FINAL REPORT [MARGINALIA] · 2020. 12. 3. · ~ Cambridge Analytical Associates ~ 1106 Commonwealth Avenue I Boston, Massachusetts 02215/ (817) 232-2207 FINAL REPORT u.s. Env1 ronmental

~ Cambridge Analytical Associates ~ 1106 Commonwealth Avenue I Boston , Massachusetts 02215/ (817) 232-2207

FINAL REPORT

u.s. Env1 ronmental Protect1 on Agency Regton I

60 Westview Street Lexi ngton, MA. 02172

Attn: Ms . Mary Jane Mactejko

PROJECT NUMBER :

CUSTOMER ORDER NIJ4BER: S1D2S6 NNJA "';.i..-

REPORT NIJ4BER: 84-1478

PREPARED BY : Oavfd L. Fi est

DATE PREPARED: February 28, 198S

l> 0 :r HJ: zo HO u>o -<:r :00 l>Z -<o HO < ,.,,

0 :oz "'" 0

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~ ~ Cambridge Analytical Associates

TABLE OF CONTENTS

I. INTROOUCTION

2. ANALYTICAl METHOOS

J 3. RESULTS

4. QUALITY ASSURANCE OOCUMENTATION

Cert1f1catton

1. INTRODUCT ION

This report s1.11111arizes results of chemical analyses performed on sampl es received by CAA on December 18, 1984. Analytical methods employed

for these analyses are described in Sect ton 2 and results are presented in

Section 3. The last section contains certtftcattons supporti ng the

analytical results.

2. ANALYTICAL METHOOS

Analytical Mthods uttltzed for s111ple analysts are sUI'MIIartzed tn

Toblo I.

3. RESULTS

Results of analyses are presented tn Table 2, 3, and 4. Quality

control results are reported tn Table 5.

,. 0

" H:I: zo HO <1>0

""'" :00 l> Z -< o :: o "'" 0 :oz mo 0 0

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I I I I

Table 1. SU!IIIIary of Organic Analytical Methods

Const 1 tuent Method Reference Method Description

Volati le Method 624 (I) Purge and trap . gas Organi c chromatography/mass Compounds spectr0111etry

Smi volat tl e Method 8270 (2) Solvent ext racti on , Organics · capfll ary gas Acid/ Base/ Neut ral chroutography/111155 Extractabl es spectr0111etry

Pest tctdos/PC8s Method 608 (I) SOlvent extraction. gas chro.atography/electron capture detection

(l)~;.:·~~:~;t~r:~· _.::::::.~~r tUAg6&17.~~~6s;~ ~PA}~t o~,:~1!~!rt~ Ohio.

(2)U.S. EPA. 1982. Test Methods for Evaluating Soltd Wasto­Phxsfcal/ChMica1 MethOds. Sicona Ed1t1on. SW-846. Office of Solid Waste. U.S. EPA. Washington, D. C.

I I

.. I I

.I Jill 1 .. =1"1 . 'rr'•

( It ~·I f~"(l

1; "' ~J: zo ~n V>O -<:< " O l> Z -< n ~ o

<

"'" 0 "Z "' O n

~

I

Client : EPA~Ion I CM Proj.ct No. : 84~1471

-· S.,l• 101 CM 10:

en cntor~NM

121 ""-tMM Ul ¥111!1 cfllorlde C41 cfltoro.thene

~51 ..n lene chloride

~cfltorOIIfllyt ... ,,, .. lctll~

Cll trlfla-t,Miclltoro.tl'lyt-.

'" cblorofor-CIOI I,MICfll~ em 1,1,t•trlctllorM1'NM

1121 ~bon t.tr~~eltloriM em llr'.-.dlctlt~

(IU .crytOflltrlll IISJ ecrol•ln (Ill 1,2-odlctll~--

em tn••a-1,3-dlclllor~

1111 trldlloroetllyl-(191 chtorocllbr~t'NN

UOI 1,t,2=trtc:tltoroetNM

~ ~::~ r­"--r~ "::'1---

CAMf!A IOGE ANALYTICAL ASSOCIATES, tiC~ U

..... ,., 1408148

Dlte S.ples Recelved 1 ~ 11, 19M Olte An•lytla Oc.pletech O.C.ber 22, 1984

Conc:.ntntlon - ug/1 lppbl

....... 8401151

1211 benzene mceot TRC901 _ 1221C:II•I,~Iclllor~ ffi)z:chi;o;ih;j;~;;;..---------------------------

n;r~;a---------

I:HI 1,1,2,2-'tltr.cl'ltoro.tf\WMI 1261 "tnchlor-o.tllyt.,. • 1271 toi...M ...

TRI401 ... TRI601

'"' __ TRUC)) TRUOI

I~ -· -~-1Co~~cMtr•tlont tnt thn the d•tec:tiOtl tl•lt .... l•tt biMk, Conc.tntlont bet-n I •nd 10 tl- the dltiiCt lon l l•lt ere listed 11 tree• ,..,.,,,Inti. O.tectlon ll•ltt tor ec:roleln ar~d •crylonltrll• •r• 100 ..,d 10 tl ... th• ~INI tMt-=tlon 11•1t ru,.etlv•ly.

l> 0

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"'" 0 :oz ~0

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8 ..

CAMBRIDGE .v!AL'I'TICAL ASSOCIATES, IPC,

Cll.,.t1 EPA Region I CM Pl"oj.ct No,: 84·1478

O.te S..pl•• ReceiYedl O.O.bef' 18, 19&4 O.te An•lyll l C:O.pleted: Dlc•bef' 22, 19&4

S.ple ID: CM ID:

tO clllor .. thene

Conc:entntlon a ugfl lppbl

Mil• II 8408152

*·IOO 84081,

iirbr~-------------------------------­

rn-~-----------------------

IU cl'lloroethane

Ul •tl'lyle~~e cl'llorlde --------------------·-----1)!•1-41cflloroetl'lyten. --------------------------._.LL_..!.Iaflcl'lloroefl\efte

tiJ tre~~s-1,2-dlcl'lloroetl'lyl--~~~~~~~~-~-~-~~~~~~~~~~~~~~~~~ C9J cl'llorotcww IIOJ 1,2-dlcllloroe~--- -------

1111 l,l,l*"'lci'IICW"'etMMI--------==------==--=---==--== iiz1 crbon tetr.cl'llorlde 1131 bt"a.dlcftiOI"''MMttl•iie------==:.:::..=:__ _____________ _

ll!LKryiOI'IItrlle ----------- -----------1151 KrO!eln iii)i;i:iiChi"oropropaine 117) trM~s•l,3-dlchloroprop;;;···------·----·-----------·----­~~Chi'Qroettlyieft.-----·-----------------------

1 191 cl'llorodlbt'c.:.~t"-M

i20T'~oroei~n• 121) benzene iiiiCis:i;-~ior~----------------------------· iHIT-chl~~-----,.-------------·-----

~or;---- --··- -------------(2,, 1,1,2,2•tetrecl'lloroetllene - ··---------i2i)i;;r~'thYI.;---------ffi)Tol _______________________________ _

m;-~---------------------

m;-~~--==--=--========------------------1301 tot•! xyten.. TR!401

~~-·- =-==~==-------=-===.-::-no--===-=- -- -:::. -= · -- o.tec:tiOn-u;;;-:-_-:::::::::==:-.: _____ _:It-::-_-:==::..~-==

1eonc:entr•tlons less th•n tt••• dstectlon liMit sre left bl•nk. Concentr•tlons bet- I •nd 10 tl•e• the detection liMit.,.. listed •• trec:e leotels (TJII, O.t.ctlon liMits for ec:roleln and .c:rytonltrlle .,.. 100 •nd 10 tl ... the no-Ins I detection liMit r .. peet!Yely,

~ 0 :r H:l: zo HO <1>0 -<:r :00 ~z -<0 HO < ""' 0 :oz mo 0 0

"' 0

CAMBRIDGE ANALYTICAL ASSOCIATES, tiC.

Teble 2 Ccont 1d). Conc.ntretlont of Priority Pol lut1nt Vol1tlle Org1nlc Collpounds C~tttod 624)

Cll•t : EPA~Ion I CM ProJect No, : 14-1471

Sellple ID : CM ID:

Cll chlot"a.tfWII C21 --(]) vllllcttlor1de ... chloroetMM

"' -"'!'..,. clllorlde

J ~:::::::=. .... ... trelt ... 1,2-dlcti!Of"''etttyt-Ill ctllorotOI"'I C10) 1 ~lctiiOI"''e1'MMIe em 111•tl"lcfll~

ctn crtlolltetrectllorl• If)) ~lc:IIIO!"'a.e"'-

C14) 1Ct'l0111trfle em ecntll111 Cl6) 1,2-dlctlloropi"''P<<• {17) ,,. ...... 1,)-dlctlloropf'Oplrll Cll) trlctllot'Oittlyt .... {19) ctllorodl~llll

"'" 1,1 ,2•trlctllor"'t'ttleM {21)

... _ C221 cl .... l,)..cllchloropf"091M {2)) 2<tllot'Oittlylw111ytettllr' {24) ......... "" 1,1 2, 2•tetractlloroettlllle ,,., tetr.chloroethyiiM (27) tol~~~n~

"" ctll~z.,.

1291 lffl !benzene UOI totll 11 lenes

Dlte s. • .,, .. Rt>c. lwed : O.C.ber a, 1984 O.te Anllyth Collpletld : o.c.ber 22, 1984

ConC~t~tretlon ... ugfl hpb)

Sl~trt.Splke

8408141NS

.,.

••• ...

Anelytlc.IBienk 84ott4a a

1eoncentntlont IMI ttlen the detection ll•lt ere left blenk. ConC~t~tretlons betlfNII I 1nd ID ""' tt11 detection ll•lt .,.. listed •• t ree• , ..... ,. cnu. DltectiOI'I ll•lts tor .cro leln and ecry!Oflltrlll .,.. too lnd 10 tl ... ttll -In• I detection ll•tt ,...pectlwely.

:0 0 3 H::t zo HO <1'0 -13 :00 :oz -10 HO < "'" 0 :oz 1'10 n 0 :0 0

. \

CAMBRIDGE A~LY'TICAl ASSOCIATES, INC.

Tabla'· Coclc.ntr1tlon• of Acld/BIIe/M!Mitral Priority Pollutant Extractable• t ... tllod 12701

Cll.nt1 EPA Rlglon I CM ProJ.ct frb,r 14~1411

lllta S.piH R.cel¥t>d : DK..W 18, 1984

lllt. Anlly•l• Cotlpl1t1•h fabl"u.-y 26, 1915

-· ~

$Mpl1 IDr CM ID1 "' 1401141

0oM:Ifltrlt 1on - ua/1 <ppbl 1

" 1401149 "' 14011"'

.. 1401151

(11 pllrlrtol ---~---~--­ktlloroptllnol --- -------- - - ------- -'" "' '" '"

2-fl1tf"'l)fferrol 2,4~1M'ttlyl,..;oo'-2,4~1clll~l

---~---noo Jtl pooc:lllor-~--------------------

! 2,4,6ootr1dllor~lllnol

__., 2,Winltrofhlftol (9) ~ltrofllrlftol

iiOi"' 4,6-41nltro-2-'11Yip1Mono_!.__ -===------·-­CI1J !*ltiiCflloroptllflol

....

--~~.------------------nm-.,----,-~----H®-----._,"Y' phenol TRIIII- 1100 6100

,_ "

l> 0 :r HJ: zo Hn CI>O -<:r :oo l>Z -<n HQ <

"'" ,!£ f'10 n §l 0

I I

~ I I

CAMBRIDGE ANALYTICAL ASSOCIATES, UIC,

T•ble l Ccont 1d) , Conee~~tntlon of Acld/Bne/Neut,.•l P,.IOI"Ity Polh.1t•nt bt,..ct•bles CMttllod 12701

Cll.nt1 EPA Region I CM ProJect No,1 14•1461

IAKINEIJJRAL aii"'llGG Ccon 1t,l (Ill eceupMhyl.ne (19) ecen•ptltt~eM

1201 2 4•cltnltroto1Hn• C2H 2 6-dhltrvtol-1n1 dlethyl p!lthel•te CHI 4-octltCII"''OIf**yl "*'Y' •ffW' (241

.. _ J: Jtooflltn:IMdl,_.yt•T"'

I , Wiplleflylflydr-u:IM

~Y'"*'r' .. ...,. 1101 fleudiiOI"''benHM

1291 -.. -Ulll .... .._ (31) dl~tylpfltflel•t•

1321 tl..-..tMN (])) ben1ldiM1

"" • ,,, butyl a.nryl phtNI•t• 1361 3,3 1-dldiiOI"'OMzldiMI 1)7) benloC•Ienth,._

"" biiU~yl*yllplltNI•t•

"" .... 1401 dl-n-oc!yl pl'ltMI•n (41) benzoCb)tl~n~

,d)p -.nth,.eceM

O.tectlon Ll•lt

TR(!I)

TRC2001 TRClOOI

TRCIOI TR(2001

ntOOOI TRt2001

TRC200) TROOOI TRC401

1200 1100 TR(lOOI lR(2001

.. .. entl'lltlon• I•" th•n til• d•tectlon ll•lt .,.. T•ft bl•nk, Conc.nt,.•tlon• MtwHn I •nd 10 tl ... ttl• ll•lt of

d•tectlon •roe list*' •• t,.ace 1~•1• CTRI ,

2M.Iyllld •• •IObenleMo

'An•lyalld•sdlpllenyl .. ln•.

,. 0 J: MJ: zo MO v>o -<J: :00 l>Z -<0 MO <:

""' 0 :oz ~0

~ 0

CN&IIOGE ANALYTICAL ASSOCIATES, IPC.

Table 3, Concentration• of Acid/Base/Neutral Priority Pollutant Edrec:table• INett.od 12701

Client: EPA Region I CM Project No, : 14-1471

SeJIPI• 10 : -· 121

"' '" "' '" 111 ll)

Z..CIIIOI"'PMfiOI ~ltropllellol

2,WI..tllylpllenol 2,Wiclll~l

pooclll~l

2 4 6-trlciiiOI"'PIIellol 2,WIA1troptleftol

CM 10:

..,.,,ropbe!lol 4,6-ocllllltro-2.....,..ylpllenol

nn ,...teatot'Opftenot .,.....,pflelltol

benzoic ecld

MK/!!EIIl1W. QIPOUII)$

111 JW!Itro&odl .. tflyt•lne (2) bltl2~1oroetllyt)~tller

Ill I 3-odlcllloroben;r-C4) I,Wicl'llorol:lenzene (5) l,~ldi!OI"'benz-

!!!,_ bltC2~111oroltot>ropytletflf' 111 JW!ltr"'OICCI~-11ropyt•lne

Ill Mxec:IIIOI"'ttllane 19) nltroben;rene UOI hopllorone 111) blsl2~111oroettK»cyl .. tflane 1121 1,2,4-trlcllloroGenzene 1131 ~teplltllel•e

114) lleuclllorobllt•dl-1151 Mxeclllorocyclop-.,tedl­(161 2-<llloron•plltii•I-

\.J~'~'M<~•~r•~~~·~~~'~"~'---------------

Dlte s .. plel Rec:elyecl: o.c-.r II, 1914 O.te Anelyalt CoMpleted : Februery 26, 1985

Concentntlon- ua / 1 lppb1 1

" 8408152

TRIIOI ,..

100 140815)

~ " HJ: zo HO <1'0 -IJ: :00 l>Z -10 HO < "'" 0 :oz mo 0 0

"' 0

Client : EPA Region I CM ProJect No. : 14 .. f.t78

S.IIPIIID : -· CM ID :

IASEJ!!U'ntAl CIDM"CCUHDS ccon•t.l (111 ecenepllttl leM

'"' eceneplltn-,,., 2 4--cllflltrotoluene 120 2,6-odlflltrotol-1221 dletft I pM'IIIIIete

'"' t-<MoropMftrt PNfirt ether 12<1 "--"" hltroeodl"*'rl•l., 1201 1,2-dl,...ylhyc!,..llfll

'"' ............ yl IIMnyl ether

J tt.ec:hl~a-_ .. _

1!01 .... .._ ()1) ........ ..,I ,..tlltilate ,,.,

fi~Dr'Mttl-

'"' biMzldh•

C:Ml ' (), butyl *zyl phtlltllate

"" 1,) 1 -dlehlorobMrldl~~e

'"' beiiiOIII.,.th~

"" b1112 .... tttyl~tny l)phtMI.te

"" .. .... 14D) dl""'ft't'Ctyl phtMiete (41) benrolblfluore~~tn-

(421 benro(kltluorefltn-COl Muo(elp r-.. 1441 1Mef10(1,2 1kdl,r-,., dlbellzo(e,lll.,.ttl~

1461 beruo(gllllper-yt-benz lelc:ohol

CAMBRIDGE ANALYTICAL ASSOC IATES, INC.

11 1408152

TRC61

100 8408151

1 Co~tce~~tr-st1onl IMI tlllfl the Ntectlon ll•lt er-e left bllflk 0 Conc.t~tr-etlons MtwMII 1 lfld 10 tl ... the 11•1t of l '\tectlon .,.. lhted II tr"IC. IIYIII CTRI.

~llyrediiiZOMftZ..,., 1AnllyZedlldlpllenyl•1fll,

~ " ~I zo ~0 11>0 -<:< :00 l>Z -<o ~o

<

"'" 0 :oz 1'10 0 0 :0 0

I I

.. I I

" I CANBAIOG£ ANALYTICAL ASSOCIATIS, IIC,

Teble 3 (c:ont 1dl, Oc:w!eentntiOI'!I of kld/BIIse/ Niutrel Priority Pollutant Elrtreetlbl•• IMithod 82701

Cll1111t 1 EPA A41glon I CM Project No, 1 84-1479

-~ Ill P'*'lol

"' "' ... "' J Ill ltl

2<odltoropflenot

2-.ltrOflhellol

2,&-c! IIWf'tly lpMflol 2, 4-41cfllorotll*lol ,-ct~ lor04-Ct'etOI

2,4, ... trlcti!Of'Otii*IOI 2,Winl~l

1101 4 ,6-dlnltro-~flyi!IMROI

1111 ,_tKMOI"'ttffenol

... ~-Ill M-nltro.od l..thyl • ln.

"' bii(:Z..Cflloroethy l ) .. t ....

"' J, l-dlclllorobeftHM

141 1 ,4~1 ch l orobeftr..

'" 1,2-cl l ch loro!MfiHN

161 bi1C2<h lorollo.,-opyt tethr 111 N-flltrCKOd l.n..,.opyt•ln~ Ill heiCKhloroetMne

191 l'lltrobeftZWII

(10) ltopPiorOM

111) bl112<hloroettlox'f)Mttlarle

Dltl S..plel Reee!Yedz Dtc•bw 11, 1984 Dlft Anllylll C:O.pleted : Febru..-y 26, 191!1'

Concentr1tlon - uo/1 lppbl 1

100 Mttrl~~: Sp ike Blenk

840815) MS 8408151

m ...

""

~TI~il=--~·~·'~··~~~'~'';'i~~~~~·:~::-::::::: ___________ '_"'-----------------------

l> 0

"' Hr zo H() 11'0 .... ,. :oo l> Z -<n H O <:

"'" 0 :oz 1'1 0 () 0

" 0

Client : EPA Region I CM. ProJ~~et No,: 14-1479

SMPI• 10: _.,.,, CM. 10:

IAS£/!!UlRAL CCII"CUUlS (COft 1t,)

(11) aceMPIItll 1-091 Ker~aplltlllfle ,,., 2,Winltrotol-(21) 2,6-dlnltrotol.,_

'"' dletllyl phtMiaft 12ll 4-oc:llloropllenyl pllenyl .,.._. ,,., .,_ C251 N-ftltroaoflpt~at~yl•l, ,,., 1,2-dlp'-ylfi,,Azlna

"" --~r'pfle!lrletfler"

J Jileuclll~zene _ .. _ .... .._

()1) dt.....e.utyl pfltMiete

"" flloiOI"'an,.,_ C))) •zldl~~a

"" . ()5) butyl MnzylolltMiaft .,., '"1 1 ""411clll~zldlne

U71 Mnzo(a)antllr-ec:Ma

"" blaC21tllyl"-yl1plltMiata

'"' cflryaena .... dl~tylohtflalaft

(41) baftzoCbltluorantMM (421 baftzoCkltluorantMM (41) beniO(alltr..

"" lnd•oCI,2,)-c:,d)pyr.M (45) dl benzoCa,ll1anthroaceM 146) bei'IZO(JIIIIperyl-

Oatec:tlon Ll•lt

CN4BRIOGE ANALYTICAL ASSOCIATES, INC,

Concentr-ation - ua/1 hpb) 1

100 .,.tr-1• Spike 1408153 MS

'" ""

iOi

...

Blank 1408151

1Coftcentratlona lass than ttla det~~etlon ll•lt are latt blank, Concantratlons batwMn 1 and 10 tl ... tlla ll•lt of 6atec:1'lon ara listed as traca l..,als CTRI,

elyzad as azobenzll!a,

1Malyzadndlphanyl•lna,

CAMBR IDGE AHAUTICAL ASSOC IATES, INC.

Cll«~t : EPA Region I O.t• 5.-pl•• R•c•lvM : o.c.-.ro II, 191, CM ProJKt No. : 14 .. 1411 O.t. A,.lysls Cosplet M: J1nuery 11, 198'

Conc.t~tr-1tlon .. !!51 / I Cl!l!b) 1

SeiiPII ID: "' " .. .. _..,,, CAA ID: 1408148 1408149 8408150 14oan1

'lSTICIDI:S NG Pall en liP~

l2l ... ....., I "' de lte..C

'" ,_..-.c etlnMnl)

"' "-'t.:tllor

"' .. .,.,,.

"' lleptKIIIor epGifl de Il l •l~ul ten

J dle ldr"lfl 4, 41...(10[

Clll .,.,,. C1 21 t.t-clolultM em

· · ·~ C14 1 .-r-111 lldeiiJ'dl em --.ulfMsultat. Cl61 ··•'4T em - "~ (181 ............ C19) --,,., f!C8..1016 e2H fiiC&o.1221 In I ...,..,, CUI f!C8..1242 (24) fiiC&o.l 248

"" PC&-1 254 ,,., ...... , ... o.t.ctiOft Ll•lt '·' '·' '·' '·'

1Conc.ntnttons '"' then till d1t.ctl0ft ll•lt 1r. l•tt blink. Conc•tretlons behtHII 1 •l'ld 10 tiNS tne detKtlon IT•It er. llst.d •• tr-ee. levels cnu. O.t~etlon ll•lts tor PC8s are t.n tt ... t"- -lnel d•tKtlon ll•lt.

l> 0 :r MJ: zo MO <1>0 -IJ: "O l>Z -co MQ < "'" ,!i! "'O 0

~ 0

'1

'. \

Client: EPA Region I CM ProJKt No. : 14·1478

CN411RIOGE NIALYTICAL ASSOCIATIS, IJC.

O.te S.plel RKehted 1 O.C.bw 18, 1914 O.te M1ly1l1 C.:.pleted : Jenu1ry 11, 1985

Cbftc~t~tntlon • ug/1 (ppb) 1

S.ple 10: 100 a.oal5l

..e:STICIOO Nil P'CII 111 121

o1-.... ..., ()) Rite~

(41 ,_~(llnclenel

'" MptiiCMor

:::1 ehllrln _! llepteclllor et1011lde I ll~lollfM

(9) dleldrht

(10) ··•'.oDE 1111 ..... 1'1

(121 ..,.......,.ultM (I))···'~

o•J INrlneiHtl.,cle (15) ..... lllfMIIIIfe ..

1111 ···'~ em ...._yct'lor CIIJ chlordene rn;-...,..... i20) P'C&-1016 (21) PCa-1221

mr ..:a-1212 iii)-;c...1242 rn;- PCB-1248 rn;-PC&-1254

~IHO

CM 10:

________ ,_.1 0.1

~ :r ~J: zo ~0 (/00 -1:< :00 l>Z -1 0 ~0 < "'" 0 :oz

"'" n 0

"' 0

Cllent1 £PA Regl011 I CM ProJect Mo. : 14-1411

S.•ple ID: -· CM ID:

f'UTICUIES NG f'C8I Ill ol-

"' ... ......,

"' Htt...ac 141 ,_...... (llrldanl)

"' -,tlld!ICII'" 161 •1411"111 111 Mlt~IOI"eporiM

: .............. lilt• dieldrin I 4 4 1--GIX

(11) eMirlll

C12l w......-.~~••• iii'r4 4'«11 114) M41rhetdetlyde

'") --lllfell&lllflt9 116) 4 4 1-«fT (11) 1 ... Ill) .. I...._ 119) -120) f!C&ool016 121) f'ICI-1221

"" f'ICI-1212 12,) f'ICI-1242 (24) f'ICI-1261

"'' f'ICI-1254 ,,., f'CB-o1260

Detection Ll•lt

CNIIRIOGE ANALYTICAL ASSOCIAT£5 , IJC,

lS Mltrhl: Spike 1401149145

.., ,,.

1oSi

tOll

'"'

Blenk 1408150 a

'·' 1eo..c.,.tretlona leaa t11111 1111 detection ll•lt .,.. lett blul!.. Ocwlcentntl011a betnen I 111d 10 tt.-s the detectiOII lf•lt .,.. llated n tree• teYela CTR) , Detection ll•lh tO!" PC8a ere ten tl•• tM _,,.., O.tectiOII ll•lt,

,. 0 3 ~:~: zo ~" V>O -<3 :00 l> Z -< n ~o

<: ,., ., :o !il 1'1 0

" 0 :0 0

Cllent1 EPA ~ion I CM Proj.ct No 1 14·1471

CNIIRIDOE AMALYTICAL ASSOC IATES, IIC,

Swrogate eo.pounc1 AKcwry Ill

Acceptlble S.,l• IDI "' " .. .. Anllylh ll•ltl CM IDr &401148 14011"9 1401150 1401151

~

Anely111 O.te "'· 22 Dtc:.22 "'· 22 Dtc:.22

10 2-Gic:M.-oettleM,cl" 71•120 "' 10, 109 100 TolweM,fl 16-119 101 102 100 101

~flmrobennne ,,_121 " n 71 10

~

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