64- 148
Toluene 18 gl 20 70- 130
1- Trichloroethane 20 gl 20 100 52- 162
2- Trichloroethane 18 gl 20 52- 150
Trichloroethene 17 gl 20 71- 157
Trichlorofluoromethane (Freon 11) 19 gl 20 17- 181
Vinyl chloride 21 gl 20 106 251
p-Xylene 39 gl 40 70- 130
Xylene 20 gl 20 102 70- 130
Surrogate 4-Bromofluorobenzene Surrogate Toluene-
Surrogate 1 Dichloroethane-Surrogate Dibromofluoromethane
52 49 56
49
gl
gl
gl
gl
50 50 50
50
105
112 100
70- 130 70- 130 70- 130 70- 130
LC5 DUD (8051244-B5D1
Prepared 16-May-08 Analyzed 17-May-
Acetone QC2 gl 20 70- 130
Benzene 18 gl 20 70- 130
Bromodichloromethane 18 gl 200 35- 155
Bromoform 17 gl 20 45- 169
Bromomethane 18 gl 20 242
Butanone (MEK) 11 QC2 1-91 20 70- 130
Carbon tetrachloride 20 gl 20 100 70- 140
Chlorobenzene 17 gl 20 70- 130
Chloroethane 15 1-91 20 14-230
Chloroform 18 1-91 20 51- 138
This laboratory report is aot valid without a1 authorized sig1ature 01 the cover page
Reportble Detection Limit BRL = Below Reporting Limit Page 10 of25
Volatie Organic Compounds - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051244 - SW846 5030 Water MS
LCS Dup 18051244-BSD1
Prepared 16-May-08 Analyzed 17-May-
Chloromethane 18 1-91 20 273
Dibromochloromethane 174 1-91 20 53- 149
Dichlorobenzene 20 1-91 20 100 18- 190
Dichlorobenzene 18 1-91 20 59- 156
Dichlorobenzene 18 1-91 20 18- 190
Dichloroethane 18 1-91 20 59- 155
Dichloroethane 19 1-91 20 49- 155
Dichloroethene 16 1-91 20 70- 130
cis- Dichloroethene 16 1-91 20 70- 130
trans- Dichloroethene 15 1-91 20 54- 156
Dichloropropane 17 1-91 20 210
cis- Dichloropropene 164 IJgl 20 227
trans- 1 Dichloropropene 164 I-gl 20 17- 183
Etlwlbenzene 18 IJgl 20 37- 162
Hexanone (MBK) 124 QC2 IJgl 20 70- 130
Methyl tert-butyl ether 184 1J91 20 70- 130
Methyl- pentanone (MIBK) 17 IJgl 20 70- 130
Methylene chloride 16 IJgl 20 221
Styrene 16 IJgl 20 70- 130
2- Tetrachloroethane 19 IJgl 20 46- 157
Tetrachloroethene 15 IJgl 20 64- 148
Toluene 17 IJgl 20 70- 130
1- Trichloroethane 19 1-91 20 52- 162
2- Trichloroethane 16 IJgl 20 52- 150
Trichloroethene 15 IJgl 20 71- 157
Trichlorofluoromethane (Freon 11) 17 IJgl 20 17- 181
Vinyl chloride 19 IJglI 20 251
p-Xylene 37 1J91 40 70- 130
Xylene 20 IJgl 20 100 70- 130
Surrogate 4-Bromofluorobenzene 51 IJgl 50 104 70- 130
Surrogate Toluene- 4B gl 50 70- 130
Surrogate 1 0ichloroethane- 53 IJgl 50 106 70- 130 Surrogate Oibromofluoromethane 50 1J9i 50 102 70- 130
Matrix S ike B051244-MS1 Source SA7B629shy
Prepared 16-May-08 Analyzed 17-May-
Benzene 18 20 BRL 70- 130IJgl
Bromodichloromethane 19 IJgl 20 BRL 35- 155
Bromoform 18 IJgl 20 BRL 45- 169
Bromomethane 16 IJgl 20 BRL 242
Carbon tetrachloride 21 IJgl 20 BRL 106 70- 140
Chlorobenzene 18 IJgl 20 BRL 70- 130
Chloroethane 16 IJgl 20 BRL 14-230
Chloroform 18 IJgl 20 BRL 51- 138
Chloromethane 19 IJgl 20 BRL 273
Dibromochloromethane 17 IJgl 20 BRL 53- 149
1 Dichlorobenzene 22 IJgl 20 BRL 112 18- 190
1 Dichlorobenzene 22 IJgl 20 BRL 110 59-156
1 Dichlorobenzene 21 IJgl 20 BRL 109 18- 190
1- Dichloroethane 19 IJgl 20 BRL 59- 155
1 Dichloroethane 18 IJgl 20 BRL 49- 155
This laboratory report is 110t mUd without an authorized signature on the covel page
Reportble Detection Limit BRL = Below Reporting Limit Page It of25
Volatile Organic Compounds - Quality Control
p
Spike Source REC RPD
Result REC imits RPD LimitAnalyte(s) Result Flag Units RDL Level
Batch 8051244 - SW846 5030 Water MS
Matrix ike S051244-MS1 Source SA7B629shy
Prepared 16-May-08 Analyzed 17-Mayshy
17 20 BRL 70- 130 1- Dichloroethene IJgl
16 20 BRL 54- 156trans- 1 Dichloroethene IJgl
21020 BRL1 Dichloropropane 17 1J91
cis- 1 Dichloropropene 17 IJgl 20 BRL 227
17- 183trans- 1 Dichloropropene 184 1J91 20 BRL
20 20 BRL 103 37- 162Ethylbenzene IJgl
15 20 BRL 221Methylene chloride IJgl
20 BRL 46- 1572- Tetrachloroethane 19 1J91
20 BRL 64- 148Tetrachloroethene 18 1J91
BRL 70- 130Toluene 18 1J91 20
105 52-1621- Trichloroethane 211 IJgl 20 BRL
18 20 BRL 52- 1502- Trichloroethane IJgl
17 20 BRL 71- 157Trichloroethene 1J91
20 BRL 17- 181Trichloroluoromethane (Freon 11) 194 IJgl
20 BRL 103 251Vinyl chloride 20 IJgl
102 70- 130Surrogate 4-Bromofluorobenzene 50 IJgl 50 50 70- 130Surrogate Toluene- 49 1J91
56 50 112 70- 130Surrogate 1 Dichloroethane- IJgl
50 100 70- 130Surrogate Dibromofluoromethane 50 IJgl
Matrix S ike Du S051244-MSD1 Source SA7S629shy
Prepared 16-May-08 Analyzed 17-Mayshy
18 20 BRL 70- 130Benzene IJgl
18 20 BRL 35- 155Bromodichloromethane IJgl
17 20 BRL 45- 169Bromoform IJgl
20 BRL 242Bromomethane 17 IJgl
20 BRL 103 70- 140Carbon tetrachloride 20 IJgl
18 20 BRL 70- 130Chlorobenzene 1J91
14-230Chloroethane 16 IJgl 20 BRL
20 51- 138Chloroform 184 IJgl BRL
Chloromethane 19 1J91 20 BRL 273
18 20 BRL 53- 149Dibromochloromethane 1J91
20 BRL 117 18- 190Dichlorobenzene 234 IJgl
20 BRL 112 59- 156Dichlorobenzene 22 IJgl
BRL 108 18- 190Dichlorobenzene 21 1J91 20
20 59- 1551 Dichloroethane 19 IJgl BRL
18 20 BRL 49- 155Dichloroethane IJgl
16 20 BRL 70- 130Dichloroethene IJgl
20 BRL 54- 156trans- Dichloroethene 154 1J91
20 BRL 210Dichloropropane 17 IJgl
0420 BRL 227cis- Dichloropropene 17 IJgl
17- 183trans- Dichloropropene 17 1J91 20 BRL
BRL 37- 162Ethylbenzene 20 1J91 20 102
Methylene chloride 15 IJgl 20 BRL 221
20 BRL 46- 1572- Tetrachloroethane 192 IJgl
20 BRL 64- 148 04Tetrachloroethene 18 IJgl
BRL 70- 130Toluene 184 1J91 20
52- 1621- Trichloroethane 20 IJgl 20 BRL 104
17 20 BRL 52- 1502- Trichloroethane IJgl
17 20 BRL 71- 157Trichloroethene IJgl
20 BRL 17-181Trichlorofluoromethane (Freon 11) 19 IJgl
This laboratory report is IIOt valid without all authorized sigllllture 011 the cover page
Page 12 of25 Reportble Detection Limit BRL = Below Reporting Limit
Semivolatile Organic Compounds by GCMS - Quality Control
Analyte(s)
Batch 8051216 - SW846 3510C
Blank 8051216-BLK1
Prepared amp Analyzed 16-May-
Isophorone
Methylnaphthalene
Methylphenol
3 amp 4-Methylphenol
Naphthalene
Nitroaniline
Nitroaniline
Nitroaniline
Nitrobenzene
Nitrophenol
Nitrophenol
Nitrosodimethylamine
N- N itrosodi-n-pro pyla mine
N itrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Pyridine
1 24-Trichlorobenzene
24 5- Trichlorophenol
246- Trichlorophenol
Surrogate 2-Fuorobipheny Surrogate 2-Fuoropheno Surrogate Nitrobenzene-Surrogate PhenoshySurrogate Terpheny-d4 Surrogate 6- Tribromopheno
LCS B051216-BS1
Prepared amp Analyzed 16-May-
Acenaphthene
Acenaphthylene
Aniline
Anthracene
AzobenzenelDi phenyld lazine
Benzidine
Benzo (a) anthracene
Benzo (a) pyrene
Benzo (b) fluoranthene
Benzo (g i) perylene
Benzo (k) fluoranthene
Benzoic acid
Benzyl alcohol
B is(2-chloroethoxy)methane
B i s (2-ch loroethyl)eth e r
Bis(2-ch loroisopropyl) ether
B is(2-ethy Ih exyl) phtha late
Bromophenyl phenyl ether
Butyl benzyl phthalate
Carbazole
Spike Source REC RPD
Result Flag Units RDL Level Result REC Limits RPD Limit
BRL gl
BRL gl
BRL gl
BRL gl 10
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gll
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
370 gl 50 30- 130 40 gl 50 15- 110 39 gl 50 30- 130 43 gl 50 15- 110 36 gl 50 30- 130 40 gl 50 15- 110
41 gl 50 40- 140
43 gI 50 40- 140
41 gl 50 40- 140
38 gl 50 40- 140
45 gl 50 40- 140
49 gl 50 153
41 gl 50 40- 140
43 gl 50 40- 140
41 gl 50 40- 140
41 gll 50 40- 140
45 gl 50 40- 140
32 gl 50 12- 149
41 gl 50 40- 140
39 gl 50 40- 140
384 gl 50 40- 140
47 gl 50 40- 140
47 gl 50 40- 140
40 gl 50 40- 140
47 gI 50 40- 140
56 gI 50 112 200
This laboratory report is lIot valid witllOut a1l authorized sigllature 011 the coverpage
Reportble Detection Limit BRL = Below Reporting Limit Page 15 of25
Semivolatile Organic Compounds by GCMS - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051216 - SW846 3510C
LCS 8051216-BS1
Prepared amp Analyzed 16-Mayshy
50 30- 1304 -C hloro-3-methylphenol 42 IJgl
40- 140Chloroaniline 39 IJgl 50
Chloronaphthalene 37 IJgl 50 40- 140
Chlorophenol 37 IJgl 50 30- 130
50 40- 140
40- 140
Chlorophenyl phenyl ether 45 IJgl
Chrysene 43 IJgl 50
Dibenzo (a h) anthracene 43 IJgl 50 40- 140
Dibenzofuran IJgl38 50 40- 140
50 40- 1401 Dichlorobenzene 35 IJgl
40- 1401 Dichlorobenzene 264 IJgl 50
40- 1401 Dichlorobenzene 434 IJgl 50
58 50 116 40- 1403 - Dichlorobenzidine IJgl
50 30- 130
40- 140 24-Dichlorophenol 38 IJgl
Diethyl phthalate 484 IJgl 50
50 40- 140Dimethyl phthalate 464 IJgl
Dlmethylphenol 39 IJgl 50 30- 130
DI-n-butyl phthalate 44 IJgll 50 40- 140
30- 130 6-Di nitro- 2-methylphenol 38 1J91 50
30- 130Dinltrophenol 36 1J91 50
42 50 40- 14024-Dlnitrotoluene 1J91
Dlnitrotoluene 1J9141 50 40- 140
Di-n-octyl phthalate 52 IJgl 50 104 40- 140
40- 140Fluoranthene 40 IJgl 50
Fluorene 41 IJgl 50 40- 140
39 50 40- 140Hexachlorobenzene IJgl
50 40- 140Hexachlorobutadiene 40 IJgl
40- 140Hexach lorocyclopentad iene 294 IJgl 50
40 50 40- 140Hexachloroethane IJgl
42 50 40-140Indeno (1 3-cd) pyrene IJgl
50 40- 140Isophorone 40 IJgl
40- 140Methylnaphthalene 394 IJgl 50
40- 140Methylphenol 39 IJgl 50
40 10 50 40- 1403 amp 4-Methylphenol IJgl
37 50 40-140Naphthalene IJgl
50 40-140Nitroaniline 39 IJgl
Nitroaniline 51 IJgl 50 102 40- 140
48 50 40- 140Nltroaniline 1J91
50 40- 140Nitrobenzene 40 IJgl
30- 130Nitrophenol 36 IJgl 50
40 IJgl 50 30- 130Nitrophenol 40- 140Nitrosodimethylamine 32 1J91 50
50 40-140N- N itrosodi-n-propyla mine 46 IJgl
40- 140N itrosodi phenyla ml ne 44 IJgl 50
41 IJgl 50 30- 130Pentachlorophenol 40- 140Phenanthrene 38 IJgl 50
50 30- 130Phenol 38 IJgl
40- 140Pyrene 424 1J91 50
40- 140Pyridine 294 1J91 50
40- 14024- Trichlorobenzene 364 IJgl 50
This laboratory report is not mlid without an authorized signature 011 the cover page
Page 16 of25 Reportble Detection Limit BRL = Below Reporting Limit
Semivolatie Organic Compounds by GCMS - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
BMch 8051216 - SW846 3510C
LC5 8051216-851
Prepared amp Analyzed 16-Mayshy
24 5- Trichlorophenol 404 gl 50 30- 130
246- Trichlorophenol 42 gl 50 30- 130
Surrogate 2-Fluorobiphenyl 29 gl 50 30- 130
Surrogate 2-Fluorophenot 27 gl 50 15- 110
Surrogate Nitrobenzene- 30 gl 50 30- 130
Surrogate Phenol- 29 gl 50 15- 110
Surrogate Terpheny-d4 30 gl 50 30- 130
Surrogate 6- Tribromopheno 324 gl 50 15- 110
This laboratory report is lIot valid without all authorized sigllature 011 tlle cover page
Reportble Detection Limit BRL = Below Reporting Limit Page 17 of25
Semivolatie Organic Compounds by GC - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051106 - SW846 3510C
Blank S051106-BLK1
Prepared amp Analyzed 15-Mayshy
Aroclor- 1016 BRL gI 0200
Aroclor- 1016 (2C) BRL gI 0200
Aroclor- 1221 BRL gI 0200
Aroclor- 1221 (2C) BRL gI 0200
Aroclor- 1232 BRL gI 0200
Aroclor- 1232 (2Cj BRL gI 0200
Aroclor- 1242 BRL gI 0200
Aroclor-1242 (2C) BRL gI 0200
Aroclor- 1248 BRL gI 0200
Aroclor- 1248 (2C) BRL gI 0200
Aroclor- 1254 BRL gI 0200
Aroclor- 1254(2Cj BRL gI 0200
Aroclor- 1260 BRL gI 0200
Aroclor- 1260 (2C) BRL gI 0200
Aroclor- 1262 BRL gI 0200
Aroclor- 1262 (2C) BRL gI 0200
Aroclor-1268 BRL gI 0200
Aroclor- 1268 (2C) BRL gI 0200
Surrogate Decachlorobiphenyl (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0231 0224 0194 0191
gI
gI
gI
gI
0200 0200 0200 0200
116 112
30- 150 30- 150 30- 150 30- 150
LC5 8051106-B51
Prepared 15-May-08 Analyzed 16-May-08
Aroclor- 1016 265 gI 0200 250 106 50- 114
Aroclor- 1 016 (2C) 240 gI 0200 250 50- 114
Aroclor- 1260 0269 gI 0200 250 107 40- 127
Aroclor-1260 (2Cj 270 gI 0200 250 108 40- 127
Surrogate Decachlorobiphenyl (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0225 0224 0188 0183
gI
gI
gI
gI
0200 0200 0200 0200
113 112
30- 150 30- 150 30- 150 30- 150
LC5 DUD rS051106-B5D1
Prepared 15-May-08 Analyzed 16-Mayshy
Aroclor- 1016 262 gl 0200 250 105 50- 114
Aroclor-1 016 (2Cj 241 gI 0200 250 50- 114
Aroclor- 1260 277 gI 0200 250 111 40- 127
Aroclor- 1260(2Cj 0260 gI 0200 250 104 40- 127
Surrogate Decachlorobipheny (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0238 0218 0189 0181
gI
gI
gI
gI
0200 0200 0200 0200
119 109
30- 150 30- 150 30- 150 30- 150
This laboratory report is lot valid without (II authorized sigllature 01 the cover page
Page 18 of25 Reportable Detection Limit BRL = Below Reporting Limit
Extractable Petroleum Hydrocarbons - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051102 - SW846 3510C
Blank 8051102-BLK1
Prepared 15-May-08 Analyzed 19-Mayshy
Non-polar material (SGT- HEM) BRL m91
LC8 8051102-B81
Prepared 15-May-08 Analyzed 19-Mayshy
Non-polar material (SGT- HEM) 184 m91 21 81 904
This laboratory report is not valid without an authorized signature 011 the cover page
Page 19 of25 Reportable Detection Limit BRL = Below Reporting Limit
Soluble Metals by EPA 200 Series Methods - Quality Control
Analyte(s) Result Flag Units RDL
Spike
Level
Source
Result REC
REC
Limits RPD
RPD
Limit
Batch 8051150 - EPA 200 Series
Blank 8051150-BLK1
Prepared amp Analyzed 21-May-
Iron
Zinc
Selenium
Nickel
Chromium
Copper
Arsenic
BRL
BRL
BRL
BRL
BRL
BRL
BRL
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0150
0050
0150
0050
0050
0050
0040
LCS 8051150-BS1
Prepared amp Analyzed 21-May-
Selenium
Zinc
Iron
Nickel
Chromium
Arsenic
Copper
123
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0150
0050
0150
0050
0050
0040
0050
103
105
101
100
85- 115
85- 115
85- 115
85- 115
85- 115
85-115
85- 115
licate B051150-DUP1 Source SA7B602shy
Prepared amp Analyzed 21-May-
Iron
Zinc
Selenium
Nickel
Copper
Chromium
Arsenic
17
0162
BRL
0015
0017
BRL
0450
QR8
mgl
mgl
mgl
mgl
mgl
mgl
mgi
0150
0050
0150
0050
0050
0050
0040
184
0186
BRL
0014
0023
BRL
0468
Matrix S ike 8051150-MS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Iron
Selenium
Nickel
Zinc
Copper
Chromium
Arsenic
19 QM2 mgl
mgll
mgl
mgl
mgl
mgl
mgl
0150
0150
0050
0050
0050
0050
0040
125
184
BRL
0014
0186
0023
BRL
0468
104
105
102
70- 130
70- 130
70-130
70- 130
70- 130
70-130
70- 130
Post S ike 8051150-PS1 Source SA78602shy
Prepared amp Analyzed 21-May-
Zinc
Iron
Selenium
Nickel
Copper
Arsenic
Chromium
18 QM2
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0050
0150
0150
0050
0050
0040
0050
0186
184
BRL
0014
0023
0468
BRL
104
104
101
85- 115
85- 115
85- 115
85-115
85-115
85- 115
85-115
Batch 8051152 - EPA200SW7000 Series
Blank B051152-BLK1
Prepared amp Analyzed 21-May-
Mercury BRL mgl 00020
This laboratory report is IIOt valid witllOut all authorized sigllature 011 the coverpage
Page 20 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Soluble Metals by EPA 200 Series Methods - Quality Control
Analyte(s) Result Flag Units RDL
Spike
Level
Source
Result REC
REC
Limits RPD
RPD
Limit
Batch 8051152 - EPA200SW7000 Series
LCS B051152-BS1
Prepared amp Analyzed 21-May-
Mercury 00576 m91 00020 00500 115 85- 115
licate B051152-DUP1 Source SA78602-01
Prepared amp Analyzed 21-May-
Mercury BRL m91 00020 BRL
Matrix S ike 8051152-MS1 Source SA78602shy
Prepared amp Analyzed 21-May-
Mercury 00632 OM m91 00020 00500 BRL 126 75- 125
Post S ike 8051152-PS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Mercury 00624 OC1 m91 00020 00500 BRL 125 85- 115
Batch 8051249 - 2008No digestion
Blank 8051249-BLK1
Prepared amp Analyzed 21-May-
Lead
Antimony
Cadmium
Silver
BRL
BRL
BRL
BRL
m91
m91
m91
m91
0002
0002
0002
0002
LCS B051249-BS1
Prepared amp Analyzed 21-May-
Antimony
Lead
Silver
Cadmium
143
145 OC2
m91
m91
m91
m91
0050
0050
0050
0040
103
115
107
116
85- 115
85- 115
85- 115
85- 115
licate 8051249-DUP1 Source SA7B602shy
Prepared amp Analyzed 21- May-
Lead
Antimony
Cadmium
Silver
0009
0002
00005
00002
ORB
m91
m91
m91
m91
0002
0002
0002
0002
0011
0003
00005
00003
Matrix S ike 8051249-MS1 Source SA78602shy
Prepared amp Analyzed 21- May-
Lead
Antimony
Cadmium
Silver
142
m91
m91
m91
m91
0050
0050
0040
0050
0011
0003
00005
00003
111
101
114
102
70- 130
70-130
70c130
70- 130
Post S ike 8051249-PS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Antimony
Cadmium
Silver
38
OC2
m91
m91
m91
0050
0040
0050
125
0003
00005
00003
110
121
109
85- 115
85- 115
85- 115
This laboratory report is flOt valid IVithout all authorized signature 011 the cOIer page
Reportable Detection Limit BRL Below Reporting Limit Page 21 of 25
General Chemistry Parameters - Quality Control
Spike Source REC RPD
Analyte( s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051049 - General Preparation
Blank S051 049-BLK1
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
Blank S051049-BLK2
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
Blank S051 049-BLK3
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
LCS S051049-BS1
Prepared amp Analyzed 14-May-
Total Residual Chlorine 046 mgl 020 0500 90- 110
LCS S051049-BS2
Prepared amp Analyzed 14-May-
Total Residual Chlorine 047 mgl 020 0500 90- 110
LCS S051049-BS3
Prepared amp Analyzed 14-May-
Total Residual Chlorine 054 mgl 020 0500 108 90-110
licate B051049-DUP1 Source SA7S544shy
Prepared amp Analyzed 14-May-
Total Residual Chlorine 012 mgl 020 010
licate S051049-DUP2 Source SA7S602-01
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020 BRL
Matrix S ike 8051049-MS1 Source SA78544-01
Prepared amp Analyzed 14-May-
Total Residual Chlorine 065 mgl 020 0500 010 110 80- 120
Matrix S ike 8051049-MS2 Source SA7B602shy
Prepared amp Analyzed 14-May-
Total Residual Chlorine mgl 500 125 BRL 108 80- 120
Reference 8051 049-SRM1
Prepared amp Analyzed 14-May-
Total Residual Chlorine 100 mgl 020 0967 103 85-115
Batch 8051094 - General Preparation
Blank 8051094-BLK1
Prepared amp Analyzed 14 May-
Hexavalent Chromium (soluble) BRL mgl 005
Blank 8051 094-BLK2
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) BRL mgl 005
LCS 8051094-BS1
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) 054 mgl 005 90- 110
licate 8051094-DUP1 Source SA78602-01
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) BRL mgl 125 BRL
Thi laboratory report is not valid without all authorized sigllature 011 the cover page
Page 22 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Page 23
Volatie Organic Compounds - Quality Control
Analyte( s)
Batch 8051244 - SW846 5030 Water MS
Blank 8051244-BLK1
Prepared 16-May-08 Analyzed 17-May-
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromochloromethane
1 Dichlorobenzene
1 Dichlorobenzene
1 Dichlorobenzene
1-Dichloroethane
1 Dichloroethane
1 1-Dichloroethene
cis- Dichloroethene
trans- 1 Dichloroethene
1 Dichloropropane
cis- 1 Dichloropropene
trans- 1 Dichloropropene
Ethylbenzene
Hexanone (MBK)
Methyl tert-butyl ether
Methyl- pentanone (MIBK)
Methylene chloride
Styrene
2- Tetrachloroethane
Tetrachloroethene
Toluene
1- Trichloroethane
2- Trichloroethane
Trichloroethene
Trichlorofluoromethane (Freon 11)
Vinyl chloride
p-Xylene
Xylene
Surrogate 4-Bromofluorobenzene Surrogate Toluene-
Surrogate 1 Dichloroethane-Surrogate Dibromofluoromethane
LCS B051244-BS1
Prepared 16-May-08 Analyzed 17 -May-
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Spike Source REC RPD
Result Flag Units RDL Level Result REC Limits RPD Limit
BRL gl 20
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl 10
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gll
BRL gi
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl 10
BRL gll
BRL gll 10
BRL gl 10
BRL gll
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
41 gl 50 70- 130 49 gl 50 70- 130 59 gl 50 119 70- 130 52 gl 50 105 70- 130
QC2 jgl 20 70- 130
18 jgl 20 70- 130
192 jgl 20 35- 155
18 jgl 20 45- 169
19 jgl 20 242
This laboratOlY repol1 is lot valid without 011 authorized sigllature 011 the cover page
Reportable Detection Limit BRL = Below Reporting Limit Page 9 of 25
Volatie Organic Compounds - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051244 - SW846 5030 Water MS
LC5 8051244B51
Prepared 16-May-08 Analyzed 17-May-
Butanone (MEK) 10 QC2 gl 20 70- 130
Carbon tetrachloride 204 gl 20 102 70- 140
Chlorobenzene 18 gl 20 70- 130
Chloroethane 164 gl 20 14-230
Chloroform 18 gll 20 51- 138
Chloromethane 21 gl 20 106 273
Dibromochloromethane 18 gl 20 53- 149
1 Dichlorobenzene 20 gl 20 104 18- 190
1 Dichlorobenzene 19 gl 20 59- 156
1 A-Dichlorobenzene 18 gl 20 18- 190
1- Dichloroethane 19 gl 20 59- 155
1 Dichloroethane 19 gl 20 49- 155
1-Dichloroethene 16 gl 20 70- 130
cis- 1 Dichloroethene 17 gl 20 70- 130
trans- 1 Dichloroethene 16 gll 20 54- 156
1 Dichloropropane 18 gl 20 210
cis- Dichloropropene 17 gl 20 227
trans- 1 Dichloropropene 17 gl 20 17- 183
Ethylbenzene 19 gl 20 37- 162
Hexanone (MBK) 124 QC2 gl 20 70- 130
Methyl tert-butyl ether 19 gl 20 70- 130
Methylshy pentanone (MIBK) 17 gl 20 70- 130
Methylene chloride 16 gl 20 221
Styrene 17 gl 20 70- 130
1 Tetrachloroethane 194 gl 20 46- 157
Tetrachloroethene 15 gl 20 64- 148
Toluene 18 gl 20 70- 130
1- Trichloroethane 20 gl 20 100 52- 162
2- Trichloroethane 18 gl 20 52- 150
Trichloroethene 17 gl 20 71- 157
Trichlorofluoromethane (Freon 11) 19 gl 20 17- 181
Vinyl chloride 21 gl 20 106 251
p-Xylene 39 gl 40 70- 130
Xylene 20 gl 20 102 70- 130
Surrogate 4-Bromofluorobenzene Surrogate Toluene-
Surrogate 1 Dichloroethane-Surrogate Dibromofluoromethane
52 49 56
49
gl
gl
gl
gl
50 50 50
50
105
112 100
70- 130 70- 130 70- 130 70- 130
LC5 DUD (8051244-B5D1
Prepared 16-May-08 Analyzed 17-May-
Acetone QC2 gl 20 70- 130
Benzene 18 gl 20 70- 130
Bromodichloromethane 18 gl 200 35- 155
Bromoform 17 gl 20 45- 169
Bromomethane 18 gl 20 242
Butanone (MEK) 11 QC2 1-91 20 70- 130
Carbon tetrachloride 20 gl 20 100 70- 140
Chlorobenzene 17 gl 20 70- 130
Chloroethane 15 1-91 20 14-230
Chloroform 18 1-91 20 51- 138
This laboratory report is aot valid without a1 authorized sig1ature 01 the cover page
Reportble Detection Limit BRL = Below Reporting Limit Page 10 of25
Volatie Organic Compounds - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051244 - SW846 5030 Water MS
LCS Dup 18051244-BSD1
Prepared 16-May-08 Analyzed 17-May-
Chloromethane 18 1-91 20 273
Dibromochloromethane 174 1-91 20 53- 149
Dichlorobenzene 20 1-91 20 100 18- 190
Dichlorobenzene 18 1-91 20 59- 156
Dichlorobenzene 18 1-91 20 18- 190
Dichloroethane 18 1-91 20 59- 155
Dichloroethane 19 1-91 20 49- 155
Dichloroethene 16 1-91 20 70- 130
cis- Dichloroethene 16 1-91 20 70- 130
trans- Dichloroethene 15 1-91 20 54- 156
Dichloropropane 17 1-91 20 210
cis- Dichloropropene 164 IJgl 20 227
trans- 1 Dichloropropene 164 I-gl 20 17- 183
Etlwlbenzene 18 IJgl 20 37- 162
Hexanone (MBK) 124 QC2 IJgl 20 70- 130
Methyl tert-butyl ether 184 1J91 20 70- 130
Methyl- pentanone (MIBK) 17 IJgl 20 70- 130
Methylene chloride 16 IJgl 20 221
Styrene 16 IJgl 20 70- 130
2- Tetrachloroethane 19 IJgl 20 46- 157
Tetrachloroethene 15 IJgl 20 64- 148
Toluene 17 IJgl 20 70- 130
1- Trichloroethane 19 1-91 20 52- 162
2- Trichloroethane 16 IJgl 20 52- 150
Trichloroethene 15 IJgl 20 71- 157
Trichlorofluoromethane (Freon 11) 17 IJgl 20 17- 181
Vinyl chloride 19 IJglI 20 251
p-Xylene 37 1J91 40 70- 130
Xylene 20 IJgl 20 100 70- 130
Surrogate 4-Bromofluorobenzene 51 IJgl 50 104 70- 130
Surrogate Toluene- 4B gl 50 70- 130
Surrogate 1 0ichloroethane- 53 IJgl 50 106 70- 130 Surrogate Oibromofluoromethane 50 1J9i 50 102 70- 130
Matrix S ike B051244-MS1 Source SA7B629shy
Prepared 16-May-08 Analyzed 17-May-
Benzene 18 20 BRL 70- 130IJgl
Bromodichloromethane 19 IJgl 20 BRL 35- 155
Bromoform 18 IJgl 20 BRL 45- 169
Bromomethane 16 IJgl 20 BRL 242
Carbon tetrachloride 21 IJgl 20 BRL 106 70- 140
Chlorobenzene 18 IJgl 20 BRL 70- 130
Chloroethane 16 IJgl 20 BRL 14-230
Chloroform 18 IJgl 20 BRL 51- 138
Chloromethane 19 IJgl 20 BRL 273
Dibromochloromethane 17 IJgl 20 BRL 53- 149
1 Dichlorobenzene 22 IJgl 20 BRL 112 18- 190
1 Dichlorobenzene 22 IJgl 20 BRL 110 59-156
1 Dichlorobenzene 21 IJgl 20 BRL 109 18- 190
1- Dichloroethane 19 IJgl 20 BRL 59- 155
1 Dichloroethane 18 IJgl 20 BRL 49- 155
This laboratory report is 110t mUd without an authorized signature on the covel page
Reportble Detection Limit BRL = Below Reporting Limit Page It of25
Volatile Organic Compounds - Quality Control
p
Spike Source REC RPD
Result REC imits RPD LimitAnalyte(s) Result Flag Units RDL Level
Batch 8051244 - SW846 5030 Water MS
Matrix ike S051244-MS1 Source SA7B629shy
Prepared 16-May-08 Analyzed 17-Mayshy
17 20 BRL 70- 130 1- Dichloroethene IJgl
16 20 BRL 54- 156trans- 1 Dichloroethene IJgl
21020 BRL1 Dichloropropane 17 1J91
cis- 1 Dichloropropene 17 IJgl 20 BRL 227
17- 183trans- 1 Dichloropropene 184 1J91 20 BRL
20 20 BRL 103 37- 162Ethylbenzene IJgl
15 20 BRL 221Methylene chloride IJgl
20 BRL 46- 1572- Tetrachloroethane 19 1J91
20 BRL 64- 148Tetrachloroethene 18 1J91
BRL 70- 130Toluene 18 1J91 20
105 52-1621- Trichloroethane 211 IJgl 20 BRL
18 20 BRL 52- 1502- Trichloroethane IJgl
17 20 BRL 71- 157Trichloroethene 1J91
20 BRL 17- 181Trichloroluoromethane (Freon 11) 194 IJgl
20 BRL 103 251Vinyl chloride 20 IJgl
102 70- 130Surrogate 4-Bromofluorobenzene 50 IJgl 50 50 70- 130Surrogate Toluene- 49 1J91
56 50 112 70- 130Surrogate 1 Dichloroethane- IJgl
50 100 70- 130Surrogate Dibromofluoromethane 50 IJgl
Matrix S ike Du S051244-MSD1 Source SA7S629shy
Prepared 16-May-08 Analyzed 17-Mayshy
18 20 BRL 70- 130Benzene IJgl
18 20 BRL 35- 155Bromodichloromethane IJgl
17 20 BRL 45- 169Bromoform IJgl
20 BRL 242Bromomethane 17 IJgl
20 BRL 103 70- 140Carbon tetrachloride 20 IJgl
18 20 BRL 70- 130Chlorobenzene 1J91
14-230Chloroethane 16 IJgl 20 BRL
20 51- 138Chloroform 184 IJgl BRL
Chloromethane 19 1J91 20 BRL 273
18 20 BRL 53- 149Dibromochloromethane 1J91
20 BRL 117 18- 190Dichlorobenzene 234 IJgl
20 BRL 112 59- 156Dichlorobenzene 22 IJgl
BRL 108 18- 190Dichlorobenzene 21 1J91 20
20 59- 1551 Dichloroethane 19 IJgl BRL
18 20 BRL 49- 155Dichloroethane IJgl
16 20 BRL 70- 130Dichloroethene IJgl
20 BRL 54- 156trans- Dichloroethene 154 1J91
20 BRL 210Dichloropropane 17 IJgl
0420 BRL 227cis- Dichloropropene 17 IJgl
17- 183trans- Dichloropropene 17 1J91 20 BRL
BRL 37- 162Ethylbenzene 20 1J91 20 102
Methylene chloride 15 IJgl 20 BRL 221
20 BRL 46- 1572- Tetrachloroethane 192 IJgl
20 BRL 64- 148 04Tetrachloroethene 18 IJgl
BRL 70- 130Toluene 184 1J91 20
52- 1621- Trichloroethane 20 IJgl 20 BRL 104
17 20 BRL 52- 1502- Trichloroethane IJgl
17 20 BRL 71- 157Trichloroethene IJgl
20 BRL 17-181Trichlorofluoromethane (Freon 11) 19 IJgl
This laboratory report is IIOt valid without all authorized sigllllture 011 the cover page
Page 12 of25 Reportble Detection Limit BRL = Below Reporting Limit
Semivolatile Organic Compounds by GCMS - Quality Control
Analyte(s)
Batch 8051216 - SW846 3510C
Blank 8051216-BLK1
Prepared amp Analyzed 16-May-
Isophorone
Methylnaphthalene
Methylphenol
3 amp 4-Methylphenol
Naphthalene
Nitroaniline
Nitroaniline
Nitroaniline
Nitrobenzene
Nitrophenol
Nitrophenol
Nitrosodimethylamine
N- N itrosodi-n-pro pyla mine
N itrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Pyridine
1 24-Trichlorobenzene
24 5- Trichlorophenol
246- Trichlorophenol
Surrogate 2-Fuorobipheny Surrogate 2-Fuoropheno Surrogate Nitrobenzene-Surrogate PhenoshySurrogate Terpheny-d4 Surrogate 6- Tribromopheno
LCS B051216-BS1
Prepared amp Analyzed 16-May-
Acenaphthene
Acenaphthylene
Aniline
Anthracene
AzobenzenelDi phenyld lazine
Benzidine
Benzo (a) anthracene
Benzo (a) pyrene
Benzo (b) fluoranthene
Benzo (g i) perylene
Benzo (k) fluoranthene
Benzoic acid
Benzyl alcohol
B is(2-chloroethoxy)methane
B i s (2-ch loroethyl)eth e r
Bis(2-ch loroisopropyl) ether
B is(2-ethy Ih exyl) phtha late
Bromophenyl phenyl ether
Butyl benzyl phthalate
Carbazole
Spike Source REC RPD
Result Flag Units RDL Level Result REC Limits RPD Limit
BRL gl
BRL gl
BRL gl
BRL gl 10
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gll
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
370 gl 50 30- 130 40 gl 50 15- 110 39 gl 50 30- 130 43 gl 50 15- 110 36 gl 50 30- 130 40 gl 50 15- 110
41 gl 50 40- 140
43 gI 50 40- 140
41 gl 50 40- 140
38 gl 50 40- 140
45 gl 50 40- 140
49 gl 50 153
41 gl 50 40- 140
43 gl 50 40- 140
41 gl 50 40- 140
41 gll 50 40- 140
45 gl 50 40- 140
32 gl 50 12- 149
41 gl 50 40- 140
39 gl 50 40- 140
384 gl 50 40- 140
47 gl 50 40- 140
47 gl 50 40- 140
40 gl 50 40- 140
47 gI 50 40- 140
56 gI 50 112 200
This laboratory report is lIot valid witllOut a1l authorized sigllature 011 the coverpage
Reportble Detection Limit BRL = Below Reporting Limit Page 15 of25
Semivolatile Organic Compounds by GCMS - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051216 - SW846 3510C
LCS 8051216-BS1
Prepared amp Analyzed 16-Mayshy
50 30- 1304 -C hloro-3-methylphenol 42 IJgl
40- 140Chloroaniline 39 IJgl 50
Chloronaphthalene 37 IJgl 50 40- 140
Chlorophenol 37 IJgl 50 30- 130
50 40- 140
40- 140
Chlorophenyl phenyl ether 45 IJgl
Chrysene 43 IJgl 50
Dibenzo (a h) anthracene 43 IJgl 50 40- 140
Dibenzofuran IJgl38 50 40- 140
50 40- 1401 Dichlorobenzene 35 IJgl
40- 1401 Dichlorobenzene 264 IJgl 50
40- 1401 Dichlorobenzene 434 IJgl 50
58 50 116 40- 1403 - Dichlorobenzidine IJgl
50 30- 130
40- 140 24-Dichlorophenol 38 IJgl
Diethyl phthalate 484 IJgl 50
50 40- 140Dimethyl phthalate 464 IJgl
Dlmethylphenol 39 IJgl 50 30- 130
DI-n-butyl phthalate 44 IJgll 50 40- 140
30- 130 6-Di nitro- 2-methylphenol 38 1J91 50
30- 130Dinltrophenol 36 1J91 50
42 50 40- 14024-Dlnitrotoluene 1J91
Dlnitrotoluene 1J9141 50 40- 140
Di-n-octyl phthalate 52 IJgl 50 104 40- 140
40- 140Fluoranthene 40 IJgl 50
Fluorene 41 IJgl 50 40- 140
39 50 40- 140Hexachlorobenzene IJgl
50 40- 140Hexachlorobutadiene 40 IJgl
40- 140Hexach lorocyclopentad iene 294 IJgl 50
40 50 40- 140Hexachloroethane IJgl
42 50 40-140Indeno (1 3-cd) pyrene IJgl
50 40- 140Isophorone 40 IJgl
40- 140Methylnaphthalene 394 IJgl 50
40- 140Methylphenol 39 IJgl 50
40 10 50 40- 1403 amp 4-Methylphenol IJgl
37 50 40-140Naphthalene IJgl
50 40-140Nitroaniline 39 IJgl
Nitroaniline 51 IJgl 50 102 40- 140
48 50 40- 140Nltroaniline 1J91
50 40- 140Nitrobenzene 40 IJgl
30- 130Nitrophenol 36 IJgl 50
40 IJgl 50 30- 130Nitrophenol 40- 140Nitrosodimethylamine 32 1J91 50
50 40-140N- N itrosodi-n-propyla mine 46 IJgl
40- 140N itrosodi phenyla ml ne 44 IJgl 50
41 IJgl 50 30- 130Pentachlorophenol 40- 140Phenanthrene 38 IJgl 50
50 30- 130Phenol 38 IJgl
40- 140Pyrene 424 1J91 50
40- 140Pyridine 294 1J91 50
40- 14024- Trichlorobenzene 364 IJgl 50
This laboratory report is not mlid without an authorized signature 011 the cover page
Page 16 of25 Reportble Detection Limit BRL = Below Reporting Limit
Semivolatie Organic Compounds by GCMS - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
BMch 8051216 - SW846 3510C
LC5 8051216-851
Prepared amp Analyzed 16-Mayshy
24 5- Trichlorophenol 404 gl 50 30- 130
246- Trichlorophenol 42 gl 50 30- 130
Surrogate 2-Fluorobiphenyl 29 gl 50 30- 130
Surrogate 2-Fluorophenot 27 gl 50 15- 110
Surrogate Nitrobenzene- 30 gl 50 30- 130
Surrogate Phenol- 29 gl 50 15- 110
Surrogate Terpheny-d4 30 gl 50 30- 130
Surrogate 6- Tribromopheno 324 gl 50 15- 110
This laboratory report is lIot valid without all authorized sigllature 011 tlle cover page
Reportble Detection Limit BRL = Below Reporting Limit Page 17 of25
Semivolatie Organic Compounds by GC - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051106 - SW846 3510C
Blank S051106-BLK1
Prepared amp Analyzed 15-Mayshy
Aroclor- 1016 BRL gI 0200
Aroclor- 1016 (2C) BRL gI 0200
Aroclor- 1221 BRL gI 0200
Aroclor- 1221 (2C) BRL gI 0200
Aroclor- 1232 BRL gI 0200
Aroclor- 1232 (2Cj BRL gI 0200
Aroclor- 1242 BRL gI 0200
Aroclor-1242 (2C) BRL gI 0200
Aroclor- 1248 BRL gI 0200
Aroclor- 1248 (2C) BRL gI 0200
Aroclor- 1254 BRL gI 0200
Aroclor- 1254(2Cj BRL gI 0200
Aroclor- 1260 BRL gI 0200
Aroclor- 1260 (2C) BRL gI 0200
Aroclor- 1262 BRL gI 0200
Aroclor- 1262 (2C) BRL gI 0200
Aroclor-1268 BRL gI 0200
Aroclor- 1268 (2C) BRL gI 0200
Surrogate Decachlorobiphenyl (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0231 0224 0194 0191
gI
gI
gI
gI
0200 0200 0200 0200
116 112
30- 150 30- 150 30- 150 30- 150
LC5 8051106-B51
Prepared 15-May-08 Analyzed 16-May-08
Aroclor- 1016 265 gI 0200 250 106 50- 114
Aroclor- 1 016 (2C) 240 gI 0200 250 50- 114
Aroclor- 1260 0269 gI 0200 250 107 40- 127
Aroclor-1260 (2Cj 270 gI 0200 250 108 40- 127
Surrogate Decachlorobiphenyl (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0225 0224 0188 0183
gI
gI
gI
gI
0200 0200 0200 0200
113 112
30- 150 30- 150 30- 150 30- 150
LC5 DUD rS051106-B5D1
Prepared 15-May-08 Analyzed 16-Mayshy
Aroclor- 1016 262 gl 0200 250 105 50- 114
Aroclor-1 016 (2Cj 241 gI 0200 250 50- 114
Aroclor- 1260 277 gI 0200 250 111 40- 127
Aroclor- 1260(2Cj 0260 gI 0200 250 104 40- 127
Surrogate Decachlorobipheny (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0238 0218 0189 0181
gI
gI
gI
gI
0200 0200 0200 0200
119 109
30- 150 30- 150 30- 150 30- 150
This laboratory report is lot valid without (II authorized sigllature 01 the cover page
Page 18 of25 Reportable Detection Limit BRL = Below Reporting Limit
Extractable Petroleum Hydrocarbons - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051102 - SW846 3510C
Blank 8051102-BLK1
Prepared 15-May-08 Analyzed 19-Mayshy
Non-polar material (SGT- HEM) BRL m91
LC8 8051102-B81
Prepared 15-May-08 Analyzed 19-Mayshy
Non-polar material (SGT- HEM) 184 m91 21 81 904
This laboratory report is not valid without an authorized signature 011 the cover page
Page 19 of25 Reportable Detection Limit BRL = Below Reporting Limit
Soluble Metals by EPA 200 Series Methods - Quality Control
Analyte(s) Result Flag Units RDL
Spike
Level
Source
Result REC
REC
Limits RPD
RPD
Limit
Batch 8051150 - EPA 200 Series
Blank 8051150-BLK1
Prepared amp Analyzed 21-May-
Iron
Zinc
Selenium
Nickel
Chromium
Copper
Arsenic
BRL
BRL
BRL
BRL
BRL
BRL
BRL
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0150
0050
0150
0050
0050
0050
0040
LCS 8051150-BS1
Prepared amp Analyzed 21-May-
Selenium
Zinc
Iron
Nickel
Chromium
Arsenic
Copper
123
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0150
0050
0150
0050
0050
0040
0050
103
105
101
100
85- 115
85- 115
85- 115
85- 115
85- 115
85-115
85- 115
licate B051150-DUP1 Source SA7B602shy
Prepared amp Analyzed 21-May-
Iron
Zinc
Selenium
Nickel
Copper
Chromium
Arsenic
17
0162
BRL
0015
0017
BRL
0450
QR8
mgl
mgl
mgl
mgl
mgl
mgl
mgi
0150
0050
0150
0050
0050
0050
0040
184
0186
BRL
0014
0023
BRL
0468
Matrix S ike 8051150-MS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Iron
Selenium
Nickel
Zinc
Copper
Chromium
Arsenic
19 QM2 mgl
mgll
mgl
mgl
mgl
mgl
mgl
0150
0150
0050
0050
0050
0050
0040
125
184
BRL
0014
0186
0023
BRL
0468
104
105
102
70- 130
70- 130
70-130
70- 130
70- 130
70-130
70- 130
Post S ike 8051150-PS1 Source SA78602shy
Prepared amp Analyzed 21-May-
Zinc
Iron
Selenium
Nickel
Copper
Arsenic
Chromium
18 QM2
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0050
0150
0150
0050
0050
0040
0050
0186
184
BRL
0014
0023
0468
BRL
104
104
101
85- 115
85- 115
85- 115
85-115
85-115
85- 115
85-115
Batch 8051152 - EPA200SW7000 Series
Blank B051152-BLK1
Prepared amp Analyzed 21-May-
Mercury BRL mgl 00020
This laboratory report is IIOt valid witllOut all authorized sigllature 011 the coverpage
Page 20 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Soluble Metals by EPA 200 Series Methods - Quality Control
Analyte(s) Result Flag Units RDL
Spike
Level
Source
Result REC
REC
Limits RPD
RPD
Limit
Batch 8051152 - EPA200SW7000 Series
LCS B051152-BS1
Prepared amp Analyzed 21-May-
Mercury 00576 m91 00020 00500 115 85- 115
licate B051152-DUP1 Source SA78602-01
Prepared amp Analyzed 21-May-
Mercury BRL m91 00020 BRL
Matrix S ike 8051152-MS1 Source SA78602shy
Prepared amp Analyzed 21-May-
Mercury 00632 OM m91 00020 00500 BRL 126 75- 125
Post S ike 8051152-PS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Mercury 00624 OC1 m91 00020 00500 BRL 125 85- 115
Batch 8051249 - 2008No digestion
Blank 8051249-BLK1
Prepared amp Analyzed 21-May-
Lead
Antimony
Cadmium
Silver
BRL
BRL
BRL
BRL
m91
m91
m91
m91
0002
0002
0002
0002
LCS B051249-BS1
Prepared amp Analyzed 21-May-
Antimony
Lead
Silver
Cadmium
143
145 OC2
m91
m91
m91
m91
0050
0050
0050
0040
103
115
107
116
85- 115
85- 115
85- 115
85- 115
licate 8051249-DUP1 Source SA7B602shy
Prepared amp Analyzed 21- May-
Lead
Antimony
Cadmium
Silver
0009
0002
00005
00002
ORB
m91
m91
m91
m91
0002
0002
0002
0002
0011
0003
00005
00003
Matrix S ike 8051249-MS1 Source SA78602shy
Prepared amp Analyzed 21- May-
Lead
Antimony
Cadmium
Silver
142
m91
m91
m91
m91
0050
0050
0040
0050
0011
0003
00005
00003
111
101
114
102
70- 130
70-130
70c130
70- 130
Post S ike 8051249-PS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Antimony
Cadmium
Silver
38
OC2
m91
m91
m91
0050
0040
0050
125
0003
00005
00003
110
121
109
85- 115
85- 115
85- 115
This laboratory report is flOt valid IVithout all authorized signature 011 the cOIer page
Reportable Detection Limit BRL Below Reporting Limit Page 21 of 25
General Chemistry Parameters - Quality Control
Spike Source REC RPD
Analyte( s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051049 - General Preparation
Blank S051 049-BLK1
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
Blank S051049-BLK2
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
Blank S051 049-BLK3
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
LCS S051049-BS1
Prepared amp Analyzed 14-May-
Total Residual Chlorine 046 mgl 020 0500 90- 110
LCS S051049-BS2
Prepared amp Analyzed 14-May-
Total Residual Chlorine 047 mgl 020 0500 90- 110
LCS S051049-BS3
Prepared amp Analyzed 14-May-
Total Residual Chlorine 054 mgl 020 0500 108 90-110
licate B051049-DUP1 Source SA7S544shy
Prepared amp Analyzed 14-May-
Total Residual Chlorine 012 mgl 020 010
licate S051049-DUP2 Source SA7S602-01
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020 BRL
Matrix S ike 8051049-MS1 Source SA78544-01
Prepared amp Analyzed 14-May-
Total Residual Chlorine 065 mgl 020 0500 010 110 80- 120
Matrix S ike 8051049-MS2 Source SA7B602shy
Prepared amp Analyzed 14-May-
Total Residual Chlorine mgl 500 125 BRL 108 80- 120
Reference 8051 049-SRM1
Prepared amp Analyzed 14-May-
Total Residual Chlorine 100 mgl 020 0967 103 85-115
Batch 8051094 - General Preparation
Blank 8051094-BLK1
Prepared amp Analyzed 14 May-
Hexavalent Chromium (soluble) BRL mgl 005
Blank 8051 094-BLK2
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) BRL mgl 005
LCS 8051094-BS1
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) 054 mgl 005 90- 110
licate 8051094-DUP1 Source SA78602-01
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) BRL mgl 125 BRL
Thi laboratory report is not valid without all authorized sigllature 011 the cover page
Page 22 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Page 24
Volatie Organic Compounds - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051244 - SW846 5030 Water MS
LC5 8051244B51
Prepared 16-May-08 Analyzed 17-May-
Butanone (MEK) 10 QC2 gl 20 70- 130
Carbon tetrachloride 204 gl 20 102 70- 140
Chlorobenzene 18 gl 20 70- 130
Chloroethane 164 gl 20 14-230
Chloroform 18 gll 20 51- 138
Chloromethane 21 gl 20 106 273
Dibromochloromethane 18 gl 20 53- 149
1 Dichlorobenzene 20 gl 20 104 18- 190
1 Dichlorobenzene 19 gl 20 59- 156
1 A-Dichlorobenzene 18 gl 20 18- 190
1- Dichloroethane 19 gl 20 59- 155
1 Dichloroethane 19 gl 20 49- 155
1-Dichloroethene 16 gl 20 70- 130
cis- 1 Dichloroethene 17 gl 20 70- 130
trans- 1 Dichloroethene 16 gll 20 54- 156
1 Dichloropropane 18 gl 20 210
cis- Dichloropropene 17 gl 20 227
trans- 1 Dichloropropene 17 gl 20 17- 183
Ethylbenzene 19 gl 20 37- 162
Hexanone (MBK) 124 QC2 gl 20 70- 130
Methyl tert-butyl ether 19 gl 20 70- 130
Methylshy pentanone (MIBK) 17 gl 20 70- 130
Methylene chloride 16 gl 20 221
Styrene 17 gl 20 70- 130
1 Tetrachloroethane 194 gl 20 46- 157
Tetrachloroethene 15 gl 20 64- 148
Toluene 18 gl 20 70- 130
1- Trichloroethane 20 gl 20 100 52- 162
2- Trichloroethane 18 gl 20 52- 150
Trichloroethene 17 gl 20 71- 157
Trichlorofluoromethane (Freon 11) 19 gl 20 17- 181
Vinyl chloride 21 gl 20 106 251
p-Xylene 39 gl 40 70- 130
Xylene 20 gl 20 102 70- 130
Surrogate 4-Bromofluorobenzene Surrogate Toluene-
Surrogate 1 Dichloroethane-Surrogate Dibromofluoromethane
52 49 56
49
gl
gl
gl
gl
50 50 50
50
105
112 100
70- 130 70- 130 70- 130 70- 130
LC5 DUD (8051244-B5D1
Prepared 16-May-08 Analyzed 17-May-
Acetone QC2 gl 20 70- 130
Benzene 18 gl 20 70- 130
Bromodichloromethane 18 gl 200 35- 155
Bromoform 17 gl 20 45- 169
Bromomethane 18 gl 20 242
Butanone (MEK) 11 QC2 1-91 20 70- 130
Carbon tetrachloride 20 gl 20 100 70- 140
Chlorobenzene 17 gl 20 70- 130
Chloroethane 15 1-91 20 14-230
Chloroform 18 1-91 20 51- 138
This laboratory report is aot valid without a1 authorized sig1ature 01 the cover page
Reportble Detection Limit BRL = Below Reporting Limit Page 10 of25
Volatie Organic Compounds - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051244 - SW846 5030 Water MS
LCS Dup 18051244-BSD1
Prepared 16-May-08 Analyzed 17-May-
Chloromethane 18 1-91 20 273
Dibromochloromethane 174 1-91 20 53- 149
Dichlorobenzene 20 1-91 20 100 18- 190
Dichlorobenzene 18 1-91 20 59- 156
Dichlorobenzene 18 1-91 20 18- 190
Dichloroethane 18 1-91 20 59- 155
Dichloroethane 19 1-91 20 49- 155
Dichloroethene 16 1-91 20 70- 130
cis- Dichloroethene 16 1-91 20 70- 130
trans- Dichloroethene 15 1-91 20 54- 156
Dichloropropane 17 1-91 20 210
cis- Dichloropropene 164 IJgl 20 227
trans- 1 Dichloropropene 164 I-gl 20 17- 183
Etlwlbenzene 18 IJgl 20 37- 162
Hexanone (MBK) 124 QC2 IJgl 20 70- 130
Methyl tert-butyl ether 184 1J91 20 70- 130
Methyl- pentanone (MIBK) 17 IJgl 20 70- 130
Methylene chloride 16 IJgl 20 221
Styrene 16 IJgl 20 70- 130
2- Tetrachloroethane 19 IJgl 20 46- 157
Tetrachloroethene 15 IJgl 20 64- 148
Toluene 17 IJgl 20 70- 130
1- Trichloroethane 19 1-91 20 52- 162
2- Trichloroethane 16 IJgl 20 52- 150
Trichloroethene 15 IJgl 20 71- 157
Trichlorofluoromethane (Freon 11) 17 IJgl 20 17- 181
Vinyl chloride 19 IJglI 20 251
p-Xylene 37 1J91 40 70- 130
Xylene 20 IJgl 20 100 70- 130
Surrogate 4-Bromofluorobenzene 51 IJgl 50 104 70- 130
Surrogate Toluene- 4B gl 50 70- 130
Surrogate 1 0ichloroethane- 53 IJgl 50 106 70- 130 Surrogate Oibromofluoromethane 50 1J9i 50 102 70- 130
Matrix S ike B051244-MS1 Source SA7B629shy
Prepared 16-May-08 Analyzed 17-May-
Benzene 18 20 BRL 70- 130IJgl
Bromodichloromethane 19 IJgl 20 BRL 35- 155
Bromoform 18 IJgl 20 BRL 45- 169
Bromomethane 16 IJgl 20 BRL 242
Carbon tetrachloride 21 IJgl 20 BRL 106 70- 140
Chlorobenzene 18 IJgl 20 BRL 70- 130
Chloroethane 16 IJgl 20 BRL 14-230
Chloroform 18 IJgl 20 BRL 51- 138
Chloromethane 19 IJgl 20 BRL 273
Dibromochloromethane 17 IJgl 20 BRL 53- 149
1 Dichlorobenzene 22 IJgl 20 BRL 112 18- 190
1 Dichlorobenzene 22 IJgl 20 BRL 110 59-156
1 Dichlorobenzene 21 IJgl 20 BRL 109 18- 190
1- Dichloroethane 19 IJgl 20 BRL 59- 155
1 Dichloroethane 18 IJgl 20 BRL 49- 155
This laboratory report is 110t mUd without an authorized signature on the covel page
Reportble Detection Limit BRL = Below Reporting Limit Page It of25
Volatile Organic Compounds - Quality Control
p
Spike Source REC RPD
Result REC imits RPD LimitAnalyte(s) Result Flag Units RDL Level
Batch 8051244 - SW846 5030 Water MS
Matrix ike S051244-MS1 Source SA7B629shy
Prepared 16-May-08 Analyzed 17-Mayshy
17 20 BRL 70- 130 1- Dichloroethene IJgl
16 20 BRL 54- 156trans- 1 Dichloroethene IJgl
21020 BRL1 Dichloropropane 17 1J91
cis- 1 Dichloropropene 17 IJgl 20 BRL 227
17- 183trans- 1 Dichloropropene 184 1J91 20 BRL
20 20 BRL 103 37- 162Ethylbenzene IJgl
15 20 BRL 221Methylene chloride IJgl
20 BRL 46- 1572- Tetrachloroethane 19 1J91
20 BRL 64- 148Tetrachloroethene 18 1J91
BRL 70- 130Toluene 18 1J91 20
105 52-1621- Trichloroethane 211 IJgl 20 BRL
18 20 BRL 52- 1502- Trichloroethane IJgl
17 20 BRL 71- 157Trichloroethene 1J91
20 BRL 17- 181Trichloroluoromethane (Freon 11) 194 IJgl
20 BRL 103 251Vinyl chloride 20 IJgl
102 70- 130Surrogate 4-Bromofluorobenzene 50 IJgl 50 50 70- 130Surrogate Toluene- 49 1J91
56 50 112 70- 130Surrogate 1 Dichloroethane- IJgl
50 100 70- 130Surrogate Dibromofluoromethane 50 IJgl
Matrix S ike Du S051244-MSD1 Source SA7S629shy
Prepared 16-May-08 Analyzed 17-Mayshy
18 20 BRL 70- 130Benzene IJgl
18 20 BRL 35- 155Bromodichloromethane IJgl
17 20 BRL 45- 169Bromoform IJgl
20 BRL 242Bromomethane 17 IJgl
20 BRL 103 70- 140Carbon tetrachloride 20 IJgl
18 20 BRL 70- 130Chlorobenzene 1J91
14-230Chloroethane 16 IJgl 20 BRL
20 51- 138Chloroform 184 IJgl BRL
Chloromethane 19 1J91 20 BRL 273
18 20 BRL 53- 149Dibromochloromethane 1J91
20 BRL 117 18- 190Dichlorobenzene 234 IJgl
20 BRL 112 59- 156Dichlorobenzene 22 IJgl
BRL 108 18- 190Dichlorobenzene 21 1J91 20
20 59- 1551 Dichloroethane 19 IJgl BRL
18 20 BRL 49- 155Dichloroethane IJgl
16 20 BRL 70- 130Dichloroethene IJgl
20 BRL 54- 156trans- Dichloroethene 154 1J91
20 BRL 210Dichloropropane 17 IJgl
0420 BRL 227cis- Dichloropropene 17 IJgl
17- 183trans- Dichloropropene 17 1J91 20 BRL
BRL 37- 162Ethylbenzene 20 1J91 20 102
Methylene chloride 15 IJgl 20 BRL 221
20 BRL 46- 1572- Tetrachloroethane 192 IJgl
20 BRL 64- 148 04Tetrachloroethene 18 IJgl
BRL 70- 130Toluene 184 1J91 20
52- 1621- Trichloroethane 20 IJgl 20 BRL 104
17 20 BRL 52- 1502- Trichloroethane IJgl
17 20 BRL 71- 157Trichloroethene IJgl
20 BRL 17-181Trichlorofluoromethane (Freon 11) 19 IJgl
This laboratory report is IIOt valid without all authorized sigllllture 011 the cover page
Page 12 of25 Reportble Detection Limit BRL = Below Reporting Limit
Semivolatile Organic Compounds by GCMS - Quality Control
Analyte(s)
Batch 8051216 - SW846 3510C
Blank 8051216-BLK1
Prepared amp Analyzed 16-May-
Isophorone
Methylnaphthalene
Methylphenol
3 amp 4-Methylphenol
Naphthalene
Nitroaniline
Nitroaniline
Nitroaniline
Nitrobenzene
Nitrophenol
Nitrophenol
Nitrosodimethylamine
N- N itrosodi-n-pro pyla mine
N itrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Pyridine
1 24-Trichlorobenzene
24 5- Trichlorophenol
246- Trichlorophenol
Surrogate 2-Fuorobipheny Surrogate 2-Fuoropheno Surrogate Nitrobenzene-Surrogate PhenoshySurrogate Terpheny-d4 Surrogate 6- Tribromopheno
LCS B051216-BS1
Prepared amp Analyzed 16-May-
Acenaphthene
Acenaphthylene
Aniline
Anthracene
AzobenzenelDi phenyld lazine
Benzidine
Benzo (a) anthracene
Benzo (a) pyrene
Benzo (b) fluoranthene
Benzo (g i) perylene
Benzo (k) fluoranthene
Benzoic acid
Benzyl alcohol
B is(2-chloroethoxy)methane
B i s (2-ch loroethyl)eth e r
Bis(2-ch loroisopropyl) ether
B is(2-ethy Ih exyl) phtha late
Bromophenyl phenyl ether
Butyl benzyl phthalate
Carbazole
Spike Source REC RPD
Result Flag Units RDL Level Result REC Limits RPD Limit
BRL gl
BRL gl
BRL gl
BRL gl 10
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gll
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
370 gl 50 30- 130 40 gl 50 15- 110 39 gl 50 30- 130 43 gl 50 15- 110 36 gl 50 30- 130 40 gl 50 15- 110
41 gl 50 40- 140
43 gI 50 40- 140
41 gl 50 40- 140
38 gl 50 40- 140
45 gl 50 40- 140
49 gl 50 153
41 gl 50 40- 140
43 gl 50 40- 140
41 gl 50 40- 140
41 gll 50 40- 140
45 gl 50 40- 140
32 gl 50 12- 149
41 gl 50 40- 140
39 gl 50 40- 140
384 gl 50 40- 140
47 gl 50 40- 140
47 gl 50 40- 140
40 gl 50 40- 140
47 gI 50 40- 140
56 gI 50 112 200
This laboratory report is lIot valid witllOut a1l authorized sigllature 011 the coverpage
Reportble Detection Limit BRL = Below Reporting Limit Page 15 of25
Semivolatile Organic Compounds by GCMS - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051216 - SW846 3510C
LCS 8051216-BS1
Prepared amp Analyzed 16-Mayshy
50 30- 1304 -C hloro-3-methylphenol 42 IJgl
40- 140Chloroaniline 39 IJgl 50
Chloronaphthalene 37 IJgl 50 40- 140
Chlorophenol 37 IJgl 50 30- 130
50 40- 140
40- 140
Chlorophenyl phenyl ether 45 IJgl
Chrysene 43 IJgl 50
Dibenzo (a h) anthracene 43 IJgl 50 40- 140
Dibenzofuran IJgl38 50 40- 140
50 40- 1401 Dichlorobenzene 35 IJgl
40- 1401 Dichlorobenzene 264 IJgl 50
40- 1401 Dichlorobenzene 434 IJgl 50
58 50 116 40- 1403 - Dichlorobenzidine IJgl
50 30- 130
40- 140 24-Dichlorophenol 38 IJgl
Diethyl phthalate 484 IJgl 50
50 40- 140Dimethyl phthalate 464 IJgl
Dlmethylphenol 39 IJgl 50 30- 130
DI-n-butyl phthalate 44 IJgll 50 40- 140
30- 130 6-Di nitro- 2-methylphenol 38 1J91 50
30- 130Dinltrophenol 36 1J91 50
42 50 40- 14024-Dlnitrotoluene 1J91
Dlnitrotoluene 1J9141 50 40- 140
Di-n-octyl phthalate 52 IJgl 50 104 40- 140
40- 140Fluoranthene 40 IJgl 50
Fluorene 41 IJgl 50 40- 140
39 50 40- 140Hexachlorobenzene IJgl
50 40- 140Hexachlorobutadiene 40 IJgl
40- 140Hexach lorocyclopentad iene 294 IJgl 50
40 50 40- 140Hexachloroethane IJgl
42 50 40-140Indeno (1 3-cd) pyrene IJgl
50 40- 140Isophorone 40 IJgl
40- 140Methylnaphthalene 394 IJgl 50
40- 140Methylphenol 39 IJgl 50
40 10 50 40- 1403 amp 4-Methylphenol IJgl
37 50 40-140Naphthalene IJgl
50 40-140Nitroaniline 39 IJgl
Nitroaniline 51 IJgl 50 102 40- 140
48 50 40- 140Nltroaniline 1J91
50 40- 140Nitrobenzene 40 IJgl
30- 130Nitrophenol 36 IJgl 50
40 IJgl 50 30- 130Nitrophenol 40- 140Nitrosodimethylamine 32 1J91 50
50 40-140N- N itrosodi-n-propyla mine 46 IJgl
40- 140N itrosodi phenyla ml ne 44 IJgl 50
41 IJgl 50 30- 130Pentachlorophenol 40- 140Phenanthrene 38 IJgl 50
50 30- 130Phenol 38 IJgl
40- 140Pyrene 424 1J91 50
40- 140Pyridine 294 1J91 50
40- 14024- Trichlorobenzene 364 IJgl 50
This laboratory report is not mlid without an authorized signature 011 the cover page
Page 16 of25 Reportble Detection Limit BRL = Below Reporting Limit
Semivolatie Organic Compounds by GCMS - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
BMch 8051216 - SW846 3510C
LC5 8051216-851
Prepared amp Analyzed 16-Mayshy
24 5- Trichlorophenol 404 gl 50 30- 130
246- Trichlorophenol 42 gl 50 30- 130
Surrogate 2-Fluorobiphenyl 29 gl 50 30- 130
Surrogate 2-Fluorophenot 27 gl 50 15- 110
Surrogate Nitrobenzene- 30 gl 50 30- 130
Surrogate Phenol- 29 gl 50 15- 110
Surrogate Terpheny-d4 30 gl 50 30- 130
Surrogate 6- Tribromopheno 324 gl 50 15- 110
This laboratory report is lIot valid without all authorized sigllature 011 tlle cover page
Reportble Detection Limit BRL = Below Reporting Limit Page 17 of25
Semivolatie Organic Compounds by GC - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051106 - SW846 3510C
Blank S051106-BLK1
Prepared amp Analyzed 15-Mayshy
Aroclor- 1016 BRL gI 0200
Aroclor- 1016 (2C) BRL gI 0200
Aroclor- 1221 BRL gI 0200
Aroclor- 1221 (2C) BRL gI 0200
Aroclor- 1232 BRL gI 0200
Aroclor- 1232 (2Cj BRL gI 0200
Aroclor- 1242 BRL gI 0200
Aroclor-1242 (2C) BRL gI 0200
Aroclor- 1248 BRL gI 0200
Aroclor- 1248 (2C) BRL gI 0200
Aroclor- 1254 BRL gI 0200
Aroclor- 1254(2Cj BRL gI 0200
Aroclor- 1260 BRL gI 0200
Aroclor- 1260 (2C) BRL gI 0200
Aroclor- 1262 BRL gI 0200
Aroclor- 1262 (2C) BRL gI 0200
Aroclor-1268 BRL gI 0200
Aroclor- 1268 (2C) BRL gI 0200
Surrogate Decachlorobiphenyl (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0231 0224 0194 0191
gI
gI
gI
gI
0200 0200 0200 0200
116 112
30- 150 30- 150 30- 150 30- 150
LC5 8051106-B51
Prepared 15-May-08 Analyzed 16-May-08
Aroclor- 1016 265 gI 0200 250 106 50- 114
Aroclor- 1 016 (2C) 240 gI 0200 250 50- 114
Aroclor- 1260 0269 gI 0200 250 107 40- 127
Aroclor-1260 (2Cj 270 gI 0200 250 108 40- 127
Surrogate Decachlorobiphenyl (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0225 0224 0188 0183
gI
gI
gI
gI
0200 0200 0200 0200
113 112
30- 150 30- 150 30- 150 30- 150
LC5 DUD rS051106-B5D1
Prepared 15-May-08 Analyzed 16-Mayshy
Aroclor- 1016 262 gl 0200 250 105 50- 114
Aroclor-1 016 (2Cj 241 gI 0200 250 50- 114
Aroclor- 1260 277 gI 0200 250 111 40- 127
Aroclor- 1260(2Cj 0260 gI 0200 250 104 40- 127
Surrogate Decachlorobipheny (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0238 0218 0189 0181
gI
gI
gI
gI
0200 0200 0200 0200
119 109
30- 150 30- 150 30- 150 30- 150
This laboratory report is lot valid without (II authorized sigllature 01 the cover page
Page 18 of25 Reportable Detection Limit BRL = Below Reporting Limit
Extractable Petroleum Hydrocarbons - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051102 - SW846 3510C
Blank 8051102-BLK1
Prepared 15-May-08 Analyzed 19-Mayshy
Non-polar material (SGT- HEM) BRL m91
LC8 8051102-B81
Prepared 15-May-08 Analyzed 19-Mayshy
Non-polar material (SGT- HEM) 184 m91 21 81 904
This laboratory report is not valid without an authorized signature 011 the cover page
Page 19 of25 Reportable Detection Limit BRL = Below Reporting Limit
Soluble Metals by EPA 200 Series Methods - Quality Control
Analyte(s) Result Flag Units RDL
Spike
Level
Source
Result REC
REC
Limits RPD
RPD
Limit
Batch 8051150 - EPA 200 Series
Blank 8051150-BLK1
Prepared amp Analyzed 21-May-
Iron
Zinc
Selenium
Nickel
Chromium
Copper
Arsenic
BRL
BRL
BRL
BRL
BRL
BRL
BRL
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0150
0050
0150
0050
0050
0050
0040
LCS 8051150-BS1
Prepared amp Analyzed 21-May-
Selenium
Zinc
Iron
Nickel
Chromium
Arsenic
Copper
123
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0150
0050
0150
0050
0050
0040
0050
103
105
101
100
85- 115
85- 115
85- 115
85- 115
85- 115
85-115
85- 115
licate B051150-DUP1 Source SA7B602shy
Prepared amp Analyzed 21-May-
Iron
Zinc
Selenium
Nickel
Copper
Chromium
Arsenic
17
0162
BRL
0015
0017
BRL
0450
QR8
mgl
mgl
mgl
mgl
mgl
mgl
mgi
0150
0050
0150
0050
0050
0050
0040
184
0186
BRL
0014
0023
BRL
0468
Matrix S ike 8051150-MS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Iron
Selenium
Nickel
Zinc
Copper
Chromium
Arsenic
19 QM2 mgl
mgll
mgl
mgl
mgl
mgl
mgl
0150
0150
0050
0050
0050
0050
0040
125
184
BRL
0014
0186
0023
BRL
0468
104
105
102
70- 130
70- 130
70-130
70- 130
70- 130
70-130
70- 130
Post S ike 8051150-PS1 Source SA78602shy
Prepared amp Analyzed 21-May-
Zinc
Iron
Selenium
Nickel
Copper
Arsenic
Chromium
18 QM2
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0050
0150
0150
0050
0050
0040
0050
0186
184
BRL
0014
0023
0468
BRL
104
104
101
85- 115
85- 115
85- 115
85-115
85-115
85- 115
85-115
Batch 8051152 - EPA200SW7000 Series
Blank B051152-BLK1
Prepared amp Analyzed 21-May-
Mercury BRL mgl 00020
This laboratory report is IIOt valid witllOut all authorized sigllature 011 the coverpage
Page 20 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Soluble Metals by EPA 200 Series Methods - Quality Control
Analyte(s) Result Flag Units RDL
Spike
Level
Source
Result REC
REC
Limits RPD
RPD
Limit
Batch 8051152 - EPA200SW7000 Series
LCS B051152-BS1
Prepared amp Analyzed 21-May-
Mercury 00576 m91 00020 00500 115 85- 115
licate B051152-DUP1 Source SA78602-01
Prepared amp Analyzed 21-May-
Mercury BRL m91 00020 BRL
Matrix S ike 8051152-MS1 Source SA78602shy
Prepared amp Analyzed 21-May-
Mercury 00632 OM m91 00020 00500 BRL 126 75- 125
Post S ike 8051152-PS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Mercury 00624 OC1 m91 00020 00500 BRL 125 85- 115
Batch 8051249 - 2008No digestion
Blank 8051249-BLK1
Prepared amp Analyzed 21-May-
Lead
Antimony
Cadmium
Silver
BRL
BRL
BRL
BRL
m91
m91
m91
m91
0002
0002
0002
0002
LCS B051249-BS1
Prepared amp Analyzed 21-May-
Antimony
Lead
Silver
Cadmium
143
145 OC2
m91
m91
m91
m91
0050
0050
0050
0040
103
115
107
116
85- 115
85- 115
85- 115
85- 115
licate 8051249-DUP1 Source SA7B602shy
Prepared amp Analyzed 21- May-
Lead
Antimony
Cadmium
Silver
0009
0002
00005
00002
ORB
m91
m91
m91
m91
0002
0002
0002
0002
0011
0003
00005
00003
Matrix S ike 8051249-MS1 Source SA78602shy
Prepared amp Analyzed 21- May-
Lead
Antimony
Cadmium
Silver
142
m91
m91
m91
m91
0050
0050
0040
0050
0011
0003
00005
00003
111
101
114
102
70- 130
70-130
70c130
70- 130
Post S ike 8051249-PS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Antimony
Cadmium
Silver
38
OC2
m91
m91
m91
0050
0040
0050
125
0003
00005
00003
110
121
109
85- 115
85- 115
85- 115
This laboratory report is flOt valid IVithout all authorized signature 011 the cOIer page
Reportable Detection Limit BRL Below Reporting Limit Page 21 of 25
General Chemistry Parameters - Quality Control
Spike Source REC RPD
Analyte( s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051049 - General Preparation
Blank S051 049-BLK1
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
Blank S051049-BLK2
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
Blank S051 049-BLK3
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
LCS S051049-BS1
Prepared amp Analyzed 14-May-
Total Residual Chlorine 046 mgl 020 0500 90- 110
LCS S051049-BS2
Prepared amp Analyzed 14-May-
Total Residual Chlorine 047 mgl 020 0500 90- 110
LCS S051049-BS3
Prepared amp Analyzed 14-May-
Total Residual Chlorine 054 mgl 020 0500 108 90-110
licate B051049-DUP1 Source SA7S544shy
Prepared amp Analyzed 14-May-
Total Residual Chlorine 012 mgl 020 010
licate S051049-DUP2 Source SA7S602-01
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020 BRL
Matrix S ike 8051049-MS1 Source SA78544-01
Prepared amp Analyzed 14-May-
Total Residual Chlorine 065 mgl 020 0500 010 110 80- 120
Matrix S ike 8051049-MS2 Source SA7B602shy
Prepared amp Analyzed 14-May-
Total Residual Chlorine mgl 500 125 BRL 108 80- 120
Reference 8051 049-SRM1
Prepared amp Analyzed 14-May-
Total Residual Chlorine 100 mgl 020 0967 103 85-115
Batch 8051094 - General Preparation
Blank 8051094-BLK1
Prepared amp Analyzed 14 May-
Hexavalent Chromium (soluble) BRL mgl 005
Blank 8051 094-BLK2
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) BRL mgl 005
LCS 8051094-BS1
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) 054 mgl 005 90- 110
licate 8051094-DUP1 Source SA78602-01
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) BRL mgl 125 BRL
Thi laboratory report is not valid without all authorized sigllature 011 the cover page
Page 22 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Page 25
Volatie Organic Compounds - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051244 - SW846 5030 Water MS
LCS Dup 18051244-BSD1
Prepared 16-May-08 Analyzed 17-May-
Chloromethane 18 1-91 20 273
Dibromochloromethane 174 1-91 20 53- 149
Dichlorobenzene 20 1-91 20 100 18- 190
Dichlorobenzene 18 1-91 20 59- 156
Dichlorobenzene 18 1-91 20 18- 190
Dichloroethane 18 1-91 20 59- 155
Dichloroethane 19 1-91 20 49- 155
Dichloroethene 16 1-91 20 70- 130
cis- Dichloroethene 16 1-91 20 70- 130
trans- Dichloroethene 15 1-91 20 54- 156
Dichloropropane 17 1-91 20 210
cis- Dichloropropene 164 IJgl 20 227
trans- 1 Dichloropropene 164 I-gl 20 17- 183
Etlwlbenzene 18 IJgl 20 37- 162
Hexanone (MBK) 124 QC2 IJgl 20 70- 130
Methyl tert-butyl ether 184 1J91 20 70- 130
Methyl- pentanone (MIBK) 17 IJgl 20 70- 130
Methylene chloride 16 IJgl 20 221
Styrene 16 IJgl 20 70- 130
2- Tetrachloroethane 19 IJgl 20 46- 157
Tetrachloroethene 15 IJgl 20 64- 148
Toluene 17 IJgl 20 70- 130
1- Trichloroethane 19 1-91 20 52- 162
2- Trichloroethane 16 IJgl 20 52- 150
Trichloroethene 15 IJgl 20 71- 157
Trichlorofluoromethane (Freon 11) 17 IJgl 20 17- 181
Vinyl chloride 19 IJglI 20 251
p-Xylene 37 1J91 40 70- 130
Xylene 20 IJgl 20 100 70- 130
Surrogate 4-Bromofluorobenzene 51 IJgl 50 104 70- 130
Surrogate Toluene- 4B gl 50 70- 130
Surrogate 1 0ichloroethane- 53 IJgl 50 106 70- 130 Surrogate Oibromofluoromethane 50 1J9i 50 102 70- 130
Matrix S ike B051244-MS1 Source SA7B629shy
Prepared 16-May-08 Analyzed 17-May-
Benzene 18 20 BRL 70- 130IJgl
Bromodichloromethane 19 IJgl 20 BRL 35- 155
Bromoform 18 IJgl 20 BRL 45- 169
Bromomethane 16 IJgl 20 BRL 242
Carbon tetrachloride 21 IJgl 20 BRL 106 70- 140
Chlorobenzene 18 IJgl 20 BRL 70- 130
Chloroethane 16 IJgl 20 BRL 14-230
Chloroform 18 IJgl 20 BRL 51- 138
Chloromethane 19 IJgl 20 BRL 273
Dibromochloromethane 17 IJgl 20 BRL 53- 149
1 Dichlorobenzene 22 IJgl 20 BRL 112 18- 190
1 Dichlorobenzene 22 IJgl 20 BRL 110 59-156
1 Dichlorobenzene 21 IJgl 20 BRL 109 18- 190
1- Dichloroethane 19 IJgl 20 BRL 59- 155
1 Dichloroethane 18 IJgl 20 BRL 49- 155
This laboratory report is 110t mUd without an authorized signature on the covel page
Reportble Detection Limit BRL = Below Reporting Limit Page It of25
Volatile Organic Compounds - Quality Control
p
Spike Source REC RPD
Result REC imits RPD LimitAnalyte(s) Result Flag Units RDL Level
Batch 8051244 - SW846 5030 Water MS
Matrix ike S051244-MS1 Source SA7B629shy
Prepared 16-May-08 Analyzed 17-Mayshy
17 20 BRL 70- 130 1- Dichloroethene IJgl
16 20 BRL 54- 156trans- 1 Dichloroethene IJgl
21020 BRL1 Dichloropropane 17 1J91
cis- 1 Dichloropropene 17 IJgl 20 BRL 227
17- 183trans- 1 Dichloropropene 184 1J91 20 BRL
20 20 BRL 103 37- 162Ethylbenzene IJgl
15 20 BRL 221Methylene chloride IJgl
20 BRL 46- 1572- Tetrachloroethane 19 1J91
20 BRL 64- 148Tetrachloroethene 18 1J91
BRL 70- 130Toluene 18 1J91 20
105 52-1621- Trichloroethane 211 IJgl 20 BRL
18 20 BRL 52- 1502- Trichloroethane IJgl
17 20 BRL 71- 157Trichloroethene 1J91
20 BRL 17- 181Trichloroluoromethane (Freon 11) 194 IJgl
20 BRL 103 251Vinyl chloride 20 IJgl
102 70- 130Surrogate 4-Bromofluorobenzene 50 IJgl 50 50 70- 130Surrogate Toluene- 49 1J91
56 50 112 70- 130Surrogate 1 Dichloroethane- IJgl
50 100 70- 130Surrogate Dibromofluoromethane 50 IJgl
Matrix S ike Du S051244-MSD1 Source SA7S629shy
Prepared 16-May-08 Analyzed 17-Mayshy
18 20 BRL 70- 130Benzene IJgl
18 20 BRL 35- 155Bromodichloromethane IJgl
17 20 BRL 45- 169Bromoform IJgl
20 BRL 242Bromomethane 17 IJgl
20 BRL 103 70- 140Carbon tetrachloride 20 IJgl
18 20 BRL 70- 130Chlorobenzene 1J91
14-230Chloroethane 16 IJgl 20 BRL
20 51- 138Chloroform 184 IJgl BRL
Chloromethane 19 1J91 20 BRL 273
18 20 BRL 53- 149Dibromochloromethane 1J91
20 BRL 117 18- 190Dichlorobenzene 234 IJgl
20 BRL 112 59- 156Dichlorobenzene 22 IJgl
BRL 108 18- 190Dichlorobenzene 21 1J91 20
20 59- 1551 Dichloroethane 19 IJgl BRL
18 20 BRL 49- 155Dichloroethane IJgl
16 20 BRL 70- 130Dichloroethene IJgl
20 BRL 54- 156trans- Dichloroethene 154 1J91
20 BRL 210Dichloropropane 17 IJgl
0420 BRL 227cis- Dichloropropene 17 IJgl
17- 183trans- Dichloropropene 17 1J91 20 BRL
BRL 37- 162Ethylbenzene 20 1J91 20 102
Methylene chloride 15 IJgl 20 BRL 221
20 BRL 46- 1572- Tetrachloroethane 192 IJgl
20 BRL 64- 148 04Tetrachloroethene 18 IJgl
BRL 70- 130Toluene 184 1J91 20
52- 1621- Trichloroethane 20 IJgl 20 BRL 104
17 20 BRL 52- 1502- Trichloroethane IJgl
17 20 BRL 71- 157Trichloroethene IJgl
20 BRL 17-181Trichlorofluoromethane (Freon 11) 19 IJgl
This laboratory report is IIOt valid without all authorized sigllllture 011 the cover page
Page 12 of25 Reportble Detection Limit BRL = Below Reporting Limit
Semivolatile Organic Compounds by GCMS - Quality Control
Analyte(s)
Batch 8051216 - SW846 3510C
Blank 8051216-BLK1
Prepared amp Analyzed 16-May-
Isophorone
Methylnaphthalene
Methylphenol
3 amp 4-Methylphenol
Naphthalene
Nitroaniline
Nitroaniline
Nitroaniline
Nitrobenzene
Nitrophenol
Nitrophenol
Nitrosodimethylamine
N- N itrosodi-n-pro pyla mine
N itrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Pyridine
1 24-Trichlorobenzene
24 5- Trichlorophenol
246- Trichlorophenol
Surrogate 2-Fuorobipheny Surrogate 2-Fuoropheno Surrogate Nitrobenzene-Surrogate PhenoshySurrogate Terpheny-d4 Surrogate 6- Tribromopheno
LCS B051216-BS1
Prepared amp Analyzed 16-May-
Acenaphthene
Acenaphthylene
Aniline
Anthracene
AzobenzenelDi phenyld lazine
Benzidine
Benzo (a) anthracene
Benzo (a) pyrene
Benzo (b) fluoranthene
Benzo (g i) perylene
Benzo (k) fluoranthene
Benzoic acid
Benzyl alcohol
B is(2-chloroethoxy)methane
B i s (2-ch loroethyl)eth e r
Bis(2-ch loroisopropyl) ether
B is(2-ethy Ih exyl) phtha late
Bromophenyl phenyl ether
Butyl benzyl phthalate
Carbazole
Spike Source REC RPD
Result Flag Units RDL Level Result REC Limits RPD Limit
BRL gl
BRL gl
BRL gl
BRL gl 10
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gll
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
370 gl 50 30- 130 40 gl 50 15- 110 39 gl 50 30- 130 43 gl 50 15- 110 36 gl 50 30- 130 40 gl 50 15- 110
41 gl 50 40- 140
43 gI 50 40- 140
41 gl 50 40- 140
38 gl 50 40- 140
45 gl 50 40- 140
49 gl 50 153
41 gl 50 40- 140
43 gl 50 40- 140
41 gl 50 40- 140
41 gll 50 40- 140
45 gl 50 40- 140
32 gl 50 12- 149
41 gl 50 40- 140
39 gl 50 40- 140
384 gl 50 40- 140
47 gl 50 40- 140
47 gl 50 40- 140
40 gl 50 40- 140
47 gI 50 40- 140
56 gI 50 112 200
This laboratory report is lIot valid witllOut a1l authorized sigllature 011 the coverpage
Reportble Detection Limit BRL = Below Reporting Limit Page 15 of25
Semivolatile Organic Compounds by GCMS - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051216 - SW846 3510C
LCS 8051216-BS1
Prepared amp Analyzed 16-Mayshy
50 30- 1304 -C hloro-3-methylphenol 42 IJgl
40- 140Chloroaniline 39 IJgl 50
Chloronaphthalene 37 IJgl 50 40- 140
Chlorophenol 37 IJgl 50 30- 130
50 40- 140
40- 140
Chlorophenyl phenyl ether 45 IJgl
Chrysene 43 IJgl 50
Dibenzo (a h) anthracene 43 IJgl 50 40- 140
Dibenzofuran IJgl38 50 40- 140
50 40- 1401 Dichlorobenzene 35 IJgl
40- 1401 Dichlorobenzene 264 IJgl 50
40- 1401 Dichlorobenzene 434 IJgl 50
58 50 116 40- 1403 - Dichlorobenzidine IJgl
50 30- 130
40- 140 24-Dichlorophenol 38 IJgl
Diethyl phthalate 484 IJgl 50
50 40- 140Dimethyl phthalate 464 IJgl
Dlmethylphenol 39 IJgl 50 30- 130
DI-n-butyl phthalate 44 IJgll 50 40- 140
30- 130 6-Di nitro- 2-methylphenol 38 1J91 50
30- 130Dinltrophenol 36 1J91 50
42 50 40- 14024-Dlnitrotoluene 1J91
Dlnitrotoluene 1J9141 50 40- 140
Di-n-octyl phthalate 52 IJgl 50 104 40- 140
40- 140Fluoranthene 40 IJgl 50
Fluorene 41 IJgl 50 40- 140
39 50 40- 140Hexachlorobenzene IJgl
50 40- 140Hexachlorobutadiene 40 IJgl
40- 140Hexach lorocyclopentad iene 294 IJgl 50
40 50 40- 140Hexachloroethane IJgl
42 50 40-140Indeno (1 3-cd) pyrene IJgl
50 40- 140Isophorone 40 IJgl
40- 140Methylnaphthalene 394 IJgl 50
40- 140Methylphenol 39 IJgl 50
40 10 50 40- 1403 amp 4-Methylphenol IJgl
37 50 40-140Naphthalene IJgl
50 40-140Nitroaniline 39 IJgl
Nitroaniline 51 IJgl 50 102 40- 140
48 50 40- 140Nltroaniline 1J91
50 40- 140Nitrobenzene 40 IJgl
30- 130Nitrophenol 36 IJgl 50
40 IJgl 50 30- 130Nitrophenol 40- 140Nitrosodimethylamine 32 1J91 50
50 40-140N- N itrosodi-n-propyla mine 46 IJgl
40- 140N itrosodi phenyla ml ne 44 IJgl 50
41 IJgl 50 30- 130Pentachlorophenol 40- 140Phenanthrene 38 IJgl 50
50 30- 130Phenol 38 IJgl
40- 140Pyrene 424 1J91 50
40- 140Pyridine 294 1J91 50
40- 14024- Trichlorobenzene 364 IJgl 50
This laboratory report is not mlid without an authorized signature 011 the cover page
Page 16 of25 Reportble Detection Limit BRL = Below Reporting Limit
Semivolatie Organic Compounds by GCMS - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
BMch 8051216 - SW846 3510C
LC5 8051216-851
Prepared amp Analyzed 16-Mayshy
24 5- Trichlorophenol 404 gl 50 30- 130
246- Trichlorophenol 42 gl 50 30- 130
Surrogate 2-Fluorobiphenyl 29 gl 50 30- 130
Surrogate 2-Fluorophenot 27 gl 50 15- 110
Surrogate Nitrobenzene- 30 gl 50 30- 130
Surrogate Phenol- 29 gl 50 15- 110
Surrogate Terpheny-d4 30 gl 50 30- 130
Surrogate 6- Tribromopheno 324 gl 50 15- 110
This laboratory report is lIot valid without all authorized sigllature 011 tlle cover page
Reportble Detection Limit BRL = Below Reporting Limit Page 17 of25
Semivolatie Organic Compounds by GC - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051106 - SW846 3510C
Blank S051106-BLK1
Prepared amp Analyzed 15-Mayshy
Aroclor- 1016 BRL gI 0200
Aroclor- 1016 (2C) BRL gI 0200
Aroclor- 1221 BRL gI 0200
Aroclor- 1221 (2C) BRL gI 0200
Aroclor- 1232 BRL gI 0200
Aroclor- 1232 (2Cj BRL gI 0200
Aroclor- 1242 BRL gI 0200
Aroclor-1242 (2C) BRL gI 0200
Aroclor- 1248 BRL gI 0200
Aroclor- 1248 (2C) BRL gI 0200
Aroclor- 1254 BRL gI 0200
Aroclor- 1254(2Cj BRL gI 0200
Aroclor- 1260 BRL gI 0200
Aroclor- 1260 (2C) BRL gI 0200
Aroclor- 1262 BRL gI 0200
Aroclor- 1262 (2C) BRL gI 0200
Aroclor-1268 BRL gI 0200
Aroclor- 1268 (2C) BRL gI 0200
Surrogate Decachlorobiphenyl (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0231 0224 0194 0191
gI
gI
gI
gI
0200 0200 0200 0200
116 112
30- 150 30- 150 30- 150 30- 150
LC5 8051106-B51
Prepared 15-May-08 Analyzed 16-May-08
Aroclor- 1016 265 gI 0200 250 106 50- 114
Aroclor- 1 016 (2C) 240 gI 0200 250 50- 114
Aroclor- 1260 0269 gI 0200 250 107 40- 127
Aroclor-1260 (2Cj 270 gI 0200 250 108 40- 127
Surrogate Decachlorobiphenyl (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0225 0224 0188 0183
gI
gI
gI
gI
0200 0200 0200 0200
113 112
30- 150 30- 150 30- 150 30- 150
LC5 DUD rS051106-B5D1
Prepared 15-May-08 Analyzed 16-Mayshy
Aroclor- 1016 262 gl 0200 250 105 50- 114
Aroclor-1 016 (2Cj 241 gI 0200 250 50- 114
Aroclor- 1260 277 gI 0200 250 111 40- 127
Aroclor- 1260(2Cj 0260 gI 0200 250 104 40- 127
Surrogate Decachlorobipheny (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0238 0218 0189 0181
gI
gI
gI
gI
0200 0200 0200 0200
119 109
30- 150 30- 150 30- 150 30- 150
This laboratory report is lot valid without (II authorized sigllature 01 the cover page
Page 18 of25 Reportable Detection Limit BRL = Below Reporting Limit
Extractable Petroleum Hydrocarbons - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051102 - SW846 3510C
Blank 8051102-BLK1
Prepared 15-May-08 Analyzed 19-Mayshy
Non-polar material (SGT- HEM) BRL m91
LC8 8051102-B81
Prepared 15-May-08 Analyzed 19-Mayshy
Non-polar material (SGT- HEM) 184 m91 21 81 904
This laboratory report is not valid without an authorized signature 011 the cover page
Page 19 of25 Reportable Detection Limit BRL = Below Reporting Limit
Soluble Metals by EPA 200 Series Methods - Quality Control
Analyte(s) Result Flag Units RDL
Spike
Level
Source
Result REC
REC
Limits RPD
RPD
Limit
Batch 8051150 - EPA 200 Series
Blank 8051150-BLK1
Prepared amp Analyzed 21-May-
Iron
Zinc
Selenium
Nickel
Chromium
Copper
Arsenic
BRL
BRL
BRL
BRL
BRL
BRL
BRL
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0150
0050
0150
0050
0050
0050
0040
LCS 8051150-BS1
Prepared amp Analyzed 21-May-
Selenium
Zinc
Iron
Nickel
Chromium
Arsenic
Copper
123
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0150
0050
0150
0050
0050
0040
0050
103
105
101
100
85- 115
85- 115
85- 115
85- 115
85- 115
85-115
85- 115
licate B051150-DUP1 Source SA7B602shy
Prepared amp Analyzed 21-May-
Iron
Zinc
Selenium
Nickel
Copper
Chromium
Arsenic
17
0162
BRL
0015
0017
BRL
0450
QR8
mgl
mgl
mgl
mgl
mgl
mgl
mgi
0150
0050
0150
0050
0050
0050
0040
184
0186
BRL
0014
0023
BRL
0468
Matrix S ike 8051150-MS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Iron
Selenium
Nickel
Zinc
Copper
Chromium
Arsenic
19 QM2 mgl
mgll
mgl
mgl
mgl
mgl
mgl
0150
0150
0050
0050
0050
0050
0040
125
184
BRL
0014
0186
0023
BRL
0468
104
105
102
70- 130
70- 130
70-130
70- 130
70- 130
70-130
70- 130
Post S ike 8051150-PS1 Source SA78602shy
Prepared amp Analyzed 21-May-
Zinc
Iron
Selenium
Nickel
Copper
Arsenic
Chromium
18 QM2
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0050
0150
0150
0050
0050
0040
0050
0186
184
BRL
0014
0023
0468
BRL
104
104
101
85- 115
85- 115
85- 115
85-115
85-115
85- 115
85-115
Batch 8051152 - EPA200SW7000 Series
Blank B051152-BLK1
Prepared amp Analyzed 21-May-
Mercury BRL mgl 00020
This laboratory report is IIOt valid witllOut all authorized sigllature 011 the coverpage
Page 20 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Soluble Metals by EPA 200 Series Methods - Quality Control
Analyte(s) Result Flag Units RDL
Spike
Level
Source
Result REC
REC
Limits RPD
RPD
Limit
Batch 8051152 - EPA200SW7000 Series
LCS B051152-BS1
Prepared amp Analyzed 21-May-
Mercury 00576 m91 00020 00500 115 85- 115
licate B051152-DUP1 Source SA78602-01
Prepared amp Analyzed 21-May-
Mercury BRL m91 00020 BRL
Matrix S ike 8051152-MS1 Source SA78602shy
Prepared amp Analyzed 21-May-
Mercury 00632 OM m91 00020 00500 BRL 126 75- 125
Post S ike 8051152-PS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Mercury 00624 OC1 m91 00020 00500 BRL 125 85- 115
Batch 8051249 - 2008No digestion
Blank 8051249-BLK1
Prepared amp Analyzed 21-May-
Lead
Antimony
Cadmium
Silver
BRL
BRL
BRL
BRL
m91
m91
m91
m91
0002
0002
0002
0002
LCS B051249-BS1
Prepared amp Analyzed 21-May-
Antimony
Lead
Silver
Cadmium
143
145 OC2
m91
m91
m91
m91
0050
0050
0050
0040
103
115
107
116
85- 115
85- 115
85- 115
85- 115
licate 8051249-DUP1 Source SA7B602shy
Prepared amp Analyzed 21- May-
Lead
Antimony
Cadmium
Silver
0009
0002
00005
00002
ORB
m91
m91
m91
m91
0002
0002
0002
0002
0011
0003
00005
00003
Matrix S ike 8051249-MS1 Source SA78602shy
Prepared amp Analyzed 21- May-
Lead
Antimony
Cadmium
Silver
142
m91
m91
m91
m91
0050
0050
0040
0050
0011
0003
00005
00003
111
101
114
102
70- 130
70-130
70c130
70- 130
Post S ike 8051249-PS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Antimony
Cadmium
Silver
38
OC2
m91
m91
m91
0050
0040
0050
125
0003
00005
00003
110
121
109
85- 115
85- 115
85- 115
This laboratory report is flOt valid IVithout all authorized signature 011 the cOIer page
Reportable Detection Limit BRL Below Reporting Limit Page 21 of 25
General Chemistry Parameters - Quality Control
Spike Source REC RPD
Analyte( s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051049 - General Preparation
Blank S051 049-BLK1
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
Blank S051049-BLK2
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
Blank S051 049-BLK3
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
LCS S051049-BS1
Prepared amp Analyzed 14-May-
Total Residual Chlorine 046 mgl 020 0500 90- 110
LCS S051049-BS2
Prepared amp Analyzed 14-May-
Total Residual Chlorine 047 mgl 020 0500 90- 110
LCS S051049-BS3
Prepared amp Analyzed 14-May-
Total Residual Chlorine 054 mgl 020 0500 108 90-110
licate B051049-DUP1 Source SA7S544shy
Prepared amp Analyzed 14-May-
Total Residual Chlorine 012 mgl 020 010
licate S051049-DUP2 Source SA7S602-01
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020 BRL
Matrix S ike 8051049-MS1 Source SA78544-01
Prepared amp Analyzed 14-May-
Total Residual Chlorine 065 mgl 020 0500 010 110 80- 120
Matrix S ike 8051049-MS2 Source SA7B602shy
Prepared amp Analyzed 14-May-
Total Residual Chlorine mgl 500 125 BRL 108 80- 120
Reference 8051 049-SRM1
Prepared amp Analyzed 14-May-
Total Residual Chlorine 100 mgl 020 0967 103 85-115
Batch 8051094 - General Preparation
Blank 8051094-BLK1
Prepared amp Analyzed 14 May-
Hexavalent Chromium (soluble) BRL mgl 005
Blank 8051 094-BLK2
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) BRL mgl 005
LCS 8051094-BS1
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) 054 mgl 005 90- 110
licate 8051094-DUP1 Source SA78602-01
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) BRL mgl 125 BRL
Thi laboratory report is not valid without all authorized sigllature 011 the cover page
Page 22 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Page 26
Volatile Organic Compounds - Quality Control
p
Spike Source REC RPD
Result REC imits RPD LimitAnalyte(s) Result Flag Units RDL Level
Batch 8051244 - SW846 5030 Water MS
Matrix ike S051244-MS1 Source SA7B629shy
Prepared 16-May-08 Analyzed 17-Mayshy
17 20 BRL 70- 130 1- Dichloroethene IJgl
16 20 BRL 54- 156trans- 1 Dichloroethene IJgl
21020 BRL1 Dichloropropane 17 1J91
cis- 1 Dichloropropene 17 IJgl 20 BRL 227
17- 183trans- 1 Dichloropropene 184 1J91 20 BRL
20 20 BRL 103 37- 162Ethylbenzene IJgl
15 20 BRL 221Methylene chloride IJgl
20 BRL 46- 1572- Tetrachloroethane 19 1J91
20 BRL 64- 148Tetrachloroethene 18 1J91
BRL 70- 130Toluene 18 1J91 20
105 52-1621- Trichloroethane 211 IJgl 20 BRL
18 20 BRL 52- 1502- Trichloroethane IJgl
17 20 BRL 71- 157Trichloroethene 1J91
20 BRL 17- 181Trichloroluoromethane (Freon 11) 194 IJgl
20 BRL 103 251Vinyl chloride 20 IJgl
102 70- 130Surrogate 4-Bromofluorobenzene 50 IJgl 50 50 70- 130Surrogate Toluene- 49 1J91
56 50 112 70- 130Surrogate 1 Dichloroethane- IJgl
50 100 70- 130Surrogate Dibromofluoromethane 50 IJgl
Matrix S ike Du S051244-MSD1 Source SA7S629shy
Prepared 16-May-08 Analyzed 17-Mayshy
18 20 BRL 70- 130Benzene IJgl
18 20 BRL 35- 155Bromodichloromethane IJgl
17 20 BRL 45- 169Bromoform IJgl
20 BRL 242Bromomethane 17 IJgl
20 BRL 103 70- 140Carbon tetrachloride 20 IJgl
18 20 BRL 70- 130Chlorobenzene 1J91
14-230Chloroethane 16 IJgl 20 BRL
20 51- 138Chloroform 184 IJgl BRL
Chloromethane 19 1J91 20 BRL 273
18 20 BRL 53- 149Dibromochloromethane 1J91
20 BRL 117 18- 190Dichlorobenzene 234 IJgl
20 BRL 112 59- 156Dichlorobenzene 22 IJgl
BRL 108 18- 190Dichlorobenzene 21 1J91 20
20 59- 1551 Dichloroethane 19 IJgl BRL
18 20 BRL 49- 155Dichloroethane IJgl
16 20 BRL 70- 130Dichloroethene IJgl
20 BRL 54- 156trans- Dichloroethene 154 1J91
20 BRL 210Dichloropropane 17 IJgl
0420 BRL 227cis- Dichloropropene 17 IJgl
17- 183trans- Dichloropropene 17 1J91 20 BRL
BRL 37- 162Ethylbenzene 20 1J91 20 102
Methylene chloride 15 IJgl 20 BRL 221
20 BRL 46- 1572- Tetrachloroethane 192 IJgl
20 BRL 64- 148 04Tetrachloroethene 18 IJgl
BRL 70- 130Toluene 184 1J91 20
52- 1621- Trichloroethane 20 IJgl 20 BRL 104
17 20 BRL 52- 1502- Trichloroethane IJgl
17 20 BRL 71- 157Trichloroethene IJgl
20 BRL 17-181Trichlorofluoromethane (Freon 11) 19 IJgl
This laboratory report is IIOt valid without all authorized sigllllture 011 the cover page
Page 12 of25 Reportble Detection Limit BRL = Below Reporting Limit
Semivolatile Organic Compounds by GCMS - Quality Control
Analyte(s)
Batch 8051216 - SW846 3510C
Blank 8051216-BLK1
Prepared amp Analyzed 16-May-
Isophorone
Methylnaphthalene
Methylphenol
3 amp 4-Methylphenol
Naphthalene
Nitroaniline
Nitroaniline
Nitroaniline
Nitrobenzene
Nitrophenol
Nitrophenol
Nitrosodimethylamine
N- N itrosodi-n-pro pyla mine
N itrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Pyridine
1 24-Trichlorobenzene
24 5- Trichlorophenol
246- Trichlorophenol
Surrogate 2-Fuorobipheny Surrogate 2-Fuoropheno Surrogate Nitrobenzene-Surrogate PhenoshySurrogate Terpheny-d4 Surrogate 6- Tribromopheno
LCS B051216-BS1
Prepared amp Analyzed 16-May-
Acenaphthene
Acenaphthylene
Aniline
Anthracene
AzobenzenelDi phenyld lazine
Benzidine
Benzo (a) anthracene
Benzo (a) pyrene
Benzo (b) fluoranthene
Benzo (g i) perylene
Benzo (k) fluoranthene
Benzoic acid
Benzyl alcohol
B is(2-chloroethoxy)methane
B i s (2-ch loroethyl)eth e r
Bis(2-ch loroisopropyl) ether
B is(2-ethy Ih exyl) phtha late
Bromophenyl phenyl ether
Butyl benzyl phthalate
Carbazole
Spike Source REC RPD
Result Flag Units RDL Level Result REC Limits RPD Limit
BRL gl
BRL gl
BRL gl
BRL gl 10
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gll
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
370 gl 50 30- 130 40 gl 50 15- 110 39 gl 50 30- 130 43 gl 50 15- 110 36 gl 50 30- 130 40 gl 50 15- 110
41 gl 50 40- 140
43 gI 50 40- 140
41 gl 50 40- 140
38 gl 50 40- 140
45 gl 50 40- 140
49 gl 50 153
41 gl 50 40- 140
43 gl 50 40- 140
41 gl 50 40- 140
41 gll 50 40- 140
45 gl 50 40- 140
32 gl 50 12- 149
41 gl 50 40- 140
39 gl 50 40- 140
384 gl 50 40- 140
47 gl 50 40- 140
47 gl 50 40- 140
40 gl 50 40- 140
47 gI 50 40- 140
56 gI 50 112 200
This laboratory report is lIot valid witllOut a1l authorized sigllature 011 the coverpage
Reportble Detection Limit BRL = Below Reporting Limit Page 15 of25
Semivolatile Organic Compounds by GCMS - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051216 - SW846 3510C
LCS 8051216-BS1
Prepared amp Analyzed 16-Mayshy
50 30- 1304 -C hloro-3-methylphenol 42 IJgl
40- 140Chloroaniline 39 IJgl 50
Chloronaphthalene 37 IJgl 50 40- 140
Chlorophenol 37 IJgl 50 30- 130
50 40- 140
40- 140
Chlorophenyl phenyl ether 45 IJgl
Chrysene 43 IJgl 50
Dibenzo (a h) anthracene 43 IJgl 50 40- 140
Dibenzofuran IJgl38 50 40- 140
50 40- 1401 Dichlorobenzene 35 IJgl
40- 1401 Dichlorobenzene 264 IJgl 50
40- 1401 Dichlorobenzene 434 IJgl 50
58 50 116 40- 1403 - Dichlorobenzidine IJgl
50 30- 130
40- 140 24-Dichlorophenol 38 IJgl
Diethyl phthalate 484 IJgl 50
50 40- 140Dimethyl phthalate 464 IJgl
Dlmethylphenol 39 IJgl 50 30- 130
DI-n-butyl phthalate 44 IJgll 50 40- 140
30- 130 6-Di nitro- 2-methylphenol 38 1J91 50
30- 130Dinltrophenol 36 1J91 50
42 50 40- 14024-Dlnitrotoluene 1J91
Dlnitrotoluene 1J9141 50 40- 140
Di-n-octyl phthalate 52 IJgl 50 104 40- 140
40- 140Fluoranthene 40 IJgl 50
Fluorene 41 IJgl 50 40- 140
39 50 40- 140Hexachlorobenzene IJgl
50 40- 140Hexachlorobutadiene 40 IJgl
40- 140Hexach lorocyclopentad iene 294 IJgl 50
40 50 40- 140Hexachloroethane IJgl
42 50 40-140Indeno (1 3-cd) pyrene IJgl
50 40- 140Isophorone 40 IJgl
40- 140Methylnaphthalene 394 IJgl 50
40- 140Methylphenol 39 IJgl 50
40 10 50 40- 1403 amp 4-Methylphenol IJgl
37 50 40-140Naphthalene IJgl
50 40-140Nitroaniline 39 IJgl
Nitroaniline 51 IJgl 50 102 40- 140
48 50 40- 140Nltroaniline 1J91
50 40- 140Nitrobenzene 40 IJgl
30- 130Nitrophenol 36 IJgl 50
40 IJgl 50 30- 130Nitrophenol 40- 140Nitrosodimethylamine 32 1J91 50
50 40-140N- N itrosodi-n-propyla mine 46 IJgl
40- 140N itrosodi phenyla ml ne 44 IJgl 50
41 IJgl 50 30- 130Pentachlorophenol 40- 140Phenanthrene 38 IJgl 50
50 30- 130Phenol 38 IJgl
40- 140Pyrene 424 1J91 50
40- 140Pyridine 294 1J91 50
40- 14024- Trichlorobenzene 364 IJgl 50
This laboratory report is not mlid without an authorized signature 011 the cover page
Page 16 of25 Reportble Detection Limit BRL = Below Reporting Limit
Semivolatie Organic Compounds by GCMS - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
BMch 8051216 - SW846 3510C
LC5 8051216-851
Prepared amp Analyzed 16-Mayshy
24 5- Trichlorophenol 404 gl 50 30- 130
246- Trichlorophenol 42 gl 50 30- 130
Surrogate 2-Fluorobiphenyl 29 gl 50 30- 130
Surrogate 2-Fluorophenot 27 gl 50 15- 110
Surrogate Nitrobenzene- 30 gl 50 30- 130
Surrogate Phenol- 29 gl 50 15- 110
Surrogate Terpheny-d4 30 gl 50 30- 130
Surrogate 6- Tribromopheno 324 gl 50 15- 110
This laboratory report is lIot valid without all authorized sigllature 011 tlle cover page
Reportble Detection Limit BRL = Below Reporting Limit Page 17 of25
Semivolatie Organic Compounds by GC - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051106 - SW846 3510C
Blank S051106-BLK1
Prepared amp Analyzed 15-Mayshy
Aroclor- 1016 BRL gI 0200
Aroclor- 1016 (2C) BRL gI 0200
Aroclor- 1221 BRL gI 0200
Aroclor- 1221 (2C) BRL gI 0200
Aroclor- 1232 BRL gI 0200
Aroclor- 1232 (2Cj BRL gI 0200
Aroclor- 1242 BRL gI 0200
Aroclor-1242 (2C) BRL gI 0200
Aroclor- 1248 BRL gI 0200
Aroclor- 1248 (2C) BRL gI 0200
Aroclor- 1254 BRL gI 0200
Aroclor- 1254(2Cj BRL gI 0200
Aroclor- 1260 BRL gI 0200
Aroclor- 1260 (2C) BRL gI 0200
Aroclor- 1262 BRL gI 0200
Aroclor- 1262 (2C) BRL gI 0200
Aroclor-1268 BRL gI 0200
Aroclor- 1268 (2C) BRL gI 0200
Surrogate Decachlorobiphenyl (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0231 0224 0194 0191
gI
gI
gI
gI
0200 0200 0200 0200
116 112
30- 150 30- 150 30- 150 30- 150
LC5 8051106-B51
Prepared 15-May-08 Analyzed 16-May-08
Aroclor- 1016 265 gI 0200 250 106 50- 114
Aroclor- 1 016 (2C) 240 gI 0200 250 50- 114
Aroclor- 1260 0269 gI 0200 250 107 40- 127
Aroclor-1260 (2Cj 270 gI 0200 250 108 40- 127
Surrogate Decachlorobiphenyl (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0225 0224 0188 0183
gI
gI
gI
gI
0200 0200 0200 0200
113 112
30- 150 30- 150 30- 150 30- 150
LC5 DUD rS051106-B5D1
Prepared 15-May-08 Analyzed 16-Mayshy
Aroclor- 1016 262 gl 0200 250 105 50- 114
Aroclor-1 016 (2Cj 241 gI 0200 250 50- 114
Aroclor- 1260 277 gI 0200 250 111 40- 127
Aroclor- 1260(2Cj 0260 gI 0200 250 104 40- 127
Surrogate Decachlorobipheny (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0238 0218 0189 0181
gI
gI
gI
gI
0200 0200 0200 0200
119 109
30- 150 30- 150 30- 150 30- 150
This laboratory report is lot valid without (II authorized sigllature 01 the cover page
Page 18 of25 Reportable Detection Limit BRL = Below Reporting Limit
Extractable Petroleum Hydrocarbons - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051102 - SW846 3510C
Blank 8051102-BLK1
Prepared 15-May-08 Analyzed 19-Mayshy
Non-polar material (SGT- HEM) BRL m91
LC8 8051102-B81
Prepared 15-May-08 Analyzed 19-Mayshy
Non-polar material (SGT- HEM) 184 m91 21 81 904
This laboratory report is not valid without an authorized signature 011 the cover page
Page 19 of25 Reportable Detection Limit BRL = Below Reporting Limit
Soluble Metals by EPA 200 Series Methods - Quality Control
Analyte(s) Result Flag Units RDL
Spike
Level
Source
Result REC
REC
Limits RPD
RPD
Limit
Batch 8051150 - EPA 200 Series
Blank 8051150-BLK1
Prepared amp Analyzed 21-May-
Iron
Zinc
Selenium
Nickel
Chromium
Copper
Arsenic
BRL
BRL
BRL
BRL
BRL
BRL
BRL
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0150
0050
0150
0050
0050
0050
0040
LCS 8051150-BS1
Prepared amp Analyzed 21-May-
Selenium
Zinc
Iron
Nickel
Chromium
Arsenic
Copper
123
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0150
0050
0150
0050
0050
0040
0050
103
105
101
100
85- 115
85- 115
85- 115
85- 115
85- 115
85-115
85- 115
licate B051150-DUP1 Source SA7B602shy
Prepared amp Analyzed 21-May-
Iron
Zinc
Selenium
Nickel
Copper
Chromium
Arsenic
17
0162
BRL
0015
0017
BRL
0450
QR8
mgl
mgl
mgl
mgl
mgl
mgl
mgi
0150
0050
0150
0050
0050
0050
0040
184
0186
BRL
0014
0023
BRL
0468
Matrix S ike 8051150-MS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Iron
Selenium
Nickel
Zinc
Copper
Chromium
Arsenic
19 QM2 mgl
mgll
mgl
mgl
mgl
mgl
mgl
0150
0150
0050
0050
0050
0050
0040
125
184
BRL
0014
0186
0023
BRL
0468
104
105
102
70- 130
70- 130
70-130
70- 130
70- 130
70-130
70- 130
Post S ike 8051150-PS1 Source SA78602shy
Prepared amp Analyzed 21-May-
Zinc
Iron
Selenium
Nickel
Copper
Arsenic
Chromium
18 QM2
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0050
0150
0150
0050
0050
0040
0050
0186
184
BRL
0014
0023
0468
BRL
104
104
101
85- 115
85- 115
85- 115
85-115
85-115
85- 115
85-115
Batch 8051152 - EPA200SW7000 Series
Blank B051152-BLK1
Prepared amp Analyzed 21-May-
Mercury BRL mgl 00020
This laboratory report is IIOt valid witllOut all authorized sigllature 011 the coverpage
Page 20 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Soluble Metals by EPA 200 Series Methods - Quality Control
Analyte(s) Result Flag Units RDL
Spike
Level
Source
Result REC
REC
Limits RPD
RPD
Limit
Batch 8051152 - EPA200SW7000 Series
LCS B051152-BS1
Prepared amp Analyzed 21-May-
Mercury 00576 m91 00020 00500 115 85- 115
licate B051152-DUP1 Source SA78602-01
Prepared amp Analyzed 21-May-
Mercury BRL m91 00020 BRL
Matrix S ike 8051152-MS1 Source SA78602shy
Prepared amp Analyzed 21-May-
Mercury 00632 OM m91 00020 00500 BRL 126 75- 125
Post S ike 8051152-PS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Mercury 00624 OC1 m91 00020 00500 BRL 125 85- 115
Batch 8051249 - 2008No digestion
Blank 8051249-BLK1
Prepared amp Analyzed 21-May-
Lead
Antimony
Cadmium
Silver
BRL
BRL
BRL
BRL
m91
m91
m91
m91
0002
0002
0002
0002
LCS B051249-BS1
Prepared amp Analyzed 21-May-
Antimony
Lead
Silver
Cadmium
143
145 OC2
m91
m91
m91
m91
0050
0050
0050
0040
103
115
107
116
85- 115
85- 115
85- 115
85- 115
licate 8051249-DUP1 Source SA7B602shy
Prepared amp Analyzed 21- May-
Lead
Antimony
Cadmium
Silver
0009
0002
00005
00002
ORB
m91
m91
m91
m91
0002
0002
0002
0002
0011
0003
00005
00003
Matrix S ike 8051249-MS1 Source SA78602shy
Prepared amp Analyzed 21- May-
Lead
Antimony
Cadmium
Silver
142
m91
m91
m91
m91
0050
0050
0040
0050
0011
0003
00005
00003
111
101
114
102
70- 130
70-130
70c130
70- 130
Post S ike 8051249-PS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Antimony
Cadmium
Silver
38
OC2
m91
m91
m91
0050
0040
0050
125
0003
00005
00003
110
121
109
85- 115
85- 115
85- 115
This laboratory report is flOt valid IVithout all authorized signature 011 the cOIer page
Reportable Detection Limit BRL Below Reporting Limit Page 21 of 25
General Chemistry Parameters - Quality Control
Spike Source REC RPD
Analyte( s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051049 - General Preparation
Blank S051 049-BLK1
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
Blank S051049-BLK2
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
Blank S051 049-BLK3
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
LCS S051049-BS1
Prepared amp Analyzed 14-May-
Total Residual Chlorine 046 mgl 020 0500 90- 110
LCS S051049-BS2
Prepared amp Analyzed 14-May-
Total Residual Chlorine 047 mgl 020 0500 90- 110
LCS S051049-BS3
Prepared amp Analyzed 14-May-
Total Residual Chlorine 054 mgl 020 0500 108 90-110
licate B051049-DUP1 Source SA7S544shy
Prepared amp Analyzed 14-May-
Total Residual Chlorine 012 mgl 020 010
licate S051049-DUP2 Source SA7S602-01
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020 BRL
Matrix S ike 8051049-MS1 Source SA78544-01
Prepared amp Analyzed 14-May-
Total Residual Chlorine 065 mgl 020 0500 010 110 80- 120
Matrix S ike 8051049-MS2 Source SA7B602shy
Prepared amp Analyzed 14-May-
Total Residual Chlorine mgl 500 125 BRL 108 80- 120
Reference 8051 049-SRM1
Prepared amp Analyzed 14-May-
Total Residual Chlorine 100 mgl 020 0967 103 85-115
Batch 8051094 - General Preparation
Blank 8051094-BLK1
Prepared amp Analyzed 14 May-
Hexavalent Chromium (soluble) BRL mgl 005
Blank 8051 094-BLK2
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) BRL mgl 005
LCS 8051094-BS1
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) 054 mgl 005 90- 110
licate 8051094-DUP1 Source SA78602-01
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) BRL mgl 125 BRL
Thi laboratory report is not valid without all authorized sigllature 011 the cover page
Page 22 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Page 27
Semivolatile Organic Compounds by GCMS - Quality Control
Analyte(s)
Batch 8051216 - SW846 3510C
Blank 8051216-BLK1
Prepared amp Analyzed 16-May-
Isophorone
Methylnaphthalene
Methylphenol
3 amp 4-Methylphenol
Naphthalene
Nitroaniline
Nitroaniline
Nitroaniline
Nitrobenzene
Nitrophenol
Nitrophenol
Nitrosodimethylamine
N- N itrosodi-n-pro pyla mine
N itrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Pyridine
1 24-Trichlorobenzene
24 5- Trichlorophenol
246- Trichlorophenol
Surrogate 2-Fuorobipheny Surrogate 2-Fuoropheno Surrogate Nitrobenzene-Surrogate PhenoshySurrogate Terpheny-d4 Surrogate 6- Tribromopheno
LCS B051216-BS1
Prepared amp Analyzed 16-May-
Acenaphthene
Acenaphthylene
Aniline
Anthracene
AzobenzenelDi phenyld lazine
Benzidine
Benzo (a) anthracene
Benzo (a) pyrene
Benzo (b) fluoranthene
Benzo (g i) perylene
Benzo (k) fluoranthene
Benzoic acid
Benzyl alcohol
B is(2-chloroethoxy)methane
B i s (2-ch loroethyl)eth e r
Bis(2-ch loroisopropyl) ether
B is(2-ethy Ih exyl) phtha late
Bromophenyl phenyl ether
Butyl benzyl phthalate
Carbazole
Spike Source REC RPD
Result Flag Units RDL Level Result REC Limits RPD Limit
BRL gl
BRL gl
BRL gl
BRL gl 10
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
BRL gll
BRL gl
BRL gl
BRL gl
BRL gl
BRL gl
370 gl 50 30- 130 40 gl 50 15- 110 39 gl 50 30- 130 43 gl 50 15- 110 36 gl 50 30- 130 40 gl 50 15- 110
41 gl 50 40- 140
43 gI 50 40- 140
41 gl 50 40- 140
38 gl 50 40- 140
45 gl 50 40- 140
49 gl 50 153
41 gl 50 40- 140
43 gl 50 40- 140
41 gl 50 40- 140
41 gll 50 40- 140
45 gl 50 40- 140
32 gl 50 12- 149
41 gl 50 40- 140
39 gl 50 40- 140
384 gl 50 40- 140
47 gl 50 40- 140
47 gl 50 40- 140
40 gl 50 40- 140
47 gI 50 40- 140
56 gI 50 112 200
This laboratory report is lIot valid witllOut a1l authorized sigllature 011 the coverpage
Reportble Detection Limit BRL = Below Reporting Limit Page 15 of25
Semivolatile Organic Compounds by GCMS - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051216 - SW846 3510C
LCS 8051216-BS1
Prepared amp Analyzed 16-Mayshy
50 30- 1304 -C hloro-3-methylphenol 42 IJgl
40- 140Chloroaniline 39 IJgl 50
Chloronaphthalene 37 IJgl 50 40- 140
Chlorophenol 37 IJgl 50 30- 130
50 40- 140
40- 140
Chlorophenyl phenyl ether 45 IJgl
Chrysene 43 IJgl 50
Dibenzo (a h) anthracene 43 IJgl 50 40- 140
Dibenzofuran IJgl38 50 40- 140
50 40- 1401 Dichlorobenzene 35 IJgl
40- 1401 Dichlorobenzene 264 IJgl 50
40- 1401 Dichlorobenzene 434 IJgl 50
58 50 116 40- 1403 - Dichlorobenzidine IJgl
50 30- 130
40- 140 24-Dichlorophenol 38 IJgl
Diethyl phthalate 484 IJgl 50
50 40- 140Dimethyl phthalate 464 IJgl
Dlmethylphenol 39 IJgl 50 30- 130
DI-n-butyl phthalate 44 IJgll 50 40- 140
30- 130 6-Di nitro- 2-methylphenol 38 1J91 50
30- 130Dinltrophenol 36 1J91 50
42 50 40- 14024-Dlnitrotoluene 1J91
Dlnitrotoluene 1J9141 50 40- 140
Di-n-octyl phthalate 52 IJgl 50 104 40- 140
40- 140Fluoranthene 40 IJgl 50
Fluorene 41 IJgl 50 40- 140
39 50 40- 140Hexachlorobenzene IJgl
50 40- 140Hexachlorobutadiene 40 IJgl
40- 140Hexach lorocyclopentad iene 294 IJgl 50
40 50 40- 140Hexachloroethane IJgl
42 50 40-140Indeno (1 3-cd) pyrene IJgl
50 40- 140Isophorone 40 IJgl
40- 140Methylnaphthalene 394 IJgl 50
40- 140Methylphenol 39 IJgl 50
40 10 50 40- 1403 amp 4-Methylphenol IJgl
37 50 40-140Naphthalene IJgl
50 40-140Nitroaniline 39 IJgl
Nitroaniline 51 IJgl 50 102 40- 140
48 50 40- 140Nltroaniline 1J91
50 40- 140Nitrobenzene 40 IJgl
30- 130Nitrophenol 36 IJgl 50
40 IJgl 50 30- 130Nitrophenol 40- 140Nitrosodimethylamine 32 1J91 50
50 40-140N- N itrosodi-n-propyla mine 46 IJgl
40- 140N itrosodi phenyla ml ne 44 IJgl 50
41 IJgl 50 30- 130Pentachlorophenol 40- 140Phenanthrene 38 IJgl 50
50 30- 130Phenol 38 IJgl
40- 140Pyrene 424 1J91 50
40- 140Pyridine 294 1J91 50
40- 14024- Trichlorobenzene 364 IJgl 50
This laboratory report is not mlid without an authorized signature 011 the cover page
Page 16 of25 Reportble Detection Limit BRL = Below Reporting Limit
Semivolatie Organic Compounds by GCMS - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
BMch 8051216 - SW846 3510C
LC5 8051216-851
Prepared amp Analyzed 16-Mayshy
24 5- Trichlorophenol 404 gl 50 30- 130
246- Trichlorophenol 42 gl 50 30- 130
Surrogate 2-Fluorobiphenyl 29 gl 50 30- 130
Surrogate 2-Fluorophenot 27 gl 50 15- 110
Surrogate Nitrobenzene- 30 gl 50 30- 130
Surrogate Phenol- 29 gl 50 15- 110
Surrogate Terpheny-d4 30 gl 50 30- 130
Surrogate 6- Tribromopheno 324 gl 50 15- 110
This laboratory report is lIot valid without all authorized sigllature 011 tlle cover page
Reportble Detection Limit BRL = Below Reporting Limit Page 17 of25
Semivolatie Organic Compounds by GC - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051106 - SW846 3510C
Blank S051106-BLK1
Prepared amp Analyzed 15-Mayshy
Aroclor- 1016 BRL gI 0200
Aroclor- 1016 (2C) BRL gI 0200
Aroclor- 1221 BRL gI 0200
Aroclor- 1221 (2C) BRL gI 0200
Aroclor- 1232 BRL gI 0200
Aroclor- 1232 (2Cj BRL gI 0200
Aroclor- 1242 BRL gI 0200
Aroclor-1242 (2C) BRL gI 0200
Aroclor- 1248 BRL gI 0200
Aroclor- 1248 (2C) BRL gI 0200
Aroclor- 1254 BRL gI 0200
Aroclor- 1254(2Cj BRL gI 0200
Aroclor- 1260 BRL gI 0200
Aroclor- 1260 (2C) BRL gI 0200
Aroclor- 1262 BRL gI 0200
Aroclor- 1262 (2C) BRL gI 0200
Aroclor-1268 BRL gI 0200
Aroclor- 1268 (2C) BRL gI 0200
Surrogate Decachlorobiphenyl (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0231 0224 0194 0191
gI
gI
gI
gI
0200 0200 0200 0200
116 112
30- 150 30- 150 30- 150 30- 150
LC5 8051106-B51
Prepared 15-May-08 Analyzed 16-May-08
Aroclor- 1016 265 gI 0200 250 106 50- 114
Aroclor- 1 016 (2C) 240 gI 0200 250 50- 114
Aroclor- 1260 0269 gI 0200 250 107 40- 127
Aroclor-1260 (2Cj 270 gI 0200 250 108 40- 127
Surrogate Decachlorobiphenyl (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0225 0224 0188 0183
gI
gI
gI
gI
0200 0200 0200 0200
113 112
30- 150 30- 150 30- 150 30- 150
LC5 DUD rS051106-B5D1
Prepared 15-May-08 Analyzed 16-Mayshy
Aroclor- 1016 262 gl 0200 250 105 50- 114
Aroclor-1 016 (2Cj 241 gI 0200 250 50- 114
Aroclor- 1260 277 gI 0200 250 111 40- 127
Aroclor- 1260(2Cj 0260 gI 0200 250 104 40- 127
Surrogate Decachlorobipheny (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0238 0218 0189 0181
gI
gI
gI
gI
0200 0200 0200 0200
119 109
30- 150 30- 150 30- 150 30- 150
This laboratory report is lot valid without (II authorized sigllature 01 the cover page
Page 18 of25 Reportable Detection Limit BRL = Below Reporting Limit
Extractable Petroleum Hydrocarbons - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051102 - SW846 3510C
Blank 8051102-BLK1
Prepared 15-May-08 Analyzed 19-Mayshy
Non-polar material (SGT- HEM) BRL m91
LC8 8051102-B81
Prepared 15-May-08 Analyzed 19-Mayshy
Non-polar material (SGT- HEM) 184 m91 21 81 904
This laboratory report is not valid without an authorized signature 011 the cover page
Page 19 of25 Reportable Detection Limit BRL = Below Reporting Limit
Soluble Metals by EPA 200 Series Methods - Quality Control
Analyte(s) Result Flag Units RDL
Spike
Level
Source
Result REC
REC
Limits RPD
RPD
Limit
Batch 8051150 - EPA 200 Series
Blank 8051150-BLK1
Prepared amp Analyzed 21-May-
Iron
Zinc
Selenium
Nickel
Chromium
Copper
Arsenic
BRL
BRL
BRL
BRL
BRL
BRL
BRL
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0150
0050
0150
0050
0050
0050
0040
LCS 8051150-BS1
Prepared amp Analyzed 21-May-
Selenium
Zinc
Iron
Nickel
Chromium
Arsenic
Copper
123
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0150
0050
0150
0050
0050
0040
0050
103
105
101
100
85- 115
85- 115
85- 115
85- 115
85- 115
85-115
85- 115
licate B051150-DUP1 Source SA7B602shy
Prepared amp Analyzed 21-May-
Iron
Zinc
Selenium
Nickel
Copper
Chromium
Arsenic
17
0162
BRL
0015
0017
BRL
0450
QR8
mgl
mgl
mgl
mgl
mgl
mgl
mgi
0150
0050
0150
0050
0050
0050
0040
184
0186
BRL
0014
0023
BRL
0468
Matrix S ike 8051150-MS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Iron
Selenium
Nickel
Zinc
Copper
Chromium
Arsenic
19 QM2 mgl
mgll
mgl
mgl
mgl
mgl
mgl
0150
0150
0050
0050
0050
0050
0040
125
184
BRL
0014
0186
0023
BRL
0468
104
105
102
70- 130
70- 130
70-130
70- 130
70- 130
70-130
70- 130
Post S ike 8051150-PS1 Source SA78602shy
Prepared amp Analyzed 21-May-
Zinc
Iron
Selenium
Nickel
Copper
Arsenic
Chromium
18 QM2
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0050
0150
0150
0050
0050
0040
0050
0186
184
BRL
0014
0023
0468
BRL
104
104
101
85- 115
85- 115
85- 115
85-115
85-115
85- 115
85-115
Batch 8051152 - EPA200SW7000 Series
Blank B051152-BLK1
Prepared amp Analyzed 21-May-
Mercury BRL mgl 00020
This laboratory report is IIOt valid witllOut all authorized sigllature 011 the coverpage
Page 20 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Soluble Metals by EPA 200 Series Methods - Quality Control
Analyte(s) Result Flag Units RDL
Spike
Level
Source
Result REC
REC
Limits RPD
RPD
Limit
Batch 8051152 - EPA200SW7000 Series
LCS B051152-BS1
Prepared amp Analyzed 21-May-
Mercury 00576 m91 00020 00500 115 85- 115
licate B051152-DUP1 Source SA78602-01
Prepared amp Analyzed 21-May-
Mercury BRL m91 00020 BRL
Matrix S ike 8051152-MS1 Source SA78602shy
Prepared amp Analyzed 21-May-
Mercury 00632 OM m91 00020 00500 BRL 126 75- 125
Post S ike 8051152-PS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Mercury 00624 OC1 m91 00020 00500 BRL 125 85- 115
Batch 8051249 - 2008No digestion
Blank 8051249-BLK1
Prepared amp Analyzed 21-May-
Lead
Antimony
Cadmium
Silver
BRL
BRL
BRL
BRL
m91
m91
m91
m91
0002
0002
0002
0002
LCS B051249-BS1
Prepared amp Analyzed 21-May-
Antimony
Lead
Silver
Cadmium
143
145 OC2
m91
m91
m91
m91
0050
0050
0050
0040
103
115
107
116
85- 115
85- 115
85- 115
85- 115
licate 8051249-DUP1 Source SA7B602shy
Prepared amp Analyzed 21- May-
Lead
Antimony
Cadmium
Silver
0009
0002
00005
00002
ORB
m91
m91
m91
m91
0002
0002
0002
0002
0011
0003
00005
00003
Matrix S ike 8051249-MS1 Source SA78602shy
Prepared amp Analyzed 21- May-
Lead
Antimony
Cadmium
Silver
142
m91
m91
m91
m91
0050
0050
0040
0050
0011
0003
00005
00003
111
101
114
102
70- 130
70-130
70c130
70- 130
Post S ike 8051249-PS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Antimony
Cadmium
Silver
38
OC2
m91
m91
m91
0050
0040
0050
125
0003
00005
00003
110
121
109
85- 115
85- 115
85- 115
This laboratory report is flOt valid IVithout all authorized signature 011 the cOIer page
Reportable Detection Limit BRL Below Reporting Limit Page 21 of 25
General Chemistry Parameters - Quality Control
Spike Source REC RPD
Analyte( s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051049 - General Preparation
Blank S051 049-BLK1
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
Blank S051049-BLK2
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
Blank S051 049-BLK3
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
LCS S051049-BS1
Prepared amp Analyzed 14-May-
Total Residual Chlorine 046 mgl 020 0500 90- 110
LCS S051049-BS2
Prepared amp Analyzed 14-May-
Total Residual Chlorine 047 mgl 020 0500 90- 110
LCS S051049-BS3
Prepared amp Analyzed 14-May-
Total Residual Chlorine 054 mgl 020 0500 108 90-110
licate B051049-DUP1 Source SA7S544shy
Prepared amp Analyzed 14-May-
Total Residual Chlorine 012 mgl 020 010
licate S051049-DUP2 Source SA7S602-01
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020 BRL
Matrix S ike 8051049-MS1 Source SA78544-01
Prepared amp Analyzed 14-May-
Total Residual Chlorine 065 mgl 020 0500 010 110 80- 120
Matrix S ike 8051049-MS2 Source SA7B602shy
Prepared amp Analyzed 14-May-
Total Residual Chlorine mgl 500 125 BRL 108 80- 120
Reference 8051 049-SRM1
Prepared amp Analyzed 14-May-
Total Residual Chlorine 100 mgl 020 0967 103 85-115
Batch 8051094 - General Preparation
Blank 8051094-BLK1
Prepared amp Analyzed 14 May-
Hexavalent Chromium (soluble) BRL mgl 005
Blank 8051 094-BLK2
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) BRL mgl 005
LCS 8051094-BS1
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) 054 mgl 005 90- 110
licate 8051094-DUP1 Source SA78602-01
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) BRL mgl 125 BRL
Thi laboratory report is not valid without all authorized sigllature 011 the cover page
Page 22 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Page 28
Semivolatile Organic Compounds by GCMS - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051216 - SW846 3510C
LCS 8051216-BS1
Prepared amp Analyzed 16-Mayshy
50 30- 1304 -C hloro-3-methylphenol 42 IJgl
40- 140Chloroaniline 39 IJgl 50
Chloronaphthalene 37 IJgl 50 40- 140
Chlorophenol 37 IJgl 50 30- 130
50 40- 140
40- 140
Chlorophenyl phenyl ether 45 IJgl
Chrysene 43 IJgl 50
Dibenzo (a h) anthracene 43 IJgl 50 40- 140
Dibenzofuran IJgl38 50 40- 140
50 40- 1401 Dichlorobenzene 35 IJgl
40- 1401 Dichlorobenzene 264 IJgl 50
40- 1401 Dichlorobenzene 434 IJgl 50
58 50 116 40- 1403 - Dichlorobenzidine IJgl
50 30- 130
40- 140 24-Dichlorophenol 38 IJgl
Diethyl phthalate 484 IJgl 50
50 40- 140Dimethyl phthalate 464 IJgl
Dlmethylphenol 39 IJgl 50 30- 130
DI-n-butyl phthalate 44 IJgll 50 40- 140
30- 130 6-Di nitro- 2-methylphenol 38 1J91 50
30- 130Dinltrophenol 36 1J91 50
42 50 40- 14024-Dlnitrotoluene 1J91
Dlnitrotoluene 1J9141 50 40- 140
Di-n-octyl phthalate 52 IJgl 50 104 40- 140
40- 140Fluoranthene 40 IJgl 50
Fluorene 41 IJgl 50 40- 140
39 50 40- 140Hexachlorobenzene IJgl
50 40- 140Hexachlorobutadiene 40 IJgl
40- 140Hexach lorocyclopentad iene 294 IJgl 50
40 50 40- 140Hexachloroethane IJgl
42 50 40-140Indeno (1 3-cd) pyrene IJgl
50 40- 140Isophorone 40 IJgl
40- 140Methylnaphthalene 394 IJgl 50
40- 140Methylphenol 39 IJgl 50
40 10 50 40- 1403 amp 4-Methylphenol IJgl
37 50 40-140Naphthalene IJgl
50 40-140Nitroaniline 39 IJgl
Nitroaniline 51 IJgl 50 102 40- 140
48 50 40- 140Nltroaniline 1J91
50 40- 140Nitrobenzene 40 IJgl
30- 130Nitrophenol 36 IJgl 50
40 IJgl 50 30- 130Nitrophenol 40- 140Nitrosodimethylamine 32 1J91 50
50 40-140N- N itrosodi-n-propyla mine 46 IJgl
40- 140N itrosodi phenyla ml ne 44 IJgl 50
41 IJgl 50 30- 130Pentachlorophenol 40- 140Phenanthrene 38 IJgl 50
50 30- 130Phenol 38 IJgl
40- 140Pyrene 424 1J91 50
40- 140Pyridine 294 1J91 50
40- 14024- Trichlorobenzene 364 IJgl 50
This laboratory report is not mlid without an authorized signature 011 the cover page
Page 16 of25 Reportble Detection Limit BRL = Below Reporting Limit
Semivolatie Organic Compounds by GCMS - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
BMch 8051216 - SW846 3510C
LC5 8051216-851
Prepared amp Analyzed 16-Mayshy
24 5- Trichlorophenol 404 gl 50 30- 130
246- Trichlorophenol 42 gl 50 30- 130
Surrogate 2-Fluorobiphenyl 29 gl 50 30- 130
Surrogate 2-Fluorophenot 27 gl 50 15- 110
Surrogate Nitrobenzene- 30 gl 50 30- 130
Surrogate Phenol- 29 gl 50 15- 110
Surrogate Terpheny-d4 30 gl 50 30- 130
Surrogate 6- Tribromopheno 324 gl 50 15- 110
This laboratory report is lIot valid without all authorized sigllature 011 tlle cover page
Reportble Detection Limit BRL = Below Reporting Limit Page 17 of25
Semivolatie Organic Compounds by GC - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051106 - SW846 3510C
Blank S051106-BLK1
Prepared amp Analyzed 15-Mayshy
Aroclor- 1016 BRL gI 0200
Aroclor- 1016 (2C) BRL gI 0200
Aroclor- 1221 BRL gI 0200
Aroclor- 1221 (2C) BRL gI 0200
Aroclor- 1232 BRL gI 0200
Aroclor- 1232 (2Cj BRL gI 0200
Aroclor- 1242 BRL gI 0200
Aroclor-1242 (2C) BRL gI 0200
Aroclor- 1248 BRL gI 0200
Aroclor- 1248 (2C) BRL gI 0200
Aroclor- 1254 BRL gI 0200
Aroclor- 1254(2Cj BRL gI 0200
Aroclor- 1260 BRL gI 0200
Aroclor- 1260 (2C) BRL gI 0200
Aroclor- 1262 BRL gI 0200
Aroclor- 1262 (2C) BRL gI 0200
Aroclor-1268 BRL gI 0200
Aroclor- 1268 (2C) BRL gI 0200
Surrogate Decachlorobiphenyl (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0231 0224 0194 0191
gI
gI
gI
gI
0200 0200 0200 0200
116 112
30- 150 30- 150 30- 150 30- 150
LC5 8051106-B51
Prepared 15-May-08 Analyzed 16-May-08
Aroclor- 1016 265 gI 0200 250 106 50- 114
Aroclor- 1 016 (2C) 240 gI 0200 250 50- 114
Aroclor- 1260 0269 gI 0200 250 107 40- 127
Aroclor-1260 (2Cj 270 gI 0200 250 108 40- 127
Surrogate Decachlorobiphenyl (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0225 0224 0188 0183
gI
gI
gI
gI
0200 0200 0200 0200
113 112
30- 150 30- 150 30- 150 30- 150
LC5 DUD rS051106-B5D1
Prepared 15-May-08 Analyzed 16-Mayshy
Aroclor- 1016 262 gl 0200 250 105 50- 114
Aroclor-1 016 (2Cj 241 gI 0200 250 50- 114
Aroclor- 1260 277 gI 0200 250 111 40- 127
Aroclor- 1260(2Cj 0260 gI 0200 250 104 40- 127
Surrogate Decachlorobipheny (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0238 0218 0189 0181
gI
gI
gI
gI
0200 0200 0200 0200
119 109
30- 150 30- 150 30- 150 30- 150
This laboratory report is lot valid without (II authorized sigllature 01 the cover page
Page 18 of25 Reportable Detection Limit BRL = Below Reporting Limit
Extractable Petroleum Hydrocarbons - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051102 - SW846 3510C
Blank 8051102-BLK1
Prepared 15-May-08 Analyzed 19-Mayshy
Non-polar material (SGT- HEM) BRL m91
LC8 8051102-B81
Prepared 15-May-08 Analyzed 19-Mayshy
Non-polar material (SGT- HEM) 184 m91 21 81 904
This laboratory report is not valid without an authorized signature 011 the cover page
Page 19 of25 Reportable Detection Limit BRL = Below Reporting Limit
Soluble Metals by EPA 200 Series Methods - Quality Control
Analyte(s) Result Flag Units RDL
Spike
Level
Source
Result REC
REC
Limits RPD
RPD
Limit
Batch 8051150 - EPA 200 Series
Blank 8051150-BLK1
Prepared amp Analyzed 21-May-
Iron
Zinc
Selenium
Nickel
Chromium
Copper
Arsenic
BRL
BRL
BRL
BRL
BRL
BRL
BRL
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0150
0050
0150
0050
0050
0050
0040
LCS 8051150-BS1
Prepared amp Analyzed 21-May-
Selenium
Zinc
Iron
Nickel
Chromium
Arsenic
Copper
123
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0150
0050
0150
0050
0050
0040
0050
103
105
101
100
85- 115
85- 115
85- 115
85- 115
85- 115
85-115
85- 115
licate B051150-DUP1 Source SA7B602shy
Prepared amp Analyzed 21-May-
Iron
Zinc
Selenium
Nickel
Copper
Chromium
Arsenic
17
0162
BRL
0015
0017
BRL
0450
QR8
mgl
mgl
mgl
mgl
mgl
mgl
mgi
0150
0050
0150
0050
0050
0050
0040
184
0186
BRL
0014
0023
BRL
0468
Matrix S ike 8051150-MS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Iron
Selenium
Nickel
Zinc
Copper
Chromium
Arsenic
19 QM2 mgl
mgll
mgl
mgl
mgl
mgl
mgl
0150
0150
0050
0050
0050
0050
0040
125
184
BRL
0014
0186
0023
BRL
0468
104
105
102
70- 130
70- 130
70-130
70- 130
70- 130
70-130
70- 130
Post S ike 8051150-PS1 Source SA78602shy
Prepared amp Analyzed 21-May-
Zinc
Iron
Selenium
Nickel
Copper
Arsenic
Chromium
18 QM2
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0050
0150
0150
0050
0050
0040
0050
0186
184
BRL
0014
0023
0468
BRL
104
104
101
85- 115
85- 115
85- 115
85-115
85-115
85- 115
85-115
Batch 8051152 - EPA200SW7000 Series
Blank B051152-BLK1
Prepared amp Analyzed 21-May-
Mercury BRL mgl 00020
This laboratory report is IIOt valid witllOut all authorized sigllature 011 the coverpage
Page 20 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Soluble Metals by EPA 200 Series Methods - Quality Control
Analyte(s) Result Flag Units RDL
Spike
Level
Source
Result REC
REC
Limits RPD
RPD
Limit
Batch 8051152 - EPA200SW7000 Series
LCS B051152-BS1
Prepared amp Analyzed 21-May-
Mercury 00576 m91 00020 00500 115 85- 115
licate B051152-DUP1 Source SA78602-01
Prepared amp Analyzed 21-May-
Mercury BRL m91 00020 BRL
Matrix S ike 8051152-MS1 Source SA78602shy
Prepared amp Analyzed 21-May-
Mercury 00632 OM m91 00020 00500 BRL 126 75- 125
Post S ike 8051152-PS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Mercury 00624 OC1 m91 00020 00500 BRL 125 85- 115
Batch 8051249 - 2008No digestion
Blank 8051249-BLK1
Prepared amp Analyzed 21-May-
Lead
Antimony
Cadmium
Silver
BRL
BRL
BRL
BRL
m91
m91
m91
m91
0002
0002
0002
0002
LCS B051249-BS1
Prepared amp Analyzed 21-May-
Antimony
Lead
Silver
Cadmium
143
145 OC2
m91
m91
m91
m91
0050
0050
0050
0040
103
115
107
116
85- 115
85- 115
85- 115
85- 115
licate 8051249-DUP1 Source SA7B602shy
Prepared amp Analyzed 21- May-
Lead
Antimony
Cadmium
Silver
0009
0002
00005
00002
ORB
m91
m91
m91
m91
0002
0002
0002
0002
0011
0003
00005
00003
Matrix S ike 8051249-MS1 Source SA78602shy
Prepared amp Analyzed 21- May-
Lead
Antimony
Cadmium
Silver
142
m91
m91
m91
m91
0050
0050
0040
0050
0011
0003
00005
00003
111
101
114
102
70- 130
70-130
70c130
70- 130
Post S ike 8051249-PS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Antimony
Cadmium
Silver
38
OC2
m91
m91
m91
0050
0040
0050
125
0003
00005
00003
110
121
109
85- 115
85- 115
85- 115
This laboratory report is flOt valid IVithout all authorized signature 011 the cOIer page
Reportable Detection Limit BRL Below Reporting Limit Page 21 of 25
General Chemistry Parameters - Quality Control
Spike Source REC RPD
Analyte( s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051049 - General Preparation
Blank S051 049-BLK1
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
Blank S051049-BLK2
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
Blank S051 049-BLK3
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
LCS S051049-BS1
Prepared amp Analyzed 14-May-
Total Residual Chlorine 046 mgl 020 0500 90- 110
LCS S051049-BS2
Prepared amp Analyzed 14-May-
Total Residual Chlorine 047 mgl 020 0500 90- 110
LCS S051049-BS3
Prepared amp Analyzed 14-May-
Total Residual Chlorine 054 mgl 020 0500 108 90-110
licate B051049-DUP1 Source SA7S544shy
Prepared amp Analyzed 14-May-
Total Residual Chlorine 012 mgl 020 010
licate S051049-DUP2 Source SA7S602-01
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020 BRL
Matrix S ike 8051049-MS1 Source SA78544-01
Prepared amp Analyzed 14-May-
Total Residual Chlorine 065 mgl 020 0500 010 110 80- 120
Matrix S ike 8051049-MS2 Source SA7B602shy
Prepared amp Analyzed 14-May-
Total Residual Chlorine mgl 500 125 BRL 108 80- 120
Reference 8051 049-SRM1
Prepared amp Analyzed 14-May-
Total Residual Chlorine 100 mgl 020 0967 103 85-115
Batch 8051094 - General Preparation
Blank 8051094-BLK1
Prepared amp Analyzed 14 May-
Hexavalent Chromium (soluble) BRL mgl 005
Blank 8051 094-BLK2
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) BRL mgl 005
LCS 8051094-BS1
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) 054 mgl 005 90- 110
licate 8051094-DUP1 Source SA78602-01
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) BRL mgl 125 BRL
Thi laboratory report is not valid without all authorized sigllature 011 the cover page
Page 22 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Page 29
Semivolatie Organic Compounds by GCMS - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
BMch 8051216 - SW846 3510C
LC5 8051216-851
Prepared amp Analyzed 16-Mayshy
24 5- Trichlorophenol 404 gl 50 30- 130
246- Trichlorophenol 42 gl 50 30- 130
Surrogate 2-Fluorobiphenyl 29 gl 50 30- 130
Surrogate 2-Fluorophenot 27 gl 50 15- 110
Surrogate Nitrobenzene- 30 gl 50 30- 130
Surrogate Phenol- 29 gl 50 15- 110
Surrogate Terpheny-d4 30 gl 50 30- 130
Surrogate 6- Tribromopheno 324 gl 50 15- 110
This laboratory report is lIot valid without all authorized sigllature 011 tlle cover page
Reportble Detection Limit BRL = Below Reporting Limit Page 17 of25
Semivolatie Organic Compounds by GC - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051106 - SW846 3510C
Blank S051106-BLK1
Prepared amp Analyzed 15-Mayshy
Aroclor- 1016 BRL gI 0200
Aroclor- 1016 (2C) BRL gI 0200
Aroclor- 1221 BRL gI 0200
Aroclor- 1221 (2C) BRL gI 0200
Aroclor- 1232 BRL gI 0200
Aroclor- 1232 (2Cj BRL gI 0200
Aroclor- 1242 BRL gI 0200
Aroclor-1242 (2C) BRL gI 0200
Aroclor- 1248 BRL gI 0200
Aroclor- 1248 (2C) BRL gI 0200
Aroclor- 1254 BRL gI 0200
Aroclor- 1254(2Cj BRL gI 0200
Aroclor- 1260 BRL gI 0200
Aroclor- 1260 (2C) BRL gI 0200
Aroclor- 1262 BRL gI 0200
Aroclor- 1262 (2C) BRL gI 0200
Aroclor-1268 BRL gI 0200
Aroclor- 1268 (2C) BRL gI 0200
Surrogate Decachlorobiphenyl (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0231 0224 0194 0191
gI
gI
gI
gI
0200 0200 0200 0200
116 112
30- 150 30- 150 30- 150 30- 150
LC5 8051106-B51
Prepared 15-May-08 Analyzed 16-May-08
Aroclor- 1016 265 gI 0200 250 106 50- 114
Aroclor- 1 016 (2C) 240 gI 0200 250 50- 114
Aroclor- 1260 0269 gI 0200 250 107 40- 127
Aroclor-1260 (2Cj 270 gI 0200 250 108 40- 127
Surrogate Decachlorobiphenyl (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0225 0224 0188 0183
gI
gI
gI
gI
0200 0200 0200 0200
113 112
30- 150 30- 150 30- 150 30- 150
LC5 DUD rS051106-B5D1
Prepared 15-May-08 Analyzed 16-Mayshy
Aroclor- 1016 262 gl 0200 250 105 50- 114
Aroclor-1 016 (2Cj 241 gI 0200 250 50- 114
Aroclor- 1260 277 gI 0200 250 111 40- 127
Aroclor- 1260(2Cj 0260 gI 0200 250 104 40- 127
Surrogate Decachlorobipheny (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0238 0218 0189 0181
gI
gI
gI
gI
0200 0200 0200 0200
119 109
30- 150 30- 150 30- 150 30- 150
This laboratory report is lot valid without (II authorized sigllature 01 the cover page
Page 18 of25 Reportable Detection Limit BRL = Below Reporting Limit
Extractable Petroleum Hydrocarbons - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051102 - SW846 3510C
Blank 8051102-BLK1
Prepared 15-May-08 Analyzed 19-Mayshy
Non-polar material (SGT- HEM) BRL m91
LC8 8051102-B81
Prepared 15-May-08 Analyzed 19-Mayshy
Non-polar material (SGT- HEM) 184 m91 21 81 904
This laboratory report is not valid without an authorized signature 011 the cover page
Page 19 of25 Reportable Detection Limit BRL = Below Reporting Limit
Soluble Metals by EPA 200 Series Methods - Quality Control
Analyte(s) Result Flag Units RDL
Spike
Level
Source
Result REC
REC
Limits RPD
RPD
Limit
Batch 8051150 - EPA 200 Series
Blank 8051150-BLK1
Prepared amp Analyzed 21-May-
Iron
Zinc
Selenium
Nickel
Chromium
Copper
Arsenic
BRL
BRL
BRL
BRL
BRL
BRL
BRL
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0150
0050
0150
0050
0050
0050
0040
LCS 8051150-BS1
Prepared amp Analyzed 21-May-
Selenium
Zinc
Iron
Nickel
Chromium
Arsenic
Copper
123
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0150
0050
0150
0050
0050
0040
0050
103
105
101
100
85- 115
85- 115
85- 115
85- 115
85- 115
85-115
85- 115
licate B051150-DUP1 Source SA7B602shy
Prepared amp Analyzed 21-May-
Iron
Zinc
Selenium
Nickel
Copper
Chromium
Arsenic
17
0162
BRL
0015
0017
BRL
0450
QR8
mgl
mgl
mgl
mgl
mgl
mgl
mgi
0150
0050
0150
0050
0050
0050
0040
184
0186
BRL
0014
0023
BRL
0468
Matrix S ike 8051150-MS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Iron
Selenium
Nickel
Zinc
Copper
Chromium
Arsenic
19 QM2 mgl
mgll
mgl
mgl
mgl
mgl
mgl
0150
0150
0050
0050
0050
0050
0040
125
184
BRL
0014
0186
0023
BRL
0468
104
105
102
70- 130
70- 130
70-130
70- 130
70- 130
70-130
70- 130
Post S ike 8051150-PS1 Source SA78602shy
Prepared amp Analyzed 21-May-
Zinc
Iron
Selenium
Nickel
Copper
Arsenic
Chromium
18 QM2
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0050
0150
0150
0050
0050
0040
0050
0186
184
BRL
0014
0023
0468
BRL
104
104
101
85- 115
85- 115
85- 115
85-115
85-115
85- 115
85-115
Batch 8051152 - EPA200SW7000 Series
Blank B051152-BLK1
Prepared amp Analyzed 21-May-
Mercury BRL mgl 00020
This laboratory report is IIOt valid witllOut all authorized sigllature 011 the coverpage
Page 20 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Soluble Metals by EPA 200 Series Methods - Quality Control
Analyte(s) Result Flag Units RDL
Spike
Level
Source
Result REC
REC
Limits RPD
RPD
Limit
Batch 8051152 - EPA200SW7000 Series
LCS B051152-BS1
Prepared amp Analyzed 21-May-
Mercury 00576 m91 00020 00500 115 85- 115
licate B051152-DUP1 Source SA78602-01
Prepared amp Analyzed 21-May-
Mercury BRL m91 00020 BRL
Matrix S ike 8051152-MS1 Source SA78602shy
Prepared amp Analyzed 21-May-
Mercury 00632 OM m91 00020 00500 BRL 126 75- 125
Post S ike 8051152-PS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Mercury 00624 OC1 m91 00020 00500 BRL 125 85- 115
Batch 8051249 - 2008No digestion
Blank 8051249-BLK1
Prepared amp Analyzed 21-May-
Lead
Antimony
Cadmium
Silver
BRL
BRL
BRL
BRL
m91
m91
m91
m91
0002
0002
0002
0002
LCS B051249-BS1
Prepared amp Analyzed 21-May-
Antimony
Lead
Silver
Cadmium
143
145 OC2
m91
m91
m91
m91
0050
0050
0050
0040
103
115
107
116
85- 115
85- 115
85- 115
85- 115
licate 8051249-DUP1 Source SA7B602shy
Prepared amp Analyzed 21- May-
Lead
Antimony
Cadmium
Silver
0009
0002
00005
00002
ORB
m91
m91
m91
m91
0002
0002
0002
0002
0011
0003
00005
00003
Matrix S ike 8051249-MS1 Source SA78602shy
Prepared amp Analyzed 21- May-
Lead
Antimony
Cadmium
Silver
142
m91
m91
m91
m91
0050
0050
0040
0050
0011
0003
00005
00003
111
101
114
102
70- 130
70-130
70c130
70- 130
Post S ike 8051249-PS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Antimony
Cadmium
Silver
38
OC2
m91
m91
m91
0050
0040
0050
125
0003
00005
00003
110
121
109
85- 115
85- 115
85- 115
This laboratory report is flOt valid IVithout all authorized signature 011 the cOIer page
Reportable Detection Limit BRL Below Reporting Limit Page 21 of 25
General Chemistry Parameters - Quality Control
Spike Source REC RPD
Analyte( s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051049 - General Preparation
Blank S051 049-BLK1
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
Blank S051049-BLK2
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
Blank S051 049-BLK3
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
LCS S051049-BS1
Prepared amp Analyzed 14-May-
Total Residual Chlorine 046 mgl 020 0500 90- 110
LCS S051049-BS2
Prepared amp Analyzed 14-May-
Total Residual Chlorine 047 mgl 020 0500 90- 110
LCS S051049-BS3
Prepared amp Analyzed 14-May-
Total Residual Chlorine 054 mgl 020 0500 108 90-110
licate B051049-DUP1 Source SA7S544shy
Prepared amp Analyzed 14-May-
Total Residual Chlorine 012 mgl 020 010
licate S051049-DUP2 Source SA7S602-01
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020 BRL
Matrix S ike 8051049-MS1 Source SA78544-01
Prepared amp Analyzed 14-May-
Total Residual Chlorine 065 mgl 020 0500 010 110 80- 120
Matrix S ike 8051049-MS2 Source SA7B602shy
Prepared amp Analyzed 14-May-
Total Residual Chlorine mgl 500 125 BRL 108 80- 120
Reference 8051 049-SRM1
Prepared amp Analyzed 14-May-
Total Residual Chlorine 100 mgl 020 0967 103 85-115
Batch 8051094 - General Preparation
Blank 8051094-BLK1
Prepared amp Analyzed 14 May-
Hexavalent Chromium (soluble) BRL mgl 005
Blank 8051 094-BLK2
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) BRL mgl 005
LCS 8051094-BS1
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) 054 mgl 005 90- 110
licate 8051094-DUP1 Source SA78602-01
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) BRL mgl 125 BRL
Thi laboratory report is not valid without all authorized sigllature 011 the cover page
Page 22 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Page 30
Semivolatie Organic Compounds by GC - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051106 - SW846 3510C
Blank S051106-BLK1
Prepared amp Analyzed 15-Mayshy
Aroclor- 1016 BRL gI 0200
Aroclor- 1016 (2C) BRL gI 0200
Aroclor- 1221 BRL gI 0200
Aroclor- 1221 (2C) BRL gI 0200
Aroclor- 1232 BRL gI 0200
Aroclor- 1232 (2Cj BRL gI 0200
Aroclor- 1242 BRL gI 0200
Aroclor-1242 (2C) BRL gI 0200
Aroclor- 1248 BRL gI 0200
Aroclor- 1248 (2C) BRL gI 0200
Aroclor- 1254 BRL gI 0200
Aroclor- 1254(2Cj BRL gI 0200
Aroclor- 1260 BRL gI 0200
Aroclor- 1260 (2C) BRL gI 0200
Aroclor- 1262 BRL gI 0200
Aroclor- 1262 (2C) BRL gI 0200
Aroclor-1268 BRL gI 0200
Aroclor- 1268 (2C) BRL gI 0200
Surrogate Decachlorobiphenyl (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0231 0224 0194 0191
gI
gI
gI
gI
0200 0200 0200 0200
116 112
30- 150 30- 150 30- 150 30- 150
LC5 8051106-B51
Prepared 15-May-08 Analyzed 16-May-08
Aroclor- 1016 265 gI 0200 250 106 50- 114
Aroclor- 1 016 (2C) 240 gI 0200 250 50- 114
Aroclor- 1260 0269 gI 0200 250 107 40- 127
Aroclor-1260 (2Cj 270 gI 0200 250 108 40- 127
Surrogate Decachlorobiphenyl (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0225 0224 0188 0183
gI
gI
gI
gI
0200 0200 0200 0200
113 112
30- 150 30- 150 30- 150 30- 150
LC5 DUD rS051106-B5D1
Prepared 15-May-08 Analyzed 16-Mayshy
Aroclor- 1016 262 gl 0200 250 105 50- 114
Aroclor-1 016 (2Cj 241 gI 0200 250 50- 114
Aroclor- 1260 277 gI 0200 250 111 40- 127
Aroclor- 1260(2Cj 0260 gI 0200 250 104 40- 127
Surrogate Decachlorobipheny (Sr) Surrogate Decachlorobiphenyl (Sr) 12C) Surrogate 4 DB-Octafluorobiphenyl (Sr) Surrogate 4 DB-Octafluorobiphenyl (Sr) I
0238 0218 0189 0181
gI
gI
gI
gI
0200 0200 0200 0200
119 109
30- 150 30- 150 30- 150 30- 150
This laboratory report is lot valid without (II authorized sigllature 01 the cover page
Page 18 of25 Reportable Detection Limit BRL = Below Reporting Limit
Extractable Petroleum Hydrocarbons - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051102 - SW846 3510C
Blank 8051102-BLK1
Prepared 15-May-08 Analyzed 19-Mayshy
Non-polar material (SGT- HEM) BRL m91
LC8 8051102-B81
Prepared 15-May-08 Analyzed 19-Mayshy
Non-polar material (SGT- HEM) 184 m91 21 81 904
This laboratory report is not valid without an authorized signature 011 the cover page
Page 19 of25 Reportable Detection Limit BRL = Below Reporting Limit
Soluble Metals by EPA 200 Series Methods - Quality Control
Analyte(s) Result Flag Units RDL
Spike
Level
Source
Result REC
REC
Limits RPD
RPD
Limit
Batch 8051150 - EPA 200 Series
Blank 8051150-BLK1
Prepared amp Analyzed 21-May-
Iron
Zinc
Selenium
Nickel
Chromium
Copper
Arsenic
BRL
BRL
BRL
BRL
BRL
BRL
BRL
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0150
0050
0150
0050
0050
0050
0040
LCS 8051150-BS1
Prepared amp Analyzed 21-May-
Selenium
Zinc
Iron
Nickel
Chromium
Arsenic
Copper
123
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0150
0050
0150
0050
0050
0040
0050
103
105
101
100
85- 115
85- 115
85- 115
85- 115
85- 115
85-115
85- 115
licate B051150-DUP1 Source SA7B602shy
Prepared amp Analyzed 21-May-
Iron
Zinc
Selenium
Nickel
Copper
Chromium
Arsenic
17
0162
BRL
0015
0017
BRL
0450
QR8
mgl
mgl
mgl
mgl
mgl
mgl
mgi
0150
0050
0150
0050
0050
0050
0040
184
0186
BRL
0014
0023
BRL
0468
Matrix S ike 8051150-MS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Iron
Selenium
Nickel
Zinc
Copper
Chromium
Arsenic
19 QM2 mgl
mgll
mgl
mgl
mgl
mgl
mgl
0150
0150
0050
0050
0050
0050
0040
125
184
BRL
0014
0186
0023
BRL
0468
104
105
102
70- 130
70- 130
70-130
70- 130
70- 130
70-130
70- 130
Post S ike 8051150-PS1 Source SA78602shy
Prepared amp Analyzed 21-May-
Zinc
Iron
Selenium
Nickel
Copper
Arsenic
Chromium
18 QM2
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0050
0150
0150
0050
0050
0040
0050
0186
184
BRL
0014
0023
0468
BRL
104
104
101
85- 115
85- 115
85- 115
85-115
85-115
85- 115
85-115
Batch 8051152 - EPA200SW7000 Series
Blank B051152-BLK1
Prepared amp Analyzed 21-May-
Mercury BRL mgl 00020
This laboratory report is IIOt valid witllOut all authorized sigllature 011 the coverpage
Page 20 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Soluble Metals by EPA 200 Series Methods - Quality Control
Analyte(s) Result Flag Units RDL
Spike
Level
Source
Result REC
REC
Limits RPD
RPD
Limit
Batch 8051152 - EPA200SW7000 Series
LCS B051152-BS1
Prepared amp Analyzed 21-May-
Mercury 00576 m91 00020 00500 115 85- 115
licate B051152-DUP1 Source SA78602-01
Prepared amp Analyzed 21-May-
Mercury BRL m91 00020 BRL
Matrix S ike 8051152-MS1 Source SA78602shy
Prepared amp Analyzed 21-May-
Mercury 00632 OM m91 00020 00500 BRL 126 75- 125
Post S ike 8051152-PS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Mercury 00624 OC1 m91 00020 00500 BRL 125 85- 115
Batch 8051249 - 2008No digestion
Blank 8051249-BLK1
Prepared amp Analyzed 21-May-
Lead
Antimony
Cadmium
Silver
BRL
BRL
BRL
BRL
m91
m91
m91
m91
0002
0002
0002
0002
LCS B051249-BS1
Prepared amp Analyzed 21-May-
Antimony
Lead
Silver
Cadmium
143
145 OC2
m91
m91
m91
m91
0050
0050
0050
0040
103
115
107
116
85- 115
85- 115
85- 115
85- 115
licate 8051249-DUP1 Source SA7B602shy
Prepared amp Analyzed 21- May-
Lead
Antimony
Cadmium
Silver
0009
0002
00005
00002
ORB
m91
m91
m91
m91
0002
0002
0002
0002
0011
0003
00005
00003
Matrix S ike 8051249-MS1 Source SA78602shy
Prepared amp Analyzed 21- May-
Lead
Antimony
Cadmium
Silver
142
m91
m91
m91
m91
0050
0050
0040
0050
0011
0003
00005
00003
111
101
114
102
70- 130
70-130
70c130
70- 130
Post S ike 8051249-PS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Antimony
Cadmium
Silver
38
OC2
m91
m91
m91
0050
0040
0050
125
0003
00005
00003
110
121
109
85- 115
85- 115
85- 115
This laboratory report is flOt valid IVithout all authorized signature 011 the cOIer page
Reportable Detection Limit BRL Below Reporting Limit Page 21 of 25
General Chemistry Parameters - Quality Control
Spike Source REC RPD
Analyte( s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051049 - General Preparation
Blank S051 049-BLK1
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
Blank S051049-BLK2
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
Blank S051 049-BLK3
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
LCS S051049-BS1
Prepared amp Analyzed 14-May-
Total Residual Chlorine 046 mgl 020 0500 90- 110
LCS S051049-BS2
Prepared amp Analyzed 14-May-
Total Residual Chlorine 047 mgl 020 0500 90- 110
LCS S051049-BS3
Prepared amp Analyzed 14-May-
Total Residual Chlorine 054 mgl 020 0500 108 90-110
licate B051049-DUP1 Source SA7S544shy
Prepared amp Analyzed 14-May-
Total Residual Chlorine 012 mgl 020 010
licate S051049-DUP2 Source SA7S602-01
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020 BRL
Matrix S ike 8051049-MS1 Source SA78544-01
Prepared amp Analyzed 14-May-
Total Residual Chlorine 065 mgl 020 0500 010 110 80- 120
Matrix S ike 8051049-MS2 Source SA7B602shy
Prepared amp Analyzed 14-May-
Total Residual Chlorine mgl 500 125 BRL 108 80- 120
Reference 8051 049-SRM1
Prepared amp Analyzed 14-May-
Total Residual Chlorine 100 mgl 020 0967 103 85-115
Batch 8051094 - General Preparation
Blank 8051094-BLK1
Prepared amp Analyzed 14 May-
Hexavalent Chromium (soluble) BRL mgl 005
Blank 8051 094-BLK2
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) BRL mgl 005
LCS 8051094-BS1
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) 054 mgl 005 90- 110
licate 8051094-DUP1 Source SA78602-01
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) BRL mgl 125 BRL
Thi laboratory report is not valid without all authorized sigllature 011 the cover page
Page 22 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Page 31
Extractable Petroleum Hydrocarbons - Quality Control
Spike Source REC RPD
Analyte(s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051102 - SW846 3510C
Blank 8051102-BLK1
Prepared 15-May-08 Analyzed 19-Mayshy
Non-polar material (SGT- HEM) BRL m91
LC8 8051102-B81
Prepared 15-May-08 Analyzed 19-Mayshy
Non-polar material (SGT- HEM) 184 m91 21 81 904
This laboratory report is not valid without an authorized signature 011 the cover page
Page 19 of25 Reportable Detection Limit BRL = Below Reporting Limit
Soluble Metals by EPA 200 Series Methods - Quality Control
Analyte(s) Result Flag Units RDL
Spike
Level
Source
Result REC
REC
Limits RPD
RPD
Limit
Batch 8051150 - EPA 200 Series
Blank 8051150-BLK1
Prepared amp Analyzed 21-May-
Iron
Zinc
Selenium
Nickel
Chromium
Copper
Arsenic
BRL
BRL
BRL
BRL
BRL
BRL
BRL
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0150
0050
0150
0050
0050
0050
0040
LCS 8051150-BS1
Prepared amp Analyzed 21-May-
Selenium
Zinc
Iron
Nickel
Chromium
Arsenic
Copper
123
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0150
0050
0150
0050
0050
0040
0050
103
105
101
100
85- 115
85- 115
85- 115
85- 115
85- 115
85-115
85- 115
licate B051150-DUP1 Source SA7B602shy
Prepared amp Analyzed 21-May-
Iron
Zinc
Selenium
Nickel
Copper
Chromium
Arsenic
17
0162
BRL
0015
0017
BRL
0450
QR8
mgl
mgl
mgl
mgl
mgl
mgl
mgi
0150
0050
0150
0050
0050
0050
0040
184
0186
BRL
0014
0023
BRL
0468
Matrix S ike 8051150-MS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Iron
Selenium
Nickel
Zinc
Copper
Chromium
Arsenic
19 QM2 mgl
mgll
mgl
mgl
mgl
mgl
mgl
0150
0150
0050
0050
0050
0050
0040
125
184
BRL
0014
0186
0023
BRL
0468
104
105
102
70- 130
70- 130
70-130
70- 130
70- 130
70-130
70- 130
Post S ike 8051150-PS1 Source SA78602shy
Prepared amp Analyzed 21-May-
Zinc
Iron
Selenium
Nickel
Copper
Arsenic
Chromium
18 QM2
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0050
0150
0150
0050
0050
0040
0050
0186
184
BRL
0014
0023
0468
BRL
104
104
101
85- 115
85- 115
85- 115
85-115
85-115
85- 115
85-115
Batch 8051152 - EPA200SW7000 Series
Blank B051152-BLK1
Prepared amp Analyzed 21-May-
Mercury BRL mgl 00020
This laboratory report is IIOt valid witllOut all authorized sigllature 011 the coverpage
Page 20 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Soluble Metals by EPA 200 Series Methods - Quality Control
Analyte(s) Result Flag Units RDL
Spike
Level
Source
Result REC
REC
Limits RPD
RPD
Limit
Batch 8051152 - EPA200SW7000 Series
LCS B051152-BS1
Prepared amp Analyzed 21-May-
Mercury 00576 m91 00020 00500 115 85- 115
licate B051152-DUP1 Source SA78602-01
Prepared amp Analyzed 21-May-
Mercury BRL m91 00020 BRL
Matrix S ike 8051152-MS1 Source SA78602shy
Prepared amp Analyzed 21-May-
Mercury 00632 OM m91 00020 00500 BRL 126 75- 125
Post S ike 8051152-PS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Mercury 00624 OC1 m91 00020 00500 BRL 125 85- 115
Batch 8051249 - 2008No digestion
Blank 8051249-BLK1
Prepared amp Analyzed 21-May-
Lead
Antimony
Cadmium
Silver
BRL
BRL
BRL
BRL
m91
m91
m91
m91
0002
0002
0002
0002
LCS B051249-BS1
Prepared amp Analyzed 21-May-
Antimony
Lead
Silver
Cadmium
143
145 OC2
m91
m91
m91
m91
0050
0050
0050
0040
103
115
107
116
85- 115
85- 115
85- 115
85- 115
licate 8051249-DUP1 Source SA7B602shy
Prepared amp Analyzed 21- May-
Lead
Antimony
Cadmium
Silver
0009
0002
00005
00002
ORB
m91
m91
m91
m91
0002
0002
0002
0002
0011
0003
00005
00003
Matrix S ike 8051249-MS1 Source SA78602shy
Prepared amp Analyzed 21- May-
Lead
Antimony
Cadmium
Silver
142
m91
m91
m91
m91
0050
0050
0040
0050
0011
0003
00005
00003
111
101
114
102
70- 130
70-130
70c130
70- 130
Post S ike 8051249-PS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Antimony
Cadmium
Silver
38
OC2
m91
m91
m91
0050
0040
0050
125
0003
00005
00003
110
121
109
85- 115
85- 115
85- 115
This laboratory report is flOt valid IVithout all authorized signature 011 the cOIer page
Reportable Detection Limit BRL Below Reporting Limit Page 21 of 25
General Chemistry Parameters - Quality Control
Spike Source REC RPD
Analyte( s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051049 - General Preparation
Blank S051 049-BLK1
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
Blank S051049-BLK2
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
Blank S051 049-BLK3
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
LCS S051049-BS1
Prepared amp Analyzed 14-May-
Total Residual Chlorine 046 mgl 020 0500 90- 110
LCS S051049-BS2
Prepared amp Analyzed 14-May-
Total Residual Chlorine 047 mgl 020 0500 90- 110
LCS S051049-BS3
Prepared amp Analyzed 14-May-
Total Residual Chlorine 054 mgl 020 0500 108 90-110
licate B051049-DUP1 Source SA7S544shy
Prepared amp Analyzed 14-May-
Total Residual Chlorine 012 mgl 020 010
licate S051049-DUP2 Source SA7S602-01
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020 BRL
Matrix S ike 8051049-MS1 Source SA78544-01
Prepared amp Analyzed 14-May-
Total Residual Chlorine 065 mgl 020 0500 010 110 80- 120
Matrix S ike 8051049-MS2 Source SA7B602shy
Prepared amp Analyzed 14-May-
Total Residual Chlorine mgl 500 125 BRL 108 80- 120
Reference 8051 049-SRM1
Prepared amp Analyzed 14-May-
Total Residual Chlorine 100 mgl 020 0967 103 85-115
Batch 8051094 - General Preparation
Blank 8051094-BLK1
Prepared amp Analyzed 14 May-
Hexavalent Chromium (soluble) BRL mgl 005
Blank 8051 094-BLK2
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) BRL mgl 005
LCS 8051094-BS1
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) 054 mgl 005 90- 110
licate 8051094-DUP1 Source SA78602-01
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) BRL mgl 125 BRL
Thi laboratory report is not valid without all authorized sigllature 011 the cover page
Page 22 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Page 32
Soluble Metals by EPA 200 Series Methods - Quality Control
Analyte(s) Result Flag Units RDL
Spike
Level
Source
Result REC
REC
Limits RPD
RPD
Limit
Batch 8051150 - EPA 200 Series
Blank 8051150-BLK1
Prepared amp Analyzed 21-May-
Iron
Zinc
Selenium
Nickel
Chromium
Copper
Arsenic
BRL
BRL
BRL
BRL
BRL
BRL
BRL
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0150
0050
0150
0050
0050
0050
0040
LCS 8051150-BS1
Prepared amp Analyzed 21-May-
Selenium
Zinc
Iron
Nickel
Chromium
Arsenic
Copper
123
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0150
0050
0150
0050
0050
0040
0050
103
105
101
100
85- 115
85- 115
85- 115
85- 115
85- 115
85-115
85- 115
licate B051150-DUP1 Source SA7B602shy
Prepared amp Analyzed 21-May-
Iron
Zinc
Selenium
Nickel
Copper
Chromium
Arsenic
17
0162
BRL
0015
0017
BRL
0450
QR8
mgl
mgl
mgl
mgl
mgl
mgl
mgi
0150
0050
0150
0050
0050
0050
0040
184
0186
BRL
0014
0023
BRL
0468
Matrix S ike 8051150-MS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Iron
Selenium
Nickel
Zinc
Copper
Chromium
Arsenic
19 QM2 mgl
mgll
mgl
mgl
mgl
mgl
mgl
0150
0150
0050
0050
0050
0050
0040
125
184
BRL
0014
0186
0023
BRL
0468
104
105
102
70- 130
70- 130
70-130
70- 130
70- 130
70-130
70- 130
Post S ike 8051150-PS1 Source SA78602shy
Prepared amp Analyzed 21-May-
Zinc
Iron
Selenium
Nickel
Copper
Arsenic
Chromium
18 QM2
mgl
mgl
mgl
mgl
mgl
mgl
mgl
0050
0150
0150
0050
0050
0040
0050
0186
184
BRL
0014
0023
0468
BRL
104
104
101
85- 115
85- 115
85- 115
85-115
85-115
85- 115
85-115
Batch 8051152 - EPA200SW7000 Series
Blank B051152-BLK1
Prepared amp Analyzed 21-May-
Mercury BRL mgl 00020
This laboratory report is IIOt valid witllOut all authorized sigllature 011 the coverpage
Page 20 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Soluble Metals by EPA 200 Series Methods - Quality Control
Analyte(s) Result Flag Units RDL
Spike
Level
Source
Result REC
REC
Limits RPD
RPD
Limit
Batch 8051152 - EPA200SW7000 Series
LCS B051152-BS1
Prepared amp Analyzed 21-May-
Mercury 00576 m91 00020 00500 115 85- 115
licate B051152-DUP1 Source SA78602-01
Prepared amp Analyzed 21-May-
Mercury BRL m91 00020 BRL
Matrix S ike 8051152-MS1 Source SA78602shy
Prepared amp Analyzed 21-May-
Mercury 00632 OM m91 00020 00500 BRL 126 75- 125
Post S ike 8051152-PS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Mercury 00624 OC1 m91 00020 00500 BRL 125 85- 115
Batch 8051249 - 2008No digestion
Blank 8051249-BLK1
Prepared amp Analyzed 21-May-
Lead
Antimony
Cadmium
Silver
BRL
BRL
BRL
BRL
m91
m91
m91
m91
0002
0002
0002
0002
LCS B051249-BS1
Prepared amp Analyzed 21-May-
Antimony
Lead
Silver
Cadmium
143
145 OC2
m91
m91
m91
m91
0050
0050
0050
0040
103
115
107
116
85- 115
85- 115
85- 115
85- 115
licate 8051249-DUP1 Source SA7B602shy
Prepared amp Analyzed 21- May-
Lead
Antimony
Cadmium
Silver
0009
0002
00005
00002
ORB
m91
m91
m91
m91
0002
0002
0002
0002
0011
0003
00005
00003
Matrix S ike 8051249-MS1 Source SA78602shy
Prepared amp Analyzed 21- May-
Lead
Antimony
Cadmium
Silver
142
m91
m91
m91
m91
0050
0050
0040
0050
0011
0003
00005
00003
111
101
114
102
70- 130
70-130
70c130
70- 130
Post S ike 8051249-PS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Antimony
Cadmium
Silver
38
OC2
m91
m91
m91
0050
0040
0050
125
0003
00005
00003
110
121
109
85- 115
85- 115
85- 115
This laboratory report is flOt valid IVithout all authorized signature 011 the cOIer page
Reportable Detection Limit BRL Below Reporting Limit Page 21 of 25
General Chemistry Parameters - Quality Control
Spike Source REC RPD
Analyte( s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051049 - General Preparation
Blank S051 049-BLK1
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
Blank S051049-BLK2
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
Blank S051 049-BLK3
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
LCS S051049-BS1
Prepared amp Analyzed 14-May-
Total Residual Chlorine 046 mgl 020 0500 90- 110
LCS S051049-BS2
Prepared amp Analyzed 14-May-
Total Residual Chlorine 047 mgl 020 0500 90- 110
LCS S051049-BS3
Prepared amp Analyzed 14-May-
Total Residual Chlorine 054 mgl 020 0500 108 90-110
licate B051049-DUP1 Source SA7S544shy
Prepared amp Analyzed 14-May-
Total Residual Chlorine 012 mgl 020 010
licate S051049-DUP2 Source SA7S602-01
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020 BRL
Matrix S ike 8051049-MS1 Source SA78544-01
Prepared amp Analyzed 14-May-
Total Residual Chlorine 065 mgl 020 0500 010 110 80- 120
Matrix S ike 8051049-MS2 Source SA7B602shy
Prepared amp Analyzed 14-May-
Total Residual Chlorine mgl 500 125 BRL 108 80- 120
Reference 8051 049-SRM1
Prepared amp Analyzed 14-May-
Total Residual Chlorine 100 mgl 020 0967 103 85-115
Batch 8051094 - General Preparation
Blank 8051094-BLK1
Prepared amp Analyzed 14 May-
Hexavalent Chromium (soluble) BRL mgl 005
Blank 8051 094-BLK2
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) BRL mgl 005
LCS 8051094-BS1
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) 054 mgl 005 90- 110
licate 8051094-DUP1 Source SA78602-01
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) BRL mgl 125 BRL
Thi laboratory report is not valid without all authorized sigllature 011 the cover page
Page 22 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Page 33
Soluble Metals by EPA 200 Series Methods - Quality Control
Analyte(s) Result Flag Units RDL
Spike
Level
Source
Result REC
REC
Limits RPD
RPD
Limit
Batch 8051152 - EPA200SW7000 Series
LCS B051152-BS1
Prepared amp Analyzed 21-May-
Mercury 00576 m91 00020 00500 115 85- 115
licate B051152-DUP1 Source SA78602-01
Prepared amp Analyzed 21-May-
Mercury BRL m91 00020 BRL
Matrix S ike 8051152-MS1 Source SA78602shy
Prepared amp Analyzed 21-May-
Mercury 00632 OM m91 00020 00500 BRL 126 75- 125
Post S ike 8051152-PS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Mercury 00624 OC1 m91 00020 00500 BRL 125 85- 115
Batch 8051249 - 2008No digestion
Blank 8051249-BLK1
Prepared amp Analyzed 21-May-
Lead
Antimony
Cadmium
Silver
BRL
BRL
BRL
BRL
m91
m91
m91
m91
0002
0002
0002
0002
LCS B051249-BS1
Prepared amp Analyzed 21-May-
Antimony
Lead
Silver
Cadmium
143
145 OC2
m91
m91
m91
m91
0050
0050
0050
0040
103
115
107
116
85- 115
85- 115
85- 115
85- 115
licate 8051249-DUP1 Source SA7B602shy
Prepared amp Analyzed 21- May-
Lead
Antimony
Cadmium
Silver
0009
0002
00005
00002
ORB
m91
m91
m91
m91
0002
0002
0002
0002
0011
0003
00005
00003
Matrix S ike 8051249-MS1 Source SA78602shy
Prepared amp Analyzed 21- May-
Lead
Antimony
Cadmium
Silver
142
m91
m91
m91
m91
0050
0050
0040
0050
0011
0003
00005
00003
111
101
114
102
70- 130
70-130
70c130
70- 130
Post S ike 8051249-PS1 Source SA78602-01
Prepared amp Analyzed 21-May-
Antimony
Cadmium
Silver
38
OC2
m91
m91
m91
0050
0040
0050
125
0003
00005
00003
110
121
109
85- 115
85- 115
85- 115
This laboratory report is flOt valid IVithout all authorized signature 011 the cOIer page
Reportable Detection Limit BRL Below Reporting Limit Page 21 of 25
General Chemistry Parameters - Quality Control
Spike Source REC RPD
Analyte( s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051049 - General Preparation
Blank S051 049-BLK1
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
Blank S051049-BLK2
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
Blank S051 049-BLK3
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
LCS S051049-BS1
Prepared amp Analyzed 14-May-
Total Residual Chlorine 046 mgl 020 0500 90- 110
LCS S051049-BS2
Prepared amp Analyzed 14-May-
Total Residual Chlorine 047 mgl 020 0500 90- 110
LCS S051049-BS3
Prepared amp Analyzed 14-May-
Total Residual Chlorine 054 mgl 020 0500 108 90-110
licate B051049-DUP1 Source SA7S544shy
Prepared amp Analyzed 14-May-
Total Residual Chlorine 012 mgl 020 010
licate S051049-DUP2 Source SA7S602-01
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020 BRL
Matrix S ike 8051049-MS1 Source SA78544-01
Prepared amp Analyzed 14-May-
Total Residual Chlorine 065 mgl 020 0500 010 110 80- 120
Matrix S ike 8051049-MS2 Source SA7B602shy
Prepared amp Analyzed 14-May-
Total Residual Chlorine mgl 500 125 BRL 108 80- 120
Reference 8051 049-SRM1
Prepared amp Analyzed 14-May-
Total Residual Chlorine 100 mgl 020 0967 103 85-115
Batch 8051094 - General Preparation
Blank 8051094-BLK1
Prepared amp Analyzed 14 May-
Hexavalent Chromium (soluble) BRL mgl 005
Blank 8051 094-BLK2
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) BRL mgl 005
LCS 8051094-BS1
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) 054 mgl 005 90- 110
licate 8051094-DUP1 Source SA78602-01
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) BRL mgl 125 BRL
Thi laboratory report is not valid without all authorized sigllature 011 the cover page
Page 22 of 25 Reportable Detection Limit BRL = Below Reporting Limit
Page 34
General Chemistry Parameters - Quality Control
Spike Source REC RPD
Analyte( s) Result Flag Units RDL Level Result REC Limits RPD Limit
Batch 8051049 - General Preparation
Blank S051 049-BLK1
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
Blank S051049-BLK2
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
Blank S051 049-BLK3
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020
LCS S051049-BS1
Prepared amp Analyzed 14-May-
Total Residual Chlorine 046 mgl 020 0500 90- 110
LCS S051049-BS2
Prepared amp Analyzed 14-May-
Total Residual Chlorine 047 mgl 020 0500 90- 110
LCS S051049-BS3
Prepared amp Analyzed 14-May-
Total Residual Chlorine 054 mgl 020 0500 108 90-110
licate B051049-DUP1 Source SA7S544shy
Prepared amp Analyzed 14-May-
Total Residual Chlorine 012 mgl 020 010
licate S051049-DUP2 Source SA7S602-01
Prepared amp Analyzed 14-May-
Total Residual Chlorine BRL mgl 020 BRL
Matrix S ike 8051049-MS1 Source SA78544-01
Prepared amp Analyzed 14-May-
Total Residual Chlorine 065 mgl 020 0500 010 110 80- 120
Matrix S ike 8051049-MS2 Source SA7B602shy
Prepared amp Analyzed 14-May-
Total Residual Chlorine mgl 500 125 BRL 108 80- 120
Reference 8051 049-SRM1
Prepared amp Analyzed 14-May-
Total Residual Chlorine 100 mgl 020 0967 103 85-115
Batch 8051094 - General Preparation
Blank 8051094-BLK1
Prepared amp Analyzed 14 May-
Hexavalent Chromium (soluble) BRL mgl 005
Blank 8051 094-BLK2
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) BRL mgl 005
LCS 8051094-BS1
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) 054 mgl 005 90- 110
licate 8051094-DUP1 Source SA78602-01
Prepared amp Analyzed 14-May-
Hexavalent Chromium (soluble) BRL mgl 125 BRL
Thi laboratory report is not valid without all authorized sigllature 011 the cover page
Page 22 of 25 Reportable Detection Limit BRL = Below Reporting Limit