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First Results from Thermal Kinetic Inductance Detectors: Highly Multiplexible Bolometric MKIDs for X-ray Spectroscopy G. Ulbricht, B.A. Mazin, P. Szypryt, A. B. Walter, C. Bockstiegel Department of Physics, University of California, Santa Barbara, CA 93106, USA LTD-16, Grenoble, July 21, 2015 Thermal Kinetic Inductance Detectors for X-Ray Spectroscopy G. Ulbricht, B.A. Mazin, P. Szypryt, A. B. Walter, C. Bockstiegel
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First Results from Thermal Kinetic Inductance Detectors ...

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Page 1: First Results from Thermal Kinetic Inductance Detectors ...

First Results from

Thermal Kinetic Inductance Detectors:

Highly Multiplexible Bolometric

MKIDs for X-ray Spectroscopy

G. Ulbricht, B.A. Mazin, P. Szypryt, A. B. Walter, C. Bockstiegel

Department of Physics, University of California, Santa Barbara, CA 93106, USA

LTD-16, Grenoble, July 21, 2015

Thermal Kinetic Inductance Detectors for X-Ray Spectroscopy G. Ulbricht, B.A. Mazin, P. Szypryt, A. B. Walter, C. Bockstiegel

Page 2: First Results from Thermal Kinetic Inductance Detectors ...

Thermal Kinetic Inductance Detectors for X-Ray Spectroscopy G. Ulbricht, B.A. Mazin, P. Szypryt, A. B. Walter, C. Bockstiegel

Why TKIDs for X-ray detection?

TKIDs

Thermal Kinetic Inductance Detectors (TKIDs):

· single pixel energy resolution an utilize frequency domain multiplexing

· usable in a big energy / wavelength range

· can utilize frequency domain multiplexing

· no read noise

· ……… promising as

X-ray detectors!

TKID vs. TES:

TES: · impressive energy resolution

· high time resolution

· multiplexing is complex and

challenging

TKID: · comparable time resolution

· much easier to multiplex

· energy resolution: …..

ideal where spatial resolution is required!

Page 3: First Results from Thermal Kinetic Inductance Detectors ...

Thermal Kinetic Inductance Detectors for X-Ray Spectroscopy G. Ulbricht, B.A. Mazin, P. Szypryt, A. B. Walter, C. Bockstiegel

TKID design

TKIDs

Many X-ray photons would penetrate the

superconductor

Microcalorimeter: inductor & absorber on

a free floating Si3N4 membrane

Page 4: First Results from Thermal Kinetic Inductance Detectors ...

Thermal Kinetic Inductance Detectors for X-Ray Spectroscopy G. Ulbricht, B.A. Mazin, P. Szypryt, A. B. Walter, C. Bockstiegel

TKIDs

TKID design

: sub-stoichiometric TiNx

Many X-ray photons would penetrate the

superconductor

Microcalorimeter: inductor & absorber on

a free floating Si3N4 membrane

Page 5: First Results from Thermal Kinetic Inductance Detectors ...

Thermal Kinetic Inductance Detectors for X-Ray Spectroscopy G. Ulbricht, B.A. Mazin, P. Szypryt, A. B. Walter, C. Bockstiegel

TKIDs

TKID design

: sub-stoichiometric TiNx

: Si3N4 (etched with XeF2)

Many X-ray photons would penetrate the

superconductor

Microcalorimeter: inductor & absorber on

a free floating Si3N4 membrane

Page 6: First Results from Thermal Kinetic Inductance Detectors ...

Thermal Kinetic Inductance Detectors for X-Ray Spectroscopy G. Ulbricht, B.A. Mazin, P. Szypryt, A. B. Walter, C. Bockstiegel

TKIDs

TKID design

: sub-stoichiometric TiNx

: Si3N4 (etched with XeF2)

: absorber (Ta or Au)

Many X-ray photons would penetrate the

superconductor

Microcalorimeter: inductor & absorber on

a free floating Si3N4 membrane

Page 7: First Results from Thermal Kinetic Inductance Detectors ...

Thermal Kinetic Inductance Detectors for X-Ray Spectroscopy G. Ulbricht, B.A. Mazin, P. Szypryt, A. B. Walter, C. Bockstiegel

TKIDs

TKID design

: sub-stoichiometric TiNx

: Si3N4 (etched with XeF2)

: absorber (Ta or Au)

Many X-ray photons would penetrate the

superconductor

Microcalorimeter: inductor & absorber on

a free floating Si3N4 membrane

Page 8: First Results from Thermal Kinetic Inductance Detectors ...

Thermal Kinetic Inductance Detectors for X-Ray Spectroscopy G. Ulbricht, B.A. Mazin, P. Szypryt, A. B. Walter, C. Bockstiegel

TKIDs

TKID design

: sub-stoichiometric TiNx

: Si3N4 (etched with XeF2)

: absorber (Ta or Au)

: Nb feedline & ground plane

Mushroom shaped absorbers planned,

current simple absorbers just to reduce

prototype complexity.

Bridges: 0.25 x 2 µm2 cross section

140 µm long

Page 9: First Results from Thermal Kinetic Inductance Detectors ...

Thermal Kinetic Inductance Detectors for X-Ray Spectroscopy G. Ulbricht, B.A. Mazin, P. Szypryt, A. B. Walter, C. Bockstiegel

Single photon pulses

Data analysis

Page 10: First Results from Thermal Kinetic Inductance Detectors ...

Thermal Kinetic Inductance Detectors for X-Ray Spectroscopy G. Ulbricht, B.A. Mazin, P. Szypryt, A. B. Walter, C. Bockstiegel

Single photon pulses

Data analysis

Page 11: First Results from Thermal Kinetic Inductance Detectors ...

Thermal Kinetic Inductance Detectors for X-Ray Spectroscopy G. Ulbricht, B.A. Mazin, P. Szypryt, A. B. Walter, C. Bockstiegel

Analysing max. pulse height doesn’t work.

Data analysis

140 150 160pulse max. [degrees]

no

. o

f e

ve

nts

140 150 160pulse max. [degrees]

no

. o

f e

ve

nts

pulse maximum [degrees]

Page 12: First Results from Thermal Kinetic Inductance Detectors ...

Thermal Kinetic Inductance Detectors for X-Ray Spectroscopy G. Ulbricht, B.A. Mazin, P. Szypryt, A. B. Walter, C. Bockstiegel

Data analysis

Pulse rise time depends on absorption location.

Page 13: First Results from Thermal Kinetic Inductance Detectors ...

Thermal Kinetic Inductance Detectors for X-Ray Spectroscopy G. Ulbricht, B.A. Mazin, P. Szypryt, A. B. Walter, C. Bockstiegel

Why fit pulses?

Pulse fitting

Page 14: First Results from Thermal Kinetic Inductance Detectors ...

Thermal Kinetic Inductance Detectors for X-Ray Spectroscopy G. Ulbricht, B.A. Mazin, P. Szypryt, A. B. Walter, C. Bockstiegel

Pulse fitting

Why fit pulses?

Page 15: First Results from Thermal Kinetic Inductance Detectors ...

Thermal Kinetic Inductance Detectors for X-Ray Spectroscopy G. Ulbricht, B.A. Mazin, P. Szypryt, A. B. Walter, C. Bockstiegel

Pulse fitting

Why fit pulses?

free parameters in pulse model: photon arrival time rise time

fall time max. membrane temperature

Page 16: First Results from Thermal Kinetic Inductance Detectors ...

Thermal Kinetic Inductance Detectors for X-Ray Spectroscopy G. Ulbricht, B.A. Mazin, P. Szypryt, A. B. Walter, C. Bockstiegel

Pulse model: resonance frequency over T

Pulse fitting

Page 17: First Results from Thermal Kinetic Inductance Detectors ...

Thermal Kinetic Inductance Detectors for X-Ray Spectroscopy G. Ulbricht, B.A. Mazin, P. Szypryt, A. B. Walter, C. Bockstiegel

Pulse model: phase shift over frequency

Pulse fitting

as measured

after feedline subtraction

Page 18: First Results from Thermal Kinetic Inductance Detectors ...

Thermal Kinetic Inductance Detectors for X-Ray Spectroscopy G. Ulbricht, B.A. Mazin, P. Szypryt, A. B. Walter, C. Bockstiegel

Pulse model: assumed temperature behaviour

Pulse fitting

Page 19: First Results from Thermal Kinetic Inductance Detectors ...

Thermal Kinetic Inductance Detectors for X-Ray Spectroscopy G. Ulbricht, B.A. Mazin, P. Szypryt, A. B. Walter, C. Bockstiegel

Pulse fitting

Pulse model: assumed temperature behaviour

Page 20: First Results from Thermal Kinetic Inductance Detectors ...

Thermal Kinetic Inductance Detectors for X-Ray Spectroscopy G. Ulbricht, B.A. Mazin, P. Szypryt, A. B. Walter, C. Bockstiegel

Pulse fitting

Pulse model: assumed temperature behaviour

Page 21: First Results from Thermal Kinetic Inductance Detectors ...

Thermal Kinetic Inductance Detectors for X-Ray Spectroscopy G. Ulbricht, B.A. Mazin, P. Szypryt, A. B. Walter, C. Bockstiegel

Pulse model construction

Pulse fitting

base temperature

increased temperature

Page 22: First Results from Thermal Kinetic Inductance Detectors ...

Thermal Kinetic Inductance Detectors for X-Ray Spectroscopy G. Ulbricht, B.A. Mazin, P. Szypryt, A. B. Walter, C. Bockstiegel

Pulse fitting

Pulse model construction

Page 23: First Results from Thermal Kinetic Inductance Detectors ...

Resolution of 75 eV at 5.9 keV, despite significant design flaws in first TKID prototype

Thermal Kinetic Inductance Detectors for X-Ray Spectroscopy G. Ulbricht, B.A. Mazin, P. Szypryt, A. B. Walter, C. Bockstiegel

Energy resolution still restrained by saturation

Achieved energy resolution

Page 24: First Results from Thermal Kinetic Inductance Detectors ...

Thermal Kinetic Inductance Detectors for X-Ray Spectroscopy G. Ulbricht, B.A. Mazin, P. Szypryt, A. B. Walter, C. Bockstiegel

Resonator saturation

Interaction between thermal design and critical temperature

Page 25: First Results from Thermal Kinetic Inductance Detectors ...

Thermal Kinetic Inductance Detectors for X-Ray Spectroscopy G. Ulbricht, B.A. Mazin, P. Szypryt, A. B. Walter, C. Bockstiegel

Resonator saturation

Interaction between thermal design and critical temperature

Page 26: First Results from Thermal Kinetic Inductance Detectors ...

Thermal Kinetic Inductance Detectors for X-Ray Spectroscopy G. Ulbricht, B.A. Mazin, P. Szypryt, A. B. Walter, C. Bockstiegel

Resonator sensitivity

Resonator saturation

Page 27: First Results from Thermal Kinetic Inductance Detectors ...

Thermal Kinetic Inductance Detectors for X-Ray Spectroscopy G. Ulbricht, B.A. Mazin, P. Szypryt, A. B. Walter, C. Bockstiegel

Wrong thermal design

Resonator saturation

too small heat capacity ΔTmembrane = 150 – 200 mK

Page 28: First Results from Thermal Kinetic Inductance Detectors ...

Thermal Kinetic Inductance Detectors for X-Ray Spectroscopy G. Ulbricht, B.A. Mazin, P. Szypryt, A. B. Walter, C. Bockstiegel

Wrong thermal design + high sensitivity = saturation

Resonator saturation

Simple extrapolation: We should be able to resolve

below 10 eV at 5.9 keV by eliminating saturation.

Page 29: First Results from Thermal Kinetic Inductance Detectors ...

Thermal Kinetic Inductance Detectors for X-Ray Spectroscopy G. Ulbricht, B.A. Mazin, P. Szypryt, A. B. Walter, C. Bockstiegel

How to eliminate saturation?

eliminating saturation:

reduce Qi:

reduces best achievable resolution

increase TiNx Tc:

reduces best achievable resolution

reduces heat capacity

increase measurement temperature:

already near upper limit

increases noise

reduce membrane heat capacity:

issues with Au absorber but

reduces best achievable resolution

…..

measure below resonance frequency:

Resonator saturation

Page 30: First Results from Thermal Kinetic Inductance Detectors ...

eliminating saturation:

reduce Qi:

reduces best achievable resolution

increase TiNx Tc:

reduces best achievable resolution

reduces heat capacity

increase measurement temperature:

already near upper limit

increases noise

reduce membrane heat capacity:

issues with Au absorber but

reduces best achievable resolution

…..

measure below resonance frequency:

Thermal Kinetic Inductance Detectors for X-Ray Spectroscopy G. Ulbricht, B.A. Mazin, P. Szypryt, A. B. Walter, C. Bockstiegel

How to eliminate saturation?

Resonator saturation

Page 31: First Results from Thermal Kinetic Inductance Detectors ...

Thermal Kinetic Inductance Detectors for X-Ray Spectroscopy G. Ulbricht, B.A. Mazin, P. Szypryt, A. B. Walter, C. Bockstiegel

Measurement below resonance.

driving a TKID below resonance frequency:

Resonator saturation

Page 32: First Results from Thermal Kinetic Inductance Detectors ...

Thermal Kinetic Inductance Detectors for X-Ray Spectroscopy G. Ulbricht, B.A. Mazin, P. Szypryt, A. B. Walter, C. Bockstiegel

No longer saturated but still high sensitivity.

Resonator saturation

Page 33: First Results from Thermal Kinetic Inductance Detectors ...

Thermal Kinetic Inductance Detectors for X-Ray Spectroscopy G. Ulbricht, B.A. Mazin, P. Szypryt, A. B. Walter, C. Bockstiegel

More challenging data analysis.

Work in progress.

Δf = 0 kHz Δf = -140 kHz

Δf = -540 kHz Δf = -340 kHz

Page 34: First Results from Thermal Kinetic Inductance Detectors ...

Thermal Kinetic Inductance Detectors for X-Ray Spectroscopy G. Ulbricht, B.A. Mazin, P. Szypryt, A. B. Walter, C. Bockstiegel

Many thanks to:

Everybody involved

Mazin group at UCSB:

Ben Mazin

Seth Meeker Matt Strader

Paul Szypryt Alex Walter Clint Bockstiegel

Giulia Collura

Page 35: First Results from Thermal Kinetic Inductance Detectors ...

Thermal Kinetic Inductance Detectors for X-Ray Spectroscopy G. Ulbricht, B.A. Mazin, P. Szypryt, A. B. Walter, C. Bockstiegel