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Particulates Found & Size < 10µm ASTM WK 21597 Not Required
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Analytical Data for Non-Hydrogen Gaseous Constituents
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The analytical data for each non-hydrogen gaseous constituent in SAE TIR J2719 is tabulated in the sequence below. The analytical data includes calibration standards, detection limit study, sample analysis, spike, or duplicate.
Non-Hydrogen Gaseous Constituents 1. Water 2. Total Hydrocarbons
2.1 Methane 2.2 Ethane, Ethene & Ethyne 2.3 Other Hydrocarbons
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Analytical Data
Injection File Name
Standard Conc.
(PPMV)
G0552,0.235 PPMV CO & 0.235 CH4 (16ML LOOP INJECTION) (OT=80C) PRE-COL IS @LIQ. N2 AND LOOP OPEN 5 MIN BEFORE AND 10 MIN AFTER VALVE TURNS. WITH PUMP. 10PSI CHECK VALVE. 001F0101.D 0.235
G0726,0.045 PPMV CO & 0.046 CH4 (16ML LOOP INJECTION) (OT=80C) PRE-COL IS @LIQ. N2 AND LOOP OPEN 5 MIN BEFORE AND 10 MIN AFTER VALVE TURNS. WITH PUMP. 10PSI CHECK VALVE. 001F0201.D 0.045
G0694, 0.00104 PPMV EACH CO & CH4 (16ML LOOP INJECTION) (OT=80C) PRE-COL IS @LIQ. N2 AND LOOP OPEN 5 MIN BEFORE AND 10 MIN AFTER VALVE TURNS. WITH PUMP.10PSI CHECK VALVE. 001F0301.D 0.00104
METHOD BLANK, JUST CARRIER GAS (16ML LOOP INJECTION) (OT=80C) PRE-COL IS @LIQ. N2 AND LOOP OPEN 5 MIN BEFORE AND 10MIN AFTER VALVE TURNS. WITH PUMP. 10PSI CHECK VALVE. 001F0401.D
10HY9001-01,KB092A,S100222,R100303 (16ML LOOP INJECTION) (OT=80C) PRE-COL IS @ LIQ. N2 AND LOOP OPEN 5 MIN BEFORE AND 10MIN AFTER VALVE TURNS. WITH PUMP. 10PSI CHECK VALVE. 001F0501.D
G0694, 0.00104 PPMV EACH CO & CH4 (16ML LOOP INJECTION) (OT=80C) PRE-COL IS @LIQ. N2 AND LOOP OPEN 5 MIN BEFORE AND 10 MIN AFTER VALVE TURNS. WITH PUMP.10PSI CHECK VALVE. 001F0601.D 0.00104
CH4 Date 3/11/2010
Ret. Time (MIN) of CH4 Area of CH4
CH4 Response Factor
Sample CH4
Conc. (ppmv)
4.851 66950 3.5E-06
4.895 13078 3.4E-06
4.91 459 2.3E-06
4.91 0 0.0E+00
4.899 521 1.2E-03
4.903 771 1.3E-06
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Analytical Data
C2 (Ethane, Ethene & Ethyne
InjectionInjection
Volume (uL)
1000UL G0345 (0.2PPMV CH4, HCCH,CH2CH2 & CH3CH3 IN H2) 1000
NOTES:U - Analytes not detected at, or above the stated detection limit.0 - A result of zero represents an undetected result at the MQL reported and does not imply an actual value.PPBV - Parts per billion volume.MQL - Method quantitation limit.Surrogate results are in units of percent recovery with control limits: 65 to 135%.The compounds in red and bold are organic halides.
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Analytical Data CO Date 3/11/2010
Injection File Name
Standard Conc.
(PPMV)Ret. Time
(MIN) of CO Area of COCO Response
FactorSample CO
Conc. (ppmv)
G0552,0.235 PPMV CO & 0.235 CH4 (16ML LOOP INJECTION) (OT=80C) PRE-COL IS @LIQ. N2 AND LOOP OPEN 5 MIN BEFORE AND 10 MIN AFTER VALVE TURNS. WITH PUMP. 10PSI CHECK VALVE. 001F0101.D 0.235 5.251 45819 5.1E-06
G0726,0.045 PPMV CO & 0.046 CH4 (16ML LOOP INJECTION) (OT=80C) PRE-COL IS @LIQ. N2 AND LOOP OPEN 5 MIN BEFORE AND 10 MIN AFTER VALVE TURNS. WITH PUMP. 10PSI CHECK VALVE. 001F0201.D 0.045 5.29 6277 7.2E-06
G0694, 0.00104 PPMV EACH CO & CH4 (16ML LOOP INJECTION) (OT=80C) PRE-COL IS @LIQ. N2 AND LOOP OPEN 5 MIN BEFORE AND 10 MIN AFTER VALVE TURNS. WITH PUMP.10PSI CHECK VALVE. 001F0301.D 0.00104 5.326 514 2.0E-06
METHOD BLANK, JUST CARRIER GAS (16ML LOOP INJECTION) (OT=80C) PRE-COL IS @LIQ. N2 AND LOOP OPEN 5 MIN BEFORE AND 10MIN AFTER VALVE TURNS. WITH PUMP. 10PSI CHECK VALVE. 001F0401.D 5.326 0 0.0E+00
10HY9001-01,KB092A,S100222,R100303 (16ML LOOP INJECTION) (OT=80C) PRE-COL IS @ LIQ. N2 AND LOOP OPEN 5 MIN BEFORE AND 10MIN AFTER VALVE TURNS. WITH PUMP. 10PSI CHECK VALVE. 001F0501.D 5.332 54 1.1E-04
G0694, 0.00104 PPMV EACH CO & CH4 (16ML LOOP INJECTION) (OT=80C) PRE-COL IS @LIQ. N2 AND LOOP OPEN 5 MIN BEFORE AND 10 MIN AFTER VALVE TURNS. WITH PUMP.10PSI CHECK VALVE. 001F0601.D 0.00104 5.32 685 1.5E-06
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Analytical Data
HCOOH ASTM D5466 Application on Hydrogen for HCOOH on 3/15/2010
FILE NAME InjectionVolume of
Hydrogen (mL)
Volume Injected (uL) of HCOOH Standard @ 37
PPMVRET TIME
OF HCOOHAREA OF HCOOH
Response Factor (RF) or Sample Conc in ppmv- Sample Vol=500mL or %
Spike Recovery
001F0101.D
10UL G0752 (37 PPMV HCOOH IN H2) WITH LN2 AND FAST MODE. CF=30MLK/MIN (SET @ 30) AND MAKE-UP FR=87.7ML/MIN. 30M 0.53MM ID 3.0UM DB5 FSCC (SC0CC 001). PUMP=MIDDLE. INJ. T=90C. DESORBED @RT H2O. 10 0.544 8.45E+05 4.4E-10
001F0501.D
10UL G0752 (37 PPMV HCOOH IN H2) WITH LN2 AND FAST MODE. CF=30MLK/MIN (SET @ 30) AND MAKE-UP FR=87.7ML/MIN. 30M 0.53MM ID 3.0UM DB5 FSCC (SC0CC 001). PUMP=MIDDLE. INJ. T=90C. DESORBED @RT H2O. 10 0.704 7.33E+05 5.0E-10
001F0601.D
500ML 10CTX046 (CTX OAKT H2, SR100224) WITH LN2 AND FAST MODE. CF=30MLK/MIN (SET @ 30) AND MAKE-UP FR=87.7ML/MIN. 30M 0.53MM ID 3.0UM DB5 FSCC (SC0CC 001). PUMP= MIDDLE. INJ. T=90C. DESORBED @RT H2O. 500 1.215 4.18E+04 4.5E-05
001F0701.D
500ML 10HY9001 (KB092A, S100222, R100303) WITH LN2 AND FAST MODE. CF=30MLK/MIN ( SET @ 30) AND MAKE-UP FR=87.7ML/MIN. 30M 0.53MM ID 3.0UM DB5 FSCC (SC0CC 001). PUMP=MIDDLE. INJ. T=90C. DESORBED @RT H2O. 500 1.165 3.08E+04 3.3E-05
001F0801.D
10UL G0752 (37 PPMV HCOOH IN H2)+500ML 10HY9001 (KB092A, S100222, R100303) WITH LN2 AND FAST MODE. CF=30MLK/MIN (SET @ 30) AND MAKE-UP FR=87.7ML/MIN. 30M 0.53MM ID 3.0UM DB5 FSCC (SC0CC 001). PUMP=MIDDLE. INJ. T=90C. DESORBED @RT H2O. 500 10 0.715 4.34E+05
HCOOH % Recovery at 0.0007 PPMV is 63%
001F0901.D
10UL G0752 (37 PPMV HCOOH IN H2)+500ML 10CTX046 (CTX OAKT H2, SR100224) WITH LN2 AND FAST MODE. CF=30MLK/MIN (SET @ 30) AND MAKE-UP FR=87.7ML/MIN. 30M 0.53MM ID 3.0UM DB5 FSCC (SC0CC 001). PUMP=MIDDLE. INJ. T=90C. DESORBED @RT H2O. 500 10 0.644 6.55E+05
HCOOH % Recovery at 0.0007 PPMV is 96%
001F1001.D
10UL G0752 (37 PPMV HCOOH IN H2) WITH LN2 AND FAST MODE. CF=30MLK/MIN (SET @ 30) AND MAKE-UP FR=87.7ML/MIN. 30M 0.53MM ID 3.0UM DB5 FSCC (SC0CC 001). PUMP=MIDDLE. INJ. T=90C. DESORBED @RT H2O. 10 0.445 5.44E+05 6.8E-10
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NH3ASTM D5466 Application on Hydrogen for NH3 on 3/15/2010
FILE NAME Injection H2 VOLUME (ML)
Volume Injected (uL) of NH3 Standard @ 5904
PPMVRET TIME OF NH3
AREA OF NH3
Response Factor (RF) or Sample Conc in ppmv-
Sample Vol=500mL or % Spike Recovery
001F0101.D
1.6UL G0743 (5904PPMV NH3 IN H2). WITH LIQ. N2. CF=30ML/MNAND MAKE-UP=82.3ML/ MIN. 30M 0.53MM ID 3.0UM DB5 FSCC (SC0CC 001). N MODE. PUMP AT 5 BACK TURNS RATE. DESORBED @RT H2O. 1.6 0.325 2.11E+05 4.5E-08
001F0301.D
1.6UL G0743 (5904PPMV NH3 IN H2). WITH LIQ. N2. CF=30ML/MNAND MAKE-UP=82.3ML/ MIN. 30M 0.53MM ID 3.0UM DB5 FSCC (SC0CC 001). N MODE. PUMP AT 5 BACK TURNS RATE. DESORBED @RT H2O. 1.6 0.328 3.17E+05 3.0E-08
001F0401.D
500ML 10CTX046 (CTX OAKT H2,SR100224). WITH LIQ. N2. CF=30ML/MNAND MAKE-UP=82. 3ML/MIN. 30M 0.53MM ID 3.0UM DB5 FSCC (SC0CC 001). N MODE. PUMP AT 5 BACK TURNS RATE. DESORBED @RT H2O. 500 0.328 0.00E+00 0.0E+00
001F0501.D
1.6UL G0743 (5904PPMV NH3 IN H2)+500ML 10CTX046 (CTX OAKT H2,SR100224). WITH LIQ. N2. CF=30ML/MNAND MAKE-UP=82.3ML/MIN. 30M 0.53MM ID 3.0UM DB5 FSCC (SC0CC 001). N MODE. PUMP AT 5 BACK TURNS RATE. DESORBED @RT H2O. 500 1.6 0.338 2.19E+05
NH3 % Recovery at 0.019 PPMV is 87%
001F0601.D
500ML 10HY9001 (KB092A, S100222, R100303). WITH LIQ. N2. CF=30ML/MNAND MAKE-UP= 82.3ML/MIN. 30M 0.53MM ID 3.0UM DB5 FSCC (SC0CC 001). N MODE. PUMP AT 5 BACK TURNS RATE. DESORBED @RT H2O. 500 0.338 0.00E+00 0.0E+00
001F0701.D
1.6UL G0743 (5904PPMV NH3 IN H2)+500ML 10HY9001 (KB092A, S100222, R100303). WITH LIQ. N2. CF=30ML/MNAND MAKE-UP=82.3ML/MIN. 30M 0.53MM ID 3.0UM DB5 FSCC (SC0CC 001). N MODE. PUMP AT 5 BACK TURNS RATE. DESORBED @RT H2O. 500 1.6 0.325 1.94E+05
NH3 % Recovery at 0.019 PPMV is 78%
001F0801.D
1.6UL G0743 (5904PPMV NH3 IN H2). WITH LIQ. N2. CF=30ML/MNAND MAKE-UP=82.3ML/ MIN. 30M 0.53MM ID 3.0UM DB5 FSCC (SC0CC 001). N MODE. PUMP AT 5 BACK TURNS RATE. DESORBED @RT H2O. 1.6 0.326 2.44E+05 3.9E-08
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Analytical Data
Cl2 ASTM D5466 Application on Hydrogen for Cl2 on 3/15/2010
FILE NAME InjectionVolume of Hydrogen
(mL)Volume Injected (uL) of Cl2
Standard @ 145 PPMVRET TIME OF
Cl2 AREA OF Cl2
Response Factor (RF) or Sample Conc in ppmv- Sample Vol=500mL or %
Spike Recovery
001F0101.D
10UL G0758(144.7 PPMV CL2 IN H2) WITH LIQ. N2. N AND FAST MODE. CF=SET @30% of 100ML/MN) AND MAKE-UP=82.3ML/MIN. 30M 0.53MM ID 3.0UM DB5 FSCC (SC0CC 001). PUMP= MIDDLE. TRAP AT RT H2O WHILE DESORBED. 10 0.487 1.17E+05 1.2E-08
001F0801.D
3.5UL G0758(144.7 PPMV CL2 IN H2) WITH LIQ. N2. N AND FAST MODE. CF=SET @30% of 100ML/MN) AND MAKE-UP=82.3ML/MIN. 30M 0.53MM ID 3.0UM DB5 FSCC (SC0CC 001). PUMP= MIDDLE. TRAP AT RT H2O WHILE DESORBED. 3.5 0.501 5.41E+05 9.4E-10
001F0901.D
3.5UL G0758(144.7 PPMV CL2 IN H2) WITH LIQ. N2. N AND FAST MODE. CF=SET @30% of 100ML/MN) AND MAKE-UP=82.3ML/MIN. 30M 0.53MM ID 3.0UM DB5 FSCC (SC0CC 001). PUMP= MIDDLE. TRAP AT RT H2O WHILE DESORBED. 3.5 0.484 4.67E+05 1.1E-09
001F1001.D
3.5UL G0758(144.7 PPMV CL2 IN H2) WITH LIQ. N2. N AND FAST MODE. CF=SET @30% of 100ML/MN) AND MAKE-UP=82.3ML/MIN. 30M 0.53MM ID 3.0UM DB5 FSCC (SC0CC 001). PUMP= MIDDLE. TRAP AT RT H2O WHILE DESORBED. 3.5 0.477 3.44E+05 1.5E-09
001F1101.D
500ML 10CTX046 (CTX OAKT H2, SR100224) WITH LIQ. N2. N AND FAST MODE. CF=SET @ 30% of 100ML/MN) AND MAKE-UP=82.3ML/MIN. 30M 0.53MM ID 3.0UM DB5 FSCC (SC0CC 001) . PUMP=MIDDLE. TRAP AT RT H2O WHILE DESORBED. 500 1.089 6.31E+04 1.4E-04
001F1201.D
500ML 10CTX046 (CTX OAKT H2, SR100224) WITH LIQ. N2. N AND FAST MODE. CF=SET @ 30% of 100ML/MN) AND MAKE-UP=82.3ML/MIN. 30M 0.53MM ID 3.0UM DB5 FSCC (SC0CC 001) . PUMP=MIDDLE. TRAP AT RT H2O WHILE DESORBED. 500 1.08 3.13E+04 7.1E-05
001F1301.D
500ML 10HY9001-01 (KB092A, S100222, R100303) WITH LIQ. N2. N AND FAST MODE. CF= SET @30% of 100ML/MN) AND MAKE-UP=82.3ML/MIN. 30M 0.53MM ID 3.0UM DB5 FSCC (SC0CC 001). PUMP=MIDDLE. TRAP AT RT H2O WHILE DESORBED. 500 1.094 2.97E+04 6.8E-05
001F1401.D
3.5UL G0758(144.7 PPMV CL2 IN H2)+500ML 10HY9001-01 (KB092A, S100222, R100303) WITH LIQ. N2. N AND FAST MODE. CF=SET @30% of 100ML/MN) AND MAKE-UP=82.3ML/MIN. 30M 0.53MM ID 3.0UM DB5 FSCC (SC0CC 001). PUMP=MIDDLE. TRAP AT RT H2O WHILE DESORBED. 500 3.5 0.64 3.51E+05
Cl2 % Recovery at 0.001 PPMV is 79%
001F1501.D
3.5UL G0758(144.7 PPMV CL2 IN H2)+500ML 10CTX046 (CTX OAKT H2, SR100224) WITH LIQ. N2. N AND FAST MODE. CF=SET @30% of 100ML/MN) AND MAKE-UP=82.3ML/MIN. 30M 0. 53MM ID 3.0UM DB5 FSCC (SC0CC 001). PUMP=MIDDLE. TRAP AT RT H2O WHILE DESORBED. 500 3.5 1.274 3.54E+05
Cl2 % Recovery at 0.001 PPMV is 80%
001F1601.D
3.5UL G0758(144.7 PPMV CL2 IN H2) WITH LIQ. N2. N AND FAST MODE. CF=SET @30% of 100ML/MN) AND MAKE-UP=82.3ML/MIN. 30M 0.53MM ID 3.0UM DB5 FSCC (SC0CC 001). PUMP= MIDDLE. TRAP AT RT H2O WHILE DESORBED. 3.5 0.463 4.71E+05 1.1E-09
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Analytical Data
HCl ASTM D5466 Application on Hydrogen for HCl on 3/15/2010
FILE NAME InjectionVolume of Hydrogen
(mL)
Volume Injected (uL) of HCl Standard @ 299
PPMVRET TIME OF
HCl AREA OF HCl
Response Factor (RF) or Sample Conc in
ppmv- Sample Vol=500mL or % Spike
Recovery
001F0101.D
1.6UL G0760 (299 PPMV HCL IN H2). WITH LIQ. N2. N AND FAST MODE. CF=30MLK/MIN ( SET @ 30) AND MAKE-UP FR=87.7ML/MIN. 30M 0.53MM ID 3.0UM DB5 FSCC (SC0CC 001). PUMP=MIDDLE.TRAP DESORBED @RT H2O. 1.6 0.5 1.12E+06 4.3E-10
001F0301.D
1.6UL G0760 (299 PPMV HCL IN H2). WITH LIQ. N2. N AND FAST MODE. CF=30MLK/MIN ( SET @ 30) AND MAKE-UP FR=87.7ML/MIN. 30M 0.53MM ID 3.0UM DB5 FSCC (SC0CC 001). PUMP=MIDDLE.TRAP DESORBED @RT H2O. 1.6 0.59 8.09E+05 5.9E-10
001F0501.D
500ML 10HY9001-01 (KB092A, S102022, R100303). WITH LIQ. N2. N AND FAST MODE. CF= 30MLK/MIN (SET @ 30) AND MAKE-UP FR=87.7ML/MIN. 30M 0.53MM ID 3.0UM DB5 FSCC ( SC0CC 001). PUMP=MIDDLE.TRAP DESORBED @RT H2O. 500 0.519 2.10E+04 1.9E-05
001F0601.D
1.6UL G0760 (299 PPMV HCL IN H2)+500ML 10HY9001-01 (KB092A, S102022, R100303). WITH LIQ. N2. N AND FAST MODE. CF=30MLK/MIN (SET @ 30) AND MAKE-UP FR=87.7ML/MIN. 30M 0.53MM ID 3.0UM DB5 FSCC (SC0CC 001). PUMP=MIDDLE.TRAP DESORBED @RT H2O. 500 1.6 0.423 1.75E+05
HCl % Recovery at 0.001 PPMV is 17%
001F0701.D
1.6UL G0760 (299 PPMV HCL IN H2)+500ML 10CTX046 (CTX OAKT H2, S100224, R100303). WITH LIQ. N2. N AND FAST MODE. CF=30MLK/MIN (SET @ 30) AND MAKE-UP FR=87.7ML/MIN. 30M 0.53MM ID 3.0UM DB5 FSCC (SC0CC 001). PUMP=MIDDLE.TRAP DESORBED @RT H2O. 500 1.6 0.523 3.20E+05
HCl % Recovery at 0.001 PPMV is 30%
001F1001.D
1.6UL G0760 (299 PPMV HCL IN H2). WITH LIQ. N2. N AND FAST MODE. CF=30MLK/MIN ( SET @ 30) AND MAKE-UP FR=87.7ML/MIN. 30M 0.53MM ID 3.0UM DB5 FSCC (SC0CC 001). PUMP=MIDDLE.TRAP DESORBED @RT H2O. 1.6 0.501 1.42E+06 3.4E-10
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Analytical Data
HBr ASTM D5466 Application on Hydrogen for HBr on 3/15/2010
FILE NAME InjectionVolume of
Hydrogen (mL)
Volume Injected (uL) of HBr
Standard @ 161 PPMV
RET TIME OF HBr AREA OF HBr
Response Factor or Sample Conc in ppmv- Sample
Vol=500mL
001F0901.D
3UL G0759(161 PPMV HBR IN H2) WITH LIQ. N2. N AND FAST MODE. CF=30MLK/MIN (SET @ 30) AND MAKE-UP FR=87.7ML/MIN. 30M 0.53MM ID 3.0UM DB5 FSCC (SC0CC 001). PUMP= MIDDLE. INJ. T=90C.TRAP DESORBED @RT H2O. 3 0.639 5.41E+05 8.9E-10
001F1101.D
3UL G0759(161 PPMV HBR IN H2) WITH LIQ. N2. N AND FAST MODE. CF=30MLK/MIN (SET @ 30) AND MAKE-UP FR=87.7ML/MIN. 30M 0.53MM ID 3.0UM DB5 FSCC (SC0CC 001). PUMP= MIDDLE. INJ. T=90C.TRAP DESORBED @RT H2O. 3 0.557 3.91E+05 1.2E-09
001F1301.D
3UL G0759(161 PPMV HBR IN H2) WITH LIQ. N2. N AND FAST MODE. CF=30MLK/MIN (SET @ 30) AND MAKE-UP FR=87.7ML/MIN. 30M 0.53MM ID 3.0UM DB5 FSCC (SC0CC 001). PUMP= MIDDLE. INJ. T=90C.TRAP DESORBED @RT H2O. 3 0.629 3.25E+05 1.5E-09
001F1501.D
500ML 10HY9001 (KB092A, S100222, R100303) WITH LIQ. N2. N AND FAST MODE. CF= 30MLK/MIN (SET @ 30) AND MAKE-UP FR=87.7ML/MIN. 30M 0.53MM ID 3.0UM DB5 FSCC ( SC0CC 001). PUMP=MIDDLE. INJ. T=90C.TRAP DESORBED @RT H2O. 500 0.654 2.24E+04 5.8E-05
001F1601.D
3UL G0759 (161 PPMV HBR IN H2)+500ML 10HY9001 (KB092A, S100222, R100303) WITH LIQ. N2. N AND FAST MODE. CF=30MLK/MIN (SET @ 30) AND MAKE-UP FR=87.7ML/MIN. 30M 0.53MM ID 3.0UM DB5 FSCC (SC0CC 001). PUMP=MIDDLE. INJ. T=90C.TRAP DESORBED @RT 500 3 0.801 2.30E+05
HBr % Recovery at 0.001 PPMV is 61%
001F1901.D
3UL G0759 (161 PPMV HBR IN H2)+500ML 10CTX046 (CTX OAKT H2, SR100224). WITH LIQ. N2. N AND FAST MODE. CF=30MLK/MIN (SET @ 30) AND MAKE-UP FR=87.7ML/MIN. 30M 0. 53MM ID 3.0UM DB5 FSCC (SC0CC 001). PUMP=MIDDLE. INJ. T=90C.TRAP DESORBED @RT H2O. 500 3 0.718 1.87E+05
HBr % Recovery at 0.001 PPMV is 50%
001F2401.D
3UL G0759(161 PPMV HBR IN H2) WITH LIQ. N2. N AND FAST MODE. CF=30MLK/MIN (SET @ 30) AND MAKE-UP FR=87.7ML/MIN. 30M 0.53MM ID 3.0UM DB5 FSCC (SC0CC 001). PUMP= MIDDLE. INJ. T=90C.TRAP DESORBED @RT H2O. (USED AFTER UN-CLOGGING AND G0758(144.7 PPMV CL2) INJECTION OF 10UL FIVE TIMES. 3 0.793 4.23E+05 1.1E-09
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