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Food and Product safety Role of EU customs Laboratories 6 nov 2015 [email protected]
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Food and Product safety - Selamat · • GC-FID, quantitative NMR (internal standard), LC-DAD-MS(MS) 28. Number of violating samples 2013 & 2014 29 Category 2013 2014 Herbal supplements

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Page 1: Food and Product safety - Selamat · • GC-FID, quantitative NMR (internal standard), LC-DAD-MS(MS) 28. Number of violating samples 2013 & 2014 29 Category 2013 2014 Herbal supplements

Food and Product safety

Role of EU customs Laboratories

6 nov 2015 [email protected]

Page 2: Food and Product safety - Selamat · • GC-FID, quantitative NMR (internal standard), LC-DAD-MS(MS) 28. Number of violating samples 2013 & 2014 29 Category 2013 2014 Herbal supplements

EU Mission of customs authorities

Protecting the financial interests of the Community and its Member

States;

Protecting the Community from unfair and illegal trade while

supporting legitimate business activities;

Ensuring the security and safety of the Community and its

residents, and the protection of the environment , where

appropriate in close cooperation with other authorities;

Maintaining a proper balance between customs controls and

facilitation of legitimate trade

Page 3: Food and Product safety - Selamat · • GC-FID, quantitative NMR (internal standard), LC-DAD-MS(MS) 28. Number of violating samples 2013 & 2014 29 Category 2013 2014 Herbal supplements

Importance of import and export EU-ChinaCountry People

billionsTotalproductionUS DollarsBillions *

RatioDollars/person

ImportEU from Chinaeuros**Billions

ExportEU toChinaeuros**Billions

China 1.40 10400 7400 302(food 2 %)

165(food 4.7 %)

EU 0.508 18500 36400

USA 0.317 17600 55520

Netherlands 0.0168 866 51500

Norway 0,00516 511 99147

12 november 2015

• * Data IMF 2014

• ** Data EU DG trade 2014

Page 4: Food and Product safety - Selamat · • GC-FID, quantitative NMR (internal standard), LC-DAD-MS(MS) 28. Number of violating samples 2013 & 2014 29 Category 2013 2014 Herbal supplements

EU trade with China

Indicator Unit Period Imports Exports

Last year BillionsEuros

2014 302 165

Rank as EU partner 2014 1 2*

Share in EU trade % 2014 17.9 9.7

Annual growth rate % 2013-2014 7.8 11.2

Annual averagegrowth rate

% 2010-2014 1.6 9.8

12 november 2015

•Data EU DG trade 2014

•* EU biggest exporter to China

Page 5: Food and Product safety - Selamat · • GC-FID, quantitative NMR (internal standard), LC-DAD-MS(MS) 28. Number of violating samples 2013 & 2014 29 Category 2013 2014 Herbal supplements

12 november 2015

Page 6: Food and Product safety - Selamat · • GC-FID, quantitative NMR (internal standard), LC-DAD-MS(MS) 28. Number of violating samples 2013 & 2014 29 Category 2013 2014 Herbal supplements
Page 7: Food and Product safety - Selamat · • GC-FID, quantitative NMR (internal standard), LC-DAD-MS(MS) 28. Number of violating samples 2013 & 2014 29 Category 2013 2014 Herbal supplements

Testen

L 226

Customs Laboratory

Page 8: Food and Product safety - Selamat · • GC-FID, quantitative NMR (internal standard), LC-DAD-MS(MS) 28. Number of violating samples 2013 & 2014 29 Category 2013 2014 Herbal supplements

Customs Laboratory

Amsterdam

62 fte

• Three Chemical Departments

• Department of Quality and ICT

• Department of Support

14000 Samples a year

Quality system

• Accreditation according ISO 17025 since 1995

Page 9: Food and Product safety - Selamat · • GC-FID, quantitative NMR (internal standard), LC-DAD-MS(MS) 28. Number of violating samples 2013 & 2014 29 Category 2013 2014 Herbal supplements

Testen

L 226

Page 10: Food and Product safety - Selamat · • GC-FID, quantitative NMR (internal standard), LC-DAD-MS(MS) 28. Number of violating samples 2013 & 2014 29 Category 2013 2014 Herbal supplements

Testen

L 226

Page 11: Food and Product safety - Selamat · • GC-FID, quantitative NMR (internal standard), LC-DAD-MS(MS) 28. Number of violating samples 2013 & 2014 29 Category 2013 2014 Herbal supplements

Testen

L 226

Page 12: Food and Product safety - Selamat · • GC-FID, quantitative NMR (internal standard), LC-DAD-MS(MS) 28. Number of violating samples 2013 & 2014 29 Category 2013 2014 Herbal supplements

Testen

L 226

Page 13: Food and Product safety - Selamat · • GC-FID, quantitative NMR (internal standard), LC-DAD-MS(MS) 28. Number of violating samples 2013 & 2014 29 Category 2013 2014 Herbal supplements

Testen

L 226

Page 14: Food and Product safety - Selamat · • GC-FID, quantitative NMR (internal standard), LC-DAD-MS(MS) 28. Number of violating samples 2013 & 2014 29 Category 2013 2014 Herbal supplements

Testen

L 226

Customs Laboratory

Page 15: Food and Product safety - Selamat · • GC-FID, quantitative NMR (internal standard), LC-DAD-MS(MS) 28. Number of violating samples 2013 & 2014 29 Category 2013 2014 Herbal supplements

Principles Customs Administration

• Strengthening of the EU external border

• Fewer logistic delays

• Cooperation with the business community and

colleague enforcement services

• Risk Management: risk analysis and more extensive intelligence

Page 16: Food and Product safety - Selamat · • GC-FID, quantitative NMR (internal standard), LC-DAD-MS(MS) 28. Number of violating samples 2013 & 2014 29 Category 2013 2014 Herbal supplements

Procedures

In the country of origin:

• Food is checked by the health authorities of the country of origin.

• The country of origin provides a health certificate for the goods

• This certificate is necessary to enter the EU with the goods

Page 17: Food and Product safety - Selamat · • GC-FID, quantitative NMR (internal standard), LC-DAD-MS(MS) 28. Number of violating samples 2013 & 2014 29 Category 2013 2014 Herbal supplements

Food from non-veterinary origin for human consumption

Page 18: Food and Product safety - Selamat · • GC-FID, quantitative NMR (internal standard), LC-DAD-MS(MS) 28. Number of violating samples 2013 & 2014 29 Category 2013 2014 Herbal supplements

Food from veterinary origin for human consumption

Page 19: Food and Product safety - Selamat · • GC-FID, quantitative NMR (internal standard), LC-DAD-MS(MS) 28. Number of violating samples 2013 & 2014 29 Category 2013 2014 Herbal supplements

Feed from non-veterinary origin for animals

Page 20: Food and Product safety - Selamat · • GC-FID, quantitative NMR (internal standard), LC-DAD-MS(MS) 28. Number of violating samples 2013 & 2014 29 Category 2013 2014 Herbal supplements

Process steps declaration

•20 •

• Entry summary declaration (ENS)• Risk analysis and selection• Electronic Pre notification of manifest data (48 hours before

arriving of vessel)• Electronic summarized declaration (SAL)• Risk analyses en selection

Page 21: Food and Product safety - Selamat · • GC-FID, quantitative NMR (internal standard), LC-DAD-MS(MS) 28. Number of violating samples 2013 & 2014 29 Category 2013 2014 Herbal supplements

Procedures

In the EU:

• 24 hours before arrival of the goods, the arrival must be notified in

the system of the Netherland Food- and Product Safety Authority

(NVWA)

• Comparison with the Customs system tells us if all of the food is

notified by the importers

• If not, the NVWA will be informed by the Customs

• All of the notified goods are included in the risk assessment and part

will be further checked by the NVWA and/or Customs

Page 22: Food and Product safety - Selamat · • GC-FID, quantitative NMR (internal standard), LC-DAD-MS(MS) 28. Number of violating samples 2013 & 2014 29 Category 2013 2014 Herbal supplements

Three sorts of inspections

• Documentary checks (Customs)

• Identity checks (food and product safety authority)

• Physical checks (food and product safety authority)

6 november 2015

Page 23: Food and Product safety - Selamat · • GC-FID, quantitative NMR (internal standard), LC-DAD-MS(MS) 28. Number of violating samples 2013 & 2014 29 Category 2013 2014 Herbal supplements

Regulations

The basic regulation is regulation 2002/178

• General principles and requirements of food law

• Establishing the European Food and Safety Authority (EFSA)

• Rapid Alert System

• Laying down procedures in matters of food safety

• Emergency measures for food and feed of Community

origin or imported from a third country (example: Fukushima)

Page 24: Food and Product safety - Selamat · • GC-FID, quantitative NMR (internal standard), LC-DAD-MS(MS) 28. Number of violating samples 2013 & 2014 29 Category 2013 2014 Herbal supplements

Regulations

Regulation 2004/882:

• On official controls performed to ensure the verification of compliance with feed and food law, animal health and animal welfare rules.

• Gives the rules to work with the basic principles of Regulation 2002/178 (Control systems of the NVWA like VGC/CLIENT)

Page 25: Food and Product safety - Selamat · • GC-FID, quantitative NMR (internal standard), LC-DAD-MS(MS) 28. Number of violating samples 2013 & 2014 29 Category 2013 2014 Herbal supplements

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Role EU-Customs Laboratories in food inspection

• For Customs Laboratories no specific task in Food Safety

• Dangerous foods encountered however in control of Medicines Act

- Food Supplements declared to contain pharmaceutical substances

- “Food Supplements” adulterated with pharmaceutical substances – predominantly herbal preparations

- Foods (coffee, tea, drinks) adulterated with pharmaceutical substances

Page 26: Food and Product safety - Selamat · • GC-FID, quantitative NMR (internal standard), LC-DAD-MS(MS) 28. Number of violating samples 2013 & 2014 29 Category 2013 2014 Herbal supplements

Role of the EU Customs Laboratoriesfood supplements

Page 27: Food and Product safety - Selamat · • GC-FID, quantitative NMR (internal standard), LC-DAD-MS(MS) 28. Number of violating samples 2013 & 2014 29 Category 2013 2014 Herbal supplements

Examples

Food supplements

• energy boosters – DMAA, stimulants

• cognitive /mood enhancers – vinpocetine, nootropics

• muscle growth – levodopa, designer steroids,

• relaxants – melatonin, picamilon

Herbal supplements and foods

• sexual stimulants (sildenafil, tadalafil, dapoxetine, ..)

• slimming products (sibutramine, phenolphthalein, spironolactone, fluoxetine, ..)

27

Page 28: Food and Product safety - Selamat · • GC-FID, quantitative NMR (internal standard), LC-DAD-MS(MS) 28. Number of violating samples 2013 & 2014 29 Category 2013 2014 Herbal supplements

Analytical techniques

Active Pharmaceutical Ingredient (API) identification

• Mainly GCMS, ESI-MSMS, FTIR, NMR

• XRF, optical rotation, APCI-MSMS, TGA,

Quantification of API’s

• required for determination of legislation (Medicines Act versus Warenwet)

• GC-FID, quantitative NMR (internal standard), LC-DAD-MS(MS)

28

Page 29: Food and Product safety - Selamat · • GC-FID, quantitative NMR (internal standard), LC-DAD-MS(MS) 28. Number of violating samples 2013 & 2014 29 Category 2013 2014 Herbal supplements

Number of violating samples 2013 & 2014

29

Category 2013 2014

Herbal supplements & foods 101 (216.400 units) 50

Food Supplements 59 (568.000 units) 24

Page 30: Food and Product safety - Selamat · • GC-FID, quantitative NMR (internal standard), LC-DAD-MS(MS) 28. Number of violating samples 2013 & 2014 29 Category 2013 2014 Herbal supplements

Food safety

• Additives

• Food Contaminants• Heavy metals

• 3-MCPD

• Acrylamide

• Mycotoxins

• PAH compounds

• Furan

• Nitrate

• Phthalate

• Solvents

• Pesticide residues

• Food contact materials

• Food crimes

• Microbes

• Genetically Modified Organisms in food (GMO)

• Use of radiation

• Labelling

• Added vitamins

• Composition, novelty food

• Health claims

• Radioactivity

• Allergens

Finnish Customs LaboratoryKalevi Siivinen 30

Page 31: Food and Product safety - Selamat · • GC-FID, quantitative NMR (internal standard), LC-DAD-MS(MS) 28. Number of violating samples 2013 & 2014 29 Category 2013 2014 Herbal supplements

Finnish Customs Laboratory, EU national reference laboratory

Vegetables, fruits, cereals :

– pesticide

– heavy metals

– mycotoxins

– GMO

– food contact materials

Kalevi Siivinen Finnish Customs Laboratory 31

Page 32: Food and Product safety - Selamat · • GC-FID, quantitative NMR (internal standard), LC-DAD-MS(MS) 28. Number of violating samples 2013 & 2014 29 Category 2013 2014 Herbal supplements

Food Samples Non-complying Notified Non-complying +

Notified

Import 3. country 1299 169 13.0 % 141 10.9 % 310 19.0 %

Internal market 2030 113 5.6 % 189 9.3 % 302 14.9 %

Total 3329 282 8.5% 330 9.9 % 612 18.4 %

Consumer goods Samples Non-complying Notified Non-complying +

Notified

Import 3. country 2125 203 9.6 % 205 9.6 % 408 19.2 %

Internal market 322 28 8.7 % 50 15.5 % 78 24.2 %

Total 2447 231 9.5 % 255 10.4 % 486 19.9 %

Kalevi Siivinen Finnish Customs Laboratory 32

Results 2014

Page 33: Food and Product safety - Selamat · • GC-FID, quantitative NMR (internal standard), LC-DAD-MS(MS) 28. Number of violating samples 2013 & 2014 29 Category 2013 2014 Herbal supplements

Foods examined in Finnish Customs Laboratory 2014

Finnish Customs LaboratoryKalevi Siivinen 33

Food categoryNumber of

lotsRejected

Rejected

%

Fruit, berries and vegetables 1376 67 4,9

Nuts and almonds 176 9 5,1

Processed foods (soups, broths, canned,

candies, juices etc.) 566 53 9,4

Cereals and bakery products 324 23 7,1

Spices and seasonings 224 37 16,5

Tea, coffee, cocoa 187 29 15,5

Food supplements, baby food, special diets 209 35 16,7

Other 267 29 10,9

Total 3329 282 8,5

Page 34: Food and Product safety - Selamat · • GC-FID, quantitative NMR (internal standard), LC-DAD-MS(MS) 28. Number of violating samples 2013 & 2014 29 Category 2013 2014 Herbal supplements

Finnish Customs LaboratoryKalevi Siivinen 34

Page 35: Food and Product safety - Selamat · • GC-FID, quantitative NMR (internal standard), LC-DAD-MS(MS) 28. Number of violating samples 2013 & 2014 29 Category 2013 2014 Herbal supplements

Consumer goods examined in Finnish Customs Laboratory 2014

Finnish Customs Laboratory

Samples Rejected Rejected %

Tableware, food contact

material

665 31 4.7

Toys 815 109 13.4

Textiles 491 26 5.3

Articles used in direct

contact with the skin

(nickel-test)

192 17 8.9

Cosmetics 144 34 23.6

Others 140 14 10.3

Total 2447 231 9.4

Kalevi Siivinen 35

Page 36: Food and Product safety - Selamat · • GC-FID, quantitative NMR (internal standard), LC-DAD-MS(MS) 28. Number of violating samples 2013 & 2014 29 Category 2013 2014 Herbal supplements

Conclusions

6 november 2015 [email protected]

EU Customs and EU Food Inspection Authorities perform the food and feed inspection together

EU Food Inspection laboratories do the majority of the chemical analyses

EU Customs Laboratories have a specific role in the control of food supplements and control of medicines act

All EU Customs Laboratories are member of the CLEN (Customs Laboratories European Network)

Page 37: Food and Product safety - Selamat · • GC-FID, quantitative NMR (internal standard), LC-DAD-MS(MS) 28. Number of violating samples 2013 & 2014 29 Category 2013 2014 Herbal supplements

Thank you for your attention

[email protected]