Top Banner
Field Chemistry Developed by Ken Cooke Kentucky Division of Water Watershed Watch Program Coordinator Modified by Mike Kemp Professor of Environmental Engineering Technology Murray State University
29

Field Chemistry Developed by Ken Cooke Kentucky Division of Water Watershed Watch Program Coordinator Modified by Mike Kemp Professor of Environmental.

Dec 23, 2015

Download

Documents

Donna Walters
Welcome message from author
This document is posted to help you gain knowledge. Please leave a comment to let me know what you think about it! Share it to your friends and learn new things together.
Transcript
Page 1: Field Chemistry Developed by Ken Cooke Kentucky Division of Water Watershed Watch Program Coordinator Modified by Mike Kemp Professor of Environmental.

Field Chemistry

Developed by Ken CookeKentucky Division of Water

Watershed Watch Program Coordinator

Modified by Mike KempProfessor of Environmental Engineering Technology

Murray State University

Page 2: Field Chemistry Developed by Ken Cooke Kentucky Division of Water Watershed Watch Program Coordinator Modified by Mike Kemp Professor of Environmental.

Field Chemistry Tests

• pH• Dissolved Oxygen• Conductivity• Temperature

*Some things are best done in person.

Page 3: Field Chemistry Developed by Ken Cooke Kentucky Division of Water Watershed Watch Program Coordinator Modified by Mike Kemp Professor of Environmental.

Field Chemistry Equipment

Testing strips such as pH paper and “dip strips” are not as accurate.

• Testing kits• Alcohol or mineral spirit • thermometers • Conductivity/TDS Meters• (calibrated) • pH meters calibrated with • 4-7-10 standard solutions

Page 4: Field Chemistry Developed by Ken Cooke Kentucky Division of Water Watershed Watch Program Coordinator Modified by Mike Kemp Professor of Environmental.

Measuring pH

Page 5: Field Chemistry Developed by Ken Cooke Kentucky Division of Water Watershed Watch Program Coordinator Modified by Mike Kemp Professor of Environmental.

pH Testing Kit

Page 6: Field Chemistry Developed by Ken Cooke Kentucky Division of Water Watershed Watch Program Coordinator Modified by Mike Kemp Professor of Environmental.

14131211109876543210

pH-Good Between 6-9 Standard Units

Acid Range

Basic or Alkaline Range

Page 7: Field Chemistry Developed by Ken Cooke Kentucky Division of Water Watershed Watch Program Coordinator Modified by Mike Kemp Professor of Environmental.

Interpreting pH Results

Page 8: Field Chemistry Developed by Ken Cooke Kentucky Division of Water Watershed Watch Program Coordinator Modified by Mike Kemp Professor of Environmental.

Measuring Dissolved Oxygen

Page 9: Field Chemistry Developed by Ken Cooke Kentucky Division of Water Watershed Watch Program Coordinator Modified by Mike Kemp Professor of Environmental.
Page 10: Field Chemistry Developed by Ken Cooke Kentucky Division of Water Watershed Watch Program Coordinator Modified by Mike Kemp Professor of Environmental.

Dissolved Oxygen Testing Kit

Page 11: Field Chemistry Developed by Ken Cooke Kentucky Division of Water Watershed Watch Program Coordinator Modified by Mike Kemp Professor of Environmental.
Page 12: Field Chemistry Developed by Ken Cooke Kentucky Division of Water Watershed Watch Program Coordinator Modified by Mike Kemp Professor of Environmental.
Page 13: Field Chemistry Developed by Ken Cooke Kentucky Division of Water Watershed Watch Program Coordinator Modified by Mike Kemp Professor of Environmental.

1514131211109876543210

Dissolved Oxygen Levels

0-4 mg/l = poor4-7 mg/l = fair7-10 mg/l = good10-14 mg/l = excellentover 14 = ? (Check your test!)

Page 14: Field Chemistry Developed by Ken Cooke Kentucky Division of Water Watershed Watch Program Coordinator Modified by Mike Kemp Professor of Environmental.

Interpreting Dissolved Oxygen Results

Page 15: Field Chemistry Developed by Ken Cooke Kentucky Division of Water Watershed Watch Program Coordinator Modified by Mike Kemp Professor of Environmental.

Dissolved Oxygen

Temperature

Page 16: Field Chemistry Developed by Ken Cooke Kentucky Division of Water Watershed Watch Program Coordinator Modified by Mike Kemp Professor of Environmental.

Measuring Conductivity

Page 17: Field Chemistry Developed by Ken Cooke Kentucky Division of Water Watershed Watch Program Coordinator Modified by Mike Kemp Professor of Environmental.

Conductivity Meter

Page 18: Field Chemistry Developed by Ken Cooke Kentucky Division of Water Watershed Watch Program Coordinator Modified by Mike Kemp Professor of Environmental.

1500140013001200110010009008007006005004003002001000

Conductivity O

il and Gas W

ell Discharge

The higher the number, the poorer the quality.

Waste W

ater Impact

Norm

al Stream

Rain

Page 19: Field Chemistry Developed by Ken Cooke Kentucky Division of Water Watershed Watch Program Coordinator Modified by Mike Kemp Professor of Environmental.
Page 20: Field Chemistry Developed by Ken Cooke Kentucky Division of Water Watershed Watch Program Coordinator Modified by Mike Kemp Professor of Environmental.

Conductivity

Flow

Page 21: Field Chemistry Developed by Ken Cooke Kentucky Division of Water Watershed Watch Program Coordinator Modified by Mike Kemp Professor of Environmental.

Field Observations

• Flow (0-5 point scale)• 24 hour rainfall (in inches)• Turbidity (0-3 point scale)

*Some things are best done in person.

Page 22: Field Chemistry Developed by Ken Cooke Kentucky Division of Water Watershed Watch Program Coordinator Modified by Mike Kemp Professor of Environmental.

0=Dry

4=Bank Full

5=Flood!

Flow Observations

0 = Dry1 = Ponded2 = Low3 = Normal4 = Bank Full5 = FLOOD!

*Get to know your creek.

Page 23: Field Chemistry Developed by Ken Cooke Kentucky Division of Water Watershed Watch Program Coordinator Modified by Mike Kemp Professor of Environmental.
Page 24: Field Chemistry Developed by Ken Cooke Kentucky Division of Water Watershed Watch Program Coordinator Modified by Mike Kemp Professor of Environmental.

Estimate rainfall in your watershedin quarter inches for the last 24 hours.

Use Weather Channel, local paper orToad Gauge.

Page 25: Field Chemistry Developed by Ken Cooke Kentucky Division of Water Watershed Watch Program Coordinator Modified by Mike Kemp Professor of Environmental.

Value Observation NTUs

0 Crystal Clear 0 NTUs

1 Clear 1-3 NTUs

2 Cloudy 4-12 NTUs

3 Muddy >12 NTUs

Turbidity (0-3 point scale)

Page 26: Field Chemistry Developed by Ken Cooke Kentucky Division of Water Watershed Watch Program Coordinator Modified by Mike Kemp Professor of Environmental.
Page 27: Field Chemistry Developed by Ken Cooke Kentucky Division of Water Watershed Watch Program Coordinator Modified by Mike Kemp Professor of Environmental.

Other Observations to Make

Putrescent or otherwise objectionable bottom deposits

Oil, scum, and floating debris in amounts that are unsightly

Nuisance levels of odor, color, other conditions

Page 28: Field Chemistry Developed by Ken Cooke Kentucky Division of Water Watershed Watch Program Coordinator Modified by Mike Kemp Professor of Environmental.

• DO kit• pH kit• Thermometer• Spent chemical waste container• Conductivity meter and screwdriver• “Blue Book” of instructions• Recording forms• Pencil• First aid kit

Field Chemistry Check List

Page 29: Field Chemistry Developed by Ken Cooke Kentucky Division of Water Watershed Watch Program Coordinator Modified by Mike Kemp Professor of Environmental.

Equipment Use

• There are hazardous chemicals in these kits!

• DO test uses a strong alkali (like bleach).

• pH test chemical is flammable.• Read Material Safety Data Sheets for

handling and disposal instructions.• Use plastic spent chemical waste

container at stream.• Dispose of waste properly at home.