Demonstration 2 Generation Fuel Ethanol Plant Bio-Energy ...

RFS

For

Demonstration 2nd Generation Fuel Ethanol Plant

Submitted to

Centre for High Technology

(Ministry of Petroleum & Natural Gas)

Under

Pradhan Mantri JI-VAN Yojana

By

Bio-Energy Engineering Working like Bees for making you Energy Independent…….

Reg. office : - 7/B, Ghaisas Layout, Surendra Nagar, Nagpur, India

Cor. office : - Office No 418 , The Address Commercia, Wakad, Pune, India

Web Address: - www.bee.net.in & www.bioenergyengineering.com

BEE-CHT-BEP-1272-22

2nd Generation Fuel Ethanol Plant 2

CONTENTS

Sr. No Sections Page No.

1 Technical Qualification Criteria 3

2 Commercial Qualification Criteria 15

3

Detail project Proposal 3.1 Project Block Diagram 3.2 Proposed Basis of Design 3.3 Process Description 3.4 Technical specifications & list of the equipments 3.5 Input Requirement 3.6 Output Generation 3.7 Product Specifications

19

4 Land Availability Document 66

5 Result of Trail 67

6 Self Declaration 68

BEE-CHT-BEP-1272-22


1. TECHNICAL QUALIFICATION CRITERIA We as a “BEE’’ ‘Bio-Energy Engineering’ trying to save Earth by contributing and taking responsibility for the Design, Engineering, supply and commissioning of Green Fuels Plant such as Biodiesel, Biogas, Biolubricants, Bio-fuel, In addition to this we took moral responsibilities for saving water by treating Solid, liquid and any other waste with our unique effluent technology a complete Zero liquid Discharge system . We also deal in turn key solutions for Starch Plant, Starch Derivative Plant, Tocopherol Plant, Lecithin Plant, Project management consultancy to execute the project on time, We would like to introduce our self as one stop complete Solution Company for Chemical Process Designing and Engineering field. Bio-Energy Engineering with over 13 years of Industrial Experience OUR EXPERTISE AREAS

! Turn key Solutions-Bio- Ethanol, Bio-Diesel, Biogas, Starch Plant, Starch Derivatives, Lecithin Plant.

! Evaporation & Drying ! Distillation & Heat Exchangers ! Reactors, Extractors & Agitators ! Micro-Brewery, Pub-Brewery ! Zero Liquid Discharge ! Water & Waste Water Management ! Fire Hydrant System ! Piping & Structural ! Project Management Services

BEE-CHT-BEP-1272-22


PROJECTS DONE

Grain based Ethanol Plant Equipment Product Capacity Client Turn Key Design, Engineering & Supply complete Plant

ENA - Extra Neutral Alcohol 20 KLPD NSCPL, Odisha

Techinal Consultancy ENA - Extra Neutral Alcohol 30 KPLD JBPL, Omerga

Project Handled Indiuivally Privilege Industries Ltd- Design.

ENA - Extra Neutral Alcohol 75 KLPD Mumbai,Maharashtra

Shri Teja Bio fuels Ltd- Design

ENA - Extra Neutral Alcohol 30 KLPD Hydrabad

Grainotch Industries Ltd- Design

ENA - Extra Neutral Alcohol 45 KLPD

Aurangabad,Maharashtra

MP Distilleries Ltd- Design.

ENA - Extra Neutral Alcohol 75 KLPD Hydrabad

Tilak Nagar Industries Ltd- Excecution

ENA - Extra Neutral Alcohol 110 KLPD Shirampur,Maharashtra

Adlers Bioenergy Ltd.- Trouble Shooting

ENA - Extra Neutral Alcohol 45 KLPD Osmanada,Maharashtra

NV Distilleries Ltd - Excecution

ENA - Extra Neutral Alcohol 100 KLPD Ambala, Punjab

Molasses based Ethanol Plant Equipment Product Capacity Client Tilak Nagar Industries Ltd- Excecution

ENA - Extra Neutral Alcohol 50 KLPD Shirampur,Maharashtra

Karmaveer Shankarrao Kale SSK Ltd- Revamping of compelte Distillery RS - Rectified Spirit 20 KLPD Kopergaon,Maharashtra Dr. Babasaheb Ambedkar SSk. LTD, Design. RS,ENA 45 KLPD Osmanada,Maharashtra Bhairavnat Sugar Pvt. Ltd Design. RS,ENA,Fuel Ethanol 45 KLPD Solapur, Maharashtra SLN Pvt. Ltd Distillery RS,ENA,Fuel Ethanol 20 KLPD Dharwad, Karanataka Starch Plant Equipment Product Capacity Client Turn Key Design, Engineering & Supply complete Plant

Strach Plant, Liquid Glucose, Maltose 90 TPD NSCPL, Odisha

Techinal Consultancy Strach Plant, Liquid Glucose, Maltose 500 TPD

Honest Derivative, Jamner


Yashwant Glucose Kharkhana SSK,

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Kolhapur


Sunanda Agro, Kolhapur

Multiple Effect Evaporator Equipment Product Capacity Client Turn key Zero Liquid discharge Multiple effect evaporators- 3 Effect R O Reject Water 90 TPD

Adani Wilmar Ltd in Mundra, being Nalco as immediate client.

Turn key Multiple effect evaporation Plant- 2 effect Meat Peptone 50 TPD

Phoenix Agro Processing and Bio Chemical Pvt. Ltd., Solapur

Turn key Multiple effect evaporation Plant- 2 effect Collagen Protein 50 TPD

Phoenix Agro Processing and Bio Chemical Pvt. Ltd., Solapur

Turn key Multiple effect evaporation Plant- 2 effect Protein Hydrolysate 50 TPD

Crescent Biotech, Solapur

Multiple effect evaporators- 5 effect engineering package Molasses Spent Wash 500 KLPD

Dr. Babasaheb Ambedkar SSk. LTD, being Mega as immediate client.

Multiple effect evaporators engineering package Liquid Glucose 40 TPD

Triveni Engineering, Ahmedabad.

Turn key Triple effect Evaporation Liquid Glucose 50 KLPD

Siddhivinayak Agro Industries Pvt. Ltd. (M.P),

Turn key double effect Evaporation Liquid Glucose 30 KLPD

Siddhivinayak Agro Industries Pvt. Ltd. (M.P),

Multiple effect evaporators- 4 effect Thin slop 150 KLPD Tecpert ,Pune Single Effect batch Evaporator Meat Peptone 30 TPD

Protech Netraceutcals, Solapur

Turn key Falling film Evaporator

Phosphatidylcholine-35 (PC-35) 30 TPD

Allied Soyatech, Bhandra.

ATFD - Agitated Thin Film Dryer / Wiped Film Evaporator Equipment Product Capacity Client

ATDF for ZDL R O Reject Water 10 TPD

Adani Wilmar Ltd in Mundra, being Nalco as immediate client.

ATFD / WFE for Food Product





Radiance Biochem Pvt Ltd, Palghar.



Radiance Biochem Pvt Ltd, Palghar.

BEE-CHT-BEP-1272-22


Food Equipment Product Capacity Client

Extractor Lecthin 5 KL Allied Soyatech, Bhandra.

Reactor Phosphatidylcholine-35 (PC-35) 3 KL


Hydrolysis Reactor Phosphatidylcholine-35 (PC-35) 5 KL


Extractor Lecthin 3 KL Radiance Biochem Pvt Ltd, Palghar.

Pharma Equipment Product Capacity Client Fermentors Design, Engineering & Supply complete Plant Bio- Fertilers 2 KL Chempharma, Banglore

Techinal Consultancy Bulk Chemcial 12 KL Siddharth Chemcial, Mumbai

Fire Alram & Hydrant system Equipment Product Capacity Client Turn Key Design, Engineering & Supply complete System

Fire Alram Hydrant System

60 KLPD Grain distillery

Ankur Biochem Pvt Ltd , Dhanbad

Turn Key Design, Engineering & Supply complete System

Fire Alram & Hydrant System 5000 Sq Ft

Floorspace Pvt Ltd, Pune

Turn Key Design, Engineering & Supply complete System

Fire Alram & Hydrant System 40000 sq ft

Commander Water Tech Pvt Ltd, Mumbai

BEE-CHT-BEP-1272-22


OUR PRESENCE

Reg. off.- 7/ B GHS L/O, Surendra Nagar, Nagpur-440015, Maharashtra, India. Cor. off.- Office No- 418, The address Commercia, Mumbai- Bangalore Highway, Wakad,

Pune-41102, Maharashtra, India Works – Plot No-2, Khadi machine, Chowisawadi, Charoli, Bhosari, Pune-412105,

Maharashtra, India Hand held. +91-9960400959, +91-9823765467

Tel. +91-712-2225377 Email Address [email protected] Web Address

www.bet.net.in www.bioeenrgyengineering.com

BRIEF RESUME OF KEY PERSONNEL

1. Vishal Vijay Gohade

EDUCATIONAL PROFILE

M-Tech in Chemical Engineering , SGBAU

B-Tech in Chemical Technology (Petroleum Refining & Petrochemical Technology) , Laxminarayan Institute of Technology (L.I.T), Nagpur

Diploma in Chemical Engineering from Shri Datta Meghe Polytechnic (S.D.M.P), Nagpur Post Graduate Diploma in Piping engineering from Vishveshwarya Institute of technology,Pune

MBA in Marketing Management and International Trade

Total Experience: 18 + years Industry: Chemical Process Industry Functional Area: Engineering Design, Procurement & Commissioning. Software tools Used: CHEMCAD, HTRI, ASPEN, and HYSYS

Director: Bio-Energy Engineering Since 2010.

Projects Executed for Clients:

Adani Willmar Ltd, Mundra. Nalco Water – ECOLAB,Pune Phoenix Agro Processing And Bio-chemical Pvt Ltd, Solapur. Crescent Biotech, Antroli. Siddharath Chemcials, Mumbai Protech Nutraceuticals, Solapur Chempharma Engineers, Bangalore Allied Soyatech, Bhandra Radiance Biochem Pvt Ltd, Palghar Floorspace Pvt Ltd, Pune Process Concept, Nagpur Ankur Biochem Pvt. Ltd, Dhanbad. Siddhivinayak Agro Industries Pvt. Ltd, Chinwada Tilak Nagar Industry, Shirampur.

BEE-CHT-BEP-1272-22


Past Experience : SRS BIODIESEL & ENGINEERING PVT LTD. Oct 08 to Oct 10. Designation: Sr.Process Manager Responsibilities:

. Design and development of Turnkey Biodiesel Plant.

. Over all Activities in Process engineering department.

. Process Standardization and Mass Energy Balance development for glycerin Purification Plant.

. Standardization of Material and Energy Balance.

. Design and development in Solvent recovery system.

. Design and development of washing systems

. Major Projects Executed:

. Omni Agro , USA - Turn key Biodiesel Project

. GAF , USA - Turn key Biodiesel Project

. Best Energy, USA- Methanol Recovery Unit

. Global Alternative Fuel, USA- Methanol and Biodiesel Recovery Unit

. Process Concept, Moberly, USA -Methanol and Biodiesel Recovery Unit

. Vapor Point -Solvent Recovery System

. WinPak, American Enw :Drum Compacting & Washing

. ACHIEVEMENTS: § Design fabrication and commissioning of 2 Ton Plant per Day

high FFA % of Biodiesel. § Recovery of H2SO4 from Methanol by salt absorption

method. § Glycerin purification plant process standardization. § Reaction time of bio-

diesel manufacturing process was reduced by using spray method. § Degumming of

bio-diesel process was stabilized and parameters standardized. § Achieved

proficiency in Hydro cyclone and centrifuges decanters. § Design of Customized

Multi-Effect Evaporator schemes for various services. § Was an integral part of the

trials and research for bio gas engine.

PRAJ INDUSTRIES, PUNE,- From Dec 06 to Oct 08

Designation: Team Leader- Process Engineer Responsibility: Process Designing &

BEE-CHT-BEP-1272-22


Development of Ethanol & Evaporation plant Software tools Used: CHEMCAD, HTRI, ASPEN, HYSYS

The Position calls for: Developing an energy efficient and cost effective scheme for the process of evaporation of various services.

o The process involving the following Key responsibilities:

- Preparing and delivering Customized schemes.

- Undertaking the complete process engineering of the entire project

- Equipment Sizing, Pump selection, preparing PFD & P&ID, finalizing the control logic, preparation of operation manuals

- Commissioning and trouble shooting of the process.

- Training of sub-ordinates and client operators on the job. Project Designed:

1. 300TPD Biodiesel Plant design and offer for HanilEra Industries Ltd.

2. PrivilegeIndustriesLtd-75KLPDDesign.

3. ShriTejaBiofuelsLtd-30KLPDDesign.

4. GrainotchIndustriesLtd-45KLPDDesign.

5. MPDistilleriesLtd-75KLPDDesign.

6. Warkem BioTech Ltd- Protein Hydrolysate plant design.

Project Commissioned: - 1) Ridhi Sidhi Gluco Bilos Ltd. Rudrapur, Asia’s biggest Starch

and Starch Derivative Manufacturer- -Evaporation Section – Liquid Glucose Acidic -

Evaporation Section – Liquid Glucose Enzymatic -Evaporation Section – Maltose

Dextrin -Evaporation Section – Dextrose Mono Hydrates

2) Gujarat Ambhuja Export Ltd, Sitarganj- Starch and Starch Derivative Manufacturer- -

Evaporation Section – Liquid Glucose Acidic -Evaporation Section – Liquid Glucose

Enzymatic -Evaporation Section – Maltose Dextrin 3) NV Distilleries Ltd, Ambala-

100 KLPD Absolute Alcohol Plant – -Alcohol Section.

-Thin Slop Evaporation section. -Thin slop Dryer Section.

INTECH ENERGY PVT LTD.PUNE- June 05- Dec 06

Designation: Department:

Process designing Engineer Design and Engineering Process Designing & Development for

BEE-CHT-BEP-1272-22


economical and

Responsibility: efficient production of Biodiesel, By-Product (Glycerin) and Biogas. Optimized the process and set-up a plant for production of bio-diesel and Glycerin purification.

ASIAN PAINT INDIA LTD,- Leading Manufacturer of Paints & By-Products- June 04- Dec 05

Designation: Department:

Responsibility:

Team Leader Process Standardisation, Standardisation of Old & New Products, Handling of worker,

Preparing of MIS, DIMAC and Other Documentation Maintaining 5’S & TPM. Worked on all module of SAP.

ACHIEVEMENTS Design of Hopper for pug mill along with fabrication

Reduced in time cycle of Epoxy resin.

PROJECTS UNDERTAKEN DURING ACADEMICS:

• Project in honor for Degree: Manufacturing of “Bio-Diesel from Karanj Oil” for meeting fast growing demand of diesel with low cost as compare to diesel.

• Project in honor for Diploma: Manufacturing of “Rice Bran Oil” as edible oil from rice bran which is waste product of rice mills which can be utilized for cost saving & replacing groundnut ,sunflower oil,etc as it content very low percentage of cholesterol

BEE-CHT-BEP-1272-22


2. Dr. Ipsita Chakravarty

Postdoctoral Industrial Experience

· Research associate (June 2019 to September 2021) Worked as RA at VNIT, Nagpur in an industry funded project on Design of an anaerobic digester for rice straw under Dr. Sachin A. Mandavgane. Developed a novel technology for on-farm rapid degradation of paddy straw using anaerobic digestion as a solution to the problem of stubble burning in Northern India. This technology has been adopted and implemented for bioconversion of paddy straw into organic manure by Merino Industries Ltd. at Hapur,India

Research Experience

Antibiotic fermentation using different modes of bioreactors.

Production and purification of Bromelain enzyme from pineapple waste

Bioethanol production from microalgae using photo bioreactors

Operational knowledge of bioreactors, spectrophotometer, GC and HPLC

Accomplishments

Received certificate of merit for research at IIT (BHU), Varanasi in 2018

Reviewer in Biofuels journal, Taylor and Francis publications

Received MHRD Institute Scholarship during PhD

Qualified GATE examination 2011.

Received academic Scholarship during B.Tech in 2007 and 2011

Achieved meritorious position in Mathematics Olympiad in 2004

Patents

Patent granted by government of India for microbial consortium developed for rapid degradation of agricultural residues into organic manure:

Dr. Sachin Mandavgane and Dr. Ipsita Chakravarty, Inoculant for rapid biodegradation and method of use, Patent NO. 360956, 2021. Provisional patent filed:

Dr. Sachin A Mandavgane, Dr. Ipsita Chakravarty, Mukesh Bisane, Bioavailable Composition for Plants From Biomass Ash/ Biochar Patent Filed On 29th March 2021 (filed)

List of publications

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Book Editorial Book Chapters · ·

·Review and Research articles SCI Journals

· Co-editor with Dr. Sachin Mandavgane and Dr. Amit Jaiswal in Elsevier book project on Fruit and Vegetable Waste Utilization and Sustainability to be published in July 2022

Kundu, S., Chakravarty, I., Ojha, S., & Kundu, K. (2019). Design and Development of Antibiotic Fermentation Using Different Processing Strategies: Challenges and Perspectives.

In Applied Microbiology and Bioengineering (pp. 163-183). Academic Press.

Chakravarty, I., Kundu, K., & Kundu, S. (2015). Daptomycin: discovery, development and

perspectives. The battle against microbial pathogens: basic science, technological advances

and educational programs, 2, 895-903.

Chakravarty, I., Parmar, V. M., & Mandavgane, S. A. (2021). Current trends in

essential oil (EO) production. Biomass Conversion and Biorefinery, 1-24.

Mishra, A., Chakravarty, I., & Mandavgane, S. (2021). Current trends in non-dairy

based synbiotics. Critical Reviews in Biotechnology, 1-18.

Chakravarty, I., & Mandavgane, S. A. (2021). Valorization of fruit and vegetable waste for biofertilizer and biogas.Journal of Food Process Engineering,44(2),

Chakravarty, I., & Kundu, S. (2019). Oligodynamic boons of daptomycin and noble metal nanoparticles packaged in an anti-MRSA topical gel formulation. Current

pharmaceutical biotechnology, 20(9), 707-718.

Singh, S., Chakravarty, I., Pandey, K. D., & Kundu, S. (2020). Development of a process model for simultaneous saccharification and fermentation (SSF) of algal

starch to third-generation bioethanol. Biofuels, 11(7), 847-855.

Non SCI Journals

· †Chakravarty I, Singh S, Kundu S, Effect of Bubble Characteristics on Mass Transfer Coefficient in an Internal Loop Airlift Bioreactor for Microbial Production of Daptomycin- Published in Vol. 2, Issue 3; 2018 International Journal of Research in Science & Engg (IJRISE) (CHEMCON 2018 Conference Paper)

· †Singh S, Chakravarty I, , Kundu S, Growth Characteristics of Isolated Microalgae Cultured in Internal Loop and External Loop Airlift Photo-bioreactors- Published in

BEE-CHT-BEP-1272-22


Vol. 2, Issue 3; 2018 International Journal of Research in Science & Engg (IJRISE) (CHEMCON 2018 Conference Paper)

· †Subir Kundu, Sukhendra Singh, Ipsita Chakravarty and Kanika Kundu, Alternative Biofuels for Sustainable Development and Environmental Control, DOI: 10.5176/2251- 189X_SEES18.55-SEES CONFERENCE 2018.

· †Shukla P, Chakravarty I, , Kundu S, Development of topical gel formulation using noble metal nanoparticles and Daptomycin against burn specific drug-resistant pathogen - Published in Vol. 2, Issue 3; 2018 International Journal of Research in Science & Engg (IJRISE) (CHEMCON 2018 Conference Paper)

· †Gunda Rohith, Ipsita Chakravarty and Subir Kundu Mycosynthesis of Gold Nanoparticles from Gold Salt using Aspergillus niger International Journal of Biotechnology and Biomedical Sciences p-ISSN 2454-4582, e-ISSN 2454-7808, Volume 2, Issue 3; July- December, 2016 pp. 207-210

· †Indrajeet, Sumedha Ojha, Sukhendra Singh, Ipsita Chakravarty and Subir Kundu Extraction and Purification of Bromelain from Pineapple Fruit Pulp and Peel and Comparative Study of

Chakravarty, I., Narasimha, P., Singh, S., Kundu, K., Singh, P., & Kundu, S. (2018). Synergistic oligodynamic effect of mycogenic bimetallic nanoparticles with

daptomycin for controlling pathogens. Int. J. Pharm. Sci. Res, 9(5), 1788-1796.

Chakravarty, I., Singh, S., & Kundu, S. (2017). Rheological Characterization of Streptomyces roseosporus for the Production of Daptomycin.Chemical and

Biochemical Engineering Quarterly, 31(3), 225-231.

Singh, S., Chakravarty, I., & Kundu, S. (2017). Mathematical modelling of bioethanol production from algal starch hydrolysate by Saccharomyces cerevisiae. Cellular and

Molecular Biology, 63(6), 83-87.

Chakravarty, I., Singh, S., & Kundu, S. (2017). Development of the processing

strategies for the production of daptomycin by free and immobilized cells of

Streptomyces roseosporus using non-conventional support matrices. International

Journal of Pharmaceutical Sciences and Research, 8(3), 1356.

Chakravarty, I., & Kundu, S. (2016). Improved production of Daptomycin in an airlift

bioreactor by morphologically modified and immobilized cells of Streptomyces

BEE-CHT-BEP-1272-22


roseosporus. AMB Express, 6(1), 1-8.

Chakravarty, I., J Pradeepam, R., Kundu, K., K Singh, P., & Kundu, S. (2015).

Mycofabrication of gold nanoparticles and evaluation of their antioxidant

activities. Current pharmaceutical biotechnology, 16(8), 747-755.

Chakravarty, I., Kundu, K., Ojha, S., & Kund, S. (2017). Development of Various Processing Strategies for New Generation Antibiotics Using Different Modes of Bioreactors. JSM

Biotechnol Bioeng, 4(1), 1073.

Barua, A., Chakravarty, I., Kundu, K., Singh, S., & Kundu, S. (2015). Sustainable and effectual bio fabrication of gold nanoparticles for screening of milk adulteration. J Nanomater

Mol Nanotechnol, 4(5), 72-79.

Conference Papers

Enzymatic Activities International Journal of Basic and Applied Biology p-ISSN: 2394-5820, e-ISSN: 2349-2539, Volume 4, Issue 1; January-March, 2017, pp. 4-7

3. Divyajyoti Biswal PhD (pursuing), Chemical Engineering Department of Chemical Engineering Visvesvaraya National Institute of Technology, Nagpur Projects:

PhD Thesis- Design and Implementation of Biomass Waste Based Biorefinery for Production of Enzyme Concoction for Pretreatment Applications To design and create environmentally and economically sustainable biorefinery process for utilization of waste biomass, isolating enzymatic cocktails via fermentative process for pretreatment purpose

M. Tech project: Valorization of Potato Waste (by Fermentation Route) Using Biorefinery Approach and Sustainability Reporting of Process Industries To

identify and extract commercially valuable compounds from industrial potato wastes using the conceptual framework of biorefinery, with emphasis on fermentation and

anaerobic digestion & sustainability reporting of process industries

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2. COMMERCIAL QUALIFICATION CRITERIA

We are working on rice straw to Ethanol considering our geographical location which has surrounding with rice production district like Bandra, Gondia, Gadchiroli & Chandrapur. We are doing continuous experimentation for converting bio mass to ethnoal following are the data we have compile till now. Table 1. Composition of original rice straw

Parameters Composition (%) Carbon 40 Nitrogen 0.76 C/N 52.63 Silica 14 Lignin 18.4 Cellulose 45.11 Hemicellulose 29.8

Table 2. Carbon to Nitrogen ratio

Table 3.Lignin, cellulose and hemicellulose content Lignocellulosic content The results for lignin, cellulose and hemicellulose degradation were considerably good. The bioculture improved digestibility. 65.6% reduction was seen in cellulose and 62.5% reduction was observed in case of hemicellulose component of paddy straw. The comparative experimental studies will be repeated for better understanding.

Sample Carbon Nitrogen C:N

Original Rice straw 40 0.76 52.63

Sample 1 20 1.85 10.8

Sample 2 20.5 1.8 11.4

Sample 3 21.2 1.87 11.3

Sample 4 22.8 2.04 11.17

Sample 5 20 1.81 11

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Sample Lignin Cellulose Hemi-cellulose Original Rice Straw 18.4 45.11 29.8 Sample 1 7.36(60% reduction

from original) 15.5(65.6% reduction from original)

11.18(62.5% reduction from original)

Sample 2 7.0 (62% reduction from original)

13.5 (70% reduction from original)


Sample 3 7.35(60% reduction from original)



Degradation efficiency of lignocellulosic content.

Figure 3. Degradation of lignocellulosic content

The cellulose, hemicellulose and lignin content were analysed with respect to time. It was seen that in 24 hours, 60-70% of the degradation occurs. Table 4. Comparison

0

0.5

1

1.5

2

2.5

3

3.5

4

4.5

0 5 10 15 20 25 30 35 40 45 50Time (Hours)

Cellulose(g)

Hemicellulose(g)

Lignin(g)

No. of Days Sample Lignin Cellulose Hemi-cellulose 0 Original Rice

Straw 18.4 45.11 29.8

1 Paddy straw treated

7.36(60% reduction from original)



2 Paddy straw treated r




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Table 5. Maturity analysis of Rice Straw Batch no./Date N as N03/Total N N-NO3 / N-

NH4+ Remark/Maturity

B01/17-01-2022 0.9 8 Mature 0.84 9.1 Mature 0.9 7.8 Mature

B-02/20-01-2022/ 0.82 7.4 Mature 0.88 8.8 Mature 0.92 8.4 Mature

0.78 9 Mature 0.8 8.6 Mature B-03/23-01-2022 0.87 8.4 Mature 0.9 9.2 Mature 0.95 8.7 Mature B-04/02-02-2022 0.8 9.5 Mature 0.82 9.4 Mature

0.89 9.2 Mature

B-05/11-02-2022 B-06/17-02-2022 0.84 9.6 Mature B-07/22-02-2022 0.93 8.5 Mature B-08/27-02-2022 0.8 9.2 Mature B-09/01-03-2022 0.76 9 Mature B-10/07-03-2022 0.9 8.6 Mature B-11/14-03-2022 0.95 8.7 Mature B-12/29-03-2022 0.8 9.5 Mature

Table 6. pH and EC content of compost Citric acid Concentration

No. of days incubation

Ratio Initial pH

Final pH

Initial EC

Final EC

2500ppm 1 1:1 9.7 9.2 3.6 2.3 1:1 8.7 2.5 1:0.7 9.3 2.7 1: 0.7 9.4 2.7

No. of Days Sample Carbon Nitrogen C/N ratio 0 Original Rice

Straw 40 0.76 52.63


20.5 1.8 11.4


30.8 1.39 22.10

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1: 0.5 9.48 2.75 1: 0.5 9.4 2.8

2500 ppm 2 1:1 9.7 8.87 3.6 2.16 1:1 8.72 2.13 1:0.7 9.17 2.66 1: 0.7 8.93 2.7 1: 0.5 9.14 2.71 1: 0.5 9.13 2.78

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3.DETAIL PROJECT PROPOSAL

SECTION 3.1:

PROJECT BLOCK DIAGRAM

CO2Exhaust

WetCake

RawMaterial

Handling/Pre-cleaning/Storage

Crushing

Pre-Treatment

Fermentation

Distillation

Decantation

Evaporation

Cake

WaterTreatmentplant&CPU

Utilities,Cooling

Tower,IAC

Boiler

Turbine,PCC,MCC

Laboratory

FireFrighteningDevices

ProductStorage

Yeast

Chemicals&Enzymes

Syrup

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SECTION 3.2

PROPOSED BASIS OF DESIGN Sr. No. Parameters Description

1. Proposed plant capacity 5300 LPD of Total Spirit

2. Ethanol 5000 LPD 99.7 % v/v Anhydrous Ethanol

3. Impure Spirit 300 lit per day Technical Alcohol

4. Feed Stock Required 20-22 TPD Bagasse/ Rice straw

5. Efficiency Fermentation Efficiency : 90 - 91 % Distillation Efficiency : 98.5 % Dehydration Efficiency : 99.5 %

6. Yield 220-250 liters of 95.0 % v/v alcohol per ton Bagasse/ Rice straw

7. % Alcohol Alcohol in Fermented Mash : 6- 8 .0 % v/v (minimum)

8. Steam Dry, saturated steam at 3.5 kg/cm2 (g.)

9. Electricity 330 KWH 415 Volts, AC, 50 Hz, 3 Phase

10. Water 100 M3/Day Process / Soft / DM water : after suitable treatment.

11. Effluent Treatment Decantation + CPU + Dryer

12. Storage Open /Covered Yard

13 Handling Automated

14 Size Reduction Vertical Hammer Mill

15 Crushed RM Handling Automated

16 Pre treatment Section -1 Screw type

17 Pre treatment Section-2 SS 304 Reactor. Automated

18 Fermentation 6 Fermenter + 1 Beer well System

19 Distillation Multi Pressure,

13. Decantation Screen type

14. CPU As per Standard practice depending on the COD &

BOD

15. ETP As per Standard practice depending on the COD &

BOD

16. Dryer Flash dryer

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SECTION 3.3:

PROCESS DESCRIPTION

Distillery operation will be consisting of the following Sections:

1. Receiving, precleaning, handling, milling

2. Premashing and Liquefaction

3. Saccharification and Fermentation

4. Distillation to produce Fuel grade Ethanol

5. Decantation to remove suspended solids in effluent

6. CPU Plant

7. Alcohol Storage

8. Water Treatment Plant and Condensate Polishing Unit

9. Boiler and Turbine

10. Electricals and Instrumentation

1. Receiving, Precleaning, Handling, Milling

Stored raw material are unloaded into a receiving hopper / pit near precleaning section. It is

conveyed by bucket elevator and fed to a screen.

Pre-cleaned raw material is fed in controlled rate to the crusher. In this unit operation it is

broken down into small particles of required size distribution. It is collected in the Hopper

and then fed to the Slurry Mixing tank at a controlled rate.

2. Fermentation -

The purpose of fermentation is to convert sugars into alcohol. Simultaneously Carbon dioxide

is produced in Stoichiometric proportions and is scrubbed and liquefied for CO2 bottling.

Closed top with sloping bottom Fermenters are employed for fermentation with adequate

external cooling system to maintain optimum fermentation temperatures. Agitators are also

provided to ensure mixing and suspension of substrate in the tank. Anaerobic conditions are

maintained to ensure high reaction rates and CO2.

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All Fermentors will be used for fermentation. Fermented wash will be stored in Beer

Well before being fed to distillation.

Yeast seed material is prepared in pre fermentors with the help of Active Dry Yeast.

Optimum temperature is maintained by circulation of cooling water. The pre-fermentors are

filled with mash and loaded with Active Dry Yeast. The purpose of the aerated pre-

fermentation is to allow time for the yeast cells to multiply and reduce the chances of

contamination in fermentors. When the Pre-Fermentor contents are transferred to the main

fermentors, the concentration of Yeast cells are high enough to substantially reduce the lag

time associated with yeast growth in fermentation.

Saccharifying enzymes are added in the fermentors. These convert the starch into sugars.

This is basically conversion of Dextrin into Dextrose. The purpose of fermentation is to

convert the fermentable substrate into alcohol. To prepare the mash for fermentation, it has

to be diluted with water.

The pH of the mash is adjusted primarily by recycled slops (which also provides for

nutrients) or by the addition of acid. Yeast is available in sufficient quantity to initiate

fermentation rapidly and complete it within 60 hours. This 60 Hrs is the main reaction time

for fermentation. In addition to this approximately 10 Hrs are require to fermentor emptying,

cleaning, filling etc.

At the start of the cycle, the Fermentor is charged with mash and contents of the pre-

Fermentor. Significant heat release takes place during fermentation. This is removed by

forced circulation cooling in external heat exchangers. The recirculating pumps also serve to

empty the fermentors into beer well. After the fermentors are emptied, they are cleaned with

water and caustic solutions and sterilized for the next batch.

CO2 evolved during fermentation carries along with it some entrained alcohol. This CO2 is

taken to a CO2 scrubber where it is washed with water to recover the entrained alcohol. The

scrubbed CO2 can then be taken to CO2 recovery plant.

BEE-CHT-BEP-1272-22


3. Multi Pressure Distillation Plant –

Multi - pressure distillation scheme has eight distillation columns. These columns operate

under different pressure conditions. Energy from column operating under high pressure is

reutilized by column operating under low pressure to conserve energy.

The columns in order of flow are: -

1. Analyser Column

2. Degassifying Column

3. Pre Rectifier Column

4. MSDS 99.7%

Fermented wash is preheated in the Fermented Wash Pre heater and fed at the top of the

Analyser column. Analyser Column is provided with the flash tank and reboiler.

Top vapors of Analyser column containing all the alcohol in the wash are sent to Prerectifier

column. Rest of the fermented wash flows down the Analyser column and is taken out as

spent wash from Analyser column bottom.

Low boiling impurities are concentrated in the Pre-rectifier column. A top draw is taken out

as impure alcohol from the top of the Pre-rectifier column. RS draw is taken from the top of

Pre rectifier column, which is sent to Purification column. Dilution water in the ratio of 1:9 is

fed to this column. The Extractive Distillation Column operates on the principle of inversion

of relative volatilities. Low boiling impurities are separated in the extractive distillation

column & bottom is sent to Rectifier cum Exhaust column. The top vapor draw is fed to

Recovery column.

The Rectifier/Exhaust column concentrates the ethanol to 96% v/v. The high-grade spirit is

drawn from the upper trays of the Rectification Column. A small head cut if required is

removed from the overhead stream to withdraw Impurities. Fusel oil build up is avoided in

the Rectifier cum exhaust column by withdrawing out side streams (fusel oils). These are sent

to the Recovery column.

In the Recovery column these fusel oils are concentrated and then sent to decanter where

these streams are diluted with water and fusel oil rich layer is separated. A Technical Alcohol

cut is taken out.

BEE-CHT-BEP-1272-22


The High spirit Draw from the Rectifier column is sent to the Simmering column where

methanol is separated in the form of a cut from the top and ENA is taken out from the

bottom. The High Grade spirit (ENA) drawn from the Simmering Column is taken to the

receiver after cooling in ENA cooler.

4. Decantation Section -

Spent wash/Thick Slops from Mash Column is pumped to Thick Slops Tank. Thick Slops is

then fed to Decanter Centrifuge through Decanter Feed Pump. In Decanter suspended solids

from Thick Slop are separated and removed as Wet Cake while Thin Slops is collected in

Thin Slops Tank. Some quantity of this thin slop from decantation is recycled back to the

liquefaction for premashing and slurry preparation. Remaining quantity is fed to Evaporation

plant.

5. Thin Slop Concentration Plant -

Thin slop evaporation plant will be designed to concentrate thin slop coming out of

decantation unit from 5% to 30% w/w solid concentration. This evaporation plant will be

multi effect evaporation with combination of falling film and forced circulation evaporators.

6. Alcohol Storage –

Product streams from the various sections are initially collected in respective daily receivers

and then transferred to bulk storage tanks. Separate vent condenser shall be provided for each

bulk storage tank.

7. Water Treatment Plant and Condensate Polishing Unit -

A State of art, modern water treatment plant shall be provided to generate lowest possible

rejects during production of process water, soft water and DM water meeting standards of the

process.

The spent lees, process condensate and washings generated during distillation, evaporation

and other biochemical reactions will be taken to a condensate polishing unit. The treatment

consists of equalization, anaerobic treatment, aerobic treatment, clarification and softening.

Soft water generated in this plant will be recycled to cooling tower basins as make up water.

8. Boiler –

A fluidized bed boiler shall be provided to produce steam and power required for the

distillery plant complex.

9. Electricals & Instrumentation -

BEE-CHT-BEP-1272-22


Electrical system shall comprise of high tension control panels, step down transformers, DG

sets, synchronization panels, main power control centre, individual MCCs for each section,

cabling, earthing, plant lighting, yard lighting etc.

Instrumentation system shall consists of DCS control system along with SCADA operation,

instrumentation cabling, hard wires, hook up of individual sections at main control room,

instrument air compressors and connections.

BEE-CHT-BEP-1272-22


SECTION 3.4

TECHNICAL SPECIFICATION & LIST OF THE EQUIPMENT REQUIRED

BAGASSE SECTION

SR. DESCRIPTION QTY. TECHNICAL DATA M.O.C

1. Bagasse Handling System 1 Capacity – 500 TPD

MS

2. Bagasse Size Reduction 1 + 1 Type : Mechanical MS

3. Bagasse conveyor 1 Type : Trough MS

4. Pump with motor 2+2 Type : Metering SS

5. Piping Lot Process Fluid : MS

6. Valves Ball Valve / Butterfly Valves / Gate / Globe Valves / NRV

Lot Process Fluid : Cast Iron

7. Instrumentation Lot PLC based --

ACID SECTION


1. Acid Treatment Tank 1 Capacity – 20000 Liters

SS 316 L

2. Screw Press Filter 1 + 1 Type : Screw SS 304

3. Bagasse conveyor 1 Type : Trough SS 304

4. Pump with motor 2+2 Type : Metering SS 304

5. Piping Lot Process Fluid : a. Acid b. Steam c. Water

PP MS MS


Lot Process Fluid : a. Fermented Wash b. Steam c. Water

SS Internal Cast Iron Cast Iron

BEE-CHT-BEP-1272-22




DISGETER SECTION


1. Digester with Agitator with Steam nozzle

2 Capacity – 1500 Liters

SS 316 L

2. Screw Press Filter 1 + 1 Type : Screw SS 304

3. Bagasse conveyor 1 Type : Trough SS 304

4. Enzyme Pump with motor 2+2 Type : Metering SS

5. Piping Lot Process Fluid : a. Wash b. Steam c. Water d. Process Air

SS 304 MS MS SS 304


Lot Process Fluid : a. Fermented Wash b. Steam c. Water d. Process Air

SS Internal Cast Iron Cast Iron SS Internal


BEE-CHT-BEP-1272-22


HYDROLYSIS SECTION


1. Reactor (with agitator)

2 Type : Vertical, Cylindrical, Capacity : 250 m3

SS 304

2. Jacket 2 Type : Jacket

MS

3. Recirculation Pumps with Motor

2+2 Type : Centrifugal Wetted Parts CF8

4. Safety system 4 Type : Suitable SS-304

5. Cleaning Nozzle 4 Type : Suitable SS-304

6. Air Filter 1 Type : HEPA Type MS frame

7. Air Blower with Motor 1 + 1 Type : Water Ring CI

8. Sealing Water Recycle System (for Air Blower)

1 1

Tank : Vertical, Cylindrical Pump : Centrifugal

MS CI

9. Water Header 1 As per BEE standards MS

10. Air Header 1 As per BEE standards SS-304

11. Pump with motor 2+2 Type : Metering SS

12. Piping Lot Process Fluid : a. Fermented Wash b. Steam c. Water d. Process Air

SS 304 MS MS SS 304


Lot Process Fluid : a. Fermented Wash b. Steam c. Water d. Process Air

SS Internal Cast Iron Cast Iron SS Internal


BEE-CHT-BEP-1272-22


ENZYME SECTION


1. Fungus Water Tank (with agitator)

1 Type :, Cylindrical, Volume : 100 m3

SS-304

2. Culture Transfer Pump With Motor

1 + 1 Type : Centrifugal SS-316

3. Pre-fermenter Cooler 2 Type : Plate Heat Exchanger (Wide Gap)

SS-316 Plate, EPDM Gasket

4. Enzyme (with agitator)

2 Type : Vertical, Cylindrical, Capacity : 100 m3

SS 304

5. Fermented Wash Cooler 3 Type : Plate Heat Exchanger (Wide Gap)

SS-316 Plate, EPDM Gasket

6. Fermented Wash Recirculation Pumps with Motor

4 Type : Centrifugal Wetted Parts CF8M

7. Safety system 2 Type : Suitable SS-304

8. Cleaning Nozzle 2 Type : Suitable SS-304

9. Air Filter 1 Type : HEPA Type MS frame

10. Air Blower with Motor 1 + 1 Type : Water Ring CI

11. Sealing Water Recycle System (for Air Blower)

1 1 1

Tank : Vertical, Cylindrical Pump : Centrifugal Cooler : PHE

MS CI SS plates

12. Water Header 1 As per BEE standards MS

13. Air Header 1 As per BEE standards SS-304

14. Enzyme Tank 2 Type : Vertical, Cylindrical HDPE / PP

15. Enzyme Pump with motor 2+2 Type : Metering SS

BEE-CHT-BEP-1272-22



16. Piping Lot Process Fluid : a. Fermented Wash b. Steam c. Water d. Process Air e. CO2 f. Nutrient

SS 304 MS MS SS 304 SS 304 SS 304


Lot Process Fluid : a. Fermented Wash b. Steam c. Water d. Process Air e. CO2 f. Nutrient

SS Internal Cast Iron Cast Iron SS Internal SS Internal SS Internal


BEE-CHT-BEP-1272-22


FERMENTATION SECTION

No. Description Qty Technical Data M.O.C

1. Pre-fermenter 1 Type : Vertical, Cylindrical Capacity : 70 m3

SS 304

2. Agitator for Pre-fermenter 1 Type : Propeller SS 304

3. Pre-fermenter Transfer Pumps

1 + 1 Type : Centrifugal SS 316

4. Pre-fermenter Coolers 1 Type : Wide gap PHE SS 316 Plate, EPDM Gasket

5. Fermenters 2 Type : Vertical, Cylindrical Capacity : 100 m3

SS 304

6. Agitators for Fermenters 2 Type : Propeller SS 304

7. Fermented Wash Coolers 2 Type : Wide gap PHE SS 316 Plate, EPDM Gasket

8. Fermented Wash Recirculation Pumps

4 + 1 Type : Centrifugal SS 316

9. Safety system 4 Type : Suitable SS 304

10. Buffer Tank 1 Type : Vertical, Cylindrical Capacity : 50 m3

SS 304

11. Agitator for Buffer Tank 1 Type : Propeller SS 304

12. Mash Feed Pump 1 + 1 Type : Centrifugal SS 316

13. Air Filter 1 Type : HEPA Type C.S.

14. Air Blowers 1 + 1 Type : Water Ring SS Internals

15. CO2 Scrubber 1 Type : Sieve Tray SS 304

16. Antifoam tank 1 Type : Vertical, Cylindrical SS 304

17. Antifoam tank pump 1 Type : Geared SS 304

18. Acid Tank 1 Type: Vertical, Cylindrical M.S. with lining

19. Acid Pump 1 + 1 Type: Centrifugal Alloy 20

BEE-CHT-BEP-1272-22


No. Description Qty Technical Data M.O.C

20. Nutrient Tank 1 Type: Vertical, Cylindrical SS 304

21. Nutrient Dosing Pump 1 + 1 Type: Metering Internal SS

22. CIP Tank * 1 Type: Vertical, Cylindrical SS 304

23. CIP Pump * 1 + 1 Type : Centrifugal Internal SS

24. Piping Lot Process Fluid - a. Fermented Mash b. Steam c. Water d. Process Air e. CO2 f. Nutrient g. TRO

SS 304 MS MS MS SS 304 SS 304 SS 304

25. Valves Ball Valve / Butterfly Valves

Lot Process Fluid - a. Fermented Mash b. Steam c. Water d. Process Air e. CO2 f. Nutrient g. TRO

SS Internal Cast Iron Cast Iron SS Internal SS Internal SS Internal Cast Iron

26. Piping and Valves Lot ––– –––

27. Electrical Lot MCC and onwards –––

28. Instrumentation Lot PLC based –––

29. Plant Structure Lot ––– MS, painted.

Note :

" * : CIP tank and pumps will be common for Liquefaction, Fermentation, Distillation and Integrated Evaporation section.

BEE-CHT-BEP-1272-22


DISTILLATION COLUMNS SR. EQUIPMENT QTY. TECHNICAL DETAILS MOC

1. Analyser Column

1 Diameter No. of trays Tray Type Tray spacing

: : : :

As Required, 20 Nos., RH Grid, 750 mm

SS 304

2. Rectifier cum Exhaust Column

1 No. of trays Tray Type Tray spacing

: : :

68 Nos. Bubble Cap 250 mm

SS 304

3. Regeneration column

1 No. of trays Tray Type Tray spacing

: : :

30 Nos. Sieve Trays 300 mm

SS 304

REBOILERS Sr. No. Equipment Qty Technical Details MOC

1. Analyser Reboiler 1 Type : Shell & Tube SS 304

2. Rectifier cum Exhaust Reboiler

1 Type : Shell & Tube SS 304

3. Regeneration Reboiler 1 Type : Shell & Tube SS 304

CONDENSERS & COOLERS Sr. No. Equipment Qty Technical Details MOC

1. Analyser Column Condenser – I


2. Analyser Column Condenser – II


3. Rectifier vent Condenser 1 Type : Shell & Tube SS 304

4. Rectifier PCV Condenser 1 Type : Shell & Tube SS 304

BEE-CHT-BEP-1272-22


Sr. No.

Equipment Qty Technical Details MOC

5. Recovery condenser 1 Type : Shell & Tube SS 304

6. Regeneration condenser 1 Type : Shell & Tube SS 304

7. Product condenser 1 Type : Shell & Tube SS 304

8. Product cooler 1 Type : Shell & Tube / PHE SS 304

9. Regeneration cooler 1 Type : Shell & Tube / PHE SS 304

10. Regeneration sub-cooler 1 Type : Shell & Tube / PHE SS 304

11. Fusel oil cooler 1 Type : Shell & Tube SS 304

TANKS AND OTHER EQUIPMENTS

Sr. No. Equipment Qty Technical Details MOC

1. Molecular sieve drums 2 Type : Vertical, Cylindrical SS 304

2. Alcohol scrubber 1 Type : Sieve tray type SS 304

3. Analyser condensate collection tank

1 Type : Vertical, Cylindrical SS 304

4. Rectifier reflux tank 1 Type : Vertical, Cylindrical SS 304

5. RS feed tank 1 Type : Vertical, Cylindrical SS 304

6. Regeneration tank 1 Type : Vertical, Cylindrical SS 304

7. Product receiver 1 Type : Vertical, Cylindrical SS 304

8. Sealing liquid tank 1 Type : Vertical, Cylindrical SS 304

9. Steam condensate collection tank

1 Type : Vertical, Cylindrical MS

BEE-CHT-BEP-1272-22


Sr. No.


10. Fusel Oil Separator 1 Type : Decanter SS 304

BOUGHT-OUT EQUIPMENTS

Sr. No. Equipment Qty Technical Details MOC

1. Fermented wash pre-heater

1+1 Type : PHE Plate : SS 316, Gasket : EPDM,

Frame : MS 2. Rectifier feed pre-

heater 1 Type : PHE Plate : SS 316,

Gasket : EPDM, Frame : MS

3. Analyser condensate pump

1 + 1 Type : Centrifugal Type Internals SS 316

4. Analyser bottom transfer pump


5. Rectifier reflux pump 1 + 1 Type : Centrifugal Type Internals SS 316

6. Rectifier spent lees transfer pump


7. RS feed pump 1 + 1 Type : Centrifugal Type Internals SS 316

8. Weak alcohol recirculation pump


9. Product transfer pump 1 + 1 Type : Centrifugal Type Internals SS 316

10. Steam condensate pump


11. Vacuum Pump (Distillation)

1 + 1 Type : Water Ring Type SS Internals

12. Vacuum Pump (Dehydration)

1 + 1 Type : Water Ring Type SS Internals

BEE-CHT-BEP-1272-22


Sr. No.


13. PIPING Lot Fluid : a. Ferm. Wash b. Slops c. Spent Lees d. Alcohol e. Steam f. Water g. Instru. Air h. Fusel Oil

SS 304 SS 304 SS 304 SS 304 / MS B MS C Class MS B Class GI SS 304

14. VALVES (Butterfly / Ball / Globe / Gate Valves)

Lot Fluid : a. Ferm. Wash b. Spent Wash c. Spent Lees d. Alcohol e. Steam f. Water g. Instru. Air h. Fusel Oil

MOC SS internal SS internal SS internal SS internal CI / CS CI / CS SS internal SS internal

15. PLC 1 Set

It will consist of marshalling cabinets, two work stations; printer and voltage safety stabilisers, memory backup and UPS battery backup. The Plant will be monitored using the PLC system. Also a few important data from utilities will also be drawn and displayed on the PLC. Redundancy factor for I/O will be provided adequately.

16. Instrumentation

Lot PLC based –––

17. Electrical

Lot MCC panel and onwards –––

BEE-CHT-BEP-1272-22


UTILITIES :

Sr. Description Specifications

1. Cooling Tower for Fermentation

Type Inlet temp. Outlet temp. Design WBT Quantity

: : : : :

Cross Flow Type, Induced Draft 34 deg C 32 deg C 28 deg C 1 No.

2. Cooling Water Circulation Pump (Fermentation)

Type Material Quantity

: : :

Centrifugal Type CI / CS 2 + 1 No.

3. Cooling Tower for Distillation & Integrated Evaporation

Type Inlet temp. Outlet temp. Design WBT Quantity

: : : : :

Cross Flow Type, Induced Draft 40 deg C 32 deg C 28 deg C 1 No.

4. Cooling Water Circulation Pump (Distillation & Integrated Evaporation)


: : :

Centrifugal Type CI / CS 2 + 1 No.

5. Air Compressor Type Op. Pressure Quantity

: : :

Screw Compressor 7.5 kg/cm2 (g.) 1 + 1 No.

6. Air Dryer Capacity Quantity

: :

Suitable 1 No.

7. Air receiver Type Capacity Quantity

: : :

Vertical, Cylindrical 1000 lit 1 No.

8. Piping and Valves.

9. Electrical and Instrumentation.

BEE-CHT-BEP-1272-22


PRODUCT RECEIVING AND BULK STORAGE SECTION :

SR. DESCRIPTION SPECIFICATIONS

1. Daily Receiver Capacity Type Material Quantity

: : : :

5 m3 Vertical, Cylindrical M.S. 3 Nos.

2. Technical Alcohol Daily Receiver Capacity Type Material Quantity

: : : :

5 m3 Vertical, Cylindrical M.S. 3 Nos.

3. Technical Alcohol Bulk Storage Capacity Type Material Quantity

: : : :

50 m3 Vertical, Cylindrical M.S. 1 No.

4. Transfer cum Issue Pump Type Material Quantity

: : :

Centrifugal Type SS 316 1 + 1 Nos.

5. Technical Alcohol Transfer cum Issue Pump


: : :

Centrifugal Type SS 316 1 + 1 Nos.

6. Alcohol Flow Meters Type Quantity

: :

Positive Displacement 1 No.

7. Vent Condenser Type Quantity

: :

Shell & Tube 2 Nos.

8. Piping and Valves. Lot.

9. Electricals and Instrumentation. Lot.

DECANTATION SECTION :

SR. EQUIPMENT QTY. TECHNICAL DETAILS MOC

1. Spent wash Feed Tank 1 Type Capacity

: :

Vertical, Cylindrical 10 m3

SS 304

BEE-CHT-BEP-1272-22


SR. EQUIPMENT QTY. TECHNICAL DETAILS MOC

2. Agitator for Spent wash Feed Tank

1 Type : Propeller SS 304

3. Spent wash Feed Pump 1 + 1 Type : Centrifugal SS 316

4. Centrifugal Decanters 1 + 1 Type : Centrifugal Separators

SS 304

5. Thin Slop Tank 1 Type Capacity

: :

Vertical, Cylindrical 10 m3

SS 304

6. Thin Slop Transfer Pump

1 Type : Centrifugal SS 316

7. Piping and Valves Lot ––– –––

8. Electrical Lot MCC and onwards –––

9. Instrumentation Lot PLC based –––

BEE-CHT-BEP-1272-22


DRYER SECTION 1. Spin Flash dryer. 2. Parameters:

a) Name of product : Lignin b) Colour of product : brownish c) Moisture of product : Less than 10 % d) Temp of product : 40 deg C to 45 deg C e) Final vapour Temp :From Dryer 75 deg C(Dry Bulb)

Steam Pressure: 1. 5 Kg/cm2 (g), 125 to 127 deg C (Minimum) 3.A) Tube Bundle a. Tube Plate :Carbon Steel Q345R. b. Head :Carbon steel Q245R. c.Heating Tube :SS304 ,Seamless, Dia -51 mm. d.Main Shaft :Carbon steel 20#, III grade forging. Centre shaft – Carbon Steel /Stainless steel. e. Angle hold bar: drawn steel. f. Shovels : SS316 L, ply ( with SS bolt +Washer +locking Nut). g. Rest : Carbon steel Q235A. B) Housing Parts a. Shell : SS316L. b. End Plates : Material Carbon Steel Q235B, liner SS316, Thickness : 3 mm . c. Vapour Hood : SS316 L. d. Inspection Doors : SS316L. e.Discharge Hopper : SS316L. f. Insulation with aluminium silicates (Thickness: 50 mm, density: 140 Kg/m3), Covers SS304 : Thickness 1 mm . g Dryer base : Carbon steel /Channel Beam . C) Driving system a .Gear box : b.Fluid Coupling c. Gear Wheel : d.Bearing Housing D) Other Parts

BEE-CHT-BEP-1272-22


a. Rotary Joints b.Flexible Hoses Notes : SS tubes to be expanded /full welded with CS Tube sheet.

1. Each dryer have 2 rupture disc for safety. 2. Final product temp before cooler – 95 to 100 deg C. 3. All Internal nut/bolt of 2 Cr 17 Ni materials. 4. Each dryer to have 4 manholes on dish end, maximum size 350 x 450 mm for

maintance & inspection doors on top housing, Size 800 x 650 mm. 5. Housing SS316L, 6. Along with each dryer gear box with coupling , Gear Wheel , Pinion , Insulation ,

Vapour hood , inspection doors , discharge hopper , rotary joints , flexible hoses , Bearing housing etc.

7. Final vapour temperature from dryer -85 – 90 deg C (Dry bulb).

Other equipment Details

Sr. No.

DESCRIPTION

Qty

Technical Specification

MOC

1 Wet Cake Conveyor

1

Type: Screw conveyors

SS304/MS

2 Feeding conveyors

1


SS304/MS

3 Discharge Conveyors

1


SS304/MS

4 Recycle conveyors

1


SS304/MS

5 High Speed Mixer

1


SS304/MS

6 Dryer Vapour Cyclone

1

Type : Tangential Vapour Nozzle Entry,

Shell & cone SS304 Support Bracket – Mild Steel

7 Wet Scrubber 1

Type : vertical /cylindrical Shell & Dishend SS304 Support Bracket – Mild Steel

8 Cyclone - I for Pneumatic Conveying

1 Type : Tangential Vapour Nozzle Entry,

Shell & cone SS304 Support Bracket – Mild steel

BEE-CHT-BEP-1272-22


Sr. No.

DESCRIPTION

Qty

Technical Specification

MOC

9 Cyclone - II for Pneumatic Conveying



10 Cyclone for Air Cooler



11 Product Storage Silo

1

Type : Tangential Vapour Nozzle Entry,


13 Sealing Tank for Wet Scrubber

1 Type: Vertical /cylindrical

Shell & Dish end : SS304 Support Bracket – MS

14 Dryer Vapour Fan along with motor and its accessories.

1

Type ; Centrifugal Drive : Direct coupled Impeller :Radical curved backwards

SS304

15 Air cooler Fan along with motor and its accessories.

1

Type ; Centrifugal Drive : Direct coupled Impeller :Radical curved backwards Fluid : Air Vapours

SS304

16

Fan for pneumatic conveying along with motor and it’s accessories.

1

Type ; Centrifugal Drive : Direct coupled Impeller :Radical curved backwards

SS304

17 Product cooler 1 Type : Horizontal double deck cooler To cool the product DDGS from 95 deg C to 45 deg C Capacity : Suitable

Housing made of carbon steel and all other contact parts and decks of SS304 with 2 mm

18 Chimney 1 Type : Vertical /cylindrical

SS304

19 Vapour liquid ducting`

1 Type : Vertical /cylindrical

SS304

20 Fan for Vapour vent

1 SS304

21) VAPOUR DUCTING

BEE-CHT-BEP-1272-22


On the stationary end cover on the feed, there is an exhaust port, which is to be connected to a centrifugal blower for exhaust the vapours to the atmosphere. Vapours duct and centrifugal blower are in SS304.

22) DRIVE ARRANGEMENT A 4 pole motor rotates the dryer at 8 rpm through a drive train of pulley’s-belts, gearbox, flexible coupling and pinion /girth gear assembly. All drive components are mounted on a common M.S. base frame.

CONDENSATE TREATMENT PLANT DETAILS OF TREATMENT UNITS No. Treatment Unit MOC Mechanical Equipment 1. Mixing Chamber RCC M-25 SS Flash Mixer 2. Equalisation Tank RCC Lined UASB Feed Pumps 3. UASB Reactor RCC M-25 GLSS-MSEP, Feed Distribution 4. Extended Aeration Tank RCC Lined 2 No. Fixed Aerator 5. Secondary Tube Settler RCC M-25 Sludge Recirculation Pumps

6. Sludge Drying Beds (Optional)

Brick Work --

7. Flash mixer RCC-M 25 Agitator 8. Flocculator RCC M-25 Flocculator Mechanism 9. Lamella Clarifier RCC M-25 -- 10. Chlorine Contact Chamber RCC M-25 Chlorine Dosing Assembly 11. Dual Media Filter -- --

12. M C C Room Brick Work / RCC M-20

--

LIST OF EQUIPMENTS

No. ITEMS NOS. SITE / SHOP / BO

1. SS “Mixer in Mixing Chamber 1 No BO 2. Dosing Pump switch Dosing assembly 4 No BO 3. UASB Feed Pumps 2 Nos BO 4. GLSS System for UASB Reactor 1 Lot BO

5. Feed Distribution System for UASB Reactor

1 No BO

6. Flare Stack & Accessories 1 Lot. BO 7. Gas Holder and Accessories 1 Lot BO 8. 15 HP Surface Aerator for Aeration Tank 2 No BO 9. Secondary Clarifier Mechanism 1 No BO

BEE-CHT-BEP-1272-22


No. ITEMS NOS. SITE / SHOP / BO

10. Sludge Recirculation Pumps 2 No. BO 11. Flash Mixer Agitator 1 No BO 12. Clari-flocculator Mechanism 1 No BO 13. Chlorine Dosing Assembly 2 No BO 14. Dual Media Filter Feed Pumps 2 Nos BO 15. Dual Media Filter 1 No BO 16. Activated Carbon Filter 1 No BO 17. High Pressure Pumps 2 No BO 18. Dosing Arrangement 1 No BO 19. Anticipant Arrangement 1 No BO 20. Pressure Gauges 1 Lot BO 21. Interconnecting Piping & Valves 1 Lot BO 22. MCC Panel & Cabling 1 Lot BO

Note :

" List of equipment mentioned is for major equipment. Some of the equipment may not

be mentioned in the proposal but will be supplied so as to achieve the performance

parameters within battery limit.

PLANT STRUCTURE : Mild Steel Structure :

• It includes structural columns, structural beams, structural grating, chequered plate, railing, structural trusses, roofing sheet, etc., as required.

• Indian Standard sections available will be used to fabricate the structure. • Railing : Post and runners will be consisting of MS pipes of 32 NB size and Toe

guard of 60 x 5 mm MS flat. • Roofing sheets will be provided as per local standards and norms.

Colour shade : As per client recommendations • Floor Grating will be Hot Dip Galvanized. (Clamped to the main structure) • Painting Specifications :

Primer : Two coats of Primer, Finish Coat : Two coats Synthetic Enamel Paint, Colour shade : As per client recommendations

BEE-CHT-BEP-1272-22


Sr. Section Details Remark

1. Liquefaction & Fermentation Plant

Structural columns, structural beams, structural grating, railing, structural trusses, roofing sheet, etc., as required. All Tanks, pumps, PHE’s will be supported on civil foundation. Operating floor, piping supports, etc., will be on structure at different levels, as required. Staircase will be provided, as required.

----

2. Distillation & Integrated Evaporation Plant

Structural columns, structural beams, structural grating, railing, structural trusses, roofing sheet, etc., as required. Distillation columns, Evaporators, VLS, etc. will be supported on civil foundation. Condensers, reboilers, piping, etc. will be supported on structure at different levels, as required. Two no. of staircases will be provided.

----

3. Decantation + DDGD Dryer section

Decantation section building will be in civil. Decanters will be supported on civil foundation. Only Structural trusses with roofing sheet will be provided, as required.

----

4. Condensate Treatment Plant

Only Structural trusses with roofing sheet will be provided, as required.

----

5. Pipe-rack Pipe-rack will be provided as per battery limits. ----

Note :

" Equipment layout and distance between sections will be as per Supplier’s standards.

BEE-CHT-BEP-1272-22


BOILER : Sr. No. Particulars Value Unit

1. Capacity 10 tons per hour 2. Pressure 5 kg/cm2 (g.) 3. Temperature 210 oC 4. Primary Fuel --- Bagasse, Coal 5. Type of Boiler --- Fluidized Bed 6. Accessories --- Fuel handling,

Feed bunker, ESP, Chimney, Ash handling

FIRE FIGHTING SYSTEM : Sr. No. Particulars Value Unit

1. Type --- Fire Hydrant Type, Local Fire Extinguishers, Water Sprinklers for Control Room, Offices and Laboratories, etc.

WATER TREATMENT PLANT

INLET WATER QUALITY ( ASSUMED ) Sr. No. Parameters Unit Result

Source Surface Water 1 Colour Hz Colorless 2 Odour Odorless 3 Turbidity NTU <10 (Assumed) 4 pH at 25 0C pH 6.5 to 7.4 5 Conductivity mho 1090 6 Total Dissolved Salts mg/ltr. 800 7 Suspended Solids mg/ltr. <10 (Assumed) 8 Calcium (as CaCO3) mg/ltr. 50 9 Magnesium (as CaCO3) mg/ltr. 50 10 Ph. Alkalinity - (as CaCO3) mg/ltr. Nil 11 M. Alkalinity - (as CaCO3) mg/ltr. 420 12 Sulphate (as SO4) mg/ltr. 16.4 13 Chlorides (as Cl) mg/ltr. 130

BEE-CHT-BEP-1272-22


14 Silica (as SiO2) mg/ltr. 8.7 Colloidal Silica (as SiO2) mg/ltr. NIL

Note :

" Inlet Water Source and Quality is assumed as above. Actual WTP design will be done as per Water Analysis Report ‘to be submitted’ by SAMPL.

BEE-CHT-BEP-1272-22


OUTLET WATER QUALITY:

A) PROCESS WATER

Description Treated Water Parameters

Unit

PH (Before pH Correction) 6.5 to 7.5

Conductivity at 25 oC (Before pH Correction) <1 µs/cm Total Silica as SiO2 (Considering Colloidal Silica NIL in inlet)

<0.02 PPM

B) SOFT WATER

1 DMF M3/hr 1 X 70 Turbidity NTU <5 2 Activated carbon Filter --- 1 No. 3 Softener --- 1 No.

4 Total Hardness (As CaCOЗ) (Considering inlet Hardness <350 PPM Max)

PPM < 5

C) DM WATER

1 DM Plant --- 1 No.

OBR M3 100 2 MB System --- 1 No. OBR M3 520

DM WATER OUTLET QUALITY: No. Parameter Unit Quantity 1 Hardness Ppm ( Max) Nil 2 pH at 25 oC 8.8 - 9.2 3 Oxygen Ppm ( Max) 0.01 4 Total Iron Ppm ( Max) 0.01 5 Total Copper Ppm ( Max) 0.01 6 Silica Ppm ( Max) 0.02 7 Conductivity at 25 oC µs/cm 0.5 8 Hydrazine Residue Ppm ( Max) Nil

BEE-CHT-BEP-1272-22


EQIUPMENT LIST – WTP

Sr. Description Qty. MOC FILTARTION UNIT

1. Raw Water Storage Tank 1 No.

---- 2. Filter Feed Pump 1 No.

---- 3. Dual Media Filter 1 No. MS 4. Air Scouring Blower for DMF

1 No. MS 5. Activated Carbon Filter 1 No.

MS After ACF, water will be go to :

• Fermentation • feed to Softener & • feed to DM Plant

6. Softener 1 No. MS 7. Resin -T42 Na+ 1 Lot 8. Brine Measuring Tank 1 No. HDPE

DM +MB UNIT 9. Strong Acid Cation 1 No. MS with

rubber lining 10. Degasser Tower

1 No. MS with

rubber lining 11. Degasser air blower 1 No. MS

Centrifugal 12. Degassed water Tank 1 No MS with

rubber lining 13. DG Water Transfer Pump 1 No SS 316 14. Strong Base Anion 1 No. MS with

rubber lining 15. Mixed Bed Unit 1 No. MS with

rubber lining 16. Blower for MB 1 No CI 17. Regeneration Tanks for HCL with Fume absorber 2 Nos. HDPE 18. Regeneration Tank for NaOH 2 Nos. HDPE 19. pH Dosing Pump 1 No.

PP 20. pH Dosing Tank 1 No.

HDPE

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Sr. Description Qty. MOC 21. MB Treated Water Tank 1 No.

SS304 22. ICPW within battery limits 1 lot

MSRL / UPVC / MS

23. Local Instrument cum Starter Panel 1 No. MS powder Coated

BEE-CHT-BEP-1272-22


LABORATORY EQUIPMENTS AND GLASSWARE REQUIRED SR. INSTRUMENT TECHNICAL SPECIFICATIONS QTY

. 1. Densitometer Technical Specifications for Densitometer for

ethanol shall be as under: Measuring range: Density: 0 g/cm³ to 3 g/cm³ Temperature: 0 °C to 90 °C (32 °F to 1194 °F) Pressure: 0 – 10 bar (0 - 145 psi) Repeatability, standard deviation: Density: 0.00001 g/cm³

Temperature: 0.01 °C (0.02 °F)

1

2. BOD incubator Technical Specifications for BOD incubator shall be as under: Temperature Range: 50 C to 600 C Temperature Accuracy: ± 0.20 C Complete with: Microprocessor based PID

controller (Auto Tuning Type) with digital display of temperature in 0 C giving accuracy of ± 0.20 C.

1

3. Hand Refractometer Technical Specifications for Hand Refractometer shall be as under: Measuring range: 0-32% Brix. Accuracy: +/-0.20% Brix. Calibration: zero calibration with water at 20°C

2

4. Hot Air Oven Technical Specifications for Hot Air Oven shall be as under: Capacity: 200 litter Heating Capacity: Room temperature to 2500 C.

1

5. Lab Centrifuge Technical Specifications for Lab Centrifuge shall be as under: It shall have digital speed indicator and 0-60 minute digital countdown timer. Salient Features: • Safety Lid interlock to prevent cover opening

during centrifugation • Dynamic brake for quick deceleration • Imbalance detector with cutoff

Max. Capacity: 100 ml X 6

1

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SR.

INSTRUMENT TECHNICAL SPECIFICATIONS QTY.

6. Muffle Furnace Technical specifications for muffle furnace shall be as under: Heating Capacity: Room Temperature to 1200 Deg C.

1

7. Water Purification System

Technical Specifications for Water Purification System shall be as under: Resistivity: Sample shall met the requirement for

ASTM type 1 Water, achieving resistivity above 18.0 Megohm.cm @ 250 C TOC: Sample shall achieve TOC level below the

specification given below after flushing. Burst Test: > 20 bar / > 290 psi. TOC < 10 ppb.

1

8. Laboratory motorized stirrer

Technical Specifications for Laboratory motorized stirrer shall be as under: Stirring Shaft: 10 X 550 (mm) Impeller: Pitched Blade Speed: 100 – 1400 RPM. Stirring Capacity: Max Volume 50 lits. Digital Speed indicator.

1

9. Laboratory hood Technical Specifications for Laboratory hood shall be as under: It shall be consisting of: • 2 utility lines, Air Monitor Device • Extract Air Manifold, Drip Cup • Following Under Bench Units on Pilth • 900 mm 2 Hinged Door 1 drawer • 545 mm 1 Hinged Door

1

10. Desiccator Desiccator with Vacuum 250 mm hg. 2

11. Constant temp. water bath

--- 1

12. Brix Hydrometer 0-10 10-20

3 3

13. Skyes Hydrometer 80-100 3 14. Plane Slides --- Lot

15. Micropipette 1000 microlitter Lot

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SR.


16. Microscope Technical Specifications for Microscope shall be as under: • Halogen illumination with 6V 30 Watt

halogen lamp • 4-position nosepiece, tilted backwards • mechanical stage 75x30, drive right and

specimen • holder with spring clip left • binocular phototube 30°/20 ( 50:50) • eyepieces 10x/20 Bright focus • objectives Plan-Achromat 4x, 10x, 40x and

100x Oil • condenser 0.9/ 1.25 • immersion oil • color filter set blue, green, yellow • Filter adapter • dust cover

2

17. Vortex Mixer Technical Specifications for Vortex Mixer shall be as under: Provision for vortex mixing. Mixing Surface Dimensions Inches (cm): 4.0

(10.1) - Foam pad

1

18. Laminar Air- Flow Unit

Technical Specifications for Laminar Air- Flow Unit shall be as under: • A horizontal laminar flow, HEPA Filtered

(with an efficiency of 99.99% on mono disperse, 0.3 micron challenge) Clean bench for class 100 meeting ISO Class 5.

• CGMP compliant. • The workspace area of 48 inch width and 24

inch depth. • The MOC of structural parts SS 304. • The work bench platform MOC -SS 304. • Work space illumination with min. 200 Lux

white fluorescent light.

1

19. Nichrome wire-Loop

≈ 5 cm long with wooden handle

5

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SR.


20. Petri plate holder Locally Available

2

21. Dispenser with plastic disposable tips

100 ul -1000 ul. 1

22. Neubaur chamber (Hemocytometer)

Counting chamber with two cover glasses.

2

23. Strainer

100 µ 3

24. Sikes Sprite Meter

Make : Zeal-England 2 Set

25. Syring

10-20 microliter Lot

26. Reagent Bottles

100 ml 250 ml 500 ml 1000 ml

16 12 18 18

27. Beakers 25 ml 50 ml 100 ml 250 ml 500 ml 1000 ml 2000 ml

10 10 10 6 6 6 3

28. Burettes with Glass stopcock

10 ml 25 ml 50 ml

6 6 6

29. Erlenmeyer Flasks

100 ml 250 ml 500 ml 1000 ml

12 12 12 6

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SR.


30. Vacuum Flask

----- 6

31. Erlenmeyer Flasks with side arm for Vacuum filtration

500/1000ml

1 each

32. Graduated Measuring Cylinder “A” class

25 ml 50 ml 100 ml 250 ml 500 ml 1000 ml

6 6 6 3 3 1

33. Pipettes “A” class 1 ml 2 ml 5 ml 10 ml

12 12 24 24

34. Hard Glass Test Tube

50 ml 100

35. Flat Bottom Test tube

50 ml 25

36. Pasteur pipette/ dropper

10 ml 20 ml

3 3

37. Pipette Bulb

1 ml 5 ml 10 ml

8 8 8

38. Petri plates

--- 40

39. Funnels

Diameter: 75 mm Diameter: 100mm

10 10

40. Glass Hydrometers

1.000 - 1.100 1.100 - 1.200 1.200 - 1.300

4 4 4

41. Pycknometer / Specific gravity bottle

50 ml

4

42. Glass rod

--- 6

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SR.


43. Spirit Lamps

--- 3

44. Baume’ Spindle and Hydrometer Cylinder

--- 1

45. Glass thermometer 80 -100 OF 6

46. Round Bottom Flask 500 6

47. Pair of tongs (Suitable for holding Erlenmeyer flask, and beakers of all capacities)

2

48. Rubber bulbs for Pipettes 10ml,25ml, 50ml capacity 5 each

49. Test tube stand (Suitable) 4 50. Spatula 12

Nos 51. Stop watch 3 52. Wire gauze with asbestos (For heating purpose of glassware during analysis) 12

53. Forceps 2 54. Sieve (1000 micron & 500 microne) 01 55. Hot plate (for titration and heating of liquids) 03

BEE-CHT-BEP-1272-22


SPECIFICATION AND DETAILS FOR ELECTRICALS

1. MOTOR CONTROL CENTRE (MCC):

MCC’ S will be made from CRCA (Cold Rolled Cold Annealed) sheet metal fabrication.

MCC will be non-drawout type, compartmentalized, non-flame proof type with HRC fuse

system and located at non-flameproof area.

MCC will be fabricated from 14/16-gauge MS CRCA sheet, floor mounted, suitable for

indoor installation, vermin/dust proof, weatherproof with IP42 degree of protection. Cable

entry shall be from the bottom as a standard feature. Top cable entry may be provided, if

required.

Each starter of MCC will consist of:

- SFU (Switch fuse unit) for compartmentalized MCC

- Contactor

- Overload Relay for compartmentalized MCC

- ON / Trip indication

- Emergency stop stay – put push button

Motor rating including and above 18.5 KW, Star Delta starter will be provided. For motor

rating including and above 18.5 KW, Current Transformer will be provided in Y – phase with

ammeter to read the current.

Incomer of MCC will be:

- MCCB (Molded Case Circuit breaker) for rating upto and including 800 Amp.

- ACB (Air Circuit breaker) for rating above 800 Amp.

BEE-CHT-BEP-1272-22


2. INTERNAL POWER WIRING

All the power wiring will be carried out by using copper cable. Cable sizes will be as

follows:

Motor rating Cable size

For DOL Starter Upto 5.5 KW 2.5 mm2

Upto 7.5 KW 4.0 mm2

Upto 9.3 KW 4.0 mm2

Upto 11.0 KW 6.0 mm2

Upto 15.0 KW 10.0 mm2

Upto 18.5 KW 10.0 mm2

Motor rating Cable size

(Supply side)

Cable size

(motor side)

For Star - Delta Starter Upto 18.5 KW 10.0 mm2 4.0 mm2

Upto 22 KW 16.0 mm2 6.0 mm2

Upto 30 KW 25.0 mm2 10.0 mm2

Upto 45 KW 50.0 mm2 25.0 mm2

3. EARTHING

Earthing would be done using G.I. pipe rods as per IS standards. G.I. conductor earthing will

be done for all electrical equipment. G.I. conductors will be used for lightning protection,

connected directly to separate earth pit.

4. POWER AND CONTROL CABLES

Individual motors will be connected to MCC by 1.1 kV grade, PVC sheathed armored cables.

Cable sizes for respective motor rating will be as follows:

BEE-CHT-BEP-1272-22


Motor upto 1.5 KW 1 No. x 3 core x 2.5 mm2 Copper

Motor above 1.5 kW to5.5 kW 1 No. x 3 core x 4.0 mm2 Copper

Motor above 5.5 KW to11 KW 1 No. x 3 core x 6.0 mm2 Aluminium

Motor 15 KW 1 No. x 3 core x 10.0 mm2 Aluminium

Motor 18.5 KW 2 Nos. x 3 core x 10.0 mm2 Aluminium

Motor above 18.5 KW to 30 KW 2 Nos. x 3core x 16.0mm2 Aluminium

Motor above 30 KW to 45 KW 2 Nos. x 3 core x 25.0 mm2 Aluminium

Motor above 45 KW to 75 KW 2 Nos. x 3 core x 50.0 mm2 Aluminium

Motor 90 KW 2 Nos. x 3 core x 70.0 mm2 Aluminium

Motor 110 KW 2 Nos x 3 core x 95.0 mm2 Aluminium

Control cable for push button

station

1 No . x 3 core x 1.5 mm2 Copper

5. PUSH BUTTON STATION

Push button station will be provided near the motor wherever required with lock and key

system. Flameproof push button station (as per IS 2148) will be provided for flameproof

section and non-flameproof push button station (as per IS 2147) will be provided for non-

flameproof section.

6. CABLE TRAYS

MS powder coated cable trays will be provided for indoor application. Cables will be buried

in trenches for outdoor cables.

7. ERECTION MATERIAL

Double compression glands will be provided in field side of cables & single compression

glands will be provided in the panel side of cables.

BEE-CHT-BEP-1272-22


SECTION 3.5

INPUT REQUIREMENT

Sr. Input Requirement

1. Raw Material Bagasse/ Rice straw

2. Process Water For Pretreatment and Fermentation

- 100-110 m3/day (max.) (without recycle)

3. Cooling Water Recirculation For Pretreatment & Distillation

- m3/hr with ∆T= 60C

For Fermentation


For Evaporation


Soft Water : (Cooling Tower make-up water)

DM / Soft Water For Dilution in Distillation

- m3/day (without spent lees recycle)

- m3/day (with spent lees recycle)

For sealing, decanters, vacuum pump etc.

- m3/day

Evaporation Design

Capacity

As required

4. Steam For Pretreatment

- 1 kg/litre @10 kg/cm2

For Fermentation

- Sterilization only

For Distillation & Integrated Evaporation

- 3.2 kg/litre @3.5 kg/cm2

For Dryer

- 1.5 kg/litre @3.5 kg/cm2

BEE-CHT-BEP-1272-22


Sr.

No.

Input Requirement

8. Sodium Hydroxide As required

9. Sulphuric Acid As required

10. Antifoam Agent As required

11. Liquozyme DS (240 KNU) As required

12. Shearzymne W As required

13. Spirizyme Plus (750 AGU) As required

14. Alkalase 2.5 L As required

15. Active Dry Yeast (95%) As required

16. CIP Chemicals As required

17.

Estimated Power Requirement

Sr. No.

Plant Section Operating KW

1. Fermentation 2. Distillation 3. Decantation & Mixer 4. CPU 5. ETP 6. Utilities 7. Alcohol Storage Total Approx. 400 to 500

SPECIFICATIONS OF RAW MATERIALS CONSIDERED

1. Bagasse /Rice Straw: Moisture : < 12 % Cellulose content : 60 – 67 % w/w Protein : 9 – 12 % Fat & Oil : 2 – 3 % Fiber & NSP : 22 – 24 % (NSP - Non Starch Polysaccharides) TVC : 1000 cfu/gm

2. PROCESS WATER / SEALING / CLEANING / TESTING WATER Process water should be filtered and shall not contain any E. COLI or COLIFORM

bacteria with total germs count being limited to 60 Nos/ml. The chloride content shall be less than 25 ppm.

3. COOLING WATER FOR CIRCULATION

BEE-CHT-BEP-1272-22


Cooling water at a temperature of 32 Deg. C max. with a total hardness of 5 ppm maximum & Total Dissolved solids of 25 ppm max.

4. SULPHURIC ACID Concentrated, Commercial Grade, Composition as below value in % W/W (a) Sulphuric Acid : 98 MIN (b) Lead : 0.001 MAX (d) Iron : 0.03 MAX (c) Arsenic : 0.0001 MAX (e) Moisture : 2 MAX 5. UREA : Standard Commercial Grade 6. DIAMMONIUM PHOSPHATE (D A P) : Standard Commercial Grade 7. NaOH : Commercial grade. 8. STEAM FOR DISTILLATION / COOKING / DRYING : Dry, saturated should be provided at the inlet of steam header and the pressure

required shall be 3.5 kg/cm2 (g.) at the steam header. The maximum variation in the steam pressure shall not be more than +/– 0.1 kg/cm2.

10. ENZYMES : As per recommendation by the Seller.

Notes:

• The electrical loads are estimated and need to be confirmed from vendors, after details

engineering. They may vary according to equipment specifications and lay out.

• Consumption of chemicals depends upon the type of raw material used.

• Constant availability of inputs like feed and utilities at desired specifications are

essential for the consistent performance for the process plant.

BEE-CHT-BEP-1272-22


SECTION 3.6 :

OUTPUT GENERATION STREAMS

1. Product 5000 lit per day @ 99.7% v/v ethanol content

2. Impure Spirit 2,500 lit per day Technical Alcohol

3. CO2 Gas About 2.5 TPD

4. Steam Condensate About 10 TPH

5. Lees 50 TPD . . . (without recycle)

6. Dryer About 20-22 TPD @ 90 % w/w solids content

SECTION 3.7: PRODUCT SPECIFICATIONS PROJECTED

ANHYDROUS ETHANOL SPECIFICATIONS Sr. No. Component Unit Value

1. Strength @ 20 oC % v/v 99.80% 2. Apperant Density Kg/cm3 788.19 – 798.78 3. Water Content % w/w 0.5 4. Identification A Passes Test 5. Identification B Passes Test 6. Acidity ml 0.08 ml of 0.1 M NaOH 7. Alkanility Nil 8. Aldehyde PPM 10 9. Benzene PPM 2 Maximum 10. Volatile Impurities Passes Test 11. Non-volatile matter PPM 50 12. Copper PPM Nil 13. Dry extract PPM Negligible 14. Specific gravity @ 20 oC / 20 oC 0.7904 – 0.7920

BEE-CHT-BEP-1272-22


SECTION 3.8

PROJECTED COST OF OPERATION

BEE-CHT-BEP-1272-22


SECTION 3.9

FUNDS REQUIRED

SR. DESCRIPTION AMOUNT (INR in Lacs)

1.

Pretreatment • Bagasse Section • Acid Section • Digester Section & Hydrolysis Section • Enzyme Section

282.00

2. Main Process Sections : • Fermentation Section • Distillation Section • Decantation Section & Dryer section • Condensate Treatment Plant • Piping and Valves for above • MCC panel and onwards electrical for above • PLC based Plant Automation work for above

775.00

3. Alcohol Storage Sections : Alcohol (Product) Receiving & Storage Section

4. Utilities: • Air-compressors, • Cooling Towers, • Cooling water recirculation pumps

5. Erection & Commissioning for above sections

6. Other Miscellaneous: • Water Treatment Plant • Fire fighting system, • Weigh Bridge & Laboratory Setup

7 Plant Structure for above sections as per Technical Annexure

8. Boiler & Turbine with Accessories : • Boiler [Capacity : 30 tons per hr, Fuel : Rice husk / coal ] • Turbine [Capacity : 2.5 MW, ] • DG set and fuel storage • PCC and electrical Synchronisation, distribution work

9. Estimation for Client Scope of Civil Work for above sections Approx. 110.00

1167.00 18% GST 210.00 10. Working Capital 120.00 TOTAL 1497.00

BEE-CHT-BEP-1272-22


4.LAND AVAILIBLITY DOCUMENT

We have already purchased land in Butibori MIDC, Nagpur admeasuring 10800 sq.metres with same directors as this company and we declare that

same will be used for 5000 liter/day 2nd generation plant.

BEE-CHT-BEP-1272-22


BEE-CHT-BEP-1272-22


5. RESULT OF OUR TRIAL

We are able to break down bagasse & rice straw at first stage of pretreatment and we are sure that further trail of hydrolysis will converted

the feed stock to Ethanol. We are getting less yield as of now high conversion achieved is 9% which will yield corresponding approx. 90 liters of ethanol. We have set our target to achieve 220-250 liters from 1 tons of

biomass (bagasse/ Rice Straw)

BEE-CHT-BEP-1272-22


7. SELF DECLARATION

We, Deponent do hereby solemnly state that the deponent is a partnership registered under

the Companies Act having its registered Office in 7/B Ghaisas Layout, Surendra Nagar,

Nagpur 440015 Maharashtra at the aforesaid address.

We are declaring that we will do operation & maintenance of 5000 liters /day 2nd

generation plant produced from bagasse or rice straw.

VERIFICATION Verified that the above contents are true and correct to the best of my

knowledge and belief . Hence verified and signed on this 24 day of May 2022 at Nagpur

FOR BIO-ENERGY ENGINEERING,

Vishal Gohade Cell: +91 9960400959 Email: [email protected]

Demonstration 2 Generation Fuel Ethanol Plant Bio-Energy ...

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