Field Sampling Data

Run5Field Sampling Data

MRI-Appfcd/R362013.APP

A R 3 I 5 6 I 8APPENDIX B 112

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AR3I5&20APPENDIX B

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INTEGRATED GAS SAMPLING DATA FORMFOR U.S. ERA METHOD 3

Plant Otf/rt £SC ZXz/z-x- Project No. 5 ,20 -/3 -.30Sampling LocatiSample Type (MFlow Control DQ\For Sampling FrPump Type

on 6TACK UPP&J?. .o&e. RunNQ.g-titJ&p/+ Date 2-/-?7ulti-Point, Sing/ice (Micro valveom M5 Console

e-Point) A' A Operator JL .- r' . £4~<~.', Critioal Orifico)1 ^ ^ Baa Type ' Sample No. S/&?-j No. N'T- ' Method 3 Train No. — '• —'tut Pumo Type —— '

Pump I.D. A)-?-, Pump I.D. - ——Flow Meter TypeFlow Meter I.D.Desired Flow ReLeak Check BefTotal Sampling 1Flow Rate (cc/mEstimated Actua

Time24 Hr Clock/£.///2 jbIZ33,<T/V3/yvjzI53Z. <TI -?£0 . s1 703, rmi?

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Comments

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DRAKE 3£20.i3 S 1 O "7MM5PH QRSAT BAGTRIAL BURN SAMPLEFor disposal call: P.GORMANMIDWEST RESEARCH INSTITUTE

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AR3I5622APPENDIX B

40 CFR 266, APPENDIX IX, METHOD 0050 -MODIFIED PARTICIPATE MATTER, HCI, AND CI2 TRAIN (MM5PH)

FIELD LABORATORY TRAIN SET-UP DATA

MRI Project No. 3620.13.30Client/Source: OHM Remediation Services Corp., Drake Chemical Superfund Site, Mobile HWI

Source Location: Lock Haven, Pennsylvania,Sampling Location: Mobile Hazardous Waste Incinerator (HWI) Stack

Run No. O Sampling Train'No. /k/n_5~ if:>H~ I_____ Sample Box No. __YSet-up person(s): J./W <- <^L_________________________________ Date: /- 3/~ "7"?

Transfer to Sampler:Relinquished By / ./f(e tL c—, —- Received By <£> /J-0—f _____ Date/Time -2-/~? 7 __*

TRAIN COMPONENT COMPONENT NO. _______________ LOADING DATA _____________

Sampling Nozzle (Quartz) rH~' * Initial Weights (grams)**Probe (Liner-Glass) ______________ * ____ Empty _____ _____ Loaded

Female Probe Outlet Blank-Off ___________- 90° Bypass __________ *

Filter Holder Front ____________ Filter Type: Whatman QM-AFilter Holder Back with

Te.flon® Filter Support _____________ Filter Number: /O45/90° Connector ___________

1st Impinger (2-Liter, Mod-GBS) _____ _ ____ 50mLs±1mL /03.L V /O 74-0.1 N H2S04

1st Impinger Replacement /vf" --feX_ 50mLs±1mL ____ —— ____ ____ ——U-Connector (A) ___________ 0.1 N H2S04

2nd Impinger (GBS) ___________ 100 mLs ±2 mLs */?-?. ifU-Connector (B) _______________ 0.1 N H2SO4

3rd Impinger (GBS) ' _____ 100 mLs ±2 mLs ^ 73. OU-Connector (C) ___________ 0. 1 N H2S04

4th Impinger (Mod-GBS) _____ _____ Empty V?P,"7U-Connector (D) _____________

5th Impinger (Mod-GBS) _____ _____ 100 mLs ±2 mLs i53"3. /U-Connector (E) ___________ ' O.IN'NaOH

6th Impinger (Mod-GBS) ______ _____ 100 mLs ±2 mLs ____ C/P . / v5"?7- /U-Connector (F) ______ ; _____ 0.1 N NaOH

7th Impinger (Mod-GBS) _____ _____ -200 g indicating silica gel |£>A£ f _U-Connector (G) ___________

8th Impinger (Mod-GBS) _____ _____ -200 g indicating silica gelImpinger Outlet Connector faft—f _____

* Before and after sampling: Nozzle openings covered with aluminum foil or Teflon® tape, and nozzle placed in Ziploc® bag.Probe liner outlet sealed with glass female blank-off, and inlet sealed with Teflon® plug. Bypass inlet covered (not sealed)with aluminum foil.

* * Initial weights of additional components exchanged during the run also entered here. All exchange component openingscovered with aluminum foil. Teflon® tape or as described above.

Component Changes After Set-up And Before Recovery And Other Comments:

0050SUCX.WPD June 26, 1996 (rev. 0050SUC3.WPD Octobar 31. 1996)

AR3I5623APPENDIX B 117

40 CFR 266, APPENDIX IX, METHOD 0050 -MODIFIED PARTICULATE MATTER, HCI, AND CI2 TRAIN (MM5PH)

FIELD LABORATORY SAMPLE RECOVERY DATAMRI Project No. 3620.13.30Client/Source: OHM Remediation Services Corp., Drake Chemical Superfund Site, Mobile HWI

Source Location: Lock Haven, PennsylvaniaSampling Location: Mobile Hazardous Waste Incinerator (HWI) StackRun No. , -^ Sampling Train No. /W/nS' Ptf~-l Sample Box No. V_____________________________TRAIN PURGE WITH ASCARITE-FILTERED AIR___________

Condensate in front-half? tv d________________________________ Purged By /U//\Date/Start Time: A/ A _____ '. ________ Stop Time A; A _____ Purge Rate: [AH = AM ' in.H,OlMoisture Removed? A I /V _____________________________________________________Transfer for Recovery: i /? / /Relinquished By D . I\J ' <Lo~ \ Received By /\^ L Sl r &&&-*•( Date/Time ,£.///<? "7 3-0 ' &!>Sample box recovery person(s): /\ . (_j{ZJ~g_ f °f ————— ________________ Date: /Z//f 7"

Probe recovery person(s): fi G-or/ncLA,"' -Surr a.*.. R. . HOUJ&-* Date: "JJ\/ ~TWeights below are in grams.______________________________ • BACK HALF RECOVERY _____________________________

ReplacementImpinger: 1st 1st 2nd 3rd 4th 5th 6th 7th 8th

Final wt. 3733/3 /ft- ff^-3 g7£.6? ?3&.f £8£.6> 5?<?.5Initial Wt. /O7t.f } 5"7,t> 671 '*£. V/V%? LSl.3 <5f~7. INet Wt. .37/9 q. 9 3.4 - /\0 /f.1/

[ Total Condensate Collected: 3 S 7 9. 2

and/or color: /"j£?A ~- A//( WiPA - CJbtAs £jj>& ^ rJ&gj rJ!a£sU & 10%*Recovery: -» -« » >-» * Impingers 1-3 »-*'•-«-•«-*'<-'*-«-• -»-» Impingers 4-6 ~ ~ ** +* ~ ~ % Blue

Sample Number: .S'lOS -,4 o 105Sample Bottle Tare Wt. /J - '1°'

~Sample Bottle Gross Wt. H~7 lo%\\ /O $7- / Before RinsesComponents Rinsed*: filter support, filter holder back, 4th-6th impingers,45/90° connector, 1st-3rd impingers, U-connectors A-B U-connectors C-E

Sample Bottle Gross Wt. $57- 2 /; ?''7/i? 7J-aeAfter RinsesNet Sample Wt. 3 "3O3 . ~~ #?3-S /•/ I.'=f~*c1ar Mass Collected Computations

Sample Mixed, Then: for HCI for CI2Aliquot Sample Number: -.-»-»-.- .5 104 _, ~.-, _ , ,5" 106 for Chloride AnalysisSample Bottle Tare Wt. Q~7. 9 9?. Q

Sample Bottle Gross Wt. 75"/• f I°l1' /O%5-5 /"? 4< ~ After AliquotingSample Bottle Final Wt. \J A ~/" /V1 A _ After SIE Check

Net Sample Wt. .3 4 031.0" IOO.Q S 15 (0. (*

_________________________________FRONT HALF RECOVERYFILTER:

Sample Number: _5~102 Description/Color:

TRAIN RINSES: Sample Number: S 101Sample Bottle Tare Wt. L(a <o.OComponents Rinsed**: nozzle, probe liner, bypass, filter holder frontSample Bottle Gross Wt. 3 "1(1. 3~~ with Acetone RinsesNet Acetone Sample Wt. I O ii. 3-~Sample Bottle Final Wt. ^> (o, ^ with added W?ter RinsesNet Water Sample Wt. -/ 3 gU= -/£ 'Z'fSf

* Using a total of 100 mLs ±2 mLs ASTM Type I water per sample, rinse components twice. Thoroughly mix each sampleand added rinses before aliquoting.

** Acetone rinses with brushing 3 times or more until perceivably clean. If any residue remains in a component, follow withASTM Type I water rinses with brushing until perceivably clean. Do not add any water rinses to the sample bottle untilafter the bottle is weighed with all of the acetone rinses.

COMMENTS: !

0050RCCX.WPO October 31. 1996 (rev. 0050RCC3.WPD October 31, 19961

APPENDIX B

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APPENDIX B 12O


Plant V-rsLte- OW*\ fO*- Proiect No. 1leZ0 -ft- OSampling LocatiSample Type (MFlow Control De\For Sampling FrPump Type

on "fZ&zk.& ldr Ci-£ru ~ -) Run No. 'T Date ~Z.-/—*?ulti-Point, Sing/ice (Microvalveam M5 Console

e-Point) /""<* Operator / ,-ff1 —, Critical Orifice) /^ Baa Type / v6 — Sample No. f//4-i No. /|/? Method 3 Tram No. //A

Pump Tvoe ^^Pump I.D. M-9 . Pump I.D. \ ^Flow Meter TypeFlow Meter I.D.Desired Flow RJLeak Check BefTotal Sampling "Flow Rate (cc/mEstimated Actua

Time24 Hr Clock/2*{(/zz£/2-'57, /z.y&/2C76

/3>/<2ff'Z.'?t ^&(J1/?'*?.£££&£ 1 411jjUi-1 pr,{tf-ft P)/ L/t-fJ

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ite (cc/min) ' t& oore Sampiina ,<y?-tz~o After Samplina J -v aTime (min) /T7 Averaae Flow Meter Readina ' /- n): Averaae ' / Hiahest X o Lowest /&&I Volume (liters

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AR315628APPENDIX B

SW-846, METHOD 0010; 40 CFR 60, APPENDIX A, METHOD 23 -MODIFIED SEMIVOLATILE ORGANICS TRAIN (MM5SV) FOR POHCs, PICs AND PCDDs/PCDFs


MRI Project No. 3620.13.30Client/Source: OHM Remediation Services Corp., Drake Chemical Superfund Site, Mobile Hazardous Waste

IncineratorSource Location: Lock Haven, Pennsylvania

Sampling Location: Incinerator Stackr - - — . .

Run No. _5 Sampling Train No. O\J " \ __________ Sample Box No. O /3~OO / ,Set-up person(s): A . C e se J S _______________________ Date: //3 \ / *3 ~1

Transfer to Sampler: . . i^\ A I [ /Relinquished By A . (Wa*v,g£g* Received By V • J\J<2a \ Date/Time 3-/f 7*7 "7 <?*? 3O

TRAIN COMPONENT COMPONENT NO. _______________ LOADING DATA

Sampling Nozzle (Quartz) - * Initial Weights (grams)**Probe (Liner-Glass) __________ * ____ Empty ___ Loaded

Female Probe Outlet Blank-Off ___________90° Bypass __________ *

Filter Holder Front ________________Filter Holder Back with Teflon®- Filter Type: Whatman QM-A

coated 316 SS Filter Support _________ _45/90° Connector ________ '

Condenser (Standard) __________ Thermocouple No. 7 3~~XAD-2 Resin Cartridge (Standard) */ L "TJ_____ -65 grams XAD-2 Resin + Surrogates 4 3* (9_____(Documentation of standards injection is separate); resin spiked on y\ [ f^ ~~7 and maintained near 4°C until use.

1st Impinger (2-L Mod-GBS) __________ Empty In 43-- (-?

1st Impinger Replacement _____ ________ Empty 'd-t' U -faU-Connector (A) ___________

2nd Impinger (Mod-GBS) __________ fOOmLs 7 7. V £~<3~7- "7U-Connector (B) _______________ ASTM Type II Water

3rd Impinger (GBS) _________^ 100 mLs V 7 6. 7 5~.*~I *:>>£>U-Connector (C) ___________ ASTM Type II Water

4th Impinger (Mod-GBS) _____ _____ Empty I(QI> 2-_,U-Connector (D) ___________

5th Impinger (Mod-GBS) __________ -200 g indicating silica gel &><*. /-QU-Connector (E) ___________

6th Impinger (Mod-GBS) ___^_______ -200 g indicating silica gel . "7 //?. ffImpinger Outlet Connector () H —'

* Before and after sampling: Nozzle openings covered with methanol/methylene chloride/toluene/acetone-rinsed aluminumfoil, and nozzle placed in Ziploc® bag. Probe liner outlet sealed with glass female blank-off, and inlet sealed with Teflon®plug. Bypass inlet covered (not sealed) with methanol/methylene chloride/toluene/acetone-rinsed aluminum foil.

** Initial weights of additional components exchanged during the run also entered here. All exchange component openingscovered with methanol/methylene chloride/toluene/acetone-rinsed aluminum foil or as described above.

* * * Cartridge weighed with blank-offs in place; then, cartridge covered with aluminum foil to seal out light during storage andsampling.

Component Changes after Set-up and before Recovery and Other Comments:

1023SUCX.WPO April 26, 1996 (rev. 1023SUC3.WPO October 25, 1996)

AR315629


FIELD LABORATORY SAMPLE RECOVERY DATA



Sampling Location: Incinerator Stack

Run No. J Sampling Train No. /viM1? 5 V ~~ I _____ Sample Box No. Q |Transfer for Recovery: _^ .Relinquished By D- L&*fi.Z-.Y Received By A- C J.r<?y\g Date/Time .d/(/<?~7.Sample box recovery person(s): /\-» Q_ -tJC& f -S>i ________ __________ Date: ,3-X//'? "7

Probe recovery person(s): P. <S-cjr>wo-/ii "V- -S~/jr/»v v,n. r -* ty i/J Z— ______ Date: y-/ 1 /^f "Weights below are in grams.__________________________ RESIN CARTRIDGE AND IMPINGERS RECOVERY ______________________

Impinger: XAD-2 ReplacementCartridge* 1st 1st 2nd 3rd 4th 5th 6th

Final wt. GO. 3737VInitial Wt. 3.0 / 0Net Wt.

and/or color:

1 ?Afr6 576,5 <_,#?. 7 -757.5 75-.0

I Total Condensate Collected: 3 S ff/. / grams]

Sample Recovery: Cartridge* — 1st-4th Impingers and Replacement 1st Impinger ~ — «-- «- % Blue

Sample Number: ?111Sample Bottle Tare Wt. /3

Transfer impinger contents only (i.e., do not add component rinses to this sample).

Sample Bottle Final Wt.Net Sample Wt. 3

Components Rinsed**: 1st-4th impingers, replacement 1st impinger, U-connectors A-C; combine rinseswith train back rinses below (sample number XX010)

__________________________ FILTER RECOVERY AND TRAIN RINSES _______________________

FILTER:Sample Number: ^109 Description/Color:

TRAIN RINSES: FRONT BACK QA RINSESSample Number: 5~108 ^110 5"l13

Sample Bottle Tare Wt. ^Components Rinsed***: Front — nozzle, probe liner, bypass, filter holder front;

Back -- filter support, filter holder back, 45/90° connector, condenser

Sample Bottle Final Wt. V3c5L~7 ~799! 1Net Sample Wt. 6§. Y £"3-%. ZL ~IO(.3

* Replace blank-offs and remove aluminum foil, then weigh the cartridge; replace aluminum foil to cover the entire cartridge.** Methanol/methylene chloride (1:1 v/v) rinses 3 times; add rinses to train back rinses (sample number XX010).

*** TRAIN FRONT/BACK RINSES: Methanol/methylene chloride (1:1 v/v) rinses with brushing of front components 3 times ormore until perceivably clean, and methanol/methylene chloride (1:1 v/v) rinses of back components 3 times, but without.brushing, and including 5-minute soaks of underlined components 3 times.QA RINSES: Follow with toluene rinses and soaks, but without brushing, in the same manner as above for the train fron'and back rinses.

COMMENTS:

1023RCCX.WPO June 4. 1996 (tov. 1023RCC3.WPO October 25. 19961



FIELD LABORATORY TRAIN SET-UP DATAFIELD BLANK TRAIN




Run No. _____ Sampling Train No. /?/./l /\.~ c/—-~ Sample Box No. O) P-SJC) -JSet-up person(s): A • Q^fcC^r^huT________________________ Date: ?-/\ / t~"l_____/ / i

Transfer t o Sampler: t i l IRelinquished By nJ'r 0.00! / ujJoul Received By Ak r" A-aP li eg LI4 Date/Time "—'____ ——'

TRAIN COMPONENT COMPONENT NO. _________________ LOADING DATA

Sampling Nozzle (Quartz) rS _____ * Initial Weights (grams)**Probe (Liner-Glass) __________ * Empty _____ ___ Loaded

Female Probe Outlet Blank-Off _____________90° Bypass ___________ *

Filter Holder Front ________ 'Filter Holder Back with Teflon®- ; Fi'ter Type: Whatman QM-A

coated 316 SS Filter Support __________ _45/90° Connector ________ ___ .

Condenser (Standard) ______ ___ Thermocouple No.XAD-2 Resin Cartridge (Standard) 9 (f } -65 grams XAD-2. Resin + Surrogates ' V7 "7. /_____(Documentation of standards injection is separate); resin spiked on (/ / V/Y "7 and maintained near 4°C until use.

1st Impinger (2-U Mod-QBS) _______ ' Empty / 0 / 2>. C?

1st Impinger Replacement __________ Empty <v A______U-Connector (A) ___________

2nd Impinger (Mod-GBS) ____________ 100mLs V frZ-3 5 % V. OU-Connector (B) ___________ ASTM Type II Water

3rd Impinger (GBS) ___________ 100mLs V/ 3U-Connector (C) ______' ASTM Type II Water

4th Impinger (Mod-GBS) _____ _____ Empty / / /> /U-Connector (D) ___________

5th Impinger (Mod-GBS) _____ ______ -200 g indicating silica gelU-Connector (E) ____________

6th Impinger (Mod-GBS) _____ _____ -200 g indicating silica gel 6? 2 '&. [Impinger Outlet Connector L) H — 7___

* Before and after use: Nozzle openings covered with methanol/methylene chloride/toluene/acetone-rinsed aluminum foil, andnozzle placed in Ziploc* bag. Probe liner outlet sealed with glass female blank-off, and inlet sealed with Teflon® plug.Bypass inlet covered (not sealed) with methanol/methylene chloride/toluene/acetone-rinsed aluminum foil.

* * Initial weights of additional components exchanged during the run also entered here. All exchange component openingscovered with methanol/methylene chloride/toluene/acetone-rinsed aluminum foil or as described above.

*** Cartridge weighed with blank-offs in place; then, cartridge covered with aluminum foil to seal out light during storage anduse.


1023SBCX.WPD April 26, 1996 (rev. 1023SBC3.WPD October 25, 19961

A R 3 I 5 6 3A n o cr M n T v


FIELD LABORATORY SAMPLE RECOVERY DATAFIELD BLANK TRAIN




Run No. &la\ K Sampling Train No. & \o.n k " "JX— Sample Box No. oTransfer for Recovery:Relinquished By tJ0-r aLe-p]ir Jol4._____ Received By AJ*r A-aa(,c4*o(4_____ Date/Time •—--___ •Sample box recovery person(s): A • C /(X.r r\d. f _________________________________ Date: 3< / \ /

Probe recovery person(s): ?• G-ofyna/y, j- Spring.* p. L£--TT> (L^l____________ Date: <?•/ i / 5 yits hfilnw nrB in nrams. ' /Weights below are in grams.

RESIN CARTRIDGE AND IMPINGERS RECOVERYImpinger: XAD-2 Replacement

Cartridge* 1st 1st 2nd 3rd 4th 5thFinal Wt. 4 97.7 /Oll-^ VtruteJ Stfi.O S -6 7 5 (,!)0.2>Initial Wt. V?7/ / lO/3-Lo

N NetWt. 0-^ 0'^

Description - , /and/or color: *- -'/ Ct2**-x/ .I -IIA J \

St .O 55?. 7 V'7'7<7 < 3 .3o.o -0. i -o. a (7-o

[ Overall Weight Difference: O . O

6th

&3JZ.J'0.\grams]

' cA^ rA»~ *-»& >oo% /J0ynSample Recovery: Cartridge* - 1s't-4 h Impingers and Replacement 1st Impinger ~ -^ - % Blue

Sample Number: 157 -S 158Sample Bottle Tare Wt. / k^. O

Transfer impinger contents only (i.e., do not add component rinses to this sample).

Sample Bottle Final Wt. 3 £?3. 7Net Sample Wt. /<?*/• "7

Components Rinsed**: 1st-4th impingers, replacement 1st impinger, U-connectors A-C; combine rinseswith train back rinses below (sample number XX1 56)

___________________________ FILTER RECOVERY AND TRAIN RINSES ____________________FILTER: . *//-+'/Sample Number: _5~ 155 Description/Color: i a-cf/u r J( \ ___________

TRAIN RINSES: FRONT BACK QA RINSESSample Number: £T 154 -5 156 159

Sample Bottle Tare Wt. <3 k-3. •?>7- ) ^ .2Components Rinsed***: Front -- nozzle, probe liner, bypass, filter holder front;

Back — filter support, filter holder back, 45/90° connector, condenser

Sample Bottle Final Wt. ty&9.O 7*2 f.*f \\?>(a.ONet Sample Wt.

.*f• 3


*** TRAIN FRONT/BACK RINSES: Methanol/methylene chloride (1:1 v/v) rinses with brushing of front components 3 times ormore in the same manner as is being done for the source sampling trains, and methanol/methylene chloride (1:1 v/v) rinsesof back components 3 times, but without brushing, and including 5-minute soaks of underlined components 3 times.QA RINSES: Follow with toluene rinses and soaks, but without brushing, in the same manner as above for the train frontand back rinses.

COMMENTS:

1O23RBCX.WPD Juna 5, 1996 (rev. 1023RBC3.WPO October 25, 19961

AR3S5632APPENDIX B 126

SW-846, METHOD 0010; 40 CFR 60, APPENDIX A, METHOD 23 -MODIFIED SEMIVOLATILE ORQANICS TRAIN (MM5SV) FOR POHCs, PICs AND PCDDs/PCDFs

FIELD REAGENT BLANK PREPARATION DATA

MRI Project No. 3620.13.30Client/Source: OHM> Remediation Services Corp., Drake Chemical Superfund Site, Mobile Hazardous Waste


Sampling Location: Incinerator StackA ' n Us / / —"7Blank(s) Prepared By: r\ • I &S €LJVXJL f___________________ Date: 3- / /'/ 7 '_____

Weights below are in grams.Sample Bottle Tare Bottle Gross Net Sample

______Reagent Blank Description_____ Number Weight Weight Weight

Methanol and methylene chloride, 1:1 v/vVolume needed: 450 mLs

MethanolLot Number: & O 3~-1? '_____

. Methylene chloride / / Q f i l lLot Number: /3 O V 0 7 S 143 9t(a(<D. I & / 7>

Methanol and methylene chloride, 1:1 v/vVolume needed: 450 mLs

Lot Numbers: same as above ~~..'-J 144 t3_ G?3.-3 /

Toluene . . . . . ' . . .Volume needed: 900 mLs

Lot Number: & L~l X"T .5T145

FilterType: Whatman QM-A

Lot Number: I "X/3v/f (4 $ 146

XAD CartridgeCartridge Number:

ASTM Type II WaterVolume needed: 200 mLs _

Lot Number: >7-/3/? 6? £ 148 / d? f. ~7 5 (0 5,7$ I Ly. \

NOTE: Lots may be identified above by a manufacturer's lot number or by the date of reagent preparation. If different lots ofa particular reagent are used, indicate the applicable test run number(s) and sampling location(s) where the train(s)loaded and/or recovered with that reagent are'used (i.e., list each reagent blank sample number with the applicable testrun number(s) and sampling location(s) below).

Sample Number For Test Run Number(s) For Sampling Location(s)

COMMENTS:

1023BLCX.WPO June 11, 1996 (rev. 10238LC3.WPO October 25, 1996)

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INTEGRATED GAS SAMPLING DATA FORMFOR U.S. EPA METHOD 3

Plant Or<3b W*\- &£- Project No. "?/Sampling LocatiSample Type (Mrlow Control De\=or Sampling FrcPump Type

Dn j j tT / ' D Run No. ^Tulti-Point, Singl'ice (MicrovalveDm M5 Console

e^Point) /tf/0 Operator^/^, Critical Orifice) /^ Baa Tvpe /ÂNo. f/ \n Method 3 Train

Pumo TvoePumD I.D. ' /y-'# Pump I.D.Flow Meter TypeRow Meter I.D.Desired Flow RELeak Check Bef<Total Sampling "1Flow Rate (cc/mEstimated Actua

Time24 Hr Clock/ZV/- 5/Z.-Z6- "/2-2V/Z -V<7/?/<?' 5"/:?z$r- 5"/ //?7*r n;(Jj&jT l v£frfa M££9$to/*jy#/c?0'5/ftf/T7>l ?'3i>-/90't-<!"?n/fZ5

(j&HI- JoDate 1.-NC5'?

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3re Samplina p&&* After Samplina /-& ~"ime (min) X77 Average Flow Meter Readina ^-<=»n): Average /a& Hiahest /&<?\ Volume (liters

Flow MeterReading/./-0

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Comments

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DRAKE 3S20.15 SJ -MM5MM ORSAT BAGTRIAL BURN SAMPLE

APPENDIX B 130

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flR3IS637APPENDIX B 131

40 CFR 60, APPENDIX A, METHOD 29 -MODIFIED MULTIPLE METALS TRAIN (MM5MM)





Run No. ^$~ Sampling Train No. /y\/yiJT /Y\/ft~3 Sample Box No. 0 1 1 ISet-up person(s): T./fl <. ( —— ___________________________ Date: /-.:?/- 9~7

Transfer to Sampler,Relinquished By j] /Wt <^- — Received By O- AJ J _______ Date/Time ,2-/-f 7

TRAIN COMPONENT COMPONENT NO. _______________ LOADING DATA

Sampling Nozzle (Quartz) /ft/??- * Initial Weights (grams)**Probe (Liner-Glass) __________ * ____ Empty ___ Loaded

Female Probe Outlet Blank-Off ____________90° Bypass ___________ *

Filter Holder Front __________Filter Holder Back with Filter Type: Whatman QM-A

Teflon® Filter Support ___________45/90° Connector ___________

1st Impinger (2-L Mod-GBS) _____ _____ Empty /Q VP- ,2-

1st Impinqer Replacement X*r~ *-f-t- = Empty ____________U-Connector (A) ___________

2nd Impinger (Mod-GBS) _____ _____ ... 100 mU ±2 mLs %£. YU-Connector (B) ___________ 5% HNO3/10% H2O2

3rd Impinger (GBS) _____ _____ 100 mLs ±2 mLs yf4. S~f/. 8"U-Connector (C) ___________ 5% HNO3/10% H2O2

4th Impinger (Mod-GBS) _____ _____ Empty t25 f?.QU-Connector (D) ____________

5th Impinger (Mod-GBS) _____ _____ -200 g indicating silica gel (a I ~l. *7 _U-Connector (E) ___________ P-5- . ?

6th Impinger (Mod-GBS) _____ _____ -200 g indicating silica gel Ha-S'Q.?-Impinger Outlet Connector U H~-/2—

* Before and after sampling: Nozzle openings covered with Parafilm* or Teflon* tape, and nozzle placed in Ziploc* bag. Probeliner outlet sealed with glass female blank-off, and inlet sealed with Teflon* plug. Bypass inlet covered (not sealed) withaluminum foil.

* * Initial weights of additional components exchanged during the run also entered here. All exchange component openingscovered with Parafilm*, Teflon* tape, or as described above.


M29S_CX.WPO June 19, 1996 (rev. M29S_C3.WPO Octobw 25, 19961


40 CFR 60, APPENDIX A, METHOD 29 -MODIFIED MULTIPLE METALS TRAIN (MM5MM)FIELD LABORATORY SAMPLE RECOVERY DATA

MRI Project No. 3620,13.30Client/Source: OHM Remediation Services Corp., Drake Chemical Superfund Site, Mobile Hazardous Waste



Run No. ~ Sampling Train No. /M/nf /MM -3 Sample Box No. O /// 7-2Transfer for Recovery:Relinquished By J?'• AJ-*~~~1________ Received By J-•/ftc. £« Date/Time_^~/~??Sample box recovery person(s): J ./frt< C — _ _____________________________________ Date: 3. ~l ~?7

Probe recovery person{s): J". $"--«•*——-, r.&vr**-*——-. £•/-/&*+*—_____________ Date: Z. —I — •??Weights below are in grams.

_________________BACK HALF RECOVERY______________________________________Replacement

Impinger: 1st 1st 2nd -3rd 4th 5th 6th

Final Wt. 3~?1<J.C( A/* PS"?.? <?oQ.3> 177.? £, VAfInitial-Wt. IWr. 1— _____/ <3-?/.3- <£~?f.? Wy, O toll.?Net Wt.

'"'•.•'' [Total Condensate Collected: _^Description , / ' ' " ' ' jand/or color: C\e s- ________ ck -r' Uf ./ Q<i*-s~ _____)___ /d

Recovery: ->-»-»>-»-»-. Impingers 1-4<^«j«-'«-<-'«j«-'<^<j«-<-«-'«j«-<r«-<-«-<-<- % BlueSample Number: v3"l17

Sample Bottle Tare Wt. /3/ .JSample Bottle Gross Wt. 5Db(,f Before Rinses

Rinse Solution: 0.1 N HNO3Components Rinsed*: filter support, filter holder back, 45/90° connector,

1st-4rd impingers, U-connectors A-C

Sample Bottle Final Wt. -T/£..£.£, After RinsesNet Sample Wt. 3 $ -l

FRONT HALF RECOVERY_____________________

FILTER: _ - , . , , ; j_Sample Number: ^116 Description/Color: L . Ftf /A. r>Jl___________________TRAIN RINSES: 7 '

Sample Number: ^^115,Sample Bottle Tare Wt. /7/.-T

Rinse Solution: 0.1 N HN03Components Rinsed**: nozzle, probe liner, bypass, filter holder front

Sample Bottle Final Wt. o2V7-7Net Sample Wt. 7k. ,3-

* Using a total of 100 mLs ±2 mLs of 0.1 N HNO3, rinse components twice.** Using a total of 100 mLs ±2 mLs of 0.1 N HN03, rinse components 3 times or more with brushing until perceivably clean.

COMMENTS:

M29R_CX.WPD September 27. 1996 (rev. M29R_C3.WPO Octpber 25. 19961

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————————————————————————— DRAKE 3S2G. 13MM=SMM nfiSAT BAGTRIAL BURN SAMPLEFor disposal call: P.GQRMA1MIDWEST RESEARCH INSTITUTE

AR3!56lf2APPENDIX B 136

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40 CFR 60, APPENDIX A, METHOD 29 - MODIFIED MULTIPLE METALS TRAIN (MM5MM)FIELD LABORATORY TRAIN SET-UP DATA




Run No. J/C Sampling Train No. /YI-MS /flM'] Sample Box No. Q/_3_Q_Q_^Set-up person(s): J- lf-Cc v . _____________________________ Date: /" 3/~ *? / ___

Transfer to Sampler: .Relinquished By T./*?*- &»~ —— Received By 0- /U-«-«-.i ______ Date/Time -3. - â^

TRAIN COMPONENT _CO.M PQMENJ_NQ- ________________ LQADifcLG_DAIA

Sampling Nozzle (Quartz) "J"' ' „_ * . Initial Weights (grams) * *Probe (Liner-Glass) ________,___*. ___._Empty__ .,„. .,„_ Lo.aderL. _ „

Female Probe Outlet Blank-Off ___.,_______ . . .90° Bypass __________ *

Filter Holder Front ___________ •Filter Holder Back with Filter Type: Whatman QM-A

Teflon® Filter Support ____,.,.._ __ . , .45/90° Connector ____„__.___ ._ ,.

1st Impinger (2-L Mod-GBS) ____ _____ Empty

1st Impinger Replacement _ ? t_'ef s___ Empty ___1~L___._U-Connector (A) ___________..

/ / f &* / T~~ "7 tf s*\2nd Impinger (Mod-GBS) _____ _____ 100 mLs ±2 mLs yfa/.Ja o / 7,uU-Connector (B) ____________ 5% HNO3/10% H2O2

3rd Impinger (GBS) _____ ____ 100 mLs ±2 mLs ....?.3t3_.U-Connector (C) _._.__..______. 5% HNO3/10% H2O2

4th Impinger (Mod-GBS) ._ __... _ .,___ EmptyU-Connector (D) ... __.._..,._„

5th Impinger (Mod-GBS) _____. .__. ___ 100 mLs ±2 mLs* **U-Connector (E) ___________. 4% KMnO4/10% H2SO4

6th Impinger (Mod-GBS) _____ _____ 100 mLs ±2 mLs** * JCI.QU-Connector (F) ___________ 4% KMnO4/10% H2S04

7th Impinger (Mod-GBS) _____ ._____ —200 g indicating silica gelU-Connector (G) ____________

8th Impinger (Mod-GBS) L_____ _____ -200 g indicating silica gelImpinger Outlet Connector __M.H' "3\——

* Before and after sampling: Nozzle openings covered with Parafilm® or Teflon® tape, and nozzle placed in Ziploc® bag. Probeliner outlet sealed with glass female blank-off, and inlet sealed with Teflon® plug. Bypass inlet covered (not sealed) withaluminum foil.

** Initial weights of additional components exchanged -during the run also entered here. All exchange component openingscovered with Parafilm®, Teflon® tape, or as described above.

*** If the reagent was exhausted before the end of a previous run," use a larger volume (e.g., 200 mLs ±2 mLs) and documentbelow. Prepare additional reagent blanks accordingly.


M29SUCX WPO June 19. 1996 (rsv. M29SUC3.WPO January 20. 1997)

A R 3 I 5 6 U UAPPENDIX B 138

40 CFR 60, APPENDIX A, METHOD 29 - MODIFIED MULTIPLE METALS TRAIN (MM5MM)FIELD LABORATORY SAMPLE RECOVERY DATA




Run No. — Sampling Train No. //l/ft- /M/h - / Sample Box No.Transfer for Recovery:Relinquished By -Ja~ ______ Received By -Stft * —— Date/TimeSample box recovery person(s): 7T. /Yl<. (^ — . _________ . _____ __ _______ .__ Date: _ . < . .

Probe recovery person(s): P. (itr-jn-* -, J, &*~.. fa'cL. m**-, _.... _._„._. Date: .2r.t~Weights below are in grams.______________________________ BACKJdALE-RECO-YERY _____ '. _______ .

Impinger: Replacement1st 1st 2nd 3rd 4th 5th 6th 7th 8th

Final wt. 3137,0 A)*-Initial Wt. AU7.3 __ I __ dr~?7.Q <J7z>.* ._fl>-3.f ft.) 6~?3 O &Y3.7Net Wt. -I") 06.1 «T~ ' XfO.f _J_OCLJS _Z2£J_ ^.^ . > A-V

[ Total Condensate Collected: _-3=EZ5_._Description . t i tand/or color: t'lo-o s __ — cl»~~ d>~-s t-(&*-r- JtHu**. a oL- Q

Recovery: •-.•-»-.•-. » -* -. Impingers 1-3 «-- <^ *^ «-• •-• «- 4th Impinger ^ Impingers 5-6 *- % Blue'Sample Number: v_T!80 J181 J182 "183

Sampla Bottle Tars Wt. /-?/ f - 7 _Â^-6 _j2&S _ HO^

Sample Bottle Gross Wt. VYZia .( _ _______ ^ %3_._._ Before RinsesRinse Solutions: 0.1 N HNO3 0.1 N HNO3 KMnO4/H2O, then 8 N HCI

Components Rinsed*: filter support, filter holder back, **4th impinger ***5th-6th impingers, U-connectors D-E45/90° connector, 1st-3rd impingers, U-connectors A-C

Sample Bottle Final Wt. V..?_0_7,_Y. _=£??.£_ .. 671,7. Jf4,..7 After RinsesNet Sample Wt.

_..„__.._________L.—.._.._.;_____ERQN.T_HALE_RECQ_YERY___ .__..FILTER:Sample Number: $"179 Description/Color:TRAIN RINSES:

Sample Number: \78Sample Bottle Tare Wt. J7/.O

Rinse Solution: 0.1 N HNO3Components Rinsed****: nozzle, probe liner, bypass, filter holder front

Sample Bottle Final Wt.Net Sample Wt. f-3-

.* Using a total of 100 mLs ±2 mLs of 0.1 N HN03, rinse components twice.** Using a .total of 100 mLs ±2 mLs of 0.1 N HN03, rinse the impinger twice.

*** Using a total of 100 mLs ±2 mLs of 4% KMn04/10% H2SO4, rinse components 3 times; then, using a total of 100 rriLs±2 mLs of ASTM Type I water, rinse components 3 times to remove all purple color. Next, using a total of 25 mLs ±0.5mLs of 8 N HCI, remove any residue from components; transfer these rinses to a separate bottle containing one half of 200mLs ±2 mLs of ASTM Type I water; rinse components with the balance of the water and transfer to bottle.

**** Using a total of 100 mLs ±2 mLs of 0.1 N HN03, rinse components 3 times or more with brushing until perceivably clean.COMMENTS:

M2SRCCX.WPO June 20. 1996 (rev. M29RCC3.WPD January 20. 1997)

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AR3l56i*7APPENDIX B 141


Plant &H-rY( /€5C Z>/e/t/c£ Project No. 34r3f ?6ZO-/3-3oSampling LocatiSample Type (MFlow Control De\For Sampling FrcPump Type £

on ST#CJ< uPP&z. Lz.vjs.e- Run No. -5 -/x*<5O% Date £-/-?9-ulti-Point, Singrice Mlcrova4viDm MB~ConsoR

e=P0irit) yW Operator Z&TAiev^CritiTOl OrifioQ) -ge- y Baq Type Sample No. 5"/? "No. A/5" /' Method 3 Train No. ——

Pump Type • ——Pump I.D. /J<T . Pump I.D. ——Flow Meter TypeFlow Meter I.D.Desired Flow RELeak Check BefTotal Sampling "Flow Rate (cc/mEstimated Actua

Time24 Hr Clock/ /#/£j/

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ite (cc/min) / nDre Sampling p/fef After Sampling #755Ime (min) /77 Average Flow Meter Reading /_5~n): Average /S~<» Hiahest /5o Lowest /To1 Volume (liters

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• 7,5-— •/.T—/, $—/,1T————

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For ^ i s P ° C H iHSTlTUTEMIDWEST L-n

APPENDIX B 142

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40 CFR 266, APPENDIX IX - MODIFIED CHROMIUM TRAIN (MM5CR)FIELD LABORATORY TRAIN SET-UP DATA


Source Location: Lock Haven, PennsylvaniaSampling Location: Mobile Hazardous Waste Incinerator (HWI) Stack

Run No. . £ Sampling Train No. _r_ _______ Original Sample Box No.Backup Sample Box No. C&--2-

Set-up person(s): T -/ l* C-<*——•__________'.—————————————————— Date: —/-g/Transfer to Sampler: , SJ j j / -> / 01Original: Relinquished By t) * /*< <• <-*—- Received By */• s - ~-J Date/Time -*-( -*'Backup: Relinquished By J~-/M<- <L.—- Received By &.AJ-*-~J

_____„_________TRAIN COMPONENT____________ ___aOjMEQNENJLND_,. „ ............. LOADING-...Note: All sample-contact components are Teflon

unless specified otherwise. —Original _ .-.Backup.*...

Sampling Nozzle (Quartz) £f\-' * *Probe (Teflon Liner/STL) with Tee Assembly including

Solution Feed Line with Sprayer Tip and Gas Outlet Tube ______**Peristaltic Pump with C-Flex, Tygon, or other inert Tubing _______*,*

1st Impinger with Unrestricted Stem Tip andSolution Feed Line with Shutoff Valve ______*.*_ ______ * * 1.75 mLs __LJ!_ N KOH

2nd Impinger with Restricted Stem Tip and Gas Inlet Line _______ _______ 75 mLs ) • ° N KOH3rd Impinger with Restricted Stem Tip and Gas Inlet Line _______ _______ .75 mLs __/lcjL__ N KOH4th Impinger w/Unrestricted Stem Tip and Gas Inlet Line _______ _____._ 75 mLs /.. D _ N KOH

5th Impinger w/Unrestricted Stem Tip & Gas Inlet/Outlet Lines _______ _______ Empty6th Impinger (Glass, Mod-GBS) _______ ._____._. -200 g indicating silica gel

Glass U-Connector ______ ...___._ - _- _ _7th Impinger (Glass, Mod-GBS) ___..__ ..._ „._ _ -200 g indicating silica gel'

Impinger Outlet Connector _r ll.' LI

_„,_,,_„__.___,.___....__.._._______LQAD1N,G_QAIA_____________._ . . . _ _ . _ . -Weights below are in grams** *: .O.rJgiaaLS.ampLe_Bux- .B.ackjjp.SampleJB.QX.

Train Sample Number: .5185 -_5"185ASample Bottle Tare Wt.

Sample Bottle Gross Wt.Initial KOH Solution Net Wt.

6th 7th 6th 7thInitial Silica Gel Impinger Wt(s).

* Backup impinger set for exchange at port change or as necessary when sampling high moisture gas streams or for longsampling runs (i.e., >2 hours).

* * Before and after sampling and during train transfer: Nozzle openings covered with Teflon® tape, and nozzle placed in Ziploc*bag. Probe liner inlet sealed with Teflon® plug. Probe liner outlet remains connected to tee assembly;-solution feed lineihlet and gas outlet tube (1st impinger stem) opening covered with Teflon® tape secured with caplugs. 1st Impinger inletsealed with Teflon® plug. Peristaltic pump loop closed.

*** Include initial weights of additional components and/or their contents (i.e., additional backups), as applicable, that areexchanged during the run. Cover all exchange component openings with Teflon® tape or as indicated above.

NOTE: If the pH of either of the first two impinger solutions was not gmater.than.8,5 after the previous run, increase the alkalinityhere, record the normality, and acquire another reagent blank set.


M5CRSUCX.WPO September 5. 1996 (rev. M5CRS23XAVPD January 20, 19971


40 CFR 266, APPENDIX IX - MODIFIED CHROMIUM TRAIN (MM5CR)FIELD LABORATORY SAMPLE RECOVERY DATA



Run No. i3 Sampling Train No. -/ L L.< L — / _. Original Sample Box No. <Backup Sample Box No.

Transfer for Recovery:Origfnal: Relinquished By •A'^—____ Received By 7\/***-.*?„ -____ Date/Time J7-/-Backup: Relinquished By P - *Jn~*4______ Received By T> /n<. Co~~— Date/Time 3- ~~1 ~ 77_ ,<3. £L..Sample box recovery person(s): J./W'- f> __________- ____________^^..Date: -2- -/-?7__

Probe assembly recovery person(s): J . 5t-w—v^.—___________________________ Date: 3—i ~ 77

TRAIN PURGES*: Original: Date/Start Time l-/-?? /S~-2-Q Stop Time /£$<3rPurged By u^>/>/r^ <^——__________ Backup: Date/Start Time 2-1 ~*?~l J/52Q Stop Time _____Purging Gas:_Pj purifiej±Mtxa_gexi__ Flow Rate: /* Liters/minute Desired Time:. ___ minutes/irnpinger box

TRAIN RECOVERY: Weights below are in grams.Impinger: ' 1st 2nd 3rd ' 4th 5th ' 6th 7th

Description/Color: . ,Original Set: Cf<t<a-~~- <J ~-~- __^c/w^_ clsf =- _ —~~ . , % Blue: _.*3-£l__ _ _ — - _ . _ .Backup Set: d»~ cJ* - c/a><- cd** - ..... ~-~ . % Blue: ASTCheck pH**: Must be greater than 8.5 in first four impingers.Original Set: ' __f .S ___ __£JC__. _ . CT_ -*'J~ - -~" Final Wt.:Backup Set: 7-° _ £=£!__- T-^ 7-*~ ~- - Final Wt.:

Total Initial Silica Gel Impinger(s) Wt. for Original and Backup Set from Set-up Data:A. . . . - - - - - - . . - - - . - - - - - - - - - - - - - - - . - - Total Silica Gel Impinger(s) Weight Gain:

Train Sample Number: -ST85 -*"185AB. ...-----. Sample Bottle Tare Wt. From Set-up Data:C. - - - - - - - - - - - - - - - - - Current Sample Bottle Gross Wt. /.? f-J ?J.f Before RinsesD. - - - - - - - - Sample Bottle Gross Wt. From Set-up Data: -5 ?7g >' VE. . . - - - - . - . . - - - - - - Net Liquid Condensate Collected _ !dL_ _ 79*73 [C - D]

TOTAL CONDENSATE COLLECTED: _//L&*?£<£ [A+totalofE]Components Rinsed***: All components from nozzle through 5th impinger

Sample Bottle Gross Wt. /5*7V--3 _ —L£j&-JL. After All Rinses AddedCheck pH a9 ****, pH: ? ? <?.* Before Adjustment

pH: _______ _______ After AdjustmentF. ...................... Sample Bottle Final Wt.

Net Sample Wt. _iV_^*iZ. . [Total of F - Total of Bj

FILTRATION OF SAMPLE NOS. 185 and 185A , 0.45 m Filter Type:Filter Lot Number:

Filtrate Sample Number: ^ "186 Residue Color: _ e&jL-Li if- „Sample Bottle Tare Wt.

Sample Bottle Gross Wt. • r?v5S" J «- Including Rinses of Filtration ApparatusNet Sample Wt. .?-2.2.7. f *- For Hexavalent Chromium Mass Collected Computations

Sample Mixed, Then:Sample Aliquot for Analysis -.-.-.-.-.-.-.-. for Cr*6

Aliquot Sample Number: -5"187Sample Bottle Tare Wt. /7-3Sample Bottle Final Wt. 33. V J^b.S

Net Sample Wt. 3 /a6.f /2-3,2.

* Gas used for purge is passed through 0.1 N KOH in an impinger before entering train.** pH checked with glass rod and pH indicator strips; solutions adjusted for subsequent runs as necessary. Void run if pH

of any impinger (1st through 4th) is s8.5..*** Using a total of about 150-200 mLs of ASTM Type I water for each impinger set, rinse components 4 times. Use a total

of at least 100 mLs to rinse the nozzle, probe liner, tee assembly, and peristaltic pump tubing 4 times.**** Thoroughly mix sample and check pH; adjust to pH 9-10 with 2 N KOH if necessary.

COMMENTS:

MSCRRCCX.WPO Septembers. 1996 (rev. M5CRH23X.WPD January 20, 19971

A R 3 I 5 6 5 IAPPENDIX B 145

SOLID WASTE FEED SAMPLING DATA

MRI Project No. 3620.13.30Client/Source: OHM Remediation Services Corp., Drake Chemical Superfund Site, Mobile Hazardous Waste Incineratoi

Source Location: Lock Haven, Pennsylvania

SAMPLING LOCATION: At the solid waste feed conveyor to the kiln in the solid waste storage and preparation building.

SAMPLING METHOD: Equal-sized grab samples of approximately 100 grams each collected with an aluminum* scoop frommaterial on the apron conveyor belt. Grab samples deposited, combined, and mixed in an aluminum* pan; then cut and splitinto 16 oz., wide mouth, precleaned, clear glass bottles. Bottles sealed with Teflon®-lined screw caps. (*As per COEprotocol.)

SAMPLING FREQUENCY: One (1) grab sample collected every 15 minutes during the run. Sampling conducted continuallyaccording to schedule except during stack port changes on the stack and delays incurred during the run as noted below.

y*%i ICTCi ^ 1 "*£ *jEf)V./ ^ ' T"T i *" *•*'SAMPLE PRESERVATION: All samples, XXÔ^stored at near water ice temperature (i.e., 4°C), and bottles wrapped inaluminum foil. All samples, XX121, stored at near water ice temperature (i.e., 4°C). All samples, XX122, stored at nearroom temperature or cooler (i.e., 26°C).

, , __ — ^ ^? .Run No. £~ Date: _/-'../...? ']L~

Composite Sample Number:Composite Sample Designation:

Grabime_ _____________________ Interruptions/.Comments

Caution: Material may contain P-naphthylamine.

/// „ /^ 6} s),, /Relinquished By _ >?fe«< ;pc <_- Received By fi*J< (/f/r( _.. _..__._ Date/TimeWSTFEEO3.WPD February 1, 1997



MRI Project No. 3620.13.30Client/Source: OHM Remediation Services Corp., Drake Chemical Superfund Site, Mobile Hazardous Waste Incinerator



SAMPLING METHOD: Equal-sized grab samples of approximately 100 grams each collected with an aluminum* scoop frommaterial on the apron conveyor belt. Grab samples deposited, combined, and mixed in an aluminum* pan; then cut and splitinto 16 oz., wide mouth, precleaned, clear glass bottles. Bottles sealed with Teflon®-lined screw caps. (*As per COE

*- \ v^ ' ...*" " v-^sT

SAMPLING FREQUENCY: One (1) grab sample collected eVecy.,.3-5'minutes during the run. Sampling conducted continuallyaccording to schedule except during stack port changes on the "stack and delays incurred during the run as noted below.

SAMPLE PRESERVATION: All samples, XX120,_/>stored at near water ice temperature (i.e., 4°C), and bottles wrapped inaluminum foil. All samples, XX121, stored at near water ice temperature (i.e., 4°C). All samples, XX122, stored at nearroom temperature or cooler (i.e., 26°C).

Run No. -> Date: *3 /' / fffZ______ Sa;/ * f ^—Composite Sample Number:

Composite Sample Designation:

GrabTime.._ ..__.___

Caution: Material may contain (3-naphthylamine.

J_J_________/__

WSTFEED3.WPD FeBttJary 1. 1997

Relinquished By Q f-z tc - 'i ' Received By Z> 'C(jlJ!s~J Date/Time 22* ' ~

AR3I5653

(lor* £~ (_SOLID WASTE FEED SAMPLING DATA (SAMPLE FOR COE) ' f* \ «/(




SAMPLING METHOD: Equal-sized grab samples of approximately 60 grams each collected with an aluminum* scoop frommaterial on the apron conveyor belt. Grab samples deposited, combined, and mixed in an aluminum* pan; then cut and splitinto a 16 oz., wide mouth, precleaned, clear glass bottle. Bottle sealed with Teflon^-lined screw cap and wrapped in aluminumfoil to seal out light. (*As per COE protocol.)

SAMPLING FREQUENCY: One (1) grab sample collected every 15 minutes during the run. Sampling conducted continuallyaccording to schedule except during stack port changes-on the stack and delays incurred during the run as noted below.

SAMPLE PRESERVATION: All samples stored at near water ice temperature (i.e., 4°C), and bottles wrapped in aluminum foil.

Run No. __••>.____ Date: _O2-/- -/.-?..?-.--—. Sampler(s): ^'L^ f- / . <> S


Grab.No... _Time_ _ ..,_'__,_.__„_,_______lnternjptions/Comments.___,^_^ Caution: Material may contain P-naphthylamine.Qy

,-7Relinquished By ., £rWSTFED3C.WPO Ftbroa'cy'l. 1997

APPENDIX B 148

SOLID WASTE FEED SAMPLING DATA (SAMPLE FOR COE) -




SAMPLING METHOD: Equal-sized grab samples of approximately 60 grams each collected with an aluminum* scoop frommaterial on the apron conveyor belt. Grab samples deposited, combined, and mixed in an aluminum* pan; then cut and splitinto a 16 oz., wide mouth, precleaned, clear glass bottle. Bottle sealed with Teflo'n®-lined screw cap and wrapped in aluminumfoil to seal out light. (*As per COE protocol.)

SAMPLING FREQUENCY: One (1) grab sample collected every 15 minutes during the run. Sampling conducted continuallyaccording to .schedule except during stack port changes on the stack and delays incurred during the run as noted below.


Run No. Q Date: .°L./,J_ l L L.,. ..-.. Sampler(s): .. "hvj._./: // .


Grab ._ lime _ .. __________ " __________ Interruptions/Comments _ _..,._.._ .. _ _._ .___.„

Cautitjn: Material may contain p-naphthylamine.-

dj •&-*3\

Relinquished ByWSTFSD3C.WPD February >f

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/"

POHC (1,4-DICHLOROBENZENE) SAMPLING DATA




SAMPLING METHOD: One (1) grab sample collected from a randomly selected POHC spike bag. Grab sample collected witha plastic scoop and placed into a 16 oz., wide mouth, precleaned, clear glass bottle. Bottle sealed with Teflon*-lined screwcap and wrapped in aluminum foil to seal out light.

SAMPLING FREQUENCY: One (1) grab sample collected during the trial burn.

SAMPLE PRESERVATION: All samples stored at near water ice temperature (i.e., 4°C), and bottles wrapped in aluminumfoil.

Run No. *T _____ Date: 2- - ( - T _____ Sampler(s):

^Grab Sample Number: f S12S

Lot Number: ~/ H < ?/ /. )

Time _________________________Interruptions/Comments

Relinquished By >/Lc (sV -t* :_____ Received By XJ £c2-fr~ Date/Time -Z-Y-f 7

POCHDCB.WPD October 28. 1996 TAR3I5662

APPENDIX B 156

POHC (NAPHTHALENE) SAMPLING DATA




SAMPLING METHOD: One (1) grab sample collected from a randomly selected POHC spike bag. Grab sample collected witha plastic scoop and placed into a 1 6 oz., wide mouth, precleaned, clear glass bottle. Bottle sealed with Teflon'Mined screwcap and wrapped in aluminum foil to seal out light.


SAMPLE PRESERVATION: All samples stored at near water ice temperature (i.e., 4°C), and bottles wrapped in aluminumfoil-

Run No. <"" Date: £-\-3~7_______ Sampler(s): 0.

Grab Sample Number:

Lot Number: VoQ I / (• (7

Time _________________________Interruptions/Comments

y 4 / jgy$ r A

Relinquished By Xy. /3*Asj_______ Received Byp

POHCNAPH.WPO October 28, 1996

157

O U «,5"

C

METALS SPIKE SAMPLING DATACondition 2




SAMPLING METHOD: One (1) grab sample of a randomly selected metals spike bag. Entire, intact bag placed into a plasticbag, and bagged package placed into a metal can. Can sealed with metal lid.


SAMPLE PRESERVATION: All samples stored at near water ice temperature (i.e., 4°C).

Run No. _JL ____ Date: JL^< — f ? __ Sampler(s):

Grab Sample Number:

Arsenic Lot Number:

Beryllium Lot Number:

Cadmium Lot Number: Ô6~Jff /\ . (

Chromium Lot Number: ~7 2-05 &/ 1- (

Lead Lot Number: ? // . Im l.i-fJ,. <? 6 of 2 /f • '_

Time., _ „ ______ Interruptions/Cnmrnents _____

ft fa

Relinquished By

METLSPK2.WPO January 20. 1997 .

Date/Time __-/-<77> /5T

APPENDIX B 158

BOTTOM ASH SAMPLING DATA

MRI Project No. 3620.13.30Client/Source^/ OHM Remediation Services Corp., Drake Chemical Superfund Site, Mobile Hazardous Waste Incinerator


SAMPLING LOCATION: In the bottom ash storage building. Grab samples collected from the front end loader used fortransfering ash from the ash pile at the final drop off of the belt conveyor system from the kiln.

SAMPLING METHOD: Equal sized grab samples of about 200 grams each collected with an aluminum* scoop. Grab samplesdeposited, combined, and mixed in an aluminum* pan; then cut and split into 16 oz., wide mouth, precleaned, clear glassbottles. Bottles sealed with Teflon®-lined screw caps. (*As per COE protocol.)


SAMPLE PRESERVATION: All samples, XX126 and XX127, stored at near water ice temperature (i.e., 4°C), and bottleswrapped in aluminum foil. All samples, XX1 28, stored at near water ice temperature (i.e., 4°C). All samples, XX1 29, storedat near room temperature or cooler (i.e., 26°C).

Run No. _2_____ Date: *•' '" ' '______ Sampler(s):

Composite Sample Number: f f~126 /^fiTl27 )\ xxj128Composite Sample Designation: I SVOC (J VOC \ QfCLP/METALSj GALBT

Grab ———_JJme ... _____________________^.laterr.uptions/_Cojxim.ej3ts____

fJ-- J<3/-v ,MX>i . r~ $

(£) J2&— i fi v~ f tt_re-l -S

Relinquished By ^ - . - . . - Received By y.^ _ __ Date/Time '__

BOTMASH3.WPD January 20, 1997


BOTTOM ASH SAMPLING DATA (DUPLICATE SAMPLES)






SAMPLE PRESERVATION: All samples, XX170 and XX171, stored at near water ice temperature (i.e., 4°C), and bottleswrapped in aluminum foil. All samples, XX172, stored at near water ice temperature (i.e., 4°C). All samples, XX1 73, storedat near room temperature or cooler (i.e., 26°C).

Run No. -3" Date: "2.-J-37 . Sampler-Is): &* 31-£

Composite Sample Number: f $"170 )/^ «"!71'\ / ri72 ^ (j 5^173Composite Sample Designation: I SVOCyt; VOC ) (CLP/METALS^ GALBT

GrabNn. _lime_ ____________________lnterxupJions/.CQmmejits_

Relinquished By Cy.,.ii Kr a4 Received By4i= .CtZ6-Jy\ Date/Time

BOTMSH3O.WPO January 20. 1997

. AR315666APPENDIX B 16O

BOTTOM ASH SAMPLING DATA (SAMPLE FOR COE)



SA'MPLING LOCATION: In the bottom ash storage building. Grab samples collected from the front end loader used fortransfering ash from the ash pile at the final drop off of the belt conveyor system from the kiln.

SAMPLING METHOD: Equal sized grab samples of about 200 grams each collected with an aluminum* scoop. Grab samplesdeposited, combined, and mixed in an aluminum* pan; then cut and split into a 16 oz., wide mouth, precleaned, clear glassbottle. Bottle sealed with Teflon®-lined screw cap. (*As per COE protocol.)



Run No. f Date: _2-~ \ ~ '7_____ Sampler(s): ^» /^ L/?./ r V____._________. ,

Composite Sample Number;Composite Sample Designation:

Grab_lime_ ____:__________!____JniBttuptiflDsZCQtnmfints__ __

±

(Hi i. - " ,. <•<• rt<fr<J^s

— £* —____

Relinquished By i^..<^^-T~^ . Received By :. , Date/Time •.

BOTMSH3C.WPD January 20, 1997

flR3l5667161

,2-)FLY ASH SAMPLING DATA



SAMPLING LOCATION: At the drop off of the fly ash pugmill discharge conveyor from the baghouse and evaporative cooler.

SAMPLING METHOD: Equal sized (approx. 100 grams) grab samples collected with an aluminum* scoop from each ofeJgbteerrftST specially spaced points over the surface and from a depth of 3 to 6 inches below the surface of the pile in thedump truck bed located under the end of the conveyor. Grab samples deposited, combined, and mixed in an aluminum* pan;then cut and split into 16 oz., wide mouth, precleaned, clear glass bottles. Bottles sealed with Tefion®-lined screw caps, (*Asper COE protocol.)

SAMPLING FREQUENCY: Grab samples collected immediately after the end of the run.

SAMPLE PRESERVATION: All samples, XX130 and XX131, stored at near water ice temperature (i.e., 4°C), and b'ottleswrapped in aluminum foil. All samples, XX1 32, stored at near water ice temperature (i.e., 4°C). All samples, XX1 33, storedat near room temperature or cooler (i.e., 26°C).

Run No. __5___ Date: ? - / -JJL7 _____ Sampler(s):/ \

Composite Sample Number: / /130 1 "Composite Sample Designation: I SVOC f

Event_Ncu __Tinne _ _____________ Interruptions/Comments

4

5

6

7

8

9

•10

Relinquished By £zJ. C t L ., . ... _ Received By .dL t& l- „ , Date/Time Z'J-J ?<T

R.YASH3.WPO January 20. 1997


FLY ASH SAMPLING DATA (DUPLICATE SAMPLES)




SAMPLING METHOD: Equal sized (approx. 100 grams) grab samples collected with an aluminum* scoop from each ofaigfatseft i'tO) specially spaced points over the surface and from a depth of 3 to 6 inches below the surface of the pile in thedurfif) truck bed located under the end of the conveyor. Grab samples deposited, combined, and mixed in an aluminum* pan;then cut and split into 16 oz., wide mouth, precleaned, clear glass bottles. Bottles sealed with Teflon®-lined screw caps. (*Asper COE protocol.)



Run No. ^"" Date: Z • I • ? ?


Event '_..Na_, _lime_ ________________.___..Interruptions/Comments.......

OG

.24 ? _ £ _ . _ .

t:... ...„..._': ?

4

5

6

7

8

9

10

Relinquished By Zi^^3*^_,, ....... Received By JL. <>{*<<*. __ .... Date/Time . I /_

FLYASH3D.WPD January 20. 1997

AR3I5669

FLY ASH SAMPLING DATA (SAMPLE FOR COE)

MRI Project No. 3620.1 3.30Client/Source: OHM Remediation Services Corp., Drake Chemical Superfund Site, Mobile Hazardous Waste Incinerator



SAMPLING METHOD: Equal sized (approx. 100 grams) grab samples collected with an aluminum* scoop from each ofT eightaf" (1g| specially spaced points over the surface and from a depth of 3 to 6 inches below the surface of the pile in the

,-tfl ^faump truck bed located under the end of the conveyor. Grab samples deposited, combined, and mixed in an aluminum* pan;then cut and split into a 16 oz., wide mouth, precleaned, clear glass bottle. Bottle sealed with Teflon®-lined screw cap. (*Asper COE protocol.)



Run No. <"____ Date: Z-~ i -:9 7 Sampler(s): /), A1-6 •-' <*-~r* ...._. .._._. _

s ~"~~ \Composite Sample Number: f 5~137 IComposite Sample Designation: I COE )

Event- NQ._ ___Tirjae_ ___..__________________later.r.up.tLans/.CQmments____.. ____ __.

Q) jL}i9 __ jLjf f> f ;»*•><, r A^.^ ^

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7

8

9

10

Relinquished By /j.^^.. __ Received By /« .{2/6*.-u-. .„.„_.. Date/Time /?-/- 7*

FLYASH3C.WPD January 20, 1997


_________Run6Field Sampling Data

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Source Location: Lock Haven, PennsylvaniaSampling Location; Mobile Hazardous Waste Incinerator (HW!) Stack

Run No. (, Sampling Train No. /W/H.Z' ' Ptf "J2 Sample Box No. {J/2.QQ fSet-up person(s): tf. ( <- OS.A A ____________________________ Date: L///f "7

Transfer to Sampler:Relinquished By "5", f lcCa./vA Received By X) . NJ g^\ ___ Date/Time ZL/'z./'i 7

~

TRAIN COMPONENT COMPONENT NO. ______________ LOADING DATA

Sampling Nozzle (Quartz) #~ ____ * Initial Weights (grams)**Probe (Liner-Glass) ____________ * ____ Empty ____ ___ Loaded

Female' Probe Outlet Blank-O,ff ___________90° Bypass __________ *

Filter Holder Front ____________ Filter Type: Whatman QM-AFilter Holder Back with

' Teflon® Filter Support ____________ __ Filter Number.- /) _____45/90° Connector ____________

1st Impinger (2-Liter, Mod-GBS) _____ ______ 50mLs±1mL /O2.l.f JO77.2.0.1 N H2SO4

1st Impinger Replacement _____ _____ • 50 mLs ±1 mL A/ar 1/f-e.ex 'U-Connector (A) ____________ ... 0.1 N H2SO4

2nd Impinger (GBS) _____ ______ 100 mLs ±2 mLs ,P7-7 >S9O. OU-Connector (B) ___________ 0.1NH2SO4

3rd Impinger (GBS) _____ _____ 100 mLs ±2 mLs ^?Q -2-U-Connector (C) ___________ 0.1 N H2SO4

4th Impinger (Mod-GBS) ______ _____ Empty• U-Connector (D) _____________ - •

5th Impinger (Mod-GBS) _____ _____ 100 mLs ±2 mLsU-Connector (E) ___________ 0.1 N NaOH

6th Impinger (Mod-GBS) _____ _____ 100 mLs ±2 mLsU-Connector (F) ___________ 0.1 N NaOH

7th Impinger (Mod-GBS) _______ _____ -200 g indicating silica gelU-Connector (G) _______________

8th Impinger (Mod-GBS) _____ _____ -200 g indicating silica gelImpinger Outlet Connector Lt ff~V _____

* Before and after sampling: Nozzle openings covered with aluminum foil or Teflon* tape, and nozzle placed in Ziploc® bag.Probe liner outlet sealed with glass female blank-off, and inlet sealed with Teflon® plug. Bypass inlet covered (not sealed)with aluminum foil.

** Initial weights of additional components exchanged during the'run also entered here. All exchange component openingscovered with aluminum foil. Teflon® tape or as described'above.


0050SUCX.WPO June'26. 1996 Irev. 0050SUC3.WPD October 31. 19961

AR3I5676



Source Location: Lock Haven, PennsylvaniaSampling Location: Mobile Hazardous Waste Incinerator (HWI) Stack ,jRun No. LQ Sampling Train No. M t^ 9 H ' <T~ ~~ Sample Box No. ffld-QOH

\TRAIN PURGE WITH ASCARITE-FILTERED AIR

Condensate in front-half? N O ______________________ Purged By AJ/H ____ ___________Date/Start Time: M/A _______ ________ Stop Time _________ Purge Rate: [AH = AJ/^ in.H,OJMoisture Removed? IVJ//V _________________________________________________Transfer for Recovery: . ^ i /Relinquished By /f . )~/dvJ Received By A . C /eA./W Date/Time 3-/2~/£j~1 /(?*] ' USample box recovery person(s): /Cw Oo-.re v-g g ' _______ bate:_______

Probe recovery person(s): if- G~o-f/*.cuii ~~TT C^nr<<f*; & • noiM-^- _________ Date: 3L./s /"\ "1Weights below are in grams.______________________________ BACK HALF RECOVERY _________________________________


Final wt. 3(-J3.S *j A .o 9/#J t2H.3 7 32 .(* S'S&t, £37.3Initial Wt. 10 77.5kNet Wt. 2_? 3 5".

cobr:

510.0

[ Total Condensate Collected: 3.g"7/. 3- j*

V/ Recovery: ->-»-*-*-. impingers 1-3 ~ <-«-«--•-*-'-•<- --» Impingers 4-6 ------ % Blue

•' Sample Number: &> 103 /3V<^'^' Vf5? ^ 105Sample Bottle Tare Wt. l/3/7,<r*^ ' 5" J

Sample Bottle Gross Wt. V<^ 3^7- /.( />5" Before RinsesComponents Rinsed*: filter support, filter holder back, 4th-6th impingers,45/90° connector, j}gt-3rd impingers, JJ-connectors A-B U-connectors C-E

Sample Bottle Gross Wt/7o< t>^ 7(a3&-efc5f7J3, 3 I <2. ~7-& After RinsesNet Sample Wt. 3 "S 5? 3--.C "7 ?$?. 7 for Mass Collected Computations

Sample Mixed, Then: for HCI for CI2Aliquot Sample Number: r//* 7^ 7 (0104 _->-.-.-. <^106 for Chloride AnalysisSample Bottle Tare Wt. i , .Sample Bottle Gross Wt. "7 /o?A~3~ o? <O~S. __ o_c ' < 77 0" / ^ 1? After AliquotingSample Bottle Final Wt. ^j A A) A After SIE Check

Net Sample Wt. 33.7V.3 /-?j?,CL 70?.

FRONT HALF RECOVERYFILTER:

Sample Number: (0 102 Description/Color: Ls 'tfr '/•ArrC< -*gVl

TRAIN RINSES: Sample Number: 6 101Sample Bottle Tare Wt. ,2.<->-? sComponents Rinsed**: nozzle, probe liner, bypass, filter holder frontSample Bottle Gross Wt. 3*?/.y with Acetone RinsesNet Acetone Sample Wt. / /Sample Bottle Final Wt. 2 OQ-Q with added Water RinsesNet Water Sample Wt. y£3 \a. 9—

A/* Using a total of 100 ml_s ±2 mLs ASTM Type I water per sample, rinse components twice. Thoroughly mix each sample

and added rinses before aliquoting.** Acetone rinses with brushing 3 times or more until perceivably clean. If any residue remains in a component, follow with

ASTM Type I water rinses with brushing until perceivably clean. Do not add any water rinses to the sample bottle untilafter the bottle is weighed with all of the acetone rinses.

COMMENTS:

OOSORCCX.WPO October 31, 1996 (r«v. 0050RCC3.WPO October 31, 1996)


THIS PAGE LEFT INTENTIONALLY BLANK

AR3I5678


FIELD REAGENT BLANK PREPARATION DATA



A /7 / ^~ i /si —-fBlank(s) Prepared By: /~J « —- /"g f j^f ___________ Oate: 9~~/?—/ /

Weights below are in grams.Sample Bottle Tare Bottle Gross ' Net Sample

_____Reagent Blank Description_____ Number Weight Weight Weight

Acetone for particulate matterVolume needed: 200 mLs '

Lot Number: /5M7V3 • 138 l(o*%.\ .3 ! 9 .- 7 lW. 3 .

Filter for particulate matterType: Whatman QM-A*

Filter Number: / (p /f JLot Number; «4lfJj3Ujrazy 6&'* . 139

TIASTM Type I Water for particulate matterVolume needed: 200 mLs

Lot Number: i3V3-&/f 6? _2 140 /V /eX- 3 (0 ff-

60 mLs ±1 mL 0.1 N H2SO4 plus20 mLs ±0.5 mL ASTM Type I Waterfor chloride0.1 N H2S04 Lot Number: TT 3'/ OH' Q

Water Lot Number: 12 S3-(*/<?/, -5* 141 °\ 1, "& / "75.7 "77 ;

50 mLs ± 1 mL 0.1 N NaOH, plus25 mLs ±0.5 mL ASTM Type I Waterf o r chloride - , • •••- . • • • • •0.1 N NaOH Lot Number: _Ej2_Z3LfjfL_

Water Lot Number: \1-/3.t,Y<;to 142 <?'o'* / 7 /• ( T?> '

NOTE: Lots may be identified above by a manufacturer's lot number or by the date of reagent preparation. If different lotsof a particular reagent are used, indicate the applicable test run number(s) and sampling location(s) where thetrain(s) loaded and/or recovered with that reagent are used (i.e., list each reagent blank sample number with theapplicable test run number(s) and sampling location(s) below).

Sample Number For Test Run Number(s) For Sampling Location(s)

COMMENTS:

0050BLX.WPO June 27, 1996 (rev. 00508L3.WPD October 31. 1996


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Plant D<>.|4- £>f//v/) K5^ Project No. Sampling LocatiSample Type (Mzlow Control De\=or Sampling Fr<Pump Type

on -\<-.\L O~J\<± (LWM') Run No. (ulti-Point, Singlrice (MicrovalveDm M5 Console

e-Point) i f Operator 6',', Critical Orifice) /''V Bag Type /-'No. ^•7 Method 3 Train

Pumo TypePump I.D. ' A-'-'? Purno I.D.Flow Meter TypeFlow Meter I.D.Desired Flow R£Leak Check BefTotal Sampling "Flow Rate (cc/mEstimated Actua

Time24 Hr Clock/21&/•2-V5"'("1<?0/-?/$"ry$<*)-$*/$ $A/1/ffO

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tore Samplina p<&&s. After Samplina /£<"ime (min) ' '// Average Flow Meter Reading ' I-On): Average (&& Hiahest / ^1 Volume (liters

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Comments

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DRAKE 3620. 13 S JLMM5SV QRSAT BAGTRIAL BURN SAMPLEFor disposal call: P. GQRMAN

flR3!558lAPPENDIX B 175

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AR315682APPENDTX R . T76






Run No. (o Sampling Train No. <S(/"J2.______ Sample Box No. ) Q»2o0_____Set-up person(s): /L/ e- -gLt , ~S".M<- &——__________________ Date: 3~/d~/£f I_______- - - ; «

Transfer to Sampler: . \Relinquished By /\-. C ;n C£SUAj?S' Received By j). f\)Q G.\_____ Date/Time <3-/9-|A7"/ jo 3O

TRAIN COMPONENT COMPONENT NO. _____________LOADING DATA_______________

Sampling Nozzle (Quartz) J/F'' * Initial Weights (grams)**Probe (Liner-Glass) _____________ * _______Empty____ Loaded

Female Probe Outlet Blank-Off ______________90° Bypass __________ *

Filter Holder Front ___________Filter Holder Back with Teflon®- Filter Type: Whatman QM-A

coated 316 SS Filter Support ___________45/90° Connector ___________

——————————— L /.o /. Condenser (Standard) ______ ____ Thermocouple No. / "7 (/)• ()XAD-2 Resin Cartridge (Standard) "7 (~~f)____ ~65 grams XAD-2 Resin + Surrogates V9£>- 6/Documentation of standards injection is separate); resin spiked on I / / <~ll£\ [ and maintained near 4°C until

1st Impinger (2-L Mod-GBS) _____ _____ Empty

1st Impinger Replacement ____________ Empty AJorU-Connector (A) ___________

2nd Impinger (Mod-GBS) _____ _____ 100mLs -S-S'Z. ~l _> £3- . oU-Connector (B) ______________ ASTM Type II Water

3rd Impinger (GBS) _____ _____ 100mLs 9 77- V ^ 7 9Û-Connector (C) ___________ ASTM Type II Water

4th Impinger (Mod-GBS) _____ _____ Empty 7 / 3. 7U-Connector (D) ___________

5th Impinger (Mod-GBS) _____ _____ -200 g indicating silica gel fr2l.U-Connector (E) ___________

6th Impinger (Mod-GBS) ____ _____ -200 g indicating silica gelImpinger Outlet Connector U H ~ 35

* Before and after sampling: Nozzle openings covered with methanol/methylene chloride/toluene/acetone-rinsed aluminumfoil, and nozzle placed in Ziploc® bag. Probe liner outlet sealed with glass female blank-off, and inlet sealed with Teflon*plug. Bypass inlet covered (not sealed) with methanol/methylene chloride/toluene/acetone-rinsed aluminum foil.

** Initial weights of additional components exchanged during the run also entered here. All exchange component openingscovered with methanol/methylene chloride/toluene/acetone-rinsed aluminum foil or as described above.

* * * Cartridge weighed with blank-offs in place; then, cartridge covered with aluminum foil to seal out light during storage andsampling.

Component Changes after Sef-up and before Recovery and Other Comments:

I023SUCX.WPD April 26. 1996 (r«v. 1023SUC3.WPD October 25. 1996)







Run No. ( o Sampling Train No. MM£ -> V "eA. Sample Box No. / 03-'% XTransfer for Recovery^ / /Relinquished BvT^ Câ r.T O Y\ Received By f\ '(L .t t cLH Date/Time SL/J~/?~1Sample box recovery person(s): A , (L 3.rg A c( < f _____________________ Date:

Probe recovery person(s): fc (5-or v a- iTT" C^y.Taflj ^-- /YdtP-c^_______ Date: 3-/?-/1 ~JWeights below are in grams. '

________RESIN CARTRIDGE AND IMPINGERS RECOVERY___________________Impinger: XAD-2 . Replacement

Cartridge* 1st 1st , 2nd 3rd 4th 5th 6thFinal Wt. S V; Lg> 3%07.3 Not flW 1( *0Initial Wt.Net Wt. 7. **

[ Total Condensate Collected:Description " J_A . d f ' ' ff : : /9 /9

and/or color: u L T (LsULfr- _\/__ CJuLjZS : CJLiLiV > cJjQAsu 5*2, /dSample Recovery: Cartridge* — 1st-4th Impingers and Replacement 1st tmpinger •" •- *- - % Blue

Sample Number: Ul11 u?112 tits _ qSample Bottle Tare Wt. V 3lftJ 'f3 tf " '

Transfer impinger contents only (i.e.] do not add component rinses to this sample).

Sample Bottle Final Wt. _____Net Sample Wt. 3 7'% ,'<-


FILTER RECOVERY AND TRAIN RINSES

FILTER: / -7" / / J-f--& >Sample Number: G7109 Description/Color: u .L f r' / i i _ u -r i T./

TRAIN RINSES: FRONT BACK QA RINSESSample Number: (y 108 6? 110 6 113

Sample Bottle Tare Wt. . Q (g3o °3.(a3• 3-~ , Y*9 /• 6>Components Rinsed***: Front -- nozzle, probe liner, bypass, filter holder front;


Sample Bottle Final Wt. "V/ 5"- 7_ '§7-7 //Net Sample Wt.


*** TRAIN FRONT/BACK RINSES: Methanol/methylene chloride (1:1 v/v) rinses with brushing of front components 3 times ormore until perceivably clean, and methanol/methylene chloride (1:1 v/v) rinses of back components 3 times, but withoutbrushing, and including 5-minute soaks of underlined components 3 times.QA RINSES: Follow with toluene rinses and soaks, but without brushing, in the same manner as above for the train frontand back rinses.

COMMENTS:

1023RCCX.WPD Juna 4. 1996 [rov. 1023RCC3.WPD October 25. 19961

AR3I568UAPPENDIX B 178

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Plant TVa&- (tyM &£. Proiect No. - xfe /T -•Jfc'Sampling LocatiSample Type (MFlow Control De\For Sampling Fr<Pump Tvpe

on *rte<-£ c'&S/C'f . Run No. ' bate •z-?-'?'?ulti-Point, Singldee (Microvalvejm MS Console

e-Point) /7 " Operator r-,- - ., Critical Orifice) /%. Baq Type /• /v/ '-. Sample No. 6/ /No. '- 7<s Method 3 Tra'rn No. V/f-

Pump Type VPump i.D. A-'-lw Pump I.D. \Flow Meter TypeFlow Meter I.D.Desired Flow RELeak Check Bef<Total Sampling "Flow Rate (cc/mEstimated Actua

Time24 Hr ClockSZ.70'*}/Z </?- 5"no*.*;nis .<?/?7<7-5"Wf-T/y*<=-5/ /" y/y*&/5t°/5l<?/•f3a>wr

/£#&

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ite (cc/miti) A->&Dre Samplina /2«-"ime (min) /-/ Averaoe Flow Meter Reading ' /-^n): Averaae /d«? Hiahest /*•&- Lowest A51 Volume (liters

Flow MeterReading/-«?/-<?Ac?/-e/'-C/.<?/-C/-<?/,a/-*/,<=>/,o

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DRAKE 3620.13 S J. J_ £MM5MM QRSAT BAGTRIAL BURN SAMPLEFor disposal call: P.GQRMAN

a r. ,-> , r- MIDWEST RESEARCH INSTITUTEflR315687

APPENDIX B 181

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MRI Project No. 3620.1 3.30Client/Source: OHM Remediation Services Corp., Drake Chemical Superfund Site, Mobile Hazardous Waste



Run No. b Sampling Train No. Mfi\J MM- 7 Sample Box No. O\^~OC>O ,Set-up person(s): A - C_-& rO nd T ______________ Date: pL./l/(? ~J

Transfer to Sampler: 'Relinquished By /4 - -«->-a~«L« — Received By 0- AJ-e- J __________ Date/Time 2. ~2-?7 /03 0 _

TRAIN COMPONENT COMPONENT NO. ________________ LOADING DATA _________________

Sampling Nozzle (Quartz) /ffjft'3- * Initial Weights (grams)**Probe (Liner-Glass) ____________ * _____ Empty ___ ___ Loaded

Female Probe Outlet Blank-Off __________90° Bypass __________ *

Filter Holder Front ___________Filter Holder Back with Filter Type: Whatman QM-A

Teflon® Filter Support ___________45/90° Connector ___________

1st Impinger (2-L Mod-GBS) _____ _____ Empty

1st Impinger Replacement ________ _______ Empty NOJ- LJS 6{U-Connector (A) ___________

2nd Impinger (Mod-GBS) ______ _______ 100 mLs ±2 mLs V<£ $"> £ ~7£>- U-Connector (B) ____________ 5% HNO3/10% H2O2

3rd Impinger (GBS) _____ _____ 100 mLs ±2 mLs SOÔ- (a 6//i 7 ______U-Connector (C) _ _________ __ 5% HNO3/10% H2O2

4th Impinger (Mod-GBS) _____ _____ Empty 4"9"7iL / _____U-Connector (D) ____________

5th Impinger (Mod-GBS) _____ _____ -200 g indicating silica gel b J o- • (aU-Connector (E) ____________

6th Impinger (Mod-GBS) _____ _____ -200 g indicating silica gel <£? -_7 3-. - 3Impinger Outlet Connector UH — o

* Before and after sampling: Nozzle openings covered with Parafilm* or Teflon"1 tape, and nozzle placed in Ziploc* bag. Probeliner outlet sealed with glass female blank-off, and inlet sealed with Teflon* plug. Bypass inlet covered (not sealed) withaluminum foil.

* * Initial weights of additional components exchanged during the run also entered here. All exchange component openingscovered with Parafilm®, Teflon® tape, or as described above.

Component Changes after Set-up and before Recovery and Other Gomments:

M29S CX.WPD Juno 19. 1996 (rev. M29S C3.WPO Oclobor 25. 1996)






Run No. L Sampling Train No. />?/faf MA1-Y Sample Box No.Transfer for Recovery:Relinauished Bv D-fJaaJ Received Bv 7-X* £~ — Date/Time _2-2~f7Sample box recovery person(s): ^>- /rf <- L*. — - Date:

Probe recovery person(s): £^ L-L-fsit^ . n > &c/j*c>s> L-Wts>s>;*c< /?» fevjlt,)*— Date:Weights below are in grams. ' ' ^ '

BACK HALF RECOVERYReplacement

Impinger: 1st 1st 2nd 3rd 4th • 5th

Final Wt. J3 J-fxD / F ? ??o.7 7 3.? ./ O/S.rInitial Wt. /OV2-r \ ~7d . ~ &//.V Wl.l (*$?.(*NetWt. WK.-5" \j^ 27 3 • ,2c,?.3 Vo4,2_ 3 $7. 2

:!: [ Total Condensate Collected:Description .and/or color: f Je-* - Cfe** - < jj t - r.l&o ^ O

Sample Number: £>117Sample Bottle Tare Wt. 73/ ,3

Sample Bottle Gross Wt. V7Y_T.<3 Before Rinses "Rinse Solution: 0.1 N HNO3

Components Rinsed*: filter support, filter holder back, 45/90° connector,1st-4rd impingers, U-connectors A-C

Sample Bottle Final Wt. ^T^^Cp-^ After RinsesNet Samole Wt. <3_0?' <o

FRONT HALF RECOVERY

FILTER: < - , ..Sample Number: ^116 Description/Color: U;U<'£e- //'*l~*-~xTRAIN RINSES: '

Sample Number: ^115Sample Bottle Tare Wt. /(*'7.t/

Rinse Solution: 0.1 N HN03Components Rinsed**: nozzle, probe liner, bypass, filter holder front

Sample Bottle Final Wt. r?&<£-~7Net Sample Wt. ?7. 3

/£JOJi-S-f?2-3-91

6th

£>si-31 2-6

, 3S?7, } ]

/£>i Blue

* Using a total of 100 mLs ±2 mLs of 0.1 N HNO3, rinse components twice.** Using a total of 100 mLs ±2 mLs of 0.1 N HNO_, rinse components 3 times or more with brushing until perceivably clean.

COMMENTS:

M29R_CX.WPD Septembsr 27, 1996 (rev. M29R_C3.WPO October 25, 1996)

AR3I569QAPPENDIX B 184

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on f -l- £&f/-o-i' &<!K;) i Run No. XL Date j? -^-5" 7ultPPoinb'Sinale-Point) Operator ^ Xv

Flow Control Device (jgfFcrovalygFor Sampling From M5 ConsolePump Tvpe S)/c,aks0-" -

Critical Orifice) Baq Tvpe/ v l, Sample No. »x No. AS 'ft Method 3 Train No. y

Pump Type /Pump I.D. >z/ H Pump I.D. /Flow Meter TypeFlow Meter I.D.Desired Flow ReLeak Check BefTotal Sampling "Flow Rate (cc/mEstimated Actua

Time24 Hr Clock/?3&/?YS-/3<y<=>/3/3-/3>3a/-? <<-•<-/&?&

;<S33./? <S&/V <s<,-x ' ^x s~/ <,-—/«r_?,-s>/<,- 5-/-&&>&

> /<e>-£ .*r*{-<~ Flow Meter Type /xt •? Flow Meter I.D. /

ite (cc/min) /<3e>ore Samplina s&s?<s-S After Samplinq jfy?Time (min) X.f < Averaae Flow Meter Readinq /'. on): Averaae /<? & Hiahest X? Lowest &\ Volume (liters

Flow MeterReading/<?&/&&/<*>&X X

s/<z3cy* £2&—

~/• ryx ^Stzyzy

/<&&/<&&S&&——

* /<?

Comments

/ -: /fi~_ &£<_? _ "^ x£}/£<9/£

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£ /£'

&£-£>£& /Cf ^&<£.

s£>4*1 £2? _/2 -*-* ^

DRAKE 3620.13 <_=. J-MM5MM QRSAT BAGTRIAL BURH SAMPLEFor disposal call: P.GQRMANMIDWEST RESEARCH INSTITUTE

flR3!5693APPENDIX B 137

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MR! Project No. 3620.13.30Client/Source: OHM Remediation Services Corp., Drake Chemical Superfund Site, Mobile Hazardous Waste



Run No. __ , _ Sampling Train No. _~ Sample Box No.Set-up person(s): <T-/Y(c f n- __________________ , __________ Date: «P ~3- ~

Transfer to Sampler:Relinquished By 77. /Vf«..<£ —— _____ Received By O • A/-Q — I __ Date/Time -£ "A -f

_ __ TRAIN COMPONENT COMPONENT NO. ________________ LOADING DATA

Sampling Nozzle (Quartz) s * Initial Weights (grams)**Probe (Liner-Glass) ____________ .* .. . . . ^_. . Empty_,___ ____Laadfid

Female Probe Outlet Blank-Off ___________90° Bypass _________ - .... * . . .

Filter Holder Front ___________ ,Filter Holder Back with Filter Type: Whatman QM-A

Teflon® Filter Support .._. ________ _45/90° Connector _________ .

1st Impinger (2-L Mod-GBS) . __.„ _____ Empty ../9jo<L-H__.._ ---

1st Impinger Replacement n#•' &*f *-™ EmptyU-Connector (A) _______ —.... ..

2nd Impinger (Mod-GBS) _______.. -. _ 100 mLs ±2 mLsU-Connector (B) _ ._.....- _._...... 5% HN03/10% H2O2

3rd Impinger (GBS) ...__________ 100mLs±2mLsU-Connector (C) _.__________., 5% HNO3/10% H2O2

4th Impinger (Mod-GBS) __________.EmptyU-Connector (D) __________^. . .

5th Impinger (Mod-GBS) _____ _____ 1 00 mLs ±2 mLs* * * __ JJO--?- __6U-Connector (E) '___________. 4% KMnO4/10% H2S0

6th Impinger (Mod-GBS) __________ 100 mLs ±2 mLs***U-Connector (F) ____________ 4% KMnO4/10% H2SO4

7th Impinger (Mod-GBS) ._____ — ._ -200 g indicating silica gel £> "f r.U-Connector (G) ___________

8th Impinger (Mod-GBS) __________- -200 g indicating silica gel ...£=> V'T/. . ._Impinger Outlet Connector JA^

* Before and after sampling: Nozzle openings covered with Parafilm® or Teflon® tape, and nozzle placed in Ziploc* bag. Probeliner outlet sealed with glass female blank-off, and inlet sealed with Teflon® plug. Bypass inlet covered (not sealed) withaluminum foil.

** Initial weights of additional components exchanged during the run also entered here. All exchange component openingscovered with Parafilm®, Teflon® tape, or as described above.

*** If the reagent was exhausted before the end of a previous run, use a larger volume (e.g., 200 mLs ±2 mLs) and documentbelow. Prepare additional reagent blanks accordingly.


M29SUCX '.VPD Junt 19. 1995 (rev. M29SUC3.WPD January 20. 1997)

3R3I5695APPENDIX B



IncineratorSource Location: Lock Ha.ven, Pennsylvania


Run No. _<L__ Sampling Train No. /ft/Kl-T /fl/V\.~2- Sample Box No. _Z°.Afj=!_____Transfer for Recovery:Relinquished By 0- M-» — •/ _______ Received By T- /*t>. £* —— Date/Time _2~2~T 7 76 J 0Sample box recovery person(s): J"./77<- C -' ________________ . . ____________ Date:

Probe recovery person(s): £*> Ae-sr,*" . JO . Z-t>^-^y f i_ tff sf. u* /? ' >jf~i__ Date:Weights below are in grams.________ __t_L .: _________________ BACK HALF RECOVERY


Final Wt.Initial Wt.Net wt.

[ Total Condensate Collected:Descriptionand/or color: _ 6s*-£i_ _ . . ... _ c/(?- <= _ clf

Recovery: ^. — -.-* -> •-.--. impingers i-3<-<-^^^^ 4th Impinger *-» Impingers 5-6 <-• % BlueSample Number: .180 ^181 <^182 6183

Sampla Bnttla Tare Wt. /3/<2.3- <£(>3.(, _..3,. ^ ,/,2/LSample Bottle Gross Wt. _f/y. .5_. .._.OiJ__ -jJ SlL t.-, __ Before Rinses

Rinse Solutions: 0.1 N HNO3 0.1 N HNO3 KMnO4/H2O, then 8 N HCIComponents Rinsed*: filter support, filter holder back, **4th impinger ***5th-6tb impingers, U-connectors D-E45/90° connector, 1st-3rd impingers, U-connectors A-C

Sample Bottle Final Wt. tf£J_3 L._ _74.4?%ST . - ..~7f. . . .3. ??.•_? After RinsesNet Sample Wt. _d2&L.Q_ .-T^/-? ._J/f?3.J. .

_______________ ...._-. ....—... _ , FRONT HALF RECOVERY

FILTER: - i r / - -L 4-r: fjuhj."**- / 1 *J~*-3Sample .Number: £.179 Description/Color:TRAIN RINSES: /

Sample Number: j£178Sample Bottle Tare Wt. ./£?- o __ ,


Sample Bottle Final Wt.Net Sample Wt.

* Using a total of 100 ml_s ±2 mLs of 0.1 N HNO3, rinse components twice.** Using a total of 100 mLs ±2 mLs of 0.1 N HNO3, rinse the impinger twice.

*** Using a total of 100 mLs ±2 mLs of 4% KMnO4/10% H2S04, rinse components 3 times; then, using a total of 100 mLs±2 mLs of ASTM Type I water, rinse components 3 times to remove all purple color. Next, using a total of 25 mLs ±0.5mLs of 8 N HCI, remove any residue from components; transfer these rinses to a separate bottle containing one half of 200mLs ±2 mLs of ASTM Type I water; rinse components witlrthe balance of the water and transfer to bottle.

**** Using a total of 100 mLs ±2 mLs of 0.1 N HNO3, rinse components 3 times or more with brushing until perceivably clean.COMMENTS:

M29RCCX.WPO Jure 20. 1996 (rev. M29RCC3.WPO January 20. 1997)

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Plant QZAxg. QH-m gsc Project No. 3<t>Z&-f£ -3£>Samolinq Location ST/KJ<: tP£.g. t&v&t. Run No. <&-c/z.£ Date 2-2-77-SnmpiP Typ« rra7iTti-Pnir|trpinrj|p-Point) MP Ooerator y^/A^y. /ue/fcFlow Control Device " grovajvgFor Sampling From M5 ConsolePump Type &£ft£>ttizsl&/tf

^Critical Orifice) Baq Type /T&jJrS' 'Sample No. (ei'SSNo. A S' Method 3 Train No. -— —

Pumo Tvoe .- ————Purno I.D. /\A5 Pump I.D. —— -Flow Meter TypeFlow Meter I.D.Desired Flow ReLeak Check BefTotal Sampling 1Flow Rate (cc/mEstimated Actua

Time24 Hr ClockIZ301231IVoo\M3O

5iq - \ \iltfOO

1 JZofftmer&s. Flow Meter Type — — 'A/5" Flow Meter I.D. — —

ite (cc/min) /5"oore Samplina •?=7xfe< • After Samolina -PftS-*Time (min) //?/- Averaqe Flow Meter Readinq J^'n): Average /JTP Hiahest /cri? Lowest /'-Si?1 Volume (liters

Flow MeterReadingI.ST1-5"——

\,ri . "—

,\ f? 7

Comments

p ,Z(,£ t.X: £

STftfe T~ •SftvU. P C_ZTyO (-,

STOP S.ftwi£\ Tt Wo 'po£.7~ C,tHVtOfo£'Pue<be. djoe:< j j V -T" ,<> /YM-F>(~3rNJfoSTO s/aoM.?>ci ifc> e oti OF i2cA.o

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DRAKn. 362O. ij t=. J- <e.MM5CR ORSAT BAGTRIAL BURN SAMPLEFor disposal call: P.GQRMANMIDWEST RESEARCH INSTITUTE


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MR! Project No. 3620.13.30Client/Source: OHM Remediation Services Corp., Drake Chemical Superfund Site, Mobile HWI


Run No. _ >... _ Sampling Train No. __ C^- ~~ I _____ ... Original Sample Box No. < I/£ -I _Backup Sample Box No. C /^ -z- _

Set-up person(s): _____________________________________ Date:Transfer to Sampler: __ _ .Original: Relinquished By J • /"- ~—- Received By fi.fO -*-) Date/Time ~ -~ /Backup: Relinquished By ^- /?><• •£— - Received By J?' X>-<W ____ Date/Time J- .-'t'?

IBA1N.CQMEQNENI ____________ COMPONFNT NO. _____ LOADINGNote: All sample-contact components are Teflon

unless specified otherwise. _O_ugiaal_ _B.ack.upJL.

Sampling Nozzle (Quartz) C&-1 *»Probe (Teflon Liner/STL) with Tee Assembly including

Solution Feed Line with Sprayer Tip and Gas Outlet Tube _____** _..Peristaltic Pump with C-Flex, Tygon, or other inert Tubing ______** _ .

1st Impinger with Unrestricted Stem Tip andSolution Feed Line with Shutoff Valve ______.** _____.»* 175 mLs __/•_____ N KOH

2nd Impinger with Restricted Stem Tip and Gas Inlet Line ________ __ .____ 75 mLs __/„_£._ N KOH3rd Impinger with Restricted Stem Tip and Gas Inlet Line .__ ____ __... _. _ 75 mLs ,.„../•<•{ N KOH4th Impinger w/Unrestricted Stem Tip and Gas Inlet Line _______ __„.„._ 75 mLs ...,/.-J-L N KOH

5th Impinger w/Unrestricted Stem Tip & Gas Inlet/Outlet Lines _______ ._____„_ Empty6th Impinger (Glass, Mod-GBS) ._.___._ _,___ __ -200 g indicating silica

Glass U-Connector ______ _.. .__ ._. __7th Impinger (Glass, Mod-GBS) _______ _.____,_ -200 g indicating silica gel

Impinger Outlet Connector It)l-'

_________ ____________________________LOADING DATAWeights below are in grams* **: _OdginaLS.ample_Bnx_ jLackup_Sample_Box_

Train Sample Number: C.185 C185ASample Bottle Tare Wt. /VLJ..3

Sample Bottle Gross Wt. ,_Initial KOH Solution Net Wt.

6th 7th • 6th 7thInitial Silica Gel Impinger Wt.s). _<


* * Before and after sampling and during train transfer: Nozzle openings covered with Teflon® tape, and nozzle placed in Ziploc'bag. Probe liner inlet sealed with Teflon® plug. Probe liner outlet remains connected to tee assembly; solution feed lineinlet and gas outlet tube (1st impinger stem) opening covered with Teflon® tape secured with caplugs. 1st Impinger inletsealed with Teflon® plug. Peristaltic pump loop closed.


NOTE: If the pH of either of the first two impinger solutions was not gceater_than-8J5 after the previous run, increase the alkalinityhere, record the normality, and acquire another reagent blank set.


MSCRSUCX.WPO Seoiemoer 5. 1996 trev. M5CRS23X .VPD January 20. 1997)





Run No. (Q Sampling Train No. <^- I_____ Original Sample Box No. £!/£—/Backup Sample Box No. C. «- -2-

Transfer for Recovery:Original: Relinquished By j L/y -4_______ Received By -I"./»?. £ - Date/Time ...&r?l,_Backup: Relinquished By Âl-a^-J_______ Received By _ 7,/>u _/"-—- Date/Time J._~2jr?2_Sample box recovery person(s): 7.*/s?lc £•——______________________ Date: 2-2.

Probe assembly recovery person(s): P-drt'-)-j &-• JJtJvs*'*-> __________._______,_ Date: _<£l

TRAIN PURSES*: Original: Date/Start Time 3.~2-?7.. /S o Stop TimePurged By J -X?7* c£ —— • ___________ Backup: Date/Start Time -2-?7 /C V.3 stop Time 7_7./-3_

, Purging Gas: Prepurified Nitrogen Flow Rate: /6 Liters/minute Desired Time: -? - minutes/impinger box

TRAIN RECOVERY: Weights below are in grams.Impinger: 1st 2nd 3rd 4th 5th . 6th 7th

Description/Color:Original Set: c(*~*~- de <- __cks? z._ c/e _....-— . '% Blue: 3$Backup Set: _ c/g _> __ sUe _ cj<*-. ct"- • —— % Blue: -3" TOCheck pH* *: Must be greater than 8.5 in first four impingers.Original Set: <?.O f-S' __J*Lf___ f-T — Final Wt.Backup Set: f- O r,^ f.-T f.T — Final Wt. _ -

Total Initial Silica Gel Impinger(s) Wt. for Original and Backup Set from Set-up Data: _.£2.LZ±.2r_ _Z f2A. .. - , - - - - - - , - —— — - - - - - - - - , - - - - - - - . Total Silica Gel Impinger(s) Weight Gain: < _/.?L2_

Train Sample Number: 6185 6185AB. - - - - - - - - - Sample Bottle Tare Wt. From Set-up Data: /.2J -3 .- ,./ 3.-f.C. - - . - - - . - . . - - - - . - Current Sample Bottle Gross Wt. _/J.6..L&— _.. ./5S.OT.J " Before RinsesD. - - - - - - - - Sample Bottle Gross Wt. From Set-up Data: _.J?3 41_ ._£3.3.fE. - . . - . - - - . - - - . , - - - Net Liquid Condensate Collected _ ?35l_4rf?. __ 51?7.jX [C - D]

TOTAL CONDENSATE COLLECTED: M3i£ht*./.bW.b [A + total of E]Components Rinsed***: All components from nozzle through 5tn impinger

Sample Bottle Gross Wt. -J<t.3&$._._ JJ-S'J.- After All Rinses AddedCheck pH _9 »»»*, pH: _2fi?_..._.. _ jf,A__. . Before Adjustment

pH: _______ __ _____ After Adjustment

[Total of F - Total of B]

FILTRATION OF SAMPLE NOS. £185 and C.185A • 0.45 m Filter Type: ll Lj— ceJTaJfl- ____Filter Lot Number: G*-£ . _____

Filtrate Sample Number: <il86 Residue Color: _ oo.Wit«— -Sample Bottle Tare Wt. /%(>• 0

Sample Bottle Gross Wt. 33 / -*• V *• Including Rinses of Filtration ApparatusNet Sample Wt. 3 I ?3- f «- For Hexavalent Chromium Mass Collected Computations

Sample Mixed, Then:Sample Aliquot for Analysis •-> -.-.•-.-.-.-.--» for Cr+6

Aliquot Sample Number: £.187Sample Bottle Tare Wt. /7.YSample Bottle Final Wt. 3 1 7 7,-J /

Net Sample Wt.

* Gas used for purge is passed through 0.1 N KOH in an impinger before entering train.** pH checked with glass rod and pH indicator strips; solutions adjusted for subsequent runs as necessary. Void run if pH

of any impinger (1st through 4thHs s8.5.*** Using a total of about: 150 200 TnLs of ASTM Type I water for each impinger set, rinse components 4 times. Use a total

of at least 100 mLs to rinse the nozzle, probe liner, tee assembly, and peristaltic pump tubing 4 times.**** Thoroughly mix sample and check pH; adjust to pH 9-10 with 2 N KOH if necessary..

COMMENTS:

M5CRHCCX.WPD SeDtsmber 5. 1996 Irev. M5CHR23X.WPD January 20, 19971








SAMPLE PRESERVATION: All samples, XX120, XX199, and XX200 stored at near water ice temperature (i.e., 4°C), andbottles wrapped in aluminum foil. All samples, XX1 21, stored at near water ice temperature (i.e., 4°C). All samples, XX1 22,stored at near room temperature or cooler (i.e., 26°C).

. 2 Sf / •' /'.Run No. . K ... Date: _±^,_~5*rl_5r ......... Sampler(s): •-> -& "t., \' /&£•*-* /,—J i o

^ ~~\ ^ ~—v. -—— -—•—V'' /--——-vComposite Sample Number: /£>120'\ Xfc12l'- \f 6-1221 \ /r(y199 * /G-200 A

Composite Sample Designation: ( SVOC^ / METALS I GALBT j ( VOC/ ( FENAC /~ __ / —— --——-

Grab.NQ_ _lime.,., ____________ „..:,.„_:__ lnientuptions/£omments._ ....__ . . . .___._ _ ,,,_ .,_...._.„

Caution: Material may contain p-naphthylamine.

Relinquished By- ^ - ^ ifer l Received By .£j < CCtL'-k~£, Date/Time Z-1- 1 ? >(<••WSTFEE03.WPD February 1. 193?

APPENDIX B 197

SOLID WASTE FEED SAMPLING DATA (SAMPLE FOR COE)

MR! Project No. 3620.13.30Client/Source: OHM Remediation Services Corp., Drake Chemical Superfund Site, Mobile Hazardous Waste Incinerator



SAMPLING METHOD: Equal-sized grab samples of approximately 60 grams each collected with an aluminum* scoop from.material on the apron conveyor belt. Grab samples deposited, combined, and mixed in an aluminum* pan; then cut and splitinto a 16 oz., wide mouth, precleaned, clear glass bottle. Bottle sealed with Teflon®-lined screw cap and wrapped in aluminumfoil to seal out light. (*As per COE protocol.)



Run No. _j?L_____ Date: "^ ~ <**- *" 7 / _ Sampler(s). 'x<5 2 ;?%_-__ T-/'' <;c,' _ ^?, , / /7 ^^


GrabNo. __T_im.e_ ______.________J_______lDterruptiQQs/-Comm.ents__.____._.

Cautiori: Material may contain p-naphthylamine.j±ii r'.i Lt-S . / !?5y 7—:—

RelinquishedWSTFEO3C.WPO Feoruarv I. 1997 s ,'££-'

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BOTTOM ASH SAMPLING DATA




SAMPLING METHOD: Equal sized grab samples of about 200 grams each collected with an aluminum* scoop. Grab samplesdeposited, combined, and mixed in an aluminum* pan; then cut and split into 16 oz., wide mouth, precleaned, clear glassbottles. Bottles sealed with Teflon*-lined screw caps. (*As per COE protocol.)



Run No. _£?____ Date: _J&_IL_!?./


GrabNo. ,__Iime_ . ______________________lnterr.uptions/.C.ommeats._,_

Relinquished By > _ J . . ... Received By AJ. ~-v_ . .„. Date/TimeAJ. ~-v£_ &JL

3OTMASH3.WPO January 20. 1997

AR3I5709APPENDIX B 2O3

BOTTOM ASH SAMPLING DATA (DUPLICATE SAMPLES)

MR! Project No. 3620.13.30Client/Source: OHM Remediation Services Corp., Drake Chemical Superfund Site, Mobile Hazardous Waste Incinerator





SAMPLE PRESERVATION: All samples, XX170 and XX171, stored at near water ice temperature (i.e., 4°C), and bottleswrapped in aluminum foil. All samples, XX172, stored at near water ice temperature (i.e., 4°C). All samples, XX173, storedat near room-temperature or cooler (i.e., 26°C).

Run No. _y2____ .Date: X, ~ A." / 7_^____ Sampler(s):

Composite Sample Number: /£?170 J\ /"£171 \ f £172Composite Sample Designation: ( SVOC^J ( VOC J • X^CLP/METALSJ ( GALBT

Grab____lntejxu piiansZCam merits_

Relinquished By _ *- . ._ Received By. _^<-. **£—- Date/Time

BOTMSH3D.WPD January 20. 1997

A - R 3 I 5 7 I OAPPENDTX R

BOTTOM ASH SAMPLING DATA (SAMPLE FOR COE)




SAMPLING METHOD: Equal sized grab samples of about 200 grams each collected with an aluminum* scoop. Grab samplesdeposited, combined, and mixed in an aluminum* pan; then cut and split into a 16 oz., wide mouth, precleaned, clear glassbottle. Bottle sealed with Teflon*-lined screw cap. (*As per COE protocol.)



Run No. _&___ Date: _JJt>?C-,?Z_,_____ Sampler(s): f _ £.f

Composite Sample Number:Composite Sample Designation: COE

Grab_Ncu_ .. _ .Time_ . .___..__...______ __... Interruptions/Comments .._ ...._ _ , _,_,__., „.. _

Relinquished By £LJ. £2&&«dz - Received By X.J. it - V Date/Time 2--1-9 7 I to? 7

30TMSH3C.WP3 January 20. 1997

A R 3 I 5 7 ! 1APPENDIX B 2OS

FLY ASH SAMPLING DATA


Source Location: Lock Haven, Pennsylvania '


SAMPLING METHOD: Equal sized (approx. 100 grams) grab samples collected with an aluminum* Scoop from each of7 ejghtsen (1 8) specially spaced points over the surface and from a depth of 3 to 6 inches below the surface of the pile in the

dump truck bed located under the end of the conveyor. Grab samples deposited, combined, and mixed in an aluminum* pan;then cut and split into 1 6 oz., wide mouth, precleaned, clear glass bottles. Bottles sealed with Teflon®-lined screw caps. (*Asper COE protocol.)



Run No. J2. ____ Date: ~~- _____ Sampler(s):


Event_ Iim.e__ __________________________ Interruptions/Comments

Relinquished By .S(dJ rr:.. _,_...... Received By _ > - - Vr^ZZTT.- Date/Time _2_" ?f5 7..

FLVASH3.WPD ânuary 20. 1997 • '

/1R3I57I2APPENDIX B 2O6

C C





SAMPLING METHOD: Equal sized (approx. 100 grams) grab samples collected with an aluminum* scoop from each ofeigbtaen (1B] specially spaced points over the surface and from a depth of 3 to 6 inches below the surface of the pile in thedump truck bed located under the end of the conveyor. Grab samples deposited, combined, and mixed in an aluminum* pan;then cut and split into 16 oz., wide mouth, precleaned, clear glass bottles. Bottles sealed with Teflon®-lined screw caps. (*Asper COE protocol.)


SAMPLE PRESERVATION: All samples, XX174 and XX175, stored at near water ice temperature (i.e., 4°C), and bottleswrapped in aluminum foil. All samples, XX176, stored at near water ice temperature (i.e., 4°C). All samples, XX1 77, storedat near room temperature or cooler (i.e., 26°C).

Run No. J&_____ Date: 2-- 2-" 9*7_____ Sampler(s): /?. /4 /- &


Event_Time_ ___________________JntemuptLonslCamtaents______

/}Relinquished By £y. C*\>r~~~~ Received By /W 6&*Y Date/Time

FLYASH3D WPO January 20. 1997

A R 3 I 5 7 I 3APPENDIX B 2O7

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SAMPLING METHOD: Equal sized (approx. 100 grams) grab samples collected with an aluminum* scoop from each ofjHstgluytin (I 8) specially spaced points over the surface and from a depth of 3 to 6 inches below the surface of the pile in thedump truck bed located under the end of the conveyor. Grab samples deposited, combined, and mixed in an aluminum* pan;then cut and split into a 16 oz., wide mouth, precleaned, clear glass bottle. Bottle sealed with Teflon®-lined screw cap. (*Asper COE protocol.)



Run No. _£_____ Date: £-£-<? 7" ___ Sampler(s): <P- /£C-3<S'2T _________________' ——\

Composite Sample Number: f 137 / ^Composite Sample Designation: V. COE 7

EventJsLo... ,Time_.... _.________^_ _.._ _ __. .-Interruptions/.CommentS- _ ....

/

Relinquished By ^.^ . Received By . & __ -— - Date/Time. Zl

FLYASH3C.VVPD January 20. 1997

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Plant bZA-££. otfi*f £SC . Proiect No. Zo- A? -:?<£>Sampling LocatiSample Type (MFlow Control De\For Sampling FrPump Type

on 3r#< /< uPP£ft £&i>et- Run No. 7- Date 2-3-9 9-ulti-Point, Sin§1/ice (MicrovalveDm M5 Consolet>£#-psre/l&r}>

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Time24 Hr Clock)3/k/3/<?)3C/OHoi/<•/<•///<•/<•/£?

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pt,( iL&& b£+3&3f~/HZJT Sftv*- Pt-£+J 6>

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DRAKE 3620.13 ' ^ 1 O -7MM5PH ORSAT BAGTRIAL BURN SAMPLEFor disposal call: P. OQRMANMIDWEST RESEARCH INSTITUTE

APPENDIX B 212

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Run No. ~7 Sampling Train No. rA fA. 5 PH " [ Sample Box No. __f__ ______Set-up person(s): / . C\,af RTvA £jT _________________________ Date:

Transfer to Sampler: /Relinquished Bv /)• C_A r&sd&f Received By 'P • h)£oJ( _____ Date/Time J./S/77 10' o

TRAIN COMPONENT COMPONENT NO. ______________ LOADING DATA ___________

Sampling Nozzle (Quartz) PH~) * Initial Weights (grams)**Probe (Liner-Glass) __________ * ' ____ Empty _____ Loaded

Female Probe Outlet Blank-Off ______90° Bypass __________ *

Filter Holder Front _________________ Filter Type: Whatman QM-AFilter Holder Back with

Teflon® Filter Support ________________ Filter Number: \ J — -45/90° Connector ___________

1st Impinger (2-Liter, Mod-GBS) _____ _____ 50mLs±1mL / O cX- 1 -1 / 07 O •0.1 N H2SO4

1st Impinger Replacement _____ _____ 50 mLs ±1 mLU-Connector (A) _____________ 0.1 N H2SO4

2nd Impinger (GBS) ______ _____ 100 mLs ±2 mLsU-Connector (B) ____________ 0.1 N H2SO4

3rd Impinger (GBS) _____ _____ 100 mLs ±2 mLs 5" 7 3. 9 (f "73 -3U-Connector (C) ___________ 0.1 N H2SO4

4th Impinger (Mod-GBS) ______ _______ Empty / %7. /U-Connector (Dl ___________

5th Impinger (Mod-GBS) _____ _____ 100 mLs ±2 mLs 5~6O- ( (/? 'jO,U-Connector (E) ___________ 0.1 N NaOH

6th Impinger (Mod-GBS) ____________ 100 mLs ±2 mLs y'tfS- I £~3*< . ~~JU-Connector (F) ___________ 0.1 N NaOH

7th Impinger (Mod-GBS) _____ _____ -200 g indicating silica gelU-Connector (G) ___________

8th Impinger (Mod-GBS) _____ _____ -200 g indicating silica gelImpinger Outlet Connector f ) f-'jf •" I____

.jO- U?

* Before and after sampling: Nozzle openings covered with aluminum foil or Teflon® tape, and nozzle placed in Ziploc® bag.Probe liner outlet sealed with glass female blank-off, and inlet sealed with Teflon® plug. Bypass inlet covered (not sealed)with aluminum foil.

* * Initial weights of additional components exchanged during the run also entered here. All exchange component openingscovered with aluminum foil, Teflon® tape or as described above.


0050SUCX.WPD June 26. 1996 (rev. 0050SUC3.WPD October 31, 19961

fiR3IS720



Source Location: Lock Haven, PennsylvaniaSampling Location: Mobile Hazardous Waste Incinerator (HWI) Stack ,1Run No. ~7 Sampling Train No. WT, S Pn~ (_______ Sample Box No. J___________________________________TRAIN PURGE WITH ASCARITE-FILTERED AIR____________________

Condensate in front-half? l\) O_______________________ Purged By A I //f________________Date/Start Time: A/ /A______ _______ Stop Time /V//4 Purge Rate: [AH = \j/A_____ in.H2OlMoisture Removed? K)/ A_______________________________________________________________Transfer for Recovery: .• A S3 tRelinquished By LX fjp*. '_____ Received By A . (l qr .A ca/" Date/Time a./3J/7'7 / ~7 /SSample box recovery person(s): /^ . C at. r^/^.d.?^__________________ Date:

Probe recovery person (s): f, 0-r1?r ,-A.A n, TT Crxcôi^,' ft^ • l-/a..</g._/______ Date: a / /<? 1Weights below are in grams._________________________________BACK HALF RECOVERY________________________________


Final Wt.VZ£l/ >^r«^J jfc<0.3 S- ( 5?33. 3Initial Wt. 10 IQ, >Net Wt.

[ Total Condensate Collected: 3S~C3.QDescriptionand/or color: ______ __**

4.6 ~ ~ ~ ~ ~ - -. % BlueSample Number: ~7 103 ,,-_ „ 7 105

Sample Bottle Tare Wt. A3 SV-/Sample Bottle Gross Wt. V"715. 3__ ^ fl I 5^ "5 Before Rinses

Components Rinsed*: filter support, filter holder back, 4th-6th impingers,45/90° connector, 1st-3rd impingers, U-connectors A-B U-connectors C-E

Sample Bottle Gross Wt. '=/,&)'?•' 3~~ !3LO~7' C After RinsesNet Sample Wt. 3 V15.C ) 7/<3>_S for Mass Collected Computations

Sample Mixed, Then: for HCI for CI2Aliquot Sample Number: -.-.-.-.-. "7104 *-> ~> — ~> ~> ~7106 for Chloride AnalysisSample Bottle Tare Wt. 5*7,9 9%-5'

Sample Bottle Gross Wt. V'7/ff 4 /R'7-3 ; ( CT\.J l?lLp.(p After AliquotingSample Bottle Final Wt. fij A KJ A After SIE Check

Net Sample Wt. 33 ,1 T7-*f (*I2.O 7T, /

. ______________________________FRONT HALF RECOVERY_________________________________________FILTER:

Sample Number: ""7 102 Description/Color: ___________7 W

TRAIN RINSES: Sample Number: 7 101 3_3.(?Sample Bottle Tare Wt. 3 LC,. •"Components Rinsed*^ nozzle, probe/finer, bypass, filter holder front

Sample Bottle Gross Wtf 3 3 !> v( with Acetone RinsesNet Acetone Sample Wt. 17 ~(*Sample Bottle Final Wt. V £» "7, ~7 with added Water RinsesNet Water Sample \Nt./y£ 7 '/ ,-f

* Using a total of 100 mLs ±2 mis ASTM Type I water per sample, rinse components twice. Thoroughly mix each sampleand added rinses before aliquoting.

** Acetone rinses with brushing 3 times or more until perceivably clean. If any residue remains in a component, follow withASTM Type I water rinses with brushing until perceivably clean. Do not add any water rinses to the sample bottle untilafter the bottle is weighed with all of the acetone rinses.

COMMENTS: '

0050RCCX.WPD October 31. 1996 (rev. OOSORCC3.WPO October 31. 19961

A R 3 I 5 7 2 !APPENDIX B 215

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. FIELD LABORATORY TRAIN SET-UP DATA

MR! Project No. 3620.13.30Client/Source: OHM Remediation Services Corp., Drake Chemical Superfund Site, Mobile Hazardous Waste



Run No. / Sampling Train No. /v\M.5 J V ~" \ Sample Box No. G ( dÔ O/Set-up person(s): A • CL^ n. r e r\ <4_? / ________________________ Date: <?-/3/ *? "^ ____

Transfer t o Sampler: - . 1Relinquished By A. LX reWW" Received By XX'AJ^^. [ _____ Date/Time J./3/?7 /°

TRAIN COMPONENT COMPONENT NO. __________ LOADING DATA __________

Sampling Nozzle (Quartz) Pc.Q>-( fp.37/r Initial Weights (grams)**Probe (Liner-Glass) • ________ * ____ Empty ____ ___ Loaded _

Female Probe Outlet Blank-Off ____________90° Bypass __________ *

Filter Holder Front _____________Filter Holder Back with Teflon®- Filter Type: Whatman QM-A

coated 316 SS Filter Support __________ _45/90° Connector __________ "

Condenser (Standard) ^ _________ Thermocouple No. > J*-~ 3XAD-2 Resin Cartridge (Standard)-^ ____ -65 grams XAD-2 Resin + Surrogates(Documentation of standards injection is separate)'; resin spiked on I / L"7/<7"7 and maintained near 4°C until use.

1st Impinger (2-L Mod-GBS) _____ ______ Empty / O V "/• (a

1st Impinger Replacement _____ _____ Empty N*U-Connector (A) ______________

2nd, Impinger (Mod-GBS) _____________ 100mLs i # k • SU-Connector (B) ___________ ASTM Type II Water

3rd Impinger (GBS) __________ 100mLs V/£?' 3-- 6" 7S". /U-Connector (C) ____________ ASTM Type I! Water

4th Impinger (Mod-GBS) ____________ Empty i b? O .«SU-Connector (D) ___________

" 5th Impinger (Mod-GBS) _____ ________ ~200 g indicating silica gel 6? 3— •>• |U-Connector (E)

6th Impinger (Mod-GBS) ____ _____ -200 g indicating silica gel / 3 3 < yImpinger Outlet Connector Lx r

* Before and after sampling: Nozzle openings covered with methanol/methylene chloride/toluene/acetone-rinsed aluminumfoil, and nozzle placed in Ziploc® bag. Probe liner outlet sealed with glass female blank-off, and inlet sealed with Teflon®plug. Bypass inlet covered (not sealed) with methanol/methylene chloride/toluene/acetone-rinsed aluminum foil.

* * Initial weights of additional components exchanged during the run also entered here. All exchange component openingscovered with methanol/methylene chloride/toluene/acetone-rinsed aluminum foil or as described above.

*** Cartridge weighed with blank-offs in place; then, cartridge covered with aluminum foil to seal out light during storage andsampling.


1023SUCX.WPD April 26. 1996 (rev. 1023SUC3.WPD October 25, 1996)

flR3!5726






/ Sampling Train No. AV At 5" J (/"' (Run No. / Sampling Train No. AV At 5" J /"' ( ___ Sample Box No. O ITransfer for Recovery: \ . _ .Relinquished By ^ • (.'Q Q.S*. \ Received By /-\ • (__/7 f /• ;3yf Date/Time A/ / V /Sample box recovery person(s): r\ > C . (\\ r<3?lf ____________________ Date: 3-/1, /^^

Probe recovery person(s): P- AJ-g^( , TV!, ûf 'A /1 \~~ O Tn'A ______ Date: ^LWeights below are in grams.

RESIN CARTRIDGE AND IMPINGERS RECOVERYImpinger:

Final Wt.Initial Wt.Net Wt.

Descriptionand/or color:

XAD-2Cartridge*

i

-.2,. 3.

ji

Replacement1 St 1 St

373^-5" >jtt jteJ}om.(e_S-Lfi

&&AS /

2nd 3rd 4th'42-1.% ?3>a3 7/7.5, / <Stfo.Z 57S'-I y .5 «2V/' e2-TS"' 31-. <?oy,-

[ Total Condensate Collected:

5th 6thi9J,3 -7V3-/{,3.1.1 73?.Y17. %-7

~3 *-fly'*i •• C~) grams]

O ?* J eJ " bSample Recovery: Cartridge* — 1st-4th Impingers and Replacement 1st Impinger ~ *- - - % Blue

Sample Number: ~7 111 7 112Sample Bottle Tare Wt. / 35&O

'• Transfer impinger contents only (i.e., do not add component rinses to this sample).

Sample Bottle Final Wt. Ilk "•?•-?Net Sample Wt.3 C? K- j?


____________________________FILTER RECOVERY AND TRAIN RINSES___________________________

FILTER: ^Sample Number: / 109 Description/Color:

TRAIN RINSES: FRONT BACK QA RINSESSample Number: ~] 108 7 11° "7 113

Sample Bottle Tare Wt. 3 k>3.5 3. (a (0 S H^l-ftComponents Rinsed***: Front -- nozzle, probe liner, bypass, filter holder front;


Sample Bottle Final Wt. ~73-%-t t O<?T7.Net Sample Wt. I3\,H 6*3. ,


*** TRAIN FRONT/BACK RINSES: Methanol/methylene chloride (1:1 v/v) rinses with brushing of front components 3 times ormore until perceivably clean, and methanol/methylene chloride (1:1 v/v) rinses of back components 3 times, but withoutbrushing, and including 5-minute soaks of underlined components,3 times.QA RINSES: Follow with toluene rinses and soaks, but without brushing, in the same manner as above for the train froand back rinses.

COMMENTS: ''~ ,


I023RCCX.WPO Jun« *. 1996 (rev I023HCC3.WPO Octobar ?5. 1996)

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Plant TVoA. Otfty k5<Z- Proiect No. 1/ 2 " Pi'-'V?Sampling LocatiSample Type (MFlow Control De\For Sampling FnPump Type

on ^ x 5K7_i7*' < 2«M-) Run No. ~1 Date -z-- -1?-?ulti-Point, Sing/ice (MicrovalveDm MS Console

e-Point) ^/° . . Operator 41 -, Critical Orifice) ^7^ Baq Type /HY/d - Sample No. "7 K5"No. /V'-/4? Method 3 Train No. (\)&

Pump Type vPump I.D. V-/<? Pump I.D. \Flow Meter TypeFlow Meter I.D.Desired Flow RiLeak Check BefTotal Sampling "Flow Rate (cc/mEstimated Actua

Time24 Hr ClockCbfi-'S/"?'7<3/•?i/r~/>-/&&./¥/*?t tJe/*j"1?/£?~Pj, f/<oJ<?tfff/&<**/*/5~/ "5<yf^y^

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ite/(cc/min) / Tt?' xore Samplina / - , After Samplinq /2 -"ime (min) /^ Averaae Flow Meter Readina // n): Average /^?c> Hiahest y ?i? Lowest /_>_»1 Volume (liter?

Flow MeterReading/.A°/--?/^c/,*>I."/.&/,&/,&/, <?/,a/.<?AC7

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Comments

'7f>iJ7" 3.,£c _ • 1 y .,'>\ PI -*- £*~'

I H/A. *{sz- 1 c f ^ 77- -' iz?.3f

j t \

DRAKE 362O'. 13 V .MM5MM OF.SAT BAGTRIAL BURN SAMPLEFor disposal call: P.GClRMANMIDWEST RESEARCH INSTITUTE

APPENDIX B

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^315731APPENDIX B 225






Run No. ~7 Sampling Train No. /h /^f ' /Yl/W- -J Sample Box No. OilSet-up person(s): -/rtc —— _________ \ _____________ : _______ ' Date: 2.

Transfer to Sampler:^Relinquished By J . /}/[, /^— Received By D • Aj.g J _____ Date/Time .2-.?-?7

TRAIN COMPONENT COMPONENT NO. ______________ LOADING DATA

Sampling Nozzle (Quartz) tf? > * . Initial Weights (grams)**Probe (Liner-Glass) __________ * ____ Empty ___ Loaded

Female Probe Outlet Blank-Off ____________90° Bypass __________ *

Filter Holder Front ________ 'Filter Holder Back with Filter Type: Whatman QM-A

Teflon® Filter Support ___________45/90° Connector _____________ .

1st Impinger (2-L Mod-GBS) ______ ______ Empty /

1st Impinger Replacement Au-/ u-fe&y- Empty _____ —— _U-Connector (A) ___________

2nd Impinger (Mod-GBS) _____ _____ 100mLs±2mLs ,*/&&. /U-Cpnnector (B) ___________ 5% HNO3/10% H20a

3rd Imoinaer (GBS) _____ 100mLs'±2mLsU-Connector'(C) ___________ 5% HNO3/10% H202

4th Impinger (Mod-GBS) _____ _____ EmptyU-Connector (D) ___________

5th Impinger (Mod-GBS) _____ _____ -200 g indicating silica gelU-Connector (E) ___________

6th Impinger (Mod-GBS) _____ _____ -200 g indicating silica gelImpinger Outlet Connector


* * Initial weights of additional components exchanged during the run also entered here. All exchange component openingscovered with Parafilm®, Teflon® tape, or as described above.


M29S_CX.WPD June 19. 1936 (rev. M29S_C3.WPO Ociobef 25, 19961

AR3I5732





Run No. ~7 Sampling Train No. AAMS XVI/K"3 Sample Box No. Q) I I ID—Transfer for Recovery:Relinquished By 0 • AJ-jz~~i Received Bv ~cf . Vlc. £>• — Date/Time 3.-3~fl /6<JSSample box rec

Probe recWeights below

Impinger:

Final Wt.Initial Wt.Net Wt.

Descriptionand/or color:

Rsnnvprv

overy oerson(s): ,7"! SW-*- /"overv person(s): j'&i/'/f"?are in grams.

Replacement1st 1st

3-717.2, /'/<-/ JSTI.V /,2<j£7,7 J,

£/*~~--»-•-»—»-»-> lmninnf>r<! 1 -4. «

' - ' Date: J.-Y-f?•pLttnti, &, £a>»/.-!sJs D.tft*') Date: 2- -9?

BACK HALF RECOVERY /'

2nd 3rd 4th 5th 6thc?- c y

F* W ^~ <P~? & / / A < » . &*/ r I ( ^ c.•T77.0 j ff.O VTC.3 <i,23. ) (tSJ tJ'U2 7 -f JfJ.t 3Z2-I -T.O /frZ-fy/

[ Total Condensate Collected: Zfel'-t.fi /'/ ]

j__ J __ _/__. ^-<_^,-^<-«J^<-^-^^^^<-^^^^,^- %Rli]fi

Sample Number: "7117Sample Bottle Tare Wt.

Sample Bottle Gross Wt. -s/-Tfc- -L. Before RinsesRinse Solution: 0.1 N HNO3

Components Rinsed*: filter support, filter holder back, 45/90° connector,1 st-4rd impingers, U-connectors A-C

Sample Bottle Final Wt. ^ t-B After RinsesNet Sample Wt. ,1^ ' } i, .2

FRONT HALF RECOVERY

FILTER: 'Sample Number: 7116 Description/Color:TRAIN RINSES:

Sample Number: 7115Sample Bottle Tare Wt. /Tfl.V

Rinse Solution: 0.1 N HNO3Components Rinsed**: nozzle, probe liner, bypass, filter holder front

Sample Bottle Final Wt.Net Sample Wt. 7f/7

* Using a total of 100 mLs ±2 ml_s of 0.1 N HNO3, rinse components twice.* * Using a total of 100 mLs ±2 mLs of 0.1 N HN03, rinse components 3 times or more with brushing until perceivably clean.

COMMENTS:

M29R_CX,WPD September 27, 1996 Irev, M29R_C3,WPD OctoOar 25, 1996)

SR3I5733APPENDIX B 227

SF ——A

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AR315735APPENDIX B 223


Plant t£Ua./<*L &<¥/*? /?$£->_________ Project No. 3&A?-ss- so_Sampling Locationi^Lc A f c / -f (£.<te,, J Run No. 7___ Date _&Sample Type ( 4gffi 5IncSir |e-Point) OperatorFlow Control Device (fficrovajve/ Critical Orifice) __ Bag Typex y/ . Sample No. 7/5"For Sampling From M5 Console No. ./is v______ Method 3 Train No. ______ /___Pump Type ^v^.—•-_____________________ Pump Type ____ /Pump I.D. _. x^g________________________ Pump I.D.Flow Meter Type ^>£>».*?£<_______________ Flow Meter Type /Flow Meter I.D. ___ y^ g-_______,____ Flow Meter I.D. _____/_Desired Flow Rate (cc/min)Leak Check Before Sampling / gj" _____ ' After SamplingTotal Sampling Time (min) xg^____ Average Flow Meter ReadingFlow Rate (cc/min): Average • /& o________ Highest / a____ LowestEstimated Actual Volume (liters)

Time24 Hr Clock/3/s-

Flow MeterReading Comments

7

DRAKE 3620.1JORSAT BAG

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Run No. 7 Sampling Train No. /ft/HS" /WA\.-{ Sample Box No. O./2- ° 0 2-Set-up person(s): t7- /Me. L-&. n *-i_____________:_______________ Date: ,3. 3 ~~7 "7

Transfer to Sampler:Relinquished By J'./H /'L-*.___ Received By _£L_/Ua~=J______ Date/Time

_ _ _ _ _ TRAIN COMPONENT _QQM_EQN£bJ_T_N.Q^ _______________LOADING DATA

Sampling Nozzle (Quartz) /?)/!}-) _ * Initial Weights (grams)* *Probe (Liner-Glass) _____ _.__._ * __.._.Empty_ _ .__Laaded_

Female Probe Outlet Blank-Off _____________90° Bypass ___________ * -

Filter Holder Front ______...._._.-. - -Filter Holder Back with Filter Type: Whatman QM-A

Teflon® Filter Support __________ . . ' .45/90° Connector ___________

1st .Impinger (2-L Mod-GBS) _, __. _____ Empty

1 st Impinger Replacement __ hlJLi~x«s:.___ Empty _U-Connector (A) ..____.______

2nd Impinger (Mod-GBS) _____ ____ . ° 100 mLs ±2 mLsU-Connector (B) _ ..__...._. __..._ 5% HNO3/10% H2O2

3rd Impinger (GBS) _..___ ..._____ 100.mLs ±2 mLs ...___ 3-3.._.U-Connector (C) ____...__ .___ 5% HNO3/10% H2O2

4th Impinger (Mod-GBS) __.„„._,.- „_ . EmptyU-Connector (D) _..__..__.. _ ..

5th Impinger (Mod-GBS) .___._.„. .„._._ 100 mLs ±2 mLs* **U-Connector (E) .._.___..... __._ - 4% KMnO4/10% H2SO4.

6th Impinger (Mod-GBS) __.__. .„___ 100 mLs ± 2 mLs* **U-Connector (F) _______.___ 4% KMnO4/10% H2S04

7th Impinger (Mod-GBS) _____ _____ -200 g indicating silica gel ___JaJ«LJ_.U-Connector (G) ___________.

8th Impinger (Mod-GBS) _____ _____ -200 g indicating silica gelImpinger Outlet Connector


** Initial weights of. additional components exchanged during the run also entered here. All exchange component openingscovered with Parafilm®, Teflon® tape, or as described above.

*** If the reagent was exhausted before the end of a previous run, use a larger volume (e.g., 200 mLs ±2 mLs) and documentbelow. Prepare additional reagent blanks accordingly.


.129SUCX.WPO June'19, 1996 (rev. M29SUC3.WPD January 20, 1 997) ,

AR3I5738





Run No. _7 ____ Sampling Train No. _/h/MS~ /M /M - / ... _Sample Box No. 6 t<2~ O f>Transfer for Recovery:Relinquished By /?•/&*«-/ _______ .Received By 3~-/tf<.£*— _____ Date/Time 3-Sample box recovery person(s): 7- /%<. £+ —

Probe recovery person(s): r-&o.'fn.<** &. LcJ- -y &,~&J*sfrt/J D,rfczJWeights below are in grams.__________________________________ BACK HALF RECOVERY


Final wt. _>.Initial Wt. JQ3JL.INetWt. .£7 0.7-*%

[ Total Condensate Collected:Description / / / I Iand/or color: < ./<>-<-*- g/qgrr-.. _ .P*2 .. ,f k~~ —CJAf . _?UJer _M4v./cJ?-r ._

Recovery: ~ ~ -•>•»«•-*•-» Impingers 1-3 •-«-*•' ~ •-«-• 4th Impinger Irrfpingerif 5-fy~ % BlueSample Number: 7180 1181 7182 7183

Sample Bottle Tare Wt. .Z SB- S- . i 2.(L_ _-2AJ,/. ./.?/, P.,., . „_Sample Bottle Gross Wt. P -d _>Q_7=JL- _7 .-. . Before. Rinses

Rinse Solutions: 0.1 N HNO3 0.1 N HNO3 KMnO4/H20, then 8 N HCIComponents Rinsed*: filter support, filter holder back, **4th impinger ***5th-6th impingers, U-connectors D-E45/90° connector, 1st-3rd impingers, U-connectors A-C

Sample Bottle Final Wt. ^' . . .. _ J » ^ _ . J-., , .r- After RinsesNet Sample Wt.

... . FRONT HALF RECOVERYFILTER: /y- > j~ JSample Number: 7179 Dpsnriptinn/nnlnr; GIT t *-**- / iTRAIN RINSES:

Sample Number: 7178Sample Bottle Tare Wt. /£<7,f


Sample Bottle Final Wt. _Net Sample Wt.

* Using a total of 100 mLs ±2 mLs of 0.1 N HNO3, rinse components twice.** Using a total of 100 mLs ±2 mLs of 0.1 N HN03, rinse the impinger twice.

*** Using a total of 100 mLs ±2 mLs of 4% KMn04/10% H2S04, rinse components 3 times; then, using a total of 100 mLs±2 mLs of ASTM Type 1 water, rinse components 3 times to remove all purple color. Next, using a total of 25 mLs ±0.5mLs of 8 N HCI, remove any residue from components; transfer these rinses to a separate bottle containing one half of 200mLs ±2 mLs of ASTM Type I water; rinse components with the balance of the water and transfer to bottle.

**** Using a total of 100 mLs ±2 mLs of 0.1 N HNO3, rinse components 3 times or more with brushing until perceivably clean.COMMENTS:

M29BCCX.WPD June 20, 1996 (rev. M29RCC3.WPO January 20. 1997)


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APPENDIX B 235


Plant blZAKZ OHM &SC Project No. IblO' /3~3OSampling LocatiSample Type (MFlow Control De\For Sampling FrPump Type

on STACi< uP>?££. t&Jg.£ Run No. -ww -j Date 2-B-9r7-ulti-Point, Sing/ice (MicrovalvcDm M5 Consolebmp#e/t-6tt

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Pump I.D. NS" Pump I.D. - ———Flow Meter TypeFlow Meter I.D.Desired Flow ReLeak Check BefTotal Sampling 1Flow Rate (cc/mEstimated Actua

Time24 Hr Clock/3/S"\8i£1 3-5"?l*-i0l/W/lyyÎS'IS"l3/(e>items'

> I2of yn 7" -/z Flow Meter Type — ——A/cT Flow Meter I.D. ————

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APPENDIX B 237 I




Run No. _ ~2- —— Sampling Train No. < .&— I ________ . Original Sample Box No. < -.Backup Sample Box No. C-/€._ -~2~

Set-up person(s): ~J~. /VL<- f*——-_________ . .. . ._____________ Date:Transfer to Sampler:Original: Relinquished By J V <- /_____. Received By ff -f^-a^—j_____ Date/Time <3 ~3 -?7

, Backup: Relinquished By J • /fr?<- /I—___ Received By ?-/O-a~»/_____ Date/Time

_______________TJBAUSLQQMEQMENI___________ COMPONENT NO. I OADINfiNote: All sample-contact components are Teflon

unless specified otherwise. .... Original— ._BackupJL_

Sampling Nozzle (Quartz) _£«Kd__**Probe (Teflon Liner/STL) with Tee Assembly including

Solution Feed Line with Sprayer Tip and Gas Outlet Tube _ . ____ _.** . ' . . .Peristaltic Pump with C-Flex, Tygon, or other inert Tubing _ _ _ __ .'** . . _..

1st Impinger with Unrestricted Stem Tip andSolution Feed Line with Shutoff Valve ___ .. _ ** ____.__._»* 175 mLs _ J—0. N KOH

2nd Impinger with Restricted Stem Tip and Gas Inlet Line ______ ___ __ 75 mLs L 0 N KOH3rd Impinger with Restricted Stem Tip and Gas Inlet Line _ _.. . ___ .. _ _ . _ 75 mLs _ . /•_.£__. N KOH4th Impinger w/Unrestricted Stem Tip and Gas Inlet Line _________ __ ... __ 75 mLs _ JL.CL.. N KOH

5th Impinger w/Unrestricted Stem Tip & Gas Inlet/Outlet Lines __ . ___ . ______ Empty6th Impinger (Glass, Mod-GBS) ______ ______ -200 g indicating silica gel

Glass U-Connector _____ . __ ; ____ . _ . . . . .7th Impinger (Glass, Mod-GBS) _______ . ___ , ____ -200 g indicating silica gel

Impinger Outlet Connector _J>'.

. ____________ ' - . - -- -- ... - - .' _________ LQAD1N.GLDAIA...Weights below are in grams***: JlrigiaaLSample.Bcuc B.ackup_Sample_B.ox_

Train Sample Number: 7185 ~?185ASample Bottle Tare Wt. __ /.£.?* A

Sample Bottle Gross Wt.Initial KOH Solution Net Wt.

. 6th 7thInitial Silica Gel Impinger Wt(s). J?33.ZL. £?/,O


* * Before and after sampling and during train transfer: Nozzle openings covered with Teflon® tape, and nozzle placed in Ziploc®bag. Probe liner inlet sealed with Teflon® plug. Probe liner outlet remains connected to tee assembly; solution feed lineinlet and gas outlet tube (1st impinger stem) opening covered with Teflon® tape secured with caplugs. 1st Impinger inletsealed with Teflon® plug. Peristaltic pump loop closed.


NOTE: If the pH of either of the first two impinger solutions was not gteater_than_8L5 after the previous run, increase the alkalinityhere, record the normality, and acquire another reagent blank set.


MSCRSUCX.WPD September 5. 1996 (rev. M5CRS23X.WPD January 20. 1997)


MRI Project No, 3620.13.30Client/Source: OHM Remediation Services Corp., Drake Chemical Superfund Site, Mobile HWI


Run No. "7 .-.- Sampling Train No. __ QLr:jL _____ _, . Original Sample Box No. ._Backup Sample Box No.

Transfer for Recovery: __Original: Relinquished By 0- ft+~4 _____ Received By _jJ-/K* <^ —— Date/Time __Backup: Relinquished By _l/L/ *~r _____ Received By TT • /??•• Cts —— Date/Time -2-J-?7_ .Sample box recovery person(s): <7./ytc. —— __________________________ Date; -2_rJ?.

Probe assembly recovery person(s): 37, /S&e} / l~ Mts*s>.* __________________ Date: "? -3 -

TRAIN PURGES*: Original: Date/Start Time 2-'~2 "f? .J&i.. Stop Time ' ' Purged By ______________ Backup: Date/Start Time ^-J-fl /? tS Stop TimePurging Gas: Prepurifieri Nitrogen Flow Rata: /^ Liters/minute Desired Time: <3 ° minutes/impinger box

TRAIN RECOVERY: Weights below are in grams.Impinger: 1st 2nd 3rd 4th 5th 6th 7th

Description/Color:Original Set: _cj£&— yr__ _ .< is-e ^ _ <=/a-^___ .ci<*~ .- _, ...__-!„ ,„_... % Blue: __../O_Backup Set: _£/£— •____ _£f4a-x_..- _ £//U ._._- <zJ&* . _.. „.„==-._ __ % Blue: _ -,/O,=Check pH**: Must be greater than 8.5 in first four impingers.Original Set: _£rJL__ ....... fr_C-_ - f -5 - Final Wt.: _ A .J_ ..Co jLS~.4Backup Set: ?. (3 .JT ____ 7-^ f- — - Final Wt,: _ <£o£L4.,

Total Initial Silica Gel Impinger(s) Wt. for Original and Backup Set from Set-up Data: __LLL!LS_A. . . . . - - . - - - - - - - - - - - - - - - - - - - - - - - - - - Total Silica Gel Impinger(s) Weight Gain: .__•<?<?, 2. _

Train Sample Number: 7185 7185AB. .......-- Sample Bottle Tare Wt. From Set-up Data: /UV.o __ /,;? ._2-C. - - - - - - - - - - - - - - - - Current Sample Bottle Gross Wt. _/3. i-£.-?L __/_35^^ Before RinsesD. - - - - - - - - Sample Bottle Gross Wt. From Set-up Data: _ fJH- .1 .. __S3:(a-J..E, - - - - - - - - - - - - - - - - Net Liquid Condensate Collected _ 23A-J— __ TJJv-?, [C - D]

TOTAL CONDENSATE COLLECTED: I &22--H [A + total of E]Components Rinsed***: All components from nozzle through 5th impinger

Sample Bottle Gross Wt. _Z.64.y.5, JFOI*S After All Rinses AddedCheck pH 2:9 ****, pH: J. ?.«...__ _P_.ff.o_ Before Adjustment

pH: . ._ .... _ _ ,„_,_ .,. After AdjustmentF. ...................... sample Bottle Final Wt. /.La J,,. . J£°L:*L

Net Sample Wt. JJ_-§i .. [Total of F - Total of 81

FILTRATION OF SAMPLE NOS. 7 185 and 7185A O.4FJ //m Filrp-r Typs: /êFilter Lot Number: _ . O . .

Filtrate Sample Number: 7186 Residue Color: _..<?irc-'ki'USample Bottle Tare Wt. /JS.Q

Sample Bottle Gross Wt. 3T>/*f. «- Including Rinses of Filtration ApparatusNet Sample Wt. "\ I 1- f «- For Hexavalent Chromium Mass Collected Computations

Sample Mixed, Then:Sample Aliquot for Analysis ^* — -.-••-.-.-<. for Cr*6

Aliquot Sample Number: 7187Sample Bottle Tare Wt. /?•£Sample Bottle Final Wt. 3 \~13._2~- yVo-7

Net Sample Wt. JQYf-2.

Gas used for purge is passed through 0.1 N KOH in an impinger before entering train.pH checked with glass rod and pH indicator strips; solutions adjusted for subsequent runs as necessary. Void run if pHof any impinger (1st through 4th) is s8.5.Using a total of about 1 50-200 mLs of ASTM Type I water for each impinger set, rinse components 4 times. Use a totalof at least 100 mLs to rinse the nozzle, probe liner, tee assembly, and peristaltic pump tubing 4 times.Thoroughly mix sample and check pH; adjust to pH 9-10 with 2 N KOH if necessary.

COMMENTS:

VSCRHCCX WPD Seotember 5, 1996 (rev,.M5CRR23X.WPO January 20. 19971

AR3!5'A5APPENDIX B 239

£ÂJ "7SOLID WASTE FEED SAMPLING DATA



SAMPLING LOCATION: At the solid waste feed conveyor to the kiln in the solid waste storage and preparation'building.



SAMPLE PRESERVATION: All samples, XX120, XX199, and XX200 stored at near water ice temperature (i.e., 4°C), andbottles wrapped in aluminum foil. All samples, XX121, stored at near water ice temperature (i.e., 4°C). All samples, XX122,stored at near room temperature or cooler (i.e., 26°C).

Run No. ~@- i Date:


Grab_ ______ -• - -__„_ .._latejrup.tio.nsZCojnments__._.._

Caution: Material may contain P-naphthylamine. //0

Relinquished By ..WSTFEED3.WPO Fetaruw/1, 1997

APPENDIX B

f<L o AJ ~7

SOLID WASTE FEED SAMPLING DATA £ oe> £ J

MRI Project No. 3620.1 3.30Client/Source: OHM Remediation Services Corp., Drake Chemical Superfund Site, Mobile Hazardous Waste Incinerator


SAMPLING LOCATION: At the solid waste feed conveyor to the kiln inJhe solid waste storage and preparation building.

SAMPLING METHOD: Equal-sized grab samples of approximately iOQ'grams each collected with an aluminum* scoop frommaterial on th'e apron conveyor belt. Grab samples deposited, combined, and mixed in an aluminum* pan; then cut and splitinto 16 oz., wide mouth, precleaned, clear glass bottles. Bottles sealed with Teflon®-lined screw caps. (*As per COEprotocol.)

SAMPLING FREQUENCY: One (1) grab sample collected every 15 minutes during the run. Sampling conducted continuallyaccording to schedule except during stack-port changes on the stack and delays incurred during the run as noted below.

SAMPLE PRESERVATION: All samples,/XX1-23, XXJDQ,' and Xy.300 stored at near water ice temperature (i.e., 4°C), andbottles wrapped in aluminum foil. All Gamptes7-XX121 ;-ctorod at neai Wdim IC'B iBinpHi'aiure (i.e., 4"C). All lampion, yiX.123,«o»d-at^»a»L-ooB»»5iiipm-luiuui L-uului (i.e.. 2C"C)T- /!

I I / /Run No. >7 Date: __f2. /3./- 2J?. . .. Sampler(s): . l c'--.

____ ^____^ .grv .Composite Sample Number: 120______ 1 1 /———T22" ' T99 200

Composite Sample Designation:

GrabJ>icL_ .. JHme..,» _____________^rrrrrr^-_lQternuptions/Comments,,,

Caution: Material may contain p-naphthylamine.

Relinquished By _ . 5., == J,- Received By / f. C-SiC-e Date/Time 2.-"->- ~> <7<--cWSTFEED3 WPO Febtuary 1. 1997

APPENDIX B 241

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7BOTTOM ASH SAMPLING DATA





SAMPLING FREQUENCY: One (1) grab sample collected every 30 minutes during the run. Sampling conducted continuallyaccording to schedule except during stack port changes on the stack and delays incurred during the run as noted below,


Run No. _T_____ Date: 4-.r_T'_ T_ _ .___ ... Sampler(s); P • '<

Composite Sample Number: 7126 7127 7128 $29Composite Sample Designation: SVOC VOC TCLP/METALS GALBT

GrabjNo._ _lime_ ______________________lntexcuptions/,Commejits__ ___„,._.,

fTt.f' 3ft-f

Relinquished B y . r . , . . Received B y .•&-< t ^ Date/Time

8OTMASH3.WPO January 20, 1997

.AR3I5753APPENDIX B 247

7BOTTOM ASH SAMPLING DATA (DUPLICATE SAMPLES)

MRI Project No. 3620.13.30 .Client/Source: OHM Remediation Services Corp., Drake Chemical Superfund Site, Mobile Hazardous Waste Incinerator



SAMPLING METHOD: Equal sized grab samples of about 200 grams each collected with an aluminum* scoop. Grab samples-deposited, combined, and mixed in an aluminum* pan; then cut and split into 16 oz., wide mouth, precleaned, clear glassbottles. Bottles sealed with Teflon®-lined screw caps. (*As per COE protocol.)



Run No. '


Grab_N_CU_. __"Gmfi__" .'""- Intprriiptinns/rnmmanta

Relinquished By /Ol_ t _. . . Received By L<- 2 -<*rV __.- Date/Time £-3*.

BOTMSH3D.WPO January 20, 1997

AR3I575L*A DDE? Kin TV D

7BOTTOM ASH SAMPLING DATA (SAMPLE FOR COE)




SAMPLING METHOD: Equal sized grab samples of about 200 grams each collected with an aluminum* scoop. Grab samplesdeposited, combined, and mixed in an aluminum* pan; then cut and split into a 16 oz., wide mouth, precleaned, clear glassbottle. Bottle sealed with Teflon®-lined screw cap. (*As per COE protocol.)



Run No. _Z____. Date: 2-' *$' 9f_____ Sampler(s): _&

Composite Sample Number:Composite Sample Designation: COE

Grab,_NrL_ Tims ____________________latercuptLonsZCojnnienls

s sRelinquished By £x<ji i r_ Received By L , t^Z^f^^ Date/Time 2-"J-f7tr

BOTMSH3CWPO January 20, 1997


7FLY ASH SAMPLING DATA

MRI Project No. 3620.13.30 , 'Client/Source: OHM Remediation Services Corp., Drake Chemical Superfund Site, Mobile Hazardous Waste Incinerator



SAMPLING METHOD: Equal sized (approx. 100 grams) grab samples collected with an aluminum* scoop from each ofeighteen (lOTspacially spaced points over the surface and from a depth of 3 to 6 inches below the surface of the pile in thedump truck bed located under the end of the conveyor. Grab samples deposited, combined, and mixed in an aluminum* pan;then cut and split into 16 oz., wide mouth, precleaned, clear glass bottles. Bottles sealed with Teflon®-lined screw caps. (*Asper COE protocol.)


SAMPLE PRESERVATION: All samples, XX130 and XX131, stored at near water ice temperature (i.e., 4°C), and bottleswrapped in aluminum foil. All samples, XX132, stored at near water ice temperature (i.e., 4?C). All samples, XX1 33, storedat near room temperature or cooler (i.e., 26°C).

Run No. "7 Date: _2jlZr £Z____ Sampler(s): __£>_j_/$±J.t


Event- .„ - ,lnterr.up.ti.ons/.Comme.nts_

Relinquished By A/sJ& yfT.-—-.,. . Received 8y -XL^-^^TT^-•--••- Date/Time £-..£-.7.7. ,///2_

PLVASH3.WPO January 20, 1997

^3/5756 25O





SAMPLING METHOD: Equal sized (approx. 100 grams) grab samples collected with an aluminum* scoop from each ofaighteen (1'Q)-spacially spaced points over the surface and from a depth of 3 to 6 inches below the surface of the pile in thedump truck bed located under the end of the conveyor. Grab samples deposited, combined, and mixed in an aluminum* pan;then cut and split into 16 oz., wide mouth, precleaned, clear glass bottles. Bottles sealed with Teflon^-lined screw caps. ("Asper COE protocol.)



Run No. _2____ Date:


Interruptions/Comments.

Relinquished By < x - M r * & — Received By ._<g£~i*d,-.- .. Date/Timef~

fl_YASH30.WPD January 20. 1997

AR3J5757APPENDIX B 251





SAMPLING METHOD: Equal sized (approx. 100 grams) grab samples collected with an aluminum* scoop from each ofuightuen (TO) spacially spaced points over the surface and from a depth of 3 to 6 inches below the surface of the pile in thedump truck bed located under the end of the conveyor. Grab samples deposited, combined, and mixed in an aluminum* pan;then cut and split into a 16 oz., wide mouth, precleaned, clear glass bottle. Bottle sealed with Teflon®-lined screw cap. (*Asper COE protocol.)



Run No. _T.____. Date: Z.- - -jZ- ____ Sampler(s): ._j£?_ /•££

Composite Sample Numbep?Composite Sample Designatio

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