Data Report for the Collection of Small Mammals and ... · hudson river hudson river data report: small mammals and american woodcock collection, analysis of floodplain earthworms,

DATA REPORT FOR THE COLLECTION OFSMALL MAMMALS AND AMERICAN WOODCOCK

FROM THE FLOODPLAIN OF THE HUDSON RIVER,NEW YORK IN YEAR 2001,

ANALYSIS OF FLOODPLAIN EARTHWORMSFROM THE YEAR 2000, AND

RE-ANALYSIS OF SELECT FLOODPLAIN SOILSAND SMALL MAMMALS FROM THE YEAR 2000

HUDSON RIVER NATURAL RESOURCEDAMAGE ASSESSMENT

HUDSON RIVER NATURAL RESOURCE TRUSTEES

STATE OF NEW YORK

U.S. DEPARTMENT OF COMMERCE

U.S. DEPARTMENT OF THE INTERIOR

FINAL

JANUARY 2010

Available from:U.S. Department of CommerceNational Oceanic and Atmospheric AdministrationHudson River NRDA, Lead Administrative TrusteeDamage Assessment Center, N/ORR311305 East-West Highway, Rm 10219Silver Spring, MD 20910-3281

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HUDSON RIVER DATA REPORT: SMALL MAMMALS AND AMERICAN WOODCOCK COLLECTION, ANALYSIS OF

FLOODPLAIN EARTHWORMS, AND RE-ANALYSIS OF SELECT FLOODPLAIN SOILS AND SMALL MAMMALS

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Natural resources of the Hudson River have been contaminated through past and ongoing discharges ofpolychlorinated biphenyls (PCBs). The Hudson River Natural Resource Trustees -- New York State, theU.S. Department of Commerce, and the U.S. Department of the Interior -- are conducting a naturalresource damage assessment (NRDA) to assess and restore those natural resources injured by PCBs.

In 2000, the Trustees conducted a screening-level investigation from Fort Edward to Stillwater, New York,and identified PCB contamination in floodplain soils and in small mammals. The Trustees expanded thisinvestigation in 2001 to refine the areas and species that may be exposed to floodplain PCBs.

Sampling in 2001 focused on small mammals and American woodcock (Scolopax minor). A total of 169small mammal samples from the year 2001, consisting of 61 short-tailed shrews, 94 deer mice and white-footed mice, and 14 voles, as well as two woodcock liver samples, were analyzed for select PCB congeners,PCB homologue groups, total PCBs, and percent lipids.

The Trustees also determined that it was appropriate to re-analyze select shrew and soil samples from 2000pursuant to the methods contained in the Trustees Analytical Quality Assurance Plan, and to analyzearchived earthworm samples from 2000 that had not been analyzed previously. Thus, in addition to thesmall mammal and woodcock liver samples collected in 2001 that were submitted for analysis, the Trusteesalso submitted to the laboratory for re-analysis 18 soil samples and 12 shrew samples from 2000 andsubmitted to the laboratory for analysis 10 earthworm composite samples from 2000.

The total PCB analytical results from this investigation are as follows:• Total PCB concentrations in earthworm samples from 2000 range from 0.03 ppm to 23.9 ppm (wet

weight basis (ww)).• Total PCB concentrations in soil samples from 2000 range from 0.11 ppm to 937 ppm (dry weight

basis).• Total PCB concentrations in shrew samples from 2000 range from 0.19 ppm to 36.7 ppm (ww).• Total PCB concentrations in small mammal samples from 2001 range from 0.02 ppm to 30.4 ppm

(ww).• Total PCB concentrations in woodcock liver samples from 2001 are 0.12 ppm and 0.13 ppm (ww).

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TABLE OF CONTENTS

1.0 INTRODUCTION ............................................................................................................................................... 1

2.0 SAMPLING AND ANALYSIS ............................................................................................................................ 12.1 2001 SAMPLING ...................................................................................................... 1

2.1.1 COLLECTION OF SMALL MAMMAL SAMPLES IN 2001 ...................... 2

2.1.2 COLLECTION OF WOODCOCK SAMPLES IN 2001 .............................. 2

2.1.3 STORAGE OF SMALL MAMMAL AND WOODCOCK SAMPLES

FROM 2001 ................................................................................................... 2

2.1.4 SHIPPING OF SAMPLES ............................................................................ 2

2.2 SAMPLE ANALYSIS ............................................................................................... 2

2.3 QUALITY ASSURANCE/QUALITY CONTROL ............................................... 3

3.0 RESULTS ........................................................................................................................................................... 5

3.1 TOTAL PCB CONCENTRATIONS ...................................................................... 8

3.2 PCB HOMOLOGUES AND CONGENERS........................................................ 10

4.0 REFERENCES ................................................................................................................................................. 13

FIGURES ................................................................................................................................................................ 15

Appendix A: Work Summary for the Collection of Small Mammals and American

Woodcock from the Floodplains of the Hudson River, New York.

Appendix B: Data Quality Assessment Report. Hudson River Natural Resource

Damage Assessment. Floodplain Study. Woodcock Liver Tissue and

Earthworm Tissue.

Appendix C: Data Quality Assessment Report. Hudson River Natural Resource

Damage Assessment. Floodplain Study. 2001 Small Mammals Tissue

and 2000 Shrews and Soils.

Appendix D: Earthworm (2000) and Woodcock Liver (2001) Tissue Data Sheets.

Appendix E: Small Mammal (2001) Tissue Data Sheets:

E1: Short-Tailed Shrew Tissue Data Sheets;

E2: Mouse Tissue Data Sheets; and

E3: Meadow Vole Tissue Data Sheets.

Appendix F: Soil and Shrew (2000) Data Sheets:

F1: 2000 Soil Data Sheets; and

F2: 2000 Short-Tailed Shrew Tissue Data Sheets.

TABLE OF CONTENTS

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1.0 INTRODUCTION1.0 INTRODUCTION1.0 INTRODUCTION1.0 INTRODUCTION1.0 INTRODUCTION

Past and continuing discharges of polychlorinated biphenyls (PCBs) have contaminated the naturalresources of the Hudson River. The Hudson River Natural Resource Trustees (Trustees) -- NewYork State, the U.S. Department of Commerce, and the U.S. Department of the Interior -- areconducting a natural resource damage assessment (NRDA) to assess and restore those naturalresources injured by PCBs (Hudson River Natural Resource Trustees 2002a). In 2000, the Trusteesconducted a screening-level investigation from Fort Edward to Stillwater, New York, and identifiedPCB contamination in floodplain soils and in small mammals. Data collected during that investigationindicate that PCB concentrations in floodplain soils in the 20 miles downstream of Fort Edwardranged from undetected to 360 parts per million (ppm) (SEA Consultants 2002).

The Hudson River floodplain provides habitat for a wide range of wildlife, including amphibians,reptiles, birds, and mammals. These organisms often are important parts of the diet for predatorssuch as mink, eagles, falcons, and owls. If floodplain soils contain PCBs, they may provide a PCBsource for floodplain biota. The floodplain may become contaminated when heavy rains andsnowmelt cause the Hudson River to overtop its banks. These flood waters bring with themcontaminated sediment that has been churned up from the river's bed. Eventually, the flood waterssubside and deposit this material on the floodplain. Typically sediment is deposited in any area wherecurrent flow is reduced in low-lying floodplain areas, by ponding, or by the presence of vegetation.Since these floodplains provide habitat for a number of species, the Trustees are working to betterunderstand to what extent floodplain PCBs should be assessed in the damage assessment.

In 2001 the Trustees expanded their floodplain investigation to refine the areas and species that maybe exposed to floodplain PCBs. This Data Report provides the results of that preliminaryinvestigation of PCB contamination of floodplain biota conducted in the year 2001 and provides theresults of further analyses of floodplain soils, earthworms, and small mammals collected from theHudson River floodplain in the year 2000. The Report documents methods, quality assurance/quality control, and data from an investigation of PCB contamination of floodplain biota conductedpursuant to the NRDA in the year 2001, analysis of earthworm samples collected in 2000, and re-analyses of select floodplain soils and small mammals collected from the Hudson River floodplain inthe year 2000. Based on the results of this preliminary investigation and other available information,the Trustees will determine whether the floodplain should be considered for a more comprehensiveassessment.

2.0 SAMPLING AND ANAL2.0 SAMPLING AND ANAL2.0 SAMPLING AND ANAL2.0 SAMPLING AND ANAL2.0 SAMPLING AND ANALYSISYSISYSISYSISYSIS

2.1 2001 SAMPLING2.1 2001 SAMPLING2.1 2001 SAMPLING2.1 2001 SAMPLING2.1 2001 SAMPLING

The Trustees' "Work Summary for the Collection of Small Mammals and American Woodcock fromthe Floodplains of the Hudson River, New York" (Appendix A) (Hudson River Natural ResourceTrustees 2004a) documents the year 2001 collection and processing of small mammals and Americanwoodcock (Scolopax minor) from the Hudson River floodplain.

Figure 1 shows the floodplain Study Areas from the 2000 and 2001 investigations. Table 1 ofAppendix A provides a list and description of the sample sites used in the 2000 and 2001 floodplaininvestigations, and the types of samples collected from each Study Area.

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2.1.1 COLLECTION OF SMALL MAMMAL SAMPLES IN 2001

Small mammal collection using snap traps began on September 4, 2001, and concluded on October 18,2001. The collection focused on 12 sites from the 2000 investigation and 11 new sites (designated StudyAreas 13 through 23) for 2001. The new sites were located downstream of the sites from the year 2000investigation and extended from the Saratoga Battlefield National Historic Park in Stillwater, New York toPoughkeepsie, New York. Small mammals were collected from 11 of the sites from the 2000 study andfrom 9 of the new sites. Field sampling staff were unable to collect small mammal samples from three ofthe sites (one site from 2000 (Study Area 9) and two sites from 2001 (Study Areas 14 and 19)). Eachsample was placed individually into a chemically clean glass jar. A total of 418 mammals were collectedfrom the Hudson River floodplain study areas in 2001. Table 2 of Appendix A provides a breakdown bystudy area and species of small mammals collected in 2001.

2.1.2 COLLECTION OF WOODCOCK SAMPLES IN 2001

The collection of American woodcock took place on September 27, 2001, using traditional hunting methods(a shotgun and dog). Two American woodcock were collected in the floodplain of the Hudson River inWashington County near Study Area 13. The liver was dissected out of each bird, using new single-usedisposable instruments, and each liver was placed into a chemically clean glass jar.

2.1.3 STORAGE OF SMALL MAMMAL AND WOODCOCK SAMPLES FROM 2001

The samples collected were entered on numbered Chain-of-Custody (COC) forms (see Appendix A) andplaced into the secure walk-in freezer at the New York State Department of Environmental Conservation(NYSDEC) Hale Creek Field Station in a sealed box for storage at -20 degrees Celsius. The samples werestored at -20 degrees Celsius until shipment to the program analytical laboratory for chemical analysis.

2.1.4 SHIPPING OF SAMPLES

On July 25, 2002, selected small mammal samples (total of 169 samples consisting of 61 short-tailed shrews,94 deer mice and white-footed mice, and 14 voles) and the two woodcock liver samples were delivered tothe program analytical laboratory for analysis. The small mammal samples were selected for analysis basedon consistency with genus and species of animals previously collected and analyzed in 2000, and consideringfor which species sufficient numbers had been captured at various study areas, based on anticipatedsubsequent compositing of animals at the program analytical laboratory.

COC forms were prepared with the appropriate signatures as the small mammal and woodcock liversamples were transferred from the Hale Creek Field Station by NYSDEC staff to the program analyticallaboratory. Strict COC was maintained to preserve sample integrity.

Samples not shipped to the analytical laboratory (two woodcock carcasses and 249 small mammal samples)have been retained in the NYSDEC Hale Creek Field Station freezer in storage at -20 degrees Celsius.

2.2 SAMPLE ANAL2.2 SAMPLE ANAL2.2 SAMPLE ANAL2.2 SAMPLE ANAL2.2 SAMPLE ANALYSISYSISYSISYSISYSIS

Chemical analyses were conducted pursuant to the Trustees' Analytical Quality Assurance Plan (HudsonRiver Natural Resource Trustees 2002b).

A total of 61 shrews and 108 mice/voles from 2001 were submitted for analysis. Shrews were analyzedas individuals. Mice were composited into 18 composites of five animals and one composite of fouranimals. Voles were composited into two composites of five animals each and one composite of fouranimals. The total number of shrews and composites analyzed was 83, grouped into six analytical batchesby the laboratory. Two woodcock liver samples from 2001 were also submitted for analysis.

The Trustees also determined that it was appropriate to re-analyze select shrew and soil samples from 2000pursuant to the methods contained in the Trustees Analytical Quality Assurance Plan, and to analyzearchived earthworm samples from 2000 that had not been analyzed previously.

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In 2000, the soil samples had been analyzed for total PCBs, and the shrew samples had beenanalyzed for total PCBs using a modified SW846 EPA Method 8082 (USEPA 1996) in which PCBswere quantified as Aroclors. By comparison, the Trustee's Analytical Quality Assurance Plan specifiesa total homologue method of quantifying PCBs using Low Resolution Mass Spectroscopy.Concentrations of specific individual PCB congeners are determined, the total concentration of eachhomologue group is determined, and the homologue groups are summed for a Total PCB value.

Thus, in addition to the small mammal and woodcock liver samples collected in 2001 that weresubmitted for analysis, the Trustees also submitted to the laboratory for re-analysis 18 soil samplesand 12 shrew samples from 2000 and submitted to the laboratory for analysis 10 earthwormcomposite samples. The soil, shrew and earthworm samples from 2000 were collected pursuant tothe Sampling and Analysis Plan for the 2000 investigation (SEA Consultants, Inc. 2000).

Samples collected in 2000 had been previously analyzed by a screening technique then stored frozenat -20 degrees Celsius until re-analysis in 2003 for this study.

The soils and shrew analyses from 2000 were each reported in a separate analytical batch, and willbe referred to as the '2000 analyses' to differentiate from the small mammals collected in 2001. Thewoodcock livers from 2001 and the earthworm composites from 2000 were analyzed in onelaboratory analytical batch.

The small mammal samples from 2001 and 2000, the woodcock livers, and the earthworm compositesamples were analyzed for select PCB congeners (see Table 3), PCB homologues, total PCBs (as sumof homologues) and percent lipids. Floodplain soil samples from 2000 were analyzed for select PCBcongeners (see Table 3), PCB homologues, total PCBs (as sum of homologues), and water content(%). The samples were prepped, extracted, and analyzed using laboratory SOPs approved by theTrustees prior to sample receipt.

Sample analysis began on August 18, 2003, and concluded on November 19, 2003.

2.3 QUALITY ASSURANCE/QUALITY CONTROL2.3 QUALITY ASSURANCE/QUALITY CONTROL2.3 QUALITY ASSURANCE/QUALITY CONTROL2.3 QUALITY ASSURANCE/QUALITY CONTROL2.3 QUALITY ASSURANCE/QUALITY CONTROL

Data validation was based on the quality assurance/quality control (QA/QC) criteria documented inthe Trustees' Analytical Quality Assurance Plan (Hudson River Natural Resource Trustees 2002b),U.S. Environmental Protection Agency (USEPA) (1999), and the following laboratory SOPs:

• SOP # HR NRDA Project Tissue Prep: Tissue Preparation and Homogenization, Revision#1.0, 9/25/02

• SOP # OP-004: Extraction of Soil, Tissue, Vegetation, and Sediment by Pressurized FluidExtraction, Revision #2.0, 8/15/02

• SOP # O-010: Determination of PCB Homologues and Individual Congeners by GC/MS -SIM, Revision # 2.2, 10/24/02

• SOP # HR NRDA % Lipids: Percent Lipids Determination, Revision # 0.0, 9/9/02• SOP # W-001: Percent Solids Determination, Revision # 2.1, 9/25/02• Additional cleanup, sample handling, storage, custody SOPs as necessary.

Sample results and related QC data were received in both an electronic and hard copy format.Electronic data were verified against the hard copy data package. The 2001 small mammal data, thewoodcock liver tissue data, and the earthworm data all received a full validation. The 2000 soil andshrew analyses received a summary validation.

The following QC elements were reviewed for data packages undergoing summary validation:• Analytical holding times• COC and sample handling

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• Method blank contamination (from summary forms)• Initial and continuing calibration (from summary forms)• Rinsate blank contamination (from sample results summaries)• Analytical accuracy: surrogates, matrix spike samples, laboratory control samples, and standard

reference material results (from summary forms)• Analytical precision: laboratory duplicate samples (from summary forms)• Internal standard areas (from summary forms)• Reported detection limits (from sample result summaries)

Full validation included review of all the items listed above for summary validation, plus the followingQC elements:

• Compound identification (from raw data)• Compound quantitation, transcription and calculation checks performed at a frequency of

10% from raw data. If an error was noted, 100% of the calculations and transcriptions forthat data set were verified.

Laboratory QC samples were used to assess the effectiveness of homogenization procedures and toevaluate laboratory-derived contamination, laboratory performance, and sample matrix effects.Quality control samples included: equipment rinsate blanks, method blanks, laboratory controlsamples (LCS), matrix spike (MS) samples, laboratory duplicate samples, and standard referencematerial (SRM) analyses. Surrogates were added to each sample analyzed for PCB congeners tofurther assess the effects of sample matrix on accuracy.

Data were qualified when associated QC sample results were outside the QC limits. The followingdefinitions provide brief explanations of the qualifiers assigned to results in the data validationprocess:

J Estimated: The associated numerical value is an estimated quantity. The analyte was detected,but the reported value may not be accurate or precise. The "J" qualification indicates the datafell outside the QC limits, but the exceedance was not sufficient to cause rejection of the data.

UJ Estimated/Not detected: An analysis was performed for the compound or analyte, but it wasnot detected and the sample quantitation or detection limit may be inaccurate or imprecise. Theassociated numerical result is the detection limit.

NJ Tentatively Identified/Estimated: The analyte was tentatively identified and the associatednumerical value is an estimated quantity.

R Rejected: Unreliable result. Data should not be used.

An SRM sample was extracted and analyzed with each analytical batch. The SRM selected for thesmall mammal tissues (including the 2000 shrew analyses), the earthworm tissue and the woodcockliver tissue was 1974b, Organics in Mussel Tissue. This SRM has certified values for 27 of the targetPCB congeners.

The data package submitted by the laboratory was reviewed to determine whether the analytical dataquality objectives (ADQO) specified in Tables 6.1a - 6.1c in the Analytical Quality Assurance Plan(Hudson River Natural Resource Trustees 2002b) were met.

Appendices B and C contain the Data Quality Assessment Reports (Hudson River Natural ResourceTrustees 2004b and 2004c) for the samples. Tables in those reports summarize the SRM results forthis preliminary investigation.

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Table 1.1 of the Trustees' Analytical Quality Assurance Plan (Hudson River Natural ResourceTrustees, 2002b) specifies the target Method Detection Limits (MDLs) for PCB congeners,homologues and total PCBs. For tissue, such as earthworm tissue composites, the target MDLs are0.1 ng/g ww (equivalent to 0.1 ppb ww) for individual congeners, and 10 ng/g (equivalent to 10 ppb)for PCB homologues and total PCBs. Actual MDLs for each PCB analyte were established by theanalytical laboratory as specified in the Analytical Quality Assurance Plan. Actual MDLs are reportedon the Data Sheets (Appendices D, E, and F) in the "Detection Limit" column.

For the 2001 small mammal analyses, one data point was rejected out of 4980 results reported by thelaboratory (83 samples, each with 47 congeners, 10 homologue groups, total PCBs, percent lipids andpercent moisture). The completeness level attained for the analysis of the field samples is greaterthan 99.99%. A total of 128 out of 4980 results (2.57%) were estimated because of laboratoryaccuracy and precision outliers. One data point was rejected based on an accuracy outlier. Therejected data point should not be used for any purpose. For all other data, the overall quality of thedata is acceptable and all results, as qualified, are considered usable.

For the 2000 shrew and soil samples, one data point was rejected out of 1770 results reported by thelaboratory (30 samples, each with 47 congeners, 10 homologue groups, and total PCBs; percent lipidsfor the 12 shrew samples; and percent moisture for the 18 soils). The completeness level attained forthe analysis of the 2000 samples is greater than 99.94%. A total of 333 out of 1770 results (18.8%)were estimated because of laboratory accuracy and precision outliers. One data point was rejectedbased on an accuracy outlier. The rejected data point should not be used for any purpose. For allother data, the overall quality of the data is acceptable and all results, as qualified, are consideredusable.

For the earthworm composites and woodcock liver tissue, out of 720 results reported by thelaboratory (12 samples each with 47 congeners, ten homologue groups, total PCBs, percent lipids andpercent moisture), a total of eight (1.1%) data points were qualified as estimated (J) because oflaboratory accuracy and precision outliers and one data point was rejected (R) due to a %R outlier.The completeness level attained for the analysis of the samples is greater than 99.8%. The rejecteddata point should not be used for any purpose. For all other data, the overall quality of the data isacceptable and the results, as qualified, are considered usable.

3.0 RESUL3.0 RESUL3.0 RESUL3.0 RESUL3.0 RESULTSTSTSTSTS

The Earthworm (2000) and Woodcock Liver (2001) Tissue Data Sheets (Appendix D), the SmallMammal (2001) Tissue Data Sheets (Appendix E) and the Soil and Shrew (2000) Data Sheets(Appendix F) provide the results of the analyses.

These Data Sheets contain information that has been extracted from the Trustees' Earthworm andWoodcock Liver Tissue Database (Hudson River Natural Resource Trustees 2004d) and the Trustees'2001 Small Mammal Tissue and 2000 Shrew and Soil Database (Hudson River Natural ResourceTrustees 2004e). Those complete databases and the accompanying Database User Manuals (HudsonRiver Natural Resource Trustees 2004f and 2004g) are not included in this report due to the size ofthe database, but will be made available upon request.

The Data Sheets contain the following fields:

Sampling Date - Sampling Date (mm/dd/yy format).

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Field ID -

For the Earthworm and Woodcock Liver Tissue Data Sheets, the field IDs were created using thefollowing format:

AAA-SSS

where AAA is an abbreviation to indicate the animal type (EW for earthworm composite, HWR forwoodcock liver tissue) and SSS is the site number where the animals were collected (two digits forearthworms, three digits for woodcocks). For example, EW-01 indicates a composite of earthwormscollected at Site 1, and HWR-001 indicates a woodcock liver from an animal collected at Site 1.

For the 2001 Small Mammals, the field IDs were created using the following format:

SS-NN-DDDDDD

where SS is the code for the site number (only one digit if the site number is less than 10), NN is thenumerical record of animals collected (e.g., "05" indicates the fifth animal collected) and DDDDDD is thecollection date (in a MMDDYY format). For example, 10-07-100401 indicates the seventh animal collectedat Site 10, taken October 4, 2001.

Some of the animals were composited prior to analysis. For composite samples, the following field IDformat was used:

Comp of Sta SS

where SS is the code for the site number (only one digit if the site number is less than 10). For example, acomposite of animals from Site 13 would be: Comp of Sta 13.

Two composites were created for Sites 12 and 20, one composite of mice and one composite of voles.These are differentiated as follows:

Comp of Sta 12 (mouse) or Comp of Sta 12 (vole)

with similar entries for the Site 20 composites.

For the 2000 shrews, the field IDs for the shrews collected in 2000 are similar to the field IDs for thesmall mammals collected in 2001, with a few additions:

S-NN-DDDDDD-MM-T-AAA

where SS, NN, and DDDDDD are the same as above. MM indicates the distance (in meters) from thetransect line through the site. T indicates the trapping method (always 'S' for snap trap for this data set),and AAA is the abbreviation for the animal type (always 'STS' for 'short-tailed shrew' for this data set). Forexample, 01-01-091000-10-S-STS indicates the first short-tailed shrew collected at Site 1, taken Sept 10,2000. The animal was collected using a snap trap, and was captured 10 meters from the transect throughSite 1.

For the 2000 soils, the field IDs for the soils use the following format:

SS-N-D-CM

where SS is the site number, N is the transect number (always '1' for this data set), D is a letter code whichindicates the sequence from the water's edge (A is closest to the water, B is further away, etc.), and CMindicates the deepest depth (in centimeters) of the soil core section.

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For example, 1-1-A15 indicates that the soil sample was collected at Site 1, at the sampling point(along the transect) closest to the river, and that the sample includes all of the soil from 0 cm to 15cm in depth. Sample 7-1-F25 would be a soil from Site 7, at the sixth sampling point away from theriver along the transect, and includes the soil from 15 cm to 25 cm in depth.

Easting - NAD83 Universal Transverse Mercator easting coordinates (meters) Zone 18N.

Northing - NAD83 Universal Transverse Mercator northing coordinates (meters) Zone 18N.

Site Number - as noted on Figure 1.

Laboratory ID - Laboratory IDs were created using the following format:

Sample delivery group B run sequence number (e.g., 0208031-01).

Analyte - For the PCB congeners, the analyte names are reported using the following format:

Clx-BZ#NNN

where Clx refers to the chlorination level, BZ# refers to the Ballschmiter and Zell (1994) number,and NNN is the congener number. For example, PCB 110 (a pentachlorinated biphenyl) is reportedas Cl5-BZ#110.

Value, Interpretive Qualifier and Units -

Value - Analytical result (3 significant figures).

Interpretive Qualifier - This field contains qualifiers applied to each data point by thelaboratory and after the data validation process. The qualifiers are defined as follows:

U Analyte was not detected. The associated value represents the detection limit

J Estimated: The associated numerical value is an estimated quantity. The analyte was detected,but the reported value may not be accurate or precise. The "J" qualification indicates the datafell outside the QC limits, but the exceedance was not sufficient to cause rejection of the data,OR that the reported result is with a range of elevated analytical uncertainty (greater than theMethod Detection Limit (MDL) value, but less than the Practical Quantitation Limit (PQL)value).

UJ Estimated/Not detected: An analysis was performed for the compound or analyte, but it wasnot detected and the sample quantitation or detection limit may be inaccurate or imprecise.The associated numerical result is the detection limit.

NJ The analyte was tentatively identified and the associated numerical value is an estimatedquantity.

D The concentration was reported from a dilution.

R Rejected: Unreliable result. Data should not be used. The values associated with R qualifiershave been removed from the databases.

Reasons for qualification are explained further in the Data Quality Assessment Reports (AppendicesB and C).

Unit - The unit of measurement of the analytical result is provided (for example, μg/kg).

Detection Limit - self-explanatory; this column includes units.

A brief description of some of the features of these data follows in sections 3.1 and 3.2 of this DataReport. Please note that the unit "μg/kg" used in the Data Sheets is equivalent to parts per billion(ppb) used in the discussion of these data in this Data Report.

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LS There are additional data fields, and data collected by the Trustees, that are not reported in this Data Report

but that are contained within the Trustees' Earthworm and Woodcock Liver Tissue Database and theTrustees' 2001 Small Mammal Tissue and 2000 Shrew and Soil Database. These include, but are notlimited to, Analytical Batch, Laboratory Flag, Analytical Method, Matrix, Extraction Date, Analysis Date,Dilution Factor, and Sample Size.

For the purpose of reporting PCB results below and in the figures attached to this report, all values flaggedwith either a U or UJ qualifier (that is, not detected; see Appendices B and C) were considered to be zeroin statistical evaluations of the data. Using zero, rather than the value reported by the laboratory for theanalyte, which represents the detection limit for the analysis, potentially underreports the true value, butavoids overreporting the true value. This is thus a conservative result; the actual PCB concentration couldbe higher.

3.13.13.13.13.1 TOT TOT TOT TOT TOTAL PCB CONCENTRAAL PCB CONCENTRAAL PCB CONCENTRAAL PCB CONCENTRAAL PCB CONCENTRATIONSTIONSTIONSTIONSTIONSTotal PCB concentrations in earthworm samples from 2000 range from 0.03 ppm to 23.9 ppm (ww) (Table1 and Figure 2).Total PCB concentrations in soil samples from 2000 range from 0.11 ppm to 937 ppm (dry weight basis)(Table 2 and Figures 3 and 4).Total PCB concentrations in shrew samples from 2000 range from 0.19 ppm to 36.7 ppm (ww) (Table 3and Figure 5).Total PCB concentrations in small mammal samples from 2001 range from 0.02 ppm to 30.4 ppm (ww)(Tables 4a-c and Figures 6, 7, and 8 for mice, voles and shrews, respectively).Total PCB concentrations in woodcock liver samples from 2001 are 0.12 ppm and 0.13 ppm (ww) (Table5).

Table 1. Summary of Total PCBs (as sum of homologues, ww) in

Earthworm Composite Samples

Composite Sample PCB ConcentrationSampling Site Size (g) (ppm)

1 27 1.23

2 20 0.49

3 28 0.03

4 26 2.42

5 28 6.31

6 33 11.30

7 26 0.18

8 22 11.30

10 26 23.90

11 16 20.30

Note that for earthworms collected in 2000, only one sample composite was collected from each of thesampling sites identified in Table 1, thus no means or standard deviations are reported.

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Table 2. Summary of Total PCBs (as sum of homologues, dry weight basis) in Soil Samples from 2000

Sampling n = Number of PCB Conc. Conc. Average ± 1 Std.

Site Samples Range (ppm) Dev. (ppm)

1 6 0.24 - 36.10 9.75 ± 13.45

7 6 0.11 - 139 33.04 ± 54.98

8 4 28.8 - 937 275.63 ± 441.83

10 1 - 114

11 1 - 204

Table 3. Summary of Total PCBs (as sum of homologues, ww) in Shrew Samples from 2000

Sampling n = Number of PCB Conc. Conc. Average ± 1 Std.

Site Samples Range (ppm) Dev. (ppm)

1 3 0.26 - 6.92 4.80 ± 3.94

7 4 0.79 - 36.70 11.17 ± 17.09

8 5 0.19 - 28.10 13.15 ± 10.13

Note that for soil and shrew samples, data are reported for only a subset of sites from which sampleswere collected in 2000 because, as discussed in Section 2.2, only a subset of samples from the 2000effort (as opposed to the entire sample set) were re-analyzed.

Table 4. Summary of Total PCBs (as sum of homologues, ww) in Small Mammal Samples from 2001

Table 4a. Mouse Composite Samples

Sampling Site Composite Sample Size

(g) PCB Concentration

(ppm) 1 115 0.23 3 111 0.02 4 116 0.17 5 152 0.19 6 117 0.46 7 107 0.17 8 108 0.21 10 107 0.07 11 121 0.63 12 83 2.13 13 133 0.03 15 114 0.04 16 113 0.30 17 102 0.42 18 118 0.09 20 100 0.24 21 123 0.09 22 110 0.04 23 108 0.05

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Composite Sample Size PCB Concentration

Sampling Site (g) (ppm)

2 159 0.05

12 152 0.18

20 220 0.15

Note that for mice and meadow voles collected in 2001, only one sample was collected from each of thesampling sites identified in Tables 4a and 4b; thus no means or standard deviations are reported.

Table 4c. Shrew Samples

Table 5. Summary of Total PCBs (as sum of homologues, ww) in Woodcock Liver Samples from 2001

PCB Conc. Range Conc. Average ± 1 Std.

Sampling Site n = Number of Samples (ppm) Dev. (ppm)

13 2 0.12 - 0.13 0.12 ± 7.07

3.2 3.2 3.2 3.2 3.2 PCB HOMOLOGUES AND CONGENERSPCB HOMOLOGUES AND CONGENERSPCB HOMOLOGUES AND CONGENERSPCB HOMOLOGUES AND CONGENERSPCB HOMOLOGUES AND CONGENERS

PCBs are synthetic (man-made) chemicals that form a group of 209 individual compounds that have similarchemical structures based on a biphenyl core with 1 to 10 chlorine atoms attached. PCBs have the genericformula C12H(10-x)Clx, where x is an integer from 1 to 10. Each individual PCB compound, called a congener,is identified by the unique number and location of chlorine atoms that attach to the compound's basestructure. Congeners differ both in their physical properties and in their effects on fish and wildlife (Safe1994; Van den Berg et al. 1998).

Sampling Site n = Number of Samples PCB Conc. Range

(ppm) Conc. Average " 1 Std.

Dev. (ppm)

1 4 0.30 - 12.9 6.06 " 6.05

7 5 0.70 - 30.40 10.83 " 12.35

8 5 0.20 - 24.20 8.65 " 11.50

13 5 0.05 - 2.76 0.66 " 1.18

15 7 0.07 - 0.50 0.18 " 0.17

16 7 2.04 - 10.60 5.61 " 2.96 17 5 2.65 - 7.71 5.50 " 2.15

18 3 0.16 - 0.64 0.35 " 0.26

20 3 0.87 - 1.08 0.99 " 0.11

21 4 0.44 - 0.76 0.61 " 0.17

22 4 0.03 - 0.09 0.06 " 0.03

23 8 0.03 - 0.09 0.05 " 0.02

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For this investigation, the samples were analyzed for the specific target PCB congeners listed in Table6. In addition, a total concentration for each homologue group was determined by summing alltarget and non-target congener concentrations within each homologue group. For any congenerreported as non-detected, zero was used in the summation.

Table 6. PCB Congener Analytes

Current Ballschmiter and Zell (1994)and IUPAC Number IUPAC Name

8 2,4'-Dichlorobiphenyl

18 2,2',5-Trichlorobiphenyl

28/31 2,4,4'-Trichlorobiphenyl/2,4',5-Trichlorobiphenyl

44 2,2',3,5'-Tetrachlorobiphenyl

45 2,2',3,6-Tetrachlorobiphenyl




56 2,3,3',4'-Tetrachlorobiphenyl


70 2,3',4',5-Tetrachlorobiphenyl

74 2,4,4',5-Tetrachlorobiphenyl


81 3,4,4',5-Tetrachlorobiphenyl

87 2,2',3,4,5'-Pentachlorobiphenyl

95 2,2',3,5',6-Pentachlorobiphenyl


101 2,2',4,5,5'-Pentachlorobiphenyl

105 2,3,3',4,4'-Pentachlorobiphenyl

110 2,3,3',4',6-Pentachlorobiphenyl

114 2,3,4,4',5-Pentachlorobiphenyl


123 2,3',4,4',5'-Pentachlorobiphenyl


128 2,2',3,3',4,4'-Hexachlorobiphenyl

138 2,2',3,4,4',5'-Hexachlorobiphenyl


149 2,2',3,4',5',6-Hexachlorobiphenyl

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and IUPAC Number IUPAC Name

151 2,2',3,5,5',6-Hexachlorobiphenyl


156 2,3,3',4,4',5-Hexachlorobiphenyl

157 2,3,3',4,4',5'-Hexachlorobiphenyl

158 2,3,3',4,4',6-Hexachlorobiphenyl



170 2,2',3,3',4,4',5-Heptachlorobiphenyl

174 2,2',3,3',4,5,6'-Heptachlorobiphenyl

177 2,2',3,3',4,5',6'-Heptachlorobiphenyl

180 2,2',3,4,4',5,5'-Heptachlorobiphenyl

183 2,2',3,4,4',5',6-Heptachlorobiphenyl

187 2,2',3,4',5,5',6-Heptachlorobiphenyl

189 2,3,3',4,4',5,5'-Heptachlorobiphenyl

194 2,2',3,3',4,4',5,5'-Octachlorobiphenyl

195 2,2',3,3',4,4',5,6-Octachlorobiphenyl

201 2,2',3,3',4,5',6,6'-Octachlorobiphenyl

206 2,2',3,3',4,4',5,5',6-Nonachlorobiphenyl

209 Decachlorobiphenyl

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4.0 REFERENCES4.0 REFERENCES4.0 REFERENCES4.0 REFERENCES4.0 REFERENCES

Ballschmiter, K. and Zell M. 1994. Analysis of polychlorinated biphenyls (PCBs) by glasscapillary gas chromatography. Fresenius' Journal of Analytical Chemistry 302:20-31.

Hudson River Natural Resource Trustees. 2002a. Hudson River Natural Resource DamageAssessment Plan. September 2002. U.S. Department of Commerce, Silver Spring, MD.

Hudson River Natural Resource Trustees. 2002b. Analytical Quality Assurance Plan for theHudson River Natural Resource Damage Assessment. Public Release Version. July 9,2002, Version 1.0. U.S. Department of Commerce, Silver Spring, MD.

Hudson River Natural Resource Trustees. 2004a. Work Summary for the Collection of SmallMammals and American Woodcock from the Floodplains of the Hudson River, NewYork. Hudson River Natural Resource Damage Assessment. Final. Public ReleaseVersion. May 27, 2004. U.S. Department of Commerce, Silver Spring, MD.

Hudson River Natural Resource Trustees. 2004b. Data Quality Assessment Report. HudsonRiver Natural Resource Damage Assessment. Floodplain Study. Woodcock Liver Tissueand Earthworm Tissue. Public Release Version. February 2, 2004. Version 1.0. U.S.Department of Commerce, Silver Spring, MD.

Hudson River Natural Resource Trustees. 2004c. Data Quality Assessment Report. HudsonRiver Natural Resource Damage Assessment. Floodplain Study. 2001 Small MammalsTissue and 2000 Shrews and Soils. Public Release Version. February 19, 2004. Version1.1. U.S. Department of Commerce, Silver Spring, MD.

Hudson River Natural Resource Trustees. 2004d. Earthworm and Woodcock Liver TissueDatabase. Version 2.0. U.S. Department of Commerce, Silver Spring, MD.

Hudson River Natural Resource Trustees. 2004e. 2001 Small Mammal Tissue and 2000Shrew and Soil Database. Version 2.0. U.S. Department of Commerce, Silver Spring,MD.

Hudson River Natural Resource Trustees. 2004f. Database User Manual for Version 2.0.Hudson River Natural Resource Damage Assessment. Floodplain Study. WoodcockLiver Tissue and Earthworm Tissue. Public Release Version. July 30, 2004. U.S.Department of Commerce, Silver Spring, MD.

Hudson River Natural Resource Trustees. 2004g. Database User Manual for Version 2.0.Hudson River Natural Resource Damage Assessment. Floodplain Study. 2001 SmallMammals Tissue and 2001 Shrews and Soils. Public Release Version. July 30, 2004. U.S.Department of Commerce, Silver Spring, MD.

Safe, S.H. 1994. Polychlorinated biphenyls (PCBs): Environmental impact, biochemical andtoxic responses, and implications for risk assessment. Critical Reviews in Toxicology 24:87-149.

SEA Consultants, Inc. 2000. Sampling and Analysis Plan, Hudson River Floodplain, NaturalResources Damage Assessment. SEA Consultants, Inc., Cambridge, Mass. ReportPrepared for Industrial Economics, Inc. September 2000.

SEA Consultants, Inc. 2002. Hudson River Natural Resources Damage Assessment,Floodplain Soil and Biota Screening Sampling Report. SEA Consultants, Inc., Cambridge,Mass. Report Prepared for Industrial Economics, Inc. SEA Project No. 2000416.01-A.

United States Environmental Protection Agency. 1996. Test Methods for Evaluating SolidWastes. SW-846. Third Edition. December.

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Functional Guidelines for Organic Data Review. Office of Emergency and Remedial Response,Washington, D.C. 20460. EPA540/R-99/008. 118 pp.

Van den Berg, M., Birnbaum, L., Bosveld, A.T.C., Brunstrom, B., Cook, P.M., Feeley, M., Giesy, J.P.,Hanberg, A., Hasegawa, R., Kennedy, S.W., Kubiak, T.J., Larsen, J.C., van Leeuwen, F.X.R., Liem,A.K.D., Nolt, C., Peterson, R.E., Poellinger, L., Safe, S., Schrenk, D., Tillitt, D.E., Tysklind, M.,Younes, M., Waern, F., and Zacharewski, T. 1998. Toxic Equivalency Factors (TEFs) for PCBs,PCDDs, PCDFs for humans and wildlife. Environmental Health Perspectives 106: 775-792.

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FIGURESFIGURESFIGURESFIGURESFIGURES

Figure 1. Hudson River Sampling Sites.

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weight, ppm).

Figure 3. Total PCB concentrations in soils collected along the Hudson River in 2000 (dry weight,ppm).

0

5

10

15

20

25

30

11 10 8 7 6 5 4 3 2 1Sample Site

Tota

l PCB

s (p

pm)

DownriverUpriver

0.1

1

10

100

1000

0 1 2 3 4 5 6

Sample Site

Tota

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Bs

(ppm

)

Total PCB concentration

Average Total PCB Concentration

11 10 8 7 1

Upriver Downriver

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Figure 4. Total PCBs (dry weight ppm) in surficial (0-15 cm) floodplain soils by site anddistance from River.

Figure 5. Total PCB concentrations in shrews collected along the Hudson River in 2000(wet weight, ppm).

0

10

20

30

40

0 1 2 3 4Sample Site

Tota

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Bs (p

pm)

Total PCB concentrationAverage Total PCB Concentration

8 7 1

Upriver Downriver

AB

CD

Site

11Site

10Site 8Site 7

Site 1

0.1

1

10

100

1000

Total PCBs (ppm)

Upriver

Downriver* Subsurface sample (15-25 cm depth)

Closer to river

Further from river

*

AB

CD

Site

11Site

10Site 8Site 7

Site 1

0.1

1

10

100

1000

Total PCBs (ppm)

Upriver

Downriver* Subsurface sample (15-25 cm depth)

Closer to river

Further from river

*

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Figure 6. Total PCB concentrations in composite mouse samples collected along the HudsonRiver in 2001 (wet weight, ppm).

Figure 7. Total PCB concentrations in composite vole samples collected along the Hudson Riverin 2001 (wet weight, ppm).

0

0.5

1

1.5

2

2.5

12 11 10 8 7 6 5 4 3 1 13 15 16 17 18 20 21 22 23

Sample Site

Tota

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s (p

pm)

Upriver Downriver

0

0.05

0.1

0.15

0.2

12 2 20

Sample Site

Tota

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s (p

pm)

Upriver Downriver

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Figure 8. Total PCBs in shrews collected along the Hudson River in 2001 (wet weight, ppm).

0.01

0.10

1.00

10.00

100.00

0 1 2 3 4 5 6 7 8 9 10 11 12 13

Sample Site

Tota

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(ppm

)


Average Total PCB concentration

8 7 1 13 15 16 17 18 20 21 22 23

Upriver Downriver

0.01

0.10

1.00

10.00

100.00

0 1 2 3 4 5 6 7 8 9 10 11 12 13

Sample Site

Tota

l PC

Bs

(ppm

)


Average Total PCB concentration

8 7 1 13 15 16 17 18 20 21 22 23

Upriver Downriver

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APPENDIX A

WORK SUMMARY FOR THE COLLECTION OF

SMALL MAMMALS AND AMERICAN WOODCOCK

FROM THE FLOODPLAINS OF THE HUDSON RIVER,

NEW YORK

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WORK SUMMARY

Collection of Small Mammals and American Woodcock from the Floodplains of the Hudson River, New York

Hudson River Natural Resource Damage Assessment

FINAL

May 27, 2004

____________________________________ Christopher Balk, Field Investigation Lead ___________________________________ Quality Assurance Coordinator

Table of Contents

1.0 Introduction.........................................................................................................................................1

2.0 Project Management ..................................................................................................................... 2

3.0 Small Mammal Collection........................................................................................................... 2

3.1 Small Mammal Collection Dates and Study Areas..................................................2 3.2 Small Mammal Collection Procedures ....................................................................2 3.3 Sample Containers and Labeling for Small Mammal Samples ...............................4 3.4 Summary of Small Mammal Samples Collected .....................................................4 4.0 American Woodcock Collection .............................................................................................. 4

4.1 American Woodcock Collection Dates and Study Sites..........................................4 4.2 American Woodcock Collection Procedures ...........................................................5 4.3 Preparation of American Woodcock Samples .........................................................5 4.4 Sample Containers and Labeling for American Woodcock Samples......................6 5.0 Sample Shipping, Analysis and Chain of Custody..........................................................6

6.0 Quality Assurance/Quality Control .........................................................................................7

7.0 References Cited ..............................................................................................................................7

List of Appendices: Appendix A: Maps for 2001 Small Mammal and Woodcock Collection Sites Appendix B: Small Mammal Data Sheet Appendix C: Chain of Custody Form

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1.0 Introduction Past and continuing discharges of polychlorinated biphenyls (PCBs) have contaminated the natural resources of the Hudson River. The Hudson River Natural Resource Trustees (Trustees) – New York State, the U.S. Department of Commerce, and the U.S. Department of the Interior – are conducting a natural resource damage assessment (NRDA) to assess and restore those natural resources injured by PCBs (Hudson River Natural Resource Trustees 2002a). This Work Summary documents a preliminary investigation of PCB contamination of floodplain biota conducted pursuant to the NRDA. In September and October 2000, as part of the Hudson River NRDA, sampling of soil and biota was conducted within the floodplain of the Hudson River between Fort Edward, New York and the Saratoga Battlefield National Historic Park (NHP) in Stillwater, New York (SEA Consultants, Inc. 2002). The purpose of the soil and biota sampling was to assist the Trustees in determining whether soil and biota containing PCBs are present in the floodplain of the Hudson River between Fort Edward and Stillwater, New York, and if additional pathway and injury assessment studies should be conducted. As part of the 2000 floodplain investigation, floodplain soil samples were collected from eleven sites along the Hudson River, and analyzed for Total PCBs, Total Organic Carbon (TOC) and grain size. Concurrent with the soil sampling activities, the New York State Department of Environmental Conservation (NYSDEC) conducted biota sampling of small mammals and earthworms at ten of the soil sampling locations and at one additional site. Whole body tissue of short-tailed shrews (Blarina brevicauda) was analyzed for total PCBs and percent lipids, and earthworms were frozen and archived. The Trustees have released a report regarding the 2000 floodplain investigation and results (SEA Consultants Inc. 2002). The results of the September/October 2000 floodplain soil and biota tissue sampling program indicate that floodplain soil in the Upper Hudson River valley between Stillwater, New York and Fort Edward, New York are contaminated by detectable levels of PCBs. In addition, the detection of PCBs in short-tailed shrew tissue indicates the bioavailability of soil PCBs to higher level organisms. In 2001 the Trustees continued the floodplain investigation, collecting small mammals from a number of the 2000 sites and from additional Hudson River floodplain locations, and collecting American woodcock (Scolopax minor) from Hudson River floodplains. This Work Summary documents those 2001 collections of small mammals and woodcocks.

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2.0 Project Management The investigation team was organized based on tasks and levels of responsibility to ensure good communication between all personnel. The Assessment Manager (Larry Gumaer, NYSDEC) had overall project oversight and responsibility for design and implementation of the investigation, and provided direction to the Field Investigation Lead (Chris Balk, NYSDEC), who was responsible for the field collection. The Field Investigation Lead worked with the Assessment Manager and Quality Assurance (QA) Coordinator to ensure that the investigation was consistent with the overall QA objectives of the NRDA. 3.0 Small Mammal Collection

3.1 Small Mammal Collection Dates and Study Areas The collection effort began on September 4, 2001, and concluded on October 18, 2001. The sample collection effort focused on the 12 sites from the 2000 investigation and 11 new sites (designated Study Areas 13 through 23) for 2001. The new study areas are shown on the maps in Appendix A. Nine of the new study areas were located between the Saratoga Battlefield NHP in Stillwater, New York, and the Federal Dam at Troy, New York, and two were located between the Federal Dam at Troy and Poughkeepsie, New York.

3.2 Small Mammal Collection Procedures Snap traps were used to make the small mammal collections. Trapping was aimed at collecting in low lying areas close to the river that showed signs of flooding, appeared to flood or were known to flood during periods of high river flow. The traps were checked on a daily basis with the exception of two instances (September 11, 2001 involving collection at Study Areas 4 and 7; and September 25, 2001 involving collection at Study Areas 13 and 21) in which traps were checked only once within 48 hours. Of the nine study areas located between Saratoga NHP and the Federal Dam at Troy, two were not used for small mammal collection. No collection was made at Study Area 14 due to the lack of suitable small mammal habitat in the floodplain and a general lack of floodplain area at the site. No collection was made at Study Area 19 due to the lack of small mammal sign and due to evidence that this site was on an island that was periodically completely inundated with floodwaters.

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All shrews and small mammals collected were placed in a Quality Assured, 60ml wide-mouth glass sample jar with a Teflon lined lid, one animal per jar, labeled and put on ice in a cooler in the field. As each sample was collected in the field it was recorded on a “Small Mammal Data Sheet” (Appendix B) and those data sheets were put into a binder to form a field log of activities. In the field, the following data were recorded on the small mammal data sheets: date, weather, capture site # / name, personnel, sample #, time, distance to a reference marker or river edge, and any notes. Each sample was identified to species, where possible, or to genus. Fresh weights for the small mammal samples were not taken due to time and personnel constraints at the time of sampling, and later, Quality Assurance/Quality Control concerns about re-opening the jars and thawing the samples to work with them precluded collecting such information. Subsequently, the program analytical laboratory recorded the weights of the samples prior to homogenization. At the end of each day, the small mammal samples collected were taken to the NYSDEC Hale Creek Field Station. The samples collected were entered on numbered Chain-of-Custody (COC) forms (Appendix C) and placed into the secure walk-in freezer at the Hale Creek Field Station in a sealed box for storage at -20 degrees Celsius. The samples were stored at -20 Celsius until shipment to the program analytical laboratory for chemical analysis. The collected animals were given sample identification numbers using a modification of the format used for the 2000 study. Sample identification numbers for 2001 were designated as follows: Example: 07-02-091201

• the first two digits (07) are the site number (Study Area 7 in this example); • the next two digits indicate that it was the second animal collected at this location; and, • the final six digits indicate the date of collection in a MM/DD/YY format, such as

091201 to indicate that it was collected on 09/12/01 (September 12, 2001).

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3.3 Sample Containers and Labeling for Small Mammal Samples

Each sample was placed individually in a chemically clean glass jar. To each sample jar was affixed a waterproof label indicating the following: Site number Project name Date and time collected Analyses requested Method of preservation Initials of sampling personnel

3.4 Summary of Small Mammal Samples Collected In the 2001 effort, small mammals were collected from 11 of the sites from the 2000 study (Site Nos. 1, 2, 3, 4, 5, 6, 7, 8, 10, 11, and 12) and from 9 of the new sites (Study Areas 13, 15, 16, 17, 18, 20, 21, 22, and 23). Table 1 provides a description of the sample sites used in the 2000 and 2001 floodplain investigations, and the types of samples collected from each site. A total of 418 mammals were collected from the Hudson River floodplain study areas in 2001. Table 2 provides a breakdown by study area and species of small mammals collected in 2001. There were a very small number of additional animals that were trapped but not collected for potential analysis due to the fact that those animals were not whole when found in the trap; the Field Investigation Lead estimates this to be less than 2 percent of the total number of animals captured. Specimens found in the trap partially eaten, dismembered, or otherwise not sufficiently intact, were discarded with a few exceptions. If the animal was largely intact it was collected for potential future analysis. 4.0 American Woodcock Collection

4.1 American Woodcock Collection Dates and Study Sites The collection took place on September 27, 2001. Three sites were selected for potential woodcock collection; those sites were as follows: in the vicinity of Site 4; north of Site 5; and, in the vicinity of Site 8. These sites were selected, based on the ability to gain access to them (considering both logistics of access and permission to access having been granted), site topography and reconnaissance at the site. Collection site locations were a waypoint recorded with a GPS unit.

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The goal of the investigation was to collect four woodcock per each of the three sites. Collection activities were focused on low lying areas close to the river that showed signs of flooding, appeared to flood or were known to flood during periods of high river flow.

4.2 American Woodcock Collection Procedures On September 27, 2001, under appropriate State and Federal permits, the Field Investigation Lead collected two American woodcock in the floodplain of the Hudson River in Washington County, along the eastern bank of the river, approximately 0.5 miles south of the southern end of the Saratoga Battlefield NHP (near Study Area 13). The birds were collected using traditional hunting methods (a shotgun and dog). Each woodcock collected was wrapped in aluminum foil and placed individually into a zippered plastic bag, labeled, and put on ice in a cooler in the field. Collected birds were each given a sample identification number, as follows: HRW-001, and HRW-002, where “HRW” represents “Hudson River Woodcock” and the numbers (-001 and -002) are the animal (specimen) numbers. Data recorded on a collection record, carcass tag, and memo to the file, included the following: site number, species, weight, beak length, capture date, and GPS waypoint of the collection site. The birds were tagged in the field, placed on ice as soon as possible, and located with a Garmin GPS 12 global positioning unit. At the end of the day, the samples collected were entered on numbered COC forms (Appendix C) and placed into the secure walk-in freezer (-20 C) at the Hale Creek Field Station in a sealed box. A total of two American woodcock were collected, both from habitat adjacent to Study Area 13. Although the goal had been to collect four woodcocks from each of three sites this could not be accomplished due to staff and time constraints.

4.3 Preparation of American Woodcock Samples On the day of collection, at the NYSDEC Hale Creek Field Station laboratory, within four hours of collection, the birds were weighed with a Fischer Scientific XT top-loading balance, and culmen lengths measured with a dial caliper. The liver was dissected out of each bird, using new single-use disposable instruments. Each liver was placed into a chemically clean glass jar with a Teflon lid and the jar labeled as described below.

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4.4 Sample Containers and Labeling for American Woodcock Samples

Each woodcock liver sample was placed individually in a chemically clean glass jar with a Teflon lid. To each sample jar was affixed a waterproof label indicating the following: Unique sample number (HRW-001 or HRW-002) Site number Date of collection Species Method of preservation Initials of sampling personnel The woodcock liver samples and their corresponding carcasses were placed in a custody-sealed box and stored in the secure walk-in freezer at the NYSDEC Hale Creek Field Station. The samples were stored at -20 degrees Celsius. Liver samples were subsequently shipped to the program analytical laboratory for chemical analysis. Carcass samples remain in frozen storage (at -20 degrees Celsius) at the NYSDEC Hale Creek Field Station. 5.0 Sample Shipping, Analysis and Chain of Custody On July 25, 2002, selected small mammal samples (total of 169 samples consisting of 61 short-tailed shrews, 94 deer mice and white-footed mice, and 14 voles) and the two woodcock liver samples were sent to the program analytical laboratory for analysis. The small mammal samples were selected for analysis based on consistency with genus and species of animals previously collected in 2000 and analyzed, and considering for which sufficient numbers had been captured at various study areas, based on anticipated subsequent compositing of animals at the program analytical laboratory. COC forms were prepared with the appropriate signatures as the small mammal and woodcock liver samples were transferred from the Hale Creek Field Station by NYSDEC staff to the program analytical laboratory. Strict maintenance of COC is important to demonstrate sample integrity. The sample jars containing the small mammal samples and the woodcock liver samples were shipped to the program analytical laboratory for analysis in the boxes in which they were originally shipped to the collector. The Field Investigation Lead delivered the samples in person. Wet ice was used to keep the samples frozen during shipment.

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The COC forms were signed by the Field Investigation Lead and kept inside a zippered plastic bag in the cooler during shipping. The COC forms accompanied the sample shipments and document the transfer of the samples from the field team to the laboratory. As the samples were received by the laboratory, they were logged in and any damaged or broken custody seals were noted. Samples not shipped to the analytical laboratory have been retained in the NYSDEC Hale Creek Field Station freezer in storage at -20 degrees Celsius. 6.0 Quality Assurance/Quality Control In July 2002 the Trustees finalized an Analytical Quality Assurance Plan (Hudson River Natural Resource Trustees 2002b). In September 2002, the Trustees issued a Quality Assurance Management Plan (as part of the NRDA Plan) (Hudson River Natural Resource Trustees 2002a). The small mammal and woodcock collections in August 2001 thus predate the Trustees’ Analytical QA Plan and the QA Management Plan. The analysis of these samples, however, post-dates these two plans. Accordingly, the analysis of the 2001 samples was conducted in a fashion to be in compliance with the requirements of the QA Management Plan and the Analytical QA Plan. Data Quality Assessment Reports document the results of the quality assurance review of data from analysis of the small mammal and woodcock liver tissue samples. The original data sheets have been retained at the Hale Creek Field Station, and will be maintained by NYSDEC and archived for a minimum of fifteen years. Any disposal of the data sheets will be coordinated with the DOI and NOAA after this timeframe unless a longer archive period is requested. Analytical data resulting from this investigation will be validated as specified in the Analytical QA Plan. 7.0 References Cited Hudson River Natural Resource Trustees. 2002a. Hudson River Natural Resource Damage Assessment Plan. September 2002. U.S. Department of Commerce, Silver Spring, MD. Hudson River Natural Resource Trustees. 2002b. Analytical Quality Assurance Plan for the Hudson River Natural Resource Damage Assessment. Public Release Version. July 9, 2002, Version 1.0. U.S. Department of Commerce, Silver Spring, MD. SEA Consultants, Inc. 2002. Hudson River Natural Resources Damage Assessment, Floodplain Soil and Biota Screening Sampling Report. SEA Consultants, Inc., Cambridge, Mass. Report Prepared for Industrial Economics, Inc. SEA Project No. 2000416.01-A. U.S. Environmental Protection Agency (USEPA). 1999. Action Memorandum: Request for removal action for the Rogers Island Site, Fort Edward, Washington County, New York, by Jack D. Harmon, On-scene Coordinator, Removal Action Branch. September 28.

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Table 1: Sampling Site Descriptions – 2000 and 2001 Floodplain Samples Site No.

Descriptive Name of Site

Location / Description Samples Collected

Sites from 2000 Floodplain Study from which Collections were made in 2001 1 Southern Park West bank of Hudson River in southern corner of

Saratoga Battlefield National Historic Park. A wide low-lying area of undisturbed wooded wetland.

2000: soil, shrews, earthworms 2001: small mammals

2 Battlefield Meadow

West bank of Hudson River near Saratoga Battlefield National Historic Park entrance. The site is a wet meadow separated from the Hudson River by an old roadbed and receives floodwaters via a culvert during high river stage.


3 River Road West bank of the Hudson River, along River Road just upstream of the Saratoga Battlefield National Historic Park. The sampling site is a small low lying, wooded wetland area adjacent to an open water scrub-shrub wetland. The site is located west of River Road and is apparently flooded via a narrow culvert (approximately 18 inch diameter) under the road.


4 Fishing Hole A large low-lying wooded wetland on the west bank of the Hudson River, south of Coveville. The site is accessed by a small boat ramp approximately 100 m south of Hanehan Road. The site is generally undisturbed, with the exception of an all-terrain vehicle (ATV) path which cuts through along the riverbank. The site appears to be frequently flooded.


5 Opposite Coveville

East bank of Hudson River, off Rt. 113 opposite Coveville. The site is an undisturbed, low-lying wooded wetland area with large quantities of debris apparently deposited from flooding events.


6 Schuylerville A wide, low-lying undisturbed mature wooded wetland site on the west bank of the Hudson River. The site is accessed through a large cornfield south of Schuylerville, just south of Schuyler Street.


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Site No.



7 Near River Mile 187

A low-lying site on the bank of the Hudson River. Half of the site is wooded, with a strip of grass adjacent to the river on the other half.


8 Peters Rd. / Floodgates

West bank of the Hudson River, just upstream of Thompson Island. The site is just south of Peters Rd. and adjacent to a large wetland area. The eastern half of the soil sampling transect is flooded directly by the Hudson. The western half of the transect is located west of County Route 29, extending into the wooded wetland area. The wetland area regularly receives floodwaters via a pair of 48-inch culverts (formerly iron floodgates) that go under Route 29. These culverts are of sufficient size and invert elevation such that flooding from the river appears to be essentially unrestricted.


9 Near River Mile 191

This small area is apparently flooded via a culvert that goes under a road, connecting the site with the Hudson River. The culvert invert was several feet above the river level at the time of sampling, and was somewhat constricted with debris.

2000: soil 2001: no samples collected

10 Canal Corp. East bank of the Hudson River, south of Fort Edward, and just north of Black House Rd. The site is a low-lying wooded wetland adjacent to a small stream channel.


11 Rogers Island East bank of Rogers Island, approximately 0.1 miles south of railroad trestle. The site is a disturbed deciduous forested area slightly elevated above the river. Soil samples previously collected on Rogers Island by the United States Environmental Protection Agency (USEPA, 1999) indicated that soils were contaminated with PCBs.


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Site No.



12 Rogers Island South

East bank of Rogers Island near the southern end of the island. The site is slightly elevated above the Hudson River (bank approximately 4 feet above river). Site is forested near the riverbank and adjacent to an old meadow. Soil samples previously collected on Rogers Island by the United States Environmental Protection Agency (USEPA, 1999) indicated that soils were contaminated with PCBs. This site was added for shrews collection (in the 2000 study) as it provided more suitable habitat than at Site 11.

2000: shrews 2001: small mammals

New Sites for 2001 13 Opposite Site

#1 Along east bank of Hudson River; mature woodland floodplain south of Site #1.

2001: small mammals, woodcock

14 South of Site 1

0.8 miles south of Site 1 along west bank of the Hudson River

No samples collected

15 Near Stillwater Union Cemetery

Along west river bank, between Stilwater Union cemetery and the Hudson River, about 1.5 miles upstream of Lock #4; wooded wetland dominated by silver maple.

2001: small mammals

16 Lock #4 Along east bank of Hudson River, adjacent to Lock #4; this site is primarily woodland adjacent to a pond and wetland.

2001: small mammals

17 Mechanicville Island

Unnamed island south of the New York State Route 67 bridge in Mechanicville; wooded island dominated by poplar.

2001: small mammals

18 Lock #2 Along west bank of Hudson River, just south of Lock #2; scrub/shrub habitat transitioning to rock/sand/gravel at the water’s edge

2001: small mammals

19 Island north of Campbell Island

An island in the Hudson River just north of Campbell Island

No samples collected

20 Campbell Island

Site is located on the northern end of Campbell Island just south of Lock #1; site is wooded, dominated by poplars with a fern understory.

2001: small mammals

21 North of Waterford

Along west bank of Hudson River; the floodplain of a river-associated wetland 1¼ miles south of the U.S. Route 4 bridge in Waterford; site is wooded, dominated by silver maples and poplars.

2001: small mammals

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22 Papscanee Island

Along east bank of Hudson River, in the Papscanee Island nature preserve; site is wooded, dominated by poplars.

2001: small mammals

23 Upper Schodack Island

Along east bank of Hudson River in the newly created Schodack Island State Park, about ¼ mile south of the boat launch; site is wooded, dominated by poplars.

2001: small mammals

Note: For Site Nos. 1 through 12, Site Nos., Descriptive Name of Site, Location/Description and Samples Collected in 2001 are from the 2000 Floodplain Study report (SEA Consultants, Inc. 2002).

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Table 2. Summary of Small Mammals Collected in 2001 from Hudson River floodplain sites (see Table 1 for site names, locations). Site No. Peromyscus

spp. (deer mice and white-footed mice)

Blarina brevicauda (short-tailed shrew)

Microtus pennsylvanicus (meadow vole)

Sorex spp. (tiny shrews)

Tamias striatus (chipmunk)

Condylura cristata (star-nosed mole)

(Microtus pinetorum)(pine vole)

Nepeozapus insignis (jumping mouse)

1 14 5 0 0 0 0 0 1 2 0 4 11 2 0 0 0 1 3 11 3 1 3 1 0 0 0 4 16 4 0 0 1 0 0 0 5 13 10 2 1 0 1 0 0 6 16 1 1 0 0 0 1 0 7 15 5 1 0 0 0 0 0 8 18 5 0 1 0 0 0 0 10 14 6 1 0 0 0 0 1 11 18 3 0 0 0 0 0 0 12 4 0 4 0 0 0 0 0 13 12 5 1 0 0 0 0 0 15 15 7 0 0 0 0 0 0 16 12 7 0 0 0 0 0 0 17 8 5 1 0 0 0 0 0 18 18 3 0 0 0 0 0 0 20 18 3 15 0 0 0 0 0 21 18 4 0 0 0 0 0 0 22 19 4 1 0 0 0 0 0 23 12 9 1 0 0 0 0 0 Total 271 93 40 7 2 1 1 3

Appendix A

Maps for 2001 Small Mammal and Woodcock Collection Sites (Sites are described in Table 1)

1

These sites are just south of the Saratoga Battlefield National Historic Park

This site is located between the Saratoga Battlefield and Stillwater

2

This site is at Lock #4 near Stillwater.

This site is on an island near Mechanicville.

3

This site is at Lock #2 south of Mechanicville These areas are near the GE plant just north of Waterford.

4

Study area just north of Waterford

Study Area 22

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Study area 23 on Upper Schodack Is.

Appendix B

Small Mammal Data Sheet

Hudson River Floodplain Biota Sampling Project Small mammal data sheet Date:___________________ Weather:__________________________ Site # / Name:__________________ Personnel:_________________________ Sample #: ____________________ Time:_____________________ NOTES: Species:_______________________________ Weight: (g) Total Length: (mm) Body Length: (mm) Distance to: Reference Marker River Edge

Appendix C

Chain of Custody Form

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APPENDIX B

DATA QUALITY ASSESSMENT REPORTHUDSON RIVER NATURAL RESOURCE

DAMAGE ASSESSMENT FLOODPLAIN STUDY

WOODCOCK LIVER TISSUE ANDEARTHWORM TISSUE

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DATA QUALITY ASSESSMENT REPORT

HUDSON RIVER NATURAL RESOURCE DAMAGE ASSESSMENT

FLOODPLAIN STUDY Woodcock Liver Tissue and Earthworm Tissue

Prepared for: State of New York

Department of Environmental Conservation

U.S. Department of Commerce National Oceanic and Atmospheric Administration

U.S. Department of Interior Fish and Wildlife Service

February 2, 2004

Version 1.0

Data Quality Assessment Earthworm and Woodcock Livers

Version 1.0 February 2, 2004

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TABLE OF CONTENTS

1.0 INTRODUCTION ................................................................................1 2.0 DATA VALIDATION PROCEDURES.................................................1 3.0 DATA QUALITY ASSESSMENT........................................................3

3.1 Holding Times and Sample Preservation......................................................................3

3.2 Instrument Calibration....................................................................................................3 3.2.1 Initial Calibration (ICAL) ...................................................................................................... 3 3.2.2 Continuing Calibration (CCAL)............................................................................................3

3.3 GC/MS Tune.....................................................................................................................4

3.4 Blank Analyses................................................................................................................4

3.5 Accuracy ..........................................................................................................................4 3.5.1 Surrogate Compounds ........................................................................................................... 4 3.5.2 Standard Reference Material (SRM) Analyses ...................................................................... 4 3.5.3 Laboratory Control Samples................................................................................................... 5 3.5.4 Matrix Spike Samples............................................................................................................. 5 3.5.5 Internal Standards .................................................................................................................. 5

3.6 Precision ..........................................................................................................................5 3.6.1 Laboratory Duplicate Samples ............................................................................................... 6

3.7 Reporting Limits and Sample Results...........................................................................6

3.8 Completeness..................................................................................................................6

3.9 Summary of Data Usability.............................................................................................6

TABLE 1: Summary of Standard Reference Material Results

TABLE 2: Laboratory Duplicate Relative Percent Difference Summary

ATTACHMENT A: Data Validation Reports by Sample Delivery Group …...…………A - 1

Data Quality AssessmentEarthworm and Woodcock Livers


1

DATA QUALITY ASSESSMENT Hudson River Natural Resource Damage Assessment

Woodcock Liver Tissue and Earthworm Tissue

1.0 INTRODUCTION

This report documents the results of a quality assurance review of data from woodcock liver tissue and earthworm tissue samples collected in support of the Hudson River Natural Resource Damage Assessment. The samples were analyzed for PCB congeners, PCB homologue groups, total PCBs, percent lipids, and percent moisture.

A total of two woodcock livers and ten earthworm composites were submitted for analysis. These samples were analyzed in one laboratory analytical batch. The tissues were prepped, extracted, and analyzed by the Woods Hole Group Environmental Laboratories (Raynham, Massachusetts) using laboratory Standard Operating Procedures (SOPs) that were submitted and reviewed prior to sample receipt.

2.0 DATA VALIDATION PROCEDURES

Data validation was based on the quality assurance/quality control (QA/QC) criteria documented in the Analytical Quality Assurance Plan for the Hudson River Natural Resource Damage Assessment, Version 1.0, July 9, 2002, and USEPA National Functional Guidelines for Organic Data Review, 1999, and the following laboratory SOPs:

• SOP # HR NRDA Project Tissue Prep: Tissue Preparation and Homogenization, Revision #1.0, 9/25/02

• SOP # OP-004: Extraction of Soil, Tissue, Vegetation, and Sediment by Pressurized Fluid Extraction, Revision #2.0, 8/15/02

• SOP # O-010: Determination of PCB Homologues and Individual Congeners by GC/MS - SIM, Revision # 2.2, 10/24/02

• SOP # HR NRDA % Lipids: Percent Lipids Determination, Revision # 0.0, 9/9/02

• SOP # W-001: Percent Solids Determination, Revision # 2.1, 9/25/02

• Additional cleanup, sample handling, storage, custody SOPs as necessary.

Sample results and related QC data were received in both an electronic and hard copy format. Electronic data were verified against the hard copy data package. All of the data received a full validation.



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The following QC elements were reviewed:

• Analytical holding times

• Chain of custody and sample handling

• GC/MS tune verification (from summary forms)

• Method blank contamination (from summary forms)

• Initial and continuing calibration (from summary forms)

• Analytical accuracy: surrogates, matrix spike samples, laboratory control samples, and standard reference material results (from summary forms)

• Analytical precision: laboratory duplicate samples (from summary forms)

• Internal standard areas (from summary forms)

• Reported detection limits (from sample result summaries)

• Compound identification (from raw data)

• Compound quantitation, transcription and calculation checks performed at a frequency of 10% from raw data. If an error was noted, 100% of the calculations and transcriptions for that data set were verified.

This report summarizes the results of data validation relative to the analytical data quality objectives (ADQO) for precision, accuracy, and completeness. The report also provides a quantitative and qualitative assessment of the data and identifies potential sources of error, uncertainty, and bias that may affect the overall usability.

Laboratory QC samples were used to assess the effectiveness of homogenization procedures and to evaluate laboratory-derived contamination, laboratory performance, and sample matrix effects. Quality control samples included: method blanks, laboratory control samples (LCS), matrix spike (MS) samples, laboratory duplicate samples, and standard reference material (SRM) analyses. Surrogates were added to each sample analyzed for PCB congeners to further assess the effects of sample matrix on accuracy.

Data were qualified when associated QC sample results were outside the QC limits. The following definitions provide brief explanations of the qualifiers assigned to results in the data validation process:



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J Estimated: The associated numerical value is an estimated quantity. The analyte was detected, but the reported value may not be accurate or precise. The “J” qualification indicates the data fell outside the QC limits, but the exceedance was not sufficient to cause rejection of the data.


3.0 DATA QUALITY ASSESSMENT

The data package submitted by the laboratory was reviewed to determine whether the analytical data quality objectives (ADQO) specified in Tables 6.1a - 6.1c in the Analytical Quality Assurance Plan were met. Each quality control element is discussed briefly below. More details are available in the individual data validation reports presented in Attachment A.

3.1 Holding Times and Sample Preservation

The primary analytes of concern for this study are persistent compounds, which have been found to remain stable in tissue after several years of storage. Due to this, no maximum holding time criterion was established. The woodcock liver tissues were extracted approximately two years after collection and the earthworm tissues were extracted approximately three years after collection. All extracts were analyzed within 30 days from sample extraction. Samples were kept frozen by the laboratory at the required temperature of -20oC ±2o.

3.2 Instrument Calibration

3.2.1 Initial Calibration (ICAL)

The ADQO specification for the initial calibration is that a minimum of a five point calibration would be performed for all analytes, and that the percent relative standard deviation (%RSD) values for all analytes are less than 20%.

All submitted ICAL data met the specified ADQO.

3.2.2 Continuing Calibration (CCAL)

The ADQO specified for the continuing (or daily) calibrations is that a CCAL must be analyzed at the beginning and end of each analytical sequence (or every 12 hours, whichever is more frequent), and that all percent difference (%D) values must be less than 20%.

All CCAL met the ADQO requirements.



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3.3 GC/MS Tune

GC/MS instrument tuning verifications were performed at the proper frequency, prior to each analytical sequence. All GC/MS tunes met the acceptance criteria specified in the laboratory standard operating procedures.

3.4 Blank Analyses

The method blank was acceptable, in that no target analytes were detected in the method blank.

3.5 Accuracy

Accuracy is evaluated by comparison of an analytical concentration to a known (true) value. Accuracy was monitored through the use of surrogate compounds in each sample, and SRM, MS, and laboratory control sample (blank spike) analyses. Each QC element is discussed below. Overall, accuracy was acceptable.

3.5.1 Surrogate Compounds

Two surrogate compounds, 13C-BZ#19 and 13C-BZ#202, were added to each sample prior to extraction.

The ADQO specified for surrogate compounds is that all percent recovery (%R) values would be within the 50% - 125% acceptance window. The recovery value from the late eluting surrogate (13C-BZ#202) is used for the quantitation of the reported target analyte concentrations.

All of the surrogate %R values were within the 50% - 125% control limits.

3.5.2 Standard Reference Material Analyses

An SRM was extracted and analyzed with the analytical batch. The SRM selected for this study was 1974b, Organics in Mussel Tissue. This SRM has certified values for 27 PCB congeners.

The ADQO for the SRM is that the reported value must be within ±20% of the 95% confidence interval of the true value, for analytes with values greater than five times the method detection limit (MDL).

The SRM accuracy results met the ADQO requirements.

Table 1 summarizes the SRM results for this study.



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3.5.3 Laboratory Control Samples

The laboratory performed laboratory control sample (LCS) analyses at the required frequency of one for every 15 samples or analytical batch, whichever was more frequent. The ADQO for the LCS analyses is that all %R values must be within the acceptance limits of 75% to 125%; however, if only one analyte %R value is outside the control limits, the laboratory is not required to re-extract the associated samples.

One LCS %R value (PCB189) was outside the 75% to 125% control limits. The LCS %R value was greater than the upper control limit, indicating a potential high bias. Associated positive results were estimated (J); reporting limits were judged as unaffected and no action was taken. Four data points were estimated based on this LCS %R outlier.

3.5.4 Matrix Spike Samples

The laboratory performed the MS analysis at the required frequency of one for every 15 samples or analytical batch. The MS sample included 47 spiked analytes. The ADQO for MS analyses is that all %R values should be within the 50% to 125% control limits. The ADQO does not apply if the concentration in the parent sample is greater than five times the concentration in the spiking solution.

A potential high bias was indicated by the recoveries for five compounds, as the %R values were greater than 125% (ranging from 129% to 433%). Positive results associated with an elevated MS %R value were estimated (J) to indicate a potential high bias. No action was taken if the compound was not detected. One data point (the detection limit for PCB123 in Sample EW-05) was associated with a 0% recovery value in the MS analysis. This data point was rejected (R).

Qualifiers were issued only to the target analyte in the parent sample associated with the MS %R outlier. Three data points were estimated (J). One data point (the detection limit for PCB123 in Sample EW-05) was rejected (R) due to a 0% recovery value in the MS analysis.

3.5.5 Internal Standards

Internal standards were added to each field and QC sample prior to injection onto the analytical instrument. The ADQO for internal standards is that the area of the internal standards in each analysis must be within ±50% of the area of the internal standard in the associated CCAL.

All internal standard areas met the ADQO.

3.6 Precision

Precision is evaluated through replicate analyses of a sample. For this study, a laboratory duplicate was analyzed with each analytical batch. No field duplicates were submitted. Overall, precision was judged as acceptable.



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3.6.1 Laboratory Duplicate Samples

For samples with positive results greater than or equal to five times the method detection limit, the ADQO specified relative percent difference (RPD) control limit for laboratory duplicates is 30%. One laboratory duplicate was submitted.

For the PCB congeners and homologue groups, one value (PCB47) was greater than 30% (at 33%). For percent lipids and percent moisture analyses, the RPD control limit is 15%. The percent moisture analyses RPD value met the ADQO, while the percent lipids RPD value (at 22%) exceeded the ADQO.

The target analyte associated with RPD outliers was estimated (J) in the parent sample. A total of two values were estimated due to laboratory precision outliers.

Table 2 summarizes the results of the laboratory duplicate analyses.

3.7 Reporting Limits and Sample Results

Method detection limits (MDLs) were determined using low level spikes in tissue from laboratory mice following procedures outlined in the US Code of Federal Regulations (40 CFR Part 136, Appendix B).

The detection limits for target congeners were generally in the range of 0.02 µg/Kg to 0.22 µg/Kg, with a co-elution of PCB31/28 at 1.38 g/Kg. There were 14 target congeners with MDL values greater than the 0.1 µg/Kg target MDL. The PCB31/28 co-elution MDL value was elevated due to interferences which could not be resolved using the selected method.

Chromatography and mass spectral identification were reviewed for a minimum of 10% of the reported congeners. No instances of potential interference were noted. All reported positive results met the identification criteria and chromatographic peak shapes were acceptable. All reported results were judged to be accurate unless qualified for some other reason.

3.8 Completeness

Out of 720 results reported by the laboratory (12 samples each with 47 congeners, ten homologue groups, total PCBs, percent lipids and percent moisture), a total of eight (1.1%) data points were qualified as estimated (J) and one data point was rejected (R). The completeness level attained for the analysis of the field samples is greater than 99.8%.

3.9 Summary of Data Usability

A total of eight out of 720 results were estimated because of laboratory accuracy and precision outliers. One data point was rejected due to a %R outlier. The rejected data point should not be



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used for any purpose. For all other data, the overall quality of the data is acceptable and the results, as qualified, are considered usable.



ATTACHMENT A

Data Validation Reports

by Sample Data Group (SDG)



A - 1

DATA VALIDATION REPORT - FULL REVIEW Hudson River

Polychlorinated Biphenyl Congeners, Lipids SDG: 0309077

Woods Hole Group This report documents the review of analytical data from the analysis of woodcock liver and earthworm tissue samples and the associated laboratory quality control samples. Samples were analyzed by Woods Hole Group Environmental Laboratories, Raynham, Massachusetts. The following table is a list of samples reviewed.

Field ID Laboratory ID Common Name EW-01 0309077-03 Earthworm composite EW-02 0309077-04 Earthworm composite EW-03 0309077-05 Earthworm composite EW-04 0309077-06 Earthworm composite EW-05 0309077-07 Earthworm composite EW-06 0309077-08 Earthworm composite EW-07 0309077-09 Earthworm composite EW-08 0309077-10 Earthworm composite EW-10 0309077-11 Earthworm composite EW-11 0309077-12 Earthworm composite

HRW-001 0309077-01 American Woodcock HRW-002 0309077-02 American Woodcock

I. DATA PACKAGE COMPLETENESS All required deliverables were submitted by the laboratory. The laboratory followed adequate corrective action processes, and all anomalies were discussed in the case narrative.

II. TECHNICAL DATA VALIDATION The quality control (QC) requirements that were reviewed are listed below.

GC/MS Instrument Performance Check Standard Reference Material Initial Calibration (ICAL) 2 Laboratory Duplicate

1 Continuing Calibration (CCAL) Internal Standards Blanks 1 Compound Identification Surrogate Compounds Calculation Verification

2 Matrix Spike (MS) 1 Reporting Limits and Sample Results 2 Laboratory Control Samples (LCS) Electronic Deliverable Transcription Check

___________________________________________________________ 1 Quality control results are discussed below, but no data were qualified. 2 Quality control outliers that impact the reported data were noted. Data qualifiers were issued as discussed below.



A - 2

Continuing Calibration (CCAL) The percent difference (%D) value for the monochlorobiphenyl homologue group was greater than the control limit of +20% in the CCAL standard analyzed October 6, 2003 at 10:58. Only dilution analyses were associated with this CCAL, and results for the monochlorobiphenyl homologue group were not reported from these analyses. No action was taken.

Matrix Spike Matrix spike (MS) analysis was performed using Sample EW-05. Target congeners were present in this sample at concentrations ranging from 0.71 µg/Kg to 662 µg/Kg, with many concentrations greater than 50 µg/Kg. If the concentration of the congener in the parent sample was greater than five times the spike concentration (9.56 µg/Kg), no qualifiers were assigned because the recovery results are masked by the high PCB concentrations in the sample.

Results for PCB18, PCB114, and PCB189 were estimated (J-8) in the parent sample as the percent recovery (%R) values were greater than 125%, but the concentrations in the parent sample were less than five times the spike amount. Recovery values for PCB77 and PCB81 were also greater than the control limit; however, these congeners were not detected in the parent sample. As the outliers indicate a potential high bias, the reporting limits were not affected. No action was taken. The value for PCB123 was rejected (R-8), as the %R value was 0%.

Laboratory Control Samples The %R value for PCB189 was greater than the 125% upper control limit in the laboratory control (LCS) sample associated with this SDG. Positive results for PCB189 were estimated (J-10) in the samples.

Laboratory Duplicate A laboratory duplicate was performed on Sample EW-07. The relative percent difference (RPD) value for congener PCB47 was greater than the 30% upper control limit (at 33%). The PCB47 value was estimated (J-9) in the parent sample.

The RPD value for the percent lipids determination was greater than the control limit of 15%, at 22%. The lipids result was estimated (J-9) in the parent sample.

Compound Identification Chromatography and mass spectral identification were reviewed for a minimum of 10% of all reported congeners. No instances of potential interference were noted. All reported positive results met the identification criteria and chromatographic peak shapes were acceptable.

Reporting Limits and Sample Results Samples EW-05, EW-06, EW-08, and EW-10 were analyzed at dilution due to levels of some congeners that were greater than the linear range of the calibration. Both the initial and the diluted



A - 3

analyses were reported. In order that only one set of data be reported, the results from the initial analysis that were greater than the linear range of the calibration were qualified do-not-report (DNR-20). Results for all compounds, except those qualified do-not-report in the initial analysis, were qualified do-not-report (DNR-14) in the dilution analyses.

For GCMS-SIM analysis, response factors are generated for each congener during the calibration process. The relative area of a peak is divided by the appropriate response factor to calculate the concentration of the congener. For the homologue groups (monochlorobiphenyl, dichlorobiphenyl, etc.), a representative response factor is used. For example, the response factor for PCB29 is used as the representative response factor for all trichlorobiphenyls.

In some cases, the reported trichlorobiphenyl and heptachlorobiphenyl homologue group total values were less than the sum of the individual congeners. This occurs because the representative response factor is sufficiently different from the target congener response factors generated during the calibration. For example, the response factor for the PCB31/28 co-elution (detected in most samples) is lower than the trichlorobiphenyl representative response factor. Since the areas are divided by the response factors, this results in a lower concentration for the total trichlorobiphenyls, even if PCB31/28 is the only detected congener in the chlorination level.

Unless all 209 congeners are calibrated, any reported total for a chlorination level will have some inherent variability. For example, for the trichlorobiphenyl and heptachlorobiphenyl results, the greatest difference between the calculated (by summing the congeners) and reported result is 2.1%. The differences for the Total Homologue values are all less than 1.0%. This is within the variability of the method, thus no action was taken.

III OVERALL ASSESSMENT

As was determined by this evaluation, the laboratory followed the specified analytical methods. Accuracy was acceptable, as demonstrated by the surrogate, LCS, standard reference material, and MS %R values, with the exceptions noted above. Precision was acceptable as demonstrated by the RPD values for the duplicate analyses, with the exceptions noted above.

Data were estimated due to MS and laboratory control sample %R outliers and laboratory precision outliers. One reporting limit was rejected due to a MS %R outlier. Data were qualified as do-not-report to indicate the usable result when multiple results were reported.

Data that has been rejected or qualified as do-not-report should not be used for any purpose. All other data, as qualified, are acceptable for use.

HUDSON RIVER



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DATA QUALITY ASSESSMENT REPORTHUDSON RIVER NATURAL RESOURCE

DAMAGE ASSESSMENT FLOODPLAIN STUDY

2001 SMALL MAMMALS TISSUE AND 2000 SHREWSAND SOILS

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DATA QUALITY ASSESSMENT REPORT

HUDSON RIVER NATURAL RESOURCE DAMAGE ASSESSMENT

FLOODPLAIN STUDY

2001 Small Mammals Tissue and

2000 Shrews and Soils

Prepared for: State of New York

Department of Environmental Conservation

U.S. Department of Commerce National Oceanic and Atmospheric Administration

U.S. Department of Interior Fish and Wildlife Service

February 19, 2004

Version 1.1

Data Quality Assessment 2001 Small Mammal and 2000 Shrew/Soils


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TABLE OF CONTENTS

1.0 INTRODUCTION ................................................................................1 2.0 DATA VALIDATION PROCEDURES.................................................1 3.0 DATA QUALITY ASSESSMENT........................................................3

3.1 Holding Times and Sample Preservation......................................................................3

3.2 Instrument Calibration....................................................................................................3 3.2.1 Initial Calibration (ICAL) ......................................................................................................... 3 3.2.2 Continuing Calibration (CCAL) ............................................................................................... 4

3.3 GC/MS Tune.....................................................................................................................4

3.4 Blank Analyses................................................................................................................4 3.4.1 Method Blanks........................................................................................................................ 4 3.4.2 Equipment Rinsate Blanks ..................................................................................................... 4

3.5 Accuracy ..........................................................................................................................5 3.5.1 Surrogate Compounds ........................................................................................................... 5 3.5.2 Standard Reference Material (SRM) Analyses ...................................................................... 5 3.5.3 Laboratory Control Samples................................................................................................... 6 3.5.4 Matrix Spike Samples............................................................................................................. 6 3.5.5 Internal Standards .................................................................................................................. 7

3.6 Precision ..........................................................................................................................7 3.6.1 Standard Reference Material (SRM) Analyses ...................................................................... 8 3.6.2 Laboratory Duplicate Samples ............................................................................................... 8

3.7 Reporting Limits and Sample Results...........................................................................8

3.8 Completeness..................................................................................................................9

3.9 Summary of Data Usability.............................................................................................9

Table 1A: Summary of Standard Reference Material Results

Table 1B: Summary of Standard Reference Material Results: Statistical Evaluation

Table 2: Small Mammal Laboratory Duplicate Relative Percent Difference Summary Attachment A Sample Index ............................................................................................. A-1 Attachment B Data Validation Reports by Sample Delivery Group (SDG) ................... B-1



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DATA QUALITY ASSESSMENT Hudson River Natural Resource Damage Assessment

Small Mammal Study

1.0 INTRODUCTION

This report documents the results of a quality assurance review of data from small mammal tissue samples collected in support of the Hudson River Natural Resource Damage Assessment. The samples were analyzed for PCB congeners, PCB homologue groups, total PCBs, percent lipids, and percent moisture. A list of the samples analyzed is provided in Attachment A.

A total of 61 shrews and 108 mice/voles were submitted for analysis. The mice were composited into 18 composites of five animals and one composite of four animals, and the voles were composited into two composites of five animals each and one composite of four animals. The total number of shrews and composites analyzed was 83, grouped into six analytical batches by the laboratory.

In addition to the small mammals that were collected in 2001, the laboratory also analyzed 18 soils and 12 shrews that were collected in 2000. The soils and shrew analyses were each reported in a separate analytical batch, and will be referred to as the ‘2000 analyses’ to differentiate from the small mammals collected in 2001. The same target analyte list was performed for the 2000 analyses and the 2001 small mammal analyses, except that percent lipids are not analyzed for the soil samples.

The mammal tissue and soils were prepped, extracted, and analyzed by the Woods Hole Group Environmental Laboratories (Raynham, Massachusetts) using laboratory Standard Operating Procedures (SOPs) that were submitted and reviewed prior to sample receipt.

2.0 DATA VALIDATION PROCEDURES

Data validation was based on the quality assurance/quality control (QA/QC) criteria documented in the Analytical Quality Assurance Plan for the Hudson River Natural Resource Damage Assessment, Version 1.0, July 9, 2002, and USEPA National Functional Guidelines for Organic Data Review, 1999, and the following Woods Hole Group Environmental Laboratories SOPs:

• SOP # HR NRDA Project Tissue Prep: Tissue Preparation and Homogenization, Revision #1.0, 9/25/02

• SOP # OP-004: Extraction of Soil, Tissue, Vegetation, and Sediment by Pressurized Fluid Extraction, Revision #2.0, 8/15/02

• SOP # O-010: Determination of PCB Homologues and Individual Congeners by GC/MS - SIM, Revision # 2.2, 10/24/02



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• SOP # HR NRDA % Lipids: Percent Lipids Determination, Revision # 0.0, 9/9/02

• SOP # W-001: Percent Solids Determination, Revision # 2.1, 9/25/02

• Additional cleanup, sample handling, storage, custody SOPs as necessary.

Sample results and related QC data were received in both an electronic and hard copy format. A minimum of 10% of all electronic data were verified against the hard copy data package. All of the 2001 small mammal data received a full validation. The 2000 analyses received a summary validation.

The following QC elements were reviewed for data packages undergoing summary validation:

• Analytical holding times

• Chain of custody and sample handling

• GC/MS tune verification (from summary forms)

• Method blank contamination (from summary forms)

• Initial and continuing calibration (from summary forms)

• Rinsate blank contamination (from sample result summaries)

• Analytical accuracy: surrogates, matrix spike samples, laboratory control samples, and standard reference material results (from summary forms)

• Analytical precision: laboratory duplicate samples (from summary forms)

• Internal standard areas (from summary forms)

• Reported detection limits (from sample result summaries)

Full validation included review of all the items listed above for summary validation, plus the following QC elements:

• Compound identification (from raw data)

• Compound quantitation, transcription and calculation checks performed at a frequency of 10% from raw data. If an error was noted, 100% of the calculations and transcriptions for that data set were verified.

This report summarizes the results of data validation relative to the analytical data quality objectives (ADQO) for precision, accuracy, and completeness. The report also provides a quantitative and



3

qualitative assessment of the data and identifies potential sources of error, uncertainty, and bias that may affect the overall usability.

Laboratory QC samples were used to assess the effectiveness of homogenization procedures and to evaluate laboratory-derived contamination, laboratory performance, and sample matrix effects. Quality control samples included: equipment rinsate blanks, method blanks, laboratory control samples (LCS), matrix spike (MS) samples, laboratory duplicate samples, and standard reference material (SRM) analyses. Surrogates were added to each sample analyzed for PCB congeners to further assess the affects of sample matrix on accuracy.

Data were qualified when associated QC sample results were outside the QC limits. The following definitions provide brief explanations of the qualifiers assigned to results in the data validation process:

J Estimated: The associated numerical value is an estimated quantity. The analyte was detected, but the reported value may not be accurate or precise. The “J” qualification indicates the data fell outside the QC limits, but the exceedance was not sufficient to cause rejection of the data.

UJ Estimated/Not detected: An analysis was performed for the compound or analyte, but it was not detected and the sample quantitation or detection limit may be inaccurate or imprecise. The associated numerical result is the detection limit.

NJ Tentatively Identified/Estimated: The analyte was tentatively identified and the associated numerical value is an estimated quantity.


3.0 DATA QUALITY ASSESSMENT

The data packages submitted by the laboratory were reviewed to determine whether the analytical data quality objectives (ADQO) specified in Tables 6.1a - 6.1c in the Analytical Quality Assurance Plan were met. Each quality control element is discussed briefly below. More details are available in the data validation reports for each data package presented in Attachment B.

3.1 Holding Times and Sample Preservation

The primary analytes of concern for this study are persistent compounds, which have been found to remain stable in tissue after several years of storage. Due to this, no maximum holding time criterion was established. For the small mammal tissues, all samples were extracted within 195 days of collection, and all extracts were analyzed within 30 days from sample extraction. The 2000 analyses were extracted over three years after collection, and analyzed within 32 days of sample extraction. Samples were kept frozen by the laboratory at the required temperature of -20oC ±2o.



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3.2 Instrument Calibration

3.2.1 Initial Calibration (ICAL)

The ADQO specification for the initial calibration is that a minimum of a five point calibration would be performed for all analytes, and that the percent relative standard deviation (%RSD) values for all analytes are less than 20%. Up to 10% of the analyte %RSD values can be greater than 20% provided that all %RSD values are less than 30%.

All submitted ICAL data met the ADQO. There were three %RSD values greater than 20% (but less than 30%) in the ICAL associated with the 2000 soil analyses. Positive results associated with %RSD outliers were estimated (J). Eighteen results (0.96% of the total of the 2000 analyses results) were qualified based on ICAL %RSD outliers.

3.2.2 Continuing Calibration (CCAL)

The ADQO for the continuing (or daily) calibrations is that a CCAL must be analyzed at the beginning and end of each analytical sequence (or every 12 hours, whichever is more frequent), and that all percent difference (%D) values should be less than 20%. Up to three %D values can be greater than 20%, provided that all %D values are less than 30%.

All CCAL met the ADQO requirements.

For the 2001 small mammal tissue analyses, one %D value was greater than 20% (but less than 30%) in six of the CCAL. These outliers were either associated only with quality control analyses (SRM, LCS, or MS), or the outlier indicated a potential high bias and the affected congener was not detected. No data were qualified based on CCAL %D outliers.

For the 2000 soil analyses, one to three %D values were greater than 20% (but less than 30%) in three of the CCAL. As the outliers indicated a potential low bias, positive results and the reporting limits for non-detected results associated with %D outliers were estimated (J/UJ). Twenty-three results (1.3% of the total of the 2000 analyses results) were qualified based on CCAL %D outliers.

3.3 GC/MS Tune

GC/MS instrument tuning verifications were performed at the proper frequency, prior to each analytical sequence. All GC/MS tunes met the acceptance criteria specified in the laboratory standard operating procedures.



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3.4 Blank Analyses

3.4.1 Method Blanks

All method blanks were acceptable, in that no target analytes were detected in any of the method blanks.

3.4.2 Equipment Rinsate Blanks

A total of six equipment rinsate blanks were collected with the small mammal tissues. The rinsate blanks were prepared by rinsing the equipment used to homogenize the small mammal tissue samples, and analyzing the rinsate.

There were no positive results for any target analytes in the rinsate blanks.

3.5 Accuracy

Accuracy is evaluated by comparison of an analytical concentration to a known (true) value. Accuracy was monitored through the use of surrogate compounds in each sample, and SRM, MS, and LCS (blank spike) analyses. Each QC element is discussed below. Overall, accuracy was acceptable for all small mammal analyses.

3.5.1 Surrogate Compounds

Two surrogate compounds, 13C-PCB19 and 13C-PCB202, were added to each sample prior to extraction.

The ADQO specified for surrogate compounds is that all percent recovery (%R) values be within the 50% - 125% acceptance window. The recovery value from the later eluting surrogate (13C-PCB202) is used for the quantitation of the reported target analyte concentrations.

All of the surrogate %R values were within the 50% - 125% control limits.


An SRM was extracted and analyzed with each analytical batch. The SRM selected for the small mammal tissues (including the 2000 shrew analyses) was 1974b, Organics in Mussel Tissue. This SRM has certified values for 27 of the target PCB congeners. One SRM analysis was submitted with each laboratory batch, so a total of seven SRM analyses (with 26 certified values each, for a total of 182 data points) were performed.

The ADQO for the SRM is that the reported value must be within ±20% of the 95% confidence interval of the true value for congeners whose concentration in the SRM is greater than five times the method detection limit (MDL). This ADQO was used by the laboratory to evaluate the reported



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results. However, during data validation, no data were qualified unless the reported value was greater than ±25% of the 95% confidence interval.

Overall, the small mammal tissue SRM accuracy results were acceptable. A total of 13 SRM results (7.1% of the total) were outside the ±20% control limit. Of the 13 outliers, four (2.2% of the total) were also outside the control limits established by ±25% of the 95% confidence interval. The four outliers were associated with the 2001 small mammal tissue analyses.

Three of these results were greater than the upper control limit (125% of the 95% confidence interval for an individual congener). The outliers were for each of the following congeners: PCB74, PCB138, and PCB180. The positive results associated with these three SRM outliers were estimated (J) to indicate a potential high bias. The result for one data point, for congener PCB158, was less than the lower control limit (75% of the 95% confidence interval). Both positive results and reporting limits associated with this outlier were estimated (J/UJ), indicating a potential low bias for positive results, or a potential that the detection limit may be elevated. Fifty-three results (1.1% of the 2001 small mammal results) in the small mammal tissue samples were estimated based on these SRM outliers.

The SRM selected for the 2000 soil analyses was 1944, New York/New Jersey Waterway Sediment. This SRM has certified values for 28 of the target PCB congeners. One SRM analysis was submitted, for a total of 28 data points.

Eleven SRM results were outside the ±20% control limit, and also outside the ±25% control limit. Seven of these results were greater than the upper control limit (125% of the 95% confidence interval for an individual congener). The outliers were for each of the following congeners: PCB31/28, PCB52, PCB118, PCB128, PCB138, PCB180, and PCB183. The positive results associated with these SRM outliers were estimated (J) to indicate a potential high bias. Four SRM results (for congeners PCB105, PCB194, PCB195, and PCB206) were less than the lower control limit (75% of the 95% confidence interval). Both positive results and reporting limits associated with these outliers were estimated (J/UJ), indicating a potential low bias for positive results, or a potential that the detection limit may be elevated. For the 2000 analyses, 197 results (11.1% of the total) were qualified based on SRM outliers.

Tables 1A and 1B summarize the small mammal SRM results for this study.

3.5.3 Laboratory Control Samples

The laboratory performed LCS analyses at the required frequency of one for every 15 samples or analytical batch, whichever was more frequent. The ADQO for the LCS analyses is that all %R values must be within the acceptance limits of 75% to 125%; however, if only one analyte %R value is outside the control limits, the laboratory is not required to re-extract the associated samples.

A total of six LCS analyses were submitted with the 2001 small mammal samples. Each LCS included 47 target analytes, for a total of 282 data points (%R values). One LCS %R value was outside the 75% to 125% control limits. The LCS %R value was greater than the upper control limit



7

and there were no associated positive results. Reporting limits were judged as unaffected and no action was taken.

Two LCS analyses were submitted with the 2000 analyses. Each LCS included 47 target analytes, for a total of 94 data points (%R values). One LCS %R value was outside the 75% to 125% control limits. The LCS %R value was less than the lower control limit. The associated positive results and reporting limits for non-detected results were estimated (J/UJ) due to the potential low bias. Eighteen data points (1.0% of the total for the 2000 analyses) were qualified based on LCS outliers.

3.5.4 Matrix Spike Samples

The laboratory performed MS analyses at the required frequency of one for every 15 samples or analytical batch. For the 2001 small mammal analyses, a total of six MS analyses were submitted. Each MS sample included 47 spiked analytes, for a total of 282 data points. The ADQO for MS analyses is that all %R values should be within the 50% to 125% control limits. The ADQO does not apply if the concentration in the parent sample is greater than five times the concentration in the spiking solution.

A potential low bias was indicated by 17 of the MS %R values, as the %R values were less than 50% (ranging from 0% to 44%). A potential high bias was indicated by the recoveries for 32 compounds, as the %R values were greater than 125% (ranging from 126% to 1857%).

Positive results associated with an elevated MS %R value were estimated (J) to indicate a potential high bias. No action was taken if the compound was not detected. Target analyte results, both detected and non-detects, associated with MS %R values less than the 50% lower control limit were estimated (J/UJ). One data point (the detection limit for PCB123 in Sample 17-03-101001) was associated with a 0% recovery value in the MS analysis. This data point was rejected (R).

Qualifiers were issued only to the target analyte in the parent sample associated with the MS %R outlier. A total of 45 data points (0.9% of the 2001 small mammal data points) were estimated (J/UJ). One data point (the detection limit for PCB123 in Sample 17-03-101001) was rejected (R) due to a 0% recovery value in the MS analysis.

For the 2000 analyses, one MS was submitted. A spiked sample analysis was not performed for the 2000 shrew analyses due to limited sample volume. For the soil MS, a potential high bias was indicated by the recoveries for six compounds, as the %R values were greater than 125% (ranging from 130% to 149%). These compounds were estimated (J) in the parent sample. One data point (the detection limit for PCB123 in Sample 7-1-B15) was associated with a 0% recovery value in the MS analysis. This data point was rejected (R). Seven data points (0.7% of the 2000 soil data points) were qualified based on MS accuracy outliers.



8

3.5.5 Internal Standards

Internal standards were added to each field and QC sample prior to injection onto the analytical instrument. The ADQO for internal standards is that the area of the internal standards in each analysis must be within ±50% of the area of the internal standard in the associated CCAL.

For the 2001 small mammal analyses, all internal standard recoveries met the ADQO. For the 2000 analyses, the areas of both internal standards were greater than the upper control limit in two soil samples (7-1-B25 and 7-1-F25). Associated positive results were estimated (J). A total of 87 data points (4.9% of the 2000 analyses total) were qualified based on internal standard outliers.

3.6 Precision

Precision is evaluated through replicate analyses of a sample. For the small mammal study, a SRM and a laboratory duplicate were analyzed with each analytical batch. No field duplicates were submitted. For the 2000 analyses, a laboratory duplicate analysis was not performed for the shrew analyses due to insufficient sample volume. A laboratory duplicate was analyzed with the soils.

Overall, precision was judged as acceptable for all analyses.


Section 3.5.2 describes the frequency and criteria for the SRM analyses performed with each analytical batch. The results for the small mammal tissue (including the 2000 shrews) SRM analyses are summarized in Tables 1A and 1B.

The average percent difference (%D) from the certified values for the small mammal SRM results ranged from 0.81% to 34% for each of the congeners with values greater than five times the MDL. Most %D values are less than 10%, indicating good overall precision among analytical batches.

3.6.2 Laboratory Duplicate Samples

For samples with positive results greater than or equal to five times the method detection limit (MDL), the AQDO specified relative percent difference (RPD) control limit for laboratory duplicates is 30%. Seven laboratory duplicates (six for the 2001 small mammal analyses, one for the 2000 soil analyses) were submitted.

Table 2 summarizes the results of the laboratory duplicate analyses. For the PCB congeners and homologue groups, a total of ten RPD values (out of 327 possible) were greater than 30%. Six of the RPD outliers were in the laboratory duplicate performed using Sample 21-02-092201 (associated with laboratory batch 0308030), which may indicate matrix effects specific to that sample.

For percent lipids and percent moisture analyses, the RPD control limit is 15%. For percent lipids, two (out of six possible) of the RPD values are greater than 15%.



9

Target analytes associated with RPD outliers were estimated (J) in the parent sample. A total of 12 data points were estimated due to laboratory precision outliers.

3.7 Reporting Limits and Sample Results

MDLs were determined using low level spikes in tissue from laboratory mice, following procedures outlined in the US Code of Federal Regulations (40 CFR Part 136, Appendix B).

For the small mammal analyses (including the 2000 shrew analyses), the detection limits for target congeners were generally in the range of 0.02 µg/Kg to 0.22 µg/Kg, with a co-elution of PCB31/28 at 1.38 g/Kg. There were 14 target congeners with MDL values greater than the 0.1 µg/Kg target MDL. The PCB31/28 co-elution MDL value was elevated due to interferences which could not be resolved using the selected method.

For the 2000 soil analyses, the detection limits for target congeners were in the range of 0.010 µg/Kg to 0.160 µg/Kg. There were four target congeners with MDL values greater than the 0.1 µg/Kg target MDL.

The separation and spectral fit for any positive result for the coplanar congeners (PCB77, PCB81, PCB126, and PCB169) were evaluated. PCB87 was found to interfere with PCB81 and PCB110 was found to interfere with PCB77. The spectra for PCB126 indicates an overall poor spectral fit. There appears to be some interference but the source of the interference could not be determined. The interference does not appear to be a PCB congener. Although not a coplanar congener, interference was also noted for PCB123. PCB149 interferes with the spectra for PCB123.

The spectral match met general identification criteria for these congeners, so the laboratory correctly reported the results as positive results. However, due to the interference, the results may be false positives or may be biased high. The potential interferences cannot be resolved without further extract cleanup (e.g., carbon column cleanup). Thus, all positive results for these congeners (PCB77, PCB81, PCB123, and PCB126) are qualified as tentatively identified at an estimated concentration (NJ).

Chromatography and mass spectral identification were reviewed for a minimum of 10% of the other reported congeners. No other instances of potential interference were noted. All reported positive results met the identification criteria and chromatographic peak shapes were acceptable. All other reported results were judged to be accurate unless qualified for some other reason.

3.8 Completeness

For the 2001 small mammal analyses, one data point was rejected out of 4980 results reported by the laboratory (83 samples, each with 47 congeners, 10 homologue groups, total PCBs, percent lipids and percent moisture). The completeness level attained for the analysis of the field samples is greater than 99.99%.



10

For the 2000 analyses, one data point was rejected out of 1770 results reported by the laboratory (30 samples, each with 47 congeners, 10 homologue groups, and total PCBs; percent lipids for the 12 shrew samples; and percent moisture for the 18 soils). The completeness level attained for the analysis of the 2000 samples is greater than 99.94%.

3.9 Summary of Data Usability

For the 2001 small mammal data, a total of 128 out of 4980 results (2.57%) were estimated because of laboratory accuracy and precision outliers. One data point was rejected based on an accuracy outlier. The rejected data point should not be used for any purpose. For all other data, the overall quality of the data is acceptable and all results, as qualified, are considered usable.

For the 2000 analyses data, a total of 333 out of 1770 results (18.8%) were estimated because of laboratory accuracy and precision outliers. One data point was rejected based on an accuracy outlier. The rejected data point should not be used for any purpose. For all other data, the overall quality of the data is acceptable and all results, as qualified, are considered usable.



11

TABLE 1-A: SUMMARY OF STANDARD REFERENCE MATERIAL ANALYTICAL RESULTS Standard Reference Material 1974b - Organic in Mussel Tissue (Mytilus edulis) Concentrations are ng/g, wet weight

SDG 0308027 0308028 0308029 0308030 0308031 0308032 2000 Shrews

0311027 True Value Uncertainty +/- 25% Limits

ng/g PCB Congener ng/g ng/g ng/g ng/g ng/g ng/g ng/g ng/g (+/-) From To PCB18 0.945 0.839 1.10 0.939 0.948 0.867 0.685 0.84 0.13 0.50 1.18 PCB28/31 7.46 6.57 6.79 7.73 8.23 6.60 7.23 6.31 0.48 4.25 8.37 PCB44 3.99 3.80 3.88 4.23 3.59 4.11 3.55 3.85 0.20 2.69 5.01 PCB49 4.47 4.23 4.24 4.50 4.90 4.65 4.27 5.66 0.23 4.02 7.31 PCB52 7.10 6.07 6.10 6.26 6.73 6.20 6.04 6.26 0.37 4.33 8.20 PCB66 6.65 5.77 5.64 6.23 6.17 5.67 5.62 6.37 0.37 4.41 8.33 PCB70 6.84 6.18 6.32 6.70 5.76 6.38 4.70 6.01 0.22 4.29 7.73 PCB74 4.76 3.27 3.64 4.01 3.88 3.87 4.08 3.55 0.23 2.43 4.67 PCB87 5.66 4.87 4.79 5.01 5.10 5.08 4.64 4.33 0.36 2.89 5.77 PCB95 5.76 4.89 5.28 5.59 6.03 5.40 5.36 6.04 0.36 4.17 7.91 PCB99 7.06 5.25 5.05 5.09 5.71 5.33 5.57 5.92 0.27 4.17 7.67 PCB101 11.6 10.5 10.4 11.4 12.1 11.3 11.7 10.70 1.10 6.93 14.5 PCB105 4.99 4.14 4.01 4.18 4.15 4.17 3.82 4.00 0.18 2.82 5.18 PCB110 9.58 8.51 8.53 9.16 9.62 8.84 8.04 10.0 0.70 6.80 13.2 PCB118 13.3 11.2 10.9 11.2 10.9 10.1 9.73 10.3 0.40 7.33 13.3 PCB128 1.97 1.65 1.65 1.61 1.77 1.55 1.48 1.79 0.12 1.22 2.36 PCB138 13.9 11.9 11.4 11.9 13.0 11.3 12.9 9.20 1.40 5.50 12.9 PCB146 2.06 1.79 1.73 1.99 1.92 1.70 1.71 1.92 0.16 1.28 2.56 PCB149 6.44 6.03 5.94 6.48 6.69 6.00 5.41 7.01 0.28 4.98 9.04 PCB151 1.76 1.82 1.89 2.13 1.97 1.68 1.66 1.86 0.16 1.24 2.49 PCB153 12.7 10.8 10.6 11.1 12.1 10.8 9.83 12.3 0.80 8.43 16.2 PCB156 0.893 0.761 0.764 0.713 0.726 0.677 0.732 0.72 0.08 0.46 0.98 PCB158 0.966 0.746 0.727 0.794 0.871 0.623 0.692 1.00 0.096 0.65 1.34 PCB170* 0.521 0.554 0.500 0.372 0.371 0.376 0.439 0.27 0.034 0.17 0.37 PCB180 1.72 1.30 1.09 1.16 1.14 1.01 1.28 1.17 0.10 0.78 1.56 PCB183 1.25 1.10 1.09 1.14 1.22 1.13 1.08 1.25 0.03 0.91 1.59 PCB187 3.35 2.64 2.62 2.66 2.90 2.62 2.67 2.94 0.15 2.06 3.83 SDG = Sample Delivery Group, also called analytical batch *The "True Value" for PCB170 is less than five times the MDL. The acceptance criteria do not apply. Shaded values are outside the acceptance criteria



12

TABLE 1-B: SUMMARY OF STANDARD REFERENCE MATERIAL RESULTS: STATISTICAL EVALUATION Standard Reference MateriaL 1974b - Organic in Mussel Tissue (Mytilus edulis) Concentrations are ng/g, wet weight

True Value Uncertainty +/- 25% Limits

ng/g Average Result

Minimum Result

Maximum Result Number of Number of

Standard Deviaton

Average vs. True

PCB Congener ng/g From To ng/g ng/g ng/g Analyses Outliers (n-1) %D PCB18 0.84 0.13 0.50 1.18 0.90 0.69 1.10 7 0 0.09 -7.5 PCB28/31 6.31 0.48 4.25 8.37 7.23 6.57 8.23 7 0 0.68 -14.6 PCB44 3.85 0.2 2.69 5.01 3.88 3.55 4.23 7 0 0.23 -0.74 PCB49 5.66 0.23 4.02 7.31 4.47 4.23 4.90 7 0 0.25 21.1 PCB52 6.26 0.37 4.33 8.20 6.36 6.04 7.10 7 0 0.41 -1.55 PCB66 6.37 0.37 4.41 8.33 5.96 5.62 6.65 7 0 0.40 6.37 PCB70 6.01 0.22 4.29 7.73 6.13 4.70 6.84 7 0 0.38 -1.93 PCB74 3.55 0.23 2.43 4.67 3.93 3.27 4.76 7 1 0.49 -10.7 PCB87 4.33 0.36 2.89 5.77 5.02 4.64 5.66 7 0 0.31 -16.0 PCB95 6.04 0.36 4.17 7.91 5.47 4.89 6.03 7 0 0.40 9.39 PCB99 5.92 0.27 4.17 7.67 5.58 5.05 7.06 7 0 0.76 5.74 PCB101 10.70 1.10 6.93 14.48 11.29 10.40 12.10 7 0 0.66 -5.47 PCB105 4.00 0.18 2.82 5.18 4.21 3.82 4.99 7 0 0.36 -5.21 PCB110 10.0 0.70 6.80 13.20 8.90 8.04 9.62 7 0 0.49 11.03 PCB118 10.3 0.4 7.33 13.28 11.05 9.73 13.30 7 0 1.07 -7.25 PCB128 1.79 0.12 1.22 2.36 1.67 1.48 1.97 7 0 0.15 6.78 PCB138 9.20 1.40 5.50 12.90 12.33 11.30 13.90 7 2 1.02 -34.0 PCB146 1.92 0.16 1.28 2.56 1.84 1.70 2.06 7 0 0.15 4.02 PCB149 7.01 0.28 4.98 9.04 6.14 5.41 6.69 7 0 0.31 12.4 PCB151 1.86 0.16 1.24 2.49 1.84 1.66 2.13 7 0 0.16 0.84 PCB153 12.3 0.80 8.43 16.18 11.13 9.83 12.70 7 0 0.85 9.49 PCB156 0.72 0.08 0.46 0.98 0.75 0.68 0.89 7 0 0.07 -4.78 PCB158 1.00 0.096 0.65 1.34 0.77 0.62 0.97 7 1 0.12 22.5 PCB170* 0.27 0.034 0.17 0.37 0.45 0.37 0.55 7 NA 0.09 -66.4 PCB180 1.17 0.1 0.78 1.56 1.24 1.01 1.72 7 1 0.26 -6.23 PCB183 1.25 0.03 0.91 1.59 1.14 1.08 1.25 7 0 0.07 8.46 PCB187 2.94 0.15 2.06 3.83 2.78 2.62 3.35 7 0 0.29 5.44 %D = [(True Value - Average Result) / True Value] X 100 *The "True Value" for PCB170 is less than five times the MDL. The acceptance criteria do not apply.



13

TABLE 2: SMALL MAMMAL LABORATORY DUPLICATE RELATIVE PERCENT DIFFERENCE SUMMARY

SDG:

0308027 7-12-

091301

0308028 16-08-091801

030802917-03-101001

030803021-02-092201

0308031Comp of

Sta 1

0308032 Comp of Sta

20

Average RPD ( % )

Number of Results

Number of Results >30%

ANALYTE 17 17 9 63 8 21 22.5 6 1 PCB31/28 18 20 9 7 - 5 11.8 5 - PCB44 114 - - - - - 114 1 1 PCB45 13 11 5 17 3 16 10.8 6 - PCB47 15 2 27 2 13 1 10.0 6 - PCB49 17 29 11 13 18 11 16.5 6 - PCB52 17 5 9 14 6 3 9.00 6 - PCB56 17 7 18 17 8 10 12.8 6 - PCB66 46 4 8 16 18 5 16.2 6 1 PCB70 17 2 18 16 4 10 11.2 6 - PCB74 13 7 8 16 8 7 9.83 6 - PCB87 18 5 10 31 4 5 12.2 6 1 PCB95 17 6 17 15 7 9 11.8 6 - PCB99 14 10 10 8 5 6 8.83 6 - PCB101 15 6 11 18 8 14 12.0 6 - PCB105 15 17 10 36 13 1 15.3 6 1 PCB110 14 4 11 14 21 12 12.7 6 - PCB114 18 6 16 17 6 12 12.5 6 - PCB118 19 - - - - - 19.0 1 - PCB126 17 39 15 35 10 7 20.5 6 2 PCB128 18 4 18 16 9 14 13.2 6 - PCB138 15 5 11 15 10 12 11.3 6 - PCB146 21.7 13 11 21 7 16 15.0 6 - PCB149 6 10 21 15 - 13.0 4 - PCB151 17 6 15 17 11 14 13.3 6 - PCB153 10 4 5 16 12 20 11.2 6 - PCB156 15 3 9 20 8 6 10.2 6 - PCB157 9 21 16 28 24 16 19.0 6 - PCB158 12 8 22 22 9 3 12.7 6 - PCB167 14 1 4 - 7 18 8.80 5 - PCB170 6 - 6 - 7 - 6.33 3 - PCB174 16 1 10 9 13 22 11.8 6 - PCB177 15 10 16 15 11 12 13.2 6 - PCB180 17 0 13 20 12 17 13.2 6 - PCB183 15 6 10 16 8 13 11.3 6 - PCB187 8 2 1 18 10 13 8.67 6 - PCB194 2 15 3 37 2 2 10.2 6 1 PCB195 14 3 6 12 19 24 13.0 6 - PCB201 14 1 4 18 14 12 10.5 6 - PCB206 17 1 8 26 16 18 14.3 6 - PCB209 16 - 8 21 - - 15.0 3 - Dichlorobiphenyls 14 3 9 61 25 15 21.2 6 1 Trichlorobiphenyls 12 6 6 12 1 16 8.83 6 - Tetrachlorobiphenyls 15 6 8 15 12 19 12.5 6 - Pentachlorobiphenyls 15 5 7 15 8 16 11.0 6 - Hexachlorobiphenyls 18 22 5 1 12 15 12.2 6 - Heptachlorobiphenyls 8 3 2 14 3 27 9.50 6 - Octachlorobiphenyls 8 0 9 10 14 26 11.2 6 - Nonachlorobiphenyls 17 1 8 26 16 18 14.3 6 - Decachlorobiphenyl 12 0 5 19 22 5 10.5 6 2 Percent Lipids 2 2 3 1 0 1 1.50 6 - Percent Moisture 286 11 Blank spaces indicate no RPD result, meaning the analyte is not detected in the parent sample and/or duplicate, or both reported values were less than 5 times the MDL. Note: RPD outliers are presented in bold. The RPD control limit for PCBs is 30%, and for percent lipids and percent moisture is 15%. For SDG 0308027 the percent moisture laboratory duplicate was performed on a separate sample, 1-06-090501.

ATTACHMENT A

Sample Index



A - 1

2001 Small Mammal Tissue Sample Index FIELD ID LABORATORY ID SPECIES COMMON NAME

1-06-090501 0308027-01 Blarina brevicauda Short-Tailed Shrew 1-16-090701 0308027-02 Blarina brevicauda Short-Tailed Shrew 1-17-090801 0308027-03 Blarina brevicauda Short-Tailed Shrew 1-18-090901 0308027-04 Blarina brevicauda Short-Tailed Shrew 1-19-090901 0308027-05 Blarina brevicauda Short-Tailed Shrew 7-03-091201 0308027-06 Blarina brevicauda Short-Tailed Shrew 7-06-091201 0308027-07 Blarina brevicauda Short-Tailed Shrew 7-12-091301 0308027-08 Blarina brevicauda Short-Tailed Shrew 7-13-091301 0308027-09 Blarina brevicauda Short-Tailed Shrew 7-16-091401 0308027-10 Blarina brevicauda Short-Tailed Shrew 8-07-091301 0308027-11 Blarina brevicauda Short-Tailed Shrew 8-12-091301 0308027-12 Blarina brevicauda Short-Tailed Shrew 8-14-091301 0308027-13 Blarina brevicauda Short-Tailed Shrew 8-20-091401 0308027-14 Blarina brevicauda Short-Tailed Shrew 8-23-091501 0308027-15 Blarina brevicauda Short-Tailed Shrew 13-03-092201 0308028-01 Blarina brevicauda Short-Tailed Shrew 13-06-092201 0308028-02 Blarina brevicauda Short-Tailed Shrew 13-08-092301 0308028-03 Blarina brevicauda Short-Tailed Shrew 13-12-092401 0308028-04 Blarina brevicauda Short-Tailed Shrew 13-14-092601 0308028-05 Blarina brevicauda Short-Tailed Shrew 15-05-091801 0308028-06 Blarina brevicauda Short-Tailed Shrew 15-11-091901 0308028-07 Blarina brevicauda Short-Tailed Shrew 15-12-091901 0308028-08 Blarina brevicauda Short-Tailed Shrew 15-16-091901 0308028-09 Blarina brevicauda Short-Tailed Shrew 15-17-092001 0308028-10 Blarina brevicauda Short-Tailed Shrew 15-21-092001 0308028-11 Blarina brevicauda Short-Tailed Shrew 15-22-092001 0308028-12 Blarina brevicauda Short-Tailed Shrew 16-05-091801 0308028-13 Blarina brevicauda Short-Tailed Shrew 16-08-091801 0308028-14 Blarina brevicauda Short-Tailed Shrew 16-11-091901 0308028-15 Blarina brevicauda Short-Tailed Shrew 16-12-091901 0308029-01 Blarina brevicauda Short-Tailed Shrew 16-13-091901 0308029-02 Blarina brevicauda Short-Tailed Shrew 16-17-092001 0308029-03 Blarina brevicauda Short-Tailed Shrew 16-18-092001 0308029-04 Blarina brevicauda Short-Tailed Shrew 17-03-101001 0308029-05 Blarina brevicauda Short-Tailed Shrew 17-04-101001 0308029-06 Blarina brevicauda Short-Tailed Shrew 17-07-101001 0308029-07 Blarina brevicauda Short-Tailed Shrew 17-09-101401 0308029-08 Blarina brevicauda Short-Tailed Shrew 17-13-101501 0308029-09 Blarina brevicauda Short-Tailed Shrew 18-08-092101 0308029-10 Blarina brevicauda Short-Tailed Shrew 18-09-092101 0308029-11 Blarina brevicauda Short-Tailed Shrew 18-15-092201 0308029-12 Blarina brevicauda Short-Tailed Shrew



A - 2

FIELD ID LABORATORY ID SPECIES COMMON NAME 20-14-101001 0308029-13 Blarina brevicauda Short-Tailed Shrew 20-29-101101 0308029-14 Blarina brevicauda Short-Tailed Shrew 20-31-101101 0308029-15 Blarina brevicauda Short-Tailed Shrew 21-02-092201 0308030-01 Blarina brevicauda Short-Tailed Shrew 21-03-092201 0308030-02 Blarina brevicauda Short-Tailed Shrew 21-06-092201 0308030-03 Blarina brevicauda Short-Tailed Shrew 21-18-092601 0308030-04 Blarina brevicauda Short-Tailed Shrew 22-15-101601 0308030-05 Blarina brevicauda Short-Tailed Shrew 22-21-101701 0308030-06 Blarina brevicauda Short-Tailed Shrew 22-22-101701 0308030-07 Blarina brevicauda Short-Tailed Shrew 22-24-101801 0308030-08 Blarina brevicauda Short-Tailed Shrew 23-06-101501 0308030-09 Blarina brevicauda Short-Tailed Shrew 23-09-101601 0308030-10 Blarina brevicauda Short-Tailed Shrew 23-11-101701 0308030-11 Blarina brevicauda Short-Tailed Shrew 23-12-101701 0308030-12 Blarina brevicauda Short-Tailed Shrew 23-16-101801 0308030-13 Blarina brevicauda Short-Tailed Shrew 23-19-101801 0308030-14 Blarina brevicauda Short-Tailed Shrew 23-20-101801 0308030-15 Blarina brevicauda Short-Tailed Shrew 23-21-101801 0308031-01 Blarina brevicauda Short-Tailed Shrew Comp of Sta 1 0308031-02 Peromyscus spp. Mouse spp. Comp of Sta 3 0308031-03 Peromyscus spp. Mouse spp. Comp of Sta 4 0308031-04 Peromyscus spp. Mouse spp. Comp of Sta 5 0308031-05 Peromyscus spp. Mouse spp. Comp of Sta 6 0308031-06 Peromyscus spp. Mouse spp. Comp of Sta 7 0308031-07 Peromyscus spp. Mouse spp. Comp of Sta 8 0308031-08 Peromyscus spp. Mouse spp. Comp of Sta 10 0308031-09 Peromyscus spp. Mouse spp. Comp of Sta 11 0308031-10 Peromyscus spp. Mouse spp. Comp of Sta 12 (mouse) 0308031-11 Peromyscus spp. Mouse spp. Comp of Sta 13 0308031-12 Peromyscus spp. Mouse spp. Comp of Sta 15 0308031-13 Peromyscus spp. Mouse spp. Comp of Sta 16 0308031-14 Peromyscus spp. Mouse spp. Comp of Sta 17 0308031-15 Peromyscus spp. Mouse spp. Comp of Sta 18 0308032-01 Peromyscus spp. Mouse spp. Comp of Sta 20 (mouse) 0308032-02 Peromyscus spp. Mouse spp. Comp of Sta 21 0308032-03 Peromyscus spp. Mouse spp. Comp of Sta 22 0308032-04 Peromyscus spp. Mouse spp. Comp of Sta 23 0308032-05 Peromyscus spp. Mouse spp. Comp of Sta 2 0308032-06 Microtus Meadow Vole Comp of Sta 12 (vole) 0308032-07 Microtus Meadow Vole Comp of Sta 20 (vole) 0308032-08 Microtus Meadow Vole



A - 3

2000 Small Mammal and Tissue Sample Index FIELD ID LABORATORY ID SPECIES COMMON NAME

01-01-091000-10-S-STS 0311027-01 Blarina brevicauda Short-Tailed Shrew 01-02-091300-15-S-STS 0311027-02 Blarina brevicauda Short-Tailed Shrew 01-03-091300-10-S-STS 0311027-03 Blarina brevicauda Short-Tailed Shrew 07-01-091200-35-S-STS 0311027-04 Blarina brevicauda Short-Tailed Shrew 07-02-091200-35-S-STS 0311027-05 Blarina brevicauda Short-Tailed Shrew 07-03-091200-17-S-STS 0311027-06 Blarina brevicauda Short-Tailed Shrew 07-04-091200-8-S-STS 0311027-07 Blarina brevicauda Short-Tailed Shrew 08-01-091200-33-S-STS 0311027-08 Blarina brevicauda Short-Tailed Shrew 08-02-091200-6-S-STS 0311027-09 Blarina brevicauda Short-Tailed Shrew 08-03-091200-3-S-STS 0311027-10 Blarina brevicauda Short-Tailed Shrew 08-04-091300-33-S-STS 0311027-11 Blarina brevicauda Short-Tailed Shrew 08-05-091300-6-S-STS 0311027-12 Blarina brevicauda Short-Tailed Shrew 7-1-A15 0309086-01 NA Sediment 7-1-B15 0309086-02 NA Sediment 7-1-B25 0309086-03 NA Sediment 7-1-C15 0309086-04 NA Sediment 7-1-D15 0309086-05 NA Sediment 7-1-F25 0309086-06 NA Sediment 8-1-A15 0309086-07 NA Sediment 8-1-B15 0309086-08 NA Sediment 8-1-B25 0309086-09 NA Sediment 8-1-B35 0309086-10 NA Sediment 1-1-A15 0309086-11 NA Sediment 1-1-B15 0309086-12 NA Sediment 1-1-B25 0309086-13 NA Sediment 1-1-B35 0309086-14 NA Sediment 1-1-C15 0309086-15 NA Sediment 1-1-D25 0309086-16 NA Sediment 10-1-B15 0309086-17 NA Sediment 11-1-A25 0309086-18 NA Sediment

ATTACHMENT B

Data Validation Reports

by Sample Delivery Group (SDG)



B - 1



Woods Hole Group

This report documents the review of analytical data from the analysis of small mammal (shrew) tissue samples and the associated laboratory quality control samples. Samples were analyzed by Woods Hole Group Environmental Laboratories, Raynham, Massachusetts.

I. DATA PACKAGE COMPLETENESS The laboratory followed adequate corrective action processes, and all anomalies were discussed in the case narrative. All deliverables were submitted by the laboratory, with the following exceptions:

• The case narrative was not signed and dated, and second and third pages of the quantitation report for the continuing calibration (CCAL) standard analyzed September 4, 2003 at 10:54 were missing from the data package. The laboratory was contacted, and provided a signed narrative and the missing data. No further action was necessary.

II. TECHNICAL DATA VALIDATION

The quality control (QC) requirements that were reviewed are listed below.

GC/MS Instrument Performance Check 2 Standard Reference Material (SRM) Initial Calibration (ICAL) 2 Laboratory Duplicate


2 Matrix Spike (MS) 2 Reporting Limits and Sample Results Laboratory Control Samples (LCS) EDD Transcription Check


Continuing Calibration (CCAL) The percent difference (%D) values of PCB123 were outside the control limit of +20% in the two CCAL analyzed September 4, 2003. Only a dilution of Sample 8-07-0091301 was associated with the CCAL. PCB123 was not reported from the dilution. No qualifiers were necessary.



B - 2

Matrix Spike (MS) Matrix spike analysis was performed using Sample 7-12-091301. Target congeners were present in this sample at concentrations ranging from 1.12 µg/Kg to 508 µg/Kg, with most concentrations greater than 50 µg/Kg. If the concentration of the congener in the parent sample was greater than five times the spike concentration (9.31 µg/Kg), no qualifiers were assigned because the recovery results were masked by the high PCB concentration in the sample.

Results for PCB44, PCB95, PCB149, PCB156, PCB167, PCB177, and PCB183 were estimated (J-8) in the parent sample (7-12-091301) as the %R values were greater than 125%, but the concentrations in the parent sample were less than five times the spike amount. Results for PCB194, PCB195, PCB206, and PCB209 were estimated (J-8) as the %R values were less than the 50% lower control limit.

Although 11 data points were estimated, it is possible that the outliers are due to the overall matrix interference resulting from the high levels of target and non-target congeners present in the sample, and not due to poor analytical technique by the laboratory. As the LCS results were acceptable, only the parent sample was qualified based on MS outliers.

Standard Reference Material (SRM) The reported concentrations for PCB74, PCB87, PCB118, PCB138, and PCB180 were greater than the upper control limits of the acceptance window [±20% of the 95% confidence interval].

The recoveries of these compounds were acceptable in the LCS analyses. No trend was noted for these compounds (i.e., the concentrations were acceptable in most of the SRM analyzed with the small mammal samples). The precision for these compounds was acceptable in the laboratory duplicate.

The reported concentrations for PCB87 and PCB118 were within a ±25% acceptance window, and no action was taken.

The reported values for PCB74, PCB138, and PCB180 were greater than 25% of the 95% confidence interval. Values for these congeners were estimated (J-12) in all associated samples.

Laboratory Duplicate A laboratory duplicate was performed on Sample 7-12-091301. The relative percent difference (RPD) values for PCB45 (114%) and PCB70 (46%) were greater than the 30% control limit. These concentrations were estimated (J-9) in the parent sample.

A positive value for PCB118 was reported in the duplicate, but PCB118 was not detected in the parent sample. The reported value was less than five times the method detection limit (MDL). No action was taken.



B - 3

Compound Identification The separation and spectral fit for any positive result for the coplanar congeners (PCB77, PCB81, PCB126, and PCB169) were evaluated. PCB87 was found to interfere with PCB81 and PCB110 was found to interfere with PCB77. The spectra for PCB126 indicates an overall poor spectral fit in Samples 1-17-090801, 1-18-090901, 7-13-091301, 7-16-091401, 8-12-091301, and 8-14-091301. There appears to be some interference, but the source of the interference could not be determined. The interference does not appear to be a PCB congener.

Although not coplanar congeners, interferences were also noted for PCB123 and PCB157. PCB149 interferes with the spectra for PCB123. For PCB157, the peak co-elutes with the non-target PCB PCB200. However, the quantitation ions for PCB157 (a hexachlorobiphenyl) and PCB200 (an octachlorobiphenyl) are sufficiently different that each congener can be resolved despite the co-elution. No action was taken for the PCB157 results.

For all other congeners with interference, the spectral match met general identification criteria for these congeners, so the laboratory correctly reported the results as positive results. However, due to the interference, the results may be false positives or may be biased high. The potential interferences cannot be resolved without further extract cleanup (e.g., carbon column cleanup). Thus, all positive results for these congeners (PCB77, PCB81, PCB123, and PCB126) should be qualified as tentatively identified at an estimated concentration (NJ-21). PCB congener PCB126 was reported as detected in 14 samples and the result was qualified NJ.

Chromatography and mass spectral identification were reviewed for a minimum of 10% of all other reported congeners. No other instances of potential interference were noted. All reported positive results met the identification criteria and chromatographic peak shapes were acceptable.

Reporting Limits and Sample Results For GCMS-SIM analysis, response factors are generated for each congener during the calibration process. The relative area of a peak is divided by the appropriate response factor to calculate the concentration of the congener. For the homologue groups (monochlorobiphenyl, dichlorobiphenyl, etc.), a representative response factor is used. For example, the response factor for PCB29 is used as the representative response factor for all trichlorobiphenyls.

In Samples 1-18-090901, 1-19-090901, 7-03-091201, 7-06-091201, 8-12-091301, and 8-20-091401, the values reported for the trichlorobiphenyl homologue group are less than the sum of the individual trichlorobiphenyl congeners reported. This occurs because the representative response factor is sufficiently different from the target congener response factors generated during the calibration. For example, the response factor for the PCB31/28 co-elution (detected in most samples) is lower than the trichlorobiphenyl representative response factor. Since the areas are divided by the response factors, this results in a lower concentration for the total trichlorobiphenyls, even if PCB31/28 is the only detected congener in the chlorination level.

Unless all 209 congeners are calibrated, any reported total for a chlorination level will have some inherent variability. For example, for the trichlorobiphenyl results, the differences between the



B - 4

calculated (by summing the congeners) and reported results range from 3.7% to 23% (higher percentages are associated with concentrations near or less than the lower calibration level). The differences for the Total Homologue values are all less than 1.0%. This is within the variability of the method, thus no action was taken.

Eight samples required dilution due to values that exceeded the linear range of the instrument. Both sets of data were reported by the laboratory. In order that only one set of data be reported, values that exceeded the linear range of the instrument were qualified as do-not-report (DNR-20) in the initial analyses and should be reported from the dilutions. The values for all analytes except those that exceeded the linear range in the initial analyses were qualified as do-not-report (DNR-14) in the dilution analyses.

III Overall Assessment

As was determined by this evaluation, the laboratory followed the specified analytical methods. Accuracy was acceptable, as demonstrated by the surrogate, laboratory control sample (LCS), standard reference material (SRM), and matrix spike (MS) percent recovery values, with the exceptions noted above. Precision was acceptable as demonstrated by the relative percent difference values for the duplicate analyses, with the exceptions noted above.

Data were estimated due to laboratory duplicate precision outliers and matrix spike and standard reference material percent recovery outliers. Data were qualified as tentatively identified due to potential interference. Data were qualified as do-not-report due to concentrations greater than the linear range of the instrument and the existence of duplicate data.

Data that have been qualified as do-not-report should not be used for any purpose. All other data, as qualified, are acceptable for use.



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Woods Hole Group


I. DATA PACKAGE COMPLETENESS

All required deliverables were submitted by the laboratory. The laboratory followed adequate corrective action processes, and all anomalies were discussed in the case narrative.

II. Technical Data Validation



1 Continuing Calibration (CCAL) Internal Standards Blanks 2 Compound Identification Surrogate Compounds 1 Calculation Verification



Continuing Calibration (CCAL) The percent difference (%D) values of PCB123 were outside the control limit of +20% in the two CCAL analyzed September 4, 2003. Only a re-extraction of Sample 15-12-091909 was associated with these CCAL, and this analysis was not reported. No qualifiers were necessary.

Matrix Spike (MS) Matrix spike analysis was performed using Sample 16-08-091801. Target congeners were present in this sample at concentrations ranging from 1.42 µg/Kg to 281 µg/Kg, with many concentrations greater than 50 µg/Kg. If the concentration of the congener in the parent sample was greater than five times the spike concentration (9.24 µg/Kg), no qualifiers were assigned because the recovery results are masked by the high PCB concentrations in the sample.

The result for PCB87 was estimated (J-8) in the parent sample as the %R value was greater than



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125%, and the parent sample concentration was less than five times the amount spiked. Results for PCB128, PCB158, PCB194, PCB206 and PCB209 were estimated (J-8) as the %R values were less than the lower control limit of 50%.

Although six data points were estimated, it is possible that the outliers are due to the overall matrix interference resulting from the high levels of target and non-target congeners present in the sample, and not due to poor analytical technique by the laboratory. As the LCS results were acceptable, only the parent sample was qualified based on MS outliers.

Standard Reference Material (SRM) The reported concentration for PCB49 was greater than the upper control limit of the acceptance window [±20% of the 95% confidence interval].

The recoveries of PCB49 was acceptable in the MS and LCS analyses. No trend was noted (i.e., the concentrations were acceptable in most of the SRM analyzed with the small mammal samples). The precision was acceptable in the laboratory duplicate. The reported concentration for PCB49 was within 25% of the 95% confidence interval, and no action was taken.

Laboratory Duplicate A laboratory duplicate was performed on Sample 16-08-091801. The relative percent difference (RPD) value for PCB128 (39%) was greater than the 30% control limit. The concentration was estimated (J-9) in the parent sample.

Compound Identification The separation and spectral fit for any positive result for the coplanar congeners (PCB77, PCB81, PCB126, and PCB169) were evaluated. PCB87 was found to interfere with PCB81 and PCB110 was found to interfere with PCB77. The spectra for PCB126 indicates an overall poor spectral fit in Samples 13-03-092201, 13-12-092401, and 16-05-091801. There appears to be some interference, but the source of the interference could not be determined. The interference does not appear to be a PCB congener.


For all other congeners with interference, the spectral match met general identification criteria for these congeners, so the laboratory correctly reported the results as positive results. However, due to the interference, the results may be false positives or may be biased high. The potential interferences cannot be resolved without further extract cleanup (e.g., carbon column cleanup). Thus, all positive results for these congeners (PCB77, PCB81, PCB123, and PCB126) should be qualified as



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tentatively identified at an estimated concentration (NJ-21). PCB congener PCB126 was reported as detected in three samples (13-03-092201, 13-12-092401, and 16-05-091801). Results were qualified NJ.


Calculation Verification The %R value for congeners PCB31/PCB28 in the matrix spike (MS) was calculated incorrectly. The laboratory reported co-eluting congeners PCB31 and PCB28 as a single result. In the recovery calculation, the amount recovered was divided by the concentration of only one congener. As a result, the reported %R exceeded the upper control limit, but the calculated %R value was acceptable.

The laboratory was contacted and submitted a corrected matrix spike recovery form on September 16, 2003. No additional action was necessary.


In several samples, the values reported for the trichlorobiphenyl homologue group are less than the sum of the individual trichlorobiphenyl congeners reported. This occurs because the representative response factor is sufficiently different from the target congener response factors generated during the calibration. For example, the response factor for the PCB31/28 co-elution (detected in most samples) is lower than the trichlorobiphenyl representative response factor. Since the areas are divided by the response factors, this results in a lower concentration for the total trichlorobiphenyls, even if PCB31/28 is the only detected congener in the chlorination level.

Unless all 209 congeners are calibrated, any reported total for a chlorination level will have some inherent variability. For example, for the trichlorobiphenyl results, the differences between the calculated (by summing the congeners) and reported results range from less than 1% to 8.2% (higher percentages are associated with concentrations near or less than the lower calibration level). The differences for the Total Homologue values are all less than 1.0%. This is within the variability of the method, thus no action was taken.



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Sample 15-12-091901 was re-extracted due to low, but passing, surrogate recoveries. The results from the re-extraction were similar to the initial extraction. As the surrogates for the initial extraction were acceptable the initial analysis was reported. The re-extracted sample results were qualified as do-not-report (DNR-14).

Samples 16-05-091801 and 16-11-091909 required dilution due to values that exceeded the linear range of the instrument. Both sets of data were reported by the laboratory. In order that only one set of data was reported, values that exceeded the linear range of the instrument were qualified as do-not-report (DNR-20) from the initial analyses. The values for all analytes, except those that had exceeded the linear range in the initial analyses, were qualified as do-not-report (DNR-14) in the dilution analyses.



Data were estimated due to laboratory duplicate precision outliers and matrix spike percent recovery outliers. Data were qualified as tentatively identified due to potential interference. Data were qualified as do-not-report due to concentrations greater than the linear range of the instrument and the existence of duplicate data.

Data that has been qualified as do-not-report should not be used for any purpose.

All other data, as qualified, are acceptable for use.



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Woods Hole Group






GC/MS Instrument Performance Check 1 Standard Reference Material (SRM) Initial Calibration (ICAL) Laboratory Duplicate




Continuing Calibration (CCAL) The percent difference (%D) values of PCB123 were outside the control limit of +20% in the CCAL analyzed September 4, 2003 at 10:54, September 5, 2003 at 1:03, and September 5, 2003 at 11:49. All outliers were high, indicating an increase in instrument response. There were no positive results for PCB123. Reporting limits were judged to be unaffected. No action was taken.




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Results for PCB95, PCB101, PCB114, PCB128, PCB149, PCB156, PCB158, PCB167, PCB177, PCB183, and PCB201 were estimated (J-8) in the parent sample as the %R values were greater than 125%, but the concentrations in the parent sample were less than five times the spike amount. Results for PCB194, PCB206 and PCB209 were estimated (J-8), as the %R values were less than the lower control limit of 50%. The value for PCB123 was rejected (R-8), as the %R value was 0%.

Although 14 data points were estimated and one data point was rejected, it is possible that the outliers are due to the overall matrix interference resulting from the high levels of target and non-target congeners present in the sample, and not due to poor analytical technique by the laboratory. As the LCS results were acceptable, only the parent sample was qualified based on MS outliers.

Standard Reference Material (SRM) The reported concentration for PCB49 was greater than the upper control limit of the acceptance window [±20% of the 95% confidence interval].

The recoveries of PCB49 was acceptable in the MS and LCS analyses. No trend was noted (i.e., the concentrations were acceptable in most of the SRM analyzed with the small mammal samples). The precision was acceptable in the laboratory duplicate. The reported concentration for PCB49 was within 25% of the 95% confidence interval, and no action was taken.

Compound Identification The separation and spectral fit for any positive result for the coplanar congeners (PCB77, PCB81, PCB126, and PCB169) were evaluated. PCB87 was found to interfere with PCB81 and PCB110 was found to interfere with PCB77.


For all other congeners with interference, the spectral match met general identification criteria for these congeners, so the laboratory correctly reported the results as positive results. However, due to the interference, the results may be false positives or may be biased high. The potential interferences cannot be resolved without further extract cleanup (e.g., carbon column cleanup). Thus, all positive results for these congeners (PCB77, PCB81, PCB123, and PCB126) should be qualified as tentatively identified at an estimated concentration (NJ-21). PCB congener PCB126 was reported as detected in three samples (16-13-091901, 16-17-092001, and 16-18-092001). Results were qualified NJ.




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Unless all 209 congeners are calibrated, any reported total for a chlorination level will have some inherent variability. For example, for the trichlorobiphenyl results, the differences between the calculated (by summing the congeners) and reported results range from 2.0% to 8.7% (higher percentages are associated with concentrations near or less than the lower calibration level). The differences for the Total Homologue values are all less than 1.0%. This is within the variability of the method, thus no action was taken.

Seven samples required dilution due to values greater than the linear range of the instrument. Both sets of data were reported by the laboratory. In order that only one set of data was reported, values that exceeded the linear range of the instrument were qualified as do-not-report (DNR-20) from the initial analyses. The values for all analytes, except those that had exceeded the linear range in the initial analyses, were qualified as do-not-report (DNR-14) in the dilution analyses.



Data were estimated due to matrix spike percent recovery outliers. Data were qualified as tentatively identified due to potential interference. Data were qualified as do-not-report due to concentrations greater than the linear range of the instrument and the existence of duplicate data. Data were rejected due to a matrix spike percent recovery outlier.




B - 12



Woods Hole Group






GC/MS Instrument Performance Check Standard Reference Material (SRM) Initial Calibration (ICAL) 2 Laboratory Duplicate Continuing Calibration (CCAL) Internal Standards Blanks 1 Compound Identification Surrogate Compounds 1 Calculation Verification




The result for PCB70 was estimated (J-8) in the parent sample as the %R value was greater than 125%, but the concentration in the parent sample was less than five times the spike amount. Results for PCB194, PCB206 and PCB209 were estimated (J-8), as the %R values were less than the lower control limit of 50%.

Although four data points were estimated, it is possible that the outliers are due to the overall matrix interference resulting from the high levels of target and non-target congeners present in the sample,



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and not due to poor analytical technique by the laboratory. As the LCS results were acceptable, only the parent sample was qualified based on MS outliers.

Laboratory Duplicate A laboratory duplicate was performed on Sample 21-02-092201. The relative percent difference (RPD) values for PCB31/28, PCB95, PCB110, PCB128, PCB195, and the trichlorobiphenyl homologue group were greater than the 30% control limit. These concentrations were estimated (J-9) in the parent sample



Calculation Verification The laboratory reported the percent total solids value as the percent moisture value. The laboratory was contacted September 23, 2003 and requested to re-submit the percent moisture data. The corrected data was received September 24, 2003. No additional action was necessary.



Unless all 209 congeners are calibrated, any reported total for a chlorination level will have some inherent variability. For example, for the trichlorobiphenyl results, the differences between the calculated (by summing the congeners) and reported results range from less than 1% to 100.4% (higher percentages are associated with concentrations near or less than the lower calibration level).



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The differences for the Total Homologue values are all less than 3.0%. This is within the variability of the method, thus no action was taken.



Data were estimated due to matrix spike percent recovery and laboratory precision outliers.

All data, as qualified, are acceptable for use.



B - 15



Woods Hole Group

This report documents the review of analytical data from the analysis of small mammal (shrew and mouse) tissue samples and the associated laboratory quality control samples. Samples were analyzed by Woods Hole Group Environmental Laboratories, Raynham, Massachusetts.









Continuing Calibration (CCAL) The percent difference (%D) value of PCB123 was outside the control limit of +20% in the CCAL analyzed on September 10, 2003. Only the method blank, laboratory control sample (LCS), and standard reference material (SRM) were associated with this CCAL. No qualifiers were necessary.

Matrix Spike (MS) Matrix spike analysis was performed using Sample “Comp of Sta 1”. The result for PCB87 was estimated (J-8) in the parent sample as the %R value was greater than 125%. The %R value for PCB189 was also greater than 125%; however, PCB189 was not detected in the parent sample. As the recovery indicates a potential high bias, reporting limits are not affected and no action was taken.



B - 16

Standard Reference Material (SRM) The reported concentrations for PCB31/28 and PCB138 were greater than the upper control limit of the acceptance window [±20% of the 95% confidence interval].

The recoveries of these compounds were acceptable in the MS and LCS analyses. No trend was noted for these compounds (i.e., the concentrations were acceptable in most of the SRM analyzed with the small mammal samples). The precision for these compounds was acceptable in the laboratory duplicate. The reported concentrations for PCB31/28 and PCB138 were within 25% of the 95% confidence interval, and no action was taken.

Laboratory Duplicate A laboratory duplicate was performed on Sample “Comp of Sta 1”. All congener relative percent difference (RPD) values were within the 30% control limit.




In several samples, the values reported for the trichlorobiphenyl or octachlorobiphenyl homologue groups are less than the sum of the individual trichlorobiphenyl congeners reported. This occurs because the representative response factor is sufficiently different from the target congener response factors generated during the calibration. For example, the response factor for the PCB31/28 co-elution (detected in most samples) is lower than the trichlorobiphenyl representative response factor. Since the areas are divided by the response factors, this results in a lower concentration for the total trichlorobiphenyls, even if PCB31/28 is the only detected congener in the chlorination level.

Unless all 209 congeners are calibrated, any reported total for a chlorination level will have some inherent variability. For example, for the trichlorobiphenyl and octachlorobiphenyl results, the differences between the calculated (by summing the congeners) and reported results range from less than 1% to 28.5% (higher percentages are associated with concentrations near or less than the lower



B - 17

calibration level). The differences for the Total Homologue values are all less than 1.5%. This is within the variability of the method, thus no action was taken.



One data point was estimated due to a matrix spike percent recovery outlier, and one data point was estimated based on a laboratory duplicate precision outlier.

All data, as qualified, are acceptable for use.



B - 18



Woods Hole Group

This report documents the review of analytical data from the analysis of small mammal (mouse and vole) tissue samples and the associated laboratory quality control samples. Samples were analyzed by Woods Hole Group Environmental Laboratories, Raynham, Massachusetts.





GC/MS Instrument Performance Check 2 Standard Reference Material (SRM) Initial Calibration (ICAL) Laboratory Duplicate Continuing Calibration (CCAL) Internal Standards Blanks 1 Compound Identification Surrogate Compounds Calculation Verification

2 Matrix Spike (MS) 1 Reporting Limits and Sample Results 1 Laboratory Control Samples (LCS) EDD Transcription Check


Matrix Spike (MS) MS analysis was performed using Sample “Comp of Sta 20” (laboratory ID 0308032-02). The percent recovery (%R) values for PCB31/28, PCB99, PCB105, PCB118, PCB138, PCB153, PCB167, PCB170, BZ189, and PCB201 were greater than the upper control limit of 125%. The results for these congeners, except PCB189, were estimated (J-8) in the parent sample. PCB189 was not detected in the parent sample. As the recovery indicates a potential high bias, reporting limits are not affected and no action was taken.

Laboratory Control Sample (LCS) The %R value for PCB189 was greater than the upper control limit of 125% in the laboratory control (LCS) sample associated with this SDG. There were no positive results for PCB189 in the samples, and reporting limits were judged to be unaffected. No action was taken.



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Standard Reference Material (SRM) The reported concentration for PCB158 was below than the lower control limit of the acceptance window [±20% of the 95% confidence interval]. The reported value for PCB158 was also less than 25% of the 95% confidence interval. Positive values and/or reporting limits for PCB158 were estimated (J/UJ-12) in all samples.

The certified value of PCB170 in the SRM is less than five times the MDL established by the laboratory for this congener. The control limits do not apply, and no action was taken.


Reporting Limits and Sample Results

For GCMS-SIM analysis, response factors are generated for each congener during the calibration process. The relative area of a peak is divided by the appropriate response factor to calculate the concentration of the congener. For the homologue groups (monochlorobiphenyl, dichlorobiphenyl, etc.), a representative response factor is used. For example, the response factor for PCB29 is used as the representative response factor for all trichlorobiphenyls.

In several samples, the values reported for the trichlorobiphenyl or octachlorobiphenyl homologue groups are less than the sum of the individual trichlorobiphenyl congeners reported. This occurs because the representative response factor is sufficiently different from the target congener response factors generated during the calibration. For example, the response factor for the PCB31/28 co-elution (detected in most samples) is lower than the trichlorobiphenyl representative response factor. Since the areas are divided by the response factors, this results in a lower concentration for the total trichlorobiphenyls, even if PCB31/28 is the only detected congener in the chlorination level.

Unless all 209 congeners are calibrated, any reported total for a chlorination level will have some inherent variability. For example, for the trichlorobiphenyl and octachlorobiphenyl results, the differences between the calculated (by summing the congeners) and reported results range from less than 1% to 22.8% (higher percentages are associated with concentrations near or less than the lower calibration level). The differences for the Total Homologue values are all less than 3.0%. This is within the variability of the method, thus no action was taken.

Note that the effect of naming samples as “Comp of Sta 20” (mouse composite, laboratory ID 0308032-02) and “Comp of Sta 20” (meadow vole composite, laboratory ID 0308032-08) produces a duplicate sample name, which may be confusing when the laboratory ID is not present.



B - 20



Data were estimated due to matrix spike percent recovery and standard reference material recovery outliers. All data, as qualified, are acceptable for use.



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DATA VALIDATION REPORT - SUMMARY (LEVEL III) REVIEW Hudson River Soil Samples from 2000 Polychlorinated Biphenyl Congeners

SDG: 0309086 Woods Hole Group

This report documents the review of analytical data from the analysis of soil samples and the associated laboratory quality control samples. Samples were analyzed by Woods Hole Group Environmental Laboratories, Raynham, Massachusetts.





GC/MS Instrument Performance Check 2 Standard Reference Material (SRM) 2 Initial Calibration (ICAL) 2 Laboratory Duplicate 2 Continuing Calibration (CCAL) 2 Internal Standards

Blanks 2 Compound Identification Surrogate Compounds 2 Reporting Limits and Sample Results

2 Matrix Spike (MS) EDD Transcription Check 2 Laboratory Control Samples (LCS)


Initial Calibration (ICAL) The ADQO specification for the initial calibration is that a minimum of a five point calibration would be performed for all analytes, and that the percent relative standard deviation (%RSD) values for all analytes are less than 20%; however, up to 10% of the analyte %RSD values can be greater than 20% provided that all %RSD values are less than 30%. All ICAL met the ADQO.

The %RSD values of PCB81 (at 21.8%), PCB167 (at 20.5%), and PCB169 (at 20.8%) were greater than the control limit of 20% in the ICAL performed November 4, 2003. Positive values for these analytes were estimated (J-5A) in the associated field samples. The reporting limits for non-detected analytes were not significantly affected, so no further action was taken.



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Continuing Calibration (CCAL) The ADQO specified for the continuing (or daily) calibrations is that a CCAL must be analyzed at the beginning and end of each analytical sequence (or every twelve hours, whichever is more frequent), and that all percent difference (%D) values must be less than 20%. However, up to 10% of the analyte %D values can be greater than 20% provided that all %D values are less than 30%. All CCAL met the ADQO.

The %D value for PCB123 (at 23.5%) was greater than the control limit of 20% in the CCAL analyzed November 5, 2003 at 10:49. The %D value for PCB126 (at 21.9%) was greater than the control limit in the CCAL analyzed November 5, 2003 at 14:28. The %D values for PCB194, PCB206, and PCB209 were greater than the control limit in the CCAL analyzed November 19, 2003 at 22:01.

Positive values and/or reporting limits for the above congeners were estimated (J/UJ-5B) in the associated field samples.

Matrix Spike (MS) MS analysis was performed using Sample 7-1-B15. Forty-three of the 47 target congeners were present in this sample, at concentrations ranging from 1.52 µg/Kg to 5290 µg/Kg, with the concentrations for 27 congeners greater than 100 µg/Kg. If the concentration of the congener in the parent sample was greater than five times the spike concentration (10.3 µg/Kg), no qualifiers were assigned because the recovery results are masked by the high PCB concentrations in the sample.

The results for PCB167, PCB183, PCB189, PCB194, PCB195, and PCB206 were estimated (J-8) in the parent sample as the %R values were greater than 125%, but the concentrations in the parent sample were less than five times the spike amount. The reporting limit for PCB123 was rejected (R-8) in the parent sample as this analyte was not detected in either the parent sample or the MS.

Although seven data points were qualified, it is possible that the outliers are due to the overall matrix interference resulting from the high levels of target and non-target congeners present in the sample, and not due to poor analytical technique by the laboratory. As the LCS results were acceptable for these compounds, only the parent sample was qualified based on MS outliers.

Laboratory Control Sample (LCS) The %R value for PCB18 was less than the 75% lower control limit (at 74%) in the LCS analysis associated with this SDG. Due to the potential low bias, positive values and or reporting limits for PCB18 were estimated (J/UJ-10) in the field samples.

Standard Reference Material (SRM) The laboratory analyzed SRM1944, New York/New Jersey Waterway Sediment. This SRM has certified values for 28 of the target PCB congeners. The reported concentration for 11 of the 28 target analytes with certified values were outside the acceptance window [±20% of the 95%



B - 23

confidence interval]. The reported values for these analytes were also outside a wider acceptance window of ±25% of the 95% confidence interval.

The reported values for PCB105, PCB194, PCB195, and PCB206 were less than 25% of the 95% confidence interval. Positive values and/or reporting limits for these analytes were estimated (J/UJ-12) in all samples.

The reported values for PCB31/28, PCB52, PCB118, PCB128, PCB138, PCB180, and PCB183 were greater than 25% of the 95% confidence interval. Positive values for these analytes were estimated (J-12) in all samples.

Laboratory Duplicate A laboratory duplicate was performed on Sample 8-1-A15. The relative percent difference (RPD) value for PCB8 (at 31%) was greater than the 30% control limit. The concentration for this analyte was estimated (J-9) in the parent sample

Internal Standards The recoveries of both the 13C-PCB15 and 13C-PCB180 internal standards in Samples 7-1-B25, 7-1-F25 and the LCS were greater than the upper control limit of 150% of the area of the respective internal standard in the associated CCAL. Positive values were estimated (J-19) in the field samples.

Compound Identification The separation and spectral fit for any positive result for the coplanar congeners (PCB77, PCB81, PCB126, and PCB169) were evaluated. PCB87 was found to interfere with PCB81 and PCB110 was found to interfere with PCB77. The spectra for PCB126 indicates an overall poor spectral fit in Sample 7-1-C15. There appears to be some interference, but the source of the interference could not be determined. The interference does not appear to be a PCB congener.

For all other congeners with interference, the spectral match met general identification criteria for these congeners, so the laboratory correctly reported the results as positive results. However, due to the interference, the results may be false positives or may be biased high. The potential interferences cannot be resolved without further extract cleanup (e.g., carbon column cleanup). Thus, all positive results for these congeners (PCB77 in 18 samples, PCB81 in two samples, and PCB126 in Sample 7-1-C15) were qualified as tentatively identified at an estimated concentration (NJ-21).


Reporting Limits and Sample Results For GCMS-SIM analysis, response factors are generated for each congener during the calibration process. The relative area of a peak is divided by the appropriate response factor to calculate the



B - 24

concentration of the congener. For the homologue groups (monochlorobiphenyl, dichlorobiphenyl, etc.), a representative response factor is used. For example, the response factor for PCB29 is used as the representative response factor for all trichlorobiphenyls.

In several samples, the values reported for the heptachlorobiphenyl homologue groups are less than the sum of the individual heptachlorobiphenyl congeners reported. This occurs because the representative response factor is sufficiently different from the target congener response factors generated during the calibration. For example, the response factor for the PCB31/28 co-elution (detected in most samples) is lower than the trichlorobiphenyl representative response factor. Since the areas are divided by the response factors, this results in a lower concentration for the total trichlorobiphenyls, even if PCB31/28 is the only detected congener in the chlorination level.

Unless all 209 congeners are calibrated, any reported total for a chlorination level will have some inherent variability. For example, for the heptachlorobiphenyl results, the differences between the calculated (by summing the congeners) and reported results range from less than 1% to 12.4% (higher percentages are associated with concentrations near or less than the lower calibration level). The differences for the Total Homologue values are all less than 1%. This is within the variability of the method, thus no action was taken.

A majority of the samples were reported from a diluted analysis due to the high levels of the target analytes present. Reporting limits were raised accordingly.

Sample 7-1-A15 was reported twice, once at a 20X dilution and once at a 40X dilution, due to the value for PCB52 being greater than the linear range of the calibration in the 20X analysis. In order that only one set of data be reported, the value for PCB52 was qualified as do-not-report (DNR-20) in the 20X analysis. All values, except that of PCB52, were qualified as do-not-report (DNR-14) in the 40X analysis.


As was determined by this evaluation, the laboratory followed the specified analytical methods. Accuracy was acceptable, as demonstrated by the surrogate, laboratory control sample (LCS), standard reference material (SRM), and matrix spike (MS) percent recovery values, with the exceptions noted above. Precision was acceptable as demonstrated by the relative percent difference values for the duplicate analyses, with the exception noted above.

Data were estimated due to LCS and MS percent recovery outliers, standard reference material and internal standard recovery outliers, laboratory duplicate precision outliers, initial calibration RSD outliers, and continuing calibration percent difference outliers. Data were rejected due to a MS percent recovery outlier.




B - 25

DATA VALIDATION REPORT - SUMMARY (LEVEL III) REVIEW Hudson River Shrew Tissue from 2000


Woods Hole Group

This report documents the review of analytical data from the analysis of small mammal (shrew) tissue samples and the associated laboratory quality control samples. Samples were analyzed by Woods Hole Group Environmental Laboratories, Raynham, Massachusetts. Refer to the Sample Index for a list of the samples reviewed.


All required deliverables were submitted by the laboratory. The laboratory followed adequate corrective action processes, and all anomalies were discussed in the case narrative. Due to limited sample volume, percent moisture analyses were not performed.



GC/MS Instrument Performance Check 1 Standard Reference Material (SRM) Initial Calibration (ICAL) 1 Laboratory Duplicate Continuing Calibration (CCAL) Internal Standards Blanks Compound Identification Surrogate Compounds 2 Reporting Limits and Sample Results

1 Matrix Spike (MS) EDD Transcription Check Laboratory Control Samples (LCS)


Matrix Spike (MS) MS analysis was not performed due to insufficient sample volume. Accuracy was evaluated using the LCS analysis and the surrogate compounds in each sample.

Standard Reference Material (SRM) The reported concentrations for PCB49 and PCB158 were below than the lower control limit of the acceptance window [±20% of the 95% confidence interval]. The reported concentration for PCB138 was greater than the upper control limit of the acceptance window.



B - 26

The reported values for these congeners were acceptable in the LCS, and no action was taken unless the reported values were outside a wider acceptance window of ±25% of the 95% confidence interval. The reported values were within ±25% of the 95% confidence interval. No data were qualified.

Laboratory Duplicate A laboratory duplicate was not performed due to insufficient sample volume. Laboratory precision could not be assessed.


In most samples, the values reported for one or more homologue groups are less than the sum of the individual congeners reported from that chlorination level. This occurs because the representative response factor is sufficiently different from the target congener response factors generated during the calibration. For example, the response factor for the PCB31/28 co-elution (detected in most samples) is lower than the trichlorobiphenyl representative response factor. Since the areas are divided by the response factors, this results in a lower concentration for the total trichlorobiphenyls, even if PCB31/28 is the only detected congener in the chlorination level.

Unless all 209 congeners are calibrated, any reported total for a chlorination level will have some inherent variability. The differences between the calculated (by summing the congeners) and reported results range from less than 1% to 78.7% (higher percentages are associated with concentrations near or less than the lower calibration level). The differences for the Total Homologue values are all less than 1%. This is within the variability of the method, thus no action was taken.

Sample 01-01-09100-10-S-STS was reported twice due to a PCB138 concentration that was greater than the linear range of the calibration in the initial analysis. In order that only one set of data be reported, the value for PCB138 was qualified do-not-report (DNR-20) in the initial analysis and should be reported from the dilution. All values, except that of PCB138, were qualified do-not-report (DNR-14) in the dilution analysis.

Several samples were analyzed as dilutions due to the high levels of target analytes present. Reporting limits were raised accordingly.



B - 27


As was determined by this evaluation, the laboratory followed the specified analytical methods. Accuracy was acceptable, as demonstrated by the surrogate, laboratory control sample (LCS), and standard reference material (SRM) percent recovery values, with the exceptions noted above. Precision not evaluated.

Data that has been qualified do-not-report should not be used for any purpose. All other data, as reported, are acceptable for use.

HUDSON RIVER



HU

DSO

N R

IVE

R DA

TA R

EP

OR

T: SM

AL

L MA

MM

AL

S AN

D A

ME

RIC

AN

WO

OD

CO

CK C

OL

LE

CT

ION

, AN

AL

YSIS O

F

FL

OO

DP

LA

IN E

AR

TH

WO

RM

S, AN

D R

E-AN

AL

YSIS O

F SE

LE

CT F

LO

OD

PL

AIN

SO

ILS A

ND

SM

AL

L MA

MM

AL

S

APPENDIX D

EARTHWORM (2000) AND WOODCOCK LIVER (2001)DATA SHEETS

HUDS

ON R

IVER



HU

DSO

N R

IVE

R D

AT

A R

EP

OR

T: S

MA

LL M

AM

MA

LS

AN

D A

ME

RIC

AN

WO

OD

CO

CK

CO

LL

EC

TIO

N, A

NA

LY

SIS

OF

FL

OO

DP

LA

IN E

AR

TH

WO

RM

S, A

ND

RE

-AN

AL

YSI

S O

F S

EL

EC

T F

LO

OD

PL

AIN

SO

ILS

AN

D S

MA

LL M

AM

MA

LS

Earthworm Tissue and Woodcock Liver Tissue Data Table Hudson NRDA Floodplain DatabaseVersion 2.0

Extracted 7/30/04

SAMPLING DATE FIELD ID

EASTING (NAD83

UTM18N)

NORTHING (NAD83

UTM18N)SITE

NUMBER LAB ID ANALYTE1

9/27/2001 HRW-001 611952 4758192 13 0309077-01 Cl2-BZ#8 0.232 U µg/Kg 0.232 µg/Kg9/27/2001 HRW-001 611952 4758192 13 0309077-01 Cl3-BZ#18 0.515 U µg/Kg 0.515 µg/Kg9/27/2001 HRW-001 611952 4758192 13 0309077-01 Cl3-BZ#31/#28 3.71 U µg/Kg 3.71 µg/Kg9/27/2001 HRW-001 611952 4758192 13 0309077-01 Cl4-BZ#44 0.353 U µg/Kg 0.353 µg/Kg9/27/2001 HRW-001 611952 4758192 13 0309077-01 Cl4-BZ#45 0.472 U µg/Kg 0.472 µg/Kg9/27/2001 HRW-001 611952 4758192 13 0309077-01 Cl4-BZ#47 0.598 U µg/Kg 0.598 µg/Kg9/27/2001 HRW-001 611952 4758192 13 0309077-01 Cl4-BZ#49 0.404 J µg/Kg 0.294 µg/Kg9/27/2001 HRW-001 611952 4758192 13 0309077-01 Cl4-BZ#52 0.876 J µg/Kg 0.334 µg/Kg9/27/2001 HRW-001 611952 4758192 13 0309077-01 Cl4-BZ#56 0.175 U µg/Kg 0.175 µg/Kg9/27/2001 HRW-001 611952 4758192 13 0309077-01 Cl4-BZ#66 0.674 J µg/Kg 0.234 µg/Kg9/27/2001 HRW-001 611952 4758192 13 0309077-01 Cl4-BZ#70 0.458 J µg/Kg 0.205 µg/Kg9/27/2001 HRW-001 611952 4758192 13 0309077-01 Cl4-BZ#74 0.754 J µg/Kg 0.361 µg/Kg9/27/2001 HRW-001 611952 4758192 13 0309077-01 Cl4-BZ#77 0.323 U µg/Kg 0.323 µg/Kg9/27/2001 HRW-001 611952 4758192 13 0309077-01 Cl4-BZ#81 0.321 U µg/Kg 0.321 µg/Kg9/27/2001 HRW-001 611952 4758192 13 0309077-01 Cl5-BZ#87 0.674 J µg/Kg 0.143 µg/Kg9/27/2001 HRW-001 611952 4758192 13 0309077-01 Cl5-BZ#95 0.498 J µg/Kg 0.111 µg/Kg9/27/2001 HRW-001 611952 4758192 13 0309077-01 Cl5-BZ#99 2.28 µg/Kg 0.0754 µg/Kg9/27/2001 HRW-001 611952 4758192 13 0309077-01 Cl5-BZ#101 2.75 µg/Kg 0.215 µg/Kg9/27/2001 HRW-001 611952 4758192 13 0309077-01 Cl5-BZ#105 1.99 µg/Kg 0.105 µg/Kg9/27/2001 HRW-001 611952 4758192 13 0309077-01 Cl5-BZ#110 1.02 J µg/Kg 0.205 µg/Kg9/27/2001 HRW-001 611952 4758192 13 0309077-01 Cl5-BZ#114 0.0943 U µg/Kg 0.0943 µg/Kg9/27/2001 HRW-001 611952 4758192 13 0309077-01 Cl5-BZ#118 5.23 µg/Kg 0.221 µg/Kg9/27/2001 HRW-001 611952 4758192 13 0309077-01 Cl5-BZ#123 0.186 U µg/Kg 0.186 µg/Kg9/27/2001 HRW-001 611952 4758192 13 0309077-01 Cl5-BZ#126 0.164 U µg/Kg 0.164 µg/Kg9/27/2001 HRW-001 611952 4758192 13 0309077-01 Cl6-BZ#128 1.04 µg/Kg 0.148 µg/Kg9/27/2001 HRW-001 611952 4758192 13 0309077-01 Cl6-BZ#138 14.0 µg/Kg 0.213 µg/Kg9/27/2001 HRW-001 611952 4758192 13 0309077-01 Cl6-BZ#146 2.57 µg/Kg 0.135 µg/Kg9/27/2001 HRW-001 611952 4758192 13 0309077-01 Cl6-BZ#149 3.30 µg/Kg 0.172 µg/Kg9/27/2001 HRW-001 611952 4758192 13 0309077-01 Cl6-BZ#151 0.286 U µg/Kg 0.286 µg/Kg9/27/2001 HRW-001 611952 4758192 13 0309077-01 Cl6-BZ#153 8.49 µg/Kg 0.245 µg/Kg9/27/2001 HRW-001 611952 4758192 13 0309077-01 Cl6-BZ#156 0.674 J µg/Kg 0.175 µg/Kg9/27/2001 HRW-001 611952 4758192 13 0309077-01 Cl6-BZ#157 0.137 U µg/Kg 0.137 µg/Kg9/27/2001 HRW-001 611952 4758192 13 0309077-01 Cl6-BZ#158 0.418 J µg/Kg 0.116 µg/Kg9/27/2001 HRW-001 611952 4758192 13 0309077-01 Cl6-BZ#167 0.566 J µg/Kg 0.148 µg/Kg9/27/2001 HRW-001 611952 4758192 13 0309077-01 Cl6-BZ#169 0.477 U µg/Kg 0.477 µg/Kg

VALUE, INTERPRETIVE QUALIFIER2 AND UNITS3

DETECTION LIMIT3

1BZ#=PCB congener Ballschmiter & Zell number 2U=Non-detected result at the detection limit J/UJ=Estimated result or detection limit 3PCB results & detection limit reported on wet weight basis 1 of 21


Extracted 7/30/04


EASTING (NAD83

UTM18N)

NORTHING (NAD83

UTM18N)SITE

NUMBER LAB ID ANALYTE1VALUE, INTERPRETIVE

QUALIFIER2 AND UNITS3DETECTION

LIMIT3

9/27/2001 HRW-001 611952 4758192 13 0309077-01 Cl7-BZ#170 1.24 J µg/Kg 0.555 µg/Kg9/27/2001 HRW-001 611952 4758192 13 0309077-01 Cl7-BZ#174 0.701 µg/Kg 0.113 µg/Kg9/27/2001 HRW-001 611952 4758192 13 0309077-01 Cl7-BZ#177 1.28 µg/Kg 0.159 µg/Kg9/27/2001 HRW-001 611952 4758192 13 0309077-01 Cl7-BZ#180 2.21 µg/Kg 0.237 µg/Kg9/27/2001 HRW-001 611952 4758192 13 0309077-01 Cl7-BZ#183 0.660 µg/Kg 0.108 µg/Kg9/27/2001 HRW-001 611952 4758192 13 0309077-01 Cl7-BZ#189 0.213 U µg/Kg 0.213 µg/Kg9/27/2001 HRW-001 611952 4758192 13 0309077-01 Cl7-BZ#187 20.0 µg/Kg 0.119 µg/Kg9/27/2001 HRW-001 611952 4758192 13 0309077-01 Cl8-BZ#194 0.539 J µg/Kg 0.248 µg/Kg9/27/2001 HRW-001 611952 4758192 13 0309077-01 Cl8-BZ#195 0.245 U µg/Kg 0.245 µg/Kg9/27/2001 HRW-001 611952 4758192 13 0309077-01 Cl8-BZ#201 1.83 µg/Kg 0.215 µg/Kg9/27/2001 HRW-001 611952 4758192 13 0309077-01 Cl9-BZ#206 0.876 J µg/Kg 0.288 µg/Kg9/27/2001 HRW-001 611952 4758192 13 0309077-01 Cl10-BZ#209 1.08 µg/Kg 0.135 µg/Kg9/27/2001 HRW-001 611952 4758192 13 0309077-01 Monochlorobiphenyls 7.92 U µg/Kg 7.92 µg/Kg9/27/2001 HRW-001 611952 4758192 13 0309077-01 Dichlorobiphenyls 0.232 U µg/Kg 0.232 µg/Kg9/27/2001 HRW-001 611952 4758192 13 0309077-01 Trichlorobiphenyls 0.795 U µg/Kg 0.795 µg/Kg9/27/2001 HRW-001 611952 4758192 13 0309077-01 Tetrachlorobiphenyls 7.65 µg/Kg 0.124 µg/Kg9/27/2001 HRW-001 611952 4758192 13 0309077-01 Pentachlorobiphenyls 26.7 µg/Kg 0.143 µg/Kg9/27/2001 HRW-001 611952 4758192 13 0309077-01 Hexachlorobiphenyls 36.4 µg/Kg 0.226 µg/Kg9/27/2001 HRW-001 611952 4758192 13 0309077-01 Heptachlorobiphenyls 29.5 µg/Kg 0.124 µg/Kg9/27/2001 HRW-001 611952 4758192 13 0309077-01 Octachlorobiphenyls 4.58 µg/Kg 0.113 µg/Kg9/27/2001 HRW-001 611952 4758192 13 0309077-01 Nonachlorobiphenyls 8.97 µg/Kg 0.288 µg/Kg9/27/2001 HRW-001 611952 4758192 13 0309077-01 Decachlorobiphenyl 1.08 µg/Kg 0.135 µg/Kg9/27/2001 HRW-001 611952 4758192 13 0309077-01 Total Homologs 115 µg/Kg 0.135 µg/Kg9/27/2001 HRW-001 611952 4758192 13 0309077-01 Percent Lipids 4.1 % 0.1 %9/27/2001 HRW-001 611952 4758192 13 0309077-01 Percent Moisture 73.3 % 0.1 %9/27/2001 HRW-002 612006 4758274 13 0309077-02 Cl2-BZ#8 0.225 U µg/Kg 0.225 µg/Kg9/27/2001 HRW-002 612006 4758274 13 0309077-02 Cl3-BZ#18 0.500 U µg/Kg 0.500 µg/Kg9/27/2001 HRW-002 612006 4758274 13 0309077-02 Cl3-BZ#31/#28 3.61 U µg/Kg 3.61 µg/Kg9/27/2001 HRW-002 612006 4758274 13 0309077-02 Cl4-BZ#44 0.343 U µg/Kg 0.343 µg/Kg9/27/2001 HRW-002 612006 4758274 13 0309077-02 Cl4-BZ#45 0.458 U µg/Kg 0.458 µg/Kg9/27/2001 HRW-002 612006 4758274 13 0309077-02 Cl4-BZ#47 0.877 J µg/Kg 0.581 µg/Kg9/27/2001 HRW-002 612006 4758274 13 0309077-02 Cl4-BZ#49 1.49 µg/Kg 0.285 µg/Kg9/27/2001 HRW-002 612006 4758274 13 0309077-02 Cl4-BZ#52 2.12 µg/Kg 0.325 µg/Kg9/27/2001 HRW-002 612006 4758274 13 0309077-02 Cl4-BZ#56 0.825 J µg/Kg 0.170 µg/Kg9/27/2001 HRW-002 612006 4758274 13 0309077-02 Cl4-BZ#66 2.86 µg/Kg 0.228 µg/Kg



Extracted 7/30/04


EASTING (NAD83

UTM18N)

NORTHING (NAD83

UTM18N)SITE



LIMIT3

9/27/2001 HRW-002 612006 4758274 13 0309077-02 Cl4-BZ#70 1.09 µg/Kg 0.199 µg/Kg9/27/2001 HRW-002 612006 4758274 13 0309077-02 Cl4-BZ#74 1.34 J µg/Kg 0.351 µg/Kg9/27/2001 HRW-002 612006 4758274 13 0309077-02 Cl4-BZ#77 0.314 U µg/Kg 0.314 µg/Kg9/27/2001 HRW-002 612006 4758274 13 0309077-02 Cl4-BZ#81 0.312 U µg/Kg 0.312 µg/Kg9/27/2001 HRW-002 612006 4758274 13 0309077-02 Cl5-BZ#87 1.53 µg/Kg 0.139 µg/Kg9/27/2001 HRW-002 612006 4758274 13 0309077-02 Cl5-BZ#95 0.851 µg/Kg 0.107 µg/Kg9/27/2001 HRW-002 612006 4758274 13 0309077-02 Cl5-BZ#99 2.07 µg/Kg 0.0733 µg/Kg9/27/2001 HRW-002 612006 4758274 13 0309077-02 Cl5-BZ#101 2.37 µg/Kg 0.209 µg/Kg9/27/2001 HRW-002 612006 4758274 13 0309077-02 Cl5-BZ#105 1.95 µg/Kg 0.102 µg/Kg9/27/2001 HRW-002 612006 4758274 13 0309077-02 Cl5-BZ#110 1.36 µg/Kg 0.199 µg/Kg9/27/2001 HRW-002 612006 4758274 13 0309077-02 Cl5-BZ#114 0.0917 U µg/Kg 0.0917 µg/Kg9/27/2001 HRW-002 612006 4758274 13 0309077-02 Cl5-BZ#118 4.44 µg/Kg 0.215 µg/Kg9/27/2001 HRW-002 612006 4758274 13 0309077-02 Cl5-BZ#123 0.181 U µg/Kg 0.181 µg/Kg9/27/2001 HRW-002 612006 4758274 13 0309077-02 Cl5-BZ#126 0.160 U µg/Kg 0.160 µg/Kg9/27/2001 HRW-002 612006 4758274 13 0309077-02 Cl6-BZ#128 0.943 µg/Kg 0.144 µg/Kg9/27/2001 HRW-002 612006 4758274 13 0309077-02 Cl6-BZ#138 10.6 µg/Kg 0.207 µg/Kg9/27/2001 HRW-002 612006 4758274 13 0309077-02 Cl6-BZ#146 2.24 µg/Kg 0.131 µg/Kg9/27/2001 HRW-002 612006 4758274 13 0309077-02 Cl6-BZ#149 1.69 µg/Kg 0.168 µg/Kg9/27/2001 HRW-002 612006 4758274 13 0309077-02 Cl6-BZ#151 0.485 J µg/Kg 0.278 µg/Kg9/27/2001 HRW-002 612006 4758274 13 0309077-02 Cl6-BZ#153 7.96 µg/Kg 0.238 µg/Kg9/27/2001 HRW-002 612006 4758274 13 0309077-02 Cl6-BZ#156 0.170 U µg/Kg 0.170 µg/Kg9/27/2001 HRW-002 612006 4758274 13 0309077-02 Cl6-BZ#157 0.134 U µg/Kg 0.134 µg/Kg9/27/2001 HRW-002 612006 4758274 13 0309077-02 Cl6-BZ#158 0.498 J µg/Kg 0.113 µg/Kg9/27/2001 HRW-002 612006 4758274 13 0309077-02 Cl6-BZ#167 0.498 J µg/Kg 0.144 µg/Kg9/27/2001 HRW-002 612006 4758274 13 0309077-02 Cl6-BZ#169 0.464 U µg/Kg 0.464 µg/Kg9/27/2001 HRW-002 612006 4758274 13 0309077-02 Cl7-BZ#170 1.26 J µg/Kg 0.540 µg/Kg9/27/2001 HRW-002 612006 4758274 13 0309077-02 Cl7-BZ#174 0.110 U µg/Kg 0.110 µg/Kg9/27/2001 HRW-002 612006 4758274 13 0309077-02 Cl7-BZ#177 0.629 J µg/Kg 0.154 µg/Kg9/27/2001 HRW-002 612006 4758274 13 0309077-02 Cl7-BZ#180 2.83 µg/Kg 0.230 µg/Kg9/27/2001 HRW-002 612006 4758274 13 0309077-02 Cl7-BZ#183 0.472 J µg/Kg 0.105 µg/Kg9/27/2001 HRW-002 612006 4758274 13 0309077-02 Cl7-BZ#189 0.207 U µg/Kg 0.207 µg/Kg9/27/2001 HRW-002 612006 4758274 13 0309077-02 Cl7-BZ#187 12.8 µg/Kg 0.115 µg/Kg9/27/2001 HRW-002 612006 4758274 13 0309077-02 Cl8-BZ#194 0.904 J µg/Kg 0.241 µg/Kg9/27/2001 HRW-002 612006 4758274 13 0309077-02 Cl8-BZ#195 0.238 U µg/Kg 0.238 µg/Kg9/27/2001 HRW-002 612006 4758274 13 0309077-02 Cl8-BZ#201 2.83 µg/Kg 0.209 µg/Kg



Extracted 7/30/04


EASTING (NAD83

UTM18N)

NORTHING (NAD83

UTM18N)SITE



LIMIT3

9/27/2001 HRW-002 612006 4758274 13 0309077-02 Cl9-BZ#206 2.66 µg/Kg 0.280 µg/Kg9/27/2001 HRW-002 612006 4758274 13 0309077-02 Cl10-BZ#209 2.92 µg/Kg 0.131 µg/Kg9/27/2001 HRW-002 612006 4758274 13 0309077-02 Monochlorobiphenyls 7.70 U µg/Kg 7.70 µg/Kg9/27/2001 HRW-002 612006 4758274 13 0309077-02 Dichlorobiphenyls 0.225 U µg/Kg 0.225 µg/Kg9/27/2001 HRW-002 612006 4758274 13 0309077-02 Trichlorobiphenyls 0.773 U µg/Kg 0.773 µg/Kg9/27/2001 HRW-002 612006 4758274 13 0309077-02 Tetrachlorobiphenyls 20.7 µg/Kg 0.120 µg/Kg9/27/2001 HRW-002 612006 4758274 13 0309077-02 Pentachlorobiphenyls 29.6 µg/Kg 0.139 µg/Kg9/27/2001 HRW-002 612006 4758274 13 0309077-02 Hexachlorobiphenyls 30.1 µg/Kg 0.220 µg/Kg9/27/2001 HRW-002 612006 4758274 13 0309077-02 Heptachlorobiphenyls 21.3 µg/Kg 0.120 µg/Kg9/27/2001 HRW-002 612006 4758274 13 0309077-02 Octachlorobiphenyls 6.39 µg/Kg 0.110 µg/Kg9/27/2001 HRW-002 612006 4758274 13 0309077-02 Nonachlorobiphenyls 14.5 µg/Kg 0.280 µg/Kg9/27/2001 HRW-002 612006 4758274 13 0309077-02 Decachlorobiphenyl 2.92 µg/Kg 0.131 µg/Kg9/27/2001 HRW-002 612006 4758274 13 0309077-02 Total Homologs 125 µg/Kg 0.131 µg/Kg9/27/2001 HRW-002 612006 4758274 13 0309077-02 Percent Lipids 4.2 % 0.1 %9/27/2001 HRW-002 612006 4758274 13 0309077-02 Percent Moisture 70.4 % 0.1 %10/3/2000 EW-01 611657 4758828 1 0309077-03 Cl2-BZ#8 1.45 µg/Kg 0.108 µg/Kg10/3/2000 EW-01 611657 4758828 1 0309077-03 Cl3-BZ#18 1.37 µg/Kg 0.240 µg/Kg10/3/2000 EW-01 611657 4758828 1 0309077-03 Cl3-BZ#31/#28 73.8 µg/Kg 1.73 µg/Kg10/3/2000 EW-01 611657 4758828 1 0309077-03 Cl4-BZ#44 19.7 µg/Kg 0.164 µg/Kg10/3/2000 EW-01 611657 4758828 1 0309077-03 Cl4-BZ#45 0.220 U µg/Kg 0.220 µg/Kg10/3/2000 EW-01 611657 4758828 1 0309077-03 Cl4-BZ#47 26.3 µg/Kg 0.279 µg/Kg10/3/2000 EW-01 611657 4758828 1 0309077-03 Cl4-BZ#49 40.6 µg/Kg 0.137 µg/Kg10/3/2000 EW-01 611657 4758828 1 0309077-03 Cl4-BZ#52 83.8 µg/Kg 0.156 µg/Kg10/3/2000 EW-01 611657 4758828 1 0309077-03 Cl4-BZ#56 34.1 µg/Kg 0.0816 µg/Kg10/3/2000 EW-01 611657 4758828 1 0309077-03 Cl4-BZ#66 56.3 µg/Kg 0.109 µg/Kg10/3/2000 EW-01 611657 4758828 1 0309077-03 Cl4-BZ#70 64.1 µg/Kg 0.0954 µg/Kg10/3/2000 EW-01 611657 4758828 1 0309077-03 Cl4-BZ#74 30.0 µg/Kg 0.168 µg/Kg10/3/2000 EW-01 611657 4758828 1 0309077-03 Cl4-BZ#77 0.151 U µg/Kg 0.151 µg/Kg10/3/2000 EW-01 611657 4758828 1 0309077-03 Cl4-BZ#81 0.149 U µg/Kg 0.149 µg/Kg10/3/2000 EW-01 611657 4758828 1 0309077-03 Cl5-BZ#87 24.8 µg/Kg 0.0665 µg/Kg10/3/2000 EW-01 611657 4758828 1 0309077-03 Cl5-BZ#95 29.8 µg/Kg 0.0515 µg/Kg10/3/2000 EW-01 611657 4758828 1 0309077-03 Cl5-BZ#99 25.7 µg/Kg 0.0352 µg/Kg10/3/2000 EW-01 611657 4758828 1 0309077-03 Cl5-BZ#101 54.1 µg/Kg 0.100 µg/Kg10/3/2000 EW-01 611657 4758828 1 0309077-03 Cl5-BZ#105 17.0 µg/Kg 0.0490 µg/Kg10/3/2000 EW-01 611657 4758828 1 0309077-03 Cl5-BZ#110 49.1 µg/Kg 0.0954 µg/Kg



Extracted 7/30/04


EASTING (NAD83

UTM18N)

NORTHING (NAD83

UTM18N)SITE



LIMIT3

10/3/2000 EW-01 611657 4758828 1 0309077-03 Cl5-BZ#114 1.66 µg/Kg 0.0439 µg/Kg10/3/2000 EW-01 611657 4758828 1 0309077-03 Cl5-BZ#118 35.2 µg/Kg 0.103 µg/Kg10/3/2000 EW-01 611657 4758828 1 0309077-03 Cl5-BZ#123 0.0866 U µg/Kg 0.0866 µg/Kg10/3/2000 EW-01 611657 4758828 1 0309077-03 Cl5-BZ#126 0.0766 U µg/Kg 0.0766 µg/Kg10/3/2000 EW-01 611657 4758828 1 0309077-03 Cl6-BZ#128 6.48 µg/Kg 0.0690 µg/Kg10/3/2000 EW-01 611657 4758828 1 0309077-03 Cl6-BZ#138 54.7 µg/Kg 0.0992 µg/Kg10/3/2000 EW-01 611657 4758828 1 0309077-03 Cl6-BZ#146 6.65 µg/Kg 0.0628 µg/Kg10/3/2000 EW-01 611657 4758828 1 0309077-03 Cl6-BZ#149 39.7 µg/Kg 0.0803 µg/Kg10/3/2000 EW-01 611657 4758828 1 0309077-03 Cl6-BZ#151 10.2 µg/Kg 0.133 µg/Kg10/3/2000 EW-01 611657 4758828 1 0309077-03 Cl6-BZ#153 21.3 µg/Kg 0.114 µg/Kg10/3/2000 EW-01 611657 4758828 1 0309077-03 Cl6-BZ#156 2.89 µg/Kg 0.0816 µg/Kg10/3/2000 EW-01 611657 4758828 1 0309077-03 Cl6-BZ#157 0.0640 U µg/Kg 0.0640 µg/Kg10/3/2000 EW-01 611657 4758828 1 0309077-03 Cl6-BZ#158 1.30 µg/Kg 0.0540 µg/Kg10/3/2000 EW-01 611657 4758828 1 0309077-03 Cl6-BZ#167 1.28 µg/Kg 0.0690 µg/Kg10/3/2000 EW-01 611657 4758828 1 0309077-03 Cl6-BZ#169 0.222 U µg/Kg 0.222 µg/Kg10/3/2000 EW-01 611657 4758828 1 0309077-03 Cl7-BZ#170 4.29 µg/Kg 0.259 µg/Kg10/3/2000 EW-01 611657 4758828 1 0309077-03 Cl7-BZ#174 3.39 µg/Kg 0.0527 µg/Kg10/3/2000 EW-01 611657 4758828 1 0309077-03 Cl7-BZ#177 2.39 µg/Kg 0.0741 µg/Kg10/3/2000 EW-01 611657 4758828 1 0309077-03 Cl7-BZ#180 3.53 µg/Kg 0.111 µg/Kg10/3/2000 EW-01 611657 4758828 1 0309077-03 Cl7-BZ#183 1.10 µg/Kg 0.0502 µg/Kg10/3/2000 EW-01 611657 4758828 1 0309077-03 Cl7-BZ#189 0.0992 U µg/Kg 0.0992 µg/Kg10/3/2000 EW-01 611657 4758828 1 0309077-03 Cl7-BZ#187 19.3 µg/Kg 0.0552 µg/Kg10/3/2000 EW-01 611657 4758828 1 0309077-03 Cl8-BZ#194 0.797 µg/Kg 0.116 µg/Kg10/3/2000 EW-01 611657 4758828 1 0309077-03 Cl8-BZ#195 0.370 J µg/Kg 0.114 µg/Kg10/3/2000 EW-01 611657 4758828 1 0309077-03 Cl8-BZ#201 3.35 µg/Kg 0.100 µg/Kg10/3/2000 EW-01 611657 4758828 1 0309077-03 Cl9-BZ#206 1.09 µg/Kg 0.134 µg/Kg10/3/2000 EW-01 611657 4758828 1 0309077-03 Cl10-BZ#209 0.276 J µg/Kg 0.0628 µg/Kg10/3/2000 EW-01 611657 4758828 1 0309077-03 Monochlorobiphenyls 3.69 U µg/Kg 3.69 µg/Kg10/3/2000 EW-01 611657 4758828 1 0309077-03 Dichlorobiphenyls 17.1 µg/Kg 0.108 µg/Kg10/3/2000 EW-01 611657 4758828 1 0309077-03 Trichlorobiphenyls 122 µg/Kg 0.370 µg/Kg10/3/2000 EW-01 611657 4758828 1 0309077-03 Tetrachlorobiphenyls 438 µg/Kg 0.0578 µg/Kg10/3/2000 EW-01 611657 4758828 1 0309077-03 Pentachlorobiphenyls 424 µg/Kg 0.0665 µg/Kg10/3/2000 EW-01 611657 4758828 1 0309077-03 Hexachlorobiphenyls 181 µg/Kg 0.105 µg/Kg10/3/2000 EW-01 611657 4758828 1 0309077-03 Heptachlorobiphenyls 36.7 µg/Kg 0.0578 µg/Kg10/3/2000 EW-01 611657 4758828 1 0309077-03 Octachlorobiphenyls 5.48 µg/Kg 0.0527 µg/Kg



Extracted 7/30/04


EASTING (NAD83

UTM18N)

NORTHING (NAD83

UTM18N)SITE



LIMIT3

10/3/2000 EW-01 611657 4758828 1 0309077-03 Nonachlorobiphenyls 6.52 µg/Kg 0.134 µg/Kg10/3/2000 EW-01 611657 4758828 1 0309077-03 Decachlorobiphenyl 0.276 J µg/Kg 0.0628 µg/Kg10/3/2000 EW-01 611657 4758828 1 0309077-03 Total Homologs 1230 µg/Kg 0.0628 µg/Kg10/3/2000 EW-01 611657 4758828 1 0309077-03 Percent Lipids 1.6 % 0.1 %10/3/2000 EW-01 611657 4758828 1 0309077-03 Percent Moisture 82.5 % 0.1 %10/3/2000 EW-02 613610 4762048 2 0309077-04 Cl2-BZ#8 2.69 µg/Kg 0.107 µg/Kg10/3/2000 EW-02 613610 4762048 2 0309077-04 Cl3-BZ#18 0.686 J µg/Kg 0.238 µg/Kg10/3/2000 EW-02 613610 4762048 2 0309077-04 Cl3-BZ#31/#28 12.8 µg/Kg 1.72 µg/Kg10/3/2000 EW-02 613610 4762048 2 0309077-04 Cl4-BZ#44 1.41 µg/Kg 0.163 µg/Kg10/3/2000 EW-02 613610 4762048 2 0309077-04 Cl4-BZ#45 0.218 U µg/Kg 0.218 µg/Kg10/3/2000 EW-02 613610 4762048 2 0309077-04 Cl4-BZ#47 1.48 µg/Kg 0.277 µg/Kg10/3/2000 EW-02 613610 4762048 2 0309077-04 Cl4-BZ#49 6.88 µg/Kg 0.136 µg/Kg10/3/2000 EW-02 613610 4762048 2 0309077-04 Cl4-BZ#52 9.23 µg/Kg 0.155 µg/Kg10/3/2000 EW-02 613610 4762048 2 0309077-04 Cl4-BZ#56 10.7 µg/Kg 0.0811 µg/Kg10/3/2000 EW-02 613610 4762048 2 0309077-04 Cl4-BZ#66 22.1 µg/Kg 0.108 µg/Kg10/3/2000 EW-02 613610 4762048 2 0309077-04 Cl4-BZ#70 21.9 µg/Kg 0.0948 µg/Kg10/3/2000 EW-02 613610 4762048 2 0309077-04 Cl4-BZ#74 11.6 µg/Kg 0.167 µg/Kg10/3/2000 EW-02 613610 4762048 2 0309077-04 Cl4-BZ#77 0.150 U µg/Kg 0.150 µg/Kg10/3/2000 EW-02 613610 4762048 2 0309077-04 Cl4-BZ#81 0.148 U µg/Kg 0.148 µg/Kg10/3/2000 EW-02 613610 4762048 2 0309077-04 Cl5-BZ#87 9.85 µg/Kg 0.0661 µg/Kg10/3/2000 EW-02 613610 4762048 2 0309077-04 Cl5-BZ#95 11.9 µg/Kg 0.0511 µg/Kg10/3/2000 EW-02 613610 4762048 2 0309077-04 Cl5-BZ#99 10.0 µg/Kg 0.0349 µg/Kg10/3/2000 EW-02 613610 4762048 2 0309077-04 Cl5-BZ#101 15.4 µg/Kg 0.0998 µg/Kg10/3/2000 EW-02 613610 4762048 2 0309077-04 Cl5-BZ#105 13.6 µg/Kg 0.0486 µg/Kg10/3/2000 EW-02 613610 4762048 2 0309077-04 Cl5-BZ#110 12.6 µg/Kg 0.0948 µg/Kg10/3/2000 EW-02 613610 4762048 2 0309077-04 Cl5-BZ#114 1.45 µg/Kg 0.0436 µg/Kg10/3/2000 EW-02 613610 4762048 2 0309077-04 Cl5-BZ#118 31.7 µg/Kg 0.102 µg/Kg10/3/2000 EW-02 613610 4762048 2 0309077-04 Cl5-BZ#123 0.0860 U µg/Kg 0.0860 µg/Kg10/3/2000 EW-02 613610 4762048 2 0309077-04 Cl5-BZ#126 0.0761 U µg/Kg 0.0761 µg/Kg10/3/2000 EW-02 613610 4762048 2 0309077-04 Cl6-BZ#128 2.70 µg/Kg 0.0686 µg/Kg10/3/2000 EW-02 613610 4762048 2 0309077-04 Cl6-BZ#138 27.4 µg/Kg 0.0985 µg/Kg10/3/2000 EW-02 613610 4762048 2 0309077-04 Cl6-BZ#146 2.99 µg/Kg 0.0623 µg/Kg10/3/2000 EW-02 613610 4762048 2 0309077-04 Cl6-BZ#149 20.7 µg/Kg 0.0798 µg/Kg10/3/2000 EW-02 613610 4762048 2 0309077-04 Cl6-BZ#151 6.16 µg/Kg 0.132 µg/Kg10/3/2000 EW-02 613610 4762048 2 0309077-04 Cl6-BZ#153 11.9 µg/Kg 0.113 µg/Kg



Extracted 7/30/04


EASTING (NAD83

UTM18N)

NORTHING (NAD83

UTM18N)SITE



LIMIT3

10/3/2000 EW-02 613610 4762048 2 0309077-04 Cl6-BZ#156 1.60 µg/Kg 0.0811 µg/Kg10/3/2000 EW-02 613610 4762048 2 0309077-04 Cl6-BZ#157 0.0636 U µg/Kg 0.0636 µg/Kg10/3/2000 EW-02 613610 4762048 2 0309077-04 Cl6-BZ#158 1.08 µg/Kg 0.0536 µg/Kg10/3/2000 EW-02 613610 4762048 2 0309077-04 Cl6-BZ#167 0.786 µg/Kg 0.0686 µg/Kg10/3/2000 EW-02 613610 4762048 2 0309077-04 Cl6-BZ#169 0.221 U µg/Kg 0.221 µg/Kg10/3/2000 EW-02 613610 4762048 2 0309077-04 Cl7-BZ#170 2.00 µg/Kg 0.257 µg/Kg10/3/2000 EW-02 613610 4762048 2 0309077-04 Cl7-BZ#174 1.50 µg/Kg 0.0524 µg/Kg10/3/2000 EW-02 613610 4762048 2 0309077-04 Cl7-BZ#177 1.51 µg/Kg 0.0736 µg/Kg10/3/2000 EW-02 613610 4762048 2 0309077-04 Cl7-BZ#180 2.32 µg/Kg 0.110 µg/Kg10/3/2000 EW-02 613610 4762048 2 0309077-04 Cl7-BZ#183 0.536 µg/Kg 0.0499 µg/Kg10/3/2000 EW-02 613610 4762048 2 0309077-04 Cl7-BZ#189 0.0985 U µg/Kg 0.0985 µg/Kg10/3/2000 EW-02 613610 4762048 2 0309077-04 Cl7-BZ#187 12.3 µg/Kg 0.0549 µg/Kg10/3/2000 EW-02 613610 4762048 2 0309077-04 Cl8-BZ#194 1.04 µg/Kg 0.115 µg/Kg10/3/2000 EW-02 613610 4762048 2 0309077-04 Cl8-BZ#195 0.330 J µg/Kg 0.113 µg/Kg10/3/2000 EW-02 613610 4762048 2 0309077-04 Cl8-BZ#201 3.92 µg/Kg 0.0998 µg/Kg10/3/2000 EW-02 613610 4762048 2 0309077-04 Cl9-BZ#206 4.46 µg/Kg 0.133 µg/Kg10/3/2000 EW-02 613610 4762048 2 0309077-04 Cl10-BZ#209 1.57 µg/Kg 0.0623 µg/Kg10/3/2000 EW-02 613610 4762048 2 0309077-04 Monochlorobiphenyls 3.67 U µg/Kg 3.67 µg/Kg10/3/2000 EW-02 613610 4762048 2 0309077-04 Dichlorobiphenyls 20.2 µg/Kg 0.107 µg/Kg10/3/2000 EW-02 613610 4762048 2 0309077-04 Trichlorobiphenyls 37.5 µg/Kg 0.368 µg/Kg10/3/2000 EW-02 613610 4762048 2 0309077-04 Tetrachlorobiphenyls 108 µg/Kg 0.0574 µg/Kg10/3/2000 EW-02 613610 4762048 2 0309077-04 Pentachlorobiphenyls 189 µg/Kg 0.0661 µg/Kg10/3/2000 EW-02 613610 4762048 2 0309077-04 Hexachlorobiphenyls 95.1 µg/Kg 0.105 µg/Kg10/3/2000 EW-02 613610 4762048 2 0309077-04 Heptachlorobiphenyls 20.3 µg/Kg 0.0574 µg/Kg10/3/2000 EW-02 613610 4762048 2 0309077-04 Octachlorobiphenyls 9.96 µg/Kg 0.0524 µg/Kg10/3/2000 EW-02 613610 4762048 2 0309077-04 Nonachlorobiphenyls 15.0 µg/Kg 0.133 µg/Kg10/3/2000 EW-02 613610 4762048 2 0309077-04 Decachlorobiphenyl 1.57 µg/Kg 0.0623 µg/Kg10/3/2000 EW-02 613610 4762048 2 0309077-04 Total Homologs 496 µg/Kg 0.0623 µg/Kg10/3/2000 EW-02 613610 4762048 2 0309077-04 Percent Lipids 2.0 % 0.1 %10/3/2000 EW-02 613610 4762048 2 0309077-04 Percent Moisture 80.1 % 0.1 %10/3/2000 EW-03 613914 4762430 3 0309077-05 Cl2-BZ#8 0.103 U µg/Kg 0.103 µg/Kg10/3/2000 EW-03 613914 4762430 3 0309077-05 Cl3-BZ#18 0.229 U µg/Kg 0.229 µg/Kg10/3/2000 EW-03 613914 4762430 3 0309077-05 Cl3-BZ#31/#28 7.17 J µg/Kg 1.65 µg/Kg10/3/2000 EW-03 613914 4762430 3 0309077-05 Cl4-BZ#44 0.157 U µg/Kg 0.157 µg/Kg10/3/2000 EW-03 613914 4762430 3 0309077-05 Cl4-BZ#45 0.210 U µg/Kg 0.210 µg/Kg



Extracted 7/30/04


EASTING (NAD83

UTM18N)

NORTHING (NAD83

UTM18N)SITE



LIMIT3

10/3/2000 EW-03 613914 4762430 3 0309077-05 Cl4-BZ#47 0.266 U µg/Kg 0.266 µg/Kg10/3/2000 EW-03 613914 4762430 3 0309077-05 Cl4-BZ#49 0.222 J µg/Kg 0.131 µg/Kg10/3/2000 EW-03 613914 4762430 3 0309077-05 Cl4-BZ#52 0.341 J µg/Kg 0.148 µg/Kg10/3/2000 EW-03 613914 4762430 3 0309077-05 Cl4-BZ#56 0.521 µg/Kg 0.0779 µg/Kg10/3/2000 EW-03 613914 4762430 3 0309077-05 Cl4-BZ#66 0.257 J µg/Kg 0.104 µg/Kg10/3/2000 EW-03 613914 4762430 3 0309077-05 Cl4-BZ#70 0.299 J µg/Kg 0.0910 µg/Kg10/3/2000 EW-03 613914 4762430 3 0309077-05 Cl4-BZ#74 0.161 U µg/Kg 0.161 µg/Kg10/3/2000 EW-03 613914 4762430 3 0309077-05 Cl4-BZ#77 0.144 U µg/Kg 0.144 µg/Kg10/3/2000 EW-03 613914 4762430 3 0309077-05 Cl4-BZ#81 0.142 U µg/Kg 0.142 µg/Kg10/3/2000 EW-03 613914 4762430 3 0309077-05 Cl5-BZ#87 0.210 J µg/Kg 0.0635 µg/Kg10/3/2000 EW-03 613914 4762430 3 0309077-05 Cl5-BZ#95 0.102 J µg/Kg 0.0491 µg/Kg10/3/2000 EW-03 613914 4762430 3 0309077-05 Cl5-BZ#99 0.407 µg/Kg 0.0335 µg/Kg10/3/2000 EW-03 613914 4762430 3 0309077-05 Cl5-BZ#101 0.443 J µg/Kg 0.0958 µg/Kg10/3/2000 EW-03 613914 4762430 3 0309077-05 Cl5-BZ#105 0.575 µg/Kg 0.0467 µg/Kg10/3/2000 EW-03 613914 4762430 3 0309077-05 Cl5-BZ#110 0.323 J µg/Kg 0.0910 µg/Kg10/3/2000 EW-03 613914 4762430 3 0309077-05 Cl5-BZ#114 0.0419 U µg/Kg 0.0419 µg/Kg10/3/2000 EW-03 613914 4762430 3 0309077-05 Cl5-BZ#118 0.659 µg/Kg 0.0982 µg/Kg10/3/2000 EW-03 613914 4762430 3 0309077-05 Cl5-BZ#123 0.0826 U µg/Kg 0.0826 µg/Kg10/3/2000 EW-03 613914 4762430 3 0309077-05 Cl5-BZ#126 0.0731 U µg/Kg 0.0731 µg/Kg10/3/2000 EW-03 613914 4762430 3 0309077-05 Cl6-BZ#128 0.0659 U µg/Kg 0.0659 µg/Kg10/3/2000 EW-03 613914 4762430 3 0309077-05 Cl6-BZ#138 1.65 µg/Kg 0.0946 µg/Kg10/3/2000 EW-03 613914 4762430 3 0309077-05 Cl6-BZ#146 0.275 J µg/Kg 0.0599 µg/Kg10/3/2000 EW-03 613914 4762430 3 0309077-05 Cl6-BZ#149 0.431 µg/Kg 0.0767 µg/Kg10/3/2000 EW-03 613914 4762430 3 0309077-05 Cl6-BZ#151 0.186 J µg/Kg 0.127 µg/Kg10/3/2000 EW-03 613914 4762430 3 0309077-05 Cl6-BZ#153 1.13 µg/Kg 0.109 µg/Kg10/3/2000 EW-03 613914 4762430 3 0309077-05 Cl6-BZ#156 0.0779 U µg/Kg 0.0779 µg/Kg10/3/2000 EW-03 613914 4762430 3 0309077-05 Cl6-BZ#157 0.0611 U µg/Kg 0.0611 µg/Kg10/3/2000 EW-03 613914 4762430 3 0309077-05 Cl6-BZ#158 0.0898 J µg/Kg 0.0515 µg/Kg10/3/2000 EW-03 613914 4762430 3 0309077-05 Cl6-BZ#167 0.0659 U µg/Kg 0.0659 µg/Kg10/3/2000 EW-03 613914 4762430 3 0309077-05 Cl6-BZ#169 0.212 U µg/Kg 0.212 µg/Kg10/3/2000 EW-03 613914 4762430 3 0309077-05 Cl7-BZ#170 0.247 U µg/Kg 0.247 µg/Kg10/3/2000 EW-03 613914 4762430 3 0309077-05 Cl7-BZ#174 0.0503 U µg/Kg 0.0503 µg/Kg10/3/2000 EW-03 613914 4762430 3 0309077-05 Cl7-BZ#177 0.0707 U µg/Kg 0.0707 µg/Kg10/3/2000 EW-03 613914 4762430 3 0309077-05 Cl7-BZ#180 0.216 J µg/Kg 0.105 µg/Kg10/3/2000 EW-03 613914 4762430 3 0309077-05 Cl7-BZ#183 0.0479 U µg/Kg 0.0479 µg/Kg



Extracted 7/30/04


EASTING (NAD83

UTM18N)

NORTHING (NAD83

UTM18N)SITE



LIMIT3

10/3/2000 EW-03 613914 4762430 3 0309077-05 Cl7-BZ#189 0.0946 U µg/Kg 0.0946 µg/Kg10/3/2000 EW-03 613914 4762430 3 0309077-05 Cl7-BZ#187 0.551 µg/Kg 0.0527 µg/Kg10/3/2000 EW-03 613914 4762430 3 0309077-05 Cl8-BZ#194 0.110 U µg/Kg 0.110 µg/Kg10/3/2000 EW-03 613914 4762430 3 0309077-05 Cl8-BZ#195 0.109 U µg/Kg 0.109 µg/Kg10/3/2000 EW-03 613914 4762430 3 0309077-05 Cl8-BZ#201 0.0958 U µg/Kg 0.0958 µg/Kg10/3/2000 EW-03 613914 4762430 3 0309077-05 Cl9-BZ#206 0.128 U µg/Kg 0.128 µg/Kg10/3/2000 EW-03 613914 4762430 3 0309077-05 Cl10-BZ#209 0.0599 U µg/Kg 0.0599 µg/Kg10/3/2000 EW-03 613914 4762430 3 0309077-05 Monochlorobiphenyls 3.52 U µg/Kg 3.52 µg/Kg10/3/2000 EW-03 613914 4762430 3 0309077-05 Dichlorobiphenyls 0.103 U µg/Kg 0.103 µg/Kg10/3/2000 EW-03 613914 4762430 3 0309077-05 Trichlorobiphenyls 7.08 µg/Kg 0.353 µg/Kg10/3/2000 EW-03 613914 4762430 3 0309077-05 Tetrachlorobiphenyls 7.14 µg/Kg 0.0551 µg/Kg10/3/2000 EW-03 613914 4762430 3 0309077-05 Pentachlorobiphenyls 10.7 µg/Kg 0.0635 µg/Kg10/3/2000 EW-03 613914 4762430 3 0309077-05 Hexachlorobiphenyls 5.58 µg/Kg 0.101 µg/Kg10/3/2000 EW-03 613914 4762430 3 0309077-05 Heptachlorobiphenyls 1.44 µg/Kg 0.0551 µg/Kg10/3/2000 EW-03 613914 4762430 3 0309077-05 Octachlorobiphenyls 0.359 µg/Kg 0.0503 µg/Kg10/3/2000 EW-03 613914 4762430 3 0309077-05 Nonachlorobiphenyls 0.128 U µg/Kg 0.128 µg/Kg10/3/2000 EW-03 613914 4762430 3 0309077-05 Decachlorobiphenyl 0.0599 U µg/Kg 0.0599 µg/Kg10/3/2000 EW-03 613914 4762430 3 0309077-05 Total Homologs 32.3 µg/Kg 0.0599 µg/Kg10/3/2000 EW-03 613914 4762430 3 0309077-05 Percent Lipids 1.8 % 0.1 %10/3/2000 EW-03 613914 4762430 3 0309077-05 Percent Moisture 77.3 % 0.1 %10/3/2000 EW-04 614694 4765912 4 0309077-06 Cl2-BZ#8 3.77 µg/Kg 0.111 µg/Kg10/3/2000 EW-04 614694 4765912 4 0309077-06 Cl3-BZ#18 6.47 µg/Kg 0.247 µg/Kg10/3/2000 EW-04 614694 4765912 4 0309077-06 Cl3-BZ#31/#28 180 µg/Kg 1.78 µg/Kg10/3/2000 EW-04 614694 4765912 4 0309077-06 Cl4-BZ#44 40.6 µg/Kg 0.170 µg/Kg10/3/2000 EW-04 614694 4765912 4 0309077-06 Cl4-BZ#45 7.16 µg/Kg 0.227 µg/Kg10/3/2000 EW-04 614694 4765912 4 0309077-06 Cl4-BZ#47 61.4 µg/Kg 0.288 µg/Kg10/3/2000 EW-04 614694 4765912 4 0309077-06 Cl4-BZ#49 102 µg/Kg 0.141 µg/Kg10/3/2000 EW-04 614694 4765912 4 0309077-06 Cl4-BZ#52 138 µg/Kg 0.161 µg/Kg10/3/2000 EW-04 614694 4765912 4 0309077-06 Cl4-BZ#56 53.7 µg/Kg 0.0842 µg/Kg10/3/2000 EW-04 614694 4765912 4 0309077-06 Cl4-BZ#66 105 µg/Kg 0.113 µg/Kg10/3/2000 EW-04 614694 4765912 4 0309077-06 Cl4-BZ#70 102 µg/Kg 0.0984 µg/Kg10/3/2000 EW-04 614694 4765912 4 0309077-06 Cl4-BZ#74 58.3 µg/Kg 0.174 µg/Kg10/3/2000 EW-04 614694 4765912 4 0309077-06 Cl4-BZ#77 0.155 U µg/Kg 0.155 µg/Kg10/3/2000 EW-04 614694 4765912 4 0309077-06 Cl4-BZ#81 0.154 U µg/Kg 0.154 µg/Kg10/3/2000 EW-04 614694 4765912 4 0309077-06 Cl5-BZ#87 38.6 µg/Kg 0.0687 µg/Kg



Extracted 7/30/04


EASTING (NAD83

UTM18N)

NORTHING (NAD83

UTM18N)SITE



LIMIT3

10/3/2000 EW-04 614694 4765912 4 0309077-06 Cl5-BZ#95 63.6 µg/Kg 0.0531 µg/Kg10/3/2000 EW-04 614694 4765912 4 0309077-06 Cl5-BZ#99 57.0 µg/Kg 0.0363 µg/Kg10/3/2000 EW-04 614694 4765912 4 0309077-06 Cl5-BZ#101 100 µg/Kg 0.104 µg/Kg10/3/2000 EW-04 614694 4765912 4 0309077-06 Cl5-BZ#105 35.8 µg/Kg 0.0505 µg/Kg10/3/2000 EW-04 614694 4765912 4 0309077-06 Cl5-BZ#110 96.5 µg/Kg 0.0984 µg/Kg10/3/2000 EW-04 614694 4765912 4 0309077-06 Cl5-BZ#114 3.37 µg/Kg 0.0453 µg/Kg10/3/2000 EW-04 614694 4765912 4 0309077-06 Cl5-BZ#118 84.8 µg/Kg 0.106 µg/Kg10/3/2000 EW-04 614694 4765912 4 0309077-06 Cl5-BZ#123 0.0894 U µg/Kg 0.0894 µg/Kg10/3/2000 EW-04 614694 4765912 4 0309077-06 Cl5-BZ#126 0.0790 U µg/Kg 0.0790 µg/Kg10/3/2000 EW-04 614694 4765912 4 0309077-06 Cl6-BZ#128 8.09 µg/Kg 0.0712 µg/Kg10/3/2000 EW-04 614694 4765912 4 0309077-06 Cl6-BZ#138 74.6 µg/Kg 0.102 µg/Kg10/3/2000 EW-04 614694 4765912 4 0309077-06 Cl6-BZ#146 12.3 µg/Kg 0.0648 µg/Kg10/3/2000 EW-04 614694 4765912 4 0309077-06 Cl6-BZ#149 50.0 µg/Kg 0.0829 µg/Kg10/3/2000 EW-04 614694 4765912 4 0309077-06 Cl6-BZ#151 10.9 µg/Kg 0.137 µg/Kg10/3/2000 EW-04 614694 4765912 4 0309077-06 Cl6-BZ#153 46.3 µg/Kg 0.118 µg/Kg10/3/2000 EW-04 614694 4765912 4 0309077-06 Cl6-BZ#156 4.88 µg/Kg 0.0842 µg/Kg10/3/2000 EW-04 614694 4765912 4 0309077-06 Cl6-BZ#157 0.978 µg/Kg 0.0661 µg/Kg10/3/2000 EW-04 614694 4765912 4 0309077-06 Cl6-BZ#158 3.98 µg/Kg 0.0557 µg/Kg10/3/2000 EW-04 614694 4765912 4 0309077-06 Cl6-BZ#167 2.44 µg/Kg 0.0712 µg/Kg10/3/2000 EW-04 614694 4765912 4 0309077-06 Cl6-BZ#169 0.229 U µg/Kg 0.229 µg/Kg10/3/2000 EW-04 614694 4765912 4 0309077-06 Cl7-BZ#170 7.51 µg/Kg 0.267 µg/Kg10/3/2000 EW-04 614694 4765912 4 0309077-06 Cl7-BZ#174 3.37 µg/Kg 0.0544 µg/Kg10/3/2000 EW-04 614694 4765912 4 0309077-06 Cl7-BZ#177 3.83 µg/Kg 0.0764 µg/Kg10/3/2000 EW-04 614694 4765912 4 0309077-06 Cl7-BZ#180 10.7 µg/Kg 0.114 µg/Kg10/3/2000 EW-04 614694 4765912 4 0309077-06 Cl7-BZ#183 2.40 µg/Kg 0.0518 µg/Kg10/3/2000 EW-04 614694 4765912 4 0309077-06 Cl7-BZ#189 0.102 U µg/Kg 0.102 µg/Kg10/3/2000 EW-04 614694 4765912 4 0309077-06 Cl7-BZ#187 26.4 µg/Kg 0.0570 µg/Kg10/3/2000 EW-04 614694 4765912 4 0309077-06 Cl8-BZ#194 1.96 µg/Kg 0.119 µg/Kg10/3/2000 EW-04 614694 4765912 4 0309077-06 Cl8-BZ#195 0.822 µg/Kg 0.118 µg/Kg10/3/2000 EW-04 614694 4765912 4 0309077-06 Cl8-BZ#201 4.77 µg/Kg 0.104 µg/Kg10/3/2000 EW-04 614694 4765912 4 0309077-06 Cl9-BZ#206 1.64 µg/Kg 0.139 µg/Kg10/3/2000 EW-04 614694 4765912 4 0309077-06 Cl10-BZ#209 0.563 µg/Kg 0.0648 µg/Kg10/3/2000 EW-04 614694 4765912 4 0309077-06 Monochlorobiphenyls 3.81 U µg/Kg 3.81 µg/Kg10/3/2000 EW-04 614694 4765912 4 0309077-06 Dichlorobiphenyls 55.8 µg/Kg 0.111 µg/Kg10/3/2000 EW-04 614694 4765912 4 0309077-06 Trichlorobiphenyls 290 µg/Kg 0.382 µg/Kg



Extracted 7/30/04


EASTING (NAD83

UTM18N)

NORTHING (NAD83

UTM18N)SITE



LIMIT3

10/3/2000 EW-04 614694 4765912 4 0309077-06 Tetrachlorobiphenyls 883 µg/Kg 0.0596 µg/Kg10/3/2000 EW-04 614694 4765912 4 0309077-06 Pentachlorobiphenyls 851 µg/Kg 0.0687 µg/Kg10/3/2000 EW-04 614694 4765912 4 0309077-06 Hexachlorobiphenyls 268 µg/Kg 0.109 µg/Kg10/3/2000 EW-04 614694 4765912 4 0309077-06 Heptachlorobiphenyls 53.1 µg/Kg 0.0596 µg/Kg10/3/2000 EW-04 614694 4765912 4 0309077-06 Octachlorobiphenyls 10.4 µg/Kg 0.0544 µg/Kg10/3/2000 EW-04 614694 4765912 4 0309077-06 Nonachlorobiphenyls 8.34 µg/Kg 0.139 µg/Kg10/3/2000 EW-04 614694 4765912 4 0309077-06 Decachlorobiphenyl 0.563 µg/Kg 0.0648 µg/Kg10/3/2000 EW-04 614694 4765912 4 0309077-06 Total Homologs 2420 µg/Kg 0.0648 µg/Kg10/3/2000 EW-04 614694 4765912 4 0309077-06 Percent Lipids 2.5 % 0.1 %10/3/2000 EW-04 614694 4765912 4 0309077-06 Percent Moisture 82.1 % 0.1 %10/3/2000 EW-05 615965 4768361 5 0309077-07 Cl2-BZ#8 5.48 µg/Kg 0.111 µg/Kg10/3/2000 EW-05 615965 4768361 5 0309077-07 Cl3-BZ#18 15.1 J µg/Kg 0.247 µg/Kg10/3/2000 EW-05 615965 4768361 5 0309077-07 Cl3-BZ#31/#28 577 µg/Kg 1.78 µg/Kg10/3/2000 EW-05 615965 4768361 5 0309077-07 Cl4-BZ#44 292 µg/Kg 0.169 µg/Kg10/3/2000 EW-05 615965 4768361 5 0309077-07 Cl4-BZ#45 18.2 µg/Kg 0.227 µg/Kg10/3/2000 EW-05 615965 4768361 5 0309077-07 Cl4-BZ#47 210 µg/Kg 0.287 µg/Kg10/3/2000 EW-05 615965 4768361 5 0309077-07 Cl4-BZ#49 284 µg/Kg 0.141 µg/Kg10/3/2000 EW-05 615965 4768361 5 0309077-07 Cl4-BZ#52 465 D µg/Kg 0.383 µg/Kg10/3/2000 EW-05 615965 4768361 5 0309077-07 Cl4-BZ#56 217 µg/Kg 0.0841 µg/Kg10/3/2000 EW-05 615965 4768361 5 0309077-07 Cl4-BZ#66 335 D µg/Kg 0.269 µg/Kg10/3/2000 EW-05 615965 4768361 5 0309077-07 Cl4-BZ#70 356 D µg/Kg 0.235 µg/Kg10/3/2000 EW-05 615965 4768361 5 0309077-07 Cl4-BZ#74 202 µg/Kg 0.173 µg/Kg10/3/2000 EW-05 615965 4768361 5 0309077-07 Cl4-BZ#77 0.155 U µg/Kg 0.155 µg/Kg10/3/2000 EW-05 615965 4768361 5 0309077-07 Cl4-BZ#81 0.154 U µg/Kg 0.154 µg/Kg10/3/2000 EW-05 615965 4768361 5 0309077-07 Cl5-BZ#87 109 µg/Kg 0.0686 µg/Kg10/3/2000 EW-05 615965 4768361 5 0309077-07 Cl5-BZ#95 172 µg/Kg 0.0531 µg/Kg10/3/2000 EW-05 615965 4768361 5 0309077-07 Cl5-BZ#99 114 µg/Kg 0.0362 µg/Kg10/3/2000 EW-05 615965 4768361 5 0309077-07 Cl5-BZ#101 214 µg/Kg 0.104 µg/Kg10/3/2000 EW-05 615965 4768361 5 0309077-07 Cl5-BZ#105 73.4 µg/Kg 0.0505 µg/Kg10/3/2000 EW-05 615965 4768361 5 0309077-07 Cl5-BZ#110 204 µg/Kg 0.0984 µg/Kg10/3/2000 EW-05 615965 4768361 5 0309077-07 Cl5-BZ#114 7.85 J µg/Kg 0.0453 µg/Kg10/3/2000 EW-05 615965 4768361 5 0309077-07 Cl5-BZ#118 141 µg/Kg 0.106 µg/Kg10/3/2000 EW-05 615965 4768361 5 0309077-07 Cl5-BZ#123 R µg/Kg 0.0893 µg/Kg10/3/2000 EW-05 615965 4768361 5 0309077-07 Cl5-BZ#126 0.0789 U µg/Kg 0.0789 µg/Kg10/3/2000 EW-05 615965 4768361 5 0309077-07 Cl6-BZ#128 11.7 µg/Kg 0.0712 µg/Kg



Extracted 7/30/04


EASTING (NAD83

UTM18N)

NORTHING (NAD83

UTM18N)SITE



LIMIT3

10/3/2000 EW-05 615965 4768361 5 0309077-07 Cl6-BZ#138 122 µg/Kg 0.102 µg/Kg10/3/2000 EW-05 615965 4768361 5 0309077-07 Cl6-BZ#146 13.8 µg/Kg 0.0647 µg/Kg10/3/2000 EW-05 615965 4768361 5 0309077-07 Cl6-BZ#149 124 µg/Kg 0.0828 µg/Kg10/3/2000 EW-05 615965 4768361 5 0309077-07 Cl6-BZ#151 32.8 µg/Kg 0.137 µg/Kg10/3/2000 EW-05 615965 4768361 5 0309077-07 Cl6-BZ#153 49.8 µg/Kg 0.118 µg/Kg10/3/2000 EW-05 615965 4768361 5 0309077-07 Cl6-BZ#156 5.71 µg/Kg 0.0841 µg/Kg10/3/2000 EW-05 615965 4768361 5 0309077-07 Cl6-BZ#157 1.22 µg/Kg 0.0660 µg/Kg10/3/2000 EW-05 615965 4768361 5 0309077-07 Cl6-BZ#158 3.56 µg/Kg 0.0557 µg/Kg10/3/2000 EW-05 615965 4768361 5 0309077-07 Cl6-BZ#167 2.45 µg/Kg 0.0712 µg/Kg10/3/2000 EW-05 615965 4768361 5 0309077-07 Cl6-BZ#169 0.229 U µg/Kg 0.229 µg/Kg10/3/2000 EW-05 615965 4768361 5 0309077-07 Cl7-BZ#170 7.03 µg/Kg 0.267 µg/Kg10/3/2000 EW-05 615965 4768361 5 0309077-07 Cl7-BZ#174 8.07 µg/Kg 0.0544 µg/Kg10/3/2000 EW-05 615965 4768361 5 0309077-07 Cl7-BZ#177 5.40 µg/Kg 0.0764 µg/Kg10/3/2000 EW-05 615965 4768361 5 0309077-07 Cl7-BZ#180 7.56 µg/Kg 0.114 µg/Kg10/3/2000 EW-05 615965 4768361 5 0309077-07 Cl7-BZ#183 2.85 µg/Kg 0.0518 µg/Kg10/3/2000 EW-05 615965 4768361 5 0309077-07 Cl7-BZ#189 0.705 J µg/Kg 0.102 µg/Kg10/3/2000 EW-05 615965 4768361 5 0309077-07 Cl7-BZ#187 58.0 µg/Kg 0.0569 µg/Kg10/3/2000 EW-05 615965 4768361 5 0309077-07 Cl8-BZ#194 1.99 µg/Kg 0.119 µg/Kg10/3/2000 EW-05 615965 4768361 5 0309077-07 Cl8-BZ#195 0.835 µg/Kg 0.118 µg/Kg10/3/2000 EW-05 615965 4768361 5 0309077-07 Cl8-BZ#201 9.60 µg/Kg 0.104 µg/Kg10/3/2000 EW-05 615965 4768361 5 0309077-07 Cl9-BZ#206 3.82 µg/Kg 0.139 µg/Kg10/3/2000 EW-05 615965 4768361 5 0309077-07 Cl10-BZ#209 1.03 µg/Kg 0.0647 µg/Kg10/3/2000 EW-05 615965 4768361 5 0309077-07 Monochlorobiphenyls 3.80 U µg/Kg 3.80 µg/Kg10/3/2000 EW-05 615965 4768361 5 0309077-07 Dichlorobiphenyls 55.4 µg/Kg 0.111 µg/Kg10/3/2000 EW-05 615965 4768361 5 0309077-07 Trichlorobiphenyls 814 µg/Kg 0.382 µg/Kg10/3/2000 EW-05 615965 4768361 5 0309077-07 Tetrachlorobiphenyls 2990 µg/Kg 0.0595 µg/Kg10/3/2000 EW-05 615965 4768361 5 0309077-07 Pentachlorobiphenyls 1860 µg/Kg 0.0686 µg/Kg10/3/2000 EW-05 615965 4768361 5 0309077-07 Hexachlorobiphenyls 449 µg/Kg 0.109 µg/Kg10/3/2000 EW-05 615965 4768361 5 0309077-07 Heptachlorobiphenyls 96.7 µg/Kg 0.0595 µg/Kg10/3/2000 EW-05 615965 4768361 5 0309077-07 Octachlorobiphenyls 17.3 µg/Kg 0.0544 µg/Kg10/3/2000 EW-05 615965 4768361 5 0309077-07 Nonachlorobiphenyls 13.6 µg/Kg 0.139 µg/Kg10/3/2000 EW-05 615965 4768361 5 0309077-07 Decachlorobiphenyl 1.03 µg/Kg 0.0647 µg/Kg10/3/2000 EW-05 615965 4768361 5 0309077-07 Total Homologs 6310 µg/Kg 0.0647 µg/Kg10/3/2000 EW-05 615965 4768361 5 0309077-07 Percent Lipids 1.8 % 0.1 %10/3/2000 EW-05 615965 4768361 5 0309077-07 Percent Moisture 80.1 % 0.1 %



Extracted 7/30/04


EASTING (NAD83

UTM18N)

NORTHING (NAD83

UTM18N)SITE



LIMIT3

10/3/2000 EW-06 615681 4772203 6 0309077-08 Cl2-BZ#8 6.70 µg/Kg 0.115 µg/Kg10/3/2000 EW-06 615681 4772203 6 0309077-08 Cl3-BZ#18 17.2 µg/Kg 0.255 µg/Kg10/3/2000 EW-06 615681 4772203 6 0309077-08 Cl3-BZ#31/#28 1090 D µg/Kg 5.94 µg/Kg10/3/2000 EW-06 615681 4772203 6 0309077-08 Cl4-BZ#44 468 D µg/Kg 0.565 µg/Kg10/3/2000 EW-06 615681 4772203 6 0309077-08 Cl4-BZ#45 36.6 µg/Kg 0.233 µg/Kg10/3/2000 EW-06 615681 4772203 6 0309077-08 Cl4-BZ#47 290 µg/Kg 0.296 µg/Kg10/3/2000 EW-06 615681 4772203 6 0309077-08 Cl4-BZ#49 652 D µg/Kg 0.470 µg/Kg10/3/2000 EW-06 615681 4772203 6 0309077-08 Cl4-BZ#52 878 D µg/Kg 0.535 µg/Kg10/3/2000 EW-06 615681 4772203 6 0309077-08 Cl4-BZ#56 421 D µg/Kg 0.280 µg/Kg10/3/2000 EW-06 615681 4772203 6 0309077-08 Cl4-BZ#66 682 D µg/Kg 0.375 µg/Kg10/3/2000 EW-06 615681 4772203 6 0309077-08 Cl4-BZ#70 628 D µg/Kg 0.328 µg/Kg10/3/2000 EW-06 615681 4772203 6 0309077-08 Cl4-BZ#74 424 D µg/Kg 0.578 µg/Kg10/3/2000 EW-06 615681 4772203 6 0309077-08 Cl4-BZ#77 0.160 U µg/Kg 0.160 µg/Kg10/3/2000 EW-06 615681 4772203 6 0309077-08 Cl4-BZ#81 0.159 U µg/Kg 0.159 µg/Kg10/3/2000 EW-06 615681 4772203 6 0309077-08 Cl5-BZ#87 213 µg/Kg 0.0706 µg/Kg10/3/2000 EW-06 615681 4772203 6 0309077-08 Cl5-BZ#95 292 µg/Kg 0.0546 µg/Kg10/3/2000 EW-06 615681 4772203 6 0309077-08 Cl5-BZ#99 222 µg/Kg 0.0373 µg/Kg10/3/2000 EW-06 615681 4772203 6 0309077-08 Cl5-BZ#101 422 D µg/Kg 0.345 µg/Kg10/3/2000 EW-06 615681 4772203 6 0309077-08 Cl5-BZ#105 152 µg/Kg 0.0520 µg/Kg10/3/2000 EW-06 615681 4772203 6 0309077-08 Cl5-BZ#110 403 D µg/Kg 0.328 µg/Kg10/3/2000 EW-06 615681 4772203 6 0309077-08 Cl5-BZ#114 19.6 µg/Kg 0.0466 µg/Kg10/3/2000 EW-06 615681 4772203 6 0309077-08 Cl5-BZ#118 288 µg/Kg 0.109 µg/Kg10/3/2000 EW-06 615681 4772203 6 0309077-08 Cl5-BZ#123 0.0919 U µg/Kg 0.0919 µg/Kg10/3/2000 EW-06 615681 4772203 6 0309077-08 Cl5-BZ#126 0.0813 U µg/Kg 0.0813 µg/Kg10/3/2000 EW-06 615681 4772203 6 0309077-08 Cl6-BZ#128 20.7 µg/Kg 0.0733 µg/Kg10/3/2000 EW-06 615681 4772203 6 0309077-08 Cl6-BZ#138 193 µg/Kg 0.105 µg/Kg10/3/2000 EW-06 615681 4772203 6 0309077-08 Cl6-BZ#146 27.8 µg/Kg 0.0666 µg/Kg10/3/2000 EW-06 615681 4772203 6 0309077-08 Cl6-BZ#149 151 µg/Kg 0.0853 µg/Kg10/3/2000 EW-06 615681 4772203 6 0309077-08 Cl6-BZ#151 35.5 µg/Kg 0.141 µg/Kg10/3/2000 EW-06 615681 4772203 6 0309077-08 Cl6-BZ#153 105 µg/Kg 0.121 µg/Kg10/3/2000 EW-06 615681 4772203 6 0309077-08 Cl6-BZ#156 14.7 µg/Kg 0.0866 µg/Kg10/3/2000 EW-06 615681 4772203 6 0309077-08 Cl6-BZ#157 2.21 µg/Kg 0.0680 µg/Kg10/3/2000 EW-06 615681 4772203 6 0309077-08 Cl6-BZ#158 9.77 µg/Kg 0.0573 µg/Kg10/3/2000 EW-06 615681 4772203 6 0309077-08 Cl6-BZ#167 6.65 µg/Kg 0.0733 µg/Kg10/3/2000 EW-06 615681 4772203 6 0309077-08 Cl6-BZ#169 0.236 U µg/Kg 0.236 µg/Kg



Extracted 7/30/04


EASTING (NAD83

UTM18N)

NORTHING (NAD83

UTM18N)SITE



LIMIT3

10/3/2000 EW-06 615681 4772203 6 0309077-08 Cl7-BZ#170 15.0 µg/Kg 0.275 µg/Kg10/3/2000 EW-06 615681 4772203 6 0309077-08 Cl7-BZ#174 9.61 µg/Kg 0.0560 µg/Kg10/3/2000 EW-06 615681 4772203 6 0309077-08 Cl7-BZ#177 8.48 µg/Kg 0.0786 µg/Kg10/3/2000 EW-06 615681 4772203 6 0309077-08 Cl7-BZ#180 25.6 µg/Kg 0.117 µg/Kg10/3/2000 EW-06 615681 4772203 6 0309077-08 Cl7-BZ#183 5.18 µg/Kg 0.0533 µg/Kg10/3/2000 EW-06 615681 4772203 6 0309077-08 Cl7-BZ#189 0.799 J µg/Kg 0.105 µg/Kg10/3/2000 EW-06 615681 4772203 6 0309077-08 Cl7-BZ#187 62.1 µg/Kg 0.0586 µg/Kg10/3/2000 EW-06 615681 4772203 6 0309077-08 Cl8-BZ#194 4.92 µg/Kg 0.123 µg/Kg10/3/2000 EW-06 615681 4772203 6 0309077-08 Cl8-BZ#195 2.02 µg/Kg 0.121 µg/Kg10/3/2000 EW-06 615681 4772203 6 0309077-08 Cl8-BZ#201 9.27 µg/Kg 0.107 µg/Kg10/3/2000 EW-06 615681 4772203 6 0309077-08 Cl9-BZ#206 3.62 µg/Kg 0.143 µg/Kg10/3/2000 EW-06 615681 4772203 6 0309077-08 Cl10-BZ#209 1.04 µg/Kg 0.0666 µg/Kg10/3/2000 EW-06 615681 4772203 6 0309077-08 Monochlorobiphenyls 3.92 U µg/Kg 3.92 µg/Kg10/3/2000 EW-06 615681 4772203 6 0309077-08 Dichlorobiphenyls 69.7 µg/Kg 0.115 µg/Kg10/3/2000 EW-06 615681 4772203 6 0309077-08 Trichlorobiphenyls 1320 µg/Kg 0.393 µg/Kg10/3/2000 EW-06 615681 4772203 6 0309077-08 Tetrachlorobiphenyls 5410 µg/Kg 0.0613 µg/Kg10/3/2000 EW-06 615681 4772203 6 0309077-08 Pentachlorobiphenyls 3600 µg/Kg 0.0706 µg/Kg10/3/2000 EW-06 615681 4772203 6 0309077-08 Hexachlorobiphenyls 733 µg/Kg 0.112 µg/Kg10/3/2000 EW-06 615681 4772203 6 0309077-08 Heptachlorobiphenyls 134 µg/Kg 0.0613 µg/Kg10/3/2000 EW-06 615681 4772203 6 0309077-08 Octachlorobiphenyls 23.1 µg/Kg 0.0560 µg/Kg10/3/2000 EW-06 615681 4772203 6 0309077-08 Nonachlorobiphenyls 11.2 µg/Kg 0.143 µg/Kg10/3/2000 EW-06 615681 4772203 6 0309077-08 Decachlorobiphenyl 1.04 µg/Kg 0.0666 µg/Kg10/3/2000 EW-06 615681 4772203 6 0309077-08 Total Homologs 11300 µg/Kg 0.0666 µg/Kg10/3/2000 EW-06 615681 4772203 6 0309077-08 Percent Lipids 1.6 % 0.1 %10/3/2000 EW-06 615681 4772203 6 0309077-08 Percent Moisture 78.1 % 0.1 %10/5/2000 EW-07 614692 4781163 7 0309077-09 Cl2-BZ#8 0.104 U µg/Kg 0.104 µg/Kg10/5/2000 EW-07 614692 4781163 7 0309077-09 Cl3-BZ#18 0.363 J µg/Kg 0.231 µg/Kg10/5/2000 EW-07 614692 4781163 7 0309077-09 Cl3-BZ#31/#28 7.13 J µg/Kg 1.66 µg/Kg10/5/2000 EW-07 614692 4781163 7 0309077-09 Cl4-BZ#44 1.27 µg/Kg 0.158 µg/Kg10/5/2000 EW-07 614692 4781163 7 0309077-09 Cl4-BZ#45 0.326 J µg/Kg 0.211 µg/Kg10/5/2000 EW-07 614692 4781163 7 0309077-09 Cl4-BZ#47 1.71 J µg/Kg 0.268 µg/Kg10/5/2000 EW-07 614692 4781163 7 0309077-09 Cl4-BZ#49 3.89 µg/Kg 0.132 µg/Kg10/5/2000 EW-07 614692 4781163 7 0309077-09 Cl4-BZ#52 5.35 µg/Kg 0.150 µg/Kg10/5/2000 EW-07 614692 4781163 7 0309077-09 Cl4-BZ#56 4.13 µg/Kg 0.0785 µg/Kg10/5/2000 EW-07 614692 4781163 7 0309077-09 Cl4-BZ#66 8.09 µg/Kg 0.105 µg/Kg



Extracted 7/30/04


EASTING (NAD83

UTM18N)

NORTHING (NAD83

UTM18N)SITE



LIMIT3

10/5/2000 EW-07 614692 4781163 7 0309077-09 Cl4-BZ#70 11.6 µg/Kg 0.0918 µg/Kg10/5/2000 EW-07 614692 4781163 7 0309077-09 Cl4-BZ#74 3.88 µg/Kg 0.162 µg/Kg10/5/2000 EW-07 614692 4781163 7 0309077-09 Cl4-BZ#77 0.145 U µg/Kg 0.145 µg/Kg10/5/2000 EW-07 614692 4781163 7 0309077-09 Cl4-BZ#81 0.144 U µg/Kg 0.144 µg/Kg10/5/2000 EW-07 614692 4781163 7 0309077-09 Cl5-BZ#87 2.89 µg/Kg 0.0640 µg/Kg10/5/2000 EW-07 614692 4781163 7 0309077-09 Cl5-BZ#95 4.31 µg/Kg 0.0495 µg/Kg10/5/2000 EW-07 614692 4781163 7 0309077-09 Cl5-BZ#99 3.88 µg/Kg 0.0338 µg/Kg10/5/2000 EW-07 614692 4781163 7 0309077-09 Cl5-BZ#101 6.25 µg/Kg 0.0967 µg/Kg10/5/2000 EW-07 614692 4781163 7 0309077-09 Cl5-BZ#105 5.31 µg/Kg 0.0471 µg/Kg10/5/2000 EW-07 614692 4781163 7 0309077-09 Cl5-BZ#110 6.83 µg/Kg 0.0918 µg/Kg10/5/2000 EW-07 614692 4781163 7 0309077-09 Cl5-BZ#114 0.0423 U µg/Kg 0.0423 µg/Kg10/5/2000 EW-07 614692 4781163 7 0309077-09 Cl5-BZ#118 10.2 µg/Kg 0.0991 µg/Kg10/5/2000 EW-07 614692 4781163 7 0309077-09 Cl5-BZ#123 0.0834 U µg/Kg 0.0834 µg/Kg10/5/2000 EW-07 614692 4781163 7 0309077-09 Cl5-BZ#126 0.0737 U µg/Kg 0.0737 µg/Kg10/5/2000 EW-07 614692 4781163 7 0309077-09 Cl6-BZ#128 1.07 µg/Kg 0.0665 µg/Kg10/5/2000 EW-07 614692 4781163 7 0309077-09 Cl6-BZ#138 8.70 µg/Kg 0.0955 µg/Kg10/5/2000 EW-07 614692 4781163 7 0309077-09 Cl6-BZ#146 0.912 µg/Kg 0.0604 µg/Kg10/5/2000 EW-07 614692 4781163 7 0309077-09 Cl6-BZ#149 6.28 µg/Kg 0.0773 µg/Kg10/5/2000 EW-07 614692 4781163 7 0309077-09 Cl6-BZ#151 1.56 µg/Kg 0.128 µg/Kg10/5/2000 EW-07 614692 4781163 7 0309077-09 Cl6-BZ#153 4.51 µg/Kg 0.110 µg/Kg10/5/2000 EW-07 614692 4781163 7 0309077-09 Cl6-BZ#156 0.598 µg/Kg 0.0785 µg/Kg10/5/2000 EW-07 614692 4781163 7 0309077-09 Cl6-BZ#157 0.115 J µg/Kg 0.0616 µg/Kg10/5/2000 EW-07 614692 4781163 7 0309077-09 Cl6-BZ#158 0.501 µg/Kg 0.0520 µg/Kg10/5/2000 EW-07 614692 4781163 7 0309077-09 Cl6-BZ#167 0.272 J µg/Kg 0.0665 µg/Kg10/5/2000 EW-07 614692 4781163 7 0309077-09 Cl6-BZ#169 0.214 U µg/Kg 0.214 µg/Kg10/5/2000 EW-07 614692 4781163 7 0309077-09 Cl7-BZ#170 0.249 U µg/Kg 0.249 µg/Kg10/5/2000 EW-07 614692 4781163 7 0309077-09 Cl7-BZ#174 0.507 µg/Kg 0.0507 µg/Kg10/5/2000 EW-07 614692 4781163 7 0309077-09 Cl7-BZ#177 0.465 µg/Kg 0.0713 µg/Kg10/5/2000 EW-07 614692 4781163 7 0309077-09 Cl7-BZ#180 0.912 µg/Kg 0.106 µg/Kg10/5/2000 EW-07 614692 4781163 7 0309077-09 Cl7-BZ#183 0.169 J µg/Kg 0.0483 µg/Kg10/5/2000 EW-07 614692 4781163 7 0309077-09 Cl7-BZ#189 0.0955 U µg/Kg 0.0955 µg/Kg10/5/2000 EW-07 614692 4781163 7 0309077-09 Cl7-BZ#187 2.66 µg/Kg 0.0532 µg/Kg10/5/2000 EW-07 614692 4781163 7 0309077-09 Cl8-BZ#194 0.302 J µg/Kg 0.111 µg/Kg10/5/2000 EW-07 614692 4781163 7 0309077-09 Cl8-BZ#195 0.110 U µg/Kg 0.110 µg/Kg10/5/2000 EW-07 614692 4781163 7 0309077-09 Cl8-BZ#201 0.0967 U µg/Kg 0.0967 µg/Kg



Extracted 7/30/04


EASTING (NAD83

UTM18N)

NORTHING (NAD83

UTM18N)SITE



LIMIT3

10/5/2000 EW-07 614692 4781163 7 0309077-09 Cl9-BZ#206 0.129 U µg/Kg 0.129 µg/Kg10/5/2000 EW-07 614692 4781163 7 0309077-09 Cl10-BZ#209 0.350 µg/Kg 0.0604 µg/Kg10/5/2000 EW-07 614692 4781163 7 0309077-09 Monochlorobiphenyls 3.55 U µg/Kg 3.55 µg/Kg10/5/2000 EW-07 614692 4781163 7 0309077-09 Dichlorobiphenyls 1.12 µg/Kg 0.104 µg/Kg10/5/2000 EW-07 614692 4781163 7 0309077-09 Trichlorobiphenyls 20.0 µg/Kg 0.356 µg/Kg10/5/2000 EW-07 614692 4781163 7 0309077-09 Tetrachlorobiphenyls 48.4 µg/Kg 0.0556 µg/Kg10/5/2000 EW-07 614692 4781163 7 0309077-09 Pentachlorobiphenyls 74.2 µg/Kg 0.0640 µg/Kg10/5/2000 EW-07 614692 4781163 7 0309077-09 Hexachlorobiphenyls 31.8 µg/Kg 0.101 µg/Kg10/5/2000 EW-07 614692 4781163 7 0309077-09 Heptachlorobiphenyls 6.10 µg/Kg 0.0556 µg/Kg10/5/2000 EW-07 614692 4781163 7 0309077-09 Octachlorobiphenyls 0.302 µg/Kg 0.0507 µg/Kg10/5/2000 EW-07 614692 4781163 7 0309077-09 Nonachlorobiphenyls 0.254 J µg/Kg 0.129 µg/Kg10/5/2000 EW-07 614692 4781163 7 0309077-09 Decachlorobiphenyl 0.350 µg/Kg 0.0604 µg/Kg10/5/2000 EW-07 614692 4781163 7 0309077-09 Total Homologs 182 µg/Kg 0.0604 µg/Kg10/5/2000 EW-07 614692 4781163 7 0309077-09 Percent Lipids 2.8 J % 0.1 %10/5/2000 EW-07 614692 4781163 7 0309077-09 Percent Moisture 80.0 % 0.1 %10/5/2000 EW-08 614784 4783341 8 0309077-10 Cl2-BZ#8 15.9 µg/Kg 0.219 µg/Kg10/5/2000 EW-08 614784 4783341 8 0309077-10 Cl3-BZ#18 28.2 µg/Kg 0.486 µg/Kg10/5/2000 EW-08 614784 4783341 8 0309077-10 Cl3-BZ#31/#28 1150 µg/Kg 3.51 µg/Kg10/5/2000 EW-08 614784 4783341 8 0309077-10 Cl4-BZ#44 587 µg/Kg 0.334 µg/Kg10/5/2000 EW-08 614784 4783341 8 0309077-10 Cl4-BZ#45 90.7 µg/Kg 0.446 µg/Kg10/5/2000 EW-08 614784 4783341 8 0309077-10 Cl4-BZ#47 461 µg/Kg 0.565 µg/Kg10/5/2000 EW-08 614784 4783341 8 0309077-10 Cl4-BZ#49 602 µg/Kg 0.278 µg/Kg10/5/2000 EW-08 614784 4783341 8 0309077-10 Cl4-BZ#52 1010 D µg/Kg 0.518 µg/Kg10/5/2000 EW-08 614784 4783341 8 0309077-10 Cl4-BZ#56 339 µg/Kg 0.166 µg/Kg10/5/2000 EW-08 614784 4783341 8 0309077-10 Cl4-BZ#66 483 µg/Kg 0.222 µg/Kg10/5/2000 EW-08 614784 4783341 8 0309077-10 Cl4-BZ#70 498 µg/Kg 0.194 µg/Kg10/5/2000 EW-08 614784 4783341 8 0309077-10 Cl4-BZ#74 389 µg/Kg 0.341 µg/Kg10/5/2000 EW-08 614784 4783341 8 0309077-10 Cl4-BZ#77 0.306 U µg/Kg 0.306 µg/Kg10/5/2000 EW-08 614784 4783341 8 0309077-10 Cl4-BZ#81 0.303 U µg/Kg 0.303 µg/Kg10/5/2000 EW-08 614784 4783341 8 0309077-10 Cl5-BZ#87 138 µg/Kg 0.135 µg/Kg10/5/2000 EW-08 614784 4783341 8 0309077-10 Cl5-BZ#95 263 µg/Kg 0.104 µg/Kg10/5/2000 EW-08 614784 4783341 8 0309077-10 Cl5-BZ#99 146 µg/Kg 0.0713 µg/Kg10/5/2000 EW-08 614784 4783341 8 0309077-10 Cl5-BZ#101 297 µg/Kg 0.204 µg/Kg10/5/2000 EW-08 614784 4783341 8 0309077-10 Cl5-BZ#105 84.6 µg/Kg 0.0993 µg/Kg10/5/2000 EW-08 614784 4783341 8 0309077-10 Cl5-BZ#110 244 µg/Kg 0.194 µg/Kg



Extracted 7/30/04


EASTING (NAD83

UTM18N)

NORTHING (NAD83

UTM18N)SITE



LIMIT3

10/5/2000 EW-08 614784 4783341 8 0309077-10 Cl5-BZ#114 12.2 µg/Kg 0.0891 µg/Kg10/5/2000 EW-08 614784 4783341 8 0309077-10 Cl5-BZ#118 178 µg/Kg 0.209 µg/Kg10/5/2000 EW-08 614784 4783341 8 0309077-10 Cl5-BZ#123 0.176 U µg/Kg 0.176 µg/Kg10/5/2000 EW-08 614784 4783341 8 0309077-10 Cl5-BZ#126 0.155 U µg/Kg 0.155 µg/Kg10/5/2000 EW-08 614784 4783341 8 0309077-10 Cl6-BZ#128 12.9 µg/Kg 0.140 µg/Kg10/5/2000 EW-08 614784 4783341 8 0309077-10 Cl6-BZ#138 122 µg/Kg 0.201 µg/Kg10/5/2000 EW-08 614784 4783341 8 0309077-10 Cl6-BZ#146 17.4 µg/Kg 0.127 µg/Kg10/5/2000 EW-08 614784 4783341 8 0309077-10 Cl6-BZ#149 99.6 µg/Kg 0.163 µg/Kg10/5/2000 EW-08 614784 4783341 8 0309077-10 Cl6-BZ#151 27.1 µg/Kg 0.270 µg/Kg10/5/2000 EW-08 614784 4783341 8 0309077-10 Cl6-BZ#153 60.6 µg/Kg 0.232 µg/Kg10/5/2000 EW-08 614784 4783341 8 0309077-10 Cl6-BZ#156 8.33 µg/Kg 0.166 µg/Kg10/5/2000 EW-08 614784 4783341 8 0309077-10 Cl6-BZ#157 0.130 U µg/Kg 0.130 µg/Kg10/5/2000 EW-08 614784 4783341 8 0309077-10 Cl6-BZ#158 6.05 µg/Kg 0.109 µg/Kg10/5/2000 EW-08 614784 4783341 8 0309077-10 Cl6-BZ#167 3.07 µg/Kg 0.140 µg/Kg10/5/2000 EW-08 614784 4783341 8 0309077-10 Cl6-BZ#169 0.451 U µg/Kg 0.451 µg/Kg10/5/2000 EW-08 614784 4783341 8 0309077-10 Cl7-BZ#170 8.26 µg/Kg 0.525 µg/Kg10/5/2000 EW-08 614784 4783341 8 0309077-10 Cl7-BZ#174 6.27 µg/Kg 0.107 µg/Kg10/5/2000 EW-08 614784 4783341 8 0309077-10 Cl7-BZ#177 5.25 µg/Kg 0.150 µg/Kg10/5/2000 EW-08 614784 4783341 8 0309077-10 Cl7-BZ#180 13.8 µg/Kg 0.224 µg/Kg10/5/2000 EW-08 614784 4783341 8 0309077-10 Cl7-BZ#183 3.34 µg/Kg 0.102 µg/Kg10/5/2000 EW-08 614784 4783341 8 0309077-10 Cl7-BZ#189 0.201 U µg/Kg 0.201 µg/Kg10/5/2000 EW-08 614784 4783341 8 0309077-10 Cl7-BZ#187 39.7 µg/Kg 0.112 µg/Kg10/5/2000 EW-08 614784 4783341 8 0309077-10 Cl8-BZ#194 0.234 U µg/Kg 0.234 µg/Kg10/5/2000 EW-08 614784 4783341 8 0309077-10 Cl8-BZ#195 0.232 U µg/Kg 0.232 µg/Kg10/5/2000 EW-08 614784 4783341 8 0309077-10 Cl8-BZ#201 0.204 U µg/Kg 0.204 µg/Kg10/5/2000 EW-08 614784 4783341 8 0309077-10 Cl9-BZ#206 2.36 µg/Kg 0.273 µg/Kg10/5/2000 EW-08 614784 4783341 8 0309077-10 Cl10-BZ#209 0.739 µg/Kg 0.127 µg/Kg10/5/2000 EW-08 614784 4783341 8 0309077-10 Monochlorobiphenyls 13.2 J µg/Kg 7.49 µg/Kg10/5/2000 EW-08 614784 4783341 8 0309077-10 Dichlorobiphenyls 109 µg/Kg 0.219 µg/Kg10/5/2000 EW-08 614784 4783341 8 0309077-10 Trichlorobiphenyls 1700 µg/Kg 0.751 µg/Kg10/5/2000 EW-08 614784 4783341 8 0309077-10 Tetrachlorobiphenyls 6460 µg/Kg 0.117 µg/Kg10/5/2000 EW-08 614784 4783341 8 0309077-10 Pentachlorobiphenyls 2440 µg/Kg 0.135 µg/Kg10/5/2000 EW-08 614784 4783341 8 0309077-10 Hexachlorobiphenyls 451 µg/Kg 0.214 µg/Kg10/5/2000 EW-08 614784 4783341 8 0309077-10 Heptachlorobiphenyls 79.3 µg/Kg 0.117 µg/Kg10/5/2000 EW-08 614784 4783341 8 0309077-10 Octachlorobiphenyls 0.107 U µg/Kg 0.107 µg/Kg



Extracted 7/30/04


EASTING (NAD83

UTM18N)

NORTHING (NAD83

UTM18N)SITE



LIMIT3

10/5/2000 EW-08 614784 4783341 8 0309077-10 Nonachlorobiphenyls 12.8 µg/Kg 0.273 µg/Kg10/5/2000 EW-08 614784 4783341 8 0309077-10 Decachlorobiphenyl 0.739 µg/Kg 0.127 µg/Kg10/5/2000 EW-08 614784 4783341 8 0309077-10 Total Homologs 11300 µg/Kg 0.127 µg/Kg10/5/2000 EW-08 614784 4783341 8 0309077-10 Percent Lipids 1.9 % 0.1 %10/5/2000 EW-08 614784 4783341 8 0309077-10 Percent Moisture 76.9 % 0.1 %10/5/2000 EW-10 614107 4788180 10 0309077-11 Cl2-BZ#8 16.0 µg/Kg 0.474 µg/Kg10/5/2000 EW-10 614107 4788180 10 0309077-11 Cl3-BZ#18 102 µg/Kg 1.05 µg/Kg10/5/2000 EW-10 614107 4788180 10 0309077-11 Cl3-BZ#31/#28 2290 µg/Kg 7.59 µg/Kg10/5/2000 EW-10 614107 4788180 10 0309077-11 Cl4-BZ#44 993 µg/Kg 0.722 µg/Kg10/5/2000 EW-10 614107 4788180 10 0309077-11 Cl4-BZ#45 101 µg/Kg 0.965 µg/Kg10/5/2000 EW-10 614107 4788180 10 0309077-11 Cl4-BZ#47 818 µg/Kg 1.22 µg/Kg10/5/2000 EW-10 614107 4788180 10 0309077-11 Cl4-BZ#49 1030 µg/Kg 0.601 µg/Kg10/5/2000 EW-10 614107 4788180 10 0309077-11 Cl4-BZ#52 1420 D µg/Kg 1.21 µg/Kg10/5/2000 EW-10 614107 4788180 10 0309077-11 Cl4-BZ#56 898 µg/Kg 0.358 µg/Kg10/5/2000 EW-10 614107 4788180 10 0309077-11 Cl4-BZ#66 1350 µg/Kg 0.480 µg/Kg10/5/2000 EW-10 614107 4788180 10 0309077-11 Cl4-BZ#70 1160 µg/Kg 0.419 µg/Kg10/5/2000 EW-10 614107 4788180 10 0309077-11 Cl4-BZ#74 967 µg/Kg 0.739 µg/Kg10/5/2000 EW-10 614107 4788180 10 0309077-11 Cl4-BZ#77 0.662 U µg/Kg 0.662 µg/Kg10/5/2000 EW-10 614107 4788180 10 0309077-11 Cl4-BZ#81 0.656 U µg/Kg 0.656 µg/Kg10/5/2000 EW-10 614107 4788180 10 0309077-11 Cl5-BZ#87 417 µg/Kg 0.292 µg/Kg10/5/2000 EW-10 614107 4788180 10 0309077-11 Cl5-BZ#95 477 µg/Kg 0.226 µg/Kg10/5/2000 EW-10 614107 4788180 10 0309077-11 Cl5-BZ#99 381 µg/Kg 0.154 µg/Kg10/5/2000 EW-10 614107 4788180 10 0309077-11 Cl5-BZ#101 755 µg/Kg 0.441 µg/Kg10/5/2000 EW-10 614107 4788180 10 0309077-11 Cl5-BZ#105 323 µg/Kg 0.215 µg/Kg10/5/2000 EW-10 614107 4788180 10 0309077-11 Cl5-BZ#110 669 µg/Kg 0.419 µg/Kg10/5/2000 EW-10 614107 4788180 10 0309077-11 Cl5-BZ#114 31.6 µg/Kg 0.193 µg/Kg10/5/2000 EW-10 614107 4788180 10 0309077-11 Cl5-BZ#118 614 µg/Kg 0.452 µg/Kg10/5/2000 EW-10 614107 4788180 10 0309077-11 Cl5-BZ#123 0.380 U µg/Kg 0.380 µg/Kg10/5/2000 EW-10 614107 4788180 10 0309077-11 Cl5-BZ#126 0.336 U µg/Kg 0.336 µg/Kg10/5/2000 EW-10 614107 4788180 10 0309077-11 Cl6-BZ#128 49.3 µg/Kg 0.303 µg/Kg10/5/2000 EW-10 614107 4788180 10 0309077-11 Cl6-BZ#138 369 µg/Kg 0.436 µg/Kg10/5/2000 EW-10 614107 4788180 10 0309077-11 Cl6-BZ#146 47.6 µg/Kg 0.276 µg/Kg10/5/2000 EW-10 614107 4788180 10 0309077-11 Cl6-BZ#149 222 µg/Kg 0.353 µg/Kg10/5/2000 EW-10 614107 4788180 10 0309077-11 Cl6-BZ#151 63.5 µg/Kg 0.585 µg/Kg10/5/2000 EW-10 614107 4788180 10 0309077-11 Cl6-BZ#153 205 µg/Kg 0.502 µg/Kg



Extracted 7/30/04


EASTING (NAD83

UTM18N)

NORTHING (NAD83

UTM18N)SITE



LIMIT3

10/5/2000 EW-10 614107 4788180 10 0309077-11 Cl6-BZ#156 32.7 µg/Kg 0.358 µg/Kg10/5/2000 EW-10 614107 4788180 10 0309077-11 Cl6-BZ#157 6.01 µg/Kg 0.281 µg/Kg10/5/2000 EW-10 614107 4788180 10 0309077-11 Cl6-BZ#158 18.1 µg/Kg 0.237 µg/Kg10/5/2000 EW-10 614107 4788180 10 0309077-11 Cl6-BZ#167 12.4 µg/Kg 0.303 µg/Kg10/5/2000 EW-10 614107 4788180 10 0309077-11 Cl6-BZ#169 0.976 U µg/Kg 0.976 µg/Kg10/5/2000 EW-10 614107 4788180 10 0309077-11 Cl7-BZ#170 31.0 µg/Kg 1.14 µg/Kg10/5/2000 EW-10 614107 4788180 10 0309077-11 Cl7-BZ#174 22.7 µg/Kg 0.232 µg/Kg10/5/2000 EW-10 614107 4788180 10 0309077-11 Cl7-BZ#177 14.2 µg/Kg 0.325 µg/Kg10/5/2000 EW-10 614107 4788180 10 0309077-11 Cl7-BZ#180 55.2 µg/Kg 0.485 µg/Kg10/5/2000 EW-10 614107 4788180 10 0309077-11 Cl7-BZ#183 11.7 µg/Kg 0.221 µg/Kg10/5/2000 EW-10 614107 4788180 10 0309077-11 Cl7-BZ#189 2.78 J µg/Kg 0.436 µg/Kg10/5/2000 EW-10 614107 4788180 10 0309077-11 Cl7-BZ#187 95.4 µg/Kg 0.243 µg/Kg10/5/2000 EW-10 614107 4788180 10 0309077-11 Cl8-BZ#194 9.18 µg/Kg 0.507 µg/Kg10/5/2000 EW-10 614107 4788180 10 0309077-11 Cl8-BZ#195 0.502 U µg/Kg 0.502 µg/Kg10/5/2000 EW-10 614107 4788180 10 0309077-11 Cl8-BZ#201 17.7 µg/Kg 0.441 µg/Kg10/5/2000 EW-10 614107 4788180 10 0309077-11 Cl9-BZ#206 5.10 µg/Kg 0.590 µg/Kg10/5/2000 EW-10 614107 4788180 10 0309077-11 Cl10-BZ#209 2.04 µg/Kg 0.276 µg/Kg10/5/2000 EW-10 614107 4788180 10 0309077-11 Monochlorobiphenyls 16.2 U µg/Kg 16.2 µg/Kg10/5/2000 EW-10 614107 4788180 10 0309077-11 Dichlorobiphenyls 176 µg/Kg 0.474 µg/Kg10/5/2000 EW-10 614107 4788180 10 0309077-11 Trichlorobiphenyls 3430 µg/Kg 1.63 µg/Kg10/5/2000 EW-10 614107 4788180 10 0309077-11 Tetrachlorobiphenyls 12200 µg/Kg 0.254 µg/Kg10/5/2000 EW-10 614107 4788180 10 0309077-11 Pentachlorobiphenyls 6510 µg/Kg 0.292 µg/Kg10/5/2000 EW-10 614107 4788180 10 0309077-11 Hexachlorobiphenyls 1300 µg/Kg 0.463 µg/Kg10/5/2000 EW-10 614107 4788180 10 0309077-11 Heptachlorobiphenyls 229 µg/Kg 0.254 µg/Kg10/5/2000 EW-10 614107 4788180 10 0309077-11 Octachlorobiphenyls 32.1 µg/Kg 0.232 µg/Kg10/5/2000 EW-10 614107 4788180 10 0309077-11 Nonachlorobiphenyls 23.2 µg/Kg 0.590 µg/Kg10/5/2000 EW-10 614107 4788180 10 0309077-11 Decachlorobiphenyl 2.04 µg/Kg 0.276 µg/Kg10/5/2000 EW-10 614107 4788180 10 0309077-11 Total Homologs 23900 µg/Kg 0.276 µg/Kg10/5/2000 EW-10 614107 4788180 10 0309077-11 Percent Lipids 2.3 % 0.1 %10/5/2000 EW-10 614107 4788180 10 0309077-11 Percent Moisture 77.8 % 0.1 %10/5/2000 EW-11 614806 4791061 11 0309077-12 Cl2-BZ#8 32.9 µg/Kg 0.528 µg/Kg10/5/2000 EW-11 614806 4791061 11 0309077-12 Cl3-BZ#18 83.8 µg/Kg 1.17 µg/Kg10/5/2000 EW-11 614806 4791061 11 0309077-12 Cl3-BZ#31/#28 1490 µg/Kg 8.46 µg/Kg10/5/2000 EW-11 614806 4791061 11 0309077-12 Cl4-BZ#44 561 µg/Kg 0.805 µg/Kg10/5/2000 EW-11 614806 4791061 11 0309077-12 Cl4-BZ#45 31.7 µg/Kg 1.08 µg/Kg



Extracted 7/30/04


EASTING (NAD83

UTM18N)

NORTHING (NAD83

UTM18N)SITE



LIMIT3

10/5/2000 EW-11 614806 4791061 11 0309077-12 Cl4-BZ#47 385 µg/Kg 1.36 µg/Kg10/5/2000 EW-11 614806 4791061 11 0309077-12 Cl4-BZ#49 880 µg/Kg 0.670 µg/Kg10/5/2000 EW-11 614806 4791061 11 0309077-12 Cl4-BZ#52 1320 µg/Kg 0.762 µg/Kg10/5/2000 EW-11 614806 4791061 11 0309077-12 Cl4-BZ#56 400 µg/Kg 0.399 µg/Kg10/5/2000 EW-11 614806 4791061 11 0309077-12 Cl4-BZ#66 657 µg/Kg 0.535 µg/Kg10/5/2000 EW-11 614806 4791061 11 0309077-12 Cl4-BZ#70 654 µg/Kg 0.467 µg/Kg10/5/2000 EW-11 614806 4791061 11 0309077-12 Cl4-BZ#74 397 µg/Kg 0.823 µg/Kg10/5/2000 EW-11 614806 4791061 11 0309077-12 Cl4-BZ#77 0.737 U µg/Kg 0.737 µg/Kg10/5/2000 EW-11 614806 4791061 11 0309077-12 Cl4-BZ#81 0.731 U µg/Kg 0.731 µg/Kg10/5/2000 EW-11 614806 4791061 11 0309077-12 Cl5-BZ#87 365 µg/Kg 0.326 µg/Kg10/5/2000 EW-11 614806 4791061 11 0309077-12 Cl5-BZ#95 639 µg/Kg 0.252 µg/Kg10/5/2000 EW-11 614806 4791061 11 0309077-12 Cl5-BZ#99 381 µg/Kg 0.172 µg/Kg10/5/2000 EW-11 614806 4791061 11 0309077-12 Cl5-BZ#101 891 µg/Kg 0.491 µg/Kg10/5/2000 EW-11 614806 4791061 11 0309077-12 Cl5-BZ#105 203 µg/Kg 0.240 µg/Kg10/5/2000 EW-11 614806 4791061 11 0309077-12 Cl5-BZ#110 863 µg/Kg 0.467 µg/Kg10/5/2000 EW-11 614806 4791061 11 0309077-12 Cl5-BZ#114 24.4 µg/Kg 0.215 µg/Kg10/5/2000 EW-11 614806 4791061 11 0309077-12 Cl5-BZ#118 537 µg/Kg 0.504 µg/Kg10/5/2000 EW-11 614806 4791061 11 0309077-12 Cl5-BZ#123 0.424 U µg/Kg 0.424 µg/Kg10/5/2000 EW-11 614806 4791061 11 0309077-12 Cl5-BZ#126 0.375 U µg/Kg 0.375 µg/Kg10/5/2000 EW-11 614806 4791061 11 0309077-12 Cl6-BZ#128 96.6 µg/Kg 0.338 µg/Kg10/5/2000 EW-11 614806 4791061 11 0309077-12 Cl6-BZ#138 824 µg/Kg 0.485 µg/Kg10/5/2000 EW-11 614806 4791061 11 0309077-12 Cl6-BZ#146 123 µg/Kg 0.307 µg/Kg10/5/2000 EW-11 614806 4791061 11 0309077-12 Cl6-BZ#149 687 µg/Kg 0.393 µg/Kg10/5/2000 EW-11 614806 4791061 11 0309077-12 Cl6-BZ#151 170 µg/Kg 0.651 µg/Kg10/5/2000 EW-11 614806 4791061 11 0309077-12 Cl6-BZ#153 476 µg/Kg 0.559 µg/Kg10/5/2000 EW-11 614806 4791061 11 0309077-12 Cl6-BZ#156 53.9 µg/Kg 0.399 µg/Kg10/5/2000 EW-11 614806 4791061 11 0309077-12 Cl6-BZ#157 9.52 µg/Kg 0.313 µg/Kg10/5/2000 EW-11 614806 4791061 11 0309077-12 Cl6-BZ#158 34.7 µg/Kg 0.264 µg/Kg10/5/2000 EW-11 614806 4791061 11 0309077-12 Cl6-BZ#167 20.6 µg/Kg 0.338 µg/Kg10/5/2000 EW-11 614806 4791061 11 0309077-12 Cl6-BZ#169 1.09 U µg/Kg 1.09 µg/Kg10/5/2000 EW-11 614806 4791061 11 0309077-12 Cl7-BZ#170 85.9 µg/Kg 1.26 µg/Kg10/5/2000 EW-11 614806 4791061 11 0309077-12 Cl7-BZ#174 51.8 µg/Kg 0.258 µg/Kg10/5/2000 EW-11 614806 4791061 11 0309077-12 Cl7-BZ#177 50.3 µg/Kg 0.362 µg/Kg10/5/2000 EW-11 614806 4791061 11 0309077-12 Cl7-BZ#180 124 µg/Kg 0.541 µg/Kg10/5/2000 EW-11 614806 4791061 11 0309077-12 Cl7-BZ#183 29.8 µg/Kg 0.246 µg/Kg



Extracted 7/30/04


EASTING (NAD83

UTM18N)

NORTHING (NAD83

UTM18N)SITE



LIMIT3

10/5/2000 EW-11 614806 4791061 11 0309077-12 Cl7-BZ#189 3.87 J µg/Kg 0.485 µg/Kg10/5/2000 EW-11 614806 4791061 11 0309077-12 Cl7-BZ#187 349 µg/Kg 0.270 µg/Kg10/5/2000 EW-11 614806 4791061 11 0309077-12 Cl8-BZ#194 26.5 µg/Kg 0.565 µg/Kg10/5/2000 EW-11 614806 4791061 11 0309077-12 Cl8-BZ#195 11.4 µg/Kg 0.559 µg/Kg10/5/2000 EW-11 614806 4791061 11 0309077-12 Cl8-BZ#201 50.2 µg/Kg 0.491 µg/Kg10/5/2000 EW-11 614806 4791061 11 0309077-12 Cl9-BZ#206 24.0 µg/Kg 0.657 µg/Kg10/5/2000 EW-11 614806 4791061 11 0309077-12 Cl10-BZ#209 5.31 µg/Kg 0.307 µg/Kg10/5/2000 EW-11 614806 4791061 11 0309077-12 Monochlorobiphenyls 18.1 U µg/Kg 18.1 µg/Kg10/5/2000 EW-11 614806 4791061 11 0309077-12 Dichlorobiphenyls 156 µg/Kg 0.528 µg/Kg10/5/2000 EW-11 614806 4791061 11 0309077-12 Trichlorobiphenyls 2020 µg/Kg 1.81 µg/Kg10/5/2000 EW-11 614806 4791061 11 0309077-12 Tetrachlorobiphenyls 7180 µg/Kg 0.283 µg/Kg10/5/2000 EW-11 614806 4791061 11 0309077-12 Pentachlorobiphenyls 6890 µg/Kg 0.326 µg/Kg10/5/2000 EW-11 614806 4791061 11 0309077-12 Hexachlorobiphenyls 3180 µg/Kg 0.516 µg/Kg10/5/2000 EW-11 614806 4791061 11 0309077-12 Heptachlorobiphenyls 728 µg/Kg 0.283 µg/Kg10/5/2000 EW-11 614806 4791061 11 0309077-12 Octachlorobiphenyls 86.0 µg/Kg 0.258 µg/Kg10/5/2000 EW-11 614806 4791061 11 0309077-12 Nonachlorobiphenyls 54.7 µg/Kg 0.657 µg/Kg10/5/2000 EW-11 614806 4791061 11 0309077-12 Decachlorobiphenyl 5.31 µg/Kg 0.307 µg/Kg10/5/2000 EW-11 614806 4791061 11 0309077-12 Total Homologs 20300 µg/Kg 0.307 µg/Kg10/5/2000 EW-11 614806 4791061 11 0309077-12 Percent Lipids 1.9 % 0.1 %10/5/2000 EW-11 614806 4791061 11 0309077-12 Percent Moisture 78.2 % 0.1 %


HUDSON RIVER



HU

DSO

N R

IVE

R DA

TA R

EP

OR

T: SM

AL

L MA

MM

AL

S AN

D A

ME

RIC

AN

WO

OD

CO

CK C

OL

LE

CT

ION

, AN

AL

YSIS O

F

FL

OO

DP

LA

IN E

AR

TH

WO

RM

S, AN

D R

E-AN

AL

YSIS O

F SE

LE

CT F

LO

OD

PL

AIN

SO

ILS A

ND

SM

AL

L MA

MM

AL

S

APPENDIX E

SMALL MAMMAL (2001) TISSUE DATA SHEETS

E1: SHORT-TAILED SHREW TISSUE DATA SHEETS

E2: MOUSE TISSUE DATA SHEETS

E3: MEADOW VOLE TISSUE DATA SHEETS

HUDS

ON R

IVER



HU

DSO

N R

IVE

R D

AT

A R

EP

OR

T: S

MA

LL M

AM

MA

LS

AN

D A

ME

RIC

AN

WO

OD

CO

CK

CO

LL

EC

TIO

N, A

NA

LY

SIS

OF

FL

OO

DP

LA

IN E

AR

TH

WO

RM

S, A

ND

RE

-AN

AL

YSI

S O

F S

EL

EC

T F

LO

OD

PL

AIN

SO

ILS

AN

D S

MA

LL M

AM

MA

LS

Short-Tailed Shrew (Blarina brevicauda) Tissue Hudson NRDA Floodplain DatabaseVersion 2.0

Extracted 7/30/04


EASTING(NAD 83UTM 18)

NORTHING(NAD 83UTM 18)

SITE NUMBER

LABORATORY ID ANALYTE

9/5/2001 1-06-090501 611675 4758823 1 0308027-01 Cl2-BZ#8 0.0845 U µg/Kg 0.0845 µg/Kg9/5/2001 1-06-090501 611675 4758823 1 0308027-01 Cl3-BZ#18 0.246 J µg/Kg 0.188 µg/Kg9/5/2001 1-06-090501 611675 4758823 1 0308027-01 Cl3-BZ#31/#28 132 µg/Kg 1.35 µg/Kg9/5/2001 1-06-090501 611675 4758823 1 0308027-01 Cl4-BZ#44 8.49 µg/Kg 0.129 µg/Kg9/5/2001 1-06-090501 611675 4758823 1 0308027-01 Cl4-BZ#45 0.192 J µg/Kg 0.172 µg/Kg9/5/2001 1-06-090501 611675 4758823 1 0308027-01 Cl4-BZ#47 193 µg/Kg 0.218 µg/Kg9/5/2001 1-06-090501 611675 4758823 1 0308027-01 Cl4-BZ#49 22.6 µg/Kg 0.107 µg/Kg9/5/2001 1-06-090501 611675 4758823 1 0308027-01 Cl4-BZ#52 92.8 µg/Kg 0.122 µg/Kg9/5/2001 1-06-090501 611675 4758823 1 0308027-01 Cl4-BZ#56 106 µg/Kg 0.0639 µg/Kg9/5/2001 1-06-090501 611675 4758823 1 0308027-01 Cl4-BZ#66 207 µg/Kg 0.0855 µg/Kg9/5/2001 1-06-090501 611675 4758823 1 0308027-01 Cl4-BZ#70 66.6 µg/Kg 0.0747 µg/Kg9/5/2001 1-06-090501 611675 4758823 1 0308027-01 Cl4-BZ#74 541 J µg/Kg 1.88 µg/Kg9/5/2001 1-06-090501 611675 4758823 1 0308027-01 Cl4-BZ#77 0.118 U µg/Kg 0.118 µg/Kg9/5/2001 1-06-090501 611675 4758823 1 0308027-01 Cl4-BZ#81 0.117 U µg/Kg 0.117 µg/Kg9/5/2001 1-06-090501 611675 4758823 1 0308027-01 Cl5-BZ#87 194 µg/Kg 0.0521 µg/Kg9/5/2001 1-06-090501 611675 4758823 1 0308027-01 Cl5-BZ#95 16.6 µg/Kg 0.0403 µg/Kg9/5/2001 1-06-090501 611675 4758823 1 0308027-01 Cl5-BZ#99 987 µg/Kg 0.392 µg/Kg9/5/2001 1-06-090501 611675 4758823 1 0308027-01 Cl5-BZ#101 66.9 µg/Kg 0.0786 µg/Kg9/5/2001 1-06-090501 611675 4758823 1 0308027-01 Cl5-BZ#105 510 µg/Kg 0.546 µg/Kg9/5/2001 1-06-090501 611675 4758823 1 0308027-01 Cl5-BZ#110 71.6 µg/Kg 0.0747 µg/Kg9/5/2001 1-06-090501 611675 4758823 1 0308027-01 Cl5-BZ#114 33.6 µg/Kg 0.0344 µg/Kg9/5/2001 1-06-090501 611675 4758823 1 0308027-01 Cl5-BZ#118 1530 µg/Kg 1.15 µg/Kg9/5/2001 1-06-090501 611675 4758823 1 0308027-01 Cl5-BZ#123 0.0678 U µg/Kg 0.0678 µg/Kg9/5/2001 1-06-090501 611675 4758823 1 0308027-01 Cl5-BZ#126 0.707 NJ µg/Kg 0.0599 µg/Kg9/5/2001 1-06-090501 611675 4758823 1 0308027-01 Cl6-BZ#128 141 µg/Kg 0.0540 µg/Kg9/5/2001 1-06-090501 611675 4758823 1 0308027-01 Cl6-BZ#138 1810 J µg/Kg 1.11 µg/Kg9/5/2001 1-06-090501 611675 4758823 1 0308027-01 Cl6-BZ#146 123 µg/Kg 0.0491 µg/Kg9/5/2001 1-06-090501 611675 4758823 1 0308027-01 Cl6-BZ#149 32.8 µg/Kg 0.0629 µg/Kg9/5/2001 1-06-090501 611675 4758823 1 0308027-01 Cl6-BZ#151 7.32 µg/Kg 0.104 µg/Kg9/5/2001 1-06-090501 611675 4758823 1 0308027-01 Cl6-BZ#153 1370 µg/Kg 1.27 µg/Kg9/5/2001 1-06-090501 611675 4758823 1 0308027-01 Cl6-BZ#156 123 µg/Kg 0.0639 µg/Kg9/5/2001 1-06-090501 611675 4758823 1 0308027-01 Cl6-BZ#157 21.5 µg/Kg 0.0501 µg/Kg9/5/2001 1-06-090501 611675 4758823 1 0308027-01 Cl6-BZ#158 42.4 µg/Kg 0.0422 µg/Kg9/5/2001 1-06-090501 611675 4758823 1 0308027-01 Cl6-BZ#167 55.7 µg/Kg 0.0540 µg/Kg

VALUE, INTERPRETIVE QUALIFIER2 AND UNITS3 DETECTION LIMIT3



Extracted 7/30/04




SITE NUMBER



9/5/2001 1-06-090501 611675 4758823 1 0308027-01 Cl6-BZ#169 0.174 U µg/Kg 0.174 µg/Kg9/5/2001 1-06-090501 611675 4758823 1 0308027-01 Cl7-BZ#170 135 µg/Kg 0.202 µg/Kg9/5/2001 1-06-090501 611675 4758823 1 0308027-01 Cl7-BZ#174 0.0413 U µg/Kg 0.0413 µg/Kg9/5/2001 1-06-090501 611675 4758823 1 0308027-01 Cl7-BZ#177 33.0 µg/Kg 0.0580 µg/Kg9/5/2001 1-06-090501 611675 4758823 1 0308027-01 Cl7-BZ#180 156 J µg/Kg 0.0865 µg/Kg9/5/2001 1-06-090501 611675 4758823 1 0308027-01 Cl7-BZ#183 34.0 µg/Kg 0.0393 µg/Kg9/5/2001 1-06-090501 611675 4758823 1 0308027-01 Cl7-BZ#187 147 µg/Kg 0.0432 µg/Kg9/5/2001 1-06-090501 611675 4758823 1 0308027-01 Cl7-BZ#189 0.0776 U µg/Kg 0.0776 µg/Kg9/5/2001 1-06-090501 611675 4758823 1 0308027-01 Cl8-BZ#194 19.4 µg/Kg 0.0904 µg/Kg9/5/2001 1-06-090501 611675 4758823 1 0308027-01 Cl8-BZ#195 8.62 µg/Kg 0.0894 µg/Kg9/5/2001 1-06-090501 611675 4758823 1 0308027-01 Cl8-BZ#201 30.4 µg/Kg 0.0786 µg/Kg9/5/2001 1-06-090501 611675 4758823 1 0308027-01 Cl9-BZ#206 16.8 µg/Kg 0.105 µg/Kg9/5/2001 1-06-090501 611675 4758823 1 0308027-01 Cl10-BZ#209 2.19 µg/Kg 0.0491 µg/Kg9/5/2001 1-06-090501 611675 4758823 1 0308027-01 Monochlorobiphenyls 2.89 U µg/Kg 2.89 µg/Kg9/5/2001 1-06-090501 611675 4758823 1 0308027-01 Dichlorobiphenyls 0.776 µg/Kg 0.0845 µg/Kg9/5/2001 1-06-090501 611675 4758823 1 0308027-01 Trichlorobiphenyls 132 µg/Kg 0.290 µg/Kg9/5/2001 1-06-090501 611675 4758823 1 0308027-01 Tetrachlorobiphenyls 1730 µg/Kg 0.644 µg/Kg9/5/2001 1-06-090501 611675 4758823 1 0308027-01 Pentachlorobiphenyls 5700 µg/Kg 0.742 µg/Kg9/5/2001 1-06-090501 611675 4758823 1 0308027-01 Hexachlorobiphenyls 4430 µg/Kg 1.18 µg/Kg9/5/2001 1-06-090501 611675 4758823 1 0308027-01 Heptachlorobiphenyls 540 µg/Kg 0.0452 µg/Kg9/5/2001 1-06-090501 611675 4758823 1 0308027-01 Octachlorobiphenyls 88.8 µg/Kg 0.0413 µg/Kg9/5/2001 1-06-090501 611675 4758823 1 0308027-01 Nonachlorobiphenyls 24.6 µg/Kg 0.105 µg/Kg9/5/2001 1-06-090501 611675 4758823 1 0308027-01 Decachlorobiphenyl 2.19 µg/Kg 0.0491 µg/Kg9/5/2001 1-06-090501 611675 4758823 1 0308027-01 Total Homologs 12900 µg/Kg 0.700 µg/Kg9/5/2001 1-06-090501 611675 4758823 1 0308027-01 Percent Lipids 3.2 % 0.1 %9/5/2001 1-06-090501 611675 4758823 1 0308027-01 Percent Moisture 68.4 % 0.1 %9/7/2001 1-16-090701 611675 4758823 1 0308027-02 Cl2-BZ#8 0.135 U µg/Kg 0.135 µg/Kg9/7/2001 1-16-090701 611675 4758823 1 0308027-02 Cl3-BZ#18 0.300 U µg/Kg 0.300 µg/Kg9/7/2001 1-16-090701 611675 4758823 1 0308027-02 Cl3-BZ#31/#28 154 µg/Kg 2.16 µg/Kg9/7/2001 1-16-090701 611675 4758823 1 0308027-02 Cl4-BZ#44 2.91 µg/Kg 0.206 µg/Kg9/7/2001 1-16-090701 611675 4758823 1 0308027-02 Cl4-BZ#45 0.275 U µg/Kg 0.275 µg/Kg9/7/2001 1-16-090701 611675 4758823 1 0308027-02 Cl4-BZ#47 62.8 µg/Kg 0.349 µg/Kg9/7/2001 1-16-090701 611675 4758823 1 0308027-02 Cl4-BZ#49 14.0 µg/Kg 0.171 µg/Kg9/7/2001 1-16-090701 611675 4758823 1 0308027-02 Cl4-BZ#52 36.3 µg/Kg 0.195 µg/Kg



Extracted 7/30/04




SITE NUMBER



9/7/2001 1-16-090701 611675 4758823 1 0308027-02 Cl4-BZ#56 84.2 µg/Kg 0.102 µg/Kg9/7/2001 1-16-090701 611675 4758823 1 0308027-02 Cl4-BZ#66 234 µg/Kg 0.137 µg/Kg9/7/2001 1-16-090701 611675 4758823 1 0308027-02 Cl4-BZ#70 89.0 µg/Kg 0.119 µg/Kg9/7/2001 1-16-090701 611675 4758823 1 0308027-02 Cl4-BZ#74 169 J µg/Kg 0.211 µg/Kg9/7/2001 1-16-090701 611675 4758823 1 0308027-02 Cl4-BZ#77 0.189 U µg/Kg 0.189 µg/Kg9/7/2001 1-16-090701 611675 4758823 1 0308027-02 Cl4-BZ#81 0.187 U µg/Kg 0.187 µg/Kg9/7/2001 1-16-090701 611675 4758823 1 0308027-02 Cl5-BZ#87 51.6 µg/Kg 0.0833 µg/Kg9/7/2001 1-16-090701 611675 4758823 1 0308027-02 Cl5-BZ#95 6.90 µg/Kg 0.0645 µg/Kg9/7/2001 1-16-090701 611675 4758823 1 0308027-02 Cl5-BZ#99 157 µg/Kg 0.0440 µg/Kg9/7/2001 1-16-090701 611675 4758823 1 0308027-02 Cl5-BZ#101 29.2 µg/Kg 0.126 µg/Kg9/7/2001 1-16-090701 611675 4758823 1 0308027-02 Cl5-BZ#105 117 µg/Kg 0.0613 µg/Kg9/7/2001 1-16-090701 611675 4758823 1 0308027-02 Cl5-BZ#110 25.0 µg/Kg 0.119 µg/Kg9/7/2001 1-16-090701 611675 4758823 1 0308027-02 Cl5-BZ#114 10.3 µg/Kg 0.0550 µg/Kg9/7/2001 1-16-090701 611675 4758823 1 0308027-02 Cl5-BZ#118 307 µg/Kg 0.129 µg/Kg9/7/2001 1-16-090701 611675 4758823 1 0308027-02 Cl5-BZ#123 0.108 U µg/Kg 0.108 µg/Kg9/7/2001 1-16-090701 611675 4758823 1 0308027-02 Cl5-BZ#126 0.291 NJ µg/Kg 0.0959 µg/Kg9/7/2001 1-16-090701 611675 4758823 1 0308027-02 Cl6-BZ#128 30.0 µg/Kg 0.0865 µg/Kg9/7/2001 1-16-090701 611675 4758823 1 0308027-02 Cl6-BZ#138 293 J µg/Kg 0.124 µg/Kg9/7/2001 1-16-090701 611675 4758823 1 0308027-02 Cl6-BZ#146 24.5 µg/Kg 0.0786 µg/Kg9/7/2001 1-16-090701 611675 4758823 1 0308027-02 Cl6-BZ#149 10.4 µg/Kg 0.101 µg/Kg9/7/2001 1-16-090701 611675 4758823 1 0308027-02 Cl6-BZ#151 2.99 µg/Kg 0.167 µg/Kg9/7/2001 1-16-090701 611675 4758823 1 0308027-02 Cl6-BZ#153 216 µg/Kg 0.143 µg/Kg9/7/2001 1-16-090701 611675 4758823 1 0308027-02 Cl6-BZ#156 27.0 µg/Kg 0.102 µg/Kg9/7/2001 1-16-090701 611675 4758823 1 0308027-02 Cl6-BZ#157 5.25 µg/Kg 0.0802 µg/Kg9/7/2001 1-16-090701 611675 4758823 1 0308027-02 Cl6-BZ#158 6.02 µg/Kg 0.0676 µg/Kg9/7/2001 1-16-090701 611675 4758823 1 0308027-02 Cl6-BZ#167 10.3 µg/Kg 0.0865 µg/Kg9/7/2001 1-16-090701 611675 4758823 1 0308027-02 Cl6-BZ#169 0.278 U µg/Kg 0.278 µg/Kg9/7/2001 1-16-090701 611675 4758823 1 0308027-02 Cl7-BZ#170 24.4 µg/Kg 0.324 µg/Kg9/7/2001 1-16-090701 611675 4758823 1 0308027-02 Cl7-BZ#174 1.82 µg/Kg 0.0660 µg/Kg9/7/2001 1-16-090701 611675 4758823 1 0308027-02 Cl7-BZ#177 5.19 µg/Kg 0.0928 µg/Kg9/7/2001 1-16-090701 611675 4758823 1 0308027-02 Cl7-BZ#180 32.4 J µg/Kg 0.138 µg/Kg9/7/2001 1-16-090701 611675 4758823 1 0308027-02 Cl7-BZ#183 5.24 µg/Kg 0.0629 µg/Kg9/7/2001 1-16-090701 611675 4758823 1 0308027-02 Cl7-BZ#187 22.2 µg/Kg 0.0692 µg/Kg9/7/2001 1-16-090701 611675 4758823 1 0308027-02 Cl7-BZ#189 0.124 U µg/Kg 0.124 µg/Kg



Extracted 7/30/04




SITE NUMBER



9/7/2001 1-16-090701 611675 4758823 1 0308027-02 Cl8-BZ#194 3.36 µg/Kg 0.145 µg/Kg9/7/2001 1-16-090701 611675 4758823 1 0308027-02 Cl8-BZ#195 1.82 µg/Kg 0.143 µg/Kg9/7/2001 1-16-090701 611675 4758823 1 0308027-02 Cl8-BZ#201 3.66 µg/Kg 0.126 µg/Kg9/7/2001 1-16-090701 611675 4758823 1 0308027-02 Cl9-BZ#206 2.49 µg/Kg 0.168 µg/Kg9/7/2001 1-16-090701 611675 4758823 1 0308027-02 Cl10-BZ#209 0.338 J µg/Kg 0.0786 µg/Kg9/7/2001 1-16-090701 611675 4758823 1 0308027-02 Monochlorobiphenyls 4.62 U µg/Kg 4.62 µg/Kg9/7/2001 1-16-090701 611675 4758823 1 0308027-02 Dichlorobiphenyls 0.668 J µg/Kg 0.135 µg/Kg9/7/2001 1-16-090701 611675 4758823 1 0308027-02 Trichlorobiphenyls 201 µg/Kg 0.464 µg/Kg9/7/2001 1-16-090701 611675 4758823 1 0308027-02 Tetrachlorobiphenyls 864 µg/Kg 0.0723 µg/Kg9/7/2001 1-16-090701 611675 4758823 1 0308027-02 Pentachlorobiphenyls 1010 µg/Kg 0.0833 µg/Kg9/7/2001 1-16-090701 611675 4758823 1 0308027-02 Hexachlorobiphenyls 708 µg/Kg 0.132 µg/Kg9/7/2001 1-16-090701 611675 4758823 1 0308027-02 Heptachlorobiphenyls 96.1 µg/Kg 0.0723 µg/Kg9/7/2001 1-16-090701 611675 4758823 1 0308027-02 Octachlorobiphenyls 14.4 µg/Kg 0.0660 µg/Kg9/7/2001 1-16-090701 611675 4758823 1 0308027-02 Nonachlorobiphenyls 5.35 µg/Kg 0.168 µg/Kg9/7/2001 1-16-090701 611675 4758823 1 0308027-02 Decachlorobiphenyl 0.338 J µg/Kg 0.0786 µg/Kg9/7/2001 1-16-090701 611675 4758823 1 0308027-02 Total Homologs 2900 µg/Kg 0.0786 µg/Kg9/7/2001 1-16-090701 611675 4758823 1 0308027-02 Percent Lipids 2.4 % 0.1 %9/7/2001 1-16-090701 611675 4758823 1 0308027-02 Percent Moisture 73.3 % 0.1 %9/8/2001 1-17-090801 611675 4758823 1 0308027-03 Cl2-BZ#8 0.118 U µg/Kg 0.118 µg/Kg9/8/2001 1-17-090801 611675 4758823 1 0308027-03 Cl3-BZ#18 0.262 U µg/Kg 0.262 µg/Kg9/8/2001 1-17-090801 611675 4758823 1 0308027-03 Cl3-BZ#31/#28 36.1 µg/Kg 1.89 µg/Kg9/8/2001 1-17-090801 611675 4758823 1 0308027-03 Cl4-BZ#44 0.817 J µg/Kg 0.180 µg/Kg9/8/2001 1-17-090801 611675 4758823 1 0308027-03 Cl4-BZ#45 0.240 U µg/Kg 0.240 µg/Kg9/8/2001 1-17-090801 611675 4758823 1 0308027-03 Cl4-BZ#47 9.72 µg/Kg 0.305 µg/Kg9/8/2001 1-17-090801 611675 4758823 1 0308027-03 Cl4-BZ#49 2.88 µg/Kg 0.150 µg/Kg9/8/2001 1-17-090801 611675 4758823 1 0308027-03 Cl4-BZ#52 6.17 µg/Kg 0.170 µg/Kg9/8/2001 1-17-090801 611675 4758823 1 0308027-03 Cl4-BZ#56 13.3 µg/Kg 0.0892 µg/Kg9/8/2001 1-17-090801 611675 4758823 1 0308027-03 Cl4-BZ#66 27.3 µg/Kg 0.119 µg/Kg9/8/2001 1-17-090801 611675 4758823 1 0308027-03 Cl4-BZ#70 9.83 µg/Kg 0.104 µg/Kg9/8/2001 1-17-090801 611675 4758823 1 0308027-03 Cl4-BZ#74 31.9 J µg/Kg 0.184 µg/Kg9/8/2001 1-17-090801 611675 4758823 1 0308027-03 Cl4-BZ#77 0.165 U µg/Kg 0.165 µg/Kg9/8/2001 1-17-090801 611675 4758823 1 0308027-03 Cl4-BZ#81 0.163 U µg/Kg 0.163 µg/Kg9/8/2001 1-17-090801 611675 4758823 1 0308027-03 Cl5-BZ#87 16.2 µg/Kg 0.0727 µg/Kg9/8/2001 1-17-090801 611675 4758823 1 0308027-03 Cl5-BZ#95 0.830 µg/Kg 0.0563 µg/Kg



Extracted 7/30/04




SITE NUMBER



9/8/2001 1-17-090801 611675 4758823 1 0308027-03 Cl5-BZ#99 101 µg/Kg 0.0384 µg/Kg9/8/2001 1-17-090801 611675 4758823 1 0308027-03 Cl5-BZ#101 3.86 µg/Kg 0.110 µg/Kg9/8/2001 1-17-090801 611675 4758823 1 0308027-03 Cl5-BZ#105 41.8 µg/Kg 0.0535 µg/Kg9/8/2001 1-17-090801 611675 4758823 1 0308027-03 Cl5-BZ#110 2.81 µg/Kg 0.104 µg/Kg9/8/2001 1-17-090801 611675 4758823 1 0308027-03 Cl5-BZ#114 4.61 µg/Kg 0.0480 µg/Kg9/8/2001 1-17-090801 611675 4758823 1 0308027-03 Cl5-BZ#118 129 µg/Kg 0.112 µg/Kg9/8/2001 1-17-090801 611675 4758823 1 0308027-03 Cl5-BZ#123 0.0947 U µg/Kg 0.0947 µg/Kg9/8/2001 1-17-090801 611675 4758823 1 0308027-03 Cl5-BZ#126 0.178 NJ µg/Kg 0.0837 µg/Kg9/8/2001 1-17-090801 611675 4758823 1 0308027-03 Cl6-BZ#128 22.6 µg/Kg 0.0755 µg/Kg9/8/2001 1-17-090801 611675 4758823 1 0308027-03 Cl6-BZ#138 408 J µg/Kg 0.247 µg/Kg9/8/2001 1-17-090801 611675 4758823 1 0308027-03 Cl6-BZ#146 30.2 µg/Kg 0.0686 µg/Kg9/8/2001 1-17-090801 611675 4758823 1 0308027-03 Cl6-BZ#149 2.71 µg/Kg 0.0878 µg/Kg9/8/2001 1-17-090801 611675 4758823 1 0308027-03 Cl6-BZ#151 0.398 J µg/Kg 0.146 µg/Kg9/8/2001 1-17-090801 611675 4758823 1 0308027-03 Cl6-BZ#153 339 µg/Kg 0.125 µg/Kg9/8/2001 1-17-090801 611675 4758823 1 0308027-03 Cl6-BZ#156 35.8 µg/Kg 0.0892 µg/Kg9/8/2001 1-17-090801 611675 4758823 1 0308027-03 Cl6-BZ#157 5.50 µg/Kg 0.0700 µg/Kg9/8/2001 1-17-090801 611675 4758823 1 0308027-03 Cl6-BZ#158 6.08 µg/Kg 0.0590 µg/Kg9/8/2001 1-17-090801 611675 4758823 1 0308027-03 Cl6-BZ#167 8.52 µg/Kg 0.0755 µg/Kg9/8/2001 1-17-090801 611675 4758823 1 0308027-03 Cl6-BZ#169 0.243 U µg/Kg 0.243 µg/Kg9/8/2001 1-17-090801 611675 4758823 1 0308027-03 Cl7-BZ#170 57.0 µg/Kg 0.283 µg/Kg9/8/2001 1-17-090801 611675 4758823 1 0308027-03 Cl7-BZ#174 0.0576 U µg/Kg 0.0576 µg/Kg9/8/2001 1-17-090801 611675 4758823 1 0308027-03 Cl7-BZ#177 3.68 µg/Kg 0.0810 µg/Kg9/8/2001 1-17-090801 611675 4758823 1 0308027-03 Cl7-BZ#180 76.0 J µg/Kg 0.121 µg/Kg9/8/2001 1-17-090801 611675 4758823 1 0308027-03 Cl7-BZ#183 17.6 µg/Kg 0.0549 µg/Kg9/8/2001 1-17-090801 611675 4758823 1 0308027-03 Cl7-BZ#187 24.9 µg/Kg 0.0604 µg/Kg9/8/2001 1-17-090801 611675 4758823 1 0308027-03 Cl7-BZ#189 0.108 U µg/Kg 0.108 µg/Kg9/8/2001 1-17-090801 611675 4758823 1 0308027-03 Cl8-BZ#194 7.88 µg/Kg 0.126 µg/Kg9/8/2001 1-17-090801 611675 4758823 1 0308027-03 Cl8-BZ#195 4.92 µg/Kg 0.125 µg/Kg9/8/2001 1-17-090801 611675 4758823 1 0308027-03 Cl8-BZ#201 6.54 µg/Kg 0.110 µg/Kg9/8/2001 1-17-090801 611675 4758823 1 0308027-03 Cl9-BZ#206 8.98 µg/Kg 0.147 µg/Kg9/8/2001 1-17-090801 611675 4758823 1 0308027-03 Cl10-BZ#209 0.837 µg/Kg 0.0686 µg/Kg9/8/2001 1-17-090801 611675 4758823 1 0308027-03 Monochlorobiphenyls 4.04 U µg/Kg 4.04 µg/Kg9/8/2001 1-17-090801 611675 4758823 1 0308027-03 Dichlorobiphenyls 0.118 U µg/Kg 0.118 µg/Kg9/8/2001 1-17-090801 611675 4758823 1 0308027-03 Trichlorobiphenyls 74.8 µg/Kg 0.405 µg/Kg



Extracted 7/30/04




SITE NUMBER



9/8/2001 1-17-090801 611675 4758823 1 0308027-03 Tetrachlorobiphenyls 137 µg/Kg 0.0631 µg/Kg9/8/2001 1-17-090801 611675 4758823 1 0308027-03 Pentachlorobiphenyls 489 µg/Kg 0.0727 µg/Kg9/8/2001 1-17-090801 611675 4758823 1 0308027-03 Hexachlorobiphenyls 958 µg/Kg 0.262 µg/Kg9/8/2001 1-17-090801 611675 4758823 1 0308027-03 Heptachlorobiphenyls 189 µg/Kg 0.0631 µg/Kg9/8/2001 1-17-090801 611675 4758823 1 0308027-03 Octachlorobiphenyls 46.3 µg/Kg 0.0576 µg/Kg9/8/2001 1-17-090801 611675 4758823 1 0308027-03 Nonachlorobiphenyls 13.0 µg/Kg 0.147 µg/Kg9/8/2001 1-17-090801 611675 4758823 1 0308027-03 Decachlorobiphenyl 0.837 µg/Kg 0.0686 µg/Kg9/8/2001 1-17-090801 611675 4758823 1 0308027-03 Total Homologs 1890 µg/Kg 0.156 µg/Kg9/8/2001 1-17-090801 611675 4758823 1 0308027-03 Percent Lipids 5.3 % 0.1 %9/8/2001 1-17-090801 611675 4758823 1 0308027-03 Percent Moisture 71.3 % 0.1 %9/9/2001 1-18-090901 611675 4758823 1 0308027-04 Cl2-BZ#8 0.117 U µg/Kg 0.117 µg/Kg9/9/2001 1-18-090901 611675 4758823 1 0308027-04 Cl3-BZ#18 0.259 U µg/Kg 0.259 µg/Kg9/9/2001 1-18-090901 611675 4758823 1 0308027-04 Cl3-BZ#31/#28 9.02 J µg/Kg 1.87 µg/Kg9/9/2001 1-18-090901 611675 4758823 1 0308027-04 Cl4-BZ#44 0.238 J µg/Kg 0.178 µg/Kg9/9/2001 1-18-090901 611675 4758823 1 0308027-04 Cl4-BZ#45 0.238 U µg/Kg 0.238 µg/Kg9/9/2001 1-18-090901 611675 4758823 1 0308027-04 Cl4-BZ#47 5.16 µg/Kg 0.302 µg/Kg9/9/2001 1-18-090901 611675 4758823 1 0308027-04 Cl4-BZ#49 0.958 µg/Kg 0.148 µg/Kg9/9/2001 1-18-090901 611675 4758823 1 0308027-04 Cl4-BZ#52 1.58 µg/Kg 0.169 µg/Kg9/9/2001 1-18-090901 611675 4758823 1 0308027-04 Cl4-BZ#56 4.64 µg/Kg 0.0883 µg/Kg9/9/2001 1-18-090901 611675 4758823 1 0308027-04 Cl4-BZ#66 11.1 µg/Kg 0.118 µg/Kg9/9/2001 1-18-090901 611675 4758823 1 0308027-04 Cl4-BZ#70 3.40 µg/Kg 0.103 µg/Kg9/9/2001 1-18-090901 611675 4758823 1 0308027-04 Cl4-BZ#74 9.76 J µg/Kg 0.182 µg/Kg9/9/2001 1-18-090901 611675 4758823 1 0308027-04 Cl4-BZ#77 0.163 U µg/Kg 0.163 µg/Kg9/9/2001 1-18-090901 611675 4758823 1 0308027-04 Cl4-BZ#81 0.162 U µg/Kg 0.162 µg/Kg9/9/2001 1-18-090901 611675 4758823 1 0308027-04 Cl5-BZ#87 5.43 µg/Kg 0.0720 µg/Kg9/9/2001 1-18-090901 611675 4758823 1 0308027-04 Cl5-BZ#95 0.231 J µg/Kg 0.0557 µg/Kg9/9/2001 1-18-090901 611675 4758823 1 0308027-04 Cl5-BZ#99 14.1 µg/Kg 0.0380 µg/Kg9/9/2001 1-18-090901 611675 4758823 1 0308027-04 Cl5-BZ#101 2.59 µg/Kg 0.109 µg/Kg9/9/2001 1-18-090901 611675 4758823 1 0308027-04 Cl5-BZ#105 9.33 µg/Kg 0.0530 µg/Kg9/9/2001 1-18-090901 611675 4758823 1 0308027-04 Cl5-BZ#110 0.937 µg/Kg 0.103 µg/Kg9/9/2001 1-18-090901 611675 4758823 1 0308027-04 Cl5-BZ#114 0.965 µg/Kg 0.0475 µg/Kg9/9/2001 1-18-090901 611675 4758823 1 0308027-04 Cl5-BZ#118 22.9 µg/Kg 0.111 µg/Kg9/9/2001 1-18-090901 611675 4758823 1 0308027-04 Cl5-BZ#123 0.0937 U µg/Kg 0.0937 µg/Kg9/9/2001 1-18-090901 611675 4758823 1 0308027-04 Cl5-BZ#126 0.190 NJ µg/Kg 0.0829 µg/Kg



Extracted 7/30/04




SITE NUMBER



9/9/2001 1-18-090901 611675 4758823 1 0308027-04 Cl6-BZ#128 2.85 µg/Kg 0.0747 µg/Kg9/9/2001 1-18-090901 611675 4758823 1 0308027-04 Cl6-BZ#138 37.7 J µg/Kg 0.107 µg/Kg9/9/2001 1-18-090901 611675 4758823 1 0308027-04 Cl6-BZ#146 4.35 µg/Kg 0.0679 µg/Kg9/9/2001 1-18-090901 611675 4758823 1 0308027-04 Cl6-BZ#149 0.842 µg/Kg 0.0869 µg/Kg9/9/2001 1-18-090901 611675 4758823 1 0308027-04 Cl6-BZ#151 0.319 J µg/Kg 0.144 µg/Kg9/9/2001 1-18-090901 611675 4758823 1 0308027-04 Cl6-BZ#153 27.1 µg/Kg 0.124 µg/Kg9/9/2001 1-18-090901 611675 4758823 1 0308027-04 Cl6-BZ#156 3.78 µg/Kg 0.0883 µg/Kg9/9/2001 1-18-090901 611675 4758823 1 0308027-04 Cl6-BZ#157 0.632 µg/Kg 0.0693 µg/Kg9/9/2001 1-18-090901 611675 4758823 1 0308027-04 Cl6-BZ#158 0.815 µg/Kg 0.0584 µg/Kg9/9/2001 1-18-090901 611675 4758823 1 0308027-04 Cl6-BZ#167 1.35 µg/Kg 0.0747 µg/Kg9/9/2001 1-18-090901 611675 4758823 1 0308027-04 Cl6-BZ#169 0.241 U µg/Kg 0.241 µg/Kg9/9/2001 1-18-090901 611675 4758823 1 0308027-04 Cl7-BZ#170 6.09 µg/Kg 0.280 µg/Kg9/9/2001 1-18-090901 611675 4758823 1 0308027-04 Cl7-BZ#174 0.0571 U µg/Kg 0.0571 µg/Kg9/9/2001 1-18-090901 611675 4758823 1 0308027-04 Cl7-BZ#177 0.985 µg/Kg 0.0802 µg/Kg9/9/2001 1-18-090901 611675 4758823 1 0308027-04 Cl7-BZ#180 9.65 J µg/Kg 0.119 µg/Kg9/9/2001 1-18-090901 611675 4758823 1 0308027-04 Cl7-BZ#183 1.27 µg/Kg 0.0543 µg/Kg9/9/2001 1-18-090901 611675 4758823 1 0308027-04 Cl7-BZ#187 12.3 µg/Kg 0.0598 µg/Kg9/9/2001 1-18-090901 611675 4758823 1 0308027-04 Cl7-BZ#189 0.107 U µg/Kg 0.107 µg/Kg9/9/2001 1-18-090901 611675 4758823 1 0308027-04 Cl8-BZ#194 1.14 µg/Kg 0.125 µg/Kg9/9/2001 1-18-090901 611675 4758823 1 0308027-04 Cl8-BZ#195 0.516 J µg/Kg 0.124 µg/Kg9/9/2001 1-18-090901 611675 4758823 1 0308027-04 Cl8-BZ#201 2.53 µg/Kg 0.109 µg/Kg9/9/2001 1-18-090901 611675 4758823 1 0308027-04 Cl9-BZ#206 1.13 µg/Kg 0.145 µg/Kg9/9/2001 1-18-090901 611675 4758823 1 0308027-04 Cl10-BZ#209 0.183 J µg/Kg 0.0679 µg/Kg9/9/2001 1-18-090901 611675 4758823 1 0308027-04 Monochlorobiphenyls 3.99 U µg/Kg 3.99 µg/Kg9/9/2001 1-18-090901 611675 4758823 1 0308027-04 Dichlorobiphenyls 0.117 U µg/Kg 0.117 µg/Kg9/9/2001 1-18-090901 611675 4758823 1 0308027-04 Trichlorobiphenyls 7.62 µg/Kg 0.401 µg/Kg9/9/2001 1-18-090901 611675 4758823 1 0308027-04 Tetrachlorobiphenyls 52.2 µg/Kg 0.0625 µg/Kg9/9/2001 1-18-090901 611675 4758823 1 0308027-04 Pentachlorobiphenyls 94.8 µg/Kg 0.0720 µg/Kg9/9/2001 1-18-090901 611675 4758823 1 0308027-04 Hexachlorobiphenyls 91.7 µg/Kg 0.114 µg/Kg9/9/2001 1-18-090901 611675 4758823 1 0308027-04 Heptachlorobiphenyls 44.8 µg/Kg 0.0625 µg/Kg9/9/2001 1-18-090901 611675 4758823 1 0308027-04 Octachlorobiphenyls 8.48 µg/Kg 0.0571 µg/Kg9/9/2001 1-18-090901 611675 4758823 1 0308027-04 Nonachlorobiphenyls 3.02 µg/Kg 0.145 µg/Kg9/9/2001 1-18-090901 611675 4758823 1 0308027-04 Decachlorobiphenyl 0.183 J µg/Kg 0.0679 µg/Kg9/9/2001 1-18-090901 611675 4758823 1 0308027-04 Total Homologs 303 µg/Kg 0.0679 µg/Kg



Extracted 7/30/04




SITE NUMBER



9/9/2001 1-18-090901 611675 4758823 1 0308027-04 Percent Lipids 3.4 % 0.1 %9/9/2001 1-18-090901 611675 4758823 1 0308027-04 Percent Moisture 48.8 % 0.1 %9/9/2001 1-19-090901 611675 4758823 1 0308027-05 Cl2-BZ#8 0.111 U µg/Kg 0.111 µg/Kg9/9/2001 1-19-090901 611675 4758823 1 0308027-05 Cl3-BZ#18 0.252 J µg/Kg 0.247 µg/Kg9/9/2001 1-19-090901 611675 4758823 1 0308027-05 Cl3-BZ#31/#28 244 µg/Kg 1.78 µg/Kg9/9/2001 1-19-090901 611675 4758823 1 0308027-05 Cl4-BZ#44 3.72 µg/Kg 0.169 µg/Kg9/9/2001 1-19-090901 611675 4758823 1 0308027-05 Cl4-BZ#45 0.227 U µg/Kg 0.227 µg/Kg9/9/2001 1-19-090901 611675 4758823 1 0308027-05 Cl4-BZ#47 208 µg/Kg 0.287 µg/Kg9/9/2001 1-19-090901 611675 4758823 1 0308027-05 Cl4-BZ#49 20.4 µg/Kg 0.141 µg/Kg9/9/2001 1-19-090901 611675 4758823 1 0308027-05 Cl4-BZ#52 80.3 µg/Kg 0.161 µg/Kg9/9/2001 1-19-090901 611675 4758823 1 0308027-05 Cl4-BZ#56 206 µg/Kg 0.0841 µg/Kg9/9/2001 1-19-090901 611675 4758823 1 0308027-05 Cl4-BZ#66 463 µg/Kg 0.653 µg/Kg9/9/2001 1-19-090901 611675 4758823 1 0308027-05 Cl4-BZ#70 116 µg/Kg 0.0984 µg/Kg9/9/2001 1-19-090901 611675 4758823 1 0308027-05 Cl4-BZ#74 746 J µg/Kg 1.01 µg/Kg9/9/2001 1-19-090901 611675 4758823 1 0308027-05 Cl4-BZ#77 0.155 U µg/Kg 0.155 µg/Kg9/9/2001 1-19-090901 611675 4758823 1 0308027-05 Cl4-BZ#81 0.154 U µg/Kg 0.154 µg/Kg9/9/2001 1-19-090901 611675 4758823 1 0308027-05 Cl5-BZ#87 240 µg/Kg 0.0686 µg/Kg9/9/2001 1-19-090901 611675 4758823 1 0308027-05 Cl5-BZ#95 8.90 µg/Kg 0.0531 µg/Kg9/9/2001 1-19-090901 611675 4758823 1 0308027-05 Cl5-BZ#99 879 µg/Kg 0.210 µg/Kg9/9/2001 1-19-090901 611675 4758823 1 0308027-05 Cl5-BZ#101 81.2 µg/Kg 0.104 µg/Kg9/9/2001 1-19-090901 611675 4758823 1 0308027-05 Cl5-BZ#105 567 µg/Kg 0.293 µg/Kg9/9/2001 1-19-090901 611675 4758823 1 0308027-05 Cl5-BZ#110 86.7 µg/Kg 0.0984 µg/Kg9/9/2001 1-19-090901 611675 4758823 1 0308027-05 Cl5-BZ#114 45.7 µg/Kg 0.0453 µg/Kg9/9/2001 1-19-090901 611675 4758823 1 0308027-05 Cl5-BZ#118 1570 µg/Kg 0.615 µg/Kg9/9/2001 1-19-090901 611675 4758823 1 0308027-05 Cl5-BZ#123 0.0893 U µg/Kg 0.0893 µg/Kg9/9/2001 1-19-090901 611675 4758823 1 0308027-05 Cl5-BZ#126 1.44 NJ µg/Kg 0.0789 µg/Kg9/9/2001 1-19-090901 611675 4758823 1 0308027-05 Cl6-BZ#128 160 µg/Kg 0.0712 µg/Kg9/9/2001 1-19-090901 611675 4758823 1 0308027-05 Cl6-BZ#138 1520 J µg/Kg 0.593 µg/Kg9/9/2001 1-19-090901 611675 4758823 1 0308027-05 Cl6-BZ#146 134 µg/Kg 0.0647 µg/Kg9/9/2001 1-19-090901 611675 4758823 1 0308027-05 Cl6-BZ#149 32.5 µg/Kg 0.0828 µg/Kg9/9/2001 1-19-090901 611675 4758823 1 0308027-05 Cl6-BZ#151 5.91 µg/Kg 0.137 µg/Kg9/9/2001 1-19-090901 611675 4758823 1 0308027-05 Cl6-BZ#153 1120 µg/Kg 0.683 µg/Kg9/9/2001 1-19-090901 611675 4758823 1 0308027-05 Cl6-BZ#156 141 µg/Kg 0.0841 µg/Kg9/9/2001 1-19-090901 611675 4758823 1 0308027-05 Cl6-BZ#157 25.1 µg/Kg 0.0660 µg/Kg



Extracted 7/30/04




SITE NUMBER



9/9/2001 1-19-090901 611675 4758823 1 0308027-05 Cl6-BZ#158 43.3 µg/Kg 0.0557 µg/Kg9/9/2001 1-19-090901 611675 4758823 1 0308027-05 Cl6-BZ#167 61.3 µg/Kg 0.0712 µg/Kg9/9/2001 1-19-090901 611675 4758823 1 0308027-05 Cl6-BZ#169 0.229 U µg/Kg 0.229 µg/Kg9/9/2001 1-19-090901 611675 4758823 1 0308027-05 Cl7-BZ#170 128 µg/Kg 0.267 µg/Kg9/9/2001 1-19-090901 611675 4758823 1 0308027-05 Cl7-BZ#174 0.0544 U µg/Kg 0.0544 µg/Kg9/9/2001 1-19-090901 611675 4758823 1 0308027-05 Cl7-BZ#177 47.1 µg/Kg 0.0764 µg/Kg9/9/2001 1-19-090901 611675 4758823 1 0308027-05 Cl7-BZ#180 147 J µg/Kg 0.114 µg/Kg9/9/2001 1-19-090901 611675 4758823 1 0308027-05 Cl7-BZ#183 31.4 µg/Kg 0.0518 µg/Kg9/9/2001 1-19-090901 611675 4758823 1 0308027-05 Cl7-BZ#187 206 µg/Kg 0.0569 µg/Kg9/9/2001 1-19-090901 611675 4758823 1 0308027-05 Cl7-BZ#189 0.102 U µg/Kg 0.102 µg/Kg9/9/2001 1-19-090901 611675 4758823 1 0308027-05 Cl8-BZ#194 8.35 µg/Kg 0.119 µg/Kg9/9/2001 1-19-090901 611675 4758823 1 0308027-05 Cl8-BZ#195 7.66 µg/Kg 0.118 µg/Kg9/9/2001 1-19-090901 611675 4758823 1 0308027-05 Cl8-BZ#201 34.7 µg/Kg 0.104 µg/Kg9/9/2001 1-19-090901 611675 4758823 1 0308027-05 Cl9-BZ#206 9.47 µg/Kg 0.139 µg/Kg9/9/2001 1-19-090901 611675 4758823 1 0308027-05 Cl10-BZ#209 0.990 µg/Kg 0.0647 µg/Kg9/9/2001 1-19-090901 611675 4758823 1 0308027-05 Monochlorobiphenyls 3.80 U µg/Kg 3.80 µg/Kg9/9/2001 1-19-090901 611675 4758823 1 0308027-05 Dichlorobiphenyls 0.641 µg/Kg 0.111 µg/Kg9/9/2001 1-19-090901 611675 4758823 1 0308027-05 Trichlorobiphenyls 210 µg/Kg 0.382 µg/Kg9/9/2001 1-19-090901 611675 4758823 1 0308027-05 Tetrachlorobiphenyls 2060 µg/Kg 0.345 µg/Kg9/9/2001 1-19-090901 611675 4758823 1 0308027-05 Pentachlorobiphenyls 5610 µg/Kg 0.398 µg/Kg9/9/2001 1-19-090901 611675 4758823 1 0308027-05 Hexachlorobiphenyls 3680 µg/Kg 0.631 µg/Kg9/9/2001 1-19-090901 611675 4758823 1 0308027-05 Heptachlorobiphenyls 552 µg/Kg 0.0595 µg/Kg9/9/2001 1-19-090901 611675 4758823 1 0308027-05 Octachlorobiphenyls 75.9 µg/Kg 0.0544 µg/Kg9/9/2001 1-19-090901 611675 4758823 1 0308027-05 Nonachlorobiphenyls 14.6 µg/Kg 0.139 µg/Kg9/9/2001 1-19-090901 611675 4758823 1 0308027-05 Decachlorobiphenyl 0.990 µg/Kg 0.0647 µg/Kg9/9/2001 1-19-090901 611675 4758823 1 0308027-05 Total Homologs 12300 µg/Kg 0.375 µg/Kg9/9/2001 1-19-090901 611675 4758823 1 0308027-05 Percent Lipids 3.1 % 0.1 %9/9/2001 1-19-090901 611675 4758823 1 0308027-05 Percent Moisture 71.2 % 0.1 %

9/12/2001 7-03-091201 614704 4781156 7 0308027-06 Cl2-BZ#8 0.121 U µg/Kg 0.121 µg/Kg9/12/2001 7-03-091201 614704 4781156 7 0308027-06 Cl3-BZ#18 1.18 J µg/Kg 0.269 µg/Kg9/12/2001 7-03-091201 614704 4781156 7 0308027-06 Cl3-BZ#31/#28 588 µg/Kg 11.2 µg/Kg9/12/2001 7-03-091201 614704 4781156 7 0308027-06 Cl4-BZ#44 41.8 µg/Kg 0.185 µg/Kg9/12/2001 7-03-091201 614704 4781156 7 0308027-06 Cl4-BZ#45 2.08 µg/Kg 0.247 µg/Kg9/12/2001 7-03-091201 614704 4781156 7 0308027-06 Cl4-BZ#47 780 µg/Kg 1.80 µg/Kg



Extracted 7/30/04




SITE NUMBER



9/12/2001 7-03-091201 614704 4781156 7 0308027-06 Cl4-BZ#49 89.6 µg/Kg 0.154 µg/Kg9/12/2001 7-03-091201 614704 4781156 7 0308027-06 Cl4-BZ#52 253 µg/Kg 0.175 µg/Kg9/12/2001 7-03-091201 614704 4781156 7 0308027-06 Cl4-BZ#56 315 µg/Kg 0.0917 µg/Kg9/12/2001 7-03-091201 614704 4781156 7 0308027-06 Cl4-BZ#66 804 µg/Kg 0.705 µg/Kg9/12/2001 7-03-091201 614704 4781156 7 0308027-06 Cl4-BZ#70 201 µg/Kg 0.107 µg/Kg9/12/2001 7-03-091201 614704 4781156 7 0308027-06 Cl4-BZ#74 1130 J µg/Kg 1.09 µg/Kg9/12/2001 7-03-091201 614704 4781156 7 0308027-06 Cl4-BZ#77 0.169 U µg/Kg 0.169 µg/Kg9/12/2001 7-03-091201 614704 4781156 7 0308027-06 Cl4-BZ#81 0.168 U µg/Kg 0.168 µg/Kg9/12/2001 7-03-091201 614704 4781156 7 0308027-06 Cl5-BZ#87 307 µg/Kg 0.0748 µg/Kg9/12/2001 7-03-091201 614704 4781156 7 0308027-06 Cl5-BZ#95 27.4 µg/Kg 0.0578 µg/Kg9/12/2001 7-03-091201 614704 4781156 7 0308027-06 Cl5-BZ#99 1040 µg/Kg 0.227 µg/Kg9/12/2001 7-03-091201 614704 4781156 7 0308027-06 Cl5-BZ#101 127 µg/Kg 0.113 µg/Kg9/12/2001 7-03-091201 614704 4781156 7 0308027-06 Cl5-BZ#105 546 µg/Kg 0.316 µg/Kg9/12/2001 7-03-091201 614704 4781156 7 0308027-06 Cl5-BZ#110 158 µg/Kg 0.107 µg/Kg9/12/2001 7-03-091201 614704 4781156 7 0308027-06 Cl5-BZ#114 53.3 µg/Kg 0.0494 µg/Kg9/12/2001 7-03-091201 614704 4781156 7 0308027-06 Cl5-BZ#118 1330 µg/Kg 0.665 µg/Kg9/12/2001 7-03-091201 614704 4781156 7 0308027-06 Cl5-BZ#123 0.0973 U µg/Kg 0.0973 µg/Kg9/12/2001 7-03-091201 614704 4781156 7 0308027-06 Cl5-BZ#126 1.04 NJ µg/Kg 0.0861 µg/Kg9/12/2001 7-03-091201 614704 4781156 7 0308027-06 Cl6-BZ#128 124 µg/Kg 0.0776 µg/Kg9/12/2001 7-03-091201 614704 4781156 7 0308027-06 Cl6-BZ#138 1260 J µg/Kg 0.640 µg/Kg9/12/2001 7-03-091201 614704 4781156 7 0308027-06 Cl6-BZ#146 183 µg/Kg 0.0705 µg/Kg9/12/2001 7-03-091201 614704 4781156 7 0308027-06 Cl6-BZ#149 43.5 µg/Kg 0.0903 µg/Kg9/12/2001 7-03-091201 614704 4781156 7 0308027-06 Cl6-BZ#151 7.72 µg/Kg 0.149 µg/Kg9/12/2001 7-03-091201 614704 4781156 7 0308027-06 Cl6-BZ#153 997 µg/Kg 0.738 µg/Kg9/12/2001 7-03-091201 614704 4781156 7 0308027-06 Cl6-BZ#156 95.6 µg/Kg 0.0917 µg/Kg9/12/2001 7-03-091201 614704 4781156 7 0308027-06 Cl6-BZ#157 17.1 µg/Kg 0.0720 µg/Kg9/12/2001 7-03-091201 614704 4781156 7 0308027-06 Cl6-BZ#158 31.6 µg/Kg 0.0607 µg/Kg9/12/2001 7-03-091201 614704 4781156 7 0308027-06 Cl6-BZ#167 35.9 µg/Kg 0.0776 µg/Kg9/12/2001 7-03-091201 614704 4781156 7 0308027-06 Cl6-BZ#169 0.250 U µg/Kg 0.250 µg/Kg9/12/2001 7-03-091201 614704 4781156 7 0308027-06 Cl7-BZ#170 119 µg/Kg 0.291 µg/Kg9/12/2001 7-03-091201 614704 4781156 7 0308027-06 Cl7-BZ#174 0.0593 U µg/Kg 0.0593 µg/Kg9/12/2001 7-03-091201 614704 4781156 7 0308027-06 Cl7-BZ#177 49.2 µg/Kg 0.0832 µg/Kg9/12/2001 7-03-091201 614704 4781156 7 0308027-06 Cl7-BZ#180 214 J µg/Kg 0.124 µg/Kg9/12/2001 7-03-091201 614704 4781156 7 0308027-06 Cl7-BZ#183 50.7 µg/Kg 0.0564 µg/Kg



Extracted 7/30/04




SITE NUMBER



9/12/2001 7-03-091201 614704 4781156 7 0308027-06 Cl7-BZ#187 473 µg/Kg 0.357 µg/Kg9/12/2001 7-03-091201 614704 4781156 7 0308027-06 Cl7-BZ#189 0.112 U µg/Kg 0.112 µg/Kg9/12/2001 7-03-091201 614704 4781156 7 0308027-06 Cl8-BZ#194 15.2 µg/Kg 0.130 µg/Kg9/12/2001 7-03-091201 614704 4781156 7 0308027-06 Cl8-BZ#195 11.6 µg/Kg 0.128 µg/Kg9/12/2001 7-03-091201 614704 4781156 7 0308027-06 Cl8-BZ#201 64.0 µg/Kg 0.113 µg/Kg9/12/2001 7-03-091201 614704 4781156 7 0308027-06 Cl9-BZ#206 15.3 µg/Kg 0.151 µg/Kg9/12/2001 7-03-091201 614704 4781156 7 0308027-06 Cl10-BZ#209 1.91 µg/Kg 0.0705 µg/Kg9/12/2001 7-03-091201 614704 4781156 7 0308027-06 Monochlorobiphenyls 4.15 U µg/Kg 4.15 µg/Kg9/12/2001 7-03-091201 614704 4781156 7 0308027-06 Dichlorobiphenyls 3.48 µg/Kg 0.121 µg/Kg9/12/2001 7-03-091201 614704 4781156 7 0308027-06 Trichlorobiphenyls 567 µg/Kg 2.39 µg/Kg9/12/2001 7-03-091201 614704 4781156 7 0308027-06 Tetrachlorobiphenyls 4380 µg/Kg 0.373 µg/Kg9/12/2001 7-03-091201 614704 4781156 7 0308027-06 Pentachlorobiphenyls 5870 µg/Kg 0.430 µg/Kg9/12/2001 7-03-091201 614704 4781156 7 0308027-06 Hexachlorobiphenyls 3210 µg/Kg 0.681 µg/Kg9/12/2001 7-03-091201 614704 4781156 7 0308027-06 Heptachlorobiphenyls 943 µg/Kg 0.373 µg/Kg9/12/2001 7-03-091201 614704 4781156 7 0308027-06 Octachlorobiphenyls 128 µg/Kg 0.0593 µg/Kg9/12/2001 7-03-091201 614704 4781156 7 0308027-06 Nonachlorobiphenyls 23.8 µg/Kg 0.151 µg/Kg9/12/2001 7-03-091201 614704 4781156 7 0308027-06 Decachlorobiphenyl 1.91 µg/Kg 0.0705 µg/Kg9/12/2001 7-03-091201 614704 4781156 7 0308027-06 Total Homologs 15200 µg/Kg 0.405 µg/Kg9/12/2001 7-03-091201 614704 4781156 7 0308027-06 Percent Lipids 3.4 % 0.1 %9/12/2001 7-03-091201 614704 4781156 7 0308027-06 Percent Moisture 72.3 % 0.1 %9/12/2001 7-06-091201 614704 4781156 7 0308027-07 Cl2-BZ#8 0.114 U µg/Kg 0.114 µg/Kg9/12/2001 7-06-091201 614704 4781156 7 0308027-07 Cl3-BZ#18 1.34 µg/Kg 0.254 µg/Kg9/12/2001 7-06-091201 614704 4781156 7 0308027-07 Cl3-BZ#31/#28 498 µg/Kg 41.8 µg/Kg9/12/2001 7-06-091201 614704 4781156 7 0308027-07 Cl4-BZ#44 158 µg/Kg 0.174 µg/Kg9/12/2001 7-06-091201 614704 4781156 7 0308027-07 Cl4-BZ#45 2.51 µg/Kg 0.233 µg/Kg9/12/2001 7-06-091201 614704 4781156 7 0308027-07 Cl4-BZ#47 2210 µg/Kg 6.74 µg/Kg9/12/2001 7-06-091201 614704 4781156 7 0308027-07 Cl4-BZ#49 257 µg/Kg 0.145 µg/Kg9/12/2001 7-06-091201 614704 4781156 7 0308027-07 Cl4-BZ#52 1060 µg/Kg 3.77 µg/Kg9/12/2001 7-06-091201 614704 4781156 7 0308027-07 Cl4-BZ#56 273 µg/Kg 0.0865 µg/Kg9/12/2001 7-06-091201 614704 4781156 7 0308027-07 Cl4-BZ#66 521 µg/Kg 2.64 µg/Kg9/12/2001 7-06-091201 614704 4781156 7 0308027-07 Cl4-BZ#70 196 µg/Kg 0.101 µg/Kg9/12/2001 7-06-091201 614704 4781156 7 0308027-07 Cl4-BZ#74 1300 J µg/Kg 4.07 µg/Kg9/12/2001 7-06-091201 614704 4781156 7 0308027-07 Cl4-BZ#77 0.160 U µg/Kg 0.160 µg/Kg9/12/2001 7-06-091201 614704 4781156 7 0308027-07 Cl4-BZ#81 0.158 U µg/Kg 0.158 µg/Kg



Extracted 7/30/04




SITE NUMBER



9/12/2001 7-06-091201 614704 4781156 7 0308027-07 Cl5-BZ#87 703 µg/Kg 1.61 µg/Kg9/12/2001 7-06-091201 614704 4781156 7 0308027-07 Cl5-BZ#95 116 µg/Kg 0.0545 µg/Kg9/12/2001 7-06-091201 614704 4781156 7 0308027-07 Cl5-BZ#99 2450 µg/Kg 0.851 µg/Kg9/12/2001 7-06-091201 614704 4781156 7 0308027-07 Cl5-BZ#101 504 µg/Kg 2.43 µg/Kg9/12/2001 7-06-091201 614704 4781156 7 0308027-07 Cl5-BZ#105 940 µg/Kg 1.18 µg/Kg9/12/2001 7-06-091201 614704 4781156 7 0308027-07 Cl5-BZ#110 312 µg/Kg 0.101 µg/Kg9/12/2001 7-06-091201 614704 4781156 7 0308027-07 Cl5-BZ#114 84.4 µg/Kg 0.0466 µg/Kg9/12/2001 7-06-091201 614704 4781156 7 0308027-07 Cl5-BZ#118 2720 µg/Kg 2.49 µg/Kg9/12/2001 7-06-091201 614704 4781156 7 0308027-07 Cl5-BZ#123 0.0918 U µg/Kg 0.0918 µg/Kg9/12/2001 7-06-091201 614704 4781156 7 0308027-07 Cl5-BZ#126 3.19 NJ µg/Kg 0.0811 µg/Kg9/12/2001 7-06-091201 614704 4781156 7 0308027-07 Cl6-BZ#128 315 µg/Kg 0.0732 µg/Kg9/12/2001 7-06-091201 614704 4781156 7 0308027-07 Cl6-BZ#138 2790 J µg/Kg 2.40 µg/Kg9/12/2001 7-06-091201 614704 4781156 7 0308027-07 Cl6-BZ#146 384 µg/Kg 1.52 µg/Kg9/12/2001 7-06-091201 614704 4781156 7 0308027-07 Cl6-BZ#149 216 µg/Kg 0.0851 µg/Kg9/12/2001 7-06-091201 614704 4781156 7 0308027-07 Cl6-BZ#151 38.1 µg/Kg 0.141 µg/Kg9/12/2001 7-06-091201 614704 4781156 7 0308027-07 Cl6-BZ#153 2060 µg/Kg 2.76 µg/Kg9/12/2001 7-06-091201 614704 4781156 7 0308027-07 Cl6-BZ#156 213 µg/Kg 0.0865 µg/Kg9/12/2001 7-06-091201 614704 4781156 7 0308027-07 Cl6-BZ#157 41.5 µg/Kg 0.0678 µg/Kg9/12/2001 7-06-091201 614704 4781156 7 0308027-07 Cl6-BZ#158 63.6 µg/Kg 0.0572 µg/Kg9/12/2001 7-06-091201 614704 4781156 7 0308027-07 Cl6-BZ#167 89.2 µg/Kg 0.0732 µg/Kg9/12/2001 7-06-091201 614704 4781156 7 0308027-07 Cl6-BZ#169 0.235 U µg/Kg 0.235 µg/Kg9/12/2001 7-06-091201 614704 4781156 7 0308027-07 Cl7-BZ#170 245 µg/Kg 0.274 µg/Kg9/12/2001 7-06-091201 614704 4781156 7 0308027-07 Cl7-BZ#174 23.8 µg/Kg 0.0559 µg/Kg9/12/2001 7-06-091201 614704 4781156 7 0308027-07 Cl7-BZ#177 127 µg/Kg 0.0785 µg/Kg9/12/2001 7-06-091201 614704 4781156 7 0308027-07 Cl7-BZ#180 403 J µg/Kg 2.67 µg/Kg9/12/2001 7-06-091201 614704 4781156 7 0308027-07 Cl7-BZ#183 88.6 µg/Kg 0.0532 µg/Kg9/12/2001 7-06-091201 614704 4781156 7 0308027-07 Cl7-BZ#187 976 µg/Kg 1.34 µg/Kg9/12/2001 7-06-091201 614704 4781156 7 0308027-07 Cl7-BZ#189 0.105 U µg/Kg 0.105 µg/Kg9/12/2001 7-06-091201 614704 4781156 7 0308027-07 Cl8-BZ#194 31.9 µg/Kg 0.122 µg/Kg9/12/2001 7-06-091201 614704 4781156 7 0308027-07 Cl8-BZ#195 21.0 µg/Kg 0.121 µg/Kg9/12/2001 7-06-091201 614704 4781156 7 0308027-07 Cl8-BZ#201 147 µg/Kg 0.106 µg/Kg9/12/2001 7-06-091201 614704 4781156 7 0308027-07 Cl9-BZ#206 29.4 µg/Kg 0.142 µg/Kg9/12/2001 7-06-091201 614704 4781156 7 0308027-07 Cl10-BZ#209 3.54 µg/Kg 0.0665 µg/Kg9/12/2001 7-06-091201 614704 4781156 7 0308027-07 Monochlorobiphenyls 3.91 U µg/Kg 3.91 µg/Kg



Extracted 7/30/04




SITE NUMBER



9/12/2001 7-06-091201 614704 4781156 7 0308027-07 Dichlorobiphenyls 6.34 µg/Kg 0.114 µg/Kg9/12/2001 7-06-091201 614704 4781156 7 0308027-07 Trichlorobiphenyls 460 µg/Kg 8.96 µg/Kg9/12/2001 7-06-091201 614704 4781156 7 0308027-07 Tetrachlorobiphenyls 7140 µg/Kg 1.40 µg/Kg9/12/2001 7-06-091201 614704 4781156 7 0308027-07 Pentachlorobiphenyls 13200 µg/Kg 1.61 µg/Kg9/12/2001 7-06-091201 614704 4781156 7 0308027-07 Hexachlorobiphenyls 7280 µg/Kg 2.55 µg/Kg9/12/2001 7-06-091201 614704 4781156 7 0308027-07 Heptachlorobiphenyls 1840 µg/Kg 1.40 µg/Kg9/12/2001 7-06-091201 614704 4781156 7 0308027-07 Octachlorobiphenyls 255 µg/Kg 0.0559 µg/Kg9/12/2001 7-06-091201 614704 4781156 7 0308027-07 Nonachlorobiphenyls 47.7 µg/Kg 0.142 µg/Kg9/12/2001 7-06-091201 614704 4781156 7 0308027-07 Decachlorobiphenyl 3.54 µg/Kg 0.0665 µg/Kg9/12/2001 7-06-091201 614704 4781156 7 0308027-07 Total Homologs 30400 µg/Kg 1.52 µg/Kg9/12/2001 7-06-091201 614704 4781156 7 0308027-07 Percent Lipids 4.9 % 0.1 %9/12/2001 7-06-091201 614704 4781156 7 0308027-07 Percent Moisture 74.4 % 0.1 %9/13/2001 7-12-091301 614704 4781156 7 0308027-08 Cl2-BZ#8 0.121 U µg/Kg 0.121 µg/Kg9/13/2001 7-12-091301 614704 4781156 7 0308027-08 Cl3-BZ#18 0.270 U µg/Kg 0.270 µg/Kg9/13/2001 7-12-091301 614704 4781156 7 0308027-08 Cl3-BZ#31/#28 367 µg/Kg 8.55 µg/Kg9/13/2001 7-12-091301 614704 4781156 7 0308027-08 Cl4-BZ#44 19.4 J µg/Kg 0.185 µg/Kg9/13/2001 7-12-091301 614704 4781156 7 0308027-08 Cl4-BZ#45 3.37 J µg/Kg 0.247 µg/Kg9/13/2001 7-12-091301 614704 4781156 7 0308027-08 Cl4-BZ#47 228 µg/Kg 0.313 µg/Kg9/13/2001 7-12-091301 614704 4781156 7 0308027-08 Cl4-BZ#49 47.5 µg/Kg 0.154 µg/Kg9/13/2001 7-12-091301 614704 4781156 7 0308027-08 Cl4-BZ#52 84.3 µg/Kg 0.175 µg/Kg9/13/2001 7-12-091301 614704 4781156 7 0308027-08 Cl4-BZ#56 132 µg/Kg 0.0918 µg/Kg9/13/2001 7-12-091301 614704 4781156 7 0308027-08 Cl4-BZ#66 317 µg/Kg 0.123 µg/Kg9/13/2001 7-12-091301 614704 4781156 7 0308027-08 Cl4-BZ#70 124 J µg/Kg 0.107 µg/Kg9/13/2001 7-12-091301 614704 4781156 7 0308027-08 Cl4-BZ#74 440 J µg/Kg 0.832 µg/Kg9/13/2001 7-12-091301 614704 4781156 7 0308027-08 Cl4-BZ#77 0.169 U µg/Kg 0.169 µg/Kg9/13/2001 7-12-091301 614704 4781156 7 0308027-08 Cl4-BZ#81 0.168 U µg/Kg 0.168 µg/Kg9/13/2001 7-12-091301 614704 4781156 7 0308027-08 Cl5-BZ#87 108 µg/Kg 0.0748 µg/Kg9/13/2001 7-12-091301 614704 4781156 7 0308027-08 Cl5-BZ#95 16.5 J µg/Kg 0.0579 µg/Kg9/13/2001 7-12-091301 614704 4781156 7 0308027-08 Cl5-BZ#99 323 µg/Kg 0.0395 µg/Kg9/13/2001 7-12-091301 614704 4781156 7 0308027-08 Cl5-BZ#101 65.5 µg/Kg 0.113 µg/Kg9/13/2001 7-12-091301 614704 4781156 7 0308027-08 Cl5-BZ#105 196 µg/Kg 0.0551 µg/Kg9/13/2001 7-12-091301 614704 4781156 7 0308027-08 Cl5-BZ#110 58.5 µg/Kg 0.107 µg/Kg9/13/2001 7-12-091301 614704 4781156 7 0308027-08 Cl5-BZ#114 21.1 µg/Kg 0.0494 µg/Kg9/13/2001 7-12-091301 614704 4781156 7 0308027-08 Cl5-BZ#118 542 µg/Kg 0.509 µg/Kg



Extracted 7/30/04




SITE NUMBER



9/13/2001 7-12-091301 614704 4781156 7 0308027-08 Cl5-BZ#123 0.0974 U µg/Kg 0.0974 µg/Kg9/13/2001 7-12-091301 614704 4781156 7 0308027-08 Cl5-BZ#126 0.508 NJ µg/Kg 0.0861 µg/Kg9/13/2001 7-12-091301 614704 4781156 7 0308027-08 Cl6-BZ#128 47.8 µg/Kg 0.0776 µg/Kg9/13/2001 7-12-091301 614704 4781156 7 0308027-08 Cl6-BZ#138 511 J µg/Kg 0.491 µg/Kg9/13/2001 7-12-091301 614704 4781156 7 0308027-08 Cl6-BZ#146 64.8 µg/Kg 0.0706 µg/Kg9/13/2001 7-12-091301 614704 4781156 7 0308027-08 Cl6-BZ#149 18.1 J µg/Kg 0.0903 µg/Kg9/13/2001 7-12-091301 614704 4781156 7 0308027-08 Cl6-BZ#151 3.99 µg/Kg 0.150 µg/Kg9/13/2001 7-12-091301 614704 4781156 7 0308027-08 Cl6-BZ#153 458 µg/Kg 0.565 µg/Kg9/13/2001 7-12-091301 614704 4781156 7 0308027-08 Cl6-BZ#156 45.3 J µg/Kg 0.0918 µg/Kg9/13/2001 7-12-091301 614704 4781156 7 0308027-08 Cl6-BZ#157 7.98 µg/Kg 0.0720 µg/Kg9/13/2001 7-12-091301 614704 4781156 7 0308027-08 Cl6-BZ#158 11.8 µg/Kg 0.0607 µg/Kg9/13/2001 7-12-091301 614704 4781156 7 0308027-08 Cl6-BZ#167 21.7 J µg/Kg 0.0776 µg/Kg9/13/2001 7-12-091301 614704 4781156 7 0308027-08 Cl6-BZ#169 0.250 U µg/Kg 0.250 µg/Kg9/13/2001 7-12-091301 614704 4781156 7 0308027-08 Cl7-BZ#170 56.5 µg/Kg 0.291 µg/Kg9/13/2001 7-12-091301 614704 4781156 7 0308027-08 Cl7-BZ#174 3.06 µg/Kg 0.0593 µg/Kg9/13/2001 7-12-091301 614704 4781156 7 0308027-08 Cl7-BZ#177 11.4 J µg/Kg 0.0833 µg/Kg9/13/2001 7-12-091301 614704 4781156 7 0308027-08 Cl7-BZ#180 97.4 J µg/Kg 0.124 µg/Kg9/13/2001 7-12-091301 614704 4781156 7 0308027-08 Cl7-BZ#183 16.5 J µg/Kg 0.0565 µg/Kg9/13/2001 7-12-091301 614704 4781156 7 0308027-08 Cl7-BZ#187 73.8 µg/Kg 0.0621 µg/Kg9/13/2001 7-12-091301 614704 4781156 7 0308027-08 Cl7-BZ#189 0.112 U µg/Kg 0.112 µg/Kg9/13/2001 7-12-091301 614704 4781156 7 0308027-08 Cl8-BZ#194 9.66 J µg/Kg 0.130 µg/Kg9/13/2001 7-12-091301 614704 4781156 7 0308027-08 Cl8-BZ#195 5.18 J µg/Kg 0.128 µg/Kg9/13/2001 7-12-091301 614704 4781156 7 0308027-08 Cl8-BZ#201 13.8 µg/Kg 0.113 µg/Kg9/13/2001 7-12-091301 614704 4781156 7 0308027-08 Cl9-BZ#206 8.44 J µg/Kg 0.151 µg/Kg9/13/2001 7-12-091301 614704 4781156 7 0308027-08 Cl10-BZ#209 1.12 J µg/Kg 0.0706 µg/Kg9/13/2001 7-12-091301 614704 4781156 7 0308027-08 Monochlorobiphenyls 4.15 U µg/Kg 4.15 µg/Kg9/13/2001 7-12-091301 614704 4781156 7 0308027-08 Dichlorobiphenyls 3.74 µg/Kg 0.121 µg/Kg9/13/2001 7-12-091301 614704 4781156 7 0308027-08 Trichlorobiphenyls 426 µg/Kg 1.83 µg/Kg9/13/2001 7-12-091301 614704 4781156 7 0308027-08 Tetrachlorobiphenyls 1790 µg/Kg 0.286 µg/Kg9/13/2001 7-12-091301 614704 4781156 7 0308027-08 Pentachlorobiphenyls 2250 µg/Kg 0.329 µg/Kg9/13/2001 7-12-091301 614704 4781156 7 0308027-08 Hexachlorobiphenyls 1360 µg/Kg 0.522 µg/Kg9/13/2001 7-12-091301 614704 4781156 7 0308027-08 Heptachlorobiphenyls 260 µg/Kg 0.0649 µg/Kg9/13/2001 7-12-091301 614704 4781156 7 0308027-08 Octachlorobiphenyls 51.1 µg/Kg 0.0593 µg/Kg9/13/2001 7-12-091301 614704 4781156 7 0308027-08 Nonachlorobiphenyls 14.0 µg/Kg 0.151 µg/Kg



Extracted 7/30/04




SITE NUMBER



9/13/2001 7-12-091301 614704 4781156 7 0308027-08 Decachlorobiphenyl 1.12 µg/Kg 0.0706 µg/Kg9/13/2001 7-12-091301 614704 4781156 7 0308027-08 Total Homologs 6180 µg/Kg 0.311 µg/Kg9/13/2001 7-12-091301 614704 4781156 7 0308027-08 Percent Lipids 5.1 % 0.1 %9/13/2001 7-12-091301 614704 4781156 7 0308027-08 Percent Moisture 72.6 % 0.1 %9/13/2001 7-13-091301 614704 4781156 7 0308027-09 Cl2-BZ#8 0.115 U µg/Kg 0.115 µg/Kg9/13/2001 7-13-091301 614704 4781156 7 0308027-09 Cl3-BZ#18 0.255 U µg/Kg 0.255 µg/Kg9/13/2001 7-13-091301 614704 4781156 7 0308027-09 Cl3-BZ#31/#28 49.8 µg/Kg 1.84 µg/Kg9/13/2001 7-13-091301 614704 4781156 7 0308027-09 Cl4-BZ#44 1.77 µg/Kg 0.175 µg/Kg9/13/2001 7-13-091301 614704 4781156 7 0308027-09 Cl4-BZ#45 0.234 U µg/Kg 0.234 µg/Kg9/13/2001 7-13-091301 614704 4781156 7 0308027-09 Cl4-BZ#47 32.1 µg/Kg 0.297 µg/Kg9/13/2001 7-13-091301 614704 4781156 7 0308027-09 Cl4-BZ#49 5.08 µg/Kg 0.146 µg/Kg9/13/2001 7-13-091301 614704 4781156 7 0308027-09 Cl4-BZ#52 9.59 µg/Kg 0.166 µg/Kg9/13/2001 7-13-091301 614704 4781156 7 0308027-09 Cl4-BZ#56 42.6 µg/Kg 0.0869 µg/Kg9/13/2001 7-13-091301 614704 4781156 7 0308027-09 Cl4-BZ#66 94.5 µg/Kg 0.116 µg/Kg9/13/2001 7-13-091301 614704 4781156 7 0308027-09 Cl4-BZ#70 22.7 µg/Kg 0.102 µg/Kg9/13/2001 7-13-091301 614704 4781156 7 0308027-09 Cl4-BZ#74 127 J µg/Kg 0.179 µg/Kg9/13/2001 7-13-091301 614704 4781156 7 0308027-09 Cl4-BZ#77 0.161 U µg/Kg 0.161 µg/Kg9/13/2001 7-13-091301 614704 4781156 7 0308027-09 Cl4-BZ#81 0.159 U µg/Kg 0.159 µg/Kg9/13/2001 7-13-091301 614704 4781156 7 0308027-09 Cl5-BZ#87 30.7 µg/Kg 0.0709 µg/Kg9/13/2001 7-13-091301 614704 4781156 7 0308027-09 Cl5-BZ#95 2.04 µg/Kg 0.0548 µg/Kg9/13/2001 7-13-091301 614704 4781156 7 0308027-09 Cl5-BZ#99 93.4 µg/Kg 0.0375 µg/Kg9/13/2001 7-13-091301 614704 4781156 7 0308027-09 Cl5-BZ#101 11.9 µg/Kg 0.107 µg/Kg9/13/2001 7-13-091301 614704 4781156 7 0308027-09 Cl5-BZ#105 65.8 µg/Kg 0.0522 µg/Kg9/13/2001 7-13-091301 614704 4781156 7 0308027-09 Cl5-BZ#110 4.37 µg/Kg 0.102 µg/Kg9/13/2001 7-13-091301 614704 4781156 7 0308027-09 Cl5-BZ#114 8.25 µg/Kg 0.0468 µg/Kg9/13/2001 7-13-091301 614704 4781156 7 0308027-09 Cl5-BZ#118 172 µg/Kg 0.110 µg/Kg9/13/2001 7-13-091301 614704 4781156 7 0308027-09 Cl5-BZ#123 0.0923 U µg/Kg 0.0923 µg/Kg9/13/2001 7-13-091301 614704 4781156 7 0308027-09 Cl5-BZ#126 0.301 NJ µg/Kg 0.0816 µg/Kg9/13/2001 7-13-091301 614704 4781156 7 0308027-09 Cl6-BZ#128 16.9 µg/Kg 0.0736 µg/Kg9/13/2001 7-13-091301 614704 4781156 7 0308027-09 Cl6-BZ#138 161 J µg/Kg 0.106 µg/Kg9/13/2001 7-13-091301 614704 4781156 7 0308027-09 Cl6-BZ#146 18.3 µg/Kg 0.0669 µg/Kg9/13/2001 7-13-091301 614704 4781156 7 0308027-09 Cl6-BZ#149 1.77 µg/Kg 0.0856 µg/Kg9/13/2001 7-13-091301 614704 4781156 7 0308027-09 Cl6-BZ#151 0.970 µg/Kg 0.142 µg/Kg9/13/2001 7-13-091301 614704 4781156 7 0308027-09 Cl6-BZ#153 150 µg/Kg 0.122 µg/Kg



Extracted 7/30/04




SITE NUMBER



9/13/2001 7-13-091301 614704 4781156 7 0308027-09 Cl6-BZ#156 16.8 µg/Kg 0.0869 µg/Kg9/13/2001 7-13-091301 614704 4781156 7 0308027-09 Cl6-BZ#157 2.93 µg/Kg 0.0682 µg/Kg9/13/2001 7-13-091301 614704 4781156 7 0308027-09 Cl6-BZ#158 2.50 µg/Kg 0.0575 µg/Kg9/13/2001 7-13-091301 614704 4781156 7 0308027-09 Cl6-BZ#167 7.20 µg/Kg 0.0736 µg/Kg9/13/2001 7-13-091301 614704 4781156 7 0308027-09 Cl6-BZ#169 0.237 U µg/Kg 0.237 µg/Kg9/13/2001 7-13-091301 614704 4781156 7 0308027-09 Cl7-BZ#170 20.9 µg/Kg 0.276 µg/Kg9/13/2001 7-13-091301 614704 4781156 7 0308027-09 Cl7-BZ#174 0.508 µg/Kg 0.0562 µg/Kg9/13/2001 7-13-091301 614704 4781156 7 0308027-09 Cl7-BZ#177 2.57 µg/Kg 0.0789 µg/Kg9/13/2001 7-13-091301 614704 4781156 7 0308027-09 Cl7-BZ#180 30.6 J µg/Kg 0.118 µg/Kg9/13/2001 7-13-091301 614704 4781156 7 0308027-09 Cl7-BZ#183 4.68 µg/Kg 0.0535 µg/Kg9/13/2001 7-13-091301 614704 4781156 7 0308027-09 Cl7-BZ#187 12.7 µg/Kg 0.0589 µg/Kg9/13/2001 7-13-091301 614704 4781156 7 0308027-09 Cl7-BZ#189 0.106 U µg/Kg 0.106 µg/Kg9/13/2001 7-13-091301 614704 4781156 7 0308027-09 Cl8-BZ#194 3.48 µg/Kg 0.123 µg/Kg9/13/2001 7-13-091301 614704 4781156 7 0308027-09 Cl8-BZ#195 1.69 µg/Kg 0.122 µg/Kg9/13/2001 7-13-091301 614704 4781156 7 0308027-09 Cl8-BZ#201 2.40 µg/Kg 0.107 µg/Kg9/13/2001 7-13-091301 614704 4781156 7 0308027-09 Cl9-BZ#206 2.50 µg/Kg 0.143 µg/Kg9/13/2001 7-13-091301 614704 4781156 7 0308027-09 Cl10-BZ#209 0.308 J µg/Kg 0.0669 µg/Kg9/13/2001 7-13-091301 614704 4781156 7 0308027-09 Monochlorobiphenyls 3.93 U µg/Kg 3.93 µg/Kg9/13/2001 7-13-091301 614704 4781156 7 0308027-09 Dichlorobiphenyls 1.38 µg/Kg 0.115 µg/Kg9/13/2001 7-13-091301 614704 4781156 7 0308027-09 Trichlorobiphenyls 90.7 µg/Kg 0.395 µg/Kg9/13/2001 7-13-091301 614704 4781156 7 0308027-09 Tetrachlorobiphenyls 397 µg/Kg 0.0615 µg/Kg9/13/2001 7-13-091301 614704 4781156 7 0308027-09 Pentachlorobiphenyls 641 µg/Kg 0.0709 µg/Kg9/13/2001 7-13-091301 614704 4781156 7 0308027-09 Hexachlorobiphenyls 416 µg/Kg 0.112 µg/Kg9/13/2001 7-13-091301 614704 4781156 7 0308027-09 Heptachlorobiphenyls 82.4 µg/Kg 0.0615 µg/Kg9/13/2001 7-13-091301 614704 4781156 7 0308027-09 Octachlorobiphenyls 16.9 µg/Kg 0.0562 µg/Kg9/13/2001 7-13-091301 614704 4781156 7 0308027-09 Nonachlorobiphenyls 4.58 µg/Kg 0.143 µg/Kg9/13/2001 7-13-091301 614704 4781156 7 0308027-09 Decachlorobiphenyl 0.308 J µg/Kg 0.0669 µg/Kg9/13/2001 7-13-091301 614704 4781156 7 0308027-09 Total Homologs 1650 µg/Kg 0.0669 µg/Kg9/13/2001 7-13-091301 614704 4781156 7 0308027-09 Percent Lipids 3.5 % 0.1 %9/13/2001 7-13-091301 614704 4781156 7 0308027-09 Percent Moisture 75.0 % 0.1 %9/14/2001 7-16-091401 614704 4781156 7 0308027-10 Cl2-BZ#8 0.0959 U µg/Kg 0.0959 µg/Kg9/14/2001 7-16-091401 614704 4781156 7 0308027-10 Cl3-BZ#18 0.213 U µg/Kg 0.213 µg/Kg9/14/2001 7-16-091401 614704 4781156 7 0308027-10 Cl3-BZ#31/#28 45.6 µg/Kg 1.54 µg/Kg9/14/2001 7-16-091401 614704 4781156 7 0308027-10 Cl4-BZ#44 1.28 µg/Kg 0.146 µg/Kg



Extracted 7/30/04




SITE NUMBER



9/14/2001 7-16-091401 614704 4781156 7 0308027-10 Cl4-BZ#45 0.195 U µg/Kg 0.195 µg/Kg9/14/2001 7-16-091401 614704 4781156 7 0308027-10 Cl4-BZ#47 16.5 µg/Kg 0.248 µg/Kg9/14/2001 7-16-091401 614704 4781156 7 0308027-10 Cl4-BZ#49 3.56 µg/Kg 0.122 µg/Kg9/14/2001 7-16-091401 614704 4781156 7 0308027-10 Cl4-BZ#52 6.76 µg/Kg 0.138 µg/Kg9/14/2001 7-16-091401 614704 4781156 7 0308027-10 Cl4-BZ#56 16.6 µg/Kg 0.0725 µg/Kg9/14/2001 7-16-091401 614704 4781156 7 0308027-10 Cl4-BZ#66 54.4 µg/Kg 0.0970 µg/Kg9/14/2001 7-16-091401 614704 4781156 7 0308027-10 Cl4-BZ#70 29.2 µg/Kg 0.0847 µg/Kg9/14/2001 7-16-091401 614704 4781156 7 0308027-10 Cl4-BZ#74 47.2 J µg/Kg 0.149 µg/Kg9/14/2001 7-16-091401 614704 4781156 7 0308027-10 Cl4-BZ#77 0.134 U µg/Kg 0.134 µg/Kg9/14/2001 7-16-091401 614704 4781156 7 0308027-10 Cl4-BZ#81 0.133 U µg/Kg 0.133 µg/Kg9/14/2001 7-16-091401 614704 4781156 7 0308027-10 Cl5-BZ#87 11.6 µg/Kg 0.0591 µg/Kg9/14/2001 7-16-091401 614704 4781156 7 0308027-10 Cl5-BZ#95 1.36 µg/Kg 0.0457 µg/Kg9/14/2001 7-16-091401 614704 4781156 7 0308027-10 Cl5-BZ#99 31.7 µg/Kg 0.0312 µg/Kg9/14/2001 7-16-091401 614704 4781156 7 0308027-10 Cl5-BZ#101 5.55 µg/Kg 0.0892 µg/Kg9/14/2001 7-16-091401 614704 4781156 7 0308027-10 Cl5-BZ#105 23.6 µg/Kg 0.0435 µg/Kg9/14/2001 7-16-091401 614704 4781156 7 0308027-10 Cl5-BZ#110 4.15 µg/Kg 0.0847 µg/Kg9/14/2001 7-16-091401 614704 4781156 7 0308027-10 Cl5-BZ#114 2.26 µg/Kg 0.0390 µg/Kg9/14/2001 7-16-091401 614704 4781156 7 0308027-10 Cl5-BZ#118 58.3 µg/Kg 0.0914 µg/Kg9/14/2001 7-16-091401 614704 4781156 7 0308027-10 Cl5-BZ#123 0.0769 U µg/Kg 0.0769 µg/Kg9/14/2001 7-16-091401 614704 4781156 7 0308027-10 Cl5-BZ#126 0.134 NJ µg/Kg 0.0680 µg/Kg9/14/2001 7-16-091401 614704 4781156 7 0308027-10 Cl6-BZ#128 3.66 µg/Kg 0.0613 µg/Kg9/14/2001 7-16-091401 614704 4781156 7 0308027-10 Cl6-BZ#138 44.7 J µg/Kg 0.0881 µg/Kg9/14/2001 7-16-091401 614704 4781156 7 0308027-10 Cl6-BZ#146 5.54 µg/Kg 0.0557 µg/Kg9/14/2001 7-16-091401 614704 4781156 7 0308027-10 Cl6-BZ#149 1.60 µg/Kg 0.0713 µg/Kg9/14/2001 7-16-091401 614704 4781156 7 0308027-10 Cl6-BZ#151 0.624 µg/Kg 0.118 µg/Kg9/14/2001 7-16-091401 614704 4781156 7 0308027-10 Cl6-BZ#153 41.8 µg/Kg 0.101 µg/Kg9/14/2001 7-16-091401 614704 4781156 7 0308027-10 Cl6-BZ#156 4.14 µg/Kg 0.0725 µg/Kg9/14/2001 7-16-091401 614704 4781156 7 0308027-10 Cl6-BZ#157 0.847 µg/Kg 0.0569 µg/Kg9/14/2001 7-16-091401 614704 4781156 7 0308027-10 Cl6-BZ#158 0.847 µg/Kg 0.0479 µg/Kg9/14/2001 7-16-091401 614704 4781156 7 0308027-10 Cl6-BZ#167 2.30 µg/Kg 0.0613 µg/Kg9/14/2001 7-16-091401 614704 4781156 7 0308027-10 Cl6-BZ#169 0.197 U µg/Kg 0.197 µg/Kg9/14/2001 7-16-091401 614704 4781156 7 0308027-10 Cl7-BZ#170 5.17 µg/Kg 0.230 µg/Kg9/14/2001 7-16-091401 614704 4781156 7 0308027-10 Cl7-BZ#174 0.407 µg/Kg 0.0468 µg/Kg9/14/2001 7-16-091401 614704 4781156 7 0308027-10 Cl7-BZ#177 1.01 µg/Kg 0.0658 µg/Kg



Extracted 7/30/04




SITE NUMBER



9/14/2001 7-16-091401 614704 4781156 7 0308027-10 Cl7-BZ#180 8.77 J µg/Kg 0.0981 µg/Kg9/14/2001 7-16-091401 614704 4781156 7 0308027-10 Cl7-BZ#183 1.46 µg/Kg 0.0446 µg/Kg9/14/2001 7-16-091401 614704 4781156 7 0308027-10 Cl7-BZ#187 4.69 µg/Kg 0.0491 µg/Kg9/14/2001 7-16-091401 614704 4781156 7 0308027-10 Cl7-BZ#189 0.0881 U µg/Kg 0.0881 µg/Kg9/14/2001 7-16-091401 614704 4781156 7 0308027-10 Cl8-BZ#194 0.864 µg/Kg 0.103 µg/Kg9/14/2001 7-16-091401 614704 4781156 7 0308027-10 Cl8-BZ#195 0.351 J µg/Kg 0.101 µg/Kg9/14/2001 7-16-091401 614704 4781156 7 0308027-10 Cl8-BZ#201 0.697 µg/Kg 0.0892 µg/Kg9/14/2001 7-16-091401 614704 4781156 7 0308027-10 Cl9-BZ#206 0.580 J µg/Kg 0.119 µg/Kg9/14/2001 7-16-091401 614704 4781156 7 0308027-10 Cl10-BZ#209 0.112 J µg/Kg 0.0557 µg/Kg9/14/2001 7-16-091401 614704 4781156 7 0308027-10 Monochlorobiphenyls 3.28 U µg/Kg 3.28 µg/Kg9/14/2001 7-16-091401 614704 4781156 7 0308027-10 Dichlorobiphenyls 0.641 µg/Kg 0.0959 µg/Kg9/14/2001 7-16-091401 614704 4781156 7 0308027-10 Trichlorobiphenyls 81.8 µg/Kg 0.329 µg/Kg9/14/2001 7-16-091401 614704 4781156 7 0308027-10 Tetrachlorobiphenyls 215 µg/Kg 0.0513 µg/Kg9/14/2001 7-16-091401 614704 4781156 7 0308027-10 Pentachlorobiphenyls 240 µg/Kg 0.0591 µg/Kg9/14/2001 7-16-091401 614704 4781156 7 0308027-10 Hexachlorobiphenyls 122 µg/Kg 0.0936 µg/Kg9/14/2001 7-16-091401 614704 4781156 7 0308027-10 Heptachlorobiphenyls 37.0 µg/Kg 0.0513 µg/Kg9/14/2001 7-16-091401 614704 4781156 7 0308027-10 Octachlorobiphenyls 5.96 µg/Kg 0.0468 µg/Kg9/14/2001 7-16-091401 614704 4781156 7 0308027-10 Nonachlorobiphenyls 1.81 µg/Kg 0.119 µg/Kg9/14/2001 7-16-091401 614704 4781156 7 0308027-10 Decachlorobiphenyl 0.112 J µg/Kg 0.0557 µg/Kg9/14/2001 7-16-091401 614704 4781156 7 0308027-10 Total Homologs 704 µg/Kg 0.0557 µg/Kg9/14/2001 7-16-091401 614704 4781156 7 0308027-10 Percent Lipids 3.3 % 0.1 %9/14/2001 7-16-091401 614704 4781156 7 0308027-10 Percent Moisture 71.6 % 0.1 %9/13/2001 8-07-091301 614814 4783340 8 0308027-11 Cl2-BZ#8 0.114 U µg/Kg 0.114 µg/Kg9/13/2001 8-07-091301 614814 4783340 8 0308027-11 Cl3-BZ#18 1.05 J µg/Kg 0.253 µg/Kg9/13/2001 8-07-091301 614814 4783340 8 0308027-11 Cl3-BZ#31/#28 258 µg/Kg 1.83 µg/Kg9/13/2001 8-07-091301 614814 4783340 8 0308027-11 Cl4-BZ#44 84.4 µg/Kg 0.174 µg/Kg9/13/2001 8-07-091301 614814 4783340 8 0308027-11 Cl4-BZ#45 2.37 µg/Kg 0.232 µg/Kg9/13/2001 8-07-091301 614814 4783340 8 0308027-11 Cl4-BZ#47 1830 µg/Kg 3.30 µg/Kg9/13/2001 8-07-091301 614814 4783340 8 0308027-11 Cl4-BZ#49 148 µg/Kg 0.145 µg/Kg9/13/2001 8-07-091301 614814 4783340 8 0308027-11 Cl4-BZ#52 651 µg/Kg 1.84 µg/Kg9/13/2001 8-07-091301 614814 4783340 8 0308027-11 Cl4-BZ#56 211 µg/Kg 0.0862 µg/Kg9/13/2001 8-07-091301 614814 4783340 8 0308027-11 Cl4-BZ#66 407 µg/Kg 1.29 µg/Kg9/13/2001 8-07-091301 614814 4783340 8 0308027-11 Cl4-BZ#70 138 µg/Kg 0.101 µg/Kg9/13/2001 8-07-091301 614814 4783340 8 0308027-11 Cl4-BZ#74 1040 J µg/Kg 1.99 µg/Kg



Extracted 7/30/04




SITE NUMBER



9/13/2001 8-07-091301 614814 4783340 8 0308027-11 Cl4-BZ#77 0.159 U µg/Kg 0.159 µg/Kg9/13/2001 8-07-091301 614814 4783340 8 0308027-11 Cl4-BZ#81 0.158 U µg/Kg 0.158 µg/Kg9/13/2001 8-07-091301 614814 4783340 8 0308027-11 Cl5-BZ#87 369 µg/Kg 0.787 µg/Kg9/13/2001 8-07-091301 614814 4783340 8 0308027-11 Cl5-BZ#95 50.1 µg/Kg 0.0544 µg/Kg9/13/2001 8-07-091301 614814 4783340 8 0308027-11 Cl5-BZ#99 1950 µg/Kg 0.416 µg/Kg9/13/2001 8-07-091301 614814 4783340 8 0308027-11 Cl5-BZ#101 239 µg/Kg 0.106 µg/Kg9/13/2001 8-07-091301 614814 4783340 8 0308027-11 Cl5-BZ#105 791 µg/Kg 0.579 µg/Kg9/13/2001 8-07-091301 614814 4783340 8 0308027-11 Cl5-BZ#110 224 µg/Kg 0.101 µg/Kg9/13/2001 8-07-091301 614814 4783340 8 0308027-11 Cl5-BZ#114 62.5 µg/Kg 0.0464 µg/Kg9/13/2001 8-07-091301 614814 4783340 8 0308027-11 Cl5-BZ#118 2260 µg/Kg 1.22 µg/Kg9/13/2001 8-07-091301 614814 4783340 8 0308027-11 Cl5-BZ#123 0.0915 U µg/Kg 0.0915 µg/Kg9/13/2001 8-07-091301 614814 4783340 8 0308027-11 Cl5-BZ#126 3.68 NJ µg/Kg 0.0809 µg/Kg9/13/2001 8-07-091301 614814 4783340 8 0308027-11 Cl6-BZ#128 212 µg/Kg 0.0729 µg/Kg9/13/2001 8-07-091301 614814 4783340 8 0308027-11 Cl6-BZ#138 2230 J µg/Kg 1.17 µg/Kg9/13/2001 8-07-091301 614814 4783340 8 0308027-11 Cl6-BZ#146 292 µg/Kg 0.0663 µg/Kg9/13/2001 8-07-091301 614814 4783340 8 0308027-11 Cl6-BZ#149 118 µg/Kg 0.0848 µg/Kg9/13/2001 8-07-091301 614814 4783340 8 0308027-11 Cl6-BZ#151 18.6 µg/Kg 0.140 µg/Kg9/13/2001 8-07-091301 614814 4783340 8 0308027-11 Cl6-BZ#153 1790 µg/Kg 1.35 µg/Kg9/13/2001 8-07-091301 614814 4783340 8 0308027-11 Cl6-BZ#156 181 µg/Kg 0.0862 µg/Kg9/13/2001 8-07-091301 614814 4783340 8 0308027-11 Cl6-BZ#157 32.4 µg/Kg 0.0676 µg/Kg9/13/2001 8-07-091301 614814 4783340 8 0308027-11 Cl6-BZ#158 69.7 µg/Kg 0.0570 µg/Kg9/13/2001 8-07-091301 614814 4783340 8 0308027-11 Cl6-BZ#167 69.6 µg/Kg 0.0729 µg/Kg9/13/2001 8-07-091301 614814 4783340 8 0308027-11 Cl6-BZ#169 0.235 U µg/Kg 0.235 µg/Kg9/13/2001 8-07-091301 614814 4783340 8 0308027-11 Cl7-BZ#170 232 µg/Kg 0.273 µg/Kg9/13/2001 8-07-091301 614814 4783340 8 0308027-11 Cl7-BZ#174 14.6 µg/Kg 0.0557 µg/Kg9/13/2001 8-07-091301 614814 4783340 8 0308027-11 Cl7-BZ#177 91.4 µg/Kg 0.0782 µg/Kg9/13/2001 8-07-091301 614814 4783340 8 0308027-11 Cl7-BZ#180 548 J µg/Kg 1.31 µg/Kg9/13/2001 8-07-091301 614814 4783340 8 0308027-11 Cl7-BZ#183 113 µg/Kg 0.0530 µg/Kg9/13/2001 8-07-091301 614814 4783340 8 0308027-11 Cl7-BZ#187 822 µg/Kg 0.653 µg/Kg9/13/2001 8-07-091301 614814 4783340 8 0308027-11 Cl7-BZ#189 9.02 µg/Kg 0.105 µg/Kg9/13/2001 8-07-091301 614814 4783340 8 0308027-11 Cl8-BZ#194 27.6 µg/Kg 0.122 µg/Kg9/13/2001 8-07-091301 614814 4783340 8 0308027-11 Cl8-BZ#195 17.0 µg/Kg 0.121 µg/Kg9/13/2001 8-07-091301 614814 4783340 8 0308027-11 Cl8-BZ#201 116 µg/Kg 0.106 µg/Kg9/13/2001 8-07-091301 614814 4783340 8 0308027-11 Cl9-BZ#206 28.6 µg/Kg 0.142 µg/Kg



Extracted 7/30/04




SITE NUMBER



9/13/2001 8-07-091301 614814 4783340 8 0308027-11 Cl10-BZ#209 3.21 µg/Kg 0.0663 µg/Kg9/13/2001 8-07-091301 614814 4783340 8 0308027-11 Monochlorobiphenyls 3.90 U µg/Kg 3.90 µg/Kg9/13/2001 8-07-091301 614814 4783340 8 0308027-11 Dichlorobiphenyls 3.55 µg/Kg 0.114 µg/Kg9/13/2001 8-07-091301 614814 4783340 8 0308027-11 Trichlorobiphenyls 398 µg/Kg 0.391 µg/Kg9/13/2001 8-07-091301 614814 4783340 8 0308027-11 Tetrachlorobiphenyls 5540 µg/Kg 0.683 µg/Kg9/13/2001 8-07-091301 614814 4783340 8 0308027-11 Pentachlorobiphenyls 10100 µg/Kg 0.787 µg/Kg9/13/2001 8-07-091301 614814 4783340 8 0308027-11 Hexachlorobiphenyls 5920 µg/Kg 1.25 µg/Kg9/13/2001 8-07-091301 614814 4783340 8 0308027-11 Heptachlorobiphenyls 1860 µg/Kg 0.683 µg/Kg9/13/2001 8-07-091301 614814 4783340 8 0308027-11 Octachlorobiphenyls 232 µg/Kg 0.0557 µg/Kg9/13/2001 8-07-091301 614814 4783340 8 0308027-11 Nonachlorobiphenyls 41.9 µg/Kg 0.142 µg/Kg9/13/2001 8-07-091301 614814 4783340 8 0308027-11 Decachlorobiphenyl 3.21 µg/Kg 0.0663 µg/Kg9/13/2001 8-07-091301 614814 4783340 8 0308027-11 Total Homologs 24200 µg/Kg 0.742 µg/Kg9/13/2001 8-07-091301 614814 4783340 8 0308027-11 Percent Lipids 4.1 % 0.1 %9/13/2001 8-07-091301 614814 4783340 8 0308027-11 Percent Moisture 71.8 % 0.1 %9/13/2001 8-12-091301 614814 4783340 8 0308027-12 Cl2-BZ#8 0.113 U µg/Kg 0.113 µg/Kg9/13/2001 8-12-091301 614814 4783340 8 0308027-12 Cl3-BZ#18 0.251 U µg/Kg 0.251 µg/Kg9/13/2001 8-12-091301 614814 4783340 8 0308027-12 Cl3-BZ#31/#28 16.0 µg/Kg 1.81 µg/Kg9/13/2001 8-12-091301 614814 4783340 8 0308027-12 Cl4-BZ#44 0.763 J µg/Kg 0.172 µg/Kg9/13/2001 8-12-091301 614814 4783340 8 0308027-12 Cl4-BZ#45 0.230 U µg/Kg 0.230 µg/Kg9/13/2001 8-12-091301 614814 4783340 8 0308027-12 Cl4-BZ#47 18.6 µg/Kg 0.292 µg/Kg9/13/2001 8-12-091301 614814 4783340 8 0308027-12 Cl4-BZ#49 1.62 µg/Kg 0.143 µg/Kg9/13/2001 8-12-091301 614814 4783340 8 0308027-12 Cl4-BZ#52 5.24 µg/Kg 0.163 µg/Kg9/13/2001 8-12-091301 614814 4783340 8 0308027-12 Cl4-BZ#56 8.54 µg/Kg 0.0855 µg/Kg9/13/2001 8-12-091301 614814 4783340 8 0308027-12 Cl4-BZ#66 21.1 µg/Kg 0.114 µg/Kg9/13/2001 8-12-091301 614814 4783340 8 0308027-12 Cl4-BZ#70 4.92 µg/Kg 0.0999 µg/Kg9/13/2001 8-12-091301 614814 4783340 8 0308027-12 Cl4-BZ#74 23.9 J µg/Kg 0.176 µg/Kg9/13/2001 8-12-091301 614814 4783340 8 0308027-12 Cl4-BZ#77 0.158 U µg/Kg 0.158 µg/Kg9/13/2001 8-12-091301 614814 4783340 8 0308027-12 Cl4-BZ#81 0.156 U µg/Kg 0.156 µg/Kg9/13/2001 8-12-091301 614814 4783340 8 0308027-12 Cl5-BZ#87 9.65 µg/Kg 0.0697 µg/Kg9/13/2001 8-12-091301 614814 4783340 8 0308027-12 Cl5-BZ#95 0.618 µg/Kg 0.0539 µg/Kg9/13/2001 8-12-091301 614814 4783340 8 0308027-12 Cl5-BZ#99 36.8 µg/Kg 0.0368 µg/Kg9/13/2001 8-12-091301 614814 4783340 8 0308027-12 Cl5-BZ#101 3.51 µg/Kg 0.105 µg/Kg9/13/2001 8-12-091301 614814 4783340 8 0308027-12 Cl5-BZ#105 23.9 µg/Kg 0.0513 µg/Kg9/13/2001 8-12-091301 614814 4783340 8 0308027-12 Cl5-BZ#110 2.65 µg/Kg 0.0999 µg/Kg



Extracted 7/30/04




SITE NUMBER



9/13/2001 8-12-091301 614814 4783340 8 0308027-12 Cl5-BZ#114 1.83 µg/Kg 0.0460 µg/Kg9/13/2001 8-12-091301 614814 4783340 8 0308027-12 Cl5-BZ#118 60.2 µg/Kg 0.108 µg/Kg9/13/2001 8-12-091301 614814 4783340 8 0308027-12 Cl5-BZ#123 0.0907 U µg/Kg 0.0907 µg/Kg9/13/2001 8-12-091301 614814 4783340 8 0308027-12 Cl5-BZ#126 0.158 NJ µg/Kg 0.0802 µg/Kg9/13/2001 8-12-091301 614814 4783340 8 0308027-12 Cl6-BZ#128 4.10 µg/Kg 0.0723 µg/Kg9/13/2001 8-12-091301 614814 4783340 8 0308027-12 Cl6-BZ#138 65.8 J µg/Kg 0.104 µg/Kg9/13/2001 8-12-091301 614814 4783340 8 0308027-12 Cl6-BZ#146 7.33 µg/Kg 0.0658 µg/Kg9/13/2001 8-12-091301 614814 4783340 8 0308027-12 Cl6-BZ#149 1.53 µg/Kg 0.0842 µg/Kg9/13/2001 8-12-091301 614814 4783340 8 0308027-12 Cl6-BZ#151 0.394 J µg/Kg 0.139 µg/Kg9/13/2001 8-12-091301 614814 4783340 8 0308027-12 Cl6-BZ#153 62.3 µg/Kg 0.120 µg/Kg9/13/2001 8-12-091301 614814 4783340 8 0308027-12 Cl6-BZ#156 5.53 µg/Kg 0.0855 µg/Kg9/13/2001 8-12-091301 614814 4783340 8 0308027-12 Cl6-BZ#157 1.05 µg/Kg 0.0671 µg/Kg9/13/2001 8-12-091301 614814 4783340 8 0308027-12 Cl6-BZ#158 0.973 µg/Kg 0.0565 µg/Kg9/13/2001 8-12-091301 614814 4783340 8 0308027-12 Cl6-BZ#167 2.96 µg/Kg 0.0723 µg/Kg9/13/2001 8-12-091301 614814 4783340 8 0308027-12 Cl6-BZ#169 0.233 U µg/Kg 0.233 µg/Kg9/13/2001 8-12-091301 614814 4783340 8 0308027-12 Cl7-BZ#170 9.29 µg/Kg 0.271 µg/Kg9/13/2001 8-12-091301 614814 4783340 8 0308027-12 Cl7-BZ#174 0.434 µg/Kg 0.0552 µg/Kg9/13/2001 8-12-091301 614814 4783340 8 0308027-12 Cl7-BZ#177 1.31 µg/Kg 0.0776 µg/Kg9/13/2001 8-12-091301 614814 4783340 8 0308027-12 Cl7-BZ#180 14.2 J µg/Kg 0.116 µg/Kg9/13/2001 8-12-091301 614814 4783340 8 0308027-12 Cl7-BZ#183 2.41 µg/Kg 0.0526 µg/Kg9/13/2001 8-12-091301 614814 4783340 8 0308027-12 Cl7-BZ#187 9.40 µg/Kg 0.0579 µg/Kg9/13/2001 8-12-091301 614814 4783340 8 0308027-12 Cl7-BZ#189 0.104 U µg/Kg 0.104 µg/Kg9/13/2001 8-12-091301 614814 4783340 8 0308027-12 Cl8-BZ#194 0.121 U µg/Kg 0.121 µg/Kg9/13/2001 8-12-091301 614814 4783340 8 0308027-12 Cl8-BZ#195 0.822 µg/Kg 0.120 µg/Kg9/13/2001 8-12-091301 614814 4783340 8 0308027-12 Cl8-BZ#201 1.54 µg/Kg 0.105 µg/Kg9/13/2001 8-12-091301 614814 4783340 8 0308027-12 Cl9-BZ#206 1.45 µg/Kg 0.141 µg/Kg9/13/2001 8-12-091301 614814 4783340 8 0308027-12 Cl10-BZ#209 0.263 J µg/Kg 0.0658 µg/Kg9/13/2001 8-12-091301 614814 4783340 8 0308027-12 Monochlorobiphenyls 3.87 U µg/Kg 3.87 µg/Kg9/13/2001 8-12-091301 614814 4783340 8 0308027-12 Dichlorobiphenyls 0.191 J µg/Kg 0.113 µg/Kg9/13/2001 8-12-091301 614814 4783340 8 0308027-12 Trichlorobiphenyls 12.9 µg/Kg 0.388 µg/Kg9/13/2001 8-12-091301 614814 4783340 8 0308027-12 Tetrachlorobiphenyls 108 µg/Kg 0.0605 µg/Kg9/13/2001 8-12-091301 614814 4783340 8 0308027-12 Pentachlorobiphenyls 232 µg/Kg 0.0697 µg/Kg9/13/2001 8-12-091301 614814 4783340 8 0308027-12 Hexachlorobiphenyls 170 µg/Kg 0.111 µg/Kg9/13/2001 8-12-091301 614814 4783340 8 0308027-12 Heptachlorobiphenyls 53.0 µg/Kg 0.0605 µg/Kg



Extracted 7/30/04




SITE NUMBER



9/13/2001 8-12-091301 614814 4783340 8 0308027-12 Octachlorobiphenyls 10.8 µg/Kg 0.0552 µg/Kg9/13/2001 8-12-091301 614814 4783340 8 0308027-12 Nonachlorobiphenyls 3.08 µg/Kg 0.141 µg/Kg9/13/2001 8-12-091301 614814 4783340 8 0308027-12 Decachlorobiphenyl 0.263 J µg/Kg 0.0658 µg/Kg9/13/2001 8-12-091301 614814 4783340 8 0308027-12 Total Homologs 590 µg/Kg 0.0658 µg/Kg9/13/2001 8-12-091301 614814 4783340 8 0308027-12 Percent Lipids 3.3 % 0.1 %9/13/2001 8-12-091301 614814 4783340 8 0308027-12 Percent Moisture 72.7 % 0.1 %9/13/2001 8-14-091301 614814 4783340 8 0308027-13 Cl2-BZ#8 0.116 U µg/Kg 0.116 µg/Kg9/13/2001 8-14-091301 614814 4783340 8 0308027-13 Cl3-BZ#18 0.258 U µg/Kg 0.258 µg/Kg9/13/2001 8-14-091301 614814 4783340 8 0308027-13 Cl3-BZ#31/#28 7.58 J µg/Kg 1.86 µg/Kg9/13/2001 8-14-091301 614814 4783340 8 0308027-13 Cl4-BZ#44 0.263 J µg/Kg 0.177 µg/Kg9/13/2001 8-14-091301 614814 4783340 8 0308027-13 Cl4-BZ#45 0.236 U µg/Kg 0.236 µg/Kg9/13/2001 8-14-091301 614814 4783340 8 0308027-13 Cl4-BZ#47 6.96 µg/Kg 0.300 µg/Kg9/13/2001 8-14-091301 614814 4783340 8 0308027-13 Cl4-BZ#49 0.668 J µg/Kg 0.147 µg/Kg9/13/2001 8-14-091301 614814 4783340 8 0308027-13 Cl4-BZ#52 1.37 µg/Kg 0.167 µg/Kg9/13/2001 8-14-091301 614814 4783340 8 0308027-13 Cl4-BZ#56 7.17 µg/Kg 0.0877 µg/Kg9/13/2001 8-14-091301 614814 4783340 8 0308027-13 Cl4-BZ#66 19.2 µg/Kg 0.117 µg/Kg9/13/2001 8-14-091301 614814 4783340 8 0308027-13 Cl4-BZ#70 3.62 µg/Kg 0.103 µg/Kg9/13/2001 8-14-091301 614814 4783340 8 0308027-13 Cl4-BZ#74 16.1 J µg/Kg 0.181 µg/Kg9/13/2001 8-14-091301 614814 4783340 8 0308027-13 Cl4-BZ#77 0.162 U µg/Kg 0.162 µg/Kg9/13/2001 8-14-091301 614814 4783340 8 0308027-13 Cl4-BZ#81 0.161 U µg/Kg 0.161 µg/Kg9/13/2001 8-14-091301 614814 4783340 8 0308027-13 Cl5-BZ#87 6.13 µg/Kg 0.0715 µg/Kg9/13/2001 8-14-091301 614814 4783340 8 0308027-13 Cl5-BZ#95 0.263 J µg/Kg 0.0553 µg/Kg9/13/2001 8-14-091301 614814 4783340 8 0308027-13 Cl5-BZ#99 22.4 µg/Kg 0.0378 µg/Kg9/13/2001 8-14-091301 614814 4783340 8 0308027-13 Cl5-BZ#101 1.54 µg/Kg 0.108 µg/Kg9/13/2001 8-14-091301 614814 4783340 8 0308027-13 Cl5-BZ#105 18.5 µg/Kg 0.0526 µg/Kg9/13/2001 8-14-091301 614814 4783340 8 0308027-13 Cl5-BZ#110 1.01 µg/Kg 0.103 µg/Kg9/13/2001 8-14-091301 614814 4783340 8 0308027-13 Cl5-BZ#114 1.65 µg/Kg 0.0472 µg/Kg9/13/2001 8-14-091301 614814 4783340 8 0308027-13 Cl5-BZ#118 46.3 µg/Kg 0.111 µg/Kg9/13/2001 8-14-091301 614814 4783340 8 0308027-13 Cl5-BZ#123 0.0931 U µg/Kg 0.0931 µg/Kg9/13/2001 8-14-091301 614814 4783340 8 0308027-13 Cl5-BZ#126 0.169 NJ µg/Kg 0.0823 µg/Kg9/13/2001 8-14-091301 614814 4783340 8 0308027-13 Cl6-BZ#128 3.18 µg/Kg 0.0742 µg/Kg9/13/2001 8-14-091301 614814 4783340 8 0308027-13 Cl6-BZ#138 52.1 J µg/Kg 0.107 µg/Kg9/13/2001 8-14-091301 614814 4783340 8 0308027-13 Cl6-BZ#146 5.28 µg/Kg 0.0675 µg/Kg9/13/2001 8-14-091301 614814 4783340 8 0308027-13 Cl6-BZ#149 0.601 µg/Kg 0.0864 µg/Kg



Extracted 7/30/04




SITE NUMBER



9/13/2001 8-14-091301 614814 4783340 8 0308027-13 Cl6-BZ#151 0.243 J µg/Kg 0.143 µg/Kg9/13/2001 8-14-091301 614814 4783340 8 0308027-13 Cl6-BZ#153 49.8 µg/Kg 0.123 µg/Kg9/13/2001 8-14-091301 614814 4783340 8 0308027-13 Cl6-BZ#156 4.93 µg/Kg 0.0877 µg/Kg9/13/2001 8-14-091301 614814 4783340 8 0308027-13 Cl6-BZ#157 0.938 µg/Kg 0.0688 µg/Kg9/13/2001 8-14-091301 614814 4783340 8 0308027-13 Cl6-BZ#158 0.715 µg/Kg 0.0580 µg/Kg9/13/2001 8-14-091301 614814 4783340 8 0308027-13 Cl6-BZ#167 2.50 µg/Kg 0.0742 µg/Kg9/13/2001 8-14-091301 614814 4783340 8 0308027-13 Cl6-BZ#169 0.239 U µg/Kg 0.239 µg/Kg9/13/2001 8-14-091301 614814 4783340 8 0308027-13 Cl7-BZ#170 6.86 µg/Kg 0.278 µg/Kg9/13/2001 8-14-091301 614814 4783340 8 0308027-13 Cl7-BZ#174 0.243 J µg/Kg 0.0567 µg/Kg9/13/2001 8-14-091301 614814 4783340 8 0308027-13 Cl7-BZ#177 0.702 µg/Kg 0.0796 µg/Kg9/13/2001 8-14-091301 614814 4783340 8 0308027-13 Cl7-BZ#180 10.2 J µg/Kg 0.119 µg/Kg9/13/2001 8-14-091301 614814 4783340 8 0308027-13 Cl7-BZ#183 1.42 µg/Kg 0.0540 µg/Kg9/13/2001 8-14-091301 614814 4783340 8 0308027-13 Cl7-BZ#187 3.85 µg/Kg 0.0594 µg/Kg9/13/2001 8-14-091301 614814 4783340 8 0308027-13 Cl7-BZ#189 0.107 U µg/Kg 0.107 µg/Kg9/13/2001 8-14-091301 614814 4783340 8 0308027-13 Cl8-BZ#194 1.37 µg/Kg 0.124 µg/Kg9/13/2001 8-14-091301 614814 4783340 8 0308027-13 Cl8-BZ#195 0.493 J µg/Kg 0.123 µg/Kg9/13/2001 8-14-091301 614814 4783340 8 0308027-13 Cl8-BZ#201 0.783 µg/Kg 0.108 µg/Kg9/13/2001 8-14-091301 614814 4783340 8 0308027-13 Cl9-BZ#206 1.09 µg/Kg 0.144 µg/Kg9/13/2001 8-14-091301 614814 4783340 8 0308027-13 Cl10-BZ#209 0.277 J µg/Kg 0.0675 µg/Kg9/13/2001 8-14-091301 614814 4783340 8 0308027-13 Monochlorobiphenyls 3.97 U µg/Kg 3.97 µg/Kg9/13/2001 8-14-091301 614814 4783340 8 0308027-13 Dichlorobiphenyls 0.116 U µg/Kg 0.116 µg/Kg9/13/2001 8-14-091301 614814 4783340 8 0308027-13 Trichlorobiphenyls 11.8 µg/Kg 0.398 µg/Kg9/13/2001 8-14-091301 614814 4783340 8 0308027-13 Tetrachlorobiphenyls 69.9 µg/Kg 0.0621 µg/Kg9/13/2001 8-14-091301 614814 4783340 8 0308027-13 Pentachlorobiphenyls 164 µg/Kg 0.0715 µg/Kg9/13/2001 8-14-091301 614814 4783340 8 0308027-13 Hexachlorobiphenyls 135 µg/Kg 0.113 µg/Kg9/13/2001 8-14-091301 614814 4783340 8 0308027-13 Heptachlorobiphenyls 37.6 µg/Kg 0.0621 µg/Kg9/13/2001 8-14-091301 614814 4783340 8 0308027-13 Octachlorobiphenyls 10.3 µg/Kg 0.0567 µg/Kg9/13/2001 8-14-091301 614814 4783340 8 0308027-13 Nonachlorobiphenyls 2.23 µg/Kg 0.144 µg/Kg9/13/2001 8-14-091301 614814 4783340 8 0308027-13 Decachlorobiphenyl 0.277 J µg/Kg 0.0675 µg/Kg9/13/2001 8-14-091301 614814 4783340 8 0308027-13 Total Homologs 431 µg/Kg 0.0675 µg/Kg9/13/2001 8-14-091301 614814 4783340 8 0308027-13 Percent Lipids 4.2 % 0.1 %9/13/2001 8-14-091301 614814 4783340 8 0308027-13 Percent Moisture 73.0 % 0.1 %9/14/2001 8-20-091401 614814 4783340 8 0308027-14 Cl2-BZ#8 0.113 U µg/Kg 0.113 µg/Kg9/14/2001 8-20-091401 614814 4783340 8 0308027-14 Cl3-BZ#18 0.252 U µg/Kg 0.252 µg/Kg



Extracted 7/30/04




SITE NUMBER



9/14/2001 8-20-091401 614814 4783340 8 0308027-14 Cl3-BZ#31/#28 6.13 J µg/Kg 1.81 µg/Kg9/14/2001 8-20-091401 614814 4783340 8 0308027-14 Cl4-BZ#44 0.277 J µg/Kg 0.173 µg/Kg9/14/2001 8-20-091401 614814 4783340 8 0308027-14 Cl4-BZ#45 0.231 U µg/Kg 0.231 µg/Kg9/14/2001 8-20-091401 614814 4783340 8 0308027-14 Cl4-BZ#47 3.81 µg/Kg 0.292 µg/Kg9/14/2001 8-20-091401 614814 4783340 8 0308027-14 Cl4-BZ#49 0.672 J µg/Kg 0.144 µg/Kg9/14/2001 8-20-091401 614814 4783340 8 0308027-14 Cl4-BZ#52 1.15 µg/Kg 0.163 µg/Kg9/14/2001 8-20-091401 614814 4783340 8 0308027-14 Cl4-BZ#56 2.75 µg/Kg 0.0856 µg/Kg9/14/2001 8-20-091401 614814 4783340 8 0308027-14 Cl4-BZ#66 7.59 µg/Kg 0.115 µg/Kg9/14/2001 8-20-091401 614814 4783340 8 0308027-14 Cl4-BZ#70 2.54 µg/Kg 0.100 µg/Kg9/14/2001 8-20-091401 614814 4783340 8 0308027-14 Cl4-BZ#74 6.07 J µg/Kg 0.176 µg/Kg9/14/2001 8-20-091401 614814 4783340 8 0308027-14 Cl4-BZ#77 0.158 U µg/Kg 0.158 µg/Kg9/14/2001 8-20-091401 614814 4783340 8 0308027-14 Cl4-BZ#81 0.157 U µg/Kg 0.157 µg/Kg9/14/2001 8-20-091401 614814 4783340 8 0308027-14 Cl5-BZ#87 2.88 µg/Kg 0.0698 µg/Kg9/14/2001 8-20-091401 614814 4783340 8 0308027-14 Cl5-BZ#95 0.250 J µg/Kg 0.0540 µg/Kg9/14/2001 8-20-091401 614814 4783340 8 0308027-14 Cl5-BZ#99 9.84 µg/Kg 0.0369 µg/Kg9/14/2001 8-20-091401 614814 4783340 8 0308027-14 Cl5-BZ#101 1.11 µg/Kg 0.105 µg/Kg9/14/2001 8-20-091401 614814 4783340 8 0308027-14 Cl5-BZ#105 0.0514 U µg/Kg 0.0514 µg/Kg9/14/2001 8-20-091401 614814 4783340 8 0308027-14 Cl5-BZ#110 0.823 µg/Kg 0.100 µg/Kg9/14/2001 8-20-091401 614814 4783340 8 0308027-14 Cl5-BZ#114 0.520 µg/Kg 0.0461 µg/Kg9/14/2001 8-20-091401 614814 4783340 8 0308027-14 Cl5-BZ#118 18.4 µg/Kg 0.108 µg/Kg9/14/2001 8-20-091401 614814 4783340 8 0308027-14 Cl5-BZ#123 0.0909 U µg/Kg 0.0909 µg/Kg9/14/2001 8-20-091401 614814 4783340 8 0308027-14 Cl5-BZ#126 0.0804 U µg/Kg 0.0804 µg/Kg9/14/2001 8-20-091401 614814 4783340 8 0308027-14 Cl6-BZ#128 1.40 µg/Kg 0.0725 µg/Kg9/14/2001 8-20-091401 614814 4783340 8 0308027-14 Cl6-BZ#138 22.3 J µg/Kg 0.104 µg/Kg9/14/2001 8-20-091401 614814 4783340 8 0308027-14 Cl6-BZ#146 2.07 µg/Kg 0.0659 µg/Kg9/14/2001 8-20-091401 614814 4783340 8 0308027-14 Cl6-BZ#149 0.514 µg/Kg 0.0843 µg/Kg9/14/2001 8-20-091401 614814 4783340 8 0308027-14 Cl6-BZ#151 0.277 J µg/Kg 0.140 µg/Kg9/14/2001 8-20-091401 614814 4783340 8 0308027-14 Cl6-BZ#153 21.2 µg/Kg 0.120 µg/Kg9/14/2001 8-20-091401 614814 4783340 8 0308027-14 Cl6-BZ#156 1.81 µg/Kg 0.0856 µg/Kg9/14/2001 8-20-091401 614814 4783340 8 0308027-14 Cl6-BZ#157 0.389 µg/Kg 0.0672 µg/Kg9/14/2001 8-20-091401 614814 4783340 8 0308027-14 Cl6-BZ#158 0.362 µg/Kg 0.0567 µg/Kg9/14/2001 8-20-091401 614814 4783340 8 0308027-14 Cl6-BZ#167 1.01 µg/Kg 0.0725 µg/Kg9/14/2001 8-20-091401 614814 4783340 8 0308027-14 Cl6-BZ#169 0.233 U µg/Kg 0.233 µg/Kg9/14/2001 8-20-091401 614814 4783340 8 0308027-14 Cl7-BZ#170 4.25 µg/Kg 0.271 µg/Kg



Extracted 7/30/04




SITE NUMBER



9/14/2001 8-20-091401 614814 4783340 8 0308027-14 Cl7-BZ#174 0.171 J µg/Kg 0.0553 µg/Kg9/14/2001 8-20-091401 614814 4783340 8 0308027-14 Cl7-BZ#177 0.474 µg/Kg 0.0777 µg/Kg9/14/2001 8-20-091401 614814 4783340 8 0308027-14 Cl7-BZ#180 5.31 J µg/Kg 0.116 µg/Kg9/14/2001 8-20-091401 614814 4783340 8 0308027-14 Cl7-BZ#183 0.902 µg/Kg 0.0527 µg/Kg9/14/2001 8-20-091401 614814 4783340 8 0308027-14 Cl7-BZ#187 2.04 µg/Kg 0.0580 µg/Kg9/14/2001 8-20-091401 614814 4783340 8 0308027-14 Cl7-BZ#189 0.104 U µg/Kg 0.104 µg/Kg9/14/2001 8-20-091401 614814 4783340 8 0308027-14 Cl8-BZ#194 0.121 U µg/Kg 0.121 µg/Kg9/14/2001 8-20-091401 614814 4783340 8 0308027-14 Cl8-BZ#195 0.454 J µg/Kg 0.120 µg/Kg9/14/2001 8-20-091401 614814 4783340 8 0308027-14 Cl8-BZ#201 0.474 J µg/Kg 0.105 µg/Kg9/14/2001 8-20-091401 614814 4783340 8 0308027-14 Cl9-BZ#206 1.11 µg/Kg 0.141 µg/Kg9/14/2001 8-20-091401 614814 4783340 8 0308027-14 Cl10-BZ#209 0.277 J µg/Kg 0.0659 µg/Kg9/14/2001 8-20-091401 614814 4783340 8 0308027-14 Monochlorobiphenyls 3.87 U µg/Kg 3.87 µg/Kg9/14/2001 8-20-091401 614814 4783340 8 0308027-14 Dichlorobiphenyls 0.283 J µg/Kg 0.113 µg/Kg9/14/2001 8-20-091401 614814 4783340 8 0308027-14 Trichlorobiphenyls 5.24 µg/Kg 0.389 µg/Kg9/14/2001 8-20-091401 614814 4783340 8 0308027-14 Tetrachlorobiphenyls 35.7 µg/Kg 0.0606 µg/Kg9/14/2001 8-20-091401 614814 4783340 8 0308027-14 Pentachlorobiphenyls 72.9 µg/Kg 0.0698 µg/Kg9/14/2001 8-20-091401 614814 4783340 8 0308027-14 Hexachlorobiphenyls 57.4 µg/Kg 0.111 µg/Kg9/14/2001 8-20-091401 614814 4783340 8 0308027-14 Heptachlorobiphenyls 25.0 µg/Kg 0.0606 µg/Kg9/14/2001 8-20-091401 614814 4783340 8 0308027-14 Octachlorobiphenyls 5.46 µg/Kg 0.0553 µg/Kg9/14/2001 8-20-091401 614814 4783340 8 0308027-14 Nonachlorobiphenyls 1.14 µg/Kg 0.141 µg/Kg9/14/2001 8-20-091401 614814 4783340 8 0308027-14 Decachlorobiphenyl 0.277 J µg/Kg 0.0659 µg/Kg9/14/2001 8-20-091401 614814 4783340 8 0308027-14 Total Homologs 204 µg/Kg 0.0659 µg/Kg9/14/2001 8-20-091401 614814 4783340 8 0308027-14 Percent Lipids 3.5 % 0.1 %9/14/2001 8-20-091401 614814 4783340 8 0308027-14 Percent Moisture 75.5 % 0.1 %9/15/2001 8-23-091501 614814 4783340 8 0308027-15 Cl2-BZ#8 0.122 U µg/Kg 0.122 µg/Kg9/15/2001 8-23-091501 614814 4783340 8 0308027-15 Cl3-BZ#18 0.574 J µg/Kg 0.271 µg/Kg9/15/2001 8-23-091501 614814 4783340 8 0308027-15 Cl3-BZ#31/#28 220 µg/Kg 1.95 µg/Kg9/15/2001 8-23-091501 614814 4783340 8 0308027-15 Cl4-BZ#44 65.6 µg/Kg 0.186 µg/Kg9/15/2001 8-23-091501 614814 4783340 8 0308027-15 Cl4-BZ#45 1.93 µg/Kg 0.248 µg/Kg9/15/2001 8-23-091501 614814 4783340 8 0308027-15 Cl4-BZ#47 1350 µg/Kg 1.83 µg/Kg9/15/2001 8-23-091501 614814 4783340 8 0308027-15 Cl4-BZ#49 81.8 µg/Kg 0.154 µg/Kg9/15/2001 8-23-091501 614814 4783340 8 0308027-15 Cl4-BZ#52 493 µg/Kg 1.02 µg/Kg9/15/2001 8-23-091501 614814 4783340 8 0308027-15 Cl4-BZ#56 216 µg/Kg 0.0921 µg/Kg9/15/2001 8-23-091501 614814 4783340 8 0308027-15 Cl4-BZ#66 331 µg/Kg 0.123 µg/Kg



Extracted 7/30/04




SITE NUMBER



9/15/2001 8-23-091501 614814 4783340 8 0308027-15 Cl4-BZ#70 131 µg/Kg 0.108 µg/Kg9/15/2001 8-23-091501 614814 4783340 8 0308027-15 Cl4-BZ#74 978 J µg/Kg 1.10 µg/Kg9/15/2001 8-23-091501 614814 4783340 8 0308027-15 Cl4-BZ#77 0.170 U µg/Kg 0.170 µg/Kg9/15/2001 8-23-091501 614814 4783340 8 0308027-15 Cl4-BZ#81 0.169 U µg/Kg 0.169 µg/Kg9/15/2001 8-23-091501 614814 4783340 8 0308027-15 Cl5-BZ#87 451 µg/Kg 0.436 µg/Kg9/15/2001 8-23-091501 614814 4783340 8 0308027-15 Cl5-BZ#95 47.9 µg/Kg 0.0581 µg/Kg9/15/2001 8-23-091501 614814 4783340 8 0308027-15 Cl5-BZ#99 1250 µg/Kg 0.230 µg/Kg9/15/2001 8-23-091501 614814 4783340 8 0308027-15 Cl5-BZ#101 257 µg/Kg 0.113 µg/Kg9/15/2001 8-23-091501 614814 4783340 8 0308027-15 Cl5-BZ#105 598 µg/Kg 0.321 µg/Kg9/15/2001 8-23-091501 614814 4783340 8 0308027-15 Cl5-BZ#110 295 µg/Kg 0.108 µg/Kg9/15/2001 8-23-091501 614814 4783340 8 0308027-15 Cl5-BZ#114 54.4 µg/Kg 0.0496 µg/Kg9/15/2001 8-23-091501 614814 4783340 8 0308027-15 Cl5-BZ#118 1550 µg/Kg 0.675 µg/Kg9/15/2001 8-23-091501 614814 4783340 8 0308027-15 Cl5-BZ#123 0.0978 U µg/Kg 0.0978 µg/Kg9/15/2001 8-23-091501 614814 4783340 8 0308027-15 Cl5-BZ#126 2.37 NJ µg/Kg 0.0864 µg/Kg9/15/2001 8-23-091501 614814 4783340 8 0308027-15 Cl6-BZ#128 149 µg/Kg 0.0779 µg/Kg9/15/2001 8-23-091501 614814 4783340 8 0308027-15 Cl6-BZ#138 1480 J µg/Kg 0.650 µg/Kg9/15/2001 8-23-091501 614814 4783340 8 0308027-15 Cl6-BZ#146 210 µg/Kg 0.0708 µg/Kg9/15/2001 8-23-091501 614814 4783340 8 0308027-15 Cl6-BZ#149 131 µg/Kg 0.0907 µg/Kg9/15/2001 8-23-091501 614814 4783340 8 0308027-15 Cl6-BZ#151 23.4 µg/Kg 0.150 µg/Kg9/15/2001 8-23-091501 614814 4783340 8 0308027-15 Cl6-BZ#153 1170 µg/Kg 0.749 µg/Kg9/15/2001 8-23-091501 614814 4783340 8 0308027-15 Cl6-BZ#156 140 µg/Kg 0.0921 µg/Kg9/15/2001 8-23-091501 614814 4783340 8 0308027-15 Cl6-BZ#157 22.8 µg/Kg 0.0723 µg/Kg9/15/2001 8-23-091501 614814 4783340 8 0308027-15 Cl6-BZ#158 46.9 µg/Kg 0.0609 µg/Kg9/15/2001 8-23-091501 614814 4783340 8 0308027-15 Cl6-BZ#167 51.6 µg/Kg 0.0779 µg/Kg9/15/2001 8-23-091501 614814 4783340 8 0308027-15 Cl6-BZ#169 0.251 U µg/Kg 0.251 µg/Kg9/15/2001 8-23-091501 614814 4783340 8 0308027-15 Cl7-BZ#170 166 µg/Kg 0.292 µg/Kg9/15/2001 8-23-091501 614814 4783340 8 0308027-15 Cl7-BZ#174 14.5 µg/Kg 0.0595 µg/Kg9/15/2001 8-23-091501 614814 4783340 8 0308027-15 Cl7-BZ#177 67.5 µg/Kg 0.0836 µg/Kg9/15/2001 8-23-091501 614814 4783340 8 0308027-15 Cl7-BZ#180 353 J µg/Kg 0.125 µg/Kg9/15/2001 8-23-091501 614814 4783340 8 0308027-15 Cl7-BZ#183 77.8 µg/Kg 0.0567 µg/Kg9/15/2001 8-23-091501 614814 4783340 8 0308027-15 Cl7-BZ#187 484 µg/Kg 0.362 µg/Kg9/15/2001 8-23-091501 614814 4783340 8 0308027-15 Cl7-BZ#189 0.112 U µg/Kg 0.112 µg/Kg9/15/2001 8-23-091501 614814 4783340 8 0308027-15 Cl8-BZ#194 24.0 µg/Kg 0.130 µg/Kg9/15/2001 8-23-091501 614814 4783340 8 0308027-15 Cl8-BZ#195 13.1 µg/Kg 0.129 µg/Kg



Extracted 7/30/04




SITE NUMBER



9/15/2001 8-23-091501 614814 4783340 8 0308027-15 Cl8-BZ#201 82.5 µg/Kg 0.113 µg/Kg9/15/2001 8-23-091501 614814 4783340 8 0308027-15 Cl9-BZ#206 16.6 µg/Kg 0.152 µg/Kg9/15/2001 8-23-091501 614814 4783340 8 0308027-15 Cl10-BZ#209 1.63 µg/Kg 0.0708 µg/Kg9/15/2001 8-23-091501 614814 4783340 8 0308027-15 Monochlorobiphenyls 4.17 U µg/Kg 4.17 µg/Kg9/15/2001 8-23-091501 614814 4783340 8 0308027-15 Dichlorobiphenyls 2.98 µg/Kg 0.122 µg/Kg9/15/2001 8-23-091501 614814 4783340 8 0308027-15 Trichlorobiphenyls 269 µg/Kg 0.418 µg/Kg9/15/2001 8-23-091501 614814 4783340 8 0308027-15 Tetrachlorobiphenyls 4390 µg/Kg 0.379 µg/Kg9/15/2001 8-23-091501 614814 4783340 8 0308027-15 Pentachlorobiphenyls 7650 µg/Kg 0.436 µg/Kg9/15/2001 8-23-091501 614814 4783340 8 0308027-15 Hexachlorobiphenyls 3990 µg/Kg 0.691 µg/Kg9/15/2001 8-23-091501 614814 4783340 8 0308027-15 Heptachlorobiphenyls 1160 µg/Kg 0.379 µg/Kg9/15/2001 8-23-091501 614814 4783340 8 0308027-15 Octachlorobiphenyls 162 µg/Kg 0.0595 µg/Kg9/15/2001 8-23-091501 614814 4783340 8 0308027-15 Nonachlorobiphenyls 27.5 µg/Kg 0.152 µg/Kg9/15/2001 8-23-091501 614814 4783340 8 0308027-15 Decachlorobiphenyl 1.63 µg/Kg 0.0708 µg/Kg9/15/2001 8-23-091501 614814 4783340 8 0308027-15 Total Homologs 17800 µg/Kg 0.412 µg/Kg9/15/2001 8-23-091501 614814 4783340 8 0308027-15 Percent Lipids 2.8 % 0.1 %9/15/2001 8-23-091501 614814 4783340 8 0308027-15 Percent Moisture 72.0 % 0.1 %9/22/2001 13-03-092201 611801 4757967 13 0308028-01 Cl2-BZ#8 0.0872 U µg/Kg 0.0872 µg/Kg9/22/2001 13-03-092201 611801 4757967 13 0308028-01 Cl3-BZ#18 0.194 U µg/Kg 0.194 µg/Kg9/22/2001 13-03-092201 611801 4757967 13 0308028-01 Cl3-BZ#31/#28 6.08 J µg/Kg 1.40 µg/Kg9/22/2001 13-03-092201 611801 4757967 13 0308028-01 Cl4-BZ#44 0.264 J µg/Kg 0.133 µg/Kg9/22/2001 13-03-092201 611801 4757967 13 0308028-01 Cl4-BZ#45 0.679 J µg/Kg 0.177 µg/Kg9/22/2001 13-03-092201 611801 4757967 13 0308028-01 Cl4-BZ#47 5.39 µg/Kg 0.225 µg/Kg9/22/2001 13-03-092201 611801 4757967 13 0308028-01 Cl4-BZ#49 0.314 J µg/Kg 0.111 µg/Kg9/22/2001 13-03-092201 611801 4757967 13 0308028-01 Cl4-BZ#52 0.466 J µg/Kg 0.126 µg/Kg9/22/2001 13-03-092201 611801 4757967 13 0308028-01 Cl4-BZ#56 4.22 µg/Kg 0.0659 µg/Kg9/22/2001 13-03-092201 611801 4757967 13 0308028-01 Cl4-BZ#66 12.7 µg/Kg 0.0882 µg/Kg9/22/2001 13-03-092201 611801 4757967 13 0308028-01 Cl4-BZ#70 1.37 µg/Kg 0.0770 µg/Kg9/22/2001 13-03-092201 611801 4757967 13 0308028-01 Cl4-BZ#74 14.4 µg/Kg 0.136 µg/Kg9/22/2001 13-03-092201 611801 4757967 13 0308028-01 Cl4-BZ#77 0.122 U µg/Kg 0.122 µg/Kg9/22/2001 13-03-092201 611801 4757967 13 0308028-01 Cl4-BZ#81 0.121 U µg/Kg 0.121 µg/Kg9/22/2001 13-03-092201 611801 4757967 13 0308028-01 Cl5-BZ#87 3.92 µg/Kg 0.0537 µg/Kg9/22/2001 13-03-092201 611801 4757967 13 0308028-01 Cl5-BZ#95 0.152 J µg/Kg 0.0416 µg/Kg9/22/2001 13-03-092201 611801 4757967 13 0308028-01 Cl5-BZ#99 18.7 µg/Kg 0.0284 µg/Kg9/22/2001 13-03-092201 611801 4757967 13 0308028-01 Cl5-BZ#101 0.846 µg/Kg 0.0811 µg/Kg



Extracted 7/30/04




SITE NUMBER



9/22/2001 13-03-092201 611801 4757967 13 0308028-01 Cl5-BZ#105 11.2 µg/Kg 0.0395 µg/Kg9/22/2001 13-03-092201 611801 4757967 13 0308028-01 Cl5-BZ#110 0.0770 U µg/Kg 0.0770 µg/Kg9/22/2001 13-03-092201 611801 4757967 13 0308028-01 Cl5-BZ#114 1.06 µg/Kg 0.0355 µg/Kg9/22/2001 13-03-092201 611801 4757967 13 0308028-01 Cl5-BZ#118 38.8 µg/Kg 0.0831 µg/Kg9/22/2001 13-03-092201 611801 4757967 13 0308028-01 Cl5-BZ#123 0.0699 U µg/Kg 0.0699 µg/Kg9/22/2001 13-03-092201 611801 4757967 13 0308028-01 Cl5-BZ#126 0.491 NJ µg/Kg 0.0618 µg/Kg9/22/2001 13-03-092201 611801 4757967 13 0308028-01 Cl6-BZ#128 2.85 µg/Kg 0.0557 µg/Kg9/22/2001 13-03-092201 611801 4757967 13 0308028-01 Cl6-BZ#138 31.9 µg/Kg 0.0801 µg/Kg9/22/2001 13-03-092201 611801 4757967 13 0308028-01 Cl6-BZ#146 3.25 µg/Kg 0.0507 µg/Kg9/22/2001 13-03-092201 611801 4757967 13 0308028-01 Cl6-BZ#149 0.334 µg/Kg 0.0649 µg/Kg9/22/2001 13-03-092201 611801 4757967 13 0308028-01 Cl6-BZ#151 0.122 J µg/Kg 0.107 µg/Kg9/22/2001 13-03-092201 611801 4757967 13 0308028-01 Cl6-BZ#153 54.4 µg/Kg 0.0922 µg/Kg9/22/2001 13-03-092201 611801 4757967 13 0308028-01 Cl6-BZ#156 3.46 µg/Kg 0.0659 µg/Kg9/22/2001 13-03-092201 611801 4757967 13 0308028-01 Cl6-BZ#157 0.730 µg/Kg 0.0517 µg/Kg9/22/2001 13-03-092201 611801 4757967 13 0308028-01 Cl6-BZ#158 0.613 µg/Kg 0.0436 µg/Kg9/22/2001 13-03-092201 611801 4757967 13 0308028-01 Cl6-BZ#167 4.04 µg/Kg 0.0557 µg/Kg9/22/2001 13-03-092201 611801 4757967 13 0308028-01 Cl6-BZ#169 0.179 U µg/Kg 0.179 µg/Kg9/22/2001 13-03-092201 611801 4757967 13 0308028-01 Cl7-BZ#170 0.209 U µg/Kg 0.209 µg/Kg9/22/2001 13-03-092201 611801 4757967 13 0308028-01 Cl7-BZ#174 0.0426 U µg/Kg 0.0426 µg/Kg9/22/2001 13-03-092201 611801 4757967 13 0308028-01 Cl7-BZ#177 0.0598 U µg/Kg 0.0598 µg/Kg9/22/2001 13-03-092201 611801 4757967 13 0308028-01 Cl7-BZ#180 7.06 µg/Kg 0.0892 µg/Kg9/22/2001 13-03-092201 611801 4757967 13 0308028-01 Cl7-BZ#183 1.32 µg/Kg 0.0405 µg/Kg9/22/2001 13-03-092201 611801 4757967 13 0308028-01 Cl7-BZ#187 1.95 µg/Kg 0.0446 µg/Kg9/22/2001 13-03-092201 611801 4757967 13 0308028-01 Cl7-BZ#189 0.0801 U µg/Kg 0.0801 µg/Kg9/22/2001 13-03-092201 611801 4757967 13 0308028-01 Cl8-BZ#194 1.04 µg/Kg 0.0932 µg/Kg9/22/2001 13-03-092201 611801 4757967 13 0308028-01 Cl8-BZ#195 0.415 J µg/Kg 0.0922 µg/Kg9/22/2001 13-03-092201 611801 4757967 13 0308028-01 Cl8-BZ#201 0.720 µg/Kg 0.0811 µg/Kg9/22/2001 13-03-092201 611801 4757967 13 0308028-01 Cl9-BZ#206 1.21 µg/Kg 0.108 µg/Kg9/22/2001 13-03-092201 611801 4757967 13 0308028-01 Cl10-BZ#209 0.198 J µg/Kg 0.0507 µg/Kg9/22/2001 13-03-092201 611801 4757967 13 0308028-01 Monochlorobiphenyls 2.98 U µg/Kg 2.98 µg/Kg9/22/2001 13-03-092201 611801 4757967 13 0308028-01 Dichlorobiphenyls 0.0872 U µg/Kg 0.0872 µg/Kg9/22/2001 13-03-092201 611801 4757967 13 0308028-01 Trichlorobiphenyls 6.04 µg/Kg 0.299 µg/Kg9/22/2001 13-03-092201 611801 4757967 13 0308028-01 Tetrachlorobiphenyls 48.3 µg/Kg 0.0466 µg/Kg9/22/2001 13-03-092201 611801 4757967 13 0308028-01 Pentachlorobiphenyls 121 µg/Kg 0.0537 µg/Kg



Extracted 7/30/04




SITE NUMBER



9/22/2001 13-03-092201 611801 4757967 13 0308028-01 Hexachlorobiphenyls 110 µg/Kg 0.0851 µg/Kg9/22/2001 13-03-092201 611801 4757967 13 0308028-01 Heptachlorobiphenyls 2.95 µg/Kg 0.0466 µg/Kg9/22/2001 13-03-092201 611801 4757967 13 0308028-01 Octachlorobiphenyls 12.3 µg/Kg 0.0426 µg/Kg9/22/2001 13-03-092201 611801 4757967 13 0308028-01 Nonachlorobiphenyls 2.26 µg/Kg 0.108 µg/Kg9/22/2001 13-03-092201 611801 4757967 13 0308028-01 Decachlorobiphenyl 0.198 J µg/Kg 0.0507 µg/Kg9/22/2001 13-03-092201 611801 4757967 13 0308028-01 Total Homologs 303 µg/Kg 0.0507 µg/Kg9/22/2001 13-03-092201 611801 4757967 13 0308028-01 Percent Lipids 2.6 % 0.1 %9/22/2001 13-03-092201 611801 4757967 13 0308028-01 Percent Moisture 71.3 % 0.1 %9/22/2001 13-06-092201 611801 4757967 13 0308028-02 Cl2-BZ#8 0.116 U µg/Kg 0.116 µg/Kg9/22/2001 13-06-092201 611801 4757967 13 0308028-02 Cl3-BZ#18 0.257 U µg/Kg 0.257 µg/Kg9/22/2001 13-06-092201 611801 4757967 13 0308028-02 Cl3-BZ#31/#28 2.44 J µg/Kg 1.85 µg/Kg9/22/2001 13-06-092201 611801 4757967 13 0308028-02 Cl4-BZ#44 0.176 U µg/Kg 0.176 µg/Kg9/22/2001 13-06-092201 611801 4757967 13 0308028-02 Cl4-BZ#45 0.471 J µg/Kg 0.235 µg/Kg9/22/2001 13-06-092201 611801 4757967 13 0308028-02 Cl4-BZ#47 0.303 J µg/Kg 0.299 µg/Kg9/22/2001 13-06-092201 611801 4757967 13 0308028-02 Cl4-BZ#49 0.242 J µg/Kg 0.147 µg/Kg9/22/2001 13-06-092201 611801 4757967 13 0308028-02 Cl4-BZ#52 0.167 U µg/Kg 0.167 µg/Kg9/22/2001 13-06-092201 611801 4757967 13 0308028-02 Cl4-BZ#56 1.10 µg/Kg 0.0874 µg/Kg9/22/2001 13-06-092201 611801 4757967 13 0308028-02 Cl4-BZ#66 2.49 µg/Kg 0.117 µg/Kg9/22/2001 13-06-092201 611801 4757967 13 0308028-02 Cl4-BZ#70 0.222 J µg/Kg 0.102 µg/Kg9/22/2001 13-06-092201 611801 4757967 13 0308028-02 Cl4-BZ#74 4.93 µg/Kg 0.180 µg/Kg9/22/2001 13-06-092201 611801 4757967 13 0308028-02 Cl4-BZ#77 0.161 U µg/Kg 0.161 µg/Kg9/22/2001 13-06-092201 611801 4757967 13 0308028-02 Cl4-BZ#81 0.160 U µg/Kg 0.160 µg/Kg9/22/2001 13-06-092201 611801 4757967 13 0308028-02 Cl5-BZ#87 1.26 µg/Kg 0.0713 µg/Kg9/22/2001 13-06-092201 611801 4757967 13 0308028-02 Cl5-BZ#95 0.0551 U µg/Kg 0.0551 µg/Kg9/22/2001 13-06-092201 611801 4757967 13 0308028-02 Cl5-BZ#99 5.05 µg/Kg 0.0377 µg/Kg9/22/2001 13-06-092201 611801 4757967 13 0308028-02 Cl5-BZ#101 0.249 J µg/Kg 0.108 µg/Kg9/22/2001 13-06-092201 611801 4757967 13 0308028-02 Cl5-BZ#105 4.11 µg/Kg 0.0524 µg/Kg9/22/2001 13-06-092201 611801 4757967 13 0308028-02 Cl5-BZ#110 0.102 U µg/Kg 0.102 µg/Kg9/22/2001 13-06-092201 611801 4757967 13 0308028-02 Cl5-BZ#114 0.0471 U µg/Kg 0.0471 µg/Kg9/22/2001 13-06-092201 611801 4757967 13 0308028-02 Cl5-BZ#118 9.43 µg/Kg 0.110 µg/Kg9/22/2001 13-06-092201 611801 4757967 13 0308028-02 Cl5-BZ#123 0.0928 U µg/Kg 0.0928 µg/Kg9/22/2001 13-06-092201 611801 4757967 13 0308028-02 Cl5-BZ#126 0.0820 U µg/Kg 0.0820 µg/Kg9/22/2001 13-06-092201 611801 4757967 13 0308028-02 Cl6-BZ#128 0.558 µg/Kg 0.0740 µg/Kg9/22/2001 13-06-092201 611801 4757967 13 0308028-02 Cl6-BZ#138 14.4 µg/Kg 0.106 µg/Kg



Extracted 7/30/04




SITE NUMBER



9/22/2001 13-06-092201 611801 4757967 13 0308028-02 Cl6-BZ#146 1.34 µg/Kg 0.0672 µg/Kg9/22/2001 13-06-092201 611801 4757967 13 0308028-02 Cl6-BZ#149 0.0861 U µg/Kg 0.0861 µg/Kg9/22/2001 13-06-092201 611801 4757967 13 0308028-02 Cl6-BZ#151 0.262 J µg/Kg 0.142 µg/Kg9/22/2001 13-06-092201 611801 4757967 13 0308028-02 Cl6-BZ#153 14.1 µg/Kg 0.122 µg/Kg9/22/2001 13-06-092201 611801 4757967 13 0308028-02 Cl6-BZ#156 1.20 µg/Kg 0.0874 µg/Kg9/22/2001 13-06-092201 611801 4757967 13 0308028-02 Cl6-BZ#157 0.262 J µg/Kg 0.0686 µg/Kg9/22/2001 13-06-092201 611801 4757967 13 0308028-02 Cl6-BZ#158 0.0578 U µg/Kg 0.0578 µg/Kg9/22/2001 13-06-092201 611801 4757967 13 0308028-02 Cl6-BZ#167 0.551 µg/Kg 0.0740 µg/Kg9/22/2001 13-06-092201 611801 4757967 13 0308028-02 Cl6-BZ#169 0.238 U µg/Kg 0.238 µg/Kg9/22/2001 13-06-092201 611801 4757967 13 0308028-02 Cl7-BZ#170 0.277 U µg/Kg 0.277 µg/Kg9/22/2001 13-06-092201 611801 4757967 13 0308028-02 Cl7-BZ#174 0.0565 U µg/Kg 0.0565 µg/Kg9/22/2001 13-06-092201 611801 4757967 13 0308028-02 Cl7-BZ#177 0.0793 U µg/Kg 0.0793 µg/Kg9/22/2001 13-06-092201 611801 4757967 13 0308028-02 Cl7-BZ#180 2.25 µg/Kg 0.118 µg/Kg9/22/2001 13-06-092201 611801 4757967 13 0308028-02 Cl7-BZ#183 0.417 µg/Kg 0.0538 µg/Kg9/22/2001 13-06-092201 611801 4757967 13 0308028-02 Cl7-BZ#187 1.28 µg/Kg 0.0592 µg/Kg9/22/2001 13-06-092201 611801 4757967 13 0308028-02 Cl7-BZ#189 0.106 U µg/Kg 0.106 µg/Kg9/22/2001 13-06-092201 611801 4757967 13 0308028-02 Cl8-BZ#194 0.124 U µg/Kg 0.124 µg/Kg9/22/2001 13-06-092201 611801 4757967 13 0308028-02 Cl8-BZ#195 0.430 J µg/Kg 0.122 µg/Kg9/22/2001 13-06-092201 611801 4757967 13 0308028-02 Cl8-BZ#201 0.262 J µg/Kg 0.108 µg/Kg9/22/2001 13-06-092201 611801 4757967 13 0308028-02 Cl9-BZ#206 0.578 J µg/Kg 0.144 µg/Kg9/22/2001 13-06-092201 611801 4757967 13 0308028-02 Cl10-BZ#209 0.161 J µg/Kg 0.0672 µg/Kg9/22/2001 13-06-092201 611801 4757967 13 0308028-02 Monochlorobiphenyls 3.95 U µg/Kg 3.95 µg/Kg9/22/2001 13-06-092201 611801 4757967 13 0308028-02 Dichlorobiphenyls 0.116 U µg/Kg 0.116 µg/Kg9/22/2001 13-06-092201 611801 4757967 13 0308028-02 Trichlorobiphenyls 2.42 µg/Kg 0.397 µg/Kg9/22/2001 13-06-092201 611801 4757967 13 0308028-02 Tetrachlorobiphenyls 20.3 µg/Kg 0.0619 µg/Kg9/22/2001 13-06-092201 611801 4757967 13 0308028-02 Pentachlorobiphenyls 34.1 µg/Kg 0.0713 µg/Kg9/22/2001 13-06-092201 611801 4757967 13 0308028-02 Hexachlorobiphenyls 35.1 µg/Kg 0.113 µg/Kg9/22/2001 13-06-092201 611801 4757967 13 0308028-02 Heptachlorobiphenyls 1.36 µg/Kg 0.0619 µg/Kg9/22/2001 13-06-092201 611801 4757967 13 0308028-02 Octachlorobiphenyls 2.61 µg/Kg 0.0565 µg/Kg9/22/2001 13-06-092201 611801 4757967 13 0308028-02 Nonachlorobiphenyls 0.578 J µg/Kg 0.144 µg/Kg9/22/2001 13-06-092201 611801 4757967 13 0308028-02 Decachlorobiphenyl 0.161 J µg/Kg 0.0672 µg/Kg9/22/2001 13-06-092201 611801 4757967 13 0308028-02 Total Homologs 96.6 µg/Kg 0.0672 µg/Kg9/22/2001 13-06-092201 611801 4757967 13 0308028-02 Percent Lipids 2.1 % 0.1 %9/22/2001 13-06-092201 611801 4757967 13 0308028-02 Percent Moisture 74.8 % 0.1 %



Extracted 7/30/04




SITE NUMBER



9/23/2001 13-08-092301 611801 4757967 13 0308028-03 Cl2-BZ#8 0.127 U µg/Kg 0.127 µg/Kg9/23/2001 13-08-092301 611801 4757967 13 0308028-03 Cl3-BZ#18 0.281 U µg/Kg 0.281 µg/Kg9/23/2001 13-08-092301 611801 4757967 13 0308028-03 Cl3-BZ#31/#28 5.83 J µg/Kg 2.03 µg/Kg9/23/2001 13-08-092301 611801 4757967 13 0308028-03 Cl4-BZ#44 0.193 U µg/Kg 0.193 µg/Kg9/23/2001 13-08-092301 611801 4757967 13 0308028-03 Cl4-BZ#45 1.22 J µg/Kg 0.258 µg/Kg9/23/2001 13-08-092301 611801 4757967 13 0308028-03 Cl4-BZ#47 0.817 J µg/Kg 0.327 µg/Kg9/23/2001 13-08-092301 611801 4757967 13 0308028-03 Cl4-BZ#49 0.161 U µg/Kg 0.161 µg/Kg9/23/2001 13-08-092301 611801 4757967 13 0308028-03 Cl4-BZ#52 0.287 J µg/Kg 0.183 µg/Kg9/23/2001 13-08-092301 611801 4757967 13 0308028-03 Cl4-BZ#56 0.641 µg/Kg 0.0957 µg/Kg9/23/2001 13-08-092301 611801 4757967 13 0308028-03 Cl4-BZ#66 1.19 µg/Kg 0.128 µg/Kg9/23/2001 13-08-092301 611801 4757967 13 0308028-03 Cl4-BZ#70 0.479 J µg/Kg 0.112 µg/Kg9/23/2001 13-08-092301 611801 4757967 13 0308028-03 Cl4-BZ#74 0.979 J µg/Kg 0.197 µg/Kg9/23/2001 13-08-092301 611801 4757967 13 0308028-03 Cl4-BZ#77 0.177 U µg/Kg 0.177 µg/Kg9/23/2001 13-08-092301 611801 4757967 13 0308028-03 Cl4-BZ#81 0.175 U µg/Kg 0.175 µg/Kg9/23/2001 13-08-092301 611801 4757967 13 0308028-03 Cl5-BZ#87 0.655 µg/Kg 0.0781 µg/Kg9/23/2001 13-08-092301 611801 4757967 13 0308028-03 Cl5-BZ#95 0.0810 J µg/Kg 0.0604 µg/Kg9/23/2001 13-08-092301 611801 4757967 13 0308028-03 Cl5-BZ#99 1.58 µg/Kg 0.0412 µg/Kg9/23/2001 13-08-092301 611801 4757967 13 0308028-03 Cl5-BZ#101 0.206 J µg/Kg 0.118 µg/Kg9/23/2001 13-08-092301 611801 4757967 13 0308028-03 Cl5-BZ#105 1.50 µg/Kg 0.0574 µg/Kg9/23/2001 13-08-092301 611801 4757967 13 0308028-03 Cl5-BZ#110 0.112 U µg/Kg 0.112 µg/Kg9/23/2001 13-08-092301 611801 4757967 13 0308028-03 Cl5-BZ#114 0.0516 U µg/Kg 0.0516 µg/Kg9/23/2001 13-08-092301 611801 4757967 13 0308028-03 Cl5-BZ#118 3.01 µg/Kg 0.121 µg/Kg9/23/2001 13-08-092301 611801 4757967 13 0308028-03 Cl5-BZ#123 0.102 U µg/Kg 0.102 µg/Kg9/23/2001 13-08-092301 611801 4757967 13 0308028-03 Cl5-BZ#126 0.0898 U µg/Kg 0.0898 µg/Kg9/23/2001 13-08-092301 611801 4757967 13 0308028-03 Cl6-BZ#128 0.589 µg/Kg 0.0810 µg/Kg9/23/2001 13-08-092301 611801 4757967 13 0308028-03 Cl6-BZ#138 8.37 µg/Kg 0.116 µg/Kg9/23/2001 13-08-092301 611801 4757967 13 0308028-03 Cl6-BZ#146 0.751 µg/Kg 0.0736 µg/Kg9/23/2001 13-08-092301 611801 4757967 13 0308028-03 Cl6-BZ#149 0.103 J µg/Kg 0.0943 µg/Kg9/23/2001 13-08-092301 611801 4757967 13 0308028-03 Cl6-BZ#151 0.156 U µg/Kg 0.156 µg/Kg9/23/2001 13-08-092301 611801 4757967 13 0308028-03 Cl6-BZ#153 9.02 µg/Kg 0.134 µg/Kg9/23/2001 13-08-092301 611801 4757967 13 0308028-03 Cl6-BZ#156 0.825 µg/Kg 0.0957 µg/Kg9/23/2001 13-08-092301 611801 4757967 13 0308028-03 Cl6-BZ#157 0.184 J µg/Kg 0.0751 µg/Kg9/23/2001 13-08-092301 611801 4757967 13 0308028-03 Cl6-BZ#158 0.184 J µg/Kg 0.0633 µg/Kg9/23/2001 13-08-092301 611801 4757967 13 0308028-03 Cl6-BZ#167 0.405 J µg/Kg 0.0810 µg/Kg



Extracted 7/30/04




SITE NUMBER



9/23/2001 13-08-092301 611801 4757967 13 0308028-03 Cl6-BZ#169 0.261 U µg/Kg 0.261 µg/Kg9/23/2001 13-08-092301 611801 4757967 13 0308028-03 Cl7-BZ#170 0.303 U µg/Kg 0.303 µg/Kg9/23/2001 13-08-092301 611801 4757967 13 0308028-03 Cl7-BZ#174 0.0619 U µg/Kg 0.0619 µg/Kg9/23/2001 13-08-092301 611801 4757967 13 0308028-03 Cl7-BZ#177 0.0869 U µg/Kg 0.0869 µg/Kg9/23/2001 13-08-092301 611801 4757967 13 0308028-03 Cl7-BZ#180 4.04 µg/Kg 0.130 µg/Kg9/23/2001 13-08-092301 611801 4757967 13 0308028-03 Cl7-BZ#183 0.398 µg/Kg 0.0589 µg/Kg9/23/2001 13-08-092301 611801 4757967 13 0308028-03 Cl7-BZ#187 0.935 µg/Kg 0.0648 µg/Kg9/23/2001 13-08-092301 611801 4757967 13 0308028-03 Cl7-BZ#189 0.116 U µg/Kg 0.116 µg/Kg9/23/2001 13-08-092301 611801 4757967 13 0308028-03 Cl8-BZ#194 0.135 U µg/Kg 0.135 µg/Kg9/23/2001 13-08-092301 611801 4757967 13 0308028-03 Cl8-BZ#195 0.134 U µg/Kg 0.134 µg/Kg9/23/2001 13-08-092301 611801 4757967 13 0308028-03 Cl8-BZ#201 0.508 J µg/Kg 0.118 µg/Kg9/23/2001 13-08-092301 611801 4757967 13 0308028-03 Cl9-BZ#206 0.552 J µg/Kg 0.158 µg/Kg9/23/2001 13-08-092301 611801 4757967 13 0308028-03 Cl10-BZ#209 0.177 J µg/Kg 0.0736 µg/Kg9/23/2001 13-08-092301 611801 4757967 13 0308028-03 Monochlorobiphenyls 4.33 U µg/Kg 4.33 µg/Kg9/23/2001 13-08-092301 611801 4757967 13 0308028-03 Dichlorobiphenyls 0.127 U µg/Kg 0.127 µg/Kg9/23/2001 13-08-092301 611801 4757967 13 0308028-03 Trichlorobiphenyls 6.48 µg/Kg 0.435 µg/Kg9/23/2001 13-08-092301 611801 4757967 13 0308028-03 Tetrachlorobiphenyls 4.10 µg/Kg 0.0678 µg/Kg9/23/2001 13-08-092301 611801 4757967 13 0308028-03 Pentachlorobiphenyls 14.0 µg/Kg 0.0781 µg/Kg9/23/2001 13-08-092301 611801 4757967 13 0308028-03 Hexachlorobiphenyls 23.1 µg/Kg 0.124 µg/Kg9/23/2001 13-08-092301 611801 4757967 13 0308028-03 Heptachlorobiphenyls 1.24 µg/Kg 0.0678 µg/Kg9/23/2001 13-08-092301 611801 4757967 13 0308028-03 Octachlorobiphenyls 1.40 µg/Kg 0.0619 µg/Kg9/23/2001 13-08-092301 611801 4757967 13 0308028-03 Nonachlorobiphenyls 0.552 J µg/Kg 0.158 µg/Kg9/23/2001 13-08-092301 611801 4757967 13 0308028-03 Decachlorobiphenyl 0.177 J µg/Kg 0.0736 µg/Kg9/23/2001 13-08-092301 611801 4757967 13 0308028-03 Total Homologs 51.0 µg/Kg 0.0736 µg/Kg9/23/2001 13-08-092301 611801 4757967 13 0308028-03 Percent Lipids 3.6 % 0.1 %9/23/2001 13-08-092301 611801 4757967 13 0308028-03 Percent Moisture 70.9 % 0.1 %9/24/2001 13-12-092401 611801 4757967 13 0308028-04 Cl2-BZ#8 0.118 U µg/Kg 0.118 µg/Kg9/24/2001 13-12-092401 611801 4757967 13 0308028-04 Cl3-BZ#18 0.263 U µg/Kg 0.263 µg/Kg9/24/2001 13-12-092401 611801 4757967 13 0308028-04 Cl3-BZ#31/#28 96.6 µg/Kg 1.89 µg/Kg9/24/2001 13-12-092401 611801 4757967 13 0308028-04 Cl4-BZ#44 0.180 U µg/Kg 0.180 µg/Kg9/24/2001 13-12-092401 611801 4757967 13 0308028-04 Cl4-BZ#45 0.241 U µg/Kg 0.241 µg/Kg9/24/2001 13-12-092401 611801 4757967 13 0308028-04 Cl4-BZ#47 78.4 µg/Kg 0.305 µg/Kg9/24/2001 13-12-092401 611801 4757967 13 0308028-04 Cl4-BZ#49 1.58 µg/Kg 0.150 µg/Kg9/24/2001 13-12-092401 611801 4757967 13 0308028-04 Cl4-BZ#52 3.69 µg/Kg 0.171 µg/Kg



Extracted 7/30/04




SITE NUMBER



9/24/2001 13-12-092401 611801 4757967 13 0308028-04 Cl4-BZ#56 60.3 µg/Kg 0.0894 µg/Kg9/24/2001 13-12-092401 611801 4757967 13 0308028-04 Cl4-BZ#66 208 µg/Kg 0.120 µg/Kg9/24/2001 13-12-092401 611801 4757967 13 0308028-04 Cl4-BZ#70 66.6 µg/Kg 0.105 µg/Kg9/24/2001 13-12-092401 611801 4757967 13 0308028-04 Cl4-BZ#74 165 µg/Kg 0.184 µg/Kg9/24/2001 13-12-092401 611801 4757967 13 0308028-04 Cl4-BZ#77 0.165 U µg/Kg 0.165 µg/Kg9/24/2001 13-12-092401 611801 4757967 13 0308028-04 Cl4-BZ#81 0.164 U µg/Kg 0.164 µg/Kg9/24/2001 13-12-092401 611801 4757967 13 0308028-04 Cl5-BZ#87 51.9 µg/Kg 0.0729 µg/Kg9/24/2001 13-12-092401 611801 4757967 13 0308028-04 Cl5-BZ#95 0.0564 U µg/Kg 0.0564 µg/Kg9/24/2001 13-12-092401 611801 4757967 13 0308028-04 Cl5-BZ#99 202 µg/Kg 0.0385 µg/Kg9/24/2001 13-12-092401 611801 4757967 13 0308028-04 Cl5-BZ#101 17.6 µg/Kg 0.110 µg/Kg9/24/2001 13-12-092401 611801 4757967 13 0308028-04 Cl5-BZ#105 109 µg/Kg 0.0536 µg/Kg9/24/2001 13-12-092401 611801 4757967 13 0308028-04 Cl5-BZ#110 6.25 µg/Kg 0.105 µg/Kg9/24/2001 13-12-092401 611801 4757967 13 0308028-04 Cl5-BZ#114 8.79 µg/Kg 0.0481 µg/Kg9/24/2001 13-12-092401 611801 4757967 13 0308028-04 Cl5-BZ#118 259 µg/Kg 0.113 µg/Kg9/24/2001 13-12-092401 611801 4757967 13 0308028-04 Cl5-BZ#123 0.0949 U µg/Kg 0.0949 µg/Kg9/24/2001 13-12-092401 611801 4757967 13 0308028-04 Cl5-BZ#126 0.406 NJ µg/Kg 0.0839 µg/Kg9/24/2001 13-12-092401 611801 4757967 13 0308028-04 Cl6-BZ#128 23.5 µg/Kg 0.0757 µg/Kg9/24/2001 13-12-092401 611801 4757967 13 0308028-04 Cl6-BZ#138 289 µg/Kg 0.109 µg/Kg9/24/2001 13-12-092401 611801 4757967 13 0308028-04 Cl6-BZ#146 35.0 µg/Kg 0.0688 µg/Kg9/24/2001 13-12-092401 611801 4757967 13 0308028-04 Cl6-BZ#149 3.12 µg/Kg 0.0880 µg/Kg9/24/2001 13-12-092401 611801 4757967 13 0308028-04 Cl6-BZ#151 0.571 J µg/Kg 0.146 µg/Kg9/24/2001 13-12-092401 611801 4757967 13 0308028-04 Cl6-BZ#153 217 µg/Kg 0.125 µg/Kg9/24/2001 13-12-092401 611801 4757967 13 0308028-04 Cl6-BZ#156 18.1 µg/Kg 0.0894 µg/Kg9/24/2001 13-12-092401 611801 4757967 13 0308028-04 Cl6-BZ#157 3.00 µg/Kg 0.0702 µg/Kg9/24/2001 13-12-092401 611801 4757967 13 0308028-04 Cl6-BZ#158 6.35 µg/Kg 0.0592 µg/Kg9/24/2001 13-12-092401 611801 4757967 13 0308028-04 Cl6-BZ#167 10.4 µg/Kg 0.0757 µg/Kg9/24/2001 13-12-092401 611801 4757967 13 0308028-04 Cl6-BZ#169 0.243 U µg/Kg 0.243 µg/Kg9/24/2001 13-12-092401 611801 4757967 13 0308028-04 Cl7-BZ#170 33.4 µg/Kg 0.283 µg/Kg9/24/2001 13-12-092401 611801 4757967 13 0308028-04 Cl7-BZ#174 0.0578 U µg/Kg 0.0578 µg/Kg9/24/2001 13-12-092401 611801 4757967 13 0308028-04 Cl7-BZ#177 6.23 µg/Kg 0.0812 µg/Kg9/24/2001 13-12-092401 611801 4757967 13 0308028-04 Cl7-BZ#180 64.2 µg/Kg 0.121 µg/Kg9/24/2001 13-12-092401 611801 4757967 13 0308028-04 Cl7-BZ#183 11.4 µg/Kg 0.0550 µg/Kg9/24/2001 13-12-092401 611801 4757967 13 0308028-04 Cl7-BZ#187 38.0 µg/Kg 0.0605 µg/Kg9/24/2001 13-12-092401 611801 4757967 13 0308028-04 Cl7-BZ#189 0.109 U µg/Kg 0.109 µg/Kg



Extracted 7/30/04




SITE NUMBER



9/24/2001 13-12-092401 611801 4757967 13 0308028-04 Cl8-BZ#194 11.1 µg/Kg 0.127 µg/Kg9/24/2001 13-12-092401 611801 4757967 13 0308028-04 Cl8-BZ#195 4.95 µg/Kg 0.125 µg/Kg9/24/2001 13-12-092401 611801 4757967 13 0308028-04 Cl8-BZ#201 9.80 µg/Kg 0.110 µg/Kg9/24/2001 13-12-092401 611801 4757967 13 0308028-04 Cl9-BZ#206 22.4 µg/Kg 0.147 µg/Kg9/24/2001 13-12-092401 611801 4757967 13 0308028-04 Cl10-BZ#209 3.51 µg/Kg 0.0688 µg/Kg9/24/2001 13-12-092401 611801 4757967 13 0308028-04 Monochlorobiphenyls 4.04 U µg/Kg 4.04 µg/Kg9/24/2001 13-12-092401 611801 4757967 13 0308028-04 Dichlorobiphenyls 0.118 U µg/Kg 0.118 µg/Kg9/24/2001 13-12-092401 611801 4757967 13 0308028-04 Trichlorobiphenyls 89.3 µg/Kg 0.406 µg/Kg9/24/2001 13-12-092401 611801 4757967 13 0308028-04 Tetrachlorobiphenyls 672 µg/Kg 0.0633 µg/Kg9/24/2001 13-12-092401 611801 4757967 13 0308028-04 Pentachlorobiphenyls 1080 µg/Kg 0.0729 µg/Kg9/24/2001 13-12-092401 611801 4757967 13 0308028-04 Hexachlorobiphenyls 677 µg/Kg 0.116 µg/Kg9/24/2001 13-12-092401 611801 4757967 13 0308028-04 Heptachlorobiphenyls 152 µg/Kg 0.0633 µg/Kg9/24/2001 13-12-092401 611801 4757967 13 0308028-04 Octachlorobiphenyls 56.6 µg/Kg 0.0578 µg/Kg9/24/2001 13-12-092401 611801 4757967 13 0308028-04 Nonachlorobiphenyls 22.4 µg/Kg 0.147 µg/Kg9/24/2001 13-12-092401 611801 4757967 13 0308028-04 Decachlorobiphenyl 3.51 µg/Kg 0.0688 µg/Kg9/24/2001 13-12-092401 611801 4757967 13 0308028-04 Total Homologs 2760 µg/Kg 0.0688 µg/Kg9/24/2001 13-12-092401 611801 4757967 13 0308028-04 Percent Lipids 1.9 % 0.1 %9/24/2001 13-12-092401 611801 4757967 13 0308028-04 Percent Moisture 72.8 % 0.1 %9/26/2001 13-14-092601 611801 4757967 13 0308028-05 Cl2-BZ#8 0.125 U µg/Kg 0.125 µg/Kg9/26/2001 13-14-092601 611801 4757967 13 0308028-05 Cl3-BZ#18 0.278 U µg/Kg 0.278 µg/Kg9/26/2001 13-14-092601 611801 4757967 13 0308028-05 Cl3-BZ#31/#28 7.83 J µg/Kg 2.00 µg/Kg9/26/2001 13-14-092601 611801 4757967 13 0308028-05 Cl4-BZ#44 0.190 U µg/Kg 0.190 µg/Kg9/26/2001 13-14-092601 611801 4757967 13 0308028-05 Cl4-BZ#45 0.254 U µg/Kg 0.254 µg/Kg9/26/2001 13-14-092601 611801 4757967 13 0308028-05 Cl4-BZ#47 1.94 µg/Kg 0.323 µg/Kg9/26/2001 13-14-092601 611801 4757967 13 0308028-05 Cl4-BZ#49 0.589 J µg/Kg 0.158 µg/Kg9/26/2001 13-14-092601 611801 4757967 13 0308028-05 Cl4-BZ#52 1.10 µg/Kg 0.180 µg/Kg9/26/2001 13-14-092601 611801 4757967 13 0308028-05 Cl4-BZ#56 1.53 µg/Kg 0.0945 µg/Kg9/26/2001 13-14-092601 611801 4757967 13 0308028-05 Cl4-BZ#66 4.50 µg/Kg 0.126 µg/Kg9/26/2001 13-14-092601 611801 4757967 13 0308028-05 Cl4-BZ#70 1.66 µg/Kg 0.111 µg/Kg9/26/2001 13-14-092601 611801 4757967 13 0308028-05 Cl4-BZ#74 3.43 µg/Kg 0.195 µg/Kg9/26/2001 13-14-092601 611801 4757967 13 0308028-05 Cl4-BZ#77 0.174 U µg/Kg 0.174 µg/Kg9/26/2001 13-14-092601 611801 4757967 13 0308028-05 Cl4-BZ#81 0.173 U µg/Kg 0.173 µg/Kg9/26/2001 13-14-092601 611801 4757967 13 0308028-05 Cl5-BZ#87 2.04 µg/Kg 0.0770 µg/Kg9/26/2001 13-14-092601 611801 4757967 13 0308028-05 Cl5-BZ#95 0.0596 U µg/Kg 0.0596 µg/Kg



Extracted 7/30/04




SITE NUMBER



9/26/2001 13-14-092601 611801 4757967 13 0308028-05 Cl5-BZ#99 4.68 µg/Kg 0.0407 µg/Kg9/26/2001 13-14-092601 611801 4757967 13 0308028-05 Cl5-BZ#101 0.981 µg/Kg 0.116 µg/Kg9/26/2001 13-14-092601 611801 4757967 13 0308028-05 Cl5-BZ#105 2.84 µg/Kg 0.0567 µg/Kg9/26/2001 13-14-092601 611801 4757967 13 0308028-05 Cl5-BZ#110 0.552 J µg/Kg 0.111 µg/Kg9/26/2001 13-14-092601 611801 4757967 13 0308028-05 Cl5-BZ#114 0.269 µg/Kg 0.0509 µg/Kg9/26/2001 13-14-092601 611801 4757967 13 0308028-05 Cl5-BZ#118 6.45 µg/Kg 0.119 µg/Kg9/26/2001 13-14-092601 611801 4757967 13 0308028-05 Cl5-BZ#123 0.100 U µg/Kg 0.100 µg/Kg9/26/2001 13-14-092601 611801 4757967 13 0308028-05 Cl5-BZ#126 0.0887 U µg/Kg 0.0887 µg/Kg9/26/2001 13-14-092601 611801 4757967 13 0308028-05 Cl6-BZ#128 0.792 µg/Kg 0.0799 µg/Kg9/26/2001 13-14-092601 611801 4757967 13 0308028-05 Cl6-BZ#138 10.0 µg/Kg 0.115 µg/Kg9/26/2001 13-14-092601 611801 4757967 13 0308028-05 Cl6-BZ#146 1.34 µg/Kg 0.0727 µg/Kg9/26/2001 13-14-092601 611801 4757967 13 0308028-05 Cl6-BZ#149 0.429 J µg/Kg 0.0930 µg/Kg9/26/2001 13-14-092601 611801 4757967 13 0308028-05 Cl6-BZ#151 0.349 J µg/Kg 0.154 µg/Kg9/26/2001 13-14-092601 611801 4757967 13 0308028-05 Cl6-BZ#153 7.43 µg/Kg 0.132 µg/Kg9/26/2001 13-14-092601 611801 4757967 13 0308028-05 Cl6-BZ#156 0.785 µg/Kg 0.0945 µg/Kg9/26/2001 13-14-092601 611801 4757967 13 0308028-05 Cl6-BZ#157 0.211 J µg/Kg 0.0741 µg/Kg9/26/2001 13-14-092601 611801 4757967 13 0308028-05 Cl6-BZ#158 0.182 J µg/Kg 0.0625 µg/Kg9/26/2001 13-14-092601 611801 4757967 13 0308028-05 Cl6-BZ#167 0.421 µg/Kg 0.0799 µg/Kg9/26/2001 13-14-092601 611801 4757967 13 0308028-05 Cl6-BZ#169 0.257 U µg/Kg 0.257 µg/Kg9/26/2001 13-14-092601 611801 4757967 13 0308028-05 Cl7-BZ#170 0.299 U µg/Kg 0.299 µg/Kg9/26/2001 13-14-092601 611801 4757967 13 0308028-05 Cl7-BZ#174 0.0611 U µg/Kg 0.0611 µg/Kg9/26/2001 13-14-092601 611801 4757967 13 0308028-05 Cl7-BZ#177 0.0858 U µg/Kg 0.0858 µg/Kg9/26/2001 13-14-092601 611801 4757967 13 0308028-05 Cl7-BZ#180 3.63 µg/Kg 0.128 µg/Kg9/26/2001 13-14-092601 611801 4757967 13 0308028-05 Cl7-BZ#183 0.509 µg/Kg 0.0581 µg/Kg9/26/2001 13-14-092601 611801 4757967 13 0308028-05 Cl7-BZ#187 2.19 µg/Kg 0.0640 µg/Kg9/26/2001 13-14-092601 611801 4757967 13 0308028-05 Cl7-BZ#189 0.115 U µg/Kg 0.115 µg/Kg9/26/2001 13-14-092601 611801 4757967 13 0308028-05 Cl8-BZ#194 0.807 µg/Kg 0.134 µg/Kg9/26/2001 13-14-092601 611801 4757967 13 0308028-05 Cl8-BZ#195 0.233 J µg/Kg 0.132 µg/Kg9/26/2001 13-14-092601 611801 4757967 13 0308028-05 Cl8-BZ#201 0.661 µg/Kg 0.116 µg/Kg9/26/2001 13-14-092601 611801 4757967 13 0308028-05 Cl9-BZ#206 0.698 J µg/Kg 0.155 µg/Kg9/26/2001 13-14-092601 611801 4757967 13 0308028-05 Cl10-BZ#209 0.189 J µg/Kg 0.0727 µg/Kg9/26/2001 13-14-092601 611801 4757967 13 0308028-05 Monochlorobiphenyls 4.27 U µg/Kg 4.27 µg/Kg9/26/2001 13-14-092601 611801 4757967 13 0308028-05 Dichlorobiphenyls 0.125 U µg/Kg 0.125 µg/Kg9/26/2001 13-14-092601 611801 4757967 13 0308028-05 Trichlorobiphenyls 7.54 µg/Kg 0.429 µg/Kg



Extracted 7/30/04




SITE NUMBER



9/26/2001 13-14-092601 611801 4757967 13 0308028-05 Tetrachlorobiphenyls 25.2 µg/Kg 0.0669 µg/Kg9/26/2001 13-14-092601 611801 4757967 13 0308028-05 Pentachlorobiphenyls 29.9 µg/Kg 0.0770 µg/Kg9/26/2001 13-14-092601 611801 4757967 13 0308028-05 Hexachlorobiphenyls 25.1 µg/Kg 0.122 µg/Kg9/26/2001 13-14-092601 611801 4757967 13 0308028-05 Heptachlorobiphenyls 10.9 µg/Kg 0.0669 µg/Kg9/26/2001 13-14-092601 611801 4757967 13 0308028-05 Octachlorobiphenyls 8.50 µg/Kg 0.0611 µg/Kg9/26/2001 13-14-092601 611801 4757967 13 0308028-05 Nonachlorobiphenyls 0.698 J µg/Kg 0.155 µg/Kg9/26/2001 13-14-092601 611801 4757967 13 0308028-05 Decachlorobiphenyl 0.189 J µg/Kg 0.0727 µg/Kg9/26/2001 13-14-092601 611801 4757967 13 0308028-05 Total Homologs 108 µg/Kg 0.0727 µg/Kg9/26/2001 13-14-092601 611801 4757967 13 0308028-05 Percent Lipids 4.7 % 0.1 %9/26/2001 13-14-092601 611801 4757967 13 0308028-05 Percent Moisture 73.8 % 0.1 %9/18/2001 15-05-091801 611552 4756404 15 0308028-06 Cl2-BZ#8 0.0924 U µg/Kg 0.0924 µg/Kg9/18/2001 15-05-091801 611552 4756404 15 0308028-06 Cl3-BZ#18 0.205 U µg/Kg 0.205 µg/Kg9/18/2001 15-05-091801 611552 4756404 15 0308028-06 Cl3-BZ#31/#28 4.57 J µg/Kg 1.48 µg/Kg9/18/2001 15-05-091801 611552 4756404 15 0308028-06 Cl4-BZ#44 0.141 U µg/Kg 0.141 µg/Kg9/18/2001 15-05-091801 611552 4756404 15 0308028-06 Cl4-BZ#45 0.188 U µg/Kg 0.188 µg/Kg9/18/2001 15-05-091801 611552 4756404 15 0308028-06 Cl4-BZ#47 1.48 µg/Kg 0.239 µg/Kg9/18/2001 15-05-091801 611552 4756404 15 0308028-06 Cl4-BZ#49 0.253 J µg/Kg 0.117 µg/Kg9/18/2001 15-05-091801 611552 4756404 15 0308028-06 Cl4-BZ#52 0.133 U µg/Kg 0.133 µg/Kg9/18/2001 15-05-091801 611552 4756404 15 0308028-06 Cl4-BZ#56 0.763 µg/Kg 0.0699 µg/Kg9/18/2001 15-05-091801 611552 4756404 15 0308028-06 Cl4-BZ#66 2.02 µg/Kg 0.0935 µg/Kg9/18/2001 15-05-091801 611552 4756404 15 0308028-06 Cl4-BZ#70 0.597 µg/Kg 0.0817 µg/Kg9/18/2001 15-05-091801 611552 4756404 15 0308028-06 Cl4-BZ#74 1.80 µg/Kg 0.144 µg/Kg9/18/2001 15-05-091801 611552 4756404 15 0308028-06 Cl4-BZ#77 0.129 U µg/Kg 0.129 µg/Kg9/18/2001 15-05-091801 611552 4756404 15 0308028-06 Cl4-BZ#81 0.128 U µg/Kg 0.128 µg/Kg9/18/2001 15-05-091801 611552 4756404 15 0308028-06 Cl5-BZ#87 1.10 µg/Kg 0.0570 µg/Kg9/18/2001 15-05-091801 611552 4756404 15 0308028-06 Cl5-BZ#95 0.124 J µg/Kg 0.0441 µg/Kg9/18/2001 15-05-091801 611552 4756404 15 0308028-06 Cl5-BZ#99 4.60 µg/Kg 0.0301 µg/Kg9/18/2001 15-05-091801 611552 4756404 15 0308028-06 Cl5-BZ#101 0.511 µg/Kg 0.0860 µg/Kg9/18/2001 15-05-091801 611552 4756404 15 0308028-06 Cl5-BZ#105 1.87 µg/Kg 0.0419 µg/Kg9/18/2001 15-05-091801 611552 4756404 15 0308028-06 Cl5-BZ#110 0.156 J µg/Kg 0.0817 µg/Kg9/18/2001 15-05-091801 611552 4756404 15 0308028-06 Cl5-BZ#114 0.274 µg/Kg 0.0376 µg/Kg9/18/2001 15-05-091801 611552 4756404 15 0308028-06 Cl5-BZ#118 4.93 µg/Kg 0.0881 µg/Kg9/18/2001 15-05-091801 611552 4756404 15 0308028-06 Cl5-BZ#123 0.0742 U µg/Kg 0.0742 µg/Kg9/18/2001 15-05-091801 611552 4756404 15 0308028-06 Cl5-BZ#126 0.0656 U µg/Kg 0.0656 µg/Kg



Extracted 7/30/04




SITE NUMBER



9/18/2001 15-05-091801 611552 4756404 15 0308028-06 Cl6-BZ#128 0.538 µg/Kg 0.0591 µg/Kg9/18/2001 15-05-091801 611552 4756404 15 0308028-06 Cl6-BZ#138 8.43 µg/Kg 0.0849 µg/Kg9/18/2001 15-05-091801 611552 4756404 15 0308028-06 Cl6-BZ#146 1.11 µg/Kg 0.0537 µg/Kg9/18/2001 15-05-091801 611552 4756404 15 0308028-06 Cl6-BZ#149 0.167 J µg/Kg 0.0688 µg/Kg9/18/2001 15-05-091801 611552 4756404 15 0308028-06 Cl6-BZ#151 0.172 J µg/Kg 0.114 µg/Kg9/18/2001 15-05-091801 611552 4756404 15 0308028-06 Cl6-BZ#153 7.98 µg/Kg 0.0978 µg/Kg9/18/2001 15-05-091801 611552 4756404 15 0308028-06 Cl6-BZ#156 0.575 µg/Kg 0.0699 µg/Kg9/18/2001 15-05-091801 611552 4756404 15 0308028-06 Cl6-BZ#157 0.188 J µg/Kg 0.0548 µg/Kg9/18/2001 15-05-091801 611552 4756404 15 0308028-06 Cl6-BZ#158 0.145 J µg/Kg 0.0462 µg/Kg9/18/2001 15-05-091801 611552 4756404 15 0308028-06 Cl6-BZ#167 0.387 µg/Kg 0.0591 µg/Kg9/18/2001 15-05-091801 611552 4756404 15 0308028-06 Cl6-BZ#169 0.190 U µg/Kg 0.190 µg/Kg9/18/2001 15-05-091801 611552 4756404 15 0308028-06 Cl7-BZ#170 0.221 U µg/Kg 0.221 µg/Kg9/18/2001 15-05-091801 611552 4756404 15 0308028-06 Cl7-BZ#174 0.0451 U µg/Kg 0.0451 µg/Kg9/18/2001 15-05-091801 611552 4756404 15 0308028-06 Cl7-BZ#177 0.0634 U µg/Kg 0.0634 µg/Kg9/18/2001 15-05-091801 611552 4756404 15 0308028-06 Cl7-BZ#180 0.0946 U µg/Kg 0.0946 µg/Kg9/18/2001 15-05-091801 611552 4756404 15 0308028-06 Cl7-BZ#183 0.451 µg/Kg 0.0430 µg/Kg9/18/2001 15-05-091801 611552 4756404 15 0308028-06 Cl7-BZ#187 1.14 µg/Kg 0.0473 µg/Kg9/18/2001 15-05-091801 611552 4756404 15 0308028-06 Cl7-BZ#189 0.0849 U µg/Kg 0.0849 µg/Kg9/18/2001 15-05-091801 611552 4756404 15 0308028-06 Cl8-BZ#194 0.462 J µg/Kg 0.0989 µg/Kg9/18/2001 15-05-091801 611552 4756404 15 0308028-06 Cl8-BZ#195 0.0978 U µg/Kg 0.0978 µg/Kg9/18/2001 15-05-091801 611552 4756404 15 0308028-06 Cl8-BZ#201 0.290 J µg/Kg 0.0860 µg/Kg9/18/2001 15-05-091801 611552 4756404 15 0308028-06 Cl9-BZ#206 0.650 µg/Kg 0.115 µg/Kg9/18/2001 15-05-091801 611552 4756404 15 0308028-06 Cl10-BZ#209 0.150 J µg/Kg 0.0537 µg/Kg9/18/2001 15-05-091801 611552 4756404 15 0308028-06 Monochlorobiphenyls 3.16 U µg/Kg 3.16 µg/Kg9/18/2001 15-05-091801 611552 4756404 15 0308028-06 Dichlorobiphenyls 0.0924 U µg/Kg 0.0924 µg/Kg9/18/2001 15-05-091801 611552 4756404 15 0308028-06 Trichlorobiphenyls 4.55 µg/Kg 0.317 µg/Kg9/18/2001 15-05-091801 611552 4756404 15 0308028-06 Tetrachlorobiphenyls 14.7 µg/Kg 0.0494 µg/Kg9/18/2001 15-05-091801 611552 4756404 15 0308028-06 Pentachlorobiphenyls 24.1 µg/Kg 0.0570 µg/Kg9/18/2001 15-05-091801 611552 4756404 15 0308028-06 Hexachlorobiphenyls 22.1 µg/Kg 0.0903 µg/Kg9/18/2001 15-05-091801 611552 4756404 15 0308028-06 Heptachlorobiphenyls 1.31 µg/Kg 0.0494 µg/Kg9/18/2001 15-05-091801 611552 4756404 15 0308028-06 Octachlorobiphenyls 4.28 µg/Kg 0.0451 µg/Kg9/18/2001 15-05-091801 611552 4756404 15 0308028-06 Nonachlorobiphenyls 0.672 µg/Kg 0.115 µg/Kg9/18/2001 15-05-091801 611552 4756404 15 0308028-06 Decachlorobiphenyl 0.150 J µg/Kg 0.0537 µg/Kg9/18/2001 15-05-091801 611552 4756404 15 0308028-06 Total Homologs 71.9 µg/Kg 0.0537 µg/Kg



Extracted 7/30/04




SITE NUMBER



9/18/2001 15-05-091801 611552 4756404 15 0308028-06 Percent Lipids 5.0 % 0.1 %9/18/2001 15-05-091801 611552 4756404 15 0308028-06 Percent Moisture 70.2 % 0.1 %9/19/2001 15-11-091901 611552 4756404 15 0308028-07 Cl2-BZ#8 0.122 U µg/Kg 0.122 µg/Kg9/19/2001 15-11-091901 611552 4756404 15 0308028-07 Cl3-BZ#18 0.271 U µg/Kg 0.271 µg/Kg9/19/2001 15-11-091901 611552 4756404 15 0308028-07 Cl3-BZ#31/#28 2.48 J µg/Kg 1.96 µg/Kg9/19/2001 15-11-091901 611552 4756404 15 0308028-07 Cl4-BZ#44 0.220 J µg/Kg 0.186 µg/Kg9/19/2001 15-11-091901 611552 4756404 15 0308028-07 Cl4-BZ#45 0.582 J µg/Kg 0.249 µg/Kg9/19/2001 15-11-091901 611552 4756404 15 0308028-07 Cl4-BZ#47 1.02 J µg/Kg 0.315 µg/Kg9/19/2001 15-11-091901 611552 4756404 15 0308028-07 Cl4-BZ#49 0.155 U µg/Kg 0.155 µg/Kg9/19/2001 15-11-091901 611552 4756404 15 0308028-07 Cl4-BZ#52 0.305 J µg/Kg 0.176 µg/Kg9/19/2001 15-11-091901 611552 4756404 15 0308028-07 Cl4-BZ#56 0.625 µg/Kg 0.0923 µg/Kg9/19/2001 15-11-091901 611552 4756404 15 0308028-07 Cl4-BZ#66 1.39 µg/Kg 0.123 µg/Kg9/19/2001 15-11-091901 611552 4756404 15 0308028-07 Cl4-BZ#70 0.511 J µg/Kg 0.108 µg/Kg9/19/2001 15-11-091901 611552 4756404 15 0308028-07 Cl4-BZ#74 1.14 µg/Kg 0.190 µg/Kg9/19/2001 15-11-091901 611552 4756404 15 0308028-07 Cl4-BZ#77 0.170 U µg/Kg 0.170 µg/Kg9/19/2001 15-11-091901 611552 4756404 15 0308028-07 Cl4-BZ#81 0.169 U µg/Kg 0.169 µg/Kg9/19/2001 15-11-091901 611552 4756404 15 0308028-07 Cl5-BZ#87 1.41 µg/Kg 0.0753 µg/Kg9/19/2001 15-11-091901 611552 4756404 15 0308028-07 Cl5-BZ#95 0.106 J µg/Kg 0.0582 µg/Kg9/19/2001 15-11-091901 611552 4756404 15 0308028-07 Cl5-BZ#99 4.03 µg/Kg 0.0398 µg/Kg9/19/2001 15-11-091901 611552 4756404 15 0308028-07 Cl5-BZ#101 0.405 J µg/Kg 0.114 µg/Kg9/19/2001 15-11-091901 611552 4756404 15 0308028-07 Cl5-BZ#105 2.04 µg/Kg 0.0554 µg/Kg9/19/2001 15-11-091901 611552 4756404 15 0308028-07 Cl5-BZ#110 0.142 J µg/Kg 0.108 µg/Kg9/19/2001 15-11-091901 611552 4756404 15 0308028-07 Cl5-BZ#114 0.249 J µg/Kg 0.0497 µg/Kg9/19/2001 15-11-091901 611552 4756404 15 0308028-07 Cl5-BZ#118 5.54 µg/Kg 0.116 µg/Kg9/19/2001 15-11-091901 611552 4756404 15 0308028-07 Cl5-BZ#123 0.0980 U µg/Kg 0.0980 µg/Kg9/19/2001 15-11-091901 611552 4756404 15 0308028-07 Cl5-BZ#126 0.0866 U µg/Kg 0.0866 µg/Kg9/19/2001 15-11-091901 611552 4756404 15 0308028-07 Cl6-BZ#128 0.689 µg/Kg 0.0781 µg/Kg9/19/2001 15-11-091901 611552 4756404 15 0308028-07 Cl6-BZ#138 11.4 µg/Kg 0.112 µg/Kg9/19/2001 15-11-091901 611552 4756404 15 0308028-07 Cl6-BZ#146 1.26 µg/Kg 0.0710 µg/Kg9/19/2001 15-11-091901 611552 4756404 15 0308028-07 Cl6-BZ#149 0.163 J µg/Kg 0.0909 µg/Kg9/19/2001 15-11-091901 611552 4756404 15 0308028-07 Cl6-BZ#151 0.270 J µg/Kg 0.150 µg/Kg9/19/2001 15-11-091901 611552 4756404 15 0308028-07 Cl6-BZ#153 10.7 µg/Kg 0.129 µg/Kg9/19/2001 15-11-091901 611552 4756404 15 0308028-07 Cl6-BZ#156 1.18 µg/Kg 0.0923 µg/Kg9/19/2001 15-11-091901 611552 4756404 15 0308028-07 Cl6-BZ#157 0.234 J µg/Kg 0.0724 µg/Kg



Extracted 7/30/04




SITE NUMBER



9/19/2001 15-11-091901 611552 4756404 15 0308028-07 Cl6-BZ#158 0.263 J µg/Kg 0.0611 µg/Kg9/19/2001 15-11-091901 611552 4756404 15 0308028-07 Cl6-BZ#167 0.604 µg/Kg 0.0781 µg/Kg9/19/2001 15-11-091901 611552 4756404 15 0308028-07 Cl6-BZ#169 0.251 U µg/Kg 0.251 µg/Kg9/19/2001 15-11-091901 611552 4756404 15 0308028-07 Cl7-BZ#170 0.292 U µg/Kg 0.292 µg/Kg9/19/2001 15-11-091901 611552 4756404 15 0308028-07 Cl7-BZ#174 0.0596 U µg/Kg 0.0596 µg/Kg9/19/2001 15-11-091901 611552 4756404 15 0308028-07 Cl7-BZ#177 0.0838 U µg/Kg 0.0838 µg/Kg9/19/2001 15-11-091901 611552 4756404 15 0308028-07 Cl7-BZ#180 3.81 µg/Kg 0.125 µg/Kg9/19/2001 15-11-091901 611552 4756404 15 0308028-07 Cl7-BZ#183 0.653 µg/Kg 0.0568 µg/Kg9/19/2001 15-11-091901 611552 4756404 15 0308028-07 Cl7-BZ#187 1.38 µg/Kg 0.0625 µg/Kg9/19/2001 15-11-091901 611552 4756404 15 0308028-07 Cl7-BZ#189 0.112 U µg/Kg 0.112 µg/Kg9/19/2001 15-11-091901 611552 4756404 15 0308028-07 Cl8-BZ#194 1.18 µg/Kg 0.131 µg/Kg9/19/2001 15-11-091901 611552 4756404 15 0308028-07 Cl8-BZ#195 0.129 U µg/Kg 0.129 µg/Kg9/19/2001 15-11-091901 611552 4756404 15 0308028-07 Cl8-BZ#201 0.632 µg/Kg 0.114 µg/Kg9/19/2001 15-11-091901 611552 4756404 15 0308028-07 Cl9-BZ#206 1.39 µg/Kg 0.152 µg/Kg9/19/2001 15-11-091901 611552 4756404 15 0308028-07 Cl10-BZ#209 0.348 J µg/Kg 0.0710 µg/Kg9/19/2001 15-11-091901 611552 4756404 15 0308028-07 Monochlorobiphenyls 4.18 U µg/Kg 4.18 µg/Kg9/19/2001 15-11-091901 611552 4756404 15 0308028-07 Dichlorobiphenyls 0.122 U µg/Kg 0.122 µg/Kg9/19/2001 15-11-091901 611552 4756404 15 0308028-07 Trichlorobiphenyls 1.89 J µg/Kg 0.419 µg/Kg9/19/2001 15-11-091901 611552 4756404 15 0308028-07 Tetrachlorobiphenyls 13.7 µg/Kg 0.0653 µg/Kg9/19/2001 15-11-091901 611552 4756404 15 0308028-07 Pentachlorobiphenyls 24.5 µg/Kg 0.0753 µg/Kg9/19/2001 15-11-091901 611552 4756404 15 0308028-07 Hexachlorobiphenyls 31.5 µg/Kg 0.119 µg/Kg9/19/2001 15-11-091901 611552 4756404 15 0308028-07 Heptachlorobiphenyls 1.74 µg/Kg 0.0653 µg/Kg9/19/2001 15-11-091901 611552 4756404 15 0308028-07 Octachlorobiphenyls 3.53 µg/Kg 0.0596 µg/Kg9/19/2001 15-11-091901 611552 4756404 15 0308028-07 Nonachlorobiphenyls 1.39 µg/Kg 0.152 µg/Kg9/19/2001 15-11-091901 611552 4756404 15 0308028-07 Decachlorobiphenyl 0.348 J µg/Kg 0.0710 µg/Kg9/19/2001 15-11-091901 611552 4756404 15 0308028-07 Total Homologs 78.6 µg/Kg 0.0710 µg/Kg9/19/2001 15-11-091901 611552 4756404 15 0308028-07 Percent Lipids 2.8 % 0.1 %9/19/2001 15-11-091901 611552 4756404 15 0308028-07 Percent Moisture 71.3 % 0.1 %9/19/2001 15-12-091901 611552 4756404 15 0308028-08 Cl2-BZ#8 0.155 U µg/Kg 0.155 µg/Kg9/19/2001 15-12-091901 611552 4756404 15 0308028-08 Cl3-BZ#18 0.344 U µg/Kg 0.344 µg/Kg9/19/2001 15-12-091901 611552 4756404 15 0308028-08 Cl3-BZ#31/#28 17.0 µg/Kg 2.48 µg/Kg9/19/2001 15-12-091901 611552 4756404 15 0308028-08 Cl4-BZ#44 0.451 J µg/Kg 0.236 µg/Kg9/19/2001 15-12-091901 611552 4756404 15 0308028-08 Cl4-BZ#45 0.577 J µg/Kg 0.316 µg/Kg9/19/2001 15-12-091901 611552 4756404 15 0308028-08 Cl4-BZ#47 11.1 µg/Kg 0.400 µg/Kg



Extracted 7/30/04




SITE NUMBER



9/19/2001 15-12-091901 611552 4756404 15 0308028-08 Cl4-BZ#49 2.01 µg/Kg 0.197 µg/Kg9/19/2001 15-12-091901 611552 4756404 15 0308028-08 Cl4-BZ#52 3.96 µg/Kg 0.224 µg/Kg9/19/2001 15-12-091901 611552 4756404 15 0308028-08 Cl4-BZ#56 12.5 µg/Kg 0.117 µg/Kg9/19/2001 15-12-091901 611552 4756404 15 0308028-08 Cl4-BZ#66 39.3 µg/Kg 0.157 µg/Kg9/19/2001 15-12-091901 611552 4756404 15 0308028-08 Cl4-BZ#70 17.2 µg/Kg 0.137 µg/Kg9/19/2001 15-12-091901 611552 4756404 15 0308028-08 Cl4-BZ#74 23.9 µg/Kg 0.242 µg/Kg9/19/2001 15-12-091901 611552 4756404 15 0308028-08 Cl4-BZ#77 0.216 U µg/Kg 0.216 µg/Kg9/19/2001 15-12-091901 611552 4756404 15 0308028-08 Cl4-BZ#81 0.215 U µg/Kg 0.215 µg/Kg9/19/2001 15-12-091901 611552 4756404 15 0308028-08 Cl5-BZ#87 9.34 µg/Kg 0.0956 µg/Kg9/19/2001 15-12-091901 611552 4756404 15 0308028-08 Cl5-BZ#95 0.893 µg/Kg 0.0739 µg/Kg9/19/2001 15-12-091901 611552 4756404 15 0308028-08 Cl5-BZ#99 32.8 µg/Kg 0.0505 µg/Kg9/19/2001 15-12-091901 611552 4756404 15 0308028-08 Cl5-BZ#101 3.90 µg/Kg 0.144 µg/Kg9/19/2001 15-12-091901 611552 4756404 15 0308028-08 Cl5-BZ#105 17.0 µg/Kg 0.0703 µg/Kg9/19/2001 15-12-091901 611552 4756404 15 0308028-08 Cl5-BZ#110 2.51 µg/Kg 0.137 µg/Kg9/19/2001 15-12-091901 611552 4756404 15 0308028-08 Cl5-BZ#114 1.78 µg/Kg 0.0631 µg/Kg9/19/2001 15-12-091901 611552 4756404 15 0308028-08 Cl5-BZ#118 39.9 µg/Kg 0.148 µg/Kg9/19/2001 15-12-091901 611552 4756404 15 0308028-08 Cl5-BZ#123 0.124 U µg/Kg 0.124 µg/Kg9/19/2001 15-12-091901 611552 4756404 15 0308028-08 Cl5-BZ#126 0.110 U µg/Kg 0.110 µg/Kg9/19/2001 15-12-091901 611552 4756404 15 0308028-08 Cl6-BZ#128 3.70 µg/Kg 0.0992 µg/Kg9/19/2001 15-12-091901 611552 4756404 15 0308028-08 Cl6-BZ#138 54.0 µg/Kg 0.142 µg/Kg9/19/2001 15-12-091901 611552 4756404 15 0308028-08 Cl6-BZ#146 7.65 µg/Kg 0.0902 µg/Kg9/19/2001 15-12-091901 611552 4756404 15 0308028-08 Cl6-BZ#149 1.34 µg/Kg 0.115 µg/Kg9/19/2001 15-12-091901 611552 4756404 15 0308028-08 Cl6-BZ#151 0.631 J µg/Kg 0.191 µg/Kg9/19/2001 15-12-091901 611552 4756404 15 0308028-08 Cl6-BZ#153 42.2 µg/Kg 0.164 µg/Kg9/19/2001 15-12-091901 611552 4756404 15 0308028-08 Cl6-BZ#156 3.64 µg/Kg 0.117 µg/Kg9/19/2001 15-12-091901 611552 4756404 15 0308028-08 Cl6-BZ#157 0.929 µg/Kg 0.0920 µg/Kg9/19/2001 15-12-091901 611552 4756404 15 0308028-08 Cl6-BZ#158 1.11 µg/Kg 0.0775 µg/Kg9/19/2001 15-12-091901 611552 4756404 15 0308028-08 Cl6-BZ#167 2.15 µg/Kg 0.0992 µg/Kg9/19/2001 15-12-091901 611552 4756404 15 0308028-08 Cl6-BZ#169 0.319 U µg/Kg 0.319 µg/Kg9/19/2001 15-12-091901 611552 4756404 15 0308028-08 Cl7-BZ#170 8.16 µg/Kg 0.371 µg/Kg9/19/2001 15-12-091901 611552 4756404 15 0308028-08 Cl7-BZ#174 0.0757 U µg/Kg 0.0757 µg/Kg9/19/2001 15-12-091901 611552 4756404 15 0308028-08 Cl7-BZ#177 0.106 U µg/Kg 0.106 µg/Kg9/19/2001 15-12-091901 611552 4756404 15 0308028-08 Cl7-BZ#180 11.5 µg/Kg 0.159 µg/Kg9/19/2001 15-12-091901 611552 4756404 15 0308028-08 Cl7-BZ#183 2.65 µg/Kg 0.0721 µg/Kg



Extracted 7/30/04




SITE NUMBER



9/19/2001 15-12-091901 611552 4756404 15 0308028-08 Cl7-BZ#187 9.80 µg/Kg 0.0793 µg/Kg9/19/2001 15-12-091901 611552 4756404 15 0308028-08 Cl7-BZ#189 0.142 U µg/Kg 0.142 µg/Kg9/19/2001 15-12-091901 611552 4756404 15 0308028-08 Cl8-BZ#194 0.166 U µg/Kg 0.166 µg/Kg9/19/2001 15-12-091901 611552 4756404 15 0308028-08 Cl8-BZ#195 0.164 U µg/Kg 0.164 µg/Kg9/19/2001 15-12-091901 611552 4756404 15 0308028-08 Cl8-BZ#201 2.15 µg/Kg 0.144 µg/Kg9/19/2001 15-12-091901 611552 4756404 15 0308028-08 Cl9-BZ#206 2.88 µg/Kg 0.193 µg/Kg9/19/2001 15-12-091901 611552 4756404 15 0308028-08 Cl10-BZ#209 0.523 µg/Kg 0.0902 µg/Kg9/19/2001 15-12-091901 611552 4756404 15 0308028-08 Monochlorobiphenyls 5.30 U µg/Kg 5.30 µg/Kg9/19/2001 15-12-091901 611552 4756404 15 0308028-08 Dichlorobiphenyls 0.155 U µg/Kg 0.155 µg/Kg9/19/2001 15-12-091901 611552 4756404 15 0308028-08 Trichlorobiphenyls 14.6 µg/Kg 0.532 µg/Kg9/19/2001 15-12-091901 611552 4756404 15 0308028-08 Tetrachlorobiphenyls 146 µg/Kg 0.0829 µg/Kg9/19/2001 15-12-091901 611552 4756404 15 0308028-08 Pentachlorobiphenyls 181 µg/Kg 0.0956 µg/Kg9/19/2001 15-12-091901 611552 4756404 15 0308028-08 Hexachlorobiphenyls 130 µg/Kg 0.152 µg/Kg9/19/2001 15-12-091901 611552 4756404 15 0308028-08 Heptachlorobiphenyls 10.1 µg/Kg 0.0829 µg/Kg9/19/2001 15-12-091901 611552 4756404 15 0308028-08 Octachlorobiphenyls 12.7 µg/Kg 0.0757 µg/Kg9/19/2001 15-12-091901 611552 4756404 15 0308028-08 Nonachlorobiphenyls 2.88 µg/Kg 0.193 µg/Kg9/19/2001 15-12-091901 611552 4756404 15 0308028-08 Decachlorobiphenyl 0.523 µg/Kg 0.0902 µg/Kg9/19/2001 15-12-091901 611552 4756404 15 0308028-08 Total Homologs 497 µg/Kg 0.0902 µg/Kg9/19/2001 15-12-091901 611552 4756404 15 0308028-08 Percent Lipids 2.3 % 0.1 %9/19/2001 15-12-091901 611552 4756404 15 0308028-08 Percent Moisture 70.8 % 0.1 %9/19/2001 15-16-091901 611552 4756404 15 0308028-09 Cl2-BZ#8 0.128 U µg/Kg 0.128 µg/Kg9/19/2001 15-16-091901 611552 4756404 15 0308028-09 Cl3-BZ#18 0.285 U µg/Kg 0.285 µg/Kg9/19/2001 15-16-091901 611552 4756404 15 0308028-09 Cl3-BZ#31/#28 5.12 J µg/Kg 2.05 µg/Kg9/19/2001 15-16-091901 611552 4756404 15 0308028-09 Cl4-BZ#44 0.201 J µg/Kg 0.195 µg/Kg9/19/2001 15-16-091901 611552 4756404 15 0308028-09 Cl4-BZ#45 0.350 J µg/Kg 0.261 µg/Kg9/19/2001 15-16-091901 611552 4756404 15 0308028-09 Cl4-BZ#47 4.91 µg/Kg 0.331 µg/Kg9/19/2001 15-16-091901 611552 4756404 15 0308028-09 Cl4-BZ#49 0.641 J µg/Kg 0.162 µg/Kg9/19/2001 15-16-091901 611552 4756404 15 0308028-09 Cl4-BZ#52 0.857 J µg/Kg 0.185 µg/Kg9/19/2001 15-16-091901 611552 4756404 15 0308028-09 Cl4-BZ#56 1.03 µg/Kg 0.0968 µg/Kg9/19/2001 15-16-091901 611552 4756404 15 0308028-09 Cl4-BZ#66 4.30 µg/Kg 0.130 µg/Kg9/19/2001 15-16-091901 611552 4756404 15 0308028-09 Cl4-BZ#70 2.29 µg/Kg 0.113 µg/Kg9/19/2001 15-16-091901 611552 4756404 15 0308028-09 Cl4-BZ#74 3.16 µg/Kg 0.200 µg/Kg9/19/2001 15-16-091901 611552 4756404 15 0308028-09 Cl4-BZ#77 0.179 U µg/Kg 0.179 µg/Kg9/19/2001 15-16-091901 611552 4756404 15 0308028-09 Cl4-BZ#81 0.177 U µg/Kg 0.177 µg/Kg



Extracted 7/30/04




SITE NUMBER



9/19/2001 15-16-091901 611552 4756404 15 0308028-09 Cl5-BZ#87 2.32 µg/Kg 0.0790 µg/Kg9/19/2001 15-16-091901 611552 4756404 15 0308028-09 Cl5-BZ#95 0.246 J µg/Kg 0.0611 µg/Kg9/19/2001 15-16-091901 611552 4756404 15 0308028-09 Cl5-BZ#99 11.5 µg/Kg 0.0417 µg/Kg9/19/2001 15-16-091901 611552 4756404 15 0308028-09 Cl5-BZ#101 1.04 µg/Kg 0.119 µg/Kg9/19/2001 15-16-091901 611552 4756404 15 0308028-09 Cl5-BZ#105 4.31 µg/Kg 0.0581 µg/Kg9/19/2001 15-16-091901 611552 4756404 15 0308028-09 Cl5-BZ#110 0.581 µg/Kg 0.113 µg/Kg9/19/2001 15-16-091901 611552 4756404 15 0308028-09 Cl5-BZ#114 0.484 µg/Kg 0.0521 µg/Kg9/19/2001 15-16-091901 611552 4756404 15 0308028-09 Cl5-BZ#118 15.3 µg/Kg 0.122 µg/Kg9/19/2001 15-16-091901 611552 4756404 15 0308028-09 Cl5-BZ#123 0.103 U µg/Kg 0.103 µg/Kg9/19/2001 15-16-091901 611552 4756404 15 0308028-09 Cl5-BZ#126 0.0909 U µg/Kg 0.0909 µg/Kg9/19/2001 15-16-091901 611552 4756404 15 0308028-09 Cl6-BZ#128 1.34 µg/Kg 0.0819 µg/Kg9/19/2001 15-16-091901 611552 4756404 15 0308028-09 Cl6-BZ#138 18.4 µg/Kg 0.118 µg/Kg9/19/2001 15-16-091901 611552 4756404 15 0308028-09 Cl6-BZ#146 2.24 µg/Kg 0.0745 µg/Kg9/19/2001 15-16-091901 611552 4756404 15 0308028-09 Cl6-BZ#149 0.350 J µg/Kg 0.0953 µg/Kg9/19/2001 15-16-091901 611552 4756404 15 0308028-09 Cl6-BZ#151 0.158 U µg/Kg 0.158 µg/Kg9/19/2001 15-16-091901 611552 4756404 15 0308028-09 Cl6-BZ#153 17.2 µg/Kg 0.136 µg/Kg9/19/2001 15-16-091901 611552 4756404 15 0308028-09 Cl6-BZ#156 1.89 µg/Kg 0.0968 µg/Kg9/19/2001 15-16-091901 611552 4756404 15 0308028-09 Cl6-BZ#157 0.447 µg/Kg 0.0760 µg/Kg9/19/2001 15-16-091901 611552 4756404 15 0308028-09 Cl6-BZ#158 0.469 µg/Kg 0.0641 µg/Kg9/19/2001 15-16-091901 611552 4756404 15 0308028-09 Cl6-BZ#167 0.983 µg/Kg 0.0819 µg/Kg9/19/2001 15-16-091901 611552 4756404 15 0308028-09 Cl6-BZ#169 0.264 U µg/Kg 0.264 µg/Kg9/19/2001 15-16-091901 611552 4756404 15 0308028-09 Cl7-BZ#170 0.307 U µg/Kg 0.307 µg/Kg9/19/2001 15-16-091901 611552 4756404 15 0308028-09 Cl7-BZ#174 0.0626 U µg/Kg 0.0626 µg/Kg9/19/2001 15-16-091901 611552 4756404 15 0308028-09 Cl7-BZ#177 0.0879 U µg/Kg 0.0879 µg/Kg9/19/2001 15-16-091901 611552 4756404 15 0308028-09 Cl7-BZ#180 5.46 µg/Kg 0.131 µg/Kg9/19/2001 15-16-091901 611552 4756404 15 0308028-09 Cl7-BZ#183 0.872 µg/Kg 0.0596 µg/Kg9/19/2001 15-16-091901 611552 4756404 15 0308028-09 Cl7-BZ#187 2.07 µg/Kg 0.0656 µg/Kg9/19/2001 15-16-091901 611552 4756404 15 0308028-09 Cl7-BZ#189 0.118 U µg/Kg 0.118 µg/Kg9/19/2001 15-16-091901 611552 4756404 15 0308028-09 Cl8-BZ#194 1.31 µg/Kg 0.137 µg/Kg9/19/2001 15-16-091901 611552 4756404 15 0308028-09 Cl8-BZ#195 0.136 U µg/Kg 0.136 µg/Kg9/19/2001 15-16-091901 611552 4756404 15 0308028-09 Cl8-BZ#201 0.812 µg/Kg 0.119 µg/Kg9/19/2001 15-16-091901 611552 4756404 15 0308028-09 Cl9-BZ#206 1.53 µg/Kg 0.159 µg/Kg9/19/2001 15-16-091901 611552 4756404 15 0308028-09 Cl10-BZ#209 0.298 J µg/Kg 0.0745 µg/Kg9/19/2001 15-16-091901 611552 4756404 15 0308028-09 Monochlorobiphenyls 4.38 U µg/Kg 4.38 µg/Kg



Extracted 7/30/04




SITE NUMBER



9/19/2001 15-16-091901 611552 4756404 15 0308028-09 Dichlorobiphenyls 0.128 U µg/Kg 0.128 µg/Kg9/19/2001 15-16-091901 611552 4756404 15 0308028-09 Trichlorobiphenyls 2.71 µg/Kg 0.440 µg/Kg9/19/2001 15-16-091901 611552 4756404 15 0308028-09 Tetrachlorobiphenyls 27.2 µg/Kg 0.0685 µg/Kg9/19/2001 15-16-091901 611552 4756404 15 0308028-09 Pentachlorobiphenyls 60.3 µg/Kg 0.0790 µg/Kg9/19/2001 15-16-091901 611552 4756404 15 0308028-09 Hexachlorobiphenyls 48.1 µg/Kg 0.125 µg/Kg9/19/2001 15-16-091901 611552 4756404 15 0308028-09 Heptachlorobiphenyls 2.79 µg/Kg 0.0685 µg/Kg9/19/2001 15-16-091901 611552 4756404 15 0308028-09 Octachlorobiphenyls 5.42 µg/Kg 0.0626 µg/Kg9/19/2001 15-16-091901 611552 4756404 15 0308028-09 Nonachlorobiphenyls 1.53 µg/Kg 0.159 µg/Kg9/19/2001 15-16-091901 611552 4756404 15 0308028-09 Decachlorobiphenyl 0.298 J µg/Kg 0.0745 µg/Kg9/19/2001 15-16-091901 611552 4756404 15 0308028-09 Total Homologs 148 µg/Kg 0.0745 µg/Kg9/19/2001 15-16-091901 611552 4756404 15 0308028-09 Percent Lipids 3.1 % 0.1 %9/19/2001 15-16-091901 611552 4756404 15 0308028-09 Percent Moisture 73.5 % 0.1 %9/20/2001 15-17-092001 611552 4756404 15 0308028-10 Cl2-BZ#8 0.103 U µg/Kg 0.103 µg/Kg9/20/2001 15-17-092001 611552 4756404 15 0308028-10 Cl3-BZ#18 0.229 U µg/Kg 0.229 µg/Kg9/20/2001 15-17-092001 611552 4756404 15 0308028-10 Cl3-BZ#31/#28 2.81 J µg/Kg 1.65 µg/Kg9/20/2001 15-17-092001 611552 4756404 15 0308028-10 Cl4-BZ#44 0.168 J µg/Kg 0.157 µg/Kg9/20/2001 15-17-092001 611552 4756404 15 0308028-10 Cl4-BZ#45 0.209 U µg/Kg 0.209 µg/Kg9/20/2001 15-17-092001 611552 4756404 15 0308028-10 Cl4-BZ#47 1.07 J µg/Kg 0.266 µg/Kg9/20/2001 15-17-092001 611552 4756404 15 0308028-10 Cl4-BZ#49 0.437 J µg/Kg 0.131 µg/Kg9/20/2001 15-17-092001 611552 4756404 15 0308028-10 Cl4-BZ#52 0.479 J µg/Kg 0.148 µg/Kg9/20/2001 15-17-092001 611552 4756404 15 0308028-10 Cl4-BZ#56 1.72 µg/Kg 0.0778 µg/Kg9/20/2001 15-17-092001 611552 4756404 15 0308028-10 Cl4-BZ#66 4.26 µg/Kg 0.104 µg/Kg9/20/2001 15-17-092001 611552 4756404 15 0308028-10 Cl4-BZ#70 0.988 µg/Kg 0.0910 µg/Kg9/20/2001 15-17-092001 611552 4756404 15 0308028-10 Cl4-BZ#74 4.10 µg/Kg 0.161 µg/Kg9/20/2001 15-17-092001 611552 4756404 15 0308028-10 Cl4-BZ#77 0.144 U µg/Kg 0.144 µg/Kg9/20/2001 15-17-092001 611552 4756404 15 0308028-10 Cl4-BZ#81 0.142 U µg/Kg 0.142 µg/Kg9/20/2001 15-17-092001 611552 4756404 15 0308028-10 Cl5-BZ#87 1.78 µg/Kg 0.0635 µg/Kg9/20/2001 15-17-092001 611552 4756404 15 0308028-10 Cl5-BZ#95 0.156 J µg/Kg 0.0491 µg/Kg9/20/2001 15-17-092001 611552 4756404 15 0308028-10 Cl5-BZ#99 5.69 µg/Kg 0.0335 µg/Kg9/20/2001 15-17-092001 611552 4756404 15 0308028-10 Cl5-BZ#101 0.623 µg/Kg 0.0958 µg/Kg9/20/2001 15-17-092001 611552 4756404 15 0308028-10 Cl5-BZ#105 3.96 µg/Kg 0.0467 µg/Kg9/20/2001 15-17-092001 611552 4756404 15 0308028-10 Cl5-BZ#110 0.245 J µg/Kg 0.0910 µg/Kg9/20/2001 15-17-092001 611552 4756404 15 0308028-10 Cl5-BZ#114 0.389 µg/Kg 0.0419 µg/Kg9/20/2001 15-17-092001 611552 4756404 15 0308028-10 Cl5-BZ#118 8.53 µg/Kg 0.0982 µg/Kg



Extracted 7/30/04




SITE NUMBER



9/20/2001 15-17-092001 611552 4756404 15 0308028-10 Cl5-BZ#123 0.0826 U µg/Kg 0.0826 µg/Kg9/20/2001 15-17-092001 611552 4756404 15 0308028-10 Cl5-BZ#126 0.0730 U µg/Kg 0.0730 µg/Kg9/20/2001 15-17-092001 611552 4756404 15 0308028-10 Cl6-BZ#128 0.748 µg/Kg 0.0659 µg/Kg9/20/2001 15-17-092001 611552 4756404 15 0308028-10 Cl6-BZ#138 10.2 µg/Kg 0.0946 µg/Kg9/20/2001 15-17-092001 611552 4756404 15 0308028-10 Cl6-BZ#146 1.11 µg/Kg 0.0599 µg/Kg9/20/2001 15-17-092001 611552 4756404 15 0308028-10 Cl6-BZ#149 0.150 J µg/Kg 0.0766 µg/Kg9/20/2001 15-17-092001 611552 4756404 15 0308028-10 Cl6-BZ#151 0.127 U µg/Kg 0.127 µg/Kg9/20/2001 15-17-092001 611552 4756404 15 0308028-10 Cl6-BZ#153 9.86 µg/Kg 0.109 µg/Kg9/20/2001 15-17-092001 611552 4756404 15 0308028-10 Cl6-BZ#156 1.06 µg/Kg 0.0778 µg/Kg9/20/2001 15-17-092001 611552 4756404 15 0308028-10 Cl6-BZ#157 0.221 J µg/Kg 0.0611 µg/Kg9/20/2001 15-17-092001 611552 4756404 15 0308028-10 Cl6-BZ#158 0.311 µg/Kg 0.0515 µg/Kg9/20/2001 15-17-092001 611552 4756404 15 0308028-10 Cl6-BZ#167 0.491 µg/Kg 0.0659 µg/Kg9/20/2001 15-17-092001 611552 4756404 15 0308028-10 Cl6-BZ#169 0.212 U µg/Kg 0.212 µg/Kg9/20/2001 15-17-092001 611552 4756404 15 0308028-10 Cl7-BZ#170 0.247 U µg/Kg 0.247 µg/Kg9/20/2001 15-17-092001 611552 4756404 15 0308028-10 Cl7-BZ#174 0.0503 U µg/Kg 0.0503 µg/Kg9/20/2001 15-17-092001 611552 4756404 15 0308028-10 Cl7-BZ#177 0.0706 U µg/Kg 0.0706 µg/Kg9/20/2001 15-17-092001 611552 4756404 15 0308028-10 Cl7-BZ#180 3.40 µg/Kg 0.105 µg/Kg9/20/2001 15-17-092001 611552 4756404 15 0308028-10 Cl7-BZ#183 0.497 µg/Kg 0.0479 µg/Kg9/20/2001 15-17-092001 611552 4756404 15 0308028-10 Cl7-BZ#187 0.868 µg/Kg 0.0527 µg/Kg9/20/2001 15-17-092001 611552 4756404 15 0308028-10 Cl7-BZ#189 0.0946 U µg/Kg 0.0946 µg/Kg9/20/2001 15-17-092001 611552 4756404 15 0308028-10 Cl8-BZ#194 1.12 µg/Kg 0.110 µg/Kg9/20/2001 15-17-092001 611552 4756404 15 0308028-10 Cl8-BZ#195 0.109 U µg/Kg 0.109 µg/Kg9/20/2001 15-17-092001 611552 4756404 15 0308028-10 Cl8-BZ#201 0.587 µg/Kg 0.0958 µg/Kg9/20/2001 15-17-092001 611552 4756404 15 0308028-10 Cl9-BZ#206 1.06 µg/Kg 0.128 µg/Kg9/20/2001 15-17-092001 611552 4756404 15 0308028-10 Cl10-BZ#209 0.275 J µg/Kg 0.0599 µg/Kg9/20/2001 15-17-092001 611552 4756404 15 0308028-10 Monochlorobiphenyls 3.52 U µg/Kg 3.52 µg/Kg9/20/2001 15-17-092001 611552 4756404 15 0308028-10 Dichlorobiphenyls 0.103 U µg/Kg 0.103 µg/Kg9/20/2001 15-17-092001 611552 4756404 15 0308028-10 Trichlorobiphenyls 2.42 µg/Kg 0.353 µg/Kg9/20/2001 15-17-092001 611552 4756404 15 0308028-10 Tetrachlorobiphenyls 18.3 µg/Kg 0.0551 µg/Kg9/20/2001 15-17-092001 611552 4756404 15 0308028-10 Pentachlorobiphenyls 35.8 µg/Kg 0.0635 µg/Kg9/20/2001 15-17-092001 611552 4756404 15 0308028-10 Hexachlorobiphenyls 27.4 µg/Kg 0.101 µg/Kg9/20/2001 15-17-092001 611552 4756404 15 0308028-10 Heptachlorobiphenyls 1.25 µg/Kg 0.0551 µg/Kg9/20/2001 15-17-092001 611552 4756404 15 0308028-10 Octachlorobiphenyls 8.77 µg/Kg 0.0503 µg/Kg9/20/2001 15-17-092001 611552 4756404 15 0308028-10 Nonachlorobiphenyls 1.06 µg/Kg 0.128 µg/Kg



Extracted 7/30/04




SITE NUMBER



9/20/2001 15-17-092001 611552 4756404 15 0308028-10 Decachlorobiphenyl 0.275 J µg/Kg 0.0599 µg/Kg9/20/2001 15-17-092001 611552 4756404 15 0308028-10 Total Homologs 95.3 µg/Kg 0.0599 µg/Kg9/20/2001 15-17-092001 611552 4756404 15 0308028-10 Percent Lipids 2.6 % 0.1 %9/20/2001 15-17-092001 611552 4756404 15 0308028-10 Percent Moisture 71.9 % 0.1 %9/20/2001 15-21-092001 611552 4756404 15 0308028-11 Cl2-BZ#8 0.122 U µg/Kg 0.122 µg/Kg9/20/2001 15-21-092001 611552 4756404 15 0308028-11 Cl3-BZ#18 0.270 U µg/Kg 0.270 µg/Kg9/20/2001 15-21-092001 611552 4756404 15 0308028-11 Cl3-BZ#31/#28 3.08 J µg/Kg 1.95 µg/Kg9/20/2001 15-21-092001 611552 4756404 15 0308028-11 Cl4-BZ#44 0.304 J µg/Kg 0.185 µg/Kg9/20/2001 15-21-092001 611552 4756404 15 0308028-11 Cl4-BZ#45 0.248 U µg/Kg 0.248 µg/Kg9/20/2001 15-21-092001 611552 4756404 15 0308028-11 Cl4-BZ#47 11.3 µg/Kg 0.314 µg/Kg9/20/2001 15-21-092001 611552 4756404 15 0308028-11 Cl4-BZ#49 0.644 J µg/Kg 0.154 µg/Kg9/20/2001 15-21-092001 611552 4756404 15 0308028-11 Cl4-BZ#52 1.08 µg/Kg 0.176 µg/Kg9/20/2001 15-21-092001 611552 4756404 15 0308028-11 Cl4-BZ#56 1.25 µg/Kg 0.0920 µg/Kg9/20/2001 15-21-092001 611552 4756404 15 0308028-11 Cl4-BZ#66 5.03 µg/Kg 0.123 µg/Kg9/20/2001 15-21-092001 611552 4756404 15 0308028-11 Cl4-BZ#70 1.49 µg/Kg 0.108 µg/Kg9/20/2001 15-21-092001 611552 4756404 15 0308028-11 Cl4-BZ#74 6.23 µg/Kg 0.190 µg/Kg9/20/2001 15-21-092001 611552 4756404 15 0308028-11 Cl4-BZ#77 0.170 U µg/Kg 0.170 µg/Kg9/20/2001 15-21-092001 611552 4756404 15 0308028-11 Cl4-BZ#81 0.168 U µg/Kg 0.168 µg/Kg9/20/2001 15-21-092001 611552 4756404 15 0308028-11 Cl5-BZ#87 2.22 µg/Kg 0.0750 µg/Kg9/20/2001 15-21-092001 611552 4756404 15 0308028-11 Cl5-BZ#95 0.318 µg/Kg 0.0580 µg/Kg9/20/2001 15-21-092001 611552 4756404 15 0308028-11 Cl5-BZ#99 28.9 µg/Kg 0.0396 µg/Kg9/20/2001 15-21-092001 611552 4756404 15 0308028-11 Cl5-BZ#101 1.03 µg/Kg 0.113 µg/Kg9/20/2001 15-21-092001 611552 4756404 15 0308028-11 Cl5-BZ#105 5.05 µg/Kg 0.0552 µg/Kg9/20/2001 15-21-092001 611552 4756404 15 0308028-11 Cl5-BZ#110 0.736 µg/Kg 0.108 µg/Kg9/20/2001 15-21-092001 611552 4756404 15 0308028-11 Cl5-BZ#114 0.771 µg/Kg 0.0495 µg/Kg9/20/2001 15-21-092001 611552 4756404 15 0308028-11 Cl5-BZ#118 21.6 µg/Kg 0.116 µg/Kg9/20/2001 15-21-092001 611552 4756404 15 0308028-11 Cl5-BZ#123 0.0977 U µg/Kg 0.0977 µg/Kg9/20/2001 15-21-092001 611552 4756404 15 0308028-11 Cl5-BZ#126 0.0863 U µg/Kg 0.0863 µg/Kg9/20/2001 15-21-092001 611552 4756404 15 0308028-11 Cl6-BZ#128 5.68 µg/Kg 0.0778 µg/Kg9/20/2001 15-21-092001 611552 4756404 15 0308028-11 Cl6-BZ#138 55.0 µg/Kg 0.112 µg/Kg9/20/2001 15-21-092001 611552 4756404 15 0308028-11 Cl6-BZ#146 6.90 µg/Kg 0.0708 µg/Kg9/20/2001 15-21-092001 611552 4756404 15 0308028-11 Cl6-BZ#149 0.686 µg/Kg 0.0906 µg/Kg9/20/2001 15-21-092001 611552 4756404 15 0308028-11 Cl6-BZ#151 0.198 J µg/Kg 0.150 µg/Kg9/20/2001 15-21-092001 611552 4756404 15 0308028-11 Cl6-BZ#153 47.1 µg/Kg 0.129 µg/Kg



Extracted 7/30/04




SITE NUMBER



9/20/2001 15-21-092001 611552 4756404 15 0308028-11 Cl6-BZ#156 3.88 µg/Kg 0.0920 µg/Kg9/20/2001 15-21-092001 611552 4756404 15 0308028-11 Cl6-BZ#157 0.644 µg/Kg 0.0722 µg/Kg9/20/2001 15-21-092001 611552 4756404 15 0308028-11 Cl6-BZ#158 1.41 µg/Kg 0.0609 µg/Kg9/20/2001 15-21-092001 611552 4756404 15 0308028-11 Cl6-BZ#167 1.09 µg/Kg 0.0778 µg/Kg9/20/2001 15-21-092001 611552 4756404 15 0308028-11 Cl6-BZ#169 0.250 U µg/Kg 0.250 µg/Kg9/20/2001 15-21-092001 611552 4756404 15 0308028-11 Cl7-BZ#170 0.292 U µg/Kg 0.292 µg/Kg9/20/2001 15-21-092001 611552 4756404 15 0308028-11 Cl7-BZ#174 0.0594 U µg/Kg 0.0594 µg/Kg9/20/2001 15-21-092001 611552 4756404 15 0308028-11 Cl7-BZ#177 0.0835 U µg/Kg 0.0835 µg/Kg9/20/2001 15-21-092001 611552 4756404 15 0308028-11 Cl7-BZ#180 10.6 µg/Kg 0.124 µg/Kg9/20/2001 15-21-092001 611552 4756404 15 0308028-11 Cl7-BZ#183 3.22 µg/Kg 0.0566 µg/Kg9/20/2001 15-21-092001 611552 4756404 15 0308028-11 Cl7-BZ#187 20.2 µg/Kg 0.0623 µg/Kg9/20/2001 15-21-092001 611552 4756404 15 0308028-11 Cl7-BZ#189 0.112 U µg/Kg 0.112 µg/Kg9/20/2001 15-21-092001 611552 4756404 15 0308028-11 Cl8-BZ#194 1.37 µg/Kg 0.130 µg/Kg9/20/2001 15-21-092001 611552 4756404 15 0308028-11 Cl8-BZ#195 0.129 U µg/Kg 0.129 µg/Kg9/20/2001 15-21-092001 611552 4756404 15 0308028-11 Cl8-BZ#201 3.25 µg/Kg 0.113 µg/Kg9/20/2001 15-21-092001 611552 4756404 15 0308028-11 Cl9-BZ#206 2.19 µg/Kg 0.151 µg/Kg9/20/2001 15-21-092001 611552 4756404 15 0308028-11 Cl10-BZ#209 0.623 µg/Kg 0.0708 µg/Kg9/20/2001 15-21-092001 611552 4756404 15 0308028-11 Monochlorobiphenyls 4.16 U µg/Kg 4.16 µg/Kg9/20/2001 15-21-092001 611552 4756404 15 0308028-11 Dichlorobiphenyls 0.122 U µg/Kg 0.122 µg/Kg9/20/2001 15-21-092001 611552 4756404 15 0308028-11 Trichlorobiphenyls 10.6 µg/Kg 0.417 µg/Kg9/20/2001 15-21-092001 611552 4756404 15 0308028-11 Tetrachlorobiphenyls 38.6 µg/Kg 0.0651 µg/Kg9/20/2001 15-21-092001 611552 4756404 15 0308028-11 Pentachlorobiphenyls 101 µg/Kg 0.0750 µg/Kg9/20/2001 15-21-092001 611552 4756404 15 0308028-11 Hexachlorobiphenyls 136 µg/Kg 0.119 µg/Kg9/20/2001 15-21-092001 611552 4756404 15 0308028-11 Heptachlorobiphenyls 19.0 µg/Kg 0.0651 µg/Kg9/20/2001 15-21-092001 611552 4756404 15 0308028-11 Octachlorobiphenyls 11.8 µg/Kg 0.0594 µg/Kg9/20/2001 15-21-092001 611552 4756404 15 0308028-11 Nonachlorobiphenyls 2.19 µg/Kg 0.151 µg/Kg9/20/2001 15-21-092001 611552 4756404 15 0308028-11 Decachlorobiphenyl 0.623 µg/Kg 0.0708 µg/Kg9/20/2001 15-21-092001 611552 4756404 15 0308028-11 Total Homologs 320 µg/Kg 0.0708 µg/Kg9/20/2001 15-21-092001 611552 4756404 15 0308028-11 Percent Lipids 3.0 % 0.1 %9/20/2001 15-21-092001 611552 4756404 15 0308028-11 Percent Moisture 71.6 % 0.1 %9/20/2001 15-22-092001 611552 4756404 15 0308028-12 Cl2-BZ#8 0.0975 U µg/Kg 0.0975 µg/Kg9/20/2001 15-22-092001 611552 4756404 15 0308028-12 Cl3-BZ#18 0.216 U µg/Kg 0.216 µg/Kg9/20/2001 15-22-092001 611552 4756404 15 0308028-12 Cl3-BZ#31/#28 5.97 J µg/Kg 1.56 µg/Kg9/20/2001 15-22-092001 611552 4756404 15 0308028-12 Cl4-BZ#44 0.148 U µg/Kg 0.148 µg/Kg



Extracted 7/30/04




SITE NUMBER



9/20/2001 15-22-092001 611552 4756404 15 0308028-12 Cl4-BZ#45 0.232 J µg/Kg 0.198 µg/Kg9/20/2001 15-22-092001 611552 4756404 15 0308028-12 Cl4-BZ#47 1.52 µg/Kg 0.252 µg/Kg9/20/2001 15-22-092001 611552 4756404 15 0308028-12 Cl4-BZ#49 0.255 J µg/Kg 0.123 µg/Kg9/20/2001 15-22-092001 611552 4756404 15 0308028-12 Cl4-BZ#52 0.368 J µg/Kg 0.140 µg/Kg9/20/2001 15-22-092001 611552 4756404 15 0308028-12 Cl4-BZ#56 0.368 J µg/Kg 0.0737 µg/Kg9/20/2001 15-22-092001 611552 4756404 15 0308028-12 Cl4-BZ#66 0.895 µg/Kg 0.0986 µg/Kg9/20/2001 15-22-092001 611552 4756404 15 0308028-12 Cl4-BZ#70 0.493 µg/Kg 0.0861 µg/Kg9/20/2001 15-22-092001 611552 4756404 15 0308028-12 Cl4-BZ#74 0.742 J µg/Kg 0.152 µg/Kg9/20/2001 15-22-092001 611552 4756404 15 0308028-12 Cl4-BZ#77 0.136 U µg/Kg 0.136 µg/Kg9/20/2001 15-22-092001 611552 4756404 15 0308028-12 Cl4-BZ#81 0.135 U µg/Kg 0.135 µg/Kg9/20/2001 15-22-092001 611552 4756404 15 0308028-12 Cl5-BZ#87 0.980 µg/Kg 0.0601 µg/Kg9/20/2001 15-22-092001 611552 4756404 15 0308028-12 Cl5-BZ#95 0.130 J µg/Kg 0.0465 µg/Kg9/20/2001 15-22-092001 611552 4756404 15 0308028-12 Cl5-BZ#99 3.91 µg/Kg 0.0317 µg/Kg9/20/2001 15-22-092001 611552 4756404 15 0308028-12 Cl5-BZ#101 0.459 µg/Kg 0.0907 µg/Kg9/20/2001 15-22-092001 611552 4756404 15 0308028-12 Cl5-BZ#105 1.26 µg/Kg 0.0442 µg/Kg9/20/2001 15-22-092001 611552 4756404 15 0308028-12 Cl5-BZ#110 0.221 J µg/Kg 0.0861 µg/Kg9/20/2001 15-22-092001 611552 4756404 15 0308028-12 Cl5-BZ#114 0.210 µg/Kg 0.0397 µg/Kg9/20/2001 15-22-092001 611552 4756404 15 0308028-12 Cl5-BZ#118 4.52 µg/Kg 0.0929 µg/Kg9/20/2001 15-22-092001 611552 4756404 15 0308028-12 Cl5-BZ#123 0.0782 U µg/Kg 0.0782 µg/Kg9/20/2001 15-22-092001 611552 4756404 15 0308028-12 Cl5-BZ#126 0.0691 U µg/Kg 0.0691 µg/Kg9/20/2001 15-22-092001 611552 4756404 15 0308028-12 Cl6-BZ#128 0.465 µg/Kg 0.0623 µg/Kg9/20/2001 15-22-092001 611552 4756404 15 0308028-12 Cl6-BZ#138 7.84 µg/Kg 0.0895 µg/Kg9/20/2001 15-22-092001 611552 4756404 15 0308028-12 Cl6-BZ#146 0.992 µg/Kg 0.0567 µg/Kg9/20/2001 15-22-092001 611552 4756404 15 0308028-12 Cl6-BZ#149 0.142 J µg/Kg 0.0725 µg/Kg9/20/2001 15-22-092001 611552 4756404 15 0308028-12 Cl6-BZ#151 0.120 U µg/Kg 0.120 µg/Kg9/20/2001 15-22-092001 611552 4756404 15 0308028-12 Cl6-BZ#153 8.18 µg/Kg 0.103 µg/Kg9/20/2001 15-22-092001 611552 4756404 15 0308028-12 Cl6-BZ#156 0.833 µg/Kg 0.0737 µg/Kg9/20/2001 15-22-092001 611552 4756404 15 0308028-12 Cl6-BZ#157 0.193 J µg/Kg 0.0578 µg/Kg9/20/2001 15-22-092001 611552 4756404 15 0308028-12 Cl6-BZ#158 0.176 J µg/Kg 0.0487 µg/Kg9/20/2001 15-22-092001 611552 4756404 15 0308028-12 Cl6-BZ#167 0.357 µg/Kg 0.0623 µg/Kg9/20/2001 15-22-092001 611552 4756404 15 0308028-12 Cl6-BZ#169 0.201 U µg/Kg 0.201 µg/Kg9/20/2001 15-22-092001 611552 4756404 15 0308028-12 Cl7-BZ#170 0.234 U µg/Kg 0.234 µg/Kg9/20/2001 15-22-092001 611552 4756404 15 0308028-12 Cl7-BZ#174 0.0476 U µg/Kg 0.0476 µg/Kg9/20/2001 15-22-092001 611552 4756404 15 0308028-12 Cl7-BZ#177 0.0669 U µg/Kg 0.0669 µg/Kg



Extracted 7/30/04




SITE NUMBER



9/20/2001 15-22-092001 611552 4756404 15 0308028-12 Cl7-BZ#180 4.30 µg/Kg 0.0997 µg/Kg9/20/2001 15-22-092001 611552 4756404 15 0308028-12 Cl7-BZ#183 0.595 µg/Kg 0.0453 µg/Kg9/20/2001 15-22-092001 611552 4756404 15 0308028-12 Cl7-BZ#187 0.924 µg/Kg 0.0499 µg/Kg9/20/2001 15-22-092001 611552 4756404 15 0308028-12 Cl7-BZ#189 0.0895 U µg/Kg 0.0895 µg/Kg9/20/2001 15-22-092001 611552 4756404 15 0308028-12 Cl8-BZ#194 0.595 µg/Kg 0.104 µg/Kg9/20/2001 15-22-092001 611552 4756404 15 0308028-12 Cl8-BZ#195 0.103 U µg/Kg 0.103 µg/Kg9/20/2001 15-22-092001 611552 4756404 15 0308028-12 Cl8-BZ#201 0.504 µg/Kg 0.0907 µg/Kg9/20/2001 15-22-092001 611552 4756404 15 0308028-12 Cl9-BZ#206 0.538 J µg/Kg 0.121 µg/Kg9/20/2001 15-22-092001 611552 4756404 15 0308028-12 Cl10-BZ#209 0.0963 J µg/Kg 0.0567 µg/Kg9/20/2001 15-22-092001 611552 4756404 15 0308028-12 Monochlorobiphenyls 3.33 U µg/Kg 3.33 µg/Kg9/20/2001 15-22-092001 611552 4756404 15 0308028-12 Dichlorobiphenyls 0.0975 U µg/Kg 0.0975 µg/Kg9/20/2001 15-22-092001 611552 4756404 15 0308028-12 Trichlorobiphenyls 9.19 µg/Kg 0.334 µg/Kg9/20/2001 15-22-092001 611552 4756404 15 0308028-12 Tetrachlorobiphenyls 11.0 µg/Kg 0.0521 µg/Kg9/20/2001 15-22-092001 611552 4756404 15 0308028-12 Pentachlorobiphenyls 18.7 µg/Kg 0.0601 µg/Kg9/20/2001 15-22-092001 611552 4756404 15 0308028-12 Hexachlorobiphenyls 20.9 µg/Kg 0.0952 µg/Kg9/20/2001 15-22-092001 611552 4756404 15 0308028-12 Heptachlorobiphenyls 1.22 µg/Kg 0.0521 µg/Kg9/20/2001 15-22-092001 611552 4756404 15 0308028-12 Octachlorobiphenyls 3.88 µg/Kg 0.0476 µg/Kg9/20/2001 15-22-092001 611552 4756404 15 0308028-12 Nonachlorobiphenyls 0.538 J µg/Kg 0.121 µg/Kg9/20/2001 15-22-092001 611552 4756404 15 0308028-12 Decachlorobiphenyl 0.0963 J µg/Kg 0.0567 µg/Kg9/20/2001 15-22-092001 611552 4756404 15 0308028-12 Total Homologs 65.4 µg/Kg 0.0567 µg/Kg9/20/2001 15-22-092001 611552 4756404 15 0308028-12 Percent Lipids 4.6 % 0.1 %9/20/2001 15-22-092001 611552 4756404 15 0308028-12 Percent Moisture 70.1 % 0.1 %9/18/2001 16-05-091801 609620 4754219 16 0308028-13 Cl2-BZ#8 0.141 U µg/Kg 0.141 µg/Kg9/18/2001 16-05-091801 609620 4754219 16 0308028-13 Cl3-BZ#18 0.314 U µg/Kg 0.314 µg/Kg9/18/2001 16-05-091801 609620 4754219 16 0308028-13 Cl3-BZ#31/#28 46.1 µg/Kg 2.26 µg/Kg9/18/2001 16-05-091801 609620 4754219 16 0308028-13 Cl4-BZ#44 13.3 µg/Kg 0.215 µg/Kg9/18/2001 16-05-091801 609620 4754219 16 0308028-13 Cl4-BZ#45 0.287 U µg/Kg 0.287 µg/Kg9/18/2001 16-05-091801 609620 4754219 16 0308028-13 Cl4-BZ#47 184 µg/Kg 0.365 µg/Kg9/18/2001 16-05-091801 609620 4754219 16 0308028-13 Cl4-BZ#49 32.4 µg/Kg 0.179 µg/Kg9/18/2001 16-05-091801 609620 4754219 16 0308028-13 Cl4-BZ#52 94.5 µg/Kg 0.204 µg/Kg9/18/2001 16-05-091801 609620 4754219 16 0308028-13 Cl4-BZ#56 44.6 µg/Kg 0.107 µg/Kg9/18/2001 16-05-091801 609620 4754219 16 0308028-13 Cl4-BZ#66 140 µg/Kg 0.143 µg/Kg9/18/2001 16-05-091801 609620 4754219 16 0308028-13 Cl4-BZ#70 68.4 µg/Kg 0.125 µg/Kg9/18/2001 16-05-091801 609620 4754219 16 0308028-13 Cl4-BZ#74 174 µg/Kg 0.220 µg/Kg



Extracted 7/30/04




SITE NUMBER



9/18/2001 16-05-091801 609620 4754219 16 0308028-13 Cl4-BZ#77 0.197 U µg/Kg 0.197 µg/Kg9/18/2001 16-05-091801 609620 4754219 16 0308028-13 Cl4-BZ#81 0.196 U µg/Kg 0.196 µg/Kg9/18/2001 16-05-091801 609620 4754219 16 0308028-13 Cl5-BZ#87 110 µg/Kg 0.0871 µg/Kg9/18/2001 16-05-091801 609620 4754219 16 0308028-13 Cl5-BZ#95 14.1 µg/Kg 0.0673 µg/Kg9/18/2001 16-05-091801 609620 4754219 16 0308028-13 Cl5-BZ#99 639 µg/Kg 0.223 µg/Kg9/18/2001 16-05-091801 609620 4754219 16 0308028-13 Cl5-BZ#101 79.4 µg/Kg 0.131 µg/Kg9/18/2001 16-05-091801 609620 4754219 16 0308028-13 Cl5-BZ#105 257 µg/Kg 0.0641 µg/Kg9/18/2001 16-05-091801 609620 4754219 16 0308028-13 Cl5-BZ#110 68.0 µg/Kg 0.125 µg/Kg9/18/2001 16-05-091801 609620 4754219 16 0308028-13 Cl5-BZ#114 14.7 µg/Kg 0.0575 µg/Kg9/18/2001 16-05-091801 609620 4754219 16 0308028-13 Cl5-BZ#118 770 µg/Kg 0.653 µg/Kg9/18/2001 16-05-091801 609620 4754219 16 0308028-13 Cl5-BZ#123 0.113 U µg/Kg 0.113 µg/Kg9/18/2001 16-05-091801 609620 4754219 16 0308028-13 Cl5-BZ#126 1.84 NJ µg/Kg 0.100 µg/Kg9/18/2001 16-05-091801 609620 4754219 16 0308028-13 Cl6-BZ#128 92.2 µg/Kg 0.0903 µg/Kg9/18/2001 16-05-091801 609620 4754219 16 0308028-13 Cl6-BZ#138 951 µg/Kg 0.629 µg/Kg9/18/2001 16-05-091801 609620 4754219 16 0308028-13 Cl6-BZ#146 129 µg/Kg 0.0821 µg/Kg9/18/2001 16-05-091801 609620 4754219 16 0308028-13 Cl6-BZ#149 38.0 µg/Kg 0.105 µg/Kg9/18/2001 16-05-091801 609620 4754219 16 0308028-13 Cl6-BZ#151 5.22 µg/Kg 0.174 µg/Kg9/18/2001 16-05-091801 609620 4754219 16 0308028-13 Cl6-BZ#153 866 µg/Kg 0.725 µg/Kg9/18/2001 16-05-091801 609620 4754219 16 0308028-13 Cl6-BZ#156 72.7 µg/Kg 0.107 µg/Kg9/18/2001 16-05-091801 609620 4754219 16 0308028-13 Cl6-BZ#157 13.4 µg/Kg 0.0838 µg/Kg9/18/2001 16-05-091801 609620 4754219 16 0308028-13 Cl6-BZ#158 18.6 µg/Kg 0.0706 µg/Kg9/18/2001 16-05-091801 609620 4754219 16 0308028-13 Cl6-BZ#167 33.7 µg/Kg 0.0903 µg/Kg9/18/2001 16-05-091801 609620 4754219 16 0308028-13 Cl6-BZ#169 0.291 U µg/Kg 0.291 µg/Kg9/18/2001 16-05-091801 609620 4754219 16 0308028-13 Cl7-BZ#170 106 µg/Kg 0.338 µg/Kg9/18/2001 16-05-091801 609620 4754219 16 0308028-13 Cl7-BZ#174 5.10 µg/Kg 0.0690 µg/Kg9/18/2001 16-05-091801 609620 4754219 16 0308028-13 Cl7-BZ#177 19.1 µg/Kg 0.0969 µg/Kg9/18/2001 16-05-091801 609620 4754219 16 0308028-13 Cl7-BZ#180 186 µg/Kg 0.145 µg/Kg9/18/2001 16-05-091801 609620 4754219 16 0308028-13 Cl7-BZ#183 33.7 µg/Kg 0.0657 µg/Kg9/18/2001 16-05-091801 609620 4754219 16 0308028-13 Cl7-BZ#187 242 µg/Kg 0.0723 µg/Kg9/18/2001 16-05-091801 609620 4754219 16 0308028-13 Cl7-BZ#189 0.130 U µg/Kg 0.130 µg/Kg9/18/2001 16-05-091801 609620 4754219 16 0308028-13 Cl8-BZ#194 18.0 µg/Kg 0.151 µg/Kg9/18/2001 16-05-091801 609620 4754219 16 0308028-13 Cl8-BZ#195 11.6 µg/Kg 0.149 µg/Kg9/18/2001 16-05-091801 609620 4754219 16 0308028-13 Cl8-BZ#201 35.1 µg/Kg 0.131 µg/Kg9/18/2001 16-05-091801 609620 4754219 16 0308028-13 Cl9-BZ#206 28.3 µg/Kg 0.176 µg/Kg



Extracted 7/30/04




SITE NUMBER



9/18/2001 16-05-091801 609620 4754219 16 0308028-13 Cl10-BZ#209 3.34 µg/Kg 0.0821 µg/Kg9/18/2001 16-05-091801 609620 4754219 16 0308028-13 Monochlorobiphenyls 4.83 U µg/Kg 4.83 µg/Kg9/18/2001 16-05-091801 609620 4754219 16 0308028-13 Dichlorobiphenyls 0.141 U µg/Kg 0.141 µg/Kg9/18/2001 16-05-091801 609620 4754219 16 0308028-13 Trichlorobiphenyls 40.6 µg/Kg 0.485 µg/Kg9/18/2001 16-05-091801 609620 4754219 16 0308028-13 Tetrachlorobiphenyls 875 µg/Kg 0.0756 µg/Kg9/18/2001 16-05-091801 609620 4754219 16 0308028-13 Pentachlorobiphenyls 3320 µg/Kg 0.422 µg/Kg9/18/2001 16-05-091801 609620 4754219 16 0308028-13 Hexachlorobiphenyls 2520 µg/Kg 0.669 µg/Kg9/18/2001 16-05-091801 609620 4754219 16 0308028-13 Heptachlorobiphenyls 575 µg/Kg 0.0756 µg/Kg9/18/2001 16-05-091801 609620 4754219 16 0308028-13 Octachlorobiphenyls 111 µg/Kg 0.0690 µg/Kg9/18/2001 16-05-091801 609620 4754219 16 0308028-13 Nonachlorobiphenyls 28.3 µg/Kg 0.176 µg/Kg9/18/2001 16-05-091801 609620 4754219 16 0308028-13 Decachlorobiphenyl 3.34 µg/Kg 0.0821 µg/Kg9/18/2001 16-05-091801 609620 4754219 16 0308028-13 Total Homologs 7700 µg/Kg 0.398 µg/Kg9/18/2001 16-05-091801 609620 4754219 16 0308028-13 Percent Lipids 2.2 % 0.1 %9/18/2001 16-05-091801 609620 4754219 16 0308028-13 Percent Moisture 70.9 % 0.1 %9/18/2001 16-08-091801 609620 4754219 16 0308028-14 Cl2-BZ#8 0.138 U µg/Kg 0.138 µg/Kg9/18/2001 16-08-091801 609620 4754219 16 0308028-14 Cl3-BZ#18 0.307 U µg/Kg 0.307 µg/Kg9/18/2001 16-08-091801 609620 4754219 16 0308028-14 Cl3-BZ#31/#28 23.3 µg/Kg 2.22 µg/Kg9/18/2001 16-08-091801 609620 4754219 16 0308028-14 Cl4-BZ#44 2.05 µg/Kg 0.211 µg/Kg9/18/2001 16-08-091801 609620 4754219 16 0308028-14 Cl4-BZ#45 0.282 U µg/Kg 0.282 µg/Kg9/18/2001 16-08-091801 609620 4754219 16 0308028-14 Cl4-BZ#47 21.1 µg/Kg 0.357 µg/Kg9/18/2001 16-08-091801 609620 4754219 16 0308028-14 Cl4-BZ#49 2.74 µg/Kg 0.175 µg/Kg9/18/2001 16-08-091801 609620 4754219 16 0308028-14 Cl4-BZ#52 5.09 µg/Kg 0.199 µg/Kg9/18/2001 16-08-091801 609620 4754219 16 0308028-14 Cl4-BZ#56 27.6 µg/Kg 0.105 µg/Kg9/18/2001 16-08-091801 609620 4754219 16 0308028-14 Cl4-BZ#66 86.2 µg/Kg 0.140 µg/Kg9/18/2001 16-08-091801 609620 4754219 16 0308028-14 Cl4-BZ#70 8.16 µg/Kg 0.122 µg/Kg9/18/2001 16-08-091801 609620 4754219 16 0308028-14 Cl4-BZ#74 88.2 µg/Kg 0.216 µg/Kg9/18/2001 16-08-091801 609620 4754219 16 0308028-14 Cl4-BZ#77 0.193 U µg/Kg 0.193 µg/Kg9/18/2001 16-08-091801 609620 4754219 16 0308028-14 Cl4-BZ#81 0.191 U µg/Kg 0.191 µg/Kg9/18/2001 16-08-091801 609620 4754219 16 0308028-14 Cl5-BZ#87 16.5 J µg/Kg 0.0853 µg/Kg9/18/2001 16-08-091801 609620 4754219 16 0308028-14 Cl5-BZ#95 1.27 µg/Kg 0.0660 µg/Kg9/18/2001 16-08-091801 609620 4754219 16 0308028-14 Cl5-BZ#99 157 µg/Kg 0.0450 µg/Kg9/18/2001 16-08-091801 609620 4754219 16 0308028-14 Cl5-BZ#101 6.35 µg/Kg 0.129 µg/Kg9/18/2001 16-08-091801 609620 4754219 16 0308028-14 Cl5-BZ#105 102 µg/Kg 0.0627 µg/Kg9/18/2001 16-08-091801 609620 4754219 16 0308028-14 Cl5-BZ#110 2.63 µg/Kg 0.122 µg/Kg



Extracted 7/30/04




SITE NUMBER



9/18/2001 16-08-091801 609620 4754219 16 0308028-14 Cl5-BZ#114 6.64 µg/Kg 0.0563 µg/Kg9/18/2001 16-08-091801 609620 4754219 16 0308028-14 Cl5-BZ#118 241 µg/Kg 0.132 µg/Kg9/18/2001 16-08-091801 609620 4754219 16 0308028-14 Cl5-BZ#123 0.111 U µg/Kg 0.111 µg/Kg9/18/2001 16-08-091801 609620 4754219 16 0308028-14 Cl5-BZ#126 0.0981 U µg/Kg 0.0981 µg/Kg9/18/2001 16-08-091801 609620 4754219 16 0308028-14 Cl6-BZ#128 34.3 J µg/Kg 0.0885 µg/Kg9/18/2001 16-08-091801 609620 4754219 16 0308028-14 Cl6-BZ#138 281 µg/Kg 0.127 µg/Kg9/18/2001 16-08-091801 609620 4754219 16 0308028-14 Cl6-BZ#146 36.4 µg/Kg 0.0804 µg/Kg9/18/2001 16-08-091801 609620 4754219 16 0308028-14 Cl6-BZ#149 2.33 µg/Kg 0.103 µg/Kg9/18/2001 16-08-091801 609620 4754219 16 0308028-14 Cl6-BZ#151 0.257 J µg/Kg 0.170 µg/Kg9/18/2001 16-08-091801 609620 4754219 16 0308028-14 Cl6-BZ#153 255 µg/Kg 0.146 µg/Kg9/18/2001 16-08-091801 609620 4754219 16 0308028-14 Cl6-BZ#156 21.3 µg/Kg 0.105 µg/Kg9/18/2001 16-08-091801 609620 4754219 16 0308028-14 Cl6-BZ#157 4.26 µg/Kg 0.0821 µg/Kg9/18/2001 16-08-091801 609620 4754219 16 0308028-14 Cl6-BZ#158 6.00 J µg/Kg 0.0692 µg/Kg9/18/2001 16-08-091801 609620 4754219 16 0308028-14 Cl6-BZ#167 13.6 µg/Kg 0.0885 µg/Kg9/18/2001 16-08-091801 609620 4754219 16 0308028-14 Cl6-BZ#169 0.285 U µg/Kg 0.285 µg/Kg9/18/2001 16-08-091801 609620 4754219 16 0308028-14 Cl7-BZ#170 35.8 µg/Kg 0.331 µg/Kg9/18/2001 16-08-091801 609620 4754219 16 0308028-14 Cl7-BZ#174 0.0676 U µg/Kg 0.0676 µg/Kg9/18/2001 16-08-091801 609620 4754219 16 0308028-14 Cl7-BZ#177 4.83 µg/Kg 0.0949 µg/Kg9/18/2001 16-08-091801 609620 4754219 16 0308028-14 Cl7-BZ#180 70.2 µg/Kg 0.142 µg/Kg9/18/2001 16-08-091801 609620 4754219 16 0308028-14 Cl7-BZ#183 10.7 µg/Kg 0.0644 µg/Kg9/18/2001 16-08-091801 609620 4754219 16 0308028-14 Cl7-BZ#187 47.9 µg/Kg 0.0708 µg/Kg9/18/2001 16-08-091801 609620 4754219 16 0308028-14 Cl7-BZ#189 0.127 U µg/Kg 0.127 µg/Kg9/18/2001 16-08-091801 609620 4754219 16 0308028-14 Cl8-BZ#194 7.20 J µg/Kg 0.148 µg/Kg9/18/2001 16-08-091801 609620 4754219 16 0308028-14 Cl8-BZ#195 4.08 µg/Kg 0.146 µg/Kg9/18/2001 16-08-091801 609620 4754219 16 0308028-14 Cl8-BZ#201 9.23 µg/Kg 0.129 µg/Kg9/18/2001 16-08-091801 609620 4754219 16 0308028-14 Cl9-BZ#206 10.5 J µg/Kg 0.172 µg/Kg9/18/2001 16-08-091801 609620 4754219 16 0308028-14 Cl10-BZ#209 1.42 J µg/Kg 0.0804 µg/Kg9/18/2001 16-08-091801 609620 4754219 16 0308028-14 Monochlorobiphenyls 4.73 U µg/Kg 4.73 µg/Kg9/18/2001 16-08-091801 609620 4754219 16 0308028-14 Dichlorobiphenyls 0.138 U µg/Kg 0.138 µg/Kg9/18/2001 16-08-091801 609620 4754219 16 0308028-14 Trichlorobiphenyls 18.0 µg/Kg 0.475 µg/Kg9/18/2001 16-08-091801 609620 4754219 16 0308028-14 Tetrachlorobiphenyls 274 µg/Kg 0.0740 µg/Kg9/18/2001 16-08-091801 609620 4754219 16 0308028-14 Pentachlorobiphenyls 852 µg/Kg 0.0853 µg/Kg9/18/2001 16-08-091801 609620 4754219 16 0308028-14 Hexachlorobiphenyls 710 µg/Kg 0.135 µg/Kg9/18/2001 16-08-091801 609620 4754219 16 0308028-14 Heptachlorobiphenyls 132 µg/Kg 0.0740 µg/Kg



Extracted 7/30/04




SITE NUMBER



9/18/2001 16-08-091801 609620 4754219 16 0308028-14 Octachlorobiphenyls 41.9 µg/Kg 0.0676 µg/Kg9/18/2001 16-08-091801 609620 4754219 16 0308028-14 Nonachlorobiphenyls 15.4 µg/Kg 0.172 µg/Kg9/18/2001 16-08-091801 609620 4754219 16 0308028-14 Decachlorobiphenyl 1.42 µg/Kg 0.0804 µg/Kg9/18/2001 16-08-091801 609620 4754219 16 0308028-14 Total Homologs 2040 µg/Kg 0.0804 µg/Kg9/18/2001 16-08-091801 609620 4754219 16 0308028-14 Percent Lipids 3.3 % 0.1 %9/18/2001 16-08-091801 609620 4754219 16 0308028-14 Percent Moisture 72.4 % 0.1 %9/19/2001 16-11-091901 609620 4754219 16 0308028-15 Cl2-BZ#8 0.105 U µg/Kg 0.105 µg/Kg9/19/2001 16-11-091901 609620 4754219 16 0308028-15 Cl3-BZ#18 0.233 U µg/Kg 0.233 µg/Kg9/19/2001 16-11-091901 609620 4754219 16 0308028-15 Cl3-BZ#31/#28 25.7 µg/Kg 1.68 µg/Kg9/19/2001 16-11-091901 609620 4754219 16 0308028-15 Cl4-BZ#44 3.46 µg/Kg 0.160 µg/Kg9/19/2001 16-11-091901 609620 4754219 16 0308028-15 Cl4-BZ#45 0.214 U µg/Kg 0.214 µg/Kg9/19/2001 16-11-091901 609620 4754219 16 0308028-15 Cl4-BZ#47 43.0 µg/Kg 0.271 µg/Kg9/19/2001 16-11-091901 609620 4754219 16 0308028-15 Cl4-BZ#49 9.62 µg/Kg 0.133 µg/Kg9/19/2001 16-11-091901 609620 4754219 16 0308028-15 Cl4-BZ#52 20.1 µg/Kg 0.151 µg/Kg9/19/2001 16-11-091901 609620 4754219 16 0308028-15 Cl4-BZ#56 19.6 µg/Kg 0.0793 µg/Kg9/19/2001 16-11-091901 609620 4754219 16 0308028-15 Cl4-BZ#66 57.7 µg/Kg 0.106 µg/Kg9/19/2001 16-11-091901 609620 4754219 16 0308028-15 Cl4-BZ#70 19.2 µg/Kg 0.0928 µg/Kg9/19/2001 16-11-091901 609620 4754219 16 0308028-15 Cl4-BZ#74 79.6 µg/Kg 0.163 µg/Kg9/19/2001 16-11-091901 609620 4754219 16 0308028-15 Cl4-BZ#77 0.147 U µg/Kg 0.147 µg/Kg9/19/2001 16-11-091901 609620 4754219 16 0308028-15 Cl4-BZ#81 0.145 U µg/Kg 0.145 µg/Kg9/19/2001 16-11-091901 609620 4754219 16 0308028-15 Cl5-BZ#87 38.8 µg/Kg 0.0647 µg/Kg9/19/2001 16-11-091901 609620 4754219 16 0308028-15 Cl5-BZ#95 4.33 µg/Kg 0.0500 µg/Kg9/19/2001 16-11-091901 609620 4754219 16 0308028-15 Cl5-BZ#99 299 µg/Kg 0.0342 µg/Kg9/19/2001 16-11-091901 609620 4754219 16 0308028-15 Cl5-BZ#101 21.5 µg/Kg 0.0976 µg/Kg9/19/2001 16-11-091901 609620 4754219 16 0308028-15 Cl5-BZ#105 157 µg/Kg 0.0476 µg/Kg9/19/2001 16-11-091901 609620 4754219 16 0308028-15 Cl5-BZ#110 15.5 µg/Kg 0.0928 µg/Kg9/19/2001 16-11-091901 609620 4754219 16 0308028-15 Cl5-BZ#114 9.93 µg/Kg 0.0427 µg/Kg9/19/2001 16-11-091901 609620 4754219 16 0308028-15 Cl5-BZ#118 547 µg/Kg 0.588 µg/Kg9/19/2001 16-11-091901 609620 4754219 16 0308028-15 Cl5-BZ#123 0.0842 U µg/Kg 0.0842 µg/Kg9/19/2001 16-11-091901 609620 4754219 16 0308028-15 Cl5-BZ#126 0.0744 U µg/Kg 0.0744 µg/Kg9/19/2001 16-11-091901 609620 4754219 16 0308028-15 Cl6-BZ#128 36.6 µg/Kg 0.0671 µg/Kg9/19/2001 16-11-091901 609620 4754219 16 0308028-15 Cl6-BZ#138 600 µg/Kg 0.567 µg/Kg9/19/2001 16-11-091901 609620 4754219 16 0308028-15 Cl6-BZ#146 62.7 µg/Kg 0.0610 µg/Kg9/19/2001 16-11-091901 609620 4754219 16 0308028-15 Cl6-BZ#149 10.0 µg/Kg 0.0781 µg/Kg



Extracted 7/30/04




SITE NUMBER



9/19/2001 16-11-091901 609620 4754219 16 0308028-15 Cl6-BZ#151 1.57 µg/Kg 0.129 µg/Kg9/19/2001 16-11-091901 609620 4754219 16 0308028-15 Cl6-BZ#153 452 µg/Kg 0.653 µg/Kg9/19/2001 16-11-091901 609620 4754219 16 0308028-15 Cl6-BZ#156 33.0 µg/Kg 0.0793 µg/Kg9/19/2001 16-11-091901 609620 4754219 16 0308028-15 Cl6-BZ#157 6.70 µg/Kg 0.0622 µg/Kg9/19/2001 16-11-091901 609620 4754219 16 0308028-15 Cl6-BZ#158 7.15 µg/Kg 0.0525 µg/Kg9/19/2001 16-11-091901 609620 4754219 16 0308028-15 Cl6-BZ#167 15.6 µg/Kg 0.0671 µg/Kg9/19/2001 16-11-091901 609620 4754219 16 0308028-15 Cl6-BZ#169 0.216 U µg/Kg 0.216 µg/Kg9/19/2001 16-11-091901 609620 4754219 16 0308028-15 Cl7-BZ#170 49.4 µg/Kg 0.251 µg/Kg9/19/2001 16-11-091901 609620 4754219 16 0308028-15 Cl7-BZ#174 1.94 µg/Kg 0.0513 µg/Kg9/19/2001 16-11-091901 609620 4754219 16 0308028-15 Cl7-BZ#177 11.9 µg/Kg 0.0720 µg/Kg9/19/2001 16-11-091901 609620 4754219 16 0308028-15 Cl7-BZ#180 66.4 µg/Kg 0.107 µg/Kg9/19/2001 16-11-091901 609620 4754219 16 0308028-15 Cl7-BZ#183 12.0 µg/Kg 0.0488 µg/Kg9/19/2001 16-11-091901 609620 4754219 16 0308028-15 Cl7-BZ#187 93.0 µg/Kg 0.0537 µg/Kg9/19/2001 16-11-091901 609620 4754219 16 0308028-15 Cl7-BZ#189 0.0964 U µg/Kg 0.0964 µg/Kg9/19/2001 16-11-091901 609620 4754219 16 0308028-15 Cl8-BZ#194 9.78 µg/Kg 0.112 µg/Kg9/19/2001 16-11-091901 609620 4754219 16 0308028-15 Cl8-BZ#195 5.34 µg/Kg 0.111 µg/Kg9/19/2001 16-11-091901 609620 4754219 16 0308028-15 Cl8-BZ#201 18.4 µg/Kg 0.0976 µg/Kg9/19/2001 16-11-091901 609620 4754219 16 0308028-15 Cl9-BZ#206 15.6 µg/Kg 0.131 µg/Kg9/19/2001 16-11-091901 609620 4754219 16 0308028-15 Cl10-BZ#209 1.87 µg/Kg 0.0610 µg/Kg9/19/2001 16-11-091901 609620 4754219 16 0308028-15 Monochlorobiphenyls 3.59 U µg/Kg 3.59 µg/Kg9/19/2001 16-11-091901 609620 4754219 16 0308028-15 Dichlorobiphenyls 0.105 U µg/Kg 0.105 µg/Kg9/19/2001 16-11-091901 609620 4754219 16 0308028-15 Trichlorobiphenyls 20.5 µg/Kg 0.360 µg/Kg9/19/2001 16-11-091901 609620 4754219 16 0308028-15 Tetrachlorobiphenyls 304 µg/Kg 0.0561 µg/Kg9/19/2001 16-11-091901 609620 4754219 16 0308028-15 Pentachlorobiphenyls 2050 µg/Kg 0.380 µg/Kg9/19/2001 16-11-091901 609620 4754219 16 0308028-15 Hexachlorobiphenyls 1450 µg/Kg 0.603 µg/Kg9/19/2001 16-11-091901 609620 4754219 16 0308028-15 Heptachlorobiphenyls 227 µg/Kg 0.0561 µg/Kg9/19/2001 16-11-091901 609620 4754219 16 0308028-15 Octachlorobiphenyls 49.1 µg/Kg 0.0513 µg/Kg9/19/2001 16-11-091901 609620 4754219 16 0308028-15 Nonachlorobiphenyls 23.4 µg/Kg 0.131 µg/Kg9/19/2001 16-11-091901 609620 4754219 16 0308028-15 Decachlorobiphenyl 1.87 µg/Kg 0.0610 µg/Kg9/19/2001 16-11-091901 609620 4754219 16 0308028-15 Total Homologs 4380 µg/Kg 0.359 µg/Kg9/19/2001 16-11-091901 609620 4754219 16 0308028-15 Percent Lipids 5.2 % 0.1 %9/19/2001 16-11-091901 609620 4754219 16 0308028-15 Percent Moisture 73.9 % 0.1 %7/19/2001 16-12-091901 609620 4754219 16 0308029-01 Cl2-BZ#8 0.119 U µg/Kg 0.119 µg/Kg7/19/2001 16-12-091901 609620 4754219 16 0308029-01 Cl3-BZ#18 0.264 U µg/Kg 0.264 µg/Kg



Extracted 7/30/04




SITE NUMBER



7/19/2001 16-12-091901 609620 4754219 16 0308029-01 Cl3-BZ#31/#28 264 µg/Kg 1.90 µg/Kg7/19/2001 16-12-091901 609620 4754219 16 0308029-01 Cl4-BZ#44 113 µg/Kg 0.181 µg/Kg7/19/2001 16-12-091901 609620 4754219 16 0308029-01 Cl4-BZ#45 1.64 µg/Kg 0.242 µg/Kg7/19/2001 16-12-091901 609620 4754219 16 0308029-01 Cl4-BZ#47 196 µg/Kg 0.306 µg/Kg7/19/2001 16-12-091901 609620 4754219 16 0308029-01 Cl4-BZ#49 121 µg/Kg 0.150 µg/Kg7/19/2001 16-12-091901 609620 4754219 16 0308029-01 Cl4-BZ#52 245 µg/Kg 0.171 µg/Kg7/19/2001 16-12-091901 609620 4754219 16 0308029-01 Cl4-BZ#56 213 µg/Kg 0.0897 µg/Kg7/19/2001 16-12-091901 609620 4754219 16 0308029-01 Cl4-BZ#66 744 µg/Kg 1.20 µg/Kg7/19/2001 16-12-091901 609620 4754219 16 0308029-01 Cl4-BZ#70 317 µg/Kg 0.105 µg/Kg7/19/2001 16-12-091901 609620 4754219 16 0308029-01 Cl4-BZ#74 385 µg/Kg 1.84 µg/Kg7/19/2001 16-12-091901 609620 4754219 16 0308029-01 Cl4-BZ#77 0.166 U µg/Kg 0.166 µg/Kg7/19/2001 16-12-091901 609620 4754219 16 0308029-01 Cl4-BZ#81 0.164 U µg/Kg 0.164 µg/Kg7/19/2001 16-12-091901 609620 4754219 16 0308029-01 Cl5-BZ#87 160 µg/Kg 0.0731 µg/Kg7/19/2001 16-12-091901 609620 4754219 16 0308029-01 Cl5-BZ#95 58.2 µg/Kg 0.0566 µg/Kg7/19/2001 16-12-091901 609620 4754219 16 0308029-01 Cl5-BZ#99 617 µg/Kg 0.386 µg/Kg7/19/2001 16-12-091901 609620 4754219 16 0308029-01 Cl5-BZ#101 134 µg/Kg 0.110 µg/Kg7/19/2001 16-12-091901 609620 4754219 16 0308029-01 Cl5-BZ#105 361 µg/Kg 0.537 µg/Kg7/19/2001 16-12-091901 609620 4754219 16 0308029-01 Cl5-BZ#110 152 µg/Kg 0.105 µg/Kg7/19/2001 16-12-091901 609620 4754219 16 0308029-01 Cl5-BZ#114 21.0 µg/Kg 0.0483 µg/Kg7/19/2001 16-12-091901 609620 4754219 16 0308029-01 Cl5-BZ#118 879 µg/Kg 1.13 µg/Kg7/19/2001 16-12-091901 609620 4754219 16 0308029-01 Cl5-BZ#123 0.0952 U µg/Kg 0.0952 µg/Kg7/19/2001 16-12-091901 609620 4754219 16 0308029-01 Cl5-BZ#126 0.0842 U µg/Kg 0.0842 µg/Kg7/19/2001 16-12-091901 609620 4754219 16 0308029-01 Cl6-BZ#128 80.6 µg/Kg 0.0759 µg/Kg7/19/2001 16-12-091901 609620 4754219 16 0308029-01 Cl6-BZ#138 1000 µg/Kg 1.09 µg/Kg7/19/2001 16-12-091901 609620 4754219 16 0308029-01 Cl6-BZ#146 150 µg/Kg 0.0690 µg/Kg7/19/2001 16-12-091901 609620 4754219 16 0308029-01 Cl6-BZ#149 59.2 µg/Kg 0.0883 µg/Kg7/19/2001 16-12-091901 609620 4754219 16 0308029-01 Cl6-BZ#151 11.6 µg/Kg 0.146 µg/Kg7/19/2001 16-12-091901 609620 4754219 16 0308029-01 Cl6-BZ#153 810 µg/Kg 1.25 µg/Kg7/19/2001 16-12-091901 609620 4754219 16 0308029-01 Cl6-BZ#156 62.4 µg/Kg 0.0897 µg/Kg7/19/2001 16-12-091901 609620 4754219 16 0308029-01 Cl6-BZ#157 12.7 µg/Kg 0.0704 µg/Kg7/19/2001 16-12-091901 609620 4754219 16 0308029-01 Cl6-BZ#158 17.2 µg/Kg 0.0593 µg/Kg7/19/2001 16-12-091901 609620 4754219 16 0308029-01 Cl6-BZ#167 43.8 µg/Kg 0.0759 µg/Kg7/19/2001 16-12-091901 609620 4754219 16 0308029-01 Cl6-BZ#169 0.244 U µg/Kg 0.244 µg/Kg7/19/2001 16-12-091901 609620 4754219 16 0308029-01 Cl7-BZ#170 104 µg/Kg 0.284 µg/Kg



Extracted 7/30/04




SITE NUMBER



7/19/2001 16-12-091901 609620 4754219 16 0308029-01 Cl7-BZ#174 3.66 µg/Kg 0.0580 µg/Kg7/19/2001 16-12-091901 609620 4754219 16 0308029-01 Cl7-BZ#177 21.4 µg/Kg 0.0814 µg/Kg7/19/2001 16-12-091901 609620 4754219 16 0308029-01 Cl7-BZ#180 164 µg/Kg 0.121 µg/Kg7/19/2001 16-12-091901 609620 4754219 16 0308029-01 Cl7-BZ#183 30.3 µg/Kg 0.0552 µg/Kg7/19/2001 16-12-091901 609620 4754219 16 0308029-01 Cl7-BZ#187 394 µg/Kg 0.606 µg/Kg7/19/2001 16-12-091901 609620 4754219 16 0308029-01 Cl7-BZ#189 0.109 U µg/Kg 0.109 µg/Kg7/19/2001 16-12-091901 609620 4754219 16 0308029-01 Cl8-BZ#194 21.2 µg/Kg 0.127 µg/Kg7/19/2001 16-12-091901 609620 4754219 16 0308029-01 Cl8-BZ#195 12.0 µg/Kg 0.126 µg/Kg7/19/2001 16-12-091901 609620 4754219 16 0308029-01 Cl8-BZ#201 49.5 µg/Kg 0.110 µg/Kg7/19/2001 16-12-091901 609620 4754219 16 0308029-01 Cl9-BZ#206 35.3 µg/Kg 0.148 µg/Kg7/19/2001 16-12-091901 609620 4754219 16 0308029-01 Cl10-BZ#209 4.64 µg/Kg 0.0690 µg/Kg7/19/2001 16-12-091901 609620 4754219 16 0308029-01 Monochlorobiphenyls 4.06 U µg/Kg 4.06 µg/Kg7/19/2001 16-12-091901 609620 4754219 16 0308029-01 Dichlorobiphenyls 2.96 µg/Kg 0.119 µg/Kg7/19/2001 16-12-091901 609620 4754219 16 0308029-01 Trichlorobiphenyls 254 µg/Kg 0.407 µg/Kg7/19/2001 16-12-091901 609620 4754219 16 0308029-01 Tetrachlorobiphenyls 2770 µg/Kg 0.633 µg/Kg7/19/2001 16-12-091901 609620 4754219 16 0308029-01 Pentachlorobiphenyls 3990 µg/Kg 0.730 µg/Kg7/19/2001 16-12-091901 609620 4754219 16 0308029-01 Hexachlorobiphenyls 2610 µg/Kg 1.16 µg/Kg7/19/2001 16-12-091901 609620 4754219 16 0308029-01 Heptachlorobiphenyls 735 µg/Kg 0.633 µg/Kg7/19/2001 16-12-091901 609620 4754219 16 0308029-01 Octachlorobiphenyls 126 µg/Kg 0.0580 µg/Kg7/19/2001 16-12-091901 609620 4754219 16 0308029-01 Nonachlorobiphenyls 53.0 µg/Kg 0.148 µg/Kg7/19/2001 16-12-091901 609620 4754219 16 0308029-01 Decachlorobiphenyl 4.64 µg/Kg 0.0690 µg/Kg7/19/2001 16-12-091901 609620 4754219 16 0308029-01 Total Homologs 10600 µg/Kg 0.688 µg/Kg7/19/2001 16-12-091901 609620 4754219 16 0308029-01 Percent Lipids 1.8 % 0.1 %7/19/2001 16-12-091901 609620 4754219 16 0308029-01 Percent Moisture 70.9 % 0.1 %7/19/2001 16-13-091901 609620 4754219 16 0308029-02 Cl2-BZ#8 0.103 U µg/Kg 0.103 µg/Kg7/19/2001 16-13-091901 609620 4754219 16 0308029-02 Cl3-BZ#18 0.228 U µg/Kg 0.228 µg/Kg7/19/2001 16-13-091901 609620 4754219 16 0308029-02 Cl3-BZ#31/#28 44.0 µg/Kg 1.64 µg/Kg7/19/2001 16-13-091901 609620 4754219 16 0308029-02 Cl4-BZ#44 7.24 µg/Kg 0.156 µg/Kg7/19/2001 16-13-091901 609620 4754219 16 0308029-02 Cl4-BZ#45 0.435 J µg/Kg 0.209 µg/Kg7/19/2001 16-13-091901 609620 4754219 16 0308029-02 Cl4-BZ#47 51.9 µg/Kg 0.265 µg/Kg7/19/2001 16-13-091901 609620 4754219 16 0308029-02 Cl4-BZ#49 18.5 µg/Kg 0.130 µg/Kg7/19/2001 16-13-091901 609620 4754219 16 0308029-02 Cl4-BZ#52 28.7 µg/Kg 0.148 µg/Kg7/19/2001 16-13-091901 609620 4754219 16 0308029-02 Cl4-BZ#56 32.4 µg/Kg 0.0775 µg/Kg7/19/2001 16-13-091901 609620 4754219 16 0308029-02 Cl4-BZ#66 101 µg/Kg 0.104 µg/Kg



Extracted 7/30/04




SITE NUMBER



7/19/2001 16-13-091901 609620 4754219 16 0308029-02 Cl4-BZ#70 48.1 µg/Kg 0.0907 µg/Kg7/19/2001 16-13-091901 609620 4754219 16 0308029-02 Cl4-BZ#74 104 µg/Kg 0.160 µg/Kg7/19/2001 16-13-091901 609620 4754219 16 0308029-02 Cl4-BZ#77 0.143 U µg/Kg 0.143 µg/Kg7/19/2001 16-13-091901 609620 4754219 16 0308029-02 Cl4-BZ#81 0.142 U µg/Kg 0.142 µg/Kg7/19/2001 16-13-091901 609620 4754219 16 0308029-02 Cl5-BZ#87 41.6 µg/Kg 0.0632 µg/Kg7/19/2001 16-13-091901 609620 4754219 16 0308029-02 Cl5-BZ#95 8.37 µg/Kg 0.0489 µg/Kg7/19/2001 16-13-091901 609620 4754219 16 0308029-02 Cl5-BZ#99 295 µg/Kg 0.0334 µg/Kg7/19/2001 16-13-091901 609620 4754219 16 0308029-02 Cl5-BZ#101 30.3 µg/Kg 0.0954 µg/Kg7/19/2001 16-13-091901 609620 4754219 16 0308029-02 Cl5-BZ#105 156 µg/Kg 0.0465 µg/Kg7/19/2001 16-13-091901 609620 4754219 16 0308029-02 Cl5-BZ#110 27.2 µg/Kg 0.0907 µg/Kg7/19/2001 16-13-091901 609620 4754219 16 0308029-02 Cl5-BZ#114 10.4 µg/Kg 0.0417 µg/Kg7/19/2001 16-13-091901 609620 4754219 16 0308029-02 Cl5-BZ#118 420 µg/Kg 0.409 µg/Kg7/19/2001 16-13-091901 609620 4754219 16 0308029-02 Cl5-BZ#123 0.0823 U µg/Kg 0.0823 µg/Kg7/19/2001 16-13-091901 609620 4754219 16 0308029-02 Cl5-BZ#126 0.924 NJ µg/Kg 0.0728 µg/Kg7/19/2001 16-13-091901 609620 4754219 16 0308029-02 Cl6-BZ#128 40.1 µg/Kg 0.0656 µg/Kg7/19/2001 16-13-091901 609620 4754219 16 0308029-02 Cl6-BZ#138 492 µg/Kg 0.394 µg/Kg7/19/2001 16-13-091901 609620 4754219 16 0308029-02 Cl6-BZ#146 70.3 µg/Kg 0.0596 µg/Kg7/19/2001 16-13-091901 609620 4754219 16 0308029-02 Cl6-BZ#149 14.7 µg/Kg 0.0763 µg/Kg7/19/2001 16-13-091901 609620 4754219 16 0308029-02 Cl6-BZ#151 2.36 µg/Kg 0.126 µg/Kg7/19/2001 16-13-091901 609620 4754219 16 0308029-02 Cl6-BZ#153 387 µg/Kg 0.454 µg/Kg7/19/2001 16-13-091901 609620 4754219 16 0308029-02 Cl6-BZ#156 39.7 µg/Kg 0.0775 µg/Kg7/19/2001 16-13-091901 609620 4754219 16 0308029-02 Cl6-BZ#157 7.28 µg/Kg 0.0608 µg/Kg7/19/2001 16-13-091901 609620 4754219 16 0308029-02 Cl6-BZ#158 6.03 µg/Kg 0.0513 µg/Kg7/19/2001 16-13-091901 609620 4754219 16 0308029-02 Cl6-BZ#167 16.2 µg/Kg 0.0656 µg/Kg7/19/2001 16-13-091901 609620 4754219 16 0308029-02 Cl6-BZ#169 0.211 U µg/Kg 0.211 µg/Kg7/19/2001 16-13-091901 609620 4754219 16 0308029-02 Cl7-BZ#170 57.6 µg/Kg 0.246 µg/Kg7/19/2001 16-13-091901 609620 4754219 16 0308029-02 Cl7-BZ#174 0.924 µg/Kg 0.0501 µg/Kg7/19/2001 16-13-091901 609620 4754219 16 0308029-02 Cl7-BZ#177 13.1 µg/Kg 0.0704 µg/Kg7/19/2001 16-13-091901 609620 4754219 16 0308029-02 Cl7-BZ#180 76.1 µg/Kg 0.105 µg/Kg7/19/2001 16-13-091901 609620 4754219 16 0308029-02 Cl7-BZ#183 14.2 µg/Kg 0.0477 µg/Kg7/19/2001 16-13-091901 609620 4754219 16 0308029-02 Cl7-BZ#187 108 µg/Kg 0.0525 µg/Kg7/19/2001 16-13-091901 609620 4754219 16 0308029-02 Cl7-BZ#189 0.0942 U µg/Kg 0.0942 µg/Kg7/19/2001 16-13-091901 609620 4754219 16 0308029-02 Cl8-BZ#194 9.40 µg/Kg 0.110 µg/Kg7/19/2001 16-13-091901 609620 4754219 16 0308029-02 Cl8-BZ#195 5.86 µg/Kg 0.108 µg/Kg



Extracted 7/30/04




SITE NUMBER



7/19/2001 16-13-091901 609620 4754219 16 0308029-02 Cl8-BZ#201 21.3 µg/Kg 0.0954 µg/Kg7/19/2001 16-13-091901 609620 4754219 16 0308029-02 Cl9-BZ#206 18.9 µg/Kg 0.128 µg/Kg7/19/2001 16-13-091901 609620 4754219 16 0308029-02 Cl10-BZ#209 2.33 µg/Kg 0.0596 µg/Kg7/19/2001 16-13-091901 609620 4754219 16 0308029-02 Monochlorobiphenyls 3.51 U µg/Kg 3.51 µg/Kg7/19/2001 16-13-091901 609620 4754219 16 0308029-02 Dichlorobiphenyls 2.56 µg/Kg 0.103 µg/Kg7/19/2001 16-13-091901 609620 4754219 16 0308029-02 Trichlorobiphenyls 52.3 µg/Kg 0.352 µg/Kg7/19/2001 16-13-091901 609620 4754219 16 0308029-02 Tetrachlorobiphenyls 461 µg/Kg 0.0549 µg/Kg7/19/2001 16-13-091901 609620 4754219 16 0308029-02 Pentachlorobiphenyls 1640 µg/Kg 0.264 µg/Kg7/19/2001 16-13-091901 609620 4754219 16 0308029-02 Hexachlorobiphenyls 1230 µg/Kg 0.419 µg/Kg7/19/2001 16-13-091901 609620 4754219 16 0308029-02 Heptachlorobiphenyls 278 µg/Kg 0.0549 µg/Kg7/19/2001 16-13-091901 609620 4754219 16 0308029-02 Octachlorobiphenyls 57.0 µg/Kg 0.0501 µg/Kg7/19/2001 16-13-091901 609620 4754219 16 0308029-02 Nonachlorobiphenyls 27.1 µg/Kg 0.128 µg/Kg7/19/2001 16-13-091901 609620 4754219 16 0308029-02 Decachlorobiphenyl 2.33 µg/Kg 0.0596 µg/Kg7/19/2001 16-13-091901 609620 4754219 16 0308029-02 Total Homologs 3780 µg/Kg 0.249 µg/Kg7/19/2001 16-13-091901 609620 4754219 16 0308029-02 Percent Lipids 2.9 % 0.1 %7/19/2001 16-13-091901 609620 4754219 16 0308029-02 Percent Moisture 73.8 % 0.1 %7/20/2001 16-17-092001 609620 4754219 16 0308029-03 Cl2-BZ#8 0.104 U µg/Kg 0.104 µg/Kg7/20/2001 16-17-092001 609620 4754219 16 0308029-03 Cl3-BZ#18 0.232 U µg/Kg 0.232 µg/Kg7/20/2001 16-17-092001 609620 4754219 16 0308029-03 Cl3-BZ#31/#28 62.9 µg/Kg 1.67 µg/Kg7/20/2001 16-17-092001 609620 4754219 16 0308029-03 Cl4-BZ#44 10.0 µg/Kg 0.159 µg/Kg7/20/2001 16-17-092001 609620 4754219 16 0308029-03 Cl4-BZ#45 0.212 U µg/Kg 0.212 µg/Kg7/20/2001 16-17-092001 609620 4754219 16 0308029-03 Cl4-BZ#47 59.2 µg/Kg 0.269 µg/Kg7/20/2001 16-17-092001 609620 4754219 16 0308029-03 Cl4-BZ#49 24.2 µg/Kg 0.132 µg/Kg7/20/2001 16-17-092001 609620 4754219 16 0308029-03 Cl4-BZ#52 55.0 µg/Kg 0.150 µg/Kg7/20/2001 16-17-092001 609620 4754219 16 0308029-03 Cl4-BZ#56 37.7 µg/Kg 0.0788 µg/Kg7/20/2001 16-17-092001 609620 4754219 16 0308029-03 Cl4-BZ#66 138 µg/Kg 0.105 µg/Kg7/20/2001 16-17-092001 609620 4754219 16 0308029-03 Cl4-BZ#70 75.4 µg/Kg 0.0922 µg/Kg7/20/2001 16-17-092001 609620 4754219 16 0308029-03 Cl4-BZ#74 101 µg/Kg 0.162 µg/Kg7/20/2001 16-17-092001 609620 4754219 16 0308029-03 Cl4-BZ#77 0.146 U µg/Kg 0.146 µg/Kg7/20/2001 16-17-092001 609620 4754219 16 0308029-03 Cl4-BZ#81 0.144 U µg/Kg 0.144 µg/Kg7/20/2001 16-17-092001 609620 4754219 16 0308029-03 Cl5-BZ#87 50.4 µg/Kg 0.0643 µg/Kg7/20/2001 16-17-092001 609620 4754219 16 0308029-03 Cl5-BZ#95 11.6 µg/Kg 0.0497 µg/Kg7/20/2001 16-17-092001 609620 4754219 16 0308029-03 Cl5-BZ#99 251 µg/Kg 0.0340 µg/Kg7/20/2001 16-17-092001 609620 4754219 16 0308029-03 Cl5-BZ#101 38.8 µg/Kg 0.0970 µg/Kg



Extracted 7/30/04




SITE NUMBER



7/20/2001 16-17-092001 609620 4754219 16 0308029-03 Cl5-BZ#105 125 µg/Kg 0.0473 µg/Kg7/20/2001 16-17-092001 609620 4754219 16 0308029-03 Cl5-BZ#110 41.2 µg/Kg 0.0922 µg/Kg7/20/2001 16-17-092001 609620 4754219 16 0308029-03 Cl5-BZ#114 7.78 µg/Kg 0.0425 µg/Kg7/20/2001 16-17-092001 609620 4754219 16 0308029-03 Cl5-BZ#118 355 µg/Kg 0.406 µg/Kg7/20/2001 16-17-092001 609620 4754219 16 0308029-03 Cl5-BZ#123 0.0837 U µg/Kg 0.0837 µg/Kg7/20/2001 16-17-092001 609620 4754219 16 0308029-03 Cl5-BZ#126 0.619 NJ µg/Kg 0.0740 µg/Kg7/20/2001 16-17-092001 609620 4754219 16 0308029-03 Cl6-BZ#128 32.6 µg/Kg 0.0667 µg/Kg7/20/2001 16-17-092001 609620 4754219 16 0308029-03 Cl6-BZ#138 462 µg/Kg 0.391 µg/Kg7/20/2001 16-17-092001 609620 4754219 16 0308029-03 Cl6-BZ#146 64.1 µg/Kg 0.0606 µg/Kg7/20/2001 16-17-092001 609620 4754219 16 0308029-03 Cl6-BZ#149 19.1 µg/Kg 0.0776 µg/Kg7/20/2001 16-17-092001 609620 4754219 16 0308029-03 Cl6-BZ#151 3.29 µg/Kg 0.129 µg/Kg7/20/2001 16-17-092001 609620 4754219 16 0308029-03 Cl6-BZ#153 370 µg/Kg 0.451 µg/Kg7/20/2001 16-17-092001 609620 4754219 16 0308029-03 Cl6-BZ#156 33.7 µg/Kg 0.0788 µg/Kg7/20/2001 16-17-092001 609620 4754219 16 0308029-03 Cl6-BZ#157 6.59 µg/Kg 0.0619 µg/Kg7/20/2001 16-17-092001 609620 4754219 16 0308029-03 Cl6-BZ#158 5.80 µg/Kg 0.0522 µg/Kg7/20/2001 16-17-092001 609620 4754219 16 0308029-03 Cl6-BZ#167 18.0 µg/Kg 0.0667 µg/Kg7/20/2001 16-17-092001 609620 4754219 16 0308029-03 Cl6-BZ#169 0.215 U µg/Kg 0.215 µg/Kg7/20/2001 16-17-092001 609620 4754219 16 0308029-03 Cl7-BZ#170 55.8 µg/Kg 0.250 µg/Kg7/20/2001 16-17-092001 609620 4754219 16 0308029-03 Cl7-BZ#174 1.25 µg/Kg 0.0509 µg/Kg7/20/2001 16-17-092001 609620 4754219 16 0308029-03 Cl7-BZ#177 12.1 µg/Kg 0.0716 µg/Kg7/20/2001 16-17-092001 609620 4754219 16 0308029-03 Cl7-BZ#180 75.9 µg/Kg 0.107 µg/Kg7/20/2001 16-17-092001 609620 4754219 16 0308029-03 Cl7-BZ#183 13.8 µg/Kg 0.0485 µg/Kg7/20/2001 16-17-092001 609620 4754219 16 0308029-03 Cl7-BZ#187 100 µg/Kg 0.0534 µg/Kg7/20/2001 16-17-092001 609620 4754219 16 0308029-03 Cl7-BZ#189 0.0958 U µg/Kg 0.0958 µg/Kg7/20/2001 16-17-092001 609620 4754219 16 0308029-03 Cl8-BZ#194 7.85 µg/Kg 0.112 µg/Kg7/20/2001 16-17-092001 609620 4754219 16 0308029-03 Cl8-BZ#195 5.73 µg/Kg 0.110 µg/Kg7/20/2001 16-17-092001 609620 4754219 16 0308029-03 Cl8-BZ#201 21.0 µg/Kg 0.0970 µg/Kg7/20/2001 16-17-092001 609620 4754219 16 0308029-03 Cl9-BZ#206 16.3 µg/Kg 0.130 µg/Kg7/20/2001 16-17-092001 609620 4754219 16 0308029-03 Cl10-BZ#209 2.00 µg/Kg 0.0606 µg/Kg7/20/2001 16-17-092001 609620 4754219 16 0308029-03 Monochlorobiphenyls 3.57 U µg/Kg 3.57 µg/Kg7/20/2001 16-17-092001 609620 4754219 16 0308029-03 Dichlorobiphenyls 1.75 µg/Kg 0.104 µg/Kg7/20/2001 16-17-092001 609620 4754219 16 0308029-03 Trichlorobiphenyls 77.6 µg/Kg 0.358 µg/Kg7/20/2001 16-17-092001 609620 4754219 16 0308029-03 Tetrachlorobiphenyls 587 µg/Kg 0.0558 µg/Kg7/20/2001 16-17-092001 609620 4754219 16 0308029-03 Pentachlorobiphenyls 1490 µg/Kg 0.263 µg/Kg



Extracted 7/30/04




SITE NUMBER



7/20/2001 16-17-092001 609620 4754219 16 0308029-03 Hexachlorobiphenyls 1160 µg/Kg 0.416 µg/Kg7/20/2001 16-17-092001 609620 4754219 16 0308029-03 Heptachlorobiphenyls 262 µg/Kg 0.0558 µg/Kg7/20/2001 16-17-092001 609620 4754219 16 0308029-03 Octachlorobiphenyls 53.2 µg/Kg 0.0509 µg/Kg7/20/2001 16-17-092001 609620 4754219 16 0308029-03 Nonachlorobiphenyls 23.8 µg/Kg 0.130 µg/Kg7/20/2001 16-17-092001 609620 4754219 16 0308029-03 Decachlorobiphenyl 2.00 µg/Kg 0.0606 µg/Kg7/20/2001 16-17-092001 609620 4754219 16 0308029-03 Total Homologs 3710 µg/Kg 0.248 µg/Kg7/20/2001 16-17-092001 609620 4754219 16 0308029-03 Percent Lipids 3.2 % 0.1 %7/20/2001 16-17-092001 609620 4754219 16 0308029-03 Percent Moisture 73.3 % 0.1 %7/20/2001 16-18-092001 609620 4754219 16 0308029-04 Cl2-BZ#8 0.118 U µg/Kg 0.118 µg/Kg7/20/2001 16-18-092001 609620 4754219 16 0308029-04 Cl3-BZ#18 0.262 U µg/Kg 0.262 µg/Kg7/20/2001 16-18-092001 609620 4754219 16 0308029-04 Cl3-BZ#31/#28 90.8 µg/Kg 1.89 µg/Kg7/20/2001 16-18-092001 609620 4754219 16 0308029-04 Cl4-BZ#44 13.6 µg/Kg 0.179 µg/Kg7/20/2001 16-18-092001 609620 4754219 16 0308029-04 Cl4-BZ#45 0.240 U µg/Kg 0.240 µg/Kg7/20/2001 16-18-092001 609620 4754219 16 0308029-04 Cl4-BZ#47 132 µg/Kg 0.304 µg/Kg7/20/2001 16-18-092001 609620 4754219 16 0308029-04 Cl4-BZ#49 37.3 µg/Kg 0.149 µg/Kg7/20/2001 16-18-092001 609620 4754219 16 0308029-04 Cl4-BZ#52 77.8 µg/Kg 0.170 µg/Kg7/20/2001 16-18-092001 609620 4754219 16 0308029-04 Cl4-BZ#56 76.6 µg/Kg 0.0891 µg/Kg7/20/2001 16-18-092001 609620 4754219 16 0308029-04 Cl4-BZ#66 221 µg/Kg 0.119 µg/Kg7/20/2001 16-18-092001 609620 4754219 16 0308029-04 Cl4-BZ#70 94.6 µg/Kg 0.104 µg/Kg7/20/2001 16-18-092001 609620 4754219 16 0308029-04 Cl4-BZ#74 254 µg/Kg 0.184 µg/Kg7/20/2001 16-18-092001 609620 4754219 16 0308029-04 Cl4-BZ#77 0.164 U µg/Kg 0.164 µg/Kg7/20/2001 16-18-092001 609620 4754219 16 0308029-04 Cl4-BZ#81 0.163 U µg/Kg 0.163 µg/Kg7/20/2001 16-18-092001 609620 4754219 16 0308029-04 Cl5-BZ#87 119 µg/Kg 0.0726 µg/Kg7/20/2001 16-18-092001 609620 4754219 16 0308029-04 Cl5-BZ#95 16.3 µg/Kg 0.0562 µg/Kg7/20/2001 16-18-092001 609620 4754219 16 0308029-04 Cl5-BZ#99 604 µg/Kg 0.356 µg/Kg7/20/2001 16-18-092001 609620 4754219 16 0308029-04 Cl5-BZ#101 69.6 µg/Kg 0.110 µg/Kg7/20/2001 16-18-092001 609620 4754219 16 0308029-04 Cl5-BZ#105 297 µg/Kg 0.0534 µg/Kg7/20/2001 16-18-092001 609620 4754219 16 0308029-04 Cl5-BZ#110 67.0 µg/Kg 0.104 µg/Kg7/20/2001 16-18-092001 609620 4754219 16 0308029-04 Cl5-BZ#114 20.6 µg/Kg 0.0480 µg/Kg7/20/2001 16-18-092001 609620 4754219 16 0308029-04 Cl5-BZ#118 776 µg/Kg 1.04 µg/Kg7/20/2001 16-18-092001 609620 4754219 16 0308029-04 Cl5-BZ#123 0.0946 U µg/Kg 0.0946 µg/Kg7/20/2001 16-18-092001 609620 4754219 16 0308029-04 Cl5-BZ#126 1.19 NJ µg/Kg 0.0836 µg/Kg7/20/2001 16-18-092001 609620 4754219 16 0308029-04 Cl6-BZ#128 65.7 µg/Kg 0.0754 µg/Kg7/20/2001 16-18-092001 609620 4754219 16 0308029-04 Cl6-BZ#138 812 µg/Kg 1.00 µg/Kg



Extracted 7/30/04




SITE NUMBER



7/20/2001 16-18-092001 609620 4754219 16 0308029-04 Cl6-BZ#146 119 µg/Kg 0.0685 µg/Kg7/20/2001 16-18-092001 609620 4754219 16 0308029-04 Cl6-BZ#149 28.4 µg/Kg 0.0877 µg/Kg7/20/2001 16-18-092001 609620 4754219 16 0308029-04 Cl6-BZ#151 4.41 µg/Kg 0.145 µg/Kg7/20/2001 16-18-092001 609620 4754219 16 0308029-04 Cl6-BZ#153 644 µg/Kg 1.16 µg/Kg7/20/2001 16-18-092001 609620 4754219 16 0308029-04 Cl6-BZ#156 63.5 µg/Kg 0.0891 µg/Kg7/20/2001 16-18-092001 609620 4754219 16 0308029-04 Cl6-BZ#157 12.7 µg/Kg 0.0699 µg/Kg7/20/2001 16-18-092001 609620 4754219 16 0308029-04 Cl6-BZ#158 14.0 µg/Kg 0.0589 µg/Kg7/20/2001 16-18-092001 609620 4754219 16 0308029-04 Cl6-BZ#167 34.1 µg/Kg 0.0754 µg/Kg7/20/2001 16-18-092001 609620 4754219 16 0308029-04 Cl6-BZ#169 0.243 U µg/Kg 0.243 µg/Kg7/20/2001 16-18-092001 609620 4754219 16 0308029-04 Cl7-BZ#170 83.6 µg/Kg 0.282 µg/Kg7/20/2001 16-18-092001 609620 4754219 16 0308029-04 Cl7-BZ#174 1.42 µg/Kg 0.0576 µg/Kg7/20/2001 16-18-092001 609620 4754219 16 0308029-04 Cl7-BZ#177 22.4 µg/Kg 0.0809 µg/Kg7/20/2001 16-18-092001 609620 4754219 16 0308029-04 Cl7-BZ#180 126 µg/Kg 0.121 µg/Kg7/20/2001 16-18-092001 609620 4754219 16 0308029-04 Cl7-BZ#183 22.7 µg/Kg 0.0548 µg/Kg7/20/2001 16-18-092001 609620 4754219 16 0308029-04 Cl7-BZ#187 196 µg/Kg 0.0603 µg/Kg7/20/2001 16-18-092001 609620 4754219 16 0308029-04 Cl7-BZ#189 0.108 U µg/Kg 0.108 µg/Kg7/20/2001 16-18-092001 609620 4754219 16 0308029-04 Cl8-BZ#194 12.8 µg/Kg 0.126 µg/Kg7/20/2001 16-18-092001 609620 4754219 16 0308029-04 Cl8-BZ#195 8.02 µg/Kg 0.125 µg/Kg7/20/2001 16-18-092001 609620 4754219 16 0308029-04 Cl8-BZ#201 34.2 µg/Kg 0.110 µg/Kg7/20/2001 16-18-092001 609620 4754219 16 0308029-04 Cl9-BZ#206 21.7 µg/Kg 0.147 µg/Kg7/20/2001 16-18-092001 609620 4754219 16 0308029-04 Cl10-BZ#209 2.46 µg/Kg 0.0685 µg/Kg7/20/2001 16-18-092001 609620 4754219 16 0308029-04 Monochlorobiphenyls 4.03 U µg/Kg 4.03 µg/Kg7/20/2001 16-18-092001 609620 4754219 16 0308029-04 Dichlorobiphenyls 2.08 µg/Kg 0.118 µg/Kg7/20/2001 16-18-092001 609620 4754219 16 0308029-04 Trichlorobiphenyls 120 µg/Kg 0.404 µg/Kg7/20/2001 16-18-092001 609620 4754219 16 0308029-04 Tetrachlorobiphenyls 1050 µg/Kg 0.0630 µg/Kg7/20/2001 16-18-092001 609620 4754219 16 0308029-04 Pentachlorobiphenyls 3180 µg/Kg 0.674 µg/Kg7/20/2001 16-18-092001 609620 4754219 16 0308029-04 Hexachlorobiphenyls 2080 µg/Kg 1.07 µg/Kg7/20/2001 16-18-092001 609620 4754219 16 0308029-04 Heptachlorobiphenyls 457 µg/Kg 0.0630 µg/Kg7/20/2001 16-18-092001 609620 4754219 16 0308029-04 Octachlorobiphenyls 81.4 µg/Kg 0.0576 µg/Kg7/20/2001 16-18-092001 609620 4754219 16 0308029-04 Nonachlorobiphenyls 30.9 µg/Kg 0.147 µg/Kg7/20/2001 16-18-092001 609620 4754219 16 0308029-04 Decachlorobiphenyl 2.46 µg/Kg 0.0685 µg/Kg7/20/2001 16-18-092001 609620 4754219 16 0308029-04 Total Homologs 7070 µg/Kg 0.636 µg/Kg7/20/2001 16-18-092001 609620 4754219 16 0308029-04 Percent Lipids 4.7 % 0.1 %7/20/2001 16-18-092001 609620 4754219 16 0308029-04 Percent Moisture 73.0 % 0.1 %



Extracted 7/30/04




SITE NUMBER



10/10/2001 17-03-101001 607475 4750334 17 0308029-05 Cl2-BZ#8 0.108 U µg/Kg 0.108 µg/Kg10/10/2001 17-03-101001 607475 4750334 17 0308029-05 Cl3-BZ#18 0.240 U µg/Kg 0.240 µg/Kg10/10/2001 17-03-101001 607475 4750334 17 0308029-05 Cl3-BZ#31/#28 238 µg/Kg 1.73 µg/Kg10/10/2001 17-03-101001 607475 4750334 17 0308029-05 Cl4-BZ#44 8.50 µg/Kg 0.164 µg/Kg10/10/2001 17-03-101001 607475 4750334 17 0308029-05 Cl4-BZ#45 0.364 J µg/Kg 0.220 µg/Kg10/10/2001 17-03-101001 607475 4750334 17 0308029-05 Cl4-BZ#47 229 µg/Kg 0.279 µg/Kg10/10/2001 17-03-101001 607475 4750334 17 0308029-05 Cl4-BZ#49 21.4 µg/Kg 0.137 µg/Kg10/10/2001 17-03-101001 607475 4750334 17 0308029-05 Cl4-BZ#52 58.0 µg/Kg 0.156 µg/Kg10/10/2001 17-03-101001 607475 4750334 17 0308029-05 Cl4-BZ#56 181 µg/Kg 0.0816 µg/Kg10/10/2001 17-03-101001 607475 4750334 17 0308029-05 Cl4-BZ#66 585 µg/Kg 0.539 µg/Kg10/10/2001 17-03-101001 607475 4750334 17 0308029-05 Cl4-BZ#70 201 µg/Kg 0.0954 µg/Kg10/10/2001 17-03-101001 607475 4750334 17 0308029-05 Cl4-BZ#74 446 µg/Kg 0.829 µg/Kg10/10/2001 17-03-101001 607475 4750334 17 0308029-05 Cl4-BZ#77 0.151 U µg/Kg 0.151 µg/Kg10/10/2001 17-03-101001 607475 4750334 17 0308029-05 Cl4-BZ#81 0.149 U µg/Kg 0.149 µg/Kg10/10/2001 17-03-101001 607475 4750334 17 0308029-05 Cl5-BZ#87 103 µg/Kg 0.0665 µg/Kg10/10/2001 17-03-101001 607475 4750334 17 0308029-05 Cl5-BZ#95 7.83 J µg/Kg 0.0515 µg/Kg10/10/2001 17-03-101001 607475 4750334 17 0308029-05 Cl5-BZ#99 405 µg/Kg 0.173 µg/Kg10/10/2001 17-03-101001 607475 4750334 17 0308029-05 Cl5-BZ#101 46.8 J µg/Kg 0.100 µg/Kg10/10/2001 17-03-101001 607475 4750334 17 0308029-05 Cl5-BZ#105 222 µg/Kg 0.0489 µg/Kg10/10/2001 17-03-101001 607475 4750334 17 0308029-05 Cl5-BZ#110 62.3 µg/Kg 0.0954 µg/Kg10/10/2001 17-03-101001 607475 4750334 17 0308029-05 Cl5-BZ#114 19.6 J µg/Kg 0.0439 µg/Kg10/10/2001 17-03-101001 607475 4750334 17 0308029-05 Cl5-BZ#118 531 µg/Kg 0.508 µg/Kg10/10/2001 17-03-101001 607475 4750334 17 0308029-05 Cl5-BZ#123 #VALUE! R µg/Kg 0.0866 µg/Kg10/10/2001 17-03-101001 607475 4750334 17 0308029-05 Cl5-BZ#126 0.0766 U µg/Kg 0.0766 µg/Kg10/10/2001 17-03-101001 607475 4750334 17 0308029-05 Cl6-BZ#128 46.6 J µg/Kg 0.0690 µg/Kg10/10/2001 17-03-101001 607475 4750334 17 0308029-05 Cl6-BZ#138 545 µg/Kg 0.489 µg/Kg10/10/2001 17-03-101001 607475 4750334 17 0308029-05 Cl6-BZ#146 93.3 µg/Kg 0.0628 µg/Kg10/10/2001 17-03-101001 607475 4750334 17 0308029-05 Cl6-BZ#149 19.9 J µg/Kg 0.0803 µg/Kg10/10/2001 17-03-101001 607475 4750334 17 0308029-05 Cl6-BZ#151 2.76 µg/Kg 0.133 µg/Kg10/10/2001 17-03-101001 607475 4750334 17 0308029-05 Cl6-BZ#153 424 µg/Kg 0.563 µg/Kg10/10/2001 17-03-101001 607475 4750334 17 0308029-05 Cl6-BZ#156 35.4 J µg/Kg 0.0816 µg/Kg10/10/2001 17-03-101001 607475 4750334 17 0308029-05 Cl6-BZ#157 6.58 µg/Kg 0.0640 µg/Kg10/10/2001 17-03-101001 607475 4750334 17 0308029-05 Cl6-BZ#158 17.2 J µg/Kg 0.0540 µg/Kg10/10/2001 17-03-101001 607475 4750334 17 0308029-05 Cl6-BZ#167 16.4 J µg/Kg 0.0690 µg/Kg



Extracted 7/30/04




SITE NUMBER



10/10/2001 17-03-101001 607475 4750334 17 0308029-05 Cl6-BZ#169 0.222 U µg/Kg 0.222 µg/Kg10/10/2001 17-03-101001 607475 4750334 17 0308029-05 Cl7-BZ#170 59.2 µg/Kg 0.259 µg/Kg10/10/2001 17-03-101001 607475 4750334 17 0308029-05 Cl7-BZ#174 0.954 µg/Kg 0.0527 µg/Kg10/10/2001 17-03-101001 607475 4750334 17 0308029-05 Cl7-BZ#177 19.4 J µg/Kg 0.0741 µg/Kg10/10/2001 17-03-101001 607475 4750334 17 0308029-05 Cl7-BZ#180 91.8 µg/Kg 0.110 µg/Kg10/10/2001 17-03-101001 607475 4750334 17 0308029-05 Cl7-BZ#183 23.0 J µg/Kg 0.0502 µg/Kg10/10/2001 17-03-101001 607475 4750334 17 0308029-05 Cl7-BZ#187 214 µg/Kg 0.0552 µg/Kg10/10/2001 17-03-101001 607475 4750334 17 0308029-05 Cl7-BZ#189 0.0992 U µg/Kg 0.0992 µg/Kg10/10/2001 17-03-101001 607475 4750334 17 0308029-05 Cl8-BZ#194 5.62 J µg/Kg 0.116 µg/Kg10/10/2001 17-03-101001 607475 4750334 17 0308029-05 Cl8-BZ#195 3.95 µg/Kg 0.114 µg/Kg10/10/2001 17-03-101001 607475 4750334 17 0308029-05 Cl8-BZ#201 29.3 J µg/Kg 0.100 µg/Kg10/10/2001 17-03-101001 607475 4750334 17 0308029-05 Cl9-BZ#206 10.8 J µg/Kg 0.134 µg/Kg10/10/2001 17-03-101001 607475 4750334 17 0308029-05 Cl10-BZ#209 1.55 J µg/Kg 0.0628 µg/Kg10/10/2001 17-03-101001 607475 4750334 17 0308029-05 Monochlorobiphenyls 3.69 U µg/Kg 3.69 µg/Kg10/10/2001 17-03-101001 607475 4750334 17 0308029-05 Dichlorobiphenyls 1.17 µg/Kg 0.108 µg/Kg10/10/2001 17-03-101001 607475 4750334 17 0308029-05 Trichlorobiphenyls 219 µg/Kg 0.370 µg/Kg10/10/2001 17-03-101001 607475 4750334 17 0308029-05 Tetrachlorobiphenyls 1950 µg/Kg 0.285 µg/Kg10/10/2001 17-03-101001 607475 4750334 17 0308029-05 Pentachlorobiphenyls 2270 µg/Kg 0.328 µg/Kg10/10/2001 17-03-101001 607475 4750334 17 0308029-05 Hexachlorobiphenyls 1390 µg/Kg 0.520 µg/Kg10/10/2001 17-03-101001 607475 4750334 17 0308029-05 Heptachlorobiphenyls 433 µg/Kg 0.0577 µg/Kg10/10/2001 17-03-101001 607475 4750334 17 0308029-05 Octachlorobiphenyls 61.9 µg/Kg 0.0527 µg/Kg10/10/2001 17-03-101001 607475 4750334 17 0308029-05 Nonachlorobiphenyls 18.4 µg/Kg 0.134 µg/Kg10/10/2001 17-03-101001 607475 4750334 17 0308029-05 Decachlorobiphenyl 1.55 µg/Kg 0.0628 µg/Kg10/10/2001 17-03-101001 607475 4750334 17 0308029-05 Total Homologs 6350 µg/Kg 0.310 µg/Kg10/10/2001 17-03-101001 607475 4750334 17 0308029-05 Percent Lipids 2.7 % 0.1 %10/10/2001 17-03-101001 607475 4750334 17 0308029-05 Percent Moisture 73.5 % 0.1 %10/10/2001 17-04-101001 607475 4750334 17 0308029-06 Cl2-BZ#8 0.142 U µg/Kg 0.142 µg/Kg10/10/2001 17-04-101001 607475 4750334 17 0308029-06 Cl3-BZ#18 0.316 U µg/Kg 0.316 µg/Kg10/10/2001 17-04-101001 607475 4750334 17 0308029-06 Cl3-BZ#31/#28 175 µg/Kg 2.28 µg/Kg10/10/2001 17-04-101001 607475 4750334 17 0308029-06 Cl4-BZ#44 6.44 µg/Kg 0.217 µg/Kg10/10/2001 17-04-101001 607475 4750334 17 0308029-06 Cl4-BZ#45 0.290 U µg/Kg 0.290 µg/Kg10/10/2001 17-04-101001 607475 4750334 17 0308029-06 Cl4-BZ#47 166 µg/Kg 0.368 µg/Kg10/10/2001 17-04-101001 607475 4750334 17 0308029-06 Cl4-BZ#49 17.7 µg/Kg 0.181 µg/Kg10/10/2001 17-04-101001 607475 4750334 17 0308029-06 Cl4-BZ#52 45.3 µg/Kg 0.205 µg/Kg



Extracted 7/30/04




SITE NUMBER



10/10/2001 17-04-101001 607475 4750334 17 0308029-06 Cl4-BZ#56 116 µg/Kg 0.108 µg/Kg10/10/2001 17-04-101001 607475 4750334 17 0308029-06 Cl4-BZ#66 334 µg/Kg 0.144 µg/Kg10/10/2001 17-04-101001 607475 4750334 17 0308029-06 Cl4-BZ#70 76.8 µg/Kg 0.126 µg/Kg10/10/2001 17-04-101001 607475 4750334 17 0308029-06 Cl4-BZ#74 303 µg/Kg 0.222 µg/Kg10/10/2001 17-04-101001 607475 4750334 17 0308029-06 Cl4-BZ#77 0.199 U µg/Kg 0.199 µg/Kg10/10/2001 17-04-101001 607475 4750334 17 0308029-06 Cl4-BZ#81 0.197 U µg/Kg 0.197 µg/Kg10/10/2001 17-04-101001 607475 4750334 17 0308029-06 Cl5-BZ#87 63.2 µg/Kg 0.0878 µg/Kg10/10/2001 17-04-101001 607475 4750334 17 0308029-06 Cl5-BZ#95 6.18 µg/Kg 0.0679 µg/Kg10/10/2001 17-04-101001 607475 4750334 17 0308029-06 Cl5-BZ#99 254 µg/Kg 0.0464 µg/Kg10/10/2001 17-04-101001 607475 4750334 17 0308029-06 Cl5-BZ#101 25.4 µg/Kg 0.132 µg/Kg10/10/2001 17-04-101001 607475 4750334 17 0308029-06 Cl5-BZ#105 136 µg/Kg 0.0646 µg/Kg10/10/2001 17-04-101001 607475 4750334 17 0308029-06 Cl5-BZ#110 29.8 µg/Kg 0.126 µg/Kg10/10/2001 17-04-101001 607475 4750334 17 0308029-06 Cl5-BZ#114 12.3 µg/Kg 0.0580 µg/Kg10/10/2001 17-04-101001 607475 4750334 17 0308029-06 Cl5-BZ#118 312 µg/Kg 0.136 µg/Kg10/10/2001 17-04-101001 607475 4750334 17 0308029-06 Cl5-BZ#123 0.114 U µg/Kg 0.114 µg/Kg10/10/2001 17-04-101001 607475 4750334 17 0308029-06 Cl5-BZ#126 0.101 U µg/Kg 0.101 µg/Kg10/10/2001 17-04-101001 607475 4750334 17 0308029-06 Cl6-BZ#128 30.5 µg/Kg 0.0911 µg/Kg10/10/2001 17-04-101001 607475 4750334 17 0308029-06 Cl6-BZ#138 317 µg/Kg 0.131 µg/Kg10/10/2001 17-04-101001 607475 4750334 17 0308029-06 Cl6-BZ#146 43.7 µg/Kg 0.0828 µg/Kg10/10/2001 17-04-101001 607475 4750334 17 0308029-06 Cl6-BZ#149 10.1 µg/Kg 0.106 µg/Kg10/10/2001 17-04-101001 607475 4750334 17 0308029-06 Cl6-BZ#151 1.75 µg/Kg 0.176 µg/Kg10/10/2001 17-04-101001 607475 4750334 17 0308029-06 Cl6-BZ#153 251 µg/Kg 0.151 µg/Kg10/10/2001 17-04-101001 607475 4750334 17 0308029-06 Cl6-BZ#156 21.5 µg/Kg 0.108 µg/Kg10/10/2001 17-04-101001 607475 4750334 17 0308029-06 Cl6-BZ#157 3.97 µg/Kg 0.0844 µg/Kg10/10/2001 17-04-101001 607475 4750334 17 0308029-06 Cl6-BZ#158 11.6 µg/Kg 0.0712 µg/Kg10/10/2001 17-04-101001 607475 4750334 17 0308029-06 Cl6-BZ#167 9.65 µg/Kg 0.0911 µg/Kg10/10/2001 17-04-101001 607475 4750334 17 0308029-06 Cl6-BZ#169 0.293 U µg/Kg 0.293 µg/Kg10/10/2001 17-04-101001 607475 4750334 17 0308029-06 Cl7-BZ#170 37.2 µg/Kg 0.341 µg/Kg10/10/2001 17-04-101001 607475 4750334 17 0308029-06 Cl7-BZ#174 0.0695 U µg/Kg 0.0695 µg/Kg10/10/2001 17-04-101001 607475 4750334 17 0308029-06 Cl7-BZ#177 8.59 µg/Kg 0.0977 µg/Kg10/10/2001 17-04-101001 607475 4750334 17 0308029-06 Cl7-BZ#180 61.8 µg/Kg 0.146 µg/Kg10/10/2001 17-04-101001 607475 4750334 17 0308029-06 Cl7-BZ#183 14.4 µg/Kg 0.0662 µg/Kg10/10/2001 17-04-101001 607475 4750334 17 0308029-06 Cl7-BZ#187 66.6 µg/Kg 0.0729 µg/Kg10/10/2001 17-04-101001 607475 4750334 17 0308029-06 Cl7-BZ#189 0.131 U µg/Kg 0.131 µg/Kg



Extracted 7/30/04




SITE NUMBER



10/10/2001 17-04-101001 607475 4750334 17 0308029-06 Cl8-BZ#194 5.37 µg/Kg 0.152 µg/Kg10/10/2001 17-04-101001 607475 4750334 17 0308029-06 Cl8-BZ#195 3.44 µg/Kg 0.151 µg/Kg10/10/2001 17-04-101001 607475 4750334 17 0308029-06 Cl8-BZ#201 10.1 µg/Kg 0.132 µg/Kg10/10/2001 17-04-101001 607475 4750334 17 0308029-06 Cl9-BZ#206 10.4 µg/Kg 0.177 µg/Kg10/10/2001 17-04-101001 607475 4750334 17 0308029-06 Cl10-BZ#209 1.78 µg/Kg 0.0828 µg/Kg10/10/2001 17-04-101001 607475 4750334 17 0308029-06 Monochlorobiphenyls 4.87 U µg/Kg 4.87 µg/Kg10/10/2001 17-04-101001 607475 4750334 17 0308029-06 Dichlorobiphenyls 13.3 µg/Kg 0.142 µg/Kg10/10/2001 17-04-101001 607475 4750334 17 0308029-06 Trichlorobiphenyls 176 µg/Kg 0.488 µg/Kg10/10/2001 17-04-101001 607475 4750334 17 0308029-06 Tetrachlorobiphenyls 1230 µg/Kg 0.0762 µg/Kg10/10/2001 17-04-101001 607475 4750334 17 0308029-06 Pentachlorobiphenyls 1370 µg/Kg 0.0878 µg/Kg10/10/2001 17-04-101001 607475 4750334 17 0308029-06 Hexachlorobiphenyls 804 µg/Kg 0.139 µg/Kg10/10/2001 17-04-101001 607475 4750334 17 0308029-06 Heptachlorobiphenyls 206 µg/Kg 0.0762 µg/Kg10/10/2001 17-04-101001 607475 4750334 17 0308029-06 Octachlorobiphenyls 43.7 µg/Kg 0.0695 µg/Kg10/10/2001 17-04-101001 607475 4750334 17 0308029-06 Nonachlorobiphenyls 16.1 µg/Kg 0.177 µg/Kg10/10/2001 17-04-101001 607475 4750334 17 0308029-06 Decachlorobiphenyl 1.78 µg/Kg 0.0828 µg/Kg10/10/2001 17-04-101001 607475 4750334 17 0308029-06 Total Homologs 3860 µg/Kg 0.0828 µg/Kg10/10/2001 17-04-101001 607475 4750334 17 0308029-06 Percent Lipids 2.0 % 0.1 %10/10/2001 17-04-101001 607475 4750334 17 0308029-06 Percent Moisture 73.4 % 0.1 %10/10/2001 17-07-101001 607475 4750334 17 0308029-07 Cl2-BZ#8 0.113 U µg/Kg 0.113 µg/Kg10/10/2001 17-07-101001 607475 4750334 17 0308029-07 Cl3-BZ#18 0.251 U µg/Kg 0.251 µg/Kg10/10/2001 17-07-101001 607475 4750334 17 0308029-07 Cl3-BZ#31/#28 242 µg/Kg 1.81 µg/Kg10/10/2001 17-07-101001 607475 4750334 17 0308029-07 Cl4-BZ#44 21.0 µg/Kg 0.172 µg/Kg10/10/2001 17-07-101001 607475 4750334 17 0308029-07 Cl4-BZ#45 0.230 U µg/Kg 0.230 µg/Kg10/10/2001 17-07-101001 607475 4750334 17 0308029-07 Cl4-BZ#47 314 µg/Kg 0.292 µg/Kg10/10/2001 17-07-101001 607475 4750334 17 0308029-07 Cl4-BZ#49 27.1 µg/Kg 0.143 µg/Kg10/10/2001 17-07-101001 607475 4750334 17 0308029-07 Cl4-BZ#52 90.7 µg/Kg 0.163 µg/Kg10/10/2001 17-07-101001 607475 4750334 17 0308029-07 Cl4-BZ#56 227 µg/Kg 0.0855 µg/Kg10/10/2001 17-07-101001 607475 4750334 17 0308029-07 Cl4-BZ#66 567 µg/Kg 0.572 µg/Kg10/10/2001 17-07-101001 607475 4750334 17 0308029-07 Cl4-BZ#70 67.7 µg/Kg 0.0999 µg/Kg10/10/2001 17-07-101001 607475 4750334 17 0308029-07 Cl4-BZ#74 597 µg/Kg 0.881 µg/Kg10/10/2001 17-07-101001 607475 4750334 17 0308029-07 Cl4-BZ#77 0.158 U µg/Kg 0.158 µg/Kg10/10/2001 17-07-101001 607475 4750334 17 0308029-07 Cl4-BZ#81 0.156 U µg/Kg 0.156 µg/Kg10/10/2001 17-07-101001 607475 4750334 17 0308029-07 Cl5-BZ#87 119 µg/Kg 0.0697 µg/Kg10/10/2001 17-07-101001 607475 4750334 17 0308029-07 Cl5-BZ#95 12.9 µg/Kg 0.0539 µg/Kg



Extracted 7/30/04




SITE NUMBER



10/10/2001 17-07-101001 607475 4750334 17 0308029-07 Cl5-BZ#99 470 µg/Kg 0.184 µg/Kg10/10/2001 17-07-101001 607475 4750334 17 0308029-07 Cl5-BZ#101 43.9 µg/Kg 0.105 µg/Kg10/10/2001 17-07-101001 607475 4750334 17 0308029-07 Cl5-BZ#105 259 µg/Kg 0.0513 µg/Kg10/10/2001 17-07-101001 607475 4750334 17 0308029-07 Cl5-BZ#110 50.5 µg/Kg 0.0999 µg/Kg10/10/2001 17-07-101001 607475 4750334 17 0308029-07 Cl5-BZ#114 23.9 µg/Kg 0.0460 µg/Kg10/10/2001 17-07-101001 607475 4750334 17 0308029-07 Cl5-BZ#118 597 µg/Kg 0.539 µg/Kg10/10/2001 17-07-101001 607475 4750334 17 0308029-07 Cl5-BZ#123 0.0907 U µg/Kg 0.0907 µg/Kg10/10/2001 17-07-101001 607475 4750334 17 0308029-07 Cl5-BZ#126 0.0802 U µg/Kg 0.0802 µg/Kg10/10/2001 17-07-101001 607475 4750334 17 0308029-07 Cl6-BZ#128 47.0 µg/Kg 0.0723 µg/Kg10/10/2001 17-07-101001 607475 4750334 17 0308029-07 Cl6-BZ#138 501 µg/Kg 0.519 µg/Kg10/10/2001 17-07-101001 607475 4750334 17 0308029-07 Cl6-BZ#146 75.4 µg/Kg 0.0658 µg/Kg10/10/2001 17-07-101001 607475 4750334 17 0308029-07 Cl6-BZ#149 15.1 µg/Kg 0.0842 µg/Kg10/10/2001 17-07-101001 607475 4750334 17 0308029-07 Cl6-BZ#151 3.01 µg/Kg 0.139 µg/Kg10/10/2001 17-07-101001 607475 4750334 17 0308029-07 Cl6-BZ#153 427 µg/Kg 0.598 µg/Kg10/10/2001 17-07-101001 607475 4750334 17 0308029-07 Cl6-BZ#156 37.6 µg/Kg 0.0855 µg/Kg10/10/2001 17-07-101001 607475 4750334 17 0308029-07 Cl6-BZ#157 7.01 µg/Kg 0.0671 µg/Kg10/10/2001 17-07-101001 607475 4750334 17 0308029-07 Cl6-BZ#158 16.6 µg/Kg 0.0565 µg/Kg10/10/2001 17-07-101001 607475 4750334 17 0308029-07 Cl6-BZ#167 19.1 µg/Kg 0.0723 µg/Kg10/10/2001 17-07-101001 607475 4750334 17 0308029-07 Cl6-BZ#169 0.233 U µg/Kg 0.233 µg/Kg10/10/2001 17-07-101001 607475 4750334 17 0308029-07 Cl7-BZ#170 61.3 µg/Kg 0.271 µg/Kg10/10/2001 17-07-101001 607475 4750334 17 0308029-07 Cl7-BZ#174 1.15 µg/Kg 0.0552 µg/Kg10/10/2001 17-07-101001 607475 4750334 17 0308029-07 Cl7-BZ#177 17.9 µg/Kg 0.0776 µg/Kg10/10/2001 17-07-101001 607475 4750334 17 0308029-07 Cl7-BZ#180 99.0 µg/Kg 0.116 µg/Kg10/10/2001 17-07-101001 607475 4750334 17 0308029-07 Cl7-BZ#183 23.7 µg/Kg 0.0526 µg/Kg10/10/2001 17-07-101001 607475 4750334 17 0308029-07 Cl7-BZ#187 162 µg/Kg 0.0579 µg/Kg10/10/2001 17-07-101001 607475 4750334 17 0308029-07 Cl7-BZ#189 0.104 U µg/Kg 0.104 µg/Kg10/10/2001 17-07-101001 607475 4750334 17 0308029-07 Cl8-BZ#194 6.66 µg/Kg 0.121 µg/Kg10/10/2001 17-07-101001 607475 4750334 17 0308029-07 Cl8-BZ#195 4.66 µg/Kg 0.120 µg/Kg10/10/2001 17-07-101001 607475 4750334 17 0308029-07 Cl8-BZ#201 26.7 µg/Kg 0.105 µg/Kg10/10/2001 17-07-101001 607475 4750334 17 0308029-07 Cl9-BZ#206 14.0 µg/Kg 0.141 µg/Kg10/10/2001 17-07-101001 607475 4750334 17 0308029-07 Cl10-BZ#209 2.00 µg/Kg 0.0658 µg/Kg10/10/2001 17-07-101001 607475 4750334 17 0308029-07 Monochlorobiphenyls 3.87 U µg/Kg 3.87 µg/Kg10/10/2001 17-07-101001 607475 4750334 17 0308029-07 Dichlorobiphenyls 0.802 µg/Kg 0.113 µg/Kg10/10/2001 17-07-101001 607475 4750334 17 0308029-07 Trichlorobiphenyls 235 µg/Kg 0.388 µg/Kg



Extracted 7/30/04




SITE NUMBER



10/10/2001 17-07-101001 607475 4750334 17 0308029-07 Tetrachlorobiphenyls 2280 µg/Kg 0.303 µg/Kg10/10/2001 17-07-101001 607475 4750334 17 0308029-07 Pentachlorobiphenyls 2570 µg/Kg 0.349 µg/Kg10/10/2001 17-07-101001 607475 4750334 17 0308029-07 Hexachlorobiphenyls 1320 µg/Kg 0.552 µg/Kg10/10/2001 17-07-101001 607475 4750334 17 0308029-07 Heptachlorobiphenyls 386 µg/Kg 0.0605 µg/Kg10/10/2001 17-07-101001 607475 4750334 17 0308029-07 Octachlorobiphenyls 65.2 µg/Kg 0.0552 µg/Kg10/10/2001 17-07-101001 607475 4750334 17 0308029-07 Nonachlorobiphenyls 14.0 µg/Kg 0.141 µg/Kg10/10/2001 17-07-101001 607475 4750334 17 0308029-07 Decachlorobiphenyl 2.00 µg/Kg 0.0658 µg/Kg10/10/2001 17-07-101001 607475 4750334 17 0308029-07 Total Homologs 6930 µg/Kg 0.329 µg/Kg10/10/2001 17-07-101001 607475 4750334 17 0308029-07 Percent Lipids 2.2 % 0.1 %10/10/2001 17-07-101001 607475 4750334 17 0308029-07 Percent Moisture 72.3 % 0.1 %10/14/2001 17-09-101401 607475 4750334 17 0308029-08 Cl2-BZ#8 0.103 U µg/Kg 0.103 µg/Kg10/14/2001 17-09-101401 607475 4750334 17 0308029-08 Cl3-BZ#18 0.228 U µg/Kg 0.228 µg/Kg10/14/2001 17-09-101401 607475 4750334 17 0308029-08 Cl3-BZ#31/#28 237 µg/Kg 1.64 µg/Kg10/14/2001 17-09-101401 607475 4750334 17 0308029-08 Cl4-BZ#44 33.5 µg/Kg 0.156 µg/Kg10/14/2001 17-09-101401 607475 4750334 17 0308029-08 Cl4-BZ#45 0.209 U µg/Kg 0.209 µg/Kg10/14/2001 17-09-101401 607475 4750334 17 0308029-08 Cl4-BZ#47 273 µg/Kg 0.265 µg/Kg10/14/2001 17-09-101401 607475 4750334 17 0308029-08 Cl4-BZ#49 62.3 µg/Kg 0.130 µg/Kg10/14/2001 17-09-101401 607475 4750334 17 0308029-08 Cl4-BZ#52 164 µg/Kg 0.148 µg/Kg10/14/2001 17-09-101401 607475 4750334 17 0308029-08 Cl4-BZ#56 186 µg/Kg 0.0776 µg/Kg10/14/2001 17-09-101401 607475 4750334 17 0308029-08 Cl4-BZ#66 522 µg/Kg 0.549 µg/Kg10/14/2001 17-09-101401 607475 4750334 17 0308029-08 Cl4-BZ#70 162 µg/Kg 0.0907 µg/Kg10/14/2001 17-09-101401 607475 4750334 17 0308029-08 Cl4-BZ#74 483 µg/Kg 0.846 µg/Kg10/14/2001 17-09-101401 607475 4750334 17 0308029-08 Cl4-BZ#77 0.143 U µg/Kg 0.143 µg/Kg10/14/2001 17-09-101401 607475 4750334 17 0308029-08 Cl4-BZ#81 0.142 U µg/Kg 0.142 µg/Kg10/14/2001 17-09-101401 607475 4750334 17 0308029-08 Cl5-BZ#87 130 µg/Kg 0.0633 µg/Kg10/14/2001 17-09-101401 607475 4750334 17 0308029-08 Cl5-BZ#95 24.7 µg/Kg 0.0489 µg/Kg10/14/2001 17-09-101401 607475 4750334 17 0308029-08 Cl5-BZ#99 464 µg/Kg 0.177 µg/Kg10/14/2001 17-09-101401 607475 4750334 17 0308029-08 Cl5-BZ#101 71.6 µg/Kg 0.0955 µg/Kg10/14/2001 17-09-101401 607475 4750334 17 0308029-08 Cl5-BZ#105 205 µg/Kg 0.0466 µg/Kg10/14/2001 17-09-101401 607475 4750334 17 0308029-08 Cl5-BZ#110 101 µg/Kg 0.0907 µg/Kg10/14/2001 17-09-101401 607475 4750334 17 0308029-08 Cl5-BZ#114 19.6 µg/Kg 0.0418 µg/Kg10/14/2001 17-09-101401 607475 4750334 17 0308029-08 Cl5-BZ#118 533 µg/Kg 0.518 µg/Kg10/14/2001 17-09-101401 607475 4750334 17 0308029-08 Cl5-BZ#123 0.0824 U µg/Kg 0.0824 µg/Kg10/14/2001 17-09-101401 607475 4750334 17 0308029-08 Cl5-BZ#126 0.0728 U µg/Kg 0.0728 µg/Kg



Extracted 7/30/04




SITE NUMBER



10/14/2001 17-09-101401 607475 4750334 17 0308029-08 Cl6-BZ#128 49.7 µg/Kg 0.0656 µg/Kg10/14/2001 17-09-101401 607475 4750334 17 0308029-08 Cl6-BZ#138 633 µg/Kg 0.499 µg/Kg10/14/2001 17-09-101401 607475 4750334 17 0308029-08 Cl6-BZ#146 89.7 µg/Kg 0.0597 µg/Kg10/14/2001 17-09-101401 607475 4750334 17 0308029-08 Cl6-BZ#149 29.2 µg/Kg 0.0764 µg/Kg10/14/2001 17-09-101401 607475 4750334 17 0308029-08 Cl6-BZ#151 5.77 µg/Kg 0.126 µg/Kg10/14/2001 17-09-101401 607475 4750334 17 0308029-08 Cl6-BZ#153 555 µg/Kg 0.575 µg/Kg10/14/2001 17-09-101401 607475 4750334 17 0308029-08 Cl6-BZ#156 41.5 µg/Kg 0.0776 µg/Kg10/14/2001 17-09-101401 607475 4750334 17 0308029-08 Cl6-BZ#157 7.53 µg/Kg 0.0609 µg/Kg10/14/2001 17-09-101401 607475 4750334 17 0308029-08 Cl6-BZ#158 16.1 µg/Kg 0.0513 µg/Kg10/14/2001 17-09-101401 607475 4750334 17 0308029-08 Cl6-BZ#167 21.4 µg/Kg 0.0656 µg/Kg10/14/2001 17-09-101401 607475 4750334 17 0308029-08 Cl6-BZ#169 0.211 U µg/Kg 0.211 µg/Kg10/14/2001 17-09-101401 607475 4750334 17 0308029-08 Cl7-BZ#170 82.5 µg/Kg 0.246 µg/Kg10/14/2001 17-09-101401 607475 4750334 17 0308029-08 Cl7-BZ#174 1.75 µg/Kg 0.0501 µg/Kg10/14/2001 17-09-101401 607475 4750334 17 0308029-08 Cl7-BZ#177 26.5 µg/Kg 0.0704 µg/Kg10/14/2001 17-09-101401 607475 4750334 17 0308029-08 Cl7-BZ#180 156 µg/Kg 0.105 µg/Kg10/14/2001 17-09-101401 607475 4750334 17 0308029-08 Cl7-BZ#183 36.4 µg/Kg 0.0477 µg/Kg10/14/2001 17-09-101401 607475 4750334 17 0308029-08 Cl7-BZ#187 204 µg/Kg 0.0525 µg/Kg10/14/2001 17-09-101401 607475 4750334 17 0308029-08 Cl7-BZ#189 0.0943 U µg/Kg 0.0943 µg/Kg10/14/2001 17-09-101401 607475 4750334 17 0308029-08 Cl8-BZ#194 14.3 µg/Kg 0.110 µg/Kg10/14/2001 17-09-101401 607475 4750334 17 0308029-08 Cl8-BZ#195 8.69 µg/Kg 0.109 µg/Kg10/14/2001 17-09-101401 607475 4750334 17 0308029-08 Cl8-BZ#201 52.7 µg/Kg 0.0955 µg/Kg10/14/2001 17-09-101401 607475 4750334 17 0308029-08 Cl9-BZ#206 26.3 µg/Kg 0.128 µg/Kg10/14/2001 17-09-101401 607475 4750334 17 0308029-08 Cl10-BZ#209 4.27 µg/Kg 0.0597 µg/Kg10/14/2001 17-09-101401 607475 4750334 17 0308029-08 Monochlorobiphenyls 3.51 U µg/Kg 3.51 µg/Kg10/14/2001 17-09-101401 607475 4750334 17 0308029-08 Dichlorobiphenyls 3.03 µg/Kg 0.103 µg/Kg10/14/2001 17-09-101401 607475 4750334 17 0308029-08 Trichlorobiphenyls 246 µg/Kg 0.352 µg/Kg10/14/2001 17-09-101401 607475 4750334 17 0308029-08 Tetrachlorobiphenyls 2330 µg/Kg 0.290 µg/Kg10/14/2001 17-09-101401 607475 4750334 17 0308029-08 Pentachlorobiphenyls 2610 µg/Kg 0.335 µg/Kg10/14/2001 17-09-101401 607475 4750334 17 0308029-08 Hexachlorobiphenyls 1680 µg/Kg 0.530 µg/Kg10/14/2001 17-09-101401 607475 4750334 17 0308029-08 Heptachlorobiphenyls 520 µg/Kg 0.0549 µg/Kg10/14/2001 17-09-101401 607475 4750334 17 0308029-08 Octachlorobiphenyls 122 µg/Kg 0.0501 µg/Kg10/14/2001 17-09-101401 607475 4750334 17 0308029-08 Nonachlorobiphenyls 37.4 µg/Kg 0.128 µg/Kg10/14/2001 17-09-101401 607475 4750334 17 0308029-08 Decachlorobiphenyl 4.27 µg/Kg 0.0597 µg/Kg10/14/2001 17-09-101401 607475 4750334 17 0308029-08 Total Homologs 7710 µg/Kg 0.316 µg/Kg



Extracted 7/30/04




SITE NUMBER



10/14/2001 17-09-101401 607475 4750334 17 0308029-08 Percent Lipids 3.6 % 0.1 %10/14/2001 17-09-101401 607475 4750334 17 0308029-08 Percent Moisture 71.1 % 0.1 %10/15/2001 17-13-101501 607475 4750334 17 0308029-09 Cl2-BZ#8 0.131 U µg/Kg 0.131 µg/Kg10/15/2001 17-13-101501 607475 4750334 17 0308029-09 Cl3-BZ#18 0.290 U µg/Kg 0.290 µg/Kg10/15/2001 17-13-101501 607475 4750334 17 0308029-09 Cl3-BZ#31/#28 208 µg/Kg 2.09 µg/Kg10/15/2001 17-13-101501 607475 4750334 17 0308029-09 Cl4-BZ#44 35.0 µg/Kg 0.199 µg/Kg10/15/2001 17-13-101501 607475 4750334 17 0308029-09 Cl4-BZ#45 0.266 U µg/Kg 0.266 µg/Kg10/15/2001 17-13-101501 607475 4750334 17 0308029-09 Cl4-BZ#47 130 µg/Kg 0.337 µg/Kg10/15/2001 17-13-101501 607475 4750334 17 0308029-09 Cl4-BZ#49 28.2 µg/Kg 0.165 µg/Kg10/15/2001 17-13-101501 607475 4750334 17 0308029-09 Cl4-BZ#52 89.4 µg/Kg 0.188 µg/Kg10/15/2001 17-13-101501 607475 4750334 17 0308029-09 Cl4-BZ#56 84.4 µg/Kg 0.0986 µg/Kg10/15/2001 17-13-101501 607475 4750334 17 0308029-09 Cl4-BZ#66 260 µg/Kg 0.132 µg/Kg10/15/2001 17-13-101501 607475 4750334 17 0308029-09 Cl4-BZ#70 139 µg/Kg 0.115 µg/Kg10/15/2001 17-13-101501 607475 4750334 17 0308029-09 Cl4-BZ#74 161 µg/Kg 0.203 µg/Kg10/15/2001 17-13-101501 607475 4750334 17 0308029-09 Cl4-BZ#77 0.182 U µg/Kg 0.182 µg/Kg10/15/2001 17-13-101501 607475 4750334 17 0308029-09 Cl4-BZ#81 0.181 U µg/Kg 0.181 µg/Kg10/15/2001 17-13-101501 607475 4750334 17 0308029-09 Cl5-BZ#87 47.8 µg/Kg 0.0804 µg/Kg10/15/2001 17-13-101501 607475 4750334 17 0308029-09 Cl5-BZ#95 12.1 µg/Kg 0.0622 µg/Kg10/15/2001 17-13-101501 607475 4750334 17 0308029-09 Cl5-BZ#99 131 µg/Kg 0.0425 µg/Kg10/15/2001 17-13-101501 607475 4750334 17 0308029-09 Cl5-BZ#101 30.1 µg/Kg 0.121 µg/Kg10/15/2001 17-13-101501 607475 4750334 17 0308029-09 Cl5-BZ#105 69.3 µg/Kg 0.0592 µg/Kg10/15/2001 17-13-101501 607475 4750334 17 0308029-09 Cl5-BZ#110 33.3 µg/Kg 0.115 µg/Kg10/15/2001 17-13-101501 607475 4750334 17 0308029-09 Cl5-BZ#114 5.66 µg/Kg 0.0531 µg/Kg10/15/2001 17-13-101501 607475 4750334 17 0308029-09 Cl5-BZ#118 151 µg/Kg 0.124 µg/Kg10/15/2001 17-13-101501 607475 4750334 17 0308029-09 Cl5-BZ#123 0.105 U µg/Kg 0.105 µg/Kg10/15/2001 17-13-101501 607475 4750334 17 0308029-09 Cl5-BZ#126 0.0926 U µg/Kg 0.0926 µg/Kg10/15/2001 17-13-101501 607475 4750334 17 0308029-09 Cl6-BZ#128 14.7 µg/Kg 0.0835 µg/Kg10/15/2001 17-13-101501 607475 4750334 17 0308029-09 Cl6-BZ#138 156 µg/Kg 0.120 µg/Kg10/15/2001 17-13-101501 607475 4750334 17 0308029-09 Cl6-BZ#146 21.5 µg/Kg 0.0759 µg/Kg10/15/2001 17-13-101501 607475 4750334 17 0308029-09 Cl6-BZ#149 10.1 µg/Kg 0.0971 µg/Kg10/15/2001 17-13-101501 607475 4750334 17 0308029-09 Cl6-BZ#151 2.66 µg/Kg 0.161 µg/Kg10/15/2001 17-13-101501 607475 4750334 17 0308029-09 Cl6-BZ#153 113 µg/Kg 0.138 µg/Kg10/15/2001 17-13-101501 607475 4750334 17 0308029-09 Cl6-BZ#156 10.5 µg/Kg 0.0986 µg/Kg10/15/2001 17-13-101501 607475 4750334 17 0308029-09 Cl6-BZ#157 2.25 µg/Kg 0.0774 µg/Kg



Extracted 7/30/04




SITE NUMBER



10/15/2001 17-13-101501 607475 4750334 17 0308029-09 Cl6-BZ#158 3.96 µg/Kg 0.0653 µg/Kg10/15/2001 17-13-101501 607475 4750334 17 0308029-09 Cl6-BZ#167 5.49 µg/Kg 0.0835 µg/Kg10/15/2001 17-13-101501 607475 4750334 17 0308029-09 Cl6-BZ#169 0.269 U µg/Kg 0.269 µg/Kg10/15/2001 17-13-101501 607475 4750334 17 0308029-09 Cl7-BZ#170 19.6 µg/Kg 0.313 µg/Kg10/15/2001 17-13-101501 607475 4750334 17 0308029-09 Cl7-BZ#174 1.17 µg/Kg 0.0637 µg/Kg10/15/2001 17-13-101501 607475 4750334 17 0308029-09 Cl7-BZ#177 7.06 µg/Kg 0.0895 µg/Kg10/15/2001 17-13-101501 607475 4750334 17 0308029-09 Cl7-BZ#180 28.5 µg/Kg 0.134 µg/Kg10/15/2001 17-13-101501 607475 4750334 17 0308029-09 Cl7-BZ#183 6.11 µg/Kg 0.0607 µg/Kg10/15/2001 17-13-101501 607475 4750334 17 0308029-09 Cl7-BZ#187 46.9 µg/Kg 0.0668 µg/Kg10/15/2001 17-13-101501 607475 4750334 17 0308029-09 Cl7-BZ#189 0.120 U µg/Kg 0.120 µg/Kg10/15/2001 17-13-101501 607475 4750334 17 0308029-09 Cl8-BZ#194 4.49 µg/Kg 0.140 µg/Kg10/15/2001 17-13-101501 607475 4750334 17 0308029-09 Cl8-BZ#195 2.55 µg/Kg 0.138 µg/Kg10/15/2001 17-13-101501 607475 4750334 17 0308029-09 Cl8-BZ#201 11.5 µg/Kg 0.121 µg/Kg10/15/2001 17-13-101501 607475 4750334 17 0308029-09 Cl9-BZ#206 8.87 µg/Kg 0.162 µg/Kg10/15/2001 17-13-101501 607475 4750334 17 0308029-09 Cl10-BZ#209 2.18 µg/Kg 0.0759 µg/Kg10/15/2001 17-13-101501 607475 4750334 17 0308029-09 Monochlorobiphenyls 4.46 U µg/Kg 4.46 µg/Kg10/15/2001 17-13-101501 607475 4750334 17 0308029-09 Dichlorobiphenyls 1.78 µg/Kg 0.131 µg/Kg10/15/2001 17-13-101501 607475 4750334 17 0308029-09 Trichlorobiphenyls 204 µg/Kg 0.448 µg/Kg10/15/2001 17-13-101501 607475 4750334 17 0308029-09 Tetrachlorobiphenyls 1080 µg/Kg 0.0698 µg/Kg10/15/2001 17-13-101501 607475 4750334 17 0308029-09 Pentachlorobiphenyls 803 µg/Kg 0.0804 µg/Kg10/15/2001 17-13-101501 607475 4750334 17 0308029-09 Hexachlorobiphenyls 389 µg/Kg 0.127 µg/Kg10/15/2001 17-13-101501 607475 4750334 17 0308029-09 Heptachlorobiphenyls 129 µg/Kg 0.0698 µg/Kg10/15/2001 17-13-101501 607475 4750334 17 0308029-09 Octachlorobiphenyls 32.6 µg/Kg 0.0637 µg/Kg10/15/2001 17-13-101501 607475 4750334 17 0308029-09 Nonachlorobiphenyls 8.87 µg/Kg 0.162 µg/Kg10/15/2001 17-13-101501 607475 4750334 17 0308029-09 Decachlorobiphenyl 2.18 µg/Kg 0.0759 µg/Kg10/15/2001 17-13-101501 607475 4750334 17 0308029-09 Total Homologs 2650 µg/Kg 0.0759 µg/Kg10/15/2001 17-13-101501 607475 4750334 17 0308029-09 Percent Lipids 2.2 % 0.1 %10/15/2001 17-13-101501 607475 4750334 17 0308029-09 Percent Moisture 74.3 % 0.1 %9/21/2001 18-08-092101 608173 4747866 18 0308029-10 Cl2-BZ#8 0.102 U µg/Kg 0.102 µg/Kg9/21/2001 18-08-092101 608173 4747866 18 0308029-10 Cl3-BZ#18 0.226 U µg/Kg 0.226 µg/Kg9/21/2001 18-08-092101 608173 4747866 18 0308029-10 Cl3-BZ#31/#28 5.02 J µg/Kg 1.63 µg/Kg9/21/2001 18-08-092101 608173 4747866 18 0308029-10 Cl4-BZ#44 0.581 J µg/Kg 0.155 µg/Kg9/21/2001 18-08-092101 608173 4747866 18 0308029-10 Cl4-BZ#45 0.373 J µg/Kg 0.207 µg/Kg9/21/2001 18-08-092101 608173 4747866 18 0308029-10 Cl4-BZ#47 3.43 µg/Kg 0.263 µg/Kg



Extracted 7/30/04




SITE NUMBER



9/21/2001 18-08-092101 608173 4747866 18 0308029-10 Cl4-BZ#49 0.699 µg/Kg 0.129 µg/Kg9/21/2001 18-08-092101 608173 4747866 18 0308029-10 Cl4-BZ#52 1.58 µg/Kg 0.147 µg/Kg9/21/2001 18-08-092101 608173 4747866 18 0308029-10 Cl4-BZ#56 2.35 µg/Kg 0.0771 µg/Kg9/21/2001 18-08-092101 608173 4747866 18 0308029-10 Cl4-BZ#66 6.97 µg/Kg 0.103 µg/Kg9/21/2001 18-08-092101 608173 4747866 18 0308029-10 Cl4-BZ#70 2.80 µg/Kg 0.0901 µg/Kg9/21/2001 18-08-092101 608173 4747866 18 0308029-10 Cl4-BZ#74 6.56 µg/Kg 0.159 µg/Kg9/21/2001 18-08-092101 608173 4747866 18 0308029-10 Cl4-BZ#77 0.142 U µg/Kg 0.142 µg/Kg9/21/2001 18-08-092101 608173 4747866 18 0308029-10 Cl4-BZ#81 0.141 U µg/Kg 0.141 µg/Kg9/21/2001 18-08-092101 608173 4747866 18 0308029-10 Cl5-BZ#87 2.22 µg/Kg 0.0628 µg/Kg9/21/2001 18-08-092101 608173 4747866 18 0308029-10 Cl5-BZ#95 0.231 J µg/Kg 0.0486 µg/Kg9/21/2001 18-08-092101 608173 4747866 18 0308029-10 Cl5-BZ#99 9.87 µg/Kg 0.0332 µg/Kg9/21/2001 18-08-092101 608173 4747866 18 0308029-10 Cl5-BZ#101 0.705 µg/Kg 0.0948 µg/Kg9/21/2001 18-08-092101 608173 4747866 18 0308029-10 Cl5-BZ#105 7.90 µg/Kg 0.0462 µg/Kg9/21/2001 18-08-092101 608173 4747866 18 0308029-10 Cl5-BZ#110 0.676 µg/Kg 0.0901 µg/Kg9/21/2001 18-08-092101 608173 4747866 18 0308029-10 Cl5-BZ#114 0.818 µg/Kg 0.0415 µg/Kg9/21/2001 18-08-092101 608173 4747866 18 0308029-10 Cl5-BZ#118 22.2 µg/Kg 0.0972 µg/Kg9/21/2001 18-08-092101 608173 4747866 18 0308029-10 Cl5-BZ#123 0.0818 U µg/Kg 0.0818 µg/Kg9/21/2001 18-08-092101 608173 4747866 18 0308029-10 Cl5-BZ#126 0.0723 U µg/Kg 0.0723 µg/Kg9/21/2001 18-08-092101 608173 4747866 18 0308029-10 Cl6-BZ#128 1.57 µg/Kg 0.0652 µg/Kg9/21/2001 18-08-092101 608173 4747866 18 0308029-10 Cl6-BZ#138 26.6 µg/Kg 0.0937 µg/Kg9/21/2001 18-08-092101 608173 4747866 18 0308029-10 Cl6-BZ#146 2.96 µg/Kg 0.0593 µg/Kg9/21/2001 18-08-092101 608173 4747866 18 0308029-10 Cl6-BZ#149 0.302 J µg/Kg 0.0759 µg/Kg9/21/2001 18-08-092101 608173 4747866 18 0308029-10 Cl6-BZ#151 0.178 J µg/Kg 0.126 µg/Kg9/21/2001 18-08-092101 608173 4747866 18 0308029-10 Cl6-BZ#153 32.1 µg/Kg 0.108 µg/Kg9/21/2001 18-08-092101 608173 4747866 18 0308029-10 Cl6-BZ#156 3.96 µg/Kg 0.0771 µg/Kg9/21/2001 18-08-092101 608173 4747866 18 0308029-10 Cl6-BZ#157 0.871 µg/Kg 0.0605 µg/Kg9/21/2001 18-08-092101 608173 4747866 18 0308029-10 Cl6-BZ#158 0.516 µg/Kg 0.0510 µg/Kg9/21/2001 18-08-092101 608173 4747866 18 0308029-10 Cl6-BZ#167 1.60 µg/Kg 0.0652 µg/Kg9/21/2001 18-08-092101 608173 4747866 18 0308029-10 Cl6-BZ#169 0.210 U µg/Kg 0.210 µg/Kg9/21/2001 18-08-092101 608173 4747866 18 0308029-10 Cl7-BZ#170 10.4 µg/Kg 0.244 µg/Kg9/21/2001 18-08-092101 608173 4747866 18 0308029-10 Cl7-BZ#174 0.0498 U µg/Kg 0.0498 µg/Kg9/21/2001 18-08-092101 608173 4747866 18 0308029-10 Cl7-BZ#177 0.0699 U µg/Kg 0.0699 µg/Kg9/21/2001 18-08-092101 608173 4747866 18 0308029-10 Cl7-BZ#180 12.5 µg/Kg 0.104 µg/Kg9/21/2001 18-08-092101 608173 4747866 18 0308029-10 Cl7-BZ#183 1.81 µg/Kg 0.0474 µg/Kg



Extracted 7/30/04




SITE NUMBER



9/21/2001 18-08-092101 608173 4747866 18 0308029-10 Cl7-BZ#187 2.29 µg/Kg 0.0522 µg/Kg9/21/2001 18-08-092101 608173 4747866 18 0308029-10 Cl7-BZ#189 0.0937 U µg/Kg 0.0937 µg/Kg9/21/2001 18-08-092101 608173 4747866 18 0308029-10 Cl8-BZ#194 1.43 µg/Kg 0.109 µg/Kg9/21/2001 18-08-092101 608173 4747866 18 0308029-10 Cl8-BZ#195 0.587 µg/Kg 0.108 µg/Kg9/21/2001 18-08-092101 608173 4747866 18 0308029-10 Cl8-BZ#201 1.23 µg/Kg 0.0948 µg/Kg9/21/2001 18-08-092101 608173 4747866 18 0308029-10 Cl9-BZ#206 1.48 µg/Kg 0.127 µg/Kg9/21/2001 18-08-092101 608173 4747866 18 0308029-10 Cl10-BZ#209 0.184 J µg/Kg 0.0593 µg/Kg9/21/2001 18-08-092101 608173 4747866 18 0308029-10 Monochlorobiphenyls 3.48 U µg/Kg 3.48 µg/Kg9/21/2001 18-08-092101 608173 4747866 18 0308029-10 Dichlorobiphenyls 0.102 U µg/Kg 0.102 µg/Kg9/21/2001 18-08-092101 608173 4747866 18 0308029-10 Trichlorobiphenyls 5.10 µg/Kg 0.350 µg/Kg9/21/2001 18-08-092101 608173 4747866 18 0308029-10 Tetrachlorobiphenyls 33.3 µg/Kg 0.0545 µg/Kg9/21/2001 18-08-092101 608173 4747866 18 0308029-10 Pentachlorobiphenyls 74.2 µg/Kg 0.0628 µg/Kg9/21/2001 18-08-092101 608173 4747866 18 0308029-10 Hexachlorobiphenyls 79.0 µg/Kg 0.0996 µg/Kg9/21/2001 18-08-092101 608173 4747866 18 0308029-10 Heptachlorobiphenyls 44.5 µg/Kg 0.0545 µg/Kg9/21/2001 18-08-092101 608173 4747866 18 0308029-10 Octachlorobiphenyls 11.6 µg/Kg 0.0498 µg/Kg9/21/2001 18-08-092101 608173 4747866 18 0308029-10 Nonachlorobiphenyls 1.48 µg/Kg 0.127 µg/Kg9/21/2001 18-08-092101 608173 4747866 18 0308029-10 Decachlorobiphenyl 0.184 J µg/Kg 0.0593 µg/Kg9/21/2001 18-08-092101 608173 4747866 18 0308029-10 Total Homologs 249 µg/Kg 0.0593 µg/Kg9/21/2001 18-08-092101 608173 4747866 18 0308029-10 Percent Lipids 2.5 % 0.1 %9/21/2001 18-08-092101 608173 4747866 18 0308029-10 Percent Moisture 73.0 % 0.1 %9/21/2001 18-09-092101 608173 4747866 18 0308029-11 Cl2-BZ#8 0.112 U µg/Kg 0.112 µg/Kg9/21/2001 18-09-092101 608173 4747866 18 0308029-11 Cl3-BZ#18 0.249 U µg/Kg 0.249 µg/Kg9/21/2001 18-09-092101 608173 4747866 18 0308029-11 Cl3-BZ#31/#28 5.84 J µg/Kg 1.80 µg/Kg9/21/2001 18-09-092101 608173 4747866 18 0308029-11 Cl4-BZ#44 0.183 J µg/Kg 0.171 µg/Kg9/21/2001 18-09-092101 608173 4747866 18 0308029-11 Cl4-BZ#45 0.228 U µg/Kg 0.228 µg/Kg9/21/2001 18-09-092101 608173 4747866 18 0308029-11 Cl4-BZ#47 5.16 µg/Kg 0.289 µg/Kg9/21/2001 18-09-092101 608173 4747866 18 0308029-11 Cl4-BZ#49 0.163 J µg/Kg 0.142 µg/Kg9/21/2001 18-09-092101 608173 4747866 18 0308029-11 Cl4-BZ#52 0.554 J µg/Kg 0.162 µg/Kg9/21/2001 18-09-092101 608173 4747866 18 0308029-11 Cl4-BZ#56 9.83 µg/Kg 0.0847 µg/Kg9/21/2001 18-09-092101 608173 4747866 18 0308029-11 Cl4-BZ#66 28.0 µg/Kg 0.113 µg/Kg9/21/2001 18-09-092101 608173 4747866 18 0308029-11 Cl4-BZ#70 1.94 µg/Kg 0.0991 µg/Kg9/21/2001 18-09-092101 608173 4747866 18 0308029-11 Cl4-BZ#74 35.0 µg/Kg 0.175 µg/Kg9/21/2001 18-09-092101 608173 4747866 18 0308029-11 Cl4-BZ#77 0.156 U µg/Kg 0.156 µg/Kg9/21/2001 18-09-092101 608173 4747866 18 0308029-11 Cl4-BZ#81 0.155 U µg/Kg 0.155 µg/Kg



Extracted 7/30/04




SITE NUMBER



9/21/2001 18-09-092101 608173 4747866 18 0308029-11 Cl5-BZ#87 7.44 µg/Kg 0.0691 µg/Kg9/21/2001 18-09-092101 608173 4747866 18 0308029-11 Cl5-BZ#95 0.124 J µg/Kg 0.0534 µg/Kg9/21/2001 18-09-092101 608173 4747866 18 0308029-11 Cl5-BZ#99 44.7 µg/Kg 0.0365 µg/Kg9/21/2001 18-09-092101 608173 4747866 18 0308029-11 Cl5-BZ#101 1.03 µg/Kg 0.104 µg/Kg9/21/2001 18-09-092101 608173 4747866 18 0308029-11 Cl5-BZ#105 28.6 µg/Kg 0.0508 µg/Kg9/21/2001 18-09-092101 608173 4747866 18 0308029-11 Cl5-BZ#110 0.254 J µg/Kg 0.0991 µg/Kg9/21/2001 18-09-092101 608173 4747866 18 0308029-11 Cl5-BZ#114 2.55 µg/Kg 0.0456 µg/Kg9/21/2001 18-09-092101 608173 4747866 18 0308029-11 Cl5-BZ#118 67.4 µg/Kg 0.107 µg/Kg9/21/2001 18-09-092101 608173 4747866 18 0308029-11 Cl5-BZ#123 0.0899 U µg/Kg 0.0899 µg/Kg9/21/2001 18-09-092101 608173 4747866 18 0308029-11 Cl5-BZ#126 0.0795 U µg/Kg 0.0795 µg/Kg9/21/2001 18-09-092101 608173 4747866 18 0308029-11 Cl6-BZ#128 5.72 µg/Kg 0.0717 µg/Kg9/21/2001 18-09-092101 608173 4747866 18 0308029-11 Cl6-BZ#138 80.5 µg/Kg 0.103 µg/Kg9/21/2001 18-09-092101 608173 4747866 18 0308029-11 Cl6-BZ#146 9.32 µg/Kg 0.0652 µg/Kg9/21/2001 18-09-092101 608173 4747866 18 0308029-11 Cl6-BZ#149 0.580 µg/Kg 0.0834 µg/Kg9/21/2001 18-09-092101 608173 4747866 18 0308029-11 Cl6-BZ#151 0.138 U µg/Kg 0.138 µg/Kg9/21/2001 18-09-092101 608173 4747866 18 0308029-11 Cl6-BZ#153 74.9 µg/Kg 0.119 µg/Kg9/21/2001 18-09-092101 608173 4747866 18 0308029-11 Cl6-BZ#156 8.34 µg/Kg 0.0847 µg/Kg9/21/2001 18-09-092101 608173 4747866 18 0308029-11 Cl6-BZ#157 1.51 µg/Kg 0.0665 µg/Kg9/21/2001 18-09-092101 608173 4747866 18 0308029-11 Cl6-BZ#158 1.46 µg/Kg 0.0561 µg/Kg9/21/2001 18-09-092101 608173 4747866 18 0308029-11 Cl6-BZ#167 2.98 µg/Kg 0.0717 µg/Kg9/21/2001 18-09-092101 608173 4747866 18 0308029-11 Cl6-BZ#169 0.231 U µg/Kg 0.231 µg/Kg9/21/2001 18-09-092101 608173 4747866 18 0308029-11 Cl7-BZ#170 19.4 µg/Kg 0.269 µg/Kg9/21/2001 18-09-092101 608173 4747866 18 0308029-11 Cl7-BZ#174 0.0547 U µg/Kg 0.0547 µg/Kg9/21/2001 18-09-092101 608173 4747866 18 0308029-11 Cl7-BZ#177 1.61 µg/Kg 0.0769 µg/Kg9/21/2001 18-09-092101 608173 4747866 18 0308029-11 Cl7-BZ#180 22.5 µg/Kg 0.115 µg/Kg9/21/2001 18-09-092101 608173 4747866 18 0308029-11 Cl7-BZ#183 4.64 µg/Kg 0.0521 µg/Kg9/21/2001 18-09-092101 608173 4747866 18 0308029-11 Cl7-BZ#187 6.84 µg/Kg 0.0574 µg/Kg9/21/2001 18-09-092101 608173 4747866 18 0308029-11 Cl7-BZ#189 0.103 U µg/Kg 0.103 µg/Kg9/21/2001 18-09-092101 608173 4747866 18 0308029-11 Cl8-BZ#194 3.79 µg/Kg 0.120 µg/Kg9/21/2001 18-09-092101 608173 4747866 18 0308029-11 Cl8-BZ#195 1.94 µg/Kg 0.119 µg/Kg9/21/2001 18-09-092101 608173 4747866 18 0308029-11 Cl8-BZ#201 2.30 µg/Kg 0.104 µg/Kg9/21/2001 18-09-092101 608173 4747866 18 0308029-11 Cl9-BZ#206 4.25 µg/Kg 0.140 µg/Kg9/21/2001 18-09-092101 608173 4747866 18 0308029-11 Cl10-BZ#209 0.671 µg/Kg 0.0652 µg/Kg9/21/2001 18-09-092101 608173 4747866 18 0308029-11 Monochlorobiphenyls 3.83 U µg/Kg 3.83 µg/Kg



Extracted 7/30/04




SITE NUMBER



9/21/2001 18-09-092101 608173 4747866 18 0308029-11 Dichlorobiphenyls 0.112 U µg/Kg 0.112 µg/Kg9/21/2001 18-09-092101 608173 4747866 18 0308029-11 Trichlorobiphenyls 5.89 µg/Kg 0.384 µg/Kg9/21/2001 18-09-092101 608173 4747866 18 0308029-11 Tetrachlorobiphenyls 94.3 µg/Kg 0.0600 µg/Kg9/21/2001 18-09-092101 608173 4747866 18 0308029-11 Pentachlorobiphenyls 244 µg/Kg 0.0691 µg/Kg9/21/2001 18-09-092101 608173 4747866 18 0308029-11 Hexachlorobiphenyls 208 µg/Kg 0.109 µg/Kg9/21/2001 18-09-092101 608173 4747866 18 0308029-11 Heptachlorobiphenyls 63.6 µg/Kg 0.0600 µg/Kg9/21/2001 18-09-092101 608173 4747866 18 0308029-11 Octachlorobiphenyls 20.7 µg/Kg 0.0547 µg/Kg9/21/2001 18-09-092101 608173 4747866 18 0308029-11 Nonachlorobiphenyls 4.33 µg/Kg 0.140 µg/Kg9/21/2001 18-09-092101 608173 4747866 18 0308029-11 Decachlorobiphenyl 0.671 µg/Kg 0.0652 µg/Kg9/21/2001 18-09-092101 608173 4747866 18 0308029-11 Total Homologs 642 µg/Kg 0.0652 µg/Kg9/21/2001 18-09-092101 608173 4747866 18 0308029-11 Percent Lipids 2.2 % 0.1 %9/21/2001 18-09-092101 608173 4747866 18 0308029-11 Percent Moisture 73.3 % 0.1 %9/22/2001 18-15-092201 608173 4747866 18 0308029-12 Cl2-BZ#8 0.110 U µg/Kg 0.110 µg/Kg9/22/2001 18-15-092201 608173 4747866 18 0308029-12 Cl3-BZ#18 0.244 U µg/Kg 0.244 µg/Kg9/22/2001 18-15-092201 608173 4747866 18 0308029-12 Cl3-BZ#31/#28 19.0 µg/Kg 1.76 µg/Kg9/22/2001 18-15-092201 608173 4747866 18 0308029-12 Cl4-BZ#44 0.447 J µg/Kg 0.168 µg/Kg9/22/2001 18-15-092201 608173 4747866 18 0308029-12 Cl4-BZ#45 0.224 U µg/Kg 0.224 µg/Kg9/22/2001 18-15-092201 608173 4747866 18 0308029-12 Cl4-BZ#47 3.25 µg/Kg 0.284 µg/Kg9/22/2001 18-15-092201 608173 4747866 18 0308029-12 Cl4-BZ#49 1.14 µg/Kg 0.139 µg/Kg9/22/2001 18-15-092201 608173 4747866 18 0308029-12 Cl4-BZ#52 1.77 µg/Kg 0.159 µg/Kg9/22/2001 18-15-092201 608173 4747866 18 0308029-12 Cl4-BZ#56 3.66 µg/Kg 0.0831 µg/Kg9/22/2001 18-15-092201 608173 4747866 18 0308029-12 Cl4-BZ#66 14.2 µg/Kg 0.111 µg/Kg9/22/2001 18-15-092201 608173 4747866 18 0308029-12 Cl4-BZ#70 6.07 µg/Kg 0.0972 µg/Kg9/22/2001 18-15-092201 608173 4747866 18 0308029-12 Cl4-BZ#74 7.28 µg/Kg 0.171 µg/Kg9/22/2001 18-15-092201 608173 4747866 18 0308029-12 Cl4-BZ#77 0.153 U µg/Kg 0.153 µg/Kg9/22/2001 18-15-092201 608173 4747866 18 0308029-12 Cl4-BZ#81 0.152 U µg/Kg 0.152 µg/Kg9/22/2001 18-15-092201 608173 4747866 18 0308029-12 Cl5-BZ#87 2.21 µg/Kg 0.0678 µg/Kg9/22/2001 18-15-092201 608173 4747866 18 0308029-12 Cl5-BZ#95 0.563 µg/Kg 0.0524 µg/Kg9/22/2001 18-15-092201 608173 4747866 18 0308029-12 Cl5-BZ#99 6.89 µg/Kg 0.0358 µg/Kg9/22/2001 18-15-092201 608173 4747866 18 0308029-12 Cl5-BZ#101 1.90 µg/Kg 0.102 µg/Kg9/22/2001 18-15-092201 608173 4747866 18 0308029-12 Cl5-BZ#105 4.30 µg/Kg 0.0499 µg/Kg9/22/2001 18-15-092201 608173 4747866 18 0308029-12 Cl5-BZ#110 1.47 µg/Kg 0.0972 µg/Kg9/22/2001 18-15-092201 608173 4747866 18 0308029-12 Cl5-BZ#114 0.345 µg/Kg 0.0448 µg/Kg9/22/2001 18-15-092201 608173 4747866 18 0308029-12 Cl5-BZ#118 8.88 µg/Kg 0.105 µg/Kg



Extracted 7/30/04




SITE NUMBER



9/22/2001 18-15-092201 608173 4747866 18 0308029-12 Cl5-BZ#123 0.0882 U µg/Kg 0.0882 µg/Kg9/22/2001 18-15-092201 608173 4747866 18 0308029-12 Cl5-BZ#126 0.0780 U µg/Kg 0.0780 µg/Kg9/22/2001 18-15-092201 608173 4747866 18 0308029-12 Cl6-BZ#128 1.14 µg/Kg 0.0703 µg/Kg9/22/2001 18-15-092201 608173 4747866 18 0308029-12 Cl6-BZ#138 9.87 µg/Kg 0.101 µg/Kg9/22/2001 18-15-092201 608173 4747866 18 0308029-12 Cl6-BZ#146 1.48 µg/Kg 0.0639 µg/Kg9/22/2001 18-15-092201 608173 4747866 18 0308029-12 Cl6-BZ#149 0.850 µg/Kg 0.0818 µg/Kg9/22/2001 18-15-092201 608173 4747866 18 0308029-12 Cl6-BZ#151 0.467 J µg/Kg 0.135 µg/Kg9/22/2001 18-15-092201 608173 4747866 18 0308029-12 Cl6-BZ#153 8.46 µg/Kg 0.116 µg/Kg9/22/2001 18-15-092201 608173 4747866 18 0308029-12 Cl6-BZ#156 0.767 µg/Kg 0.0831 µg/Kg9/22/2001 18-15-092201 608173 4747866 18 0308029-12 Cl6-BZ#157 0.173 J µg/Kg 0.0652 µg/Kg9/22/2001 18-15-092201 608173 4747866 18 0308029-12 Cl6-BZ#158 0.352 µg/Kg 0.0550 µg/Kg9/22/2001 18-15-092201 608173 4747866 18 0308029-12 Cl6-BZ#167 0.339 J µg/Kg 0.0703 µg/Kg9/22/2001 18-15-092201 608173 4747866 18 0308029-12 Cl6-BZ#169 0.226 U µg/Kg 0.226 µg/Kg9/22/2001 18-15-092201 608173 4747866 18 0308029-12 Cl7-BZ#170 0.263 U µg/Kg 0.263 µg/Kg9/22/2001 18-15-092201 608173 4747866 18 0308029-12 Cl7-BZ#174 0.0537 U µg/Kg 0.0537 µg/Kg9/22/2001 18-15-092201 608173 4747866 18 0308029-12 Cl7-BZ#177 0.729 µg/Kg 0.0754 µg/Kg9/22/2001 18-15-092201 608173 4747866 18 0308029-12 Cl7-BZ#180 0.112 U µg/Kg 0.112 µg/Kg9/22/2001 18-15-092201 608173 4747866 18 0308029-12 Cl7-BZ#183 0.671 µg/Kg 0.0511 µg/Kg9/22/2001 18-15-092201 608173 4747866 18 0308029-12 Cl7-BZ#187 3.73 µg/Kg 0.0563 µg/Kg9/22/2001 18-15-092201 608173 4747866 18 0308029-12 Cl7-BZ#189 0.101 U µg/Kg 0.101 µg/Kg9/22/2001 18-15-092201 608173 4747866 18 0308029-12 Cl8-BZ#194 0.537 J µg/Kg 0.118 µg/Kg9/22/2001 18-15-092201 608173 4747866 18 0308029-12 Cl8-BZ#195 0.116 U µg/Kg 0.116 µg/Kg9/22/2001 18-15-092201 608173 4747866 18 0308029-12 Cl8-BZ#201 1.07 µg/Kg 0.102 µg/Kg9/22/2001 18-15-092201 608173 4747866 18 0308029-12 Cl9-BZ#206 0.761 µg/Kg 0.137 µg/Kg9/22/2001 18-15-092201 608173 4747866 18 0308029-12 Cl10-BZ#209 0.301 J µg/Kg 0.0639 µg/Kg9/22/2001 18-15-092201 608173 4747866 18 0308029-12 Monochlorobiphenyls 3.76 U µg/Kg 3.76 µg/Kg9/22/2001 18-15-092201 608173 4747866 18 0308029-12 Dichlorobiphenyls 0.110 U µg/Kg 0.110 µg/Kg9/22/2001 18-15-092201 608173 4747866 18 0308029-12 Trichlorobiphenyls 19.2 µg/Kg 0.377 µg/Kg9/22/2001 18-15-092201 608173 4747866 18 0308029-12 Tetrachlorobiphenyls 48.5 µg/Kg 0.0588 µg/Kg9/22/2001 18-15-092201 608173 4747866 18 0308029-12 Pentachlorobiphenyls 48.9 µg/Kg 0.0678 µg/Kg9/22/2001 18-15-092201 608173 4747866 18 0308029-12 Hexachlorobiphenyls 27.2 µg/Kg 0.107 µg/Kg9/22/2001 18-15-092201 608173 4747866 18 0308029-12 Heptachlorobiphenyls 5.54 µg/Kg 0.0588 µg/Kg9/22/2001 18-15-092201 608173 4747866 18 0308029-12 Octachlorobiphenyls 6.07 µg/Kg 0.0537 µg/Kg9/22/2001 18-15-092201 608173 4747866 18 0308029-12 Nonachlorobiphenyls 1.45 µg/Kg 0.137 µg/Kg



Extracted 7/30/04




SITE NUMBER



9/22/2001 18-15-092201 608173 4747866 18 0308029-12 Decachlorobiphenyl 0.301 J µg/Kg 0.0639 µg/Kg9/22/2001 18-15-092201 608173 4747866 18 0308029-12 Total Homologs 157 µg/Kg 0.0639 µg/Kg9/22/2001 18-15-092201 608173 4747866 18 0308029-12 Percent Lipids 3.8 % 0.1 %9/22/2001 18-15-092201 608173 4747866 18 0308029-12 Percent Moisture 70.2 % 0.1 %

10/11/2001 20-14-101001 609713 4741759 20 0308029-13 Cl2-BZ#8 0.114 U µg/Kg 0.114 µg/Kg10/11/2001 20-14-101001 609713 4741759 20 0308029-13 Cl3-BZ#18 0.253 U µg/Kg 0.253 µg/Kg10/11/2001 20-14-101001 609713 4741759 20 0308029-13 Cl3-BZ#31/#28 65.7 µg/Kg 1.83 µg/Kg10/11/2001 20-14-101001 609713 4741759 20 0308029-13 Cl4-BZ#44 1.81 µg/Kg 0.174 µg/Kg10/11/2001 20-14-101001 609713 4741759 20 0308029-13 Cl4-BZ#45 0.232 U µg/Kg 0.232 µg/Kg10/11/2001 20-14-101001 609713 4741759 20 0308029-13 Cl4-BZ#47 48.7 µg/Kg 0.294 µg/Kg10/11/2001 20-14-101001 609713 4741759 20 0308029-13 Cl4-BZ#49 4.27 µg/Kg 0.145 µg/Kg10/11/2001 20-14-101001 609713 4741759 20 0308029-13 Cl4-BZ#52 6.71 µg/Kg 0.164 µg/Kg10/11/2001 20-14-101001 609713 4741759 20 0308029-13 Cl4-BZ#56 26.2 µg/Kg 0.0862 µg/Kg10/11/2001 20-14-101001 609713 4741759 20 0308029-13 Cl4-BZ#66 93.5 µg/Kg 0.115 µg/Kg10/11/2001 20-14-101001 609713 4741759 20 0308029-13 Cl4-BZ#70 19.8 µg/Kg 0.101 µg/Kg10/11/2001 20-14-101001 609713 4741759 20 0308029-13 Cl4-BZ#74 68.5 µg/Kg 0.178 µg/Kg10/11/2001 20-14-101001 609713 4741759 20 0308029-13 Cl4-BZ#77 0.159 U µg/Kg 0.159 µg/Kg10/11/2001 20-14-101001 609713 4741759 20 0308029-13 Cl4-BZ#81 0.158 U µg/Kg 0.158 µg/Kg10/11/2001 20-14-101001 609713 4741759 20 0308029-13 Cl5-BZ#87 17.7 µg/Kg 0.0703 µg/Kg10/11/2001 20-14-101001 609713 4741759 20 0308029-13 Cl5-BZ#95 1.76 µg/Kg 0.0544 µg/Kg10/11/2001 20-14-101001 609713 4741759 20 0308029-13 Cl5-BZ#99 71.3 µg/Kg 0.0371 µg/Kg10/11/2001 20-14-101001 609713 4741759 20 0308029-13 Cl5-BZ#101 5.33 µg/Kg 0.106 µg/Kg10/11/2001 20-14-101001 609713 4741759 20 0308029-13 Cl5-BZ#105 29.2 µg/Kg 0.0517 µg/Kg10/11/2001 20-14-101001 609713 4741759 20 0308029-13 Cl5-BZ#110 2.72 µg/Kg 0.101 µg/Kg10/11/2001 20-14-101001 609713 4741759 20 0308029-13 Cl5-BZ#114 2.49 µg/Kg 0.0464 µg/Kg10/11/2001 20-14-101001 609713 4741759 20 0308029-13 Cl5-BZ#118 70.2 µg/Kg 0.109 µg/Kg10/11/2001 20-14-101001 609713 4741759 20 0308029-13 Cl5-BZ#123 0.0915 U µg/Kg 0.0915 µg/Kg10/11/2001 20-14-101001 609713 4741759 20 0308029-13 Cl5-BZ#126 0.0809 U µg/Kg 0.0809 µg/Kg10/11/2001 20-14-101001 609713 4741759 20 0308029-13 Cl6-BZ#128 7.88 µg/Kg 0.0729 µg/Kg10/11/2001 20-14-101001 609713 4741759 20 0308029-13 Cl6-BZ#138 90.5 µg/Kg 0.105 µg/Kg10/11/2001 20-14-101001 609713 4741759 20 0308029-13 Cl6-BZ#146 9.97 µg/Kg 0.0663 µg/Kg10/11/2001 20-14-101001 609713 4741759 20 0308029-13 Cl6-BZ#149 1.92 µg/Kg 0.0849 µg/Kg10/11/2001 20-14-101001 609713 4741759 20 0308029-13 Cl6-BZ#151 0.597 J µg/Kg 0.140 µg/Kg10/11/2001 20-14-101001 609713 4741759 20 0308029-13 Cl6-BZ#153 72.3 µg/Kg 0.121 µg/Kg



Extracted 7/30/04




SITE NUMBER



10/11/2001 20-14-101001 609713 4741759 20 0308029-13 Cl6-BZ#156 5.27 µg/Kg 0.0862 µg/Kg10/11/2001 20-14-101001 609713 4741759 20 0308029-13 Cl6-BZ#157 1.17 µg/Kg 0.0676 µg/Kg10/11/2001 20-14-101001 609713 4741759 20 0308029-13 Cl6-BZ#158 2.21 µg/Kg 0.0570 µg/Kg10/11/2001 20-14-101001 609713 4741759 20 0308029-13 Cl6-BZ#167 2.59 µg/Kg 0.0729 µg/Kg10/11/2001 20-14-101001 609713 4741759 20 0308029-13 Cl6-BZ#169 0.235 U µg/Kg 0.235 µg/Kg10/11/2001 20-14-101001 609713 4741759 20 0308029-13 Cl7-BZ#170 15.6 µg/Kg 0.273 µg/Kg10/11/2001 20-14-101001 609713 4741759 20 0308029-13 Cl7-BZ#174 0.0557 U µg/Kg 0.0557 µg/Kg10/11/2001 20-14-101001 609713 4741759 20 0308029-13 Cl7-BZ#177 0.0782 U µg/Kg 0.0782 µg/Kg10/11/2001 20-14-101001 609713 4741759 20 0308029-13 Cl7-BZ#180 14.5 µg/Kg 0.117 µg/Kg10/11/2001 20-14-101001 609713 4741759 20 0308029-13 Cl7-BZ#183 3.43 µg/Kg 0.0530 µg/Kg10/11/2001 20-14-101001 609713 4741759 20 0308029-13 Cl7-BZ#187 8.19 µg/Kg 0.0583 µg/Kg10/11/2001 20-14-101001 609713 4741759 20 0308029-13 Cl7-BZ#189 0.105 U µg/Kg 0.105 µg/Kg10/11/2001 20-14-101001 609713 4741759 20 0308029-13 Cl8-BZ#194 0.769 µg/Kg 0.122 µg/Kg10/11/2001 20-14-101001 609713 4741759 20 0308029-13 Cl8-BZ#195 1.09 µg/Kg 0.121 µg/Kg10/11/2001 20-14-101001 609713 4741759 20 0308029-13 Cl8-BZ#201 2.02 µg/Kg 0.106 µg/Kg10/11/2001 20-14-101001 609713 4741759 20 0308029-13 Cl9-BZ#206 3.36 µg/Kg 0.142 µg/Kg10/11/2001 20-14-101001 609713 4741759 20 0308029-13 Cl10-BZ#209 0.570 µg/Kg 0.0663 µg/Kg10/11/2001 20-14-101001 609713 4741759 20 0308029-13 Monochlorobiphenyls 3.90 U µg/Kg 3.90 µg/Kg10/11/2001 20-14-101001 609713 4741759 20 0308029-13 Dichlorobiphenyls 1.53 µg/Kg 0.114 µg/Kg10/11/2001 20-14-101001 609713 4741759 20 0308029-13 Trichlorobiphenyls 80.0 µg/Kg 0.391 µg/Kg10/11/2001 20-14-101001 609713 4741759 20 0308029-13 Tetrachlorobiphenyls 320 µg/Kg 0.0610 µg/Kg10/11/2001 20-14-101001 609713 4741759 20 0308029-13 Pentachlorobiphenyls 325 µg/Kg 0.0703 µg/Kg10/11/2001 20-14-101001 609713 4741759 20 0308029-13 Hexachlorobiphenyls 220 µg/Kg 0.111 µg/Kg10/11/2001 20-14-101001 609713 4741759 20 0308029-13 Heptachlorobiphenyls 61.1 µg/Kg 0.0610 µg/Kg10/11/2001 20-14-101001 609713 4741759 20 0308029-13 Octachlorobiphenyls 18.7 µg/Kg 0.0557 µg/Kg10/11/2001 20-14-101001 609713 4741759 20 0308029-13 Nonachlorobiphenyls 5.53 µg/Kg 0.142 µg/Kg10/11/2001 20-14-101001 609713 4741759 20 0308029-13 Decachlorobiphenyl 0.570 µg/Kg 0.0663 µg/Kg10/11/2001 20-14-101001 609713 4741759 20 0308029-13 Total Homologs 1030 µg/Kg 0.0663 µg/Kg10/11/2001 20-14-101001 609713 4741759 20 0308029-13 Percent Lipids 3.0 % 0.1 %10/11/2001 20-14-101001 609713 4741759 20 0308029-13 Percent Moisture 71.5 % 0.1 %10/11/2001 20-29-101101 609713 4741759 20 0308029-14 Cl2-BZ#8 0.0986 U µg/Kg 0.0986 µg/Kg10/11/2001 20-29-101101 609713 4741759 20 0308029-14 Cl3-BZ#18 0.219 U µg/Kg 0.219 µg/Kg10/11/2001 20-29-101101 609713 4741759 20 0308029-14 Cl3-BZ#31/#28 47.6 µg/Kg 1.58 µg/Kg10/11/2001 20-29-101101 609713 4741759 20 0308029-14 Cl4-BZ#44 0.321 J µg/Kg 0.150 µg/Kg



Extracted 7/30/04




SITE NUMBER



10/11/2001 20-29-101101 609713 4741759 20 0308029-14 Cl4-BZ#45 0.201 U µg/Kg 0.201 µg/Kg10/11/2001 20-29-101101 609713 4741759 20 0308029-14 Cl4-BZ#47 25.5 µg/Kg 0.255 µg/Kg10/11/2001 20-29-101101 609713 4741759 20 0308029-14 Cl4-BZ#49 1.96 µg/Kg 0.125 µg/Kg10/11/2001 20-29-101101 609713 4741759 20 0308029-14 Cl4-BZ#52 3.40 µg/Kg 0.142 µg/Kg10/11/2001 20-29-101101 609713 4741759 20 0308029-14 Cl4-BZ#56 19.2 µg/Kg 0.0745 µg/Kg10/11/2001 20-29-101101 609713 4741759 20 0308029-14 Cl4-BZ#66 71.0 µg/Kg 0.0997 µg/Kg10/11/2001 20-29-101101 609713 4741759 20 0308029-14 Cl4-BZ#70 15.5 µg/Kg 0.0871 µg/Kg10/11/2001 20-29-101101 609713 4741759 20 0308029-14 Cl4-BZ#74 56.0 µg/Kg 0.154 µg/Kg10/11/2001 20-29-101101 609713 4741759 20 0308029-14 Cl4-BZ#77 0.138 U µg/Kg 0.138 µg/Kg10/11/2001 20-29-101101 609713 4741759 20 0308029-14 Cl4-BZ#81 0.136 U µg/Kg 0.136 µg/Kg10/11/2001 20-29-101101 609713 4741759 20 0308029-14 Cl5-BZ#87 19.3 µg/Kg 0.0608 µg/Kg10/11/2001 20-29-101101 609713 4741759 20 0308029-14 Cl5-BZ#95 0.820 µg/Kg 0.0470 µg/Kg10/11/2001 20-29-101101 609713 4741759 20 0308029-14 Cl5-BZ#99 83.0 µg/Kg 0.0321 µg/Kg10/11/2001 20-29-101101 609713 4741759 20 0308029-14 Cl5-BZ#101 5.16 µg/Kg 0.0917 µg/Kg10/11/2001 20-29-101101 609713 4741759 20 0308029-14 Cl5-BZ#105 35.2 µg/Kg 0.0447 µg/Kg10/11/2001 20-29-101101 609713 4741759 20 0308029-14 Cl5-BZ#110 2.32 µg/Kg 0.0871 µg/Kg10/11/2001 20-29-101101 609713 4741759 20 0308029-14 Cl5-BZ#114 3.13 µg/Kg 0.0401 µg/Kg10/11/2001 20-29-101101 609713 4741759 20 0308029-14 Cl5-BZ#118 85.4 µg/Kg 0.0940 µg/Kg10/11/2001 20-29-101101 609713 4741759 20 0308029-14 Cl5-BZ#123 0.0791 U µg/Kg 0.0791 µg/Kg10/11/2001 20-29-101101 609713 4741759 20 0308029-14 Cl5-BZ#126 0.0699 U µg/Kg 0.0699 µg/Kg10/11/2001 20-29-101101 609713 4741759 20 0308029-14 Cl6-BZ#128 9.95 µg/Kg 0.0631 µg/Kg10/11/2001 20-29-101101 609713 4741759 20 0308029-14 Cl6-BZ#138 140 µg/Kg 0.0906 µg/Kg10/11/2001 20-29-101101 609713 4741759 20 0308029-14 Cl6-BZ#146 19.4 µg/Kg 0.0573 µg/Kg10/11/2001 20-29-101101 609713 4741759 20 0308029-14 Cl6-BZ#149 2.29 µg/Kg 0.0734 µg/Kg10/11/2001 20-29-101101 609713 4741759 20 0308029-14 Cl6-BZ#151 0.682 µg/Kg 0.122 µg/Kg10/11/2001 20-29-101101 609713 4741759 20 0308029-14 Cl6-BZ#153 109 µg/Kg 0.104 µg/Kg10/11/2001 20-29-101101 609713 4741759 20 0308029-14 Cl6-BZ#156 7.70 µg/Kg 0.0745 µg/Kg10/11/2001 20-29-101101 609713 4741759 20 0308029-14 Cl6-BZ#157 1.46 µg/Kg 0.0585 µg/Kg10/11/2001 20-29-101101 609713 4741759 20 0308029-14 Cl6-BZ#158 2.18 µg/Kg 0.0493 µg/Kg10/11/2001 20-29-101101 609713 4741759 20 0308029-14 Cl6-BZ#167 4.09 µg/Kg 0.0631 µg/Kg10/11/2001 20-29-101101 609713 4741759 20 0308029-14 Cl6-BZ#169 0.203 U µg/Kg 0.203 µg/Kg10/11/2001 20-29-101101 609713 4741759 20 0308029-14 Cl7-BZ#170 15.6 µg/Kg 0.236 µg/Kg10/11/2001 20-29-101101 609713 4741759 20 0308029-14 Cl7-BZ#174 0.0482 U µg/Kg 0.0482 µg/Kg10/11/2001 20-29-101101 609713 4741759 20 0308029-14 Cl7-BZ#177 3.69 µg/Kg 0.0676 µg/Kg



Extracted 7/30/04




SITE NUMBER



10/11/2001 20-29-101101 609713 4741759 20 0308029-14 Cl7-BZ#180 19.4 µg/Kg 0.101 µg/Kg10/11/2001 20-29-101101 609713 4741759 20 0308029-14 Cl7-BZ#183 4.14 µg/Kg 0.0459 µg/Kg10/11/2001 20-29-101101 609713 4741759 20 0308029-14 Cl7-BZ#187 24.4 µg/Kg 0.0504 µg/Kg10/11/2001 20-29-101101 609713 4741759 20 0308029-14 Cl7-BZ#189 0.0906 U µg/Kg 0.0906 µg/Kg10/11/2001 20-29-101101 609713 4741759 20 0308029-14 Cl8-BZ#194 1.49 µg/Kg 0.105 µg/Kg10/11/2001 20-29-101101 609713 4741759 20 0308029-14 Cl8-BZ#195 1.24 µg/Kg 0.104 µg/Kg10/11/2001 20-29-101101 609713 4741759 20 0308029-14 Cl8-BZ#201 4.65 µg/Kg 0.0917 µg/Kg10/11/2001 20-29-101101 609713 4741759 20 0308029-14 Cl9-BZ#206 3.25 µg/Kg 0.123 µg/Kg10/11/2001 20-29-101101 609713 4741759 20 0308029-14 Cl10-BZ#209 0.539 µg/Kg 0.0573 µg/Kg10/11/2001 20-29-101101 609713 4741759 20 0308029-14 Monochlorobiphenyls 3.37 U µg/Kg 3.37 µg/Kg10/11/2001 20-29-101101 609713 4741759 20 0308029-14 Dichlorobiphenyls 0.567 µg/Kg 0.0986 µg/Kg10/11/2001 20-29-101101 609713 4741759 20 0308029-14 Trichlorobiphenyls 46.9 µg/Kg 0.338 µg/Kg10/11/2001 20-29-101101 609713 4741759 20 0308029-14 Tetrachlorobiphenyls 225 µg/Kg 0.0527 µg/Kg10/11/2001 20-29-101101 609713 4741759 20 0308029-14 Pentachlorobiphenyls 370 µg/Kg 0.0608 µg/Kg10/11/2001 20-29-101101 609713 4741759 20 0308029-14 Hexachlorobiphenyls 331 µg/Kg 0.0963 µg/Kg10/11/2001 20-29-101101 609713 4741759 20 0308029-14 Heptachlorobiphenyls 87.6 µg/Kg 0.0527 µg/Kg10/11/2001 20-29-101101 609713 4741759 20 0308029-14 Octachlorobiphenyls 16.1 µg/Kg 0.0482 µg/Kg10/11/2001 20-29-101101 609713 4741759 20 0308029-14 Nonachlorobiphenyls 5.14 µg/Kg 0.123 µg/Kg10/11/2001 20-29-101101 609713 4741759 20 0308029-14 Decachlorobiphenyl 0.539 µg/Kg 0.0573 µg/Kg10/11/2001 20-29-101101 609713 4741759 20 0308029-14 Total Homologs 1080 µg/Kg 0.0573 µg/Kg10/11/2001 20-29-101101 609713 4741759 20 0308029-14 Percent Lipids 2.9 % 0.1 %10/11/2001 20-29-101101 609713 4741759 20 0308029-14 Percent Moisture 71.5 % 0.1 %10/11/2001 20-31-101101 609713 4741759 20 0308029-15 Cl2-BZ#8 0.103 U µg/Kg 0.103 µg/Kg10/11/2001 20-31-101101 609713 4741759 20 0308029-15 Cl3-BZ#18 0.229 U µg/Kg 0.229 µg/Kg10/11/2001 20-31-101101 609713 4741759 20 0308029-15 Cl3-BZ#31/#28 41.6 µg/Kg 1.65 µg/Kg10/11/2001 20-31-101101 609713 4741759 20 0308029-15 Cl4-BZ#44 0.234 J µg/Kg 0.157 µg/Kg10/11/2001 20-31-101101 609713 4741759 20 0308029-15 Cl4-BZ#45 0.210 U µg/Kg 0.210 µg/Kg10/11/2001 20-31-101101 609713 4741759 20 0308029-15 Cl4-BZ#47 29.9 µg/Kg 0.266 µg/Kg10/11/2001 20-31-101101 609713 4741759 20 0308029-15 Cl4-BZ#49 0.911 µg/Kg 0.131 µg/Kg10/11/2001 20-31-101101 609713 4741759 20 0308029-15 Cl4-BZ#52 1.64 µg/Kg 0.149 µg/Kg10/11/2001 20-31-101101 609713 4741759 20 0308029-15 Cl4-BZ#56 16.1 µg/Kg 0.0779 µg/Kg10/11/2001 20-31-101101 609713 4741759 20 0308029-15 Cl4-BZ#66 64.8 µg/Kg 0.104 µg/Kg10/11/2001 20-31-101101 609713 4741759 20 0308029-15 Cl4-BZ#70 11.5 µg/Kg 0.0911 µg/Kg10/11/2001 20-31-101101 609713 4741759 20 0308029-15 Cl4-BZ#74 46.3 µg/Kg 0.161 µg/Kg



Extracted 7/30/04




SITE NUMBER



10/11/2001 20-31-101101 609713 4741759 20 0308029-15 Cl4-BZ#77 0.144 U µg/Kg 0.144 µg/Kg10/11/2001 20-31-101101 609713 4741759 20 0308029-15 Cl4-BZ#81 0.143 U µg/Kg 0.143 µg/Kg10/11/2001 20-31-101101 609713 4741759 20 0308029-15 Cl5-BZ#87 16.0 µg/Kg 0.0635 µg/Kg10/11/2001 20-31-101101 609713 4741759 20 0308029-15 Cl5-BZ#95 0.0492 U µg/Kg 0.0492 µg/Kg10/11/2001 20-31-101101 609713 4741759 20 0308029-15 Cl5-BZ#99 63.6 µg/Kg 0.0336 µg/Kg10/11/2001 20-31-101101 609713 4741759 20 0308029-15 Cl5-BZ#101 4.62 µg/Kg 0.0959 µg/Kg10/11/2001 20-31-101101 609713 4741759 20 0308029-15 Cl5-BZ#105 24.5 µg/Kg 0.0468 µg/Kg10/11/2001 20-31-101101 609713 4741759 20 0308029-15 Cl5-BZ#110 0.791 µg/Kg 0.0911 µg/Kg10/11/2001 20-31-101101 609713 4741759 20 0308029-15 Cl5-BZ#114 2.31 µg/Kg 0.0420 µg/Kg10/11/2001 20-31-101101 609713 4741759 20 0308029-15 Cl5-BZ#118 64.0 µg/Kg 0.0983 µg/Kg10/11/2001 20-31-101101 609713 4741759 20 0308029-15 Cl5-BZ#123 0.0827 U µg/Kg 0.0827 µg/Kg10/11/2001 20-31-101101 609713 4741759 20 0308029-15 Cl5-BZ#126 0.0731 U µg/Kg 0.0731 µg/Kg10/11/2001 20-31-101101 609713 4741759 20 0308029-15 Cl6-BZ#128 6.64 µg/Kg 0.0659 µg/Kg10/11/2001 20-31-101101 609713 4741759 20 0308029-15 Cl6-BZ#138 95.6 µg/Kg 0.0947 µg/Kg10/11/2001 20-31-101101 609713 4741759 20 0308029-15 Cl6-BZ#146 12.6 µg/Kg 0.0599 µg/Kg10/11/2001 20-31-101101 609713 4741759 20 0308029-15 Cl6-BZ#149 0.935 µg/Kg 0.0767 µg/Kg10/11/2001 20-31-101101 609713 4741759 20 0308029-15 Cl6-BZ#151 0.156 J µg/Kg 0.127 µg/Kg10/11/2001 20-31-101101 609713 4741759 20 0308029-15 Cl6-BZ#153 90.6 µg/Kg 0.109 µg/Kg10/11/2001 20-31-101101 609713 4741759 20 0308029-15 Cl6-BZ#156 6.18 µg/Kg 0.0779 µg/Kg10/11/2001 20-31-101101 609713 4741759 20 0308029-15 Cl6-BZ#157 0.917 µg/Kg 0.0611 µg/Kg10/11/2001 20-31-101101 609713 4741759 20 0308029-15 Cl6-BZ#158 1.30 µg/Kg 0.0516 µg/Kg10/11/2001 20-31-101101 609713 4741759 20 0308029-15 Cl6-BZ#167 3.02 µg/Kg 0.0659 µg/Kg10/11/2001 20-31-101101 609713 4741759 20 0308029-15 Cl6-BZ#169 0.212 U µg/Kg 0.212 µg/Kg10/11/2001 20-31-101101 609713 4741759 20 0308029-15 Cl7-BZ#170 16.8 µg/Kg 0.247 µg/Kg10/11/2001 20-31-101101 609713 4741759 20 0308029-15 Cl7-BZ#174 0.0504 U µg/Kg 0.0504 µg/Kg10/11/2001 20-31-101101 609713 4741759 20 0308029-15 Cl7-BZ#177 0.0707 U µg/Kg 0.0707 µg/Kg10/11/2001 20-31-101101 609713 4741759 20 0308029-15 Cl7-BZ#180 20.0 µg/Kg 0.105 µg/Kg10/11/2001 20-31-101101 609713 4741759 20 0308029-15 Cl7-BZ#183 3.60 µg/Kg 0.0480 µg/Kg10/11/2001 20-31-101101 609713 4741759 20 0308029-15 Cl7-BZ#187 12.5 µg/Kg 0.0528 µg/Kg10/11/2001 20-31-101101 609713 4741759 20 0308029-15 Cl7-BZ#189 0.0947 U µg/Kg 0.0947 µg/Kg10/11/2001 20-31-101101 609713 4741759 20 0308029-15 Cl8-BZ#194 2.36 µg/Kg 0.110 µg/Kg10/11/2001 20-31-101101 609713 4741759 20 0308029-15 Cl8-BZ#195 1.42 µg/Kg 0.109 µg/Kg10/11/2001 20-31-101101 609713 4741759 20 0308029-15 Cl8-BZ#201 3.09 µg/Kg 0.0959 µg/Kg10/11/2001 20-31-101101 609713 4741759 20 0308029-15 Cl9-BZ#206 8.55 µg/Kg 0.128 µg/Kg



Extracted 7/30/04




SITE NUMBER



10/11/2001 20-31-101101 609713 4741759 20 0308029-15 Cl10-BZ#209 1.37 µg/Kg 0.0599 µg/Kg10/11/2001 20-31-101101 609713 4741759 20 0308029-15 Monochlorobiphenyls 3.52 U µg/Kg 3.52 µg/Kg10/11/2001 20-31-101101 609713 4741759 20 0308029-15 Dichlorobiphenyls 0.486 J µg/Kg 0.103 µg/Kg10/11/2001 20-31-101101 609713 4741759 20 0308029-15 Trichlorobiphenyls 41.7 µg/Kg 0.354 µg/Kg10/11/2001 20-31-101101 609713 4741759 20 0308029-15 Tetrachlorobiphenyls 205 µg/Kg 0.0552 µg/Kg10/11/2001 20-31-101101 609713 4741759 20 0308029-15 Pentachlorobiphenyls 278 µg/Kg 0.0635 µg/Kg10/11/2001 20-31-101101 609713 4741759 20 0308029-15 Hexachlorobiphenyls 246 µg/Kg 0.101 µg/Kg10/11/2001 20-31-101101 609713 4741759 20 0308029-15 Heptachlorobiphenyls 66.2 µg/Kg 0.0552 µg/Kg10/11/2001 20-31-101101 609713 4741759 20 0308029-15 Octachlorobiphenyls 21.4 µg/Kg 0.0504 µg/Kg10/11/2001 20-31-101101 609713 4741759 20 0308029-15 Nonachlorobiphenyls 12.3 µg/Kg 0.128 µg/Kg10/11/2001 20-31-101101 609713 4741759 20 0308029-15 Decachlorobiphenyl 1.37 µg/Kg 0.0599 µg/Kg10/11/2001 20-31-101101 609713 4741759 20 0308029-15 Total Homologs 873 µg/Kg 0.0599 µg/Kg10/11/2001 20-31-101101 609713 4741759 20 0308029-15 Percent Lipids 2.9 % 0.1 %10/11/2001 20-31-101101 609713 4741759 20 0308029-15 Percent Moisture 70.3 % 0.1 %9/22/2001 21-02-092201 609281 4740033 21 0308030-01 Cl2-BZ#8 0.101 U µg/Kg 0.101 µg/Kg9/22/2001 21-02-092201 609281 4740033 21 0308030-01 Cl3-BZ#18 0.223 U µg/Kg 0.223 µg/Kg9/22/2001 21-02-092201 609281 4740033 21 0308030-01 Cl3-BZ#31/#28 11.4 J µg/Kg 1.61 µg/Kg9/22/2001 21-02-092201 609281 4740033 21 0308030-01 Cl4-BZ#44 0.176 J µg/Kg 0.153 µg/Kg9/22/2001 21-02-092201 609281 4740033 21 0308030-01 Cl4-BZ#45 0.205 U µg/Kg 0.205 µg/Kg9/22/2001 21-02-092201 609281 4740033 21 0308030-01 Cl4-BZ#47 2.06 µg/Kg 0.260 µg/Kg9/22/2001 21-02-092201 609281 4740033 21 0308030-01 Cl4-BZ#49 0.526 J µg/Kg 0.127 µg/Kg9/22/2001 21-02-092201 609281 4740033 21 0308030-01 Cl4-BZ#52 0.456 J µg/Kg 0.145 µg/Kg9/22/2001 21-02-092201 609281 4740033 21 0308030-01 Cl4-BZ#56 4.58 µg/Kg 0.0760 µg/Kg9/22/2001 21-02-092201 609281 4740033 21 0308030-01 Cl4-BZ#66 17.8 µg/Kg 0.102 µg/Kg9/22/2001 21-02-092201 609281 4740033 21 0308030-01 Cl4-BZ#70 4.73 J µg/Kg 0.0889 µg/Kg9/22/2001 21-02-092201 609281 4740033 21 0308030-01 Cl4-BZ#74 9.52 µg/Kg 0.157 µg/Kg9/22/2001 21-02-092201 609281 4740033 21 0308030-01 Cl4-BZ#77 0.140 U µg/Kg 0.140 µg/Kg9/22/2001 21-02-092201 609281 4740033 21 0308030-01 Cl4-BZ#81 0.139 U µg/Kg 0.139 µg/Kg9/22/2001 21-02-092201 609281 4740033 21 0308030-01 Cl5-BZ#87 5.80 µg/Kg 0.0620 µg/Kg9/22/2001 21-02-092201 609281 4740033 21 0308030-01 Cl5-BZ#95 0.246 J µg/Kg 0.0480 µg/Kg9/22/2001 21-02-092201 609281 4740033 21 0308030-01 Cl5-BZ#99 19.5 µg/Kg 0.0328 µg/Kg9/22/2001 21-02-092201 609281 4740033 21 0308030-01 Cl5-BZ#101 1.54 µg/Kg 0.0936 µg/Kg9/22/2001 21-02-092201 609281 4740033 21 0308030-01 Cl5-BZ#105 15.0 µg/Kg 0.0456 µg/Kg9/22/2001 21-02-092201 609281 4740033 21 0308030-01 Cl5-BZ#110 0.854 J µg/Kg 0.0889 µg/Kg



Extracted 7/30/04




SITE NUMBER



9/22/2001 21-02-092201 609281 4740033 21 0308030-01 Cl5-BZ#114 0.772 µg/Kg 0.0409 µg/Kg9/22/2001 21-02-092201 609281 4740033 21 0308030-01 Cl5-BZ#118 39.4 µg/Kg 0.0959 µg/Kg9/22/2001 21-02-092201 609281 4740033 21 0308030-01 Cl5-BZ#123 0.0807 U µg/Kg 0.0807 µg/Kg9/22/2001 21-02-092201 609281 4740033 21 0308030-01 Cl5-BZ#126 0.0714 U µg/Kg 0.0714 µg/Kg9/22/2001 21-02-092201 609281 4740033 21 0308030-01 Cl6-BZ#128 4.59 J µg/Kg 0.0643 µg/Kg9/22/2001 21-02-092201 609281 4740033 21 0308030-01 Cl6-BZ#138 69.8 µg/Kg 0.0924 µg/Kg9/22/2001 21-02-092201 609281 4740033 21 0308030-01 Cl6-BZ#146 8.40 µg/Kg 0.0585 µg/Kg9/22/2001 21-02-092201 609281 4740033 21 0308030-01 Cl6-BZ#149 0.866 µg/Kg 0.0749 µg/Kg9/22/2001 21-02-092201 609281 4740033 21 0308030-01 Cl6-BZ#151 0.345 J µg/Kg 0.124 µg/Kg9/22/2001 21-02-092201 609281 4740033 21 0308030-01 Cl6-BZ#153 63.2 µg/Kg 0.106 µg/Kg9/22/2001 21-02-092201 609281 4740033 21 0308030-01 Cl6-BZ#156 4.78 µg/Kg 0.0760 µg/Kg9/22/2001 21-02-092201 609281 4740033 21 0308030-01 Cl6-BZ#157 1.00 µg/Kg 0.0597 µg/Kg9/22/2001 21-02-092201 609281 4740033 21 0308030-01 Cl6-BZ#158 0.994 µg/Kg 0.0503 µg/Kg9/22/2001 21-02-092201 609281 4740033 21 0308030-01 Cl6-BZ#167 2.73 µg/Kg 0.0643 µg/Kg9/22/2001 21-02-092201 609281 4740033 21 0308030-01 Cl6-BZ#169 0.207 U µg/Kg 0.207 µg/Kg9/22/2001 21-02-092201 609281 4740033 21 0308030-01 Cl7-BZ#170 0.241 U µg/Kg 0.241 µg/Kg9/22/2001 21-02-092201 609281 4740033 21 0308030-01 Cl7-BZ#174 0.0491 U µg/Kg 0.0491 µg/Kg9/22/2001 21-02-092201 609281 4740033 21 0308030-01 Cl7-BZ#177 1.81 µg/Kg 0.0690 µg/Kg9/22/2001 21-02-092201 609281 4740033 21 0308030-01 Cl7-BZ#180 13.1 µg/Kg 0.103 µg/Kg9/22/2001 21-02-092201 609281 4740033 21 0308030-01 Cl7-BZ#183 1.97 µg/Kg 0.0468 µg/Kg9/22/2001 21-02-092201 609281 4740033 21 0308030-01 Cl7-BZ#187 9.60 µg/Kg 0.0515 µg/Kg9/22/2001 21-02-092201 609281 4740033 21 0308030-01 Cl7-BZ#189 0.0924 U µg/Kg 0.0924 µg/Kg9/22/2001 21-02-092201 609281 4740033 21 0308030-01 Cl8-BZ#194 0.252 J µg/Kg 0.108 µg/Kg9/22/2001 21-02-092201 609281 4740033 21 0308030-01 Cl8-BZ#195 1.15 J µg/Kg 0.106 µg/Kg9/22/2001 21-02-092201 609281 4740033 21 0308030-01 Cl8-BZ#201 2.98 µg/Kg 0.0936 µg/Kg9/22/2001 21-02-092201 609281 4740033 21 0308030-01 Cl9-BZ#206 3.40 J µg/Kg 0.125 µg/Kg9/22/2001 21-02-092201 609281 4740033 21 0308030-01 Cl10-BZ#209 0.895 J µg/Kg 0.0585 µg/Kg9/22/2001 21-02-092201 609281 4740033 21 0308030-01 Monochlorobiphenyls 3.44 U µg/Kg 3.44 µg/Kg9/22/2001 21-02-092201 609281 4740033 21 0308030-01 Dichlorobiphenyls 0.287 J µg/Kg 0.101 µg/Kg9/22/2001 21-02-092201 609281 4740033 21 0308030-01 Trichlorobiphenyls 11.1 J µg/Kg 0.345 µg/Kg9/22/2001 21-02-092201 609281 4740033 21 0308030-01 Tetrachlorobiphenyls 49.2 µg/Kg 0.0538 µg/Kg9/22/2001 21-02-092201 609281 4740033 21 0308030-01 Pentachlorobiphenyls 136 µg/Kg 0.0620 µg/Kg9/22/2001 21-02-092201 609281 4740033 21 0308030-01 Hexachlorobiphenyls 175 µg/Kg 0.0983 µg/Kg9/22/2001 21-02-092201 609281 4740033 21 0308030-01 Heptachlorobiphenyls 45.4 µg/Kg 0.0538 µg/Kg



Extracted 7/30/04




SITE NUMBER



9/22/2001 21-02-092201 609281 4740033 21 0308030-01 Octachlorobiphenyls 13.1 µg/Kg 0.0491 µg/Kg9/22/2001 21-02-092201 609281 4740033 21 0308030-01 Nonachlorobiphenyls 5.22 µg/Kg 0.125 µg/Kg9/22/2001 21-02-092201 609281 4740033 21 0308030-01 Decachlorobiphenyl 0.895 µg/Kg 0.0585 µg/Kg9/22/2001 21-02-092201 609281 4740033 21 0308030-01 Total Homologs 436 µg/Kg 0.0585 µg/Kg9/22/2001 21-02-092201 609281 4740033 21 0308030-01 Percent Lipids 2.4 J % 0.1 %9/22/2001 21-02-092201 609281 4740033 21 0308030-01 Percent Moisture 77.2 % 0.1 %9/22/2001 21-03-092201 609281 4740033 21 0308030-02 Cl2-BZ#8 0.120 U µg/Kg 0.120 µg/Kg9/22/2001 21-03-092201 609281 4740033 21 0308030-02 Cl3-BZ#18 0.267 U µg/Kg 0.267 µg/Kg9/22/2001 21-03-092201 609281 4740033 21 0308030-02 Cl3-BZ#31/#28 6.12 J µg/Kg 1.93 µg/Kg9/22/2001 21-03-092201 609281 4740033 21 0308030-02 Cl4-BZ#44 0.183 U µg/Kg 0.183 µg/Kg9/22/2001 21-03-092201 609281 4740033 21 0308030-02 Cl4-BZ#45 0.245 U µg/Kg 0.245 µg/Kg9/22/2001 21-03-092201 609281 4740033 21 0308030-02 Cl4-BZ#47 2.29 µg/Kg 0.311 µg/Kg9/22/2001 21-03-092201 609281 4740033 21 0308030-02 Cl4-BZ#49 0.560 J µg/Kg 0.153 µg/Kg9/22/2001 21-03-092201 609281 4740033 21 0308030-02 Cl4-BZ#52 0.448 J µg/Kg 0.174 µg/Kg9/22/2001 21-03-092201 609281 4740033 21 0308030-02 Cl4-BZ#56 4.40 µg/Kg 0.0910 µg/Kg9/22/2001 21-03-092201 609281 4740033 21 0308030-02 Cl4-BZ#66 15.2 µg/Kg 0.122 µg/Kg9/22/2001 21-03-092201 609281 4740033 21 0308030-02 Cl4-BZ#70 3.84 µg/Kg 0.106 µg/Kg9/22/2001 21-03-092201 609281 4740033 21 0308030-02 Cl4-BZ#74 8.39 µg/Kg 0.188 µg/Kg9/22/2001 21-03-092201 609281 4740033 21 0308030-02 Cl4-BZ#77 0.168 U µg/Kg 0.168 µg/Kg9/22/2001 21-03-092201 609281 4740033 21 0308030-02 Cl4-BZ#81 0.167 U µg/Kg 0.167 µg/Kg9/22/2001 21-03-092201 609281 4740033 21 0308030-02 Cl5-BZ#87 6.38 µg/Kg 0.0742 µg/Kg9/22/2001 21-03-092201 609281 4740033 21 0308030-02 Cl5-BZ#95 0.245 J µg/Kg 0.0574 µg/Kg9/22/2001 21-03-092201 609281 4740033 21 0308030-02 Cl5-BZ#99 20.2 µg/Kg 0.0392 µg/Kg9/22/2001 21-03-092201 609281 4740033 21 0308030-02 Cl5-BZ#101 2.23 µg/Kg 0.112 µg/Kg9/22/2001 21-03-092201 609281 4740033 21 0308030-02 Cl5-BZ#105 16.1 µg/Kg 0.0546 µg/Kg9/22/2001 21-03-092201 609281 4740033 21 0308030-02 Cl5-BZ#110 0.819 µg/Kg 0.106 µg/Kg9/22/2001 21-03-092201 609281 4740033 21 0308030-02 Cl5-BZ#114 0.749 µg/Kg 0.0490 µg/Kg9/22/2001 21-03-092201 609281 4740033 21 0308030-02 Cl5-BZ#118 44.7 µg/Kg 0.115 µg/Kg9/22/2001 21-03-092201 609281 4740033 21 0308030-02 Cl5-BZ#123 0.0966 U µg/Kg 0.0966 µg/Kg9/22/2001 21-03-092201 609281 4740033 21 0308030-02 Cl5-BZ#126 0.0854 U µg/Kg 0.0854 µg/Kg9/22/2001 21-03-092201 609281 4740033 21 0308030-02 Cl6-BZ#128 5.80 µg/Kg 0.0770 µg/Kg9/22/2001 21-03-092201 609281 4740033 21 0308030-02 Cl6-BZ#138 81.6 µg/Kg 0.111 µg/Kg9/22/2001 21-03-092201 609281 4740033 21 0308030-02 Cl6-BZ#146 10.3 µg/Kg 0.0700 µg/Kg9/22/2001 21-03-092201 609281 4740033 21 0308030-02 Cl6-BZ#149 1.26 µg/Kg 0.0896 µg/Kg



Extracted 7/30/04




SITE NUMBER



9/22/2001 21-03-092201 609281 4740033 21 0308030-02 Cl6-BZ#151 0.511 J µg/Kg 0.148 µg/Kg9/22/2001 21-03-092201 609281 4740033 21 0308030-02 Cl6-BZ#153 75.2 µg/Kg 0.127 µg/Kg9/22/2001 21-03-092201 609281 4740033 21 0308030-02 Cl6-BZ#156 5.36 µg/Kg 0.0910 µg/Kg9/22/2001 21-03-092201 609281 4740033 21 0308030-02 Cl6-BZ#157 1.11 µg/Kg 0.0714 µg/Kg9/22/2001 21-03-092201 609281 4740033 21 0308030-02 Cl6-BZ#158 1.30 µg/Kg 0.0602 µg/Kg9/22/2001 21-03-092201 609281 4740033 21 0308030-02 Cl6-BZ#167 3.50 µg/Kg 0.0770 µg/Kg9/22/2001 21-03-092201 609281 4740033 21 0308030-02 Cl6-BZ#169 0.248 U µg/Kg 0.248 µg/Kg9/22/2001 21-03-092201 609281 4740033 21 0308030-02 Cl7-BZ#170 0.289 U µg/Kg 0.289 µg/Kg9/22/2001 21-03-092201 609281 4740033 21 0308030-02 Cl7-BZ#174 0.0588 U µg/Kg 0.0588 µg/Kg9/22/2001 21-03-092201 609281 4740033 21 0308030-02 Cl7-BZ#177 1.58 µg/Kg 0.0826 µg/Kg9/22/2001 21-03-092201 609281 4740033 21 0308030-02 Cl7-BZ#180 16.5 µg/Kg 0.123 µg/Kg9/22/2001 21-03-092201 609281 4740033 21 0308030-02 Cl7-BZ#183 2.03 µg/Kg 0.0560 µg/Kg9/22/2001 21-03-092201 609281 4740033 21 0308030-02 Cl7-BZ#187 14.8 µg/Kg 0.0616 µg/Kg9/22/2001 21-03-092201 609281 4740033 21 0308030-02 Cl7-BZ#189 0.111 U µg/Kg 0.111 µg/Kg9/22/2001 21-03-092201 609281 4740033 21 0308030-02 Cl8-BZ#194 0.721 µg/Kg 0.129 µg/Kg9/22/2001 21-03-092201 609281 4740033 21 0308030-02 Cl8-BZ#195 1.60 µg/Kg 0.127 µg/Kg9/22/2001 21-03-092201 609281 4740033 21 0308030-02 Cl8-BZ#201 3.77 µg/Kg 0.112 µg/Kg9/22/2001 21-03-092201 609281 4740033 21 0308030-02 Cl9-BZ#206 5.94 µg/Kg 0.150 µg/Kg9/22/2001 21-03-092201 609281 4740033 21 0308030-02 Cl10-BZ#209 1.34 µg/Kg 0.0700 µg/Kg9/22/2001 21-03-092201 609281 4740033 21 0308030-02 Monochlorobiphenyls 4.12 U µg/Kg 4.12 µg/Kg9/22/2001 21-03-092201 609281 4740033 21 0308030-02 Dichlorobiphenyls 0.147 J µg/Kg 0.120 µg/Kg9/22/2001 21-03-092201 609281 4740033 21 0308030-02 Trichlorobiphenyls 5.23 µg/Kg 0.413 µg/Kg9/22/2001 21-03-092201 609281 4740033 21 0308030-02 Tetrachlorobiphenyls 43.5 µg/Kg 0.0644 µg/Kg9/22/2001 21-03-092201 609281 4740033 21 0308030-02 Pentachlorobiphenyls 148 µg/Kg 0.0742 µg/Kg9/22/2001 21-03-092201 609281 4740033 21 0308030-02 Hexachlorobiphenyls 203 µg/Kg 0.118 µg/Kg9/22/2001 21-03-092201 609281 4740033 21 0308030-02 Heptachlorobiphenyls 65.5 µg/Kg 0.0644 µg/Kg9/22/2001 21-03-092201 609281 4740033 21 0308030-02 Octachlorobiphenyls 20.9 µg/Kg 0.0588 µg/Kg9/22/2001 21-03-092201 609281 4740033 21 0308030-02 Nonachlorobiphenyls 9.01 µg/Kg 0.150 µg/Kg9/22/2001 21-03-092201 609281 4740033 21 0308030-02 Decachlorobiphenyl 1.34 µg/Kg 0.0700 µg/Kg9/22/2001 21-03-092201 609281 4740033 21 0308030-02 Total Homologs 497 µg/Kg 0.0700 µg/Kg9/22/2001 21-03-092201 609281 4740033 21 0308030-02 Percent Lipids 2.0 % 0.1 %9/22/2001 21-03-092201 609281 4740033 21 0308030-02 Percent Moisture 70.6 % 0.1 %9/22/2001 21-06-092201 609281 4740033 21 0308030-03 Cl2-BZ#8 0.117 U µg/Kg 0.117 µg/Kg9/22/2001 21-06-092201 609281 4740033 21 0308030-03 Cl3-BZ#18 0.259 U µg/Kg 0.259 µg/Kg



Extracted 7/30/04




SITE NUMBER



9/22/2001 21-06-092201 609281 4740033 21 0308030-03 Cl3-BZ#31/#28 4.37 J µg/Kg 1.87 µg/Kg9/22/2001 21-06-092201 609281 4740033 21 0308030-03 Cl4-BZ#44 0.178 U µg/Kg 0.178 µg/Kg9/22/2001 21-06-092201 609281 4740033 21 0308030-03 Cl4-BZ#45 0.237 U µg/Kg 0.237 µg/Kg9/22/2001 21-06-092201 609281 4740033 21 0308030-03 Cl4-BZ#47 3.56 µg/Kg 0.301 µg/Kg9/22/2001 21-06-092201 609281 4740033 21 0308030-03 Cl4-BZ#49 0.644 J µg/Kg 0.148 µg/Kg9/22/2001 21-06-092201 609281 4740033 21 0308030-03 Cl4-BZ#52 0.346 J µg/Kg 0.168 µg/Kg9/22/2001 21-06-092201 609281 4740033 21 0308030-03 Cl4-BZ#56 5.36 µg/Kg 0.0881 µg/Kg9/22/2001 21-06-092201 609281 4740033 21 0308030-03 Cl4-BZ#66 26.7 µg/Kg 0.118 µg/Kg9/22/2001 21-06-092201 609281 4740033 21 0308030-03 Cl4-BZ#70 5.50 µg/Kg 0.103 µg/Kg9/22/2001 21-06-092201 609281 4740033 21 0308030-03 Cl4-BZ#74 9.71 µg/Kg 0.182 µg/Kg9/22/2001 21-06-092201 609281 4740033 21 0308030-03 Cl4-BZ#77 0.163 U µg/Kg 0.163 µg/Kg9/22/2001 21-06-092201 609281 4740033 21 0308030-03 Cl4-BZ#81 0.161 U µg/Kg 0.161 µg/Kg9/22/2001 21-06-092201 609281 4740033 21 0308030-03 Cl5-BZ#87 8.69 µg/Kg 0.0718 µg/Kg9/22/2001 21-06-092201 609281 4740033 21 0308030-03 Cl5-BZ#95 0.264 J µg/Kg 0.0556 µg/Kg9/22/2001 21-06-092201 609281 4740033 21 0308030-03 Cl5-BZ#99 30.0 µg/Kg 0.0380 µg/Kg9/22/2001 21-06-092201 609281 4740033 21 0308030-03 Cl5-BZ#101 3.36 µg/Kg 0.108 µg/Kg9/22/2001 21-06-092201 609281 4740033 21 0308030-03 Cl5-BZ#105 25.4 µg/Kg 0.0529 µg/Kg9/22/2001 21-06-092201 609281 4740033 21 0308030-03 Cl5-BZ#110 1.14 µg/Kg 0.103 µg/Kg9/22/2001 21-06-092201 609281 4740033 21 0308030-03 Cl5-BZ#114 1.05 µg/Kg 0.0474 µg/Kg9/22/2001 21-06-092201 609281 4740033 21 0308030-03 Cl5-BZ#118 68.2 µg/Kg 0.111 µg/Kg9/22/2001 21-06-092201 609281 4740033 21 0308030-03 Cl5-BZ#123 0.0935 U µg/Kg 0.0935 µg/Kg9/22/2001 21-06-092201 609281 4740033 21 0308030-03 Cl5-BZ#126 0.0827 U µg/Kg 0.0827 µg/Kg9/22/2001 21-06-092201 609281 4740033 21 0308030-03 Cl6-BZ#128 8.94 µg/Kg 0.0746 µg/Kg9/22/2001 21-06-092201 609281 4740033 21 0308030-03 Cl6-BZ#138 132 µg/Kg 0.107 µg/Kg9/22/2001 21-06-092201 609281 4740033 21 0308030-03 Cl6-BZ#146 15.9 µg/Kg 0.0678 µg/Kg9/22/2001 21-06-092201 609281 4740033 21 0308030-03 Cl6-BZ#149 1.86 µg/Kg 0.0868 µg/Kg9/22/2001 21-06-092201 609281 4740033 21 0308030-03 Cl6-BZ#151 0.651 J µg/Kg 0.144 µg/Kg9/22/2001 21-06-092201 609281 4740033 21 0308030-03 Cl6-BZ#153 108 µg/Kg 0.123 µg/Kg9/22/2001 21-06-092201 609281 4740033 21 0308030-03 Cl6-BZ#156 9.07 µg/Kg 0.0881 µg/Kg9/22/2001 21-06-092201 609281 4740033 21 0308030-03 Cl6-BZ#157 1.62 µg/Kg 0.0691 µg/Kg9/22/2001 21-06-092201 609281 4740033 21 0308030-03 Cl6-BZ#158 2.18 µg/Kg 0.0583 µg/Kg9/22/2001 21-06-092201 609281 4740033 21 0308030-03 Cl6-BZ#167 5.31 µg/Kg 0.0746 µg/Kg9/22/2001 21-06-092201 609281 4740033 21 0308030-03 Cl6-BZ#169 0.240 U µg/Kg 0.240 µg/Kg9/22/2001 21-06-092201 609281 4740033 21 0308030-03 Cl7-BZ#170 15.7 µg/Kg 0.279 µg/Kg



Extracted 7/30/04




SITE NUMBER



9/22/2001 21-06-092201 609281 4740033 21 0308030-03 Cl7-BZ#174 0.0569 U µg/Kg 0.0569 µg/Kg9/22/2001 21-06-092201 609281 4740033 21 0308030-03 Cl7-BZ#177 3.05 µg/Kg 0.0800 µg/Kg9/22/2001 21-06-092201 609281 4740033 21 0308030-03 Cl7-BZ#180 22.2 µg/Kg 0.119 µg/Kg9/22/2001 21-06-092201 609281 4740033 21 0308030-03 Cl7-BZ#183 3.14 µg/Kg 0.0542 µg/Kg9/22/2001 21-06-092201 609281 4740033 21 0308030-03 Cl7-BZ#187 20.8 µg/Kg 0.0596 µg/Kg9/22/2001 21-06-092201 609281 4740033 21 0308030-03 Cl7-BZ#189 0.107 U µg/Kg 0.107 µg/Kg9/22/2001 21-06-092201 609281 4740033 21 0308030-03 Cl8-BZ#194 0.468 J µg/Kg 0.125 µg/Kg9/22/2001 21-06-092201 609281 4740033 21 0308030-03 Cl8-BZ#195 1.99 µg/Kg 0.123 µg/Kg9/22/2001 21-06-092201 609281 4740033 21 0308030-03 Cl8-BZ#201 5.36 µg/Kg 0.108 µg/Kg9/22/2001 21-06-092201 609281 4740033 21 0308030-03 Cl9-BZ#206 7.66 µg/Kg 0.145 µg/Kg9/22/2001 21-06-092201 609281 4740033 21 0308030-03 Cl10-BZ#209 2.50 µg/Kg 0.0678 µg/Kg9/22/2001 21-06-092201 609281 4740033 21 0308030-03 Monochlorobiphenyls 3.99 U µg/Kg 3.99 µg/Kg9/22/2001 21-06-092201 609281 4740033 21 0308030-03 Dichlorobiphenyls 0.169 J µg/Kg 0.117 µg/Kg9/22/2001 21-06-092201 609281 4740033 21 0308030-03 Trichlorobiphenyls 4.39 µg/Kg 0.400 µg/Kg9/22/2001 21-06-092201 609281 4740033 21 0308030-03 Tetrachlorobiphenyls 66.1 µg/Kg 0.0624 µg/Kg9/22/2001 21-06-092201 609281 4740033 21 0308030-03 Pentachlorobiphenyls 231 µg/Kg 0.0718 µg/Kg9/22/2001 21-06-092201 609281 4740033 21 0308030-03 Hexachlorobiphenyls 320 µg/Kg 0.114 µg/Kg9/22/2001 21-06-092201 609281 4740033 21 0308030-03 Heptachlorobiphenyls 76.0 µg/Kg 0.0624 µg/Kg9/22/2001 21-06-092201 609281 4740033 21 0308030-03 Octachlorobiphenyls 25.4 µg/Kg 0.0569 µg/Kg9/22/2001 21-06-092201 609281 4740033 21 0308030-03 Nonachlorobiphenyls 11.9 µg/Kg 0.145 µg/Kg9/22/2001 21-06-092201 609281 4740033 21 0308030-03 Decachlorobiphenyl 2.50 µg/Kg 0.0678 µg/Kg9/22/2001 21-06-092201 609281 4740033 21 0308030-03 Total Homologs 737 µg/Kg 0.0678 µg/Kg9/22/2001 21-06-092201 609281 4740033 21 0308030-03 Percent Lipids 2.6 % 0.1 %9/22/2001 21-06-092201 609281 4740033 21 0308030-03 Percent Moisture 72.3 % 0.1 %9/26/2001 21-18-092601 609281 4740033 21 0308030-04 Cl2-BZ#8 0.119 U µg/Kg 0.119 µg/Kg9/26/2001 21-18-092601 609281 4740033 21 0308030-04 Cl3-BZ#18 0.265 U µg/Kg 0.265 µg/Kg9/26/2001 21-18-092601 609281 4740033 21 0308030-04 Cl3-BZ#31/#28 12.3 µg/Kg 1.91 µg/Kg9/26/2001 21-18-092601 609281 4740033 21 0308030-04 Cl4-BZ#44 0.201 J µg/Kg 0.182 µg/Kg9/26/2001 21-18-092601 609281 4740033 21 0308030-04 Cl4-BZ#45 0.243 U µg/Kg 0.243 µg/Kg9/26/2001 21-18-092601 609281 4740033 21 0308030-04 Cl4-BZ#47 7.35 µg/Kg 0.308 µg/Kg9/26/2001 21-18-092601 609281 4740033 21 0308030-04 Cl4-BZ#49 1.36 µg/Kg 0.151 µg/Kg9/26/2001 21-18-092601 609281 4740033 21 0308030-04 Cl4-BZ#52 2.03 µg/Kg 0.172 µg/Kg9/26/2001 21-18-092601 609281 4740033 21 0308030-04 Cl4-BZ#56 5.96 µg/Kg 0.0902 µg/Kg9/26/2001 21-18-092601 609281 4740033 21 0308030-04 Cl4-BZ#66 26.9 µg/Kg 0.121 µg/Kg



Extracted 7/30/04




SITE NUMBER



9/26/2001 21-18-092601 609281 4740033 21 0308030-04 Cl4-BZ#70 8.35 µg/Kg 0.105 µg/Kg9/26/2001 21-18-092601 609281 4740033 21 0308030-04 Cl4-BZ#74 14.1 µg/Kg 0.186 µg/Kg9/26/2001 21-18-092601 609281 4740033 21 0308030-04 Cl4-BZ#77 0.167 U µg/Kg 0.167 µg/Kg9/26/2001 21-18-092601 609281 4740033 21 0308030-04 Cl4-BZ#81 0.165 U µg/Kg 0.165 µg/Kg9/26/2001 21-18-092601 609281 4740033 21 0308030-04 Cl5-BZ#87 12.3 µg/Kg 0.0736 µg/Kg9/26/2001 21-18-092601 609281 4740033 21 0308030-04 Cl5-BZ#95 1.19 µg/Kg 0.0569 µg/Kg9/26/2001 21-18-092601 609281 4740033 21 0308030-04 Cl5-BZ#99 39.9 µg/Kg 0.0389 µg/Kg9/26/2001 21-18-092601 609281 4740033 21 0308030-04 Cl5-BZ#101 4.64 µg/Kg 0.111 µg/Kg9/26/2001 21-18-092601 609281 4740033 21 0308030-04 Cl5-BZ#105 23.8 µg/Kg 0.0541 µg/Kg9/26/2001 21-18-092601 609281 4740033 21 0308030-04 Cl5-BZ#110 3.90 µg/Kg 0.105 µg/Kg9/26/2001 21-18-092601 609281 4740033 21 0308030-04 Cl5-BZ#114 1.40 µg/Kg 0.0486 µg/Kg9/26/2001 21-18-092601 609281 4740033 21 0308030-04 Cl5-BZ#118 64.8 µg/Kg 0.114 µg/Kg9/26/2001 21-18-092601 609281 4740033 21 0308030-04 Cl5-BZ#123 0.0958 U µg/Kg 0.0958 µg/Kg9/26/2001 21-18-092601 609281 4740033 21 0308030-04 Cl5-BZ#126 0.0847 U µg/Kg 0.0847 µg/Kg9/26/2001 21-18-092601 609281 4740033 21 0308030-04 Cl6-BZ#128 9.14 µg/Kg 0.0764 µg/Kg9/26/2001 21-18-092601 609281 4740033 21 0308030-04 Cl6-BZ#138 130 µg/Kg 0.110 µg/Kg9/26/2001 21-18-092601 609281 4740033 21 0308030-04 Cl6-BZ#146 15.5 µg/Kg 0.0694 µg/Kg9/26/2001 21-18-092601 609281 4740033 21 0308030-04 Cl6-BZ#149 4.62 µg/Kg 0.0889 µg/Kg9/26/2001 21-18-092601 609281 4740033 21 0308030-04 Cl6-BZ#151 1.35 µg/Kg 0.147 µg/Kg9/26/2001 21-18-092601 609281 4740033 21 0308030-04 Cl6-BZ#153 104 µg/Kg 0.126 µg/Kg9/26/2001 21-18-092601 609281 4740033 21 0308030-04 Cl6-BZ#156 7.96 µg/Kg 0.0902 µg/Kg9/26/2001 21-18-092601 609281 4740033 21 0308030-04 Cl6-BZ#157 1.61 µg/Kg 0.0708 µg/Kg9/26/2001 21-18-092601 609281 4740033 21 0308030-04 Cl6-BZ#158 2.00 µg/Kg 0.0597 µg/Kg9/26/2001 21-18-092601 609281 4740033 21 0308030-04 Cl6-BZ#167 4.76 µg/Kg 0.0764 µg/Kg9/26/2001 21-18-092601 609281 4740033 21 0308030-04 Cl6-BZ#169 0.246 U µg/Kg 0.246 µg/Kg9/26/2001 21-18-092601 609281 4740033 21 0308030-04 Cl7-BZ#170 15.8 µg/Kg 0.286 µg/Kg9/26/2001 21-18-092601 609281 4740033 21 0308030-04 Cl7-BZ#174 0.0583 U µg/Kg 0.0583 µg/Kg9/26/2001 21-18-092601 609281 4740033 21 0308030-04 Cl7-BZ#177 3.21 µg/Kg 0.0819 µg/Kg9/26/2001 21-18-092601 609281 4740033 21 0308030-04 Cl7-BZ#180 24.2 µg/Kg 0.122 µg/Kg9/26/2001 21-18-092601 609281 4740033 21 0308030-04 Cl7-BZ#183 3.79 µg/Kg 0.0555 µg/Kg9/26/2001 21-18-092601 609281 4740033 21 0308030-04 Cl7-BZ#187 20.1 µg/Kg 0.0611 µg/Kg9/26/2001 21-18-092601 609281 4740033 21 0308030-04 Cl7-BZ#189 0.110 U µg/Kg 0.110 µg/Kg9/26/2001 21-18-092601 609281 4740033 21 0308030-04 Cl8-BZ#194 3.94 µg/Kg 0.128 µg/Kg9/26/2001 21-18-092601 609281 4740033 21 0308030-04 Cl8-BZ#195 1.76 µg/Kg 0.126 µg/Kg



Extracted 7/30/04




SITE NUMBER



9/26/2001 21-18-092601 609281 4740033 21 0308030-04 Cl8-BZ#201 4.78 µg/Kg 0.111 µg/Kg9/26/2001 21-18-092601 609281 4740033 21 0308030-04 Cl9-BZ#206 5.84 µg/Kg 0.149 µg/Kg9/26/2001 21-18-092601 609281 4740033 21 0308030-04 Cl10-BZ#209 3.51 µg/Kg 0.0694 µg/Kg9/26/2001 21-18-092601 609281 4740033 21 0308030-04 Monochlorobiphenyls 4.08 U µg/Kg 4.08 µg/Kg9/26/2001 21-18-092601 609281 4740033 21 0308030-04 Dichlorobiphenyls 0.153 J µg/Kg 0.119 µg/Kg9/26/2001 21-18-092601 609281 4740033 21 0308030-04 Trichlorobiphenyls 5.80 µg/Kg 0.410 µg/Kg9/26/2001 21-18-092601 609281 4740033 21 0308030-04 Tetrachlorobiphenyls 83.3 µg/Kg 0.0639 µg/Kg9/26/2001 21-18-092601 609281 4740033 21 0308030-04 Pentachlorobiphenyls 250 µg/Kg 0.0736 µg/Kg9/26/2001 21-18-092601 609281 4740033 21 0308030-04 Hexachlorobiphenyls 314 µg/Kg 0.117 µg/Kg9/26/2001 21-18-092601 609281 4740033 21 0308030-04 Heptachlorobiphenyls 76.6 µg/Kg 0.0639 µg/Kg9/26/2001 21-18-092601 609281 4740033 21 0308030-04 Octachlorobiphenyls 20.8 µg/Kg 0.0583 µg/Kg9/26/2001 21-18-092601 609281 4740033 21 0308030-04 Nonachlorobiphenyls 9.41 µg/Kg 0.149 µg/Kg9/26/2001 21-18-092601 609281 4740033 21 0308030-04 Decachlorobiphenyl 3.51 µg/Kg 0.0694 µg/Kg9/26/2001 21-18-092601 609281 4740033 21 0308030-04 Total Homologs 764 µg/Kg 0.0694 µg/Kg9/26/2001 21-18-092601 609281 4740033 21 0308030-04 Percent Lipids 3.4 % 0.1 %9/26/2001 21-18-092601 609281 4740033 21 0308030-04 Percent Moisture 73.1 % 0.1 %

10/16/2001 22-15-101601 602339 4715386 22 0308030-05 Cl2-BZ#8 0.121 U µg/Kg 0.121 µg/Kg10/16/2001 22-15-101601 602339 4715386 22 0308030-05 Cl3-BZ#18 0.268 U µg/Kg 0.268 µg/Kg10/16/2001 22-15-101601 602339 4715386 22 0308030-05 Cl3-BZ#31/#28 1.93 U µg/Kg 1.93 µg/Kg10/16/2001 22-15-101601 602339 4715386 22 0308030-05 Cl4-BZ#44 0.184 U µg/Kg 0.184 µg/Kg10/16/2001 22-15-101601 602339 4715386 22 0308030-05 Cl4-BZ#45 0.245 U µg/Kg 0.245 µg/Kg10/16/2001 22-15-101601 602339 4715386 22 0308030-05 Cl4-BZ#47 1.18 J µg/Kg 0.311 µg/Kg10/16/2001 22-15-101601 602339 4715386 22 0308030-05 Cl4-BZ#49 0.153 U µg/Kg 0.153 µg/Kg10/16/2001 22-15-101601 602339 4715386 22 0308030-05 Cl4-BZ#52 0.217 J µg/Kg 0.174 µg/Kg10/16/2001 22-15-101601 602339 4715386 22 0308030-05 Cl4-BZ#56 0.610 µg/Kg 0.0911 µg/Kg10/16/2001 22-15-101601 602339 4715386 22 0308030-05 Cl4-BZ#66 1.87 µg/Kg 0.122 µg/Kg10/16/2001 22-15-101601 602339 4715386 22 0308030-05 Cl4-BZ#70 0.491 J µg/Kg 0.106 µg/Kg10/16/2001 22-15-101601 602339 4715386 22 0308030-05 Cl4-BZ#74 0.960 µg/Kg 0.188 µg/Kg10/16/2001 22-15-101601 602339 4715386 22 0308030-05 Cl4-BZ#77 0.168 U µg/Kg 0.168 µg/Kg10/16/2001 22-15-101601 602339 4715386 22 0308030-05 Cl4-BZ#81 0.167 U µg/Kg 0.167 µg/Kg10/16/2001 22-15-101601 602339 4715386 22 0308030-05 Cl5-BZ#87 0.645 µg/Kg 0.0743 µg/Kg10/16/2001 22-15-101601 602339 4715386 22 0308030-05 Cl5-BZ#95 0.0575 U µg/Kg 0.0575 µg/Kg10/16/2001 22-15-101601 602339 4715386 22 0308030-05 Cl5-BZ#99 3.86 µg/Kg 0.0393 µg/Kg10/16/2001 22-15-101601 602339 4715386 22 0308030-05 Cl5-BZ#101 0.343 J µg/Kg 0.112 µg/Kg



Extracted 7/30/04




SITE NUMBER



10/16/2001 22-15-101601 602339 4715386 22 0308030-05 Cl5-BZ#105 1.83 µg/Kg 0.0547 µg/Kg10/16/2001 22-15-101601 602339 4715386 22 0308030-05 Cl5-BZ#110 0.106 U µg/Kg 0.106 µg/Kg10/16/2001 22-15-101601 602339 4715386 22 0308030-05 Cl5-BZ#114 0.196 J µg/Kg 0.0491 µg/Kg10/16/2001 22-15-101601 602339 4715386 22 0308030-05 Cl5-BZ#118 4.96 µg/Kg 0.115 µg/Kg10/16/2001 22-15-101601 602339 4715386 22 0308030-05 Cl5-BZ#123 0.0967 U µg/Kg 0.0967 µg/Kg10/16/2001 22-15-101601 602339 4715386 22 0308030-05 Cl5-BZ#126 0.0855 U µg/Kg 0.0855 µg/Kg10/16/2001 22-15-101601 602339 4715386 22 0308030-05 Cl6-BZ#128 0.834 µg/Kg 0.0771 µg/Kg10/16/2001 22-15-101601 602339 4715386 22 0308030-05 Cl6-BZ#138 13.3 µg/Kg 0.111 µg/Kg10/16/2001 22-15-101601 602339 4715386 22 0308030-05 Cl6-BZ#146 1.51 µg/Kg 0.0701 µg/Kg10/16/2001 22-15-101601 602339 4715386 22 0308030-05 Cl6-BZ#149 0.203 J µg/Kg 0.0897 µg/Kg10/16/2001 22-15-101601 602339 4715386 22 0308030-05 Cl6-BZ#151 0.149 U µg/Kg 0.149 µg/Kg10/16/2001 22-15-101601 602339 4715386 22 0308030-05 Cl6-BZ#153 15.0 µg/Kg 0.128 µg/Kg10/16/2001 22-15-101601 602339 4715386 22 0308030-05 Cl6-BZ#156 1.06 µg/Kg 0.0911 µg/Kg10/16/2001 22-15-101601 602339 4715386 22 0308030-05 Cl6-BZ#157 0.189 J µg/Kg 0.0715 µg/Kg10/16/2001 22-15-101601 602339 4715386 22 0308030-05 Cl6-BZ#158 0.336 µg/Kg 0.0603 µg/Kg10/16/2001 22-15-101601 602339 4715386 22 0308030-05 Cl6-BZ#167 0.526 µg/Kg 0.0771 µg/Kg10/16/2001 22-15-101601 602339 4715386 22 0308030-05 Cl6-BZ#169 0.248 U µg/Kg 0.248 µg/Kg10/16/2001 22-15-101601 602339 4715386 22 0308030-05 Cl7-BZ#170 0.289 U µg/Kg 0.289 µg/Kg10/16/2001 22-15-101601 602339 4715386 22 0308030-05 Cl7-BZ#174 0.0589 U µg/Kg 0.0589 µg/Kg10/16/2001 22-15-101601 602339 4715386 22 0308030-05 Cl7-BZ#177 0.0827 U µg/Kg 0.0827 µg/Kg10/16/2001 22-15-101601 602339 4715386 22 0308030-05 Cl7-BZ#180 6.15 µg/Kg 0.123 µg/Kg10/16/2001 22-15-101601 602339 4715386 22 0308030-05 Cl7-BZ#183 0.883 µg/Kg 0.0561 µg/Kg10/16/2001 22-15-101601 602339 4715386 22 0308030-05 Cl7-BZ#187 2.35 µg/Kg 0.0617 µg/Kg10/16/2001 22-15-101601 602339 4715386 22 0308030-05 Cl7-BZ#189 0.111 U µg/Kg 0.111 µg/Kg10/16/2001 22-15-101601 602339 4715386 22 0308030-05 Cl8-BZ#194 0.129 U µg/Kg 0.129 µg/Kg10/16/2001 22-15-101601 602339 4715386 22 0308030-05 Cl8-BZ#195 0.128 U µg/Kg 0.128 µg/Kg10/16/2001 22-15-101601 602339 4715386 22 0308030-05 Cl8-BZ#201 0.631 µg/Kg 0.112 µg/Kg10/16/2001 22-15-101601 602339 4715386 22 0308030-05 Cl9-BZ#206 2.06 µg/Kg 0.150 µg/Kg10/16/2001 22-15-101601 602339 4715386 22 0308030-05 Cl10-BZ#209 1.06 µg/Kg 0.0701 µg/Kg10/16/2001 22-15-101601 602339 4715386 22 0308030-05 Monochlorobiphenyls 4.12 U µg/Kg 4.12 µg/Kg10/16/2001 22-15-101601 602339 4715386 22 0308030-05 Dichlorobiphenyls 0.121 U µg/Kg 0.121 µg/Kg10/16/2001 22-15-101601 602339 4715386 22 0308030-05 Trichlorobiphenyls 0.414 U µg/Kg 0.414 µg/Kg10/16/2001 22-15-101601 602339 4715386 22 0308030-05 Tetrachlorobiphenyls 10.1 µg/Kg 0.0645 µg/Kg10/16/2001 22-15-101601 602339 4715386 22 0308030-05 Pentachlorobiphenyls 23.6 µg/Kg 0.0743 µg/Kg



Extracted 7/30/04




SITE NUMBER



10/16/2001 22-15-101601 602339 4715386 22 0308030-05 Hexachlorobiphenyls 37.4 µg/Kg 0.118 µg/Kg10/16/2001 22-15-101601 602339 4715386 22 0308030-05 Heptachlorobiphenyls 12.8 µg/Kg 0.0645 µg/Kg10/16/2001 22-15-101601 602339 4715386 22 0308030-05 Octachlorobiphenyls 3.20 µg/Kg 0.0589 µg/Kg10/16/2001 22-15-101601 602339 4715386 22 0308030-05 Nonachlorobiphenyls 2.06 µg/Kg 0.150 µg/Kg10/16/2001 22-15-101601 602339 4715386 22 0308030-05 Decachlorobiphenyl 1.06 µg/Kg 0.0701 µg/Kg10/16/2001 22-15-101601 602339 4715386 22 0308030-05 Total Homologs 90.3 µg/Kg 0.0701 µg/Kg10/16/2001 22-15-101601 602339 4715386 22 0308030-05 Percent Lipids 2.5 % 0.1 %10/16/2001 22-15-101601 602339 4715386 22 0308030-05 Percent Moisture 69.6 % 0.1 %10/17/2001 22-21-101701 602339 4715386 22 0308030-06 Cl2-BZ#8 0.125 U µg/Kg 0.125 µg/Kg10/17/2001 22-21-101701 602339 4715386 22 0308030-06 Cl3-BZ#18 0.277 U µg/Kg 0.277 µg/Kg10/17/2001 22-21-101701 602339 4715386 22 0308030-06 Cl3-BZ#31/#28 3.29 J µg/Kg 2.00 µg/Kg10/17/2001 22-21-101701 602339 4715386 22 0308030-06 Cl4-BZ#44 0.190 U µg/Kg 0.190 µg/Kg10/17/2001 22-21-101701 602339 4715386 22 0308030-06 Cl4-BZ#45 0.254 U µg/Kg 0.254 µg/Kg10/17/2001 22-21-101701 602339 4715386 22 0308030-06 Cl4-BZ#47 0.399 J µg/Kg 0.322 µg/Kg10/17/2001 22-21-101701 602339 4715386 22 0308030-06 Cl4-BZ#49 0.158 U µg/Kg 0.158 µg/Kg10/17/2001 22-21-101701 602339 4715386 22 0308030-06 Cl4-BZ#52 0.180 U µg/Kg 0.180 µg/Kg10/17/2001 22-21-101701 602339 4715386 22 0308030-06 Cl4-BZ#56 0.559 µg/Kg 0.0943 µg/Kg10/17/2001 22-21-101701 602339 4715386 22 0308030-06 Cl4-BZ#66 0.871 µg/Kg 0.126 µg/Kg10/17/2001 22-21-101701 602339 4715386 22 0308030-06 Cl4-BZ#70 0.110 U µg/Kg 0.110 µg/Kg10/17/2001 22-21-101701 602339 4715386 22 0308030-06 Cl4-BZ#74 0.414 J µg/Kg 0.194 µg/Kg10/17/2001 22-21-101701 602339 4715386 22 0308030-06 Cl4-BZ#77 0.174 U µg/Kg 0.174 µg/Kg10/17/2001 22-21-101701 602339 4715386 22 0308030-06 Cl4-BZ#81 0.173 U µg/Kg 0.173 µg/Kg10/17/2001 22-21-101701 602339 4715386 22 0308030-06 Cl5-BZ#87 0.218 J µg/Kg 0.0769 µg/Kg10/17/2001 22-21-101701 602339 4715386 22 0308030-06 Cl5-BZ#95 0.0595 U µg/Kg 0.0595 µg/Kg10/17/2001 22-21-101701 602339 4715386 22 0308030-06 Cl5-BZ#99 1.27 µg/Kg 0.0406 µg/Kg10/17/2001 22-21-101701 602339 4715386 22 0308030-06 Cl5-BZ#101 0.131 J µg/Kg 0.116 µg/Kg10/17/2001 22-21-101701 602339 4715386 22 0308030-06 Cl5-BZ#105 0.689 µg/Kg 0.0566 µg/Kg10/17/2001 22-21-101701 602339 4715386 22 0308030-06 Cl5-BZ#110 0.110 U µg/Kg 0.110 µg/Kg10/17/2001 22-21-101701 602339 4715386 22 0308030-06 Cl5-BZ#114 0.102 J µg/Kg 0.0508 µg/Kg10/17/2001 22-21-101701 602339 4715386 22 0308030-06 Cl5-BZ#118 2.15 µg/Kg 0.119 µg/Kg10/17/2001 22-21-101701 602339 4715386 22 0308030-06 Cl5-BZ#123 0.100 U µg/Kg 0.100 µg/Kg10/17/2001 22-21-101701 602339 4715386 22 0308030-06 Cl5-BZ#126 0.0885 U µg/Kg 0.0885 µg/Kg10/17/2001 22-21-101701 602339 4715386 22 0308030-06 Cl6-BZ#128 0.298 J µg/Kg 0.0798 µg/Kg10/17/2001 22-21-101701 602339 4715386 22 0308030-06 Cl6-BZ#138 4.69 µg/Kg 0.115 µg/Kg



Extracted 7/30/04




SITE NUMBER



10/17/2001 22-21-101701 602339 4715386 22 0308030-06 Cl6-BZ#146 0.530 µg/Kg 0.0726 µg/Kg10/17/2001 22-21-101701 602339 4715386 22 0308030-06 Cl6-BZ#149 0.0929 U µg/Kg 0.0929 µg/Kg10/17/2001 22-21-101701 602339 4715386 22 0308030-06 Cl6-BZ#151 0.154 U µg/Kg 0.154 µg/Kg10/17/2001 22-21-101701 602339 4715386 22 0308030-06 Cl6-BZ#153 6.49 µg/Kg 0.132 µg/Kg10/17/2001 22-21-101701 602339 4715386 22 0308030-06 Cl6-BZ#156 0.443 J µg/Kg 0.0943 µg/Kg10/17/2001 22-21-101701 602339 4715386 22 0308030-06 Cl6-BZ#157 0.0740 U µg/Kg 0.0740 µg/Kg10/17/2001 22-21-101701 602339 4715386 22 0308030-06 Cl6-BZ#158 0.0871 J µg/Kg 0.0624 µg/Kg10/17/2001 22-21-101701 602339 4715386 22 0308030-06 Cl6-BZ#167 0.247 J µg/Kg 0.0798 µg/Kg10/17/2001 22-21-101701 602339 4715386 22 0308030-06 Cl6-BZ#169 0.257 U µg/Kg 0.257 µg/Kg10/17/2001 22-21-101701 602339 4715386 22 0308030-06 Cl7-BZ#170 0.299 U µg/Kg 0.299 µg/Kg10/17/2001 22-21-101701 602339 4715386 22 0308030-06 Cl7-BZ#174 0.0610 U µg/Kg 0.0610 µg/Kg10/17/2001 22-21-101701 602339 4715386 22 0308030-06 Cl7-BZ#177 0.0856 U µg/Kg 0.0856 µg/Kg10/17/2001 22-21-101701 602339 4715386 22 0308030-06 Cl7-BZ#180 2.42 µg/Kg 0.128 µg/Kg10/17/2001 22-21-101701 602339 4715386 22 0308030-06 Cl7-BZ#183 0.0580 U µg/Kg 0.0580 µg/Kg10/17/2001 22-21-101701 602339 4715386 22 0308030-06 Cl7-BZ#187 0.798 µg/Kg 0.0639 µg/Kg10/17/2001 22-21-101701 602339 4715386 22 0308030-06 Cl7-BZ#189 0.115 U µg/Kg 0.115 µg/Kg10/17/2001 22-21-101701 602339 4715386 22 0308030-06 Cl8-BZ#194 0.133 U µg/Kg 0.133 µg/Kg10/17/2001 22-21-101701 602339 4715386 22 0308030-06 Cl8-BZ#195 0.132 U µg/Kg 0.132 µg/Kg10/17/2001 22-21-101701 602339 4715386 22 0308030-06 Cl8-BZ#201 0.116 U µg/Kg 0.116 µg/Kg10/17/2001 22-21-101701 602339 4715386 22 0308030-06 Cl9-BZ#206 0.987 µg/Kg 0.155 µg/Kg10/17/2001 22-21-101701 602339 4715386 22 0308030-06 Cl10-BZ#209 0.581 µg/Kg 0.0726 µg/Kg10/17/2001 22-21-101701 602339 4715386 22 0308030-06 Monochlorobiphenyls 4.27 U µg/Kg 4.27 µg/Kg10/17/2001 22-21-101701 602339 4715386 22 0308030-06 Dichlorobiphenyls 0.125 U µg/Kg 0.125 µg/Kg10/17/2001 22-21-101701 602339 4715386 22 0308030-06 Trichlorobiphenyls 3.34 µg/Kg 0.428 µg/Kg10/17/2001 22-21-101701 602339 4715386 22 0308030-06 Tetrachlorobiphenyls 6.05 µg/Kg 0.0668 µg/Kg10/17/2001 22-21-101701 602339 4715386 22 0308030-06 Pentachlorobiphenyls 13.8 µg/Kg 0.0769 µg/Kg10/17/2001 22-21-101701 602339 4715386 22 0308030-06 Hexachlorobiphenyls 13.7 µg/Kg 0.122 µg/Kg10/17/2001 22-21-101701 602339 4715386 22 0308030-06 Heptachlorobiphenyls 7.76 µg/Kg 0.0668 µg/Kg10/17/2001 22-21-101701 602339 4715386 22 0308030-06 Octachlorobiphenyls 0.0610 U µg/Kg 0.0610 µg/Kg10/17/2001 22-21-101701 602339 4715386 22 0308030-06 Nonachlorobiphenyls 0.994 µg/Kg 0.155 µg/Kg10/17/2001 22-21-101701 602339 4715386 22 0308030-06 Decachlorobiphenyl 0.581 µg/Kg 0.0726 µg/Kg10/17/2001 22-21-101701 602339 4715386 22 0308030-06 Total Homologs 46.2 µg/Kg 0.0726 µg/Kg10/17/2001 22-21-101701 602339 4715386 22 0308030-06 Percent Lipids 1.6 % 0.1 %10/17/2001 22-21-101701 602339 4715386 22 0308030-06 Percent Moisture 72.8 % 0.1 %



Extracted 7/30/04




SITE NUMBER



10/17/2001 22-22-101701 602339 4715386 22 0308030-07 Cl2-BZ#8 0.124 U µg/Kg 0.124 µg/Kg10/17/2001 22-22-101701 602339 4715386 22 0308030-07 Cl3-BZ#18 0.276 U µg/Kg 0.276 µg/Kg10/17/2001 22-22-101701 602339 4715386 22 0308030-07 Cl3-BZ#31/#28 3.36 J µg/Kg 1.99 µg/Kg10/17/2001 22-22-101701 602339 4715386 22 0308030-07 Cl4-BZ#44 0.190 U µg/Kg 0.190 µg/Kg10/17/2001 22-22-101701 602339 4715386 22 0308030-07 Cl4-BZ#45 0.253 U µg/Kg 0.253 µg/Kg10/17/2001 22-22-101701 602339 4715386 22 0308030-07 Cl4-BZ#47 1.16 J µg/Kg 0.321 µg/Kg10/17/2001 22-22-101701 602339 4715386 22 0308030-07 Cl4-BZ#49 0.158 U µg/Kg 0.158 µg/Kg10/17/2001 22-22-101701 602339 4715386 22 0308030-07 Cl4-BZ#52 0.181 J µg/Kg 0.179 µg/Kg10/17/2001 22-22-101701 602339 4715386 22 0308030-07 Cl4-BZ#56 0.615 µg/Kg 0.0940 µg/Kg10/17/2001 22-22-101701 602339 4715386 22 0308030-07 Cl4-BZ#66 1.84 µg/Kg 0.126 µg/Kg10/17/2001 22-22-101701 602339 4715386 22 0308030-07 Cl4-BZ#70 0.427 J µg/Kg 0.110 µg/Kg10/17/2001 22-22-101701 602339 4715386 22 0308030-07 Cl4-BZ#74 0.868 J µg/Kg 0.194 µg/Kg10/17/2001 22-22-101701 602339 4715386 22 0308030-07 Cl4-BZ#77 0.174 U µg/Kg 0.174 µg/Kg10/17/2001 22-22-101701 602339 4715386 22 0308030-07 Cl4-BZ#81 0.172 U µg/Kg 0.172 µg/Kg10/17/2001 22-22-101701 602339 4715386 22 0308030-07 Cl5-BZ#87 0.607 µg/Kg 0.0767 µg/Kg10/17/2001 22-22-101701 602339 4715386 22 0308030-07 Cl5-BZ#95 0.0593 U µg/Kg 0.0593 µg/Kg10/17/2001 22-22-101701 602339 4715386 22 0308030-07 Cl5-BZ#99 4.19 µg/Kg 0.0405 µg/Kg10/17/2001 22-22-101701 602339 4715386 22 0308030-07 Cl5-BZ#101 0.231 J µg/Kg 0.116 µg/Kg10/17/2001 22-22-101701 602339 4715386 22 0308030-07 Cl5-BZ#105 1.81 µg/Kg 0.0564 µg/Kg10/17/2001 22-22-101701 602339 4715386 22 0308030-07 Cl5-BZ#110 0.174 J µg/Kg 0.110 µg/Kg10/17/2001 22-22-101701 602339 4715386 22 0308030-07 Cl5-BZ#114 0.210 J µg/Kg 0.0506 µg/Kg10/17/2001 22-22-101701 602339 4715386 22 0308030-07 Cl5-BZ#118 4.55 µg/Kg 0.119 µg/Kg10/17/2001 22-22-101701 602339 4715386 22 0308030-07 Cl5-BZ#123 0.0998 U µg/Kg 0.0998 µg/Kg10/17/2001 22-22-101701 602339 4715386 22 0308030-07 Cl5-BZ#126 0.0882 U µg/Kg 0.0882 µg/Kg10/17/2001 22-22-101701 602339 4715386 22 0308030-07 Cl6-BZ#128 0.947 µg/Kg 0.0795 µg/Kg10/17/2001 22-22-101701 602339 4715386 22 0308030-07 Cl6-BZ#138 12.1 µg/Kg 0.114 µg/Kg10/17/2001 22-22-101701 602339 4715386 22 0308030-07 Cl6-BZ#146 1.55 µg/Kg 0.0723 µg/Kg10/17/2001 22-22-101701 602339 4715386 22 0308030-07 Cl6-BZ#149 0.224 J µg/Kg 0.0926 µg/Kg10/17/2001 22-22-101701 602339 4715386 22 0308030-07 Cl6-BZ#151 0.153 U µg/Kg 0.153 µg/Kg10/17/2001 22-22-101701 602339 4715386 22 0308030-07 Cl6-BZ#153 13.0 µg/Kg 0.132 µg/Kg10/17/2001 22-22-101701 602339 4715386 22 0308030-07 Cl6-BZ#156 0.795 µg/Kg 0.0940 µg/Kg10/17/2001 22-22-101701 602339 4715386 22 0308030-07 Cl6-BZ#157 0.195 J µg/Kg 0.0738 µg/Kg10/17/2001 22-22-101701 602339 4715386 22 0308030-07 Cl6-BZ#158 0.340 µg/Kg 0.0622 µg/Kg10/17/2001 22-22-101701 602339 4715386 22 0308030-07 Cl6-BZ#167 0.463 µg/Kg 0.0795 µg/Kg



Extracted 7/30/04




SITE NUMBER



10/17/2001 22-22-101701 602339 4715386 22 0308030-07 Cl6-BZ#169 0.256 U µg/Kg 0.256 µg/Kg10/17/2001 22-22-101701 602339 4715386 22 0308030-07 Cl7-BZ#170 0.298 U µg/Kg 0.298 µg/Kg10/17/2001 22-22-101701 602339 4715386 22 0308030-07 Cl7-BZ#174 0.0607 U µg/Kg 0.0607 µg/Kg10/17/2001 22-22-101701 602339 4715386 22 0308030-07 Cl7-BZ#177 0.0853 U µg/Kg 0.0853 µg/Kg10/17/2001 22-22-101701 602339 4715386 22 0308030-07 Cl7-BZ#180 4.82 µg/Kg 0.127 µg/Kg10/17/2001 22-22-101701 602339 4715386 22 0308030-07 Cl7-BZ#183 0.795 µg/Kg 0.0579 µg/Kg10/17/2001 22-22-101701 602339 4715386 22 0308030-07 Cl7-BZ#187 2.16 µg/Kg 0.0636 µg/Kg10/17/2001 22-22-101701 602339 4715386 22 0308030-07 Cl7-BZ#189 0.114 U µg/Kg 0.114 µg/Kg10/17/2001 22-22-101701 602339 4715386 22 0308030-07 Cl8-BZ#194 0.133 U µg/Kg 0.133 µg/Kg10/17/2001 22-22-101701 602339 4715386 22 0308030-07 Cl8-BZ#195 0.434 J µg/Kg 0.132 µg/Kg10/17/2001 22-22-101701 602339 4715386 22 0308030-07 Cl8-BZ#201 0.513 J µg/Kg 0.116 µg/Kg10/17/2001 22-22-101701 602339 4715386 22 0308030-07 Cl9-BZ#206 2.07 µg/Kg 0.155 µg/Kg10/17/2001 22-22-101701 602339 4715386 22 0308030-07 Cl10-BZ#209 1.02 µg/Kg 0.0723 µg/Kg10/17/2001 22-22-101701 602339 4715386 22 0308030-07 Monochlorobiphenyls 4.25 U µg/Kg 4.25 µg/Kg10/17/2001 22-22-101701 602339 4715386 22 0308030-07 Dichlorobiphenyls 0.124 U µg/Kg 0.124 µg/Kg10/17/2001 22-22-101701 602339 4715386 22 0308030-07 Trichlorobiphenyls 5.00 µg/Kg 0.427 µg/Kg10/17/2001 22-22-101701 602339 4715386 22 0308030-07 Tetrachlorobiphenyls 10.4 µg/Kg 0.0665 µg/Kg10/17/2001 22-22-101701 602339 4715386 22 0308030-07 Pentachlorobiphenyls 22.2 µg/Kg 0.0767 µg/Kg10/17/2001 22-22-101701 602339 4715386 22 0308030-07 Hexachlorobiphenyls 32.8 µg/Kg 0.122 µg/Kg10/17/2001 22-22-101701 602339 4715386 22 0308030-07 Heptachlorobiphenyls 9.75 µg/Kg 0.0665 µg/Kg10/17/2001 22-22-101701 602339 4715386 22 0308030-07 Octachlorobiphenyls 2.35 µg/Kg 0.0607 µg/Kg10/17/2001 22-22-101701 602339 4715386 22 0308030-07 Nonachlorobiphenyls 4.09 µg/Kg 0.155 µg/Kg10/17/2001 22-22-101701 602339 4715386 22 0308030-07 Decachlorobiphenyl 1.02 µg/Kg 0.0723 µg/Kg10/17/2001 22-22-101701 602339 4715386 22 0308030-07 Total Homologs 87.7 µg/Kg 0.0723 µg/Kg10/17/2001 22-22-101701 602339 4715386 22 0308030-07 Percent Lipids 1.1 % 0.1 %10/17/2001 22-22-101701 602339 4715386 22 0308030-07 Percent Moisture 74.5 % 0.1 %10/18/2001 22-24-101801 602339 4715386 22 0308030-08 Cl2-BZ#8 0.112 U µg/Kg 0.112 µg/Kg10/18/2001 22-24-101801 602339 4715386 22 0308030-08 Cl3-BZ#18 0.250 U µg/Kg 0.250 µg/Kg10/18/2001 22-24-101801 602339 4715386 22 0308030-08 Cl3-BZ#31/#28 4.51 J µg/Kg 1.80 µg/Kg10/18/2001 22-24-101801 602339 4715386 22 0308030-08 Cl4-BZ#44 0.171 U µg/Kg 0.171 µg/Kg10/18/2001 22-24-101801 602339 4715386 22 0308030-08 Cl4-BZ#45 0.229 U µg/Kg 0.229 µg/Kg10/18/2001 22-24-101801 602339 4715386 22 0308030-08 Cl4-BZ#47 0.290 U µg/Kg 0.290 µg/Kg10/18/2001 22-24-101801 602339 4715386 22 0308030-08 Cl4-BZ#49 0.142 U µg/Kg 0.142 µg/Kg10/18/2001 22-24-101801 602339 4715386 22 0308030-08 Cl4-BZ#52 0.281 J µg/Kg 0.162 µg/Kg



Extracted 7/30/04




SITE NUMBER



10/18/2001 22-24-101801 602339 4715386 22 0308030-08 Cl4-BZ#56 0.0850 U µg/Kg 0.0850 µg/Kg10/18/2001 22-24-101801 602339 4715386 22 0308030-08 Cl4-BZ#66 1.12 µg/Kg 0.114 µg/Kg10/18/2001 22-24-101801 602339 4715386 22 0308030-08 Cl4-BZ#70 0.190 J µg/Kg 0.0993 µg/Kg10/18/2001 22-24-101801 602339 4715386 22 0308030-08 Cl4-BZ#74 0.229 J µg/Kg 0.175 µg/Kg10/18/2001 22-24-101801 602339 4715386 22 0308030-08 Cl4-BZ#77 0.157 U µg/Kg 0.157 µg/Kg10/18/2001 22-24-101801 602339 4715386 22 0308030-08 Cl4-BZ#81 0.155 U µg/Kg 0.155 µg/Kg10/18/2001 22-24-101801 602339 4715386 22 0308030-08 Cl5-BZ#87 0.144 J µg/Kg 0.0693 µg/Kg10/18/2001 22-24-101801 602339 4715386 22 0308030-08 Cl5-BZ#95 0.0536 U µg/Kg 0.0536 µg/Kg10/18/2001 22-24-101801 602339 4715386 22 0308030-08 Cl5-BZ#99 0.758 µg/Kg 0.0366 µg/Kg10/18/2001 22-24-101801 602339 4715386 22 0308030-08 Cl5-BZ#101 0.118 J µg/Kg 0.105 µg/Kg10/18/2001 22-24-101801 602339 4715386 22 0308030-08 Cl5-BZ#105 0.373 µg/Kg 0.0510 µg/Kg10/18/2001 22-24-101801 602339 4715386 22 0308030-08 Cl5-BZ#110 0.0993 U µg/Kg 0.0993 µg/Kg10/18/2001 22-24-101801 602339 4715386 22 0308030-08 Cl5-BZ#114 0.0457 U µg/Kg 0.0457 µg/Kg10/18/2001 22-24-101801 602339 4715386 22 0308030-08 Cl5-BZ#118 1.06 µg/Kg 0.107 µg/Kg10/18/2001 22-24-101801 602339 4715386 22 0308030-08 Cl5-BZ#123 0.0902 U µg/Kg 0.0902 µg/Kg10/18/2001 22-24-101801 602339 4715386 22 0308030-08 Cl5-BZ#126 0.0797 U µg/Kg 0.0797 µg/Kg10/18/2001 22-24-101801 602339 4715386 22 0308030-08 Cl6-BZ#128 0.209 J µg/Kg 0.0719 µg/Kg10/18/2001 22-24-101801 602339 4715386 22 0308030-08 Cl6-BZ#138 3.48 µg/Kg 0.103 µg/Kg10/18/2001 22-24-101801 602339 4715386 22 0308030-08 Cl6-BZ#146 0.490 µg/Kg 0.0654 µg/Kg10/18/2001 22-24-101801 602339 4715386 22 0308030-08 Cl6-BZ#149 0.0837 U µg/Kg 0.0837 µg/Kg10/18/2001 22-24-101801 602339 4715386 22 0308030-08 Cl6-BZ#151 0.139 U µg/Kg 0.139 µg/Kg10/18/2001 22-24-101801 602339 4715386 22 0308030-08 Cl6-BZ#153 3.62 µg/Kg 0.119 µg/Kg10/18/2001 22-24-101801 602339 4715386 22 0308030-08 Cl6-BZ#156 0.255 J µg/Kg 0.0850 µg/Kg10/18/2001 22-24-101801 602339 4715386 22 0308030-08 Cl6-BZ#157 0.137 J µg/Kg 0.0667 µg/Kg10/18/2001 22-24-101801 602339 4715386 22 0308030-08 Cl6-BZ#158 0.105 J µg/Kg 0.0562 µg/Kg10/18/2001 22-24-101801 602339 4715386 22 0308030-08 Cl6-BZ#167 0.144 J µg/Kg 0.0719 µg/Kg10/18/2001 22-24-101801 602339 4715386 22 0308030-08 Cl6-BZ#169 0.231 U µg/Kg 0.231 µg/Kg10/18/2001 22-24-101801 602339 4715386 22 0308030-08 Cl7-BZ#170 0.269 U µg/Kg 0.269 µg/Kg10/18/2001 22-24-101801 602339 4715386 22 0308030-08 Cl7-BZ#174 0.0549 U µg/Kg 0.0549 µg/Kg10/18/2001 22-24-101801 602339 4715386 22 0308030-08 Cl7-BZ#177 0.0771 U µg/Kg 0.0771 µg/Kg10/18/2001 22-24-101801 602339 4715386 22 0308030-08 Cl7-BZ#180 0.115 U µg/Kg 0.115 µg/Kg10/18/2001 22-24-101801 602339 4715386 22 0308030-08 Cl7-BZ#183 0.275 µg/Kg 0.0523 µg/Kg10/18/2001 22-24-101801 602339 4715386 22 0308030-08 Cl7-BZ#187 0.928 µg/Kg 0.0575 µg/Kg10/18/2001 22-24-101801 602339 4715386 22 0308030-08 Cl7-BZ#189 0.103 U µg/Kg 0.103 µg/Kg



Extracted 7/30/04




SITE NUMBER



10/18/2001 22-24-101801 602339 4715386 22 0308030-08 Cl8-BZ#194 0.120 U µg/Kg 0.120 µg/Kg10/18/2001 22-24-101801 602339 4715386 22 0308030-08 Cl8-BZ#195 0.119 U µg/Kg 0.119 µg/Kg10/18/2001 22-24-101801 602339 4715386 22 0308030-08 Cl8-BZ#201 0.307 J µg/Kg 0.105 µg/Kg10/18/2001 22-24-101801 602339 4715386 22 0308030-08 Cl9-BZ#206 0.536 J µg/Kg 0.140 µg/Kg10/18/2001 22-24-101801 602339 4715386 22 0308030-08 Cl10-BZ#209 0.248 J µg/Kg 0.0654 µg/Kg10/18/2001 22-24-101801 602339 4715386 22 0308030-08 Monochlorobiphenyls 3.84 U µg/Kg 3.84 µg/Kg10/18/2001 22-24-101801 602339 4715386 22 0308030-08 Dichlorobiphenyls 0.112 U µg/Kg 0.112 µg/Kg10/18/2001 22-24-101801 602339 4715386 22 0308030-08 Trichlorobiphenyls 4.52 µg/Kg 0.386 µg/Kg10/18/2001 22-24-101801 602339 4715386 22 0308030-08 Tetrachlorobiphenyls 4.08 µg/Kg 0.0601 µg/Kg10/18/2001 22-24-101801 602339 4715386 22 0308030-08 Pentachlorobiphenyls 6.77 µg/Kg 0.0693 µg/Kg10/18/2001 22-24-101801 602339 4715386 22 0308030-08 Hexachlorobiphenyls 8.90 µg/Kg 0.110 µg/Kg10/18/2001 22-24-101801 602339 4715386 22 0308030-08 Heptachlorobiphenyls 1.19 µg/Kg 0.0601 µg/Kg10/18/2001 22-24-101801 602339 4715386 22 0308030-08 Octachlorobiphenyls 0.242 J µg/Kg 0.0549 µg/Kg10/18/2001 22-24-101801 602339 4715386 22 0308030-08 Nonachlorobiphenyls 0.595 J µg/Kg 0.140 µg/Kg10/18/2001 22-24-101801 602339 4715386 22 0308030-08 Decachlorobiphenyl 0.248 J µg/Kg 0.0654 µg/Kg10/18/2001 22-24-101801 602339 4715386 22 0308030-08 Total Homologs 26.5 µg/Kg 0.0654 µg/Kg10/18/2001 22-24-101801 602339 4715386 22 0308030-08 Percent Lipids 1.2 % 0.1 %10/18/2001 22-24-101801 602339 4715386 22 0308030-08 Percent Moisture 72.2 % 0.1 %10/15/2001 23-06-101501 600373 4705549 23 0308030-09 Cl2-BZ#8 0.120 U µg/Kg 0.120 µg/Kg10/15/2001 23-06-101501 600373 4705549 23 0308030-09 Cl3-BZ#18 0.266 U µg/Kg 0.266 µg/Kg10/15/2001 23-06-101501 600373 4705549 23 0308030-09 Cl3-BZ#31/#28 13.4 µg/Kg 1.92 µg/Kg10/15/2001 23-06-101501 600373 4705549 23 0308030-09 Cl4-BZ#44 0.183 U µg/Kg 0.183 µg/Kg10/15/2001 23-06-101501 600373 4705549 23 0308030-09 Cl4-BZ#45 0.244 U µg/Kg 0.244 µg/Kg10/15/2001 23-06-101501 600373 4705549 23 0308030-09 Cl4-BZ#47 0.558 J µg/Kg 0.310 µg/Kg10/15/2001 23-06-101501 600373 4705549 23 0308030-09 Cl4-BZ#49 0.152 U µg/Kg 0.152 µg/Kg10/15/2001 23-06-101501 600373 4705549 23 0308030-09 Cl4-BZ#52 0.202 J µg/Kg 0.173 µg/Kg10/15/2001 23-06-101501 600373 4705549 23 0308030-09 Cl4-BZ#56 0.0907 U µg/Kg 0.0907 µg/Kg10/15/2001 23-06-101501 600373 4705549 23 0308030-09 Cl4-BZ#66 0.844 µg/Kg 0.121 µg/Kg10/15/2001 23-06-101501 600373 4705549 23 0308030-09 Cl4-BZ#70 0.300 J µg/Kg 0.106 µg/Kg10/15/2001 23-06-101501 600373 4705549 23 0308030-09 Cl4-BZ#74 0.544 J µg/Kg 0.187 µg/Kg10/15/2001 23-06-101501 600373 4705549 23 0308030-09 Cl4-BZ#77 0.167 U µg/Kg 0.167 µg/Kg10/15/2001 23-06-101501 600373 4705549 23 0308030-09 Cl4-BZ#81 0.166 U µg/Kg 0.166 µg/Kg10/15/2001 23-06-101501 600373 4705549 23 0308030-09 Cl5-BZ#87 0.314 J µg/Kg 0.0740 µg/Kg10/15/2001 23-06-101501 600373 4705549 23 0308030-09 Cl5-BZ#95 0.0572 U µg/Kg 0.0572 µg/Kg



Extracted 7/30/04




SITE NUMBER



10/15/2001 23-06-101501 600373 4705549 23 0308030-09 Cl5-BZ#99 1.02 µg/Kg 0.0391 µg/Kg10/15/2001 23-06-101501 600373 4705549 23 0308030-09 Cl5-BZ#101 0.147 J µg/Kg 0.112 µg/Kg10/15/2001 23-06-101501 600373 4705549 23 0308030-09 Cl5-BZ#105 0.739 µg/Kg 0.0544 µg/Kg10/15/2001 23-06-101501 600373 4705549 23 0308030-09 Cl5-BZ#110 0.106 U µg/Kg 0.106 µg/Kg10/15/2001 23-06-101501 600373 4705549 23 0308030-09 Cl5-BZ#114 0.0488 U µg/Kg 0.0488 µg/Kg10/15/2001 23-06-101501 600373 4705549 23 0308030-09 Cl5-BZ#118 1.42 µg/Kg 0.114 µg/Kg10/15/2001 23-06-101501 600373 4705549 23 0308030-09 Cl5-BZ#123 0.0963 U µg/Kg 0.0963 µg/Kg10/15/2001 23-06-101501 600373 4705549 23 0308030-09 Cl5-BZ#126 0.0851 U µg/Kg 0.0851 µg/Kg10/15/2001 23-06-101501 600373 4705549 23 0308030-09 Cl6-BZ#128 0.412 µg/Kg 0.0767 µg/Kg10/15/2001 23-06-101501 600373 4705549 23 0308030-09 Cl6-BZ#138 5.32 µg/Kg 0.110 µg/Kg10/15/2001 23-06-101501 600373 4705549 23 0308030-09 Cl6-BZ#146 0.481 µg/Kg 0.0698 µg/Kg10/15/2001 23-06-101501 600373 4705549 23 0308030-09 Cl6-BZ#149 0.0907 J µg/Kg 0.0893 µg/Kg10/15/2001 23-06-101501 600373 4705549 23 0308030-09 Cl6-BZ#151 0.148 U µg/Kg 0.148 µg/Kg10/15/2001 23-06-101501 600373 4705549 23 0308030-09 Cl6-BZ#153 5.20 µg/Kg 0.127 µg/Kg10/15/2001 23-06-101501 600373 4705549 23 0308030-09 Cl6-BZ#156 0.223 J µg/Kg 0.0907 µg/Kg10/15/2001 23-06-101501 600373 4705549 23 0308030-09 Cl6-BZ#157 0.0837 J µg/Kg 0.0712 µg/Kg10/15/2001 23-06-101501 600373 4705549 23 0308030-09 Cl6-BZ#158 0.0977 J µg/Kg 0.0600 µg/Kg10/15/2001 23-06-101501 600373 4705549 23 0308030-09 Cl6-BZ#167 0.202 J µg/Kg 0.0767 µg/Kg10/15/2001 23-06-101501 600373 4705549 23 0308030-09 Cl6-BZ#169 0.247 U µg/Kg 0.247 µg/Kg10/15/2001 23-06-101501 600373 4705549 23 0308030-09 Cl7-BZ#170 0.287 U µg/Kg 0.287 µg/Kg10/15/2001 23-06-101501 600373 4705549 23 0308030-09 Cl7-BZ#174 0.0586 U µg/Kg 0.0586 µg/Kg10/15/2001 23-06-101501 600373 4705549 23 0308030-09 Cl7-BZ#177 0.0823 U µg/Kg 0.0823 µg/Kg10/15/2001 23-06-101501 600373 4705549 23 0308030-09 Cl7-BZ#180 0.123 U µg/Kg 0.123 µg/Kg10/15/2001 23-06-101501 600373 4705549 23 0308030-09 Cl7-BZ#183 0.412 µg/Kg 0.0558 µg/Kg10/15/2001 23-06-101501 600373 4705549 23 0308030-09 Cl7-BZ#187 0.635 µg/Kg 0.0614 µg/Kg10/15/2001 23-06-101501 600373 4705549 23 0308030-09 Cl7-BZ#189 0.110 U µg/Kg 0.110 µg/Kg10/15/2001 23-06-101501 600373 4705549 23 0308030-09 Cl8-BZ#194 0.128 U µg/Kg 0.128 µg/Kg10/15/2001 23-06-101501 600373 4705549 23 0308030-09 Cl8-BZ#195 0.127 U µg/Kg 0.127 µg/Kg10/15/2001 23-06-101501 600373 4705549 23 0308030-09 Cl8-BZ#201 0.112 U µg/Kg 0.112 µg/Kg10/15/2001 23-06-101501 600373 4705549 23 0308030-09 Cl9-BZ#206 4.10 µg/Kg 0.149 µg/Kg10/15/2001 23-06-101501 600373 4705549 23 0308030-09 Cl10-BZ#209 3.24 µg/Kg 0.0698 µg/Kg10/15/2001 23-06-101501 600373 4705549 23 0308030-09 Monochlorobiphenyls 4.10 U µg/Kg 4.10 µg/Kg10/15/2001 23-06-101501 600373 4705549 23 0308030-09 Dichlorobiphenyls 0.120 U µg/Kg 0.120 µg/Kg10/15/2001 23-06-101501 600373 4705549 23 0308030-09 Trichlorobiphenyls 12.0 µg/Kg 0.412 µg/Kg



Extracted 7/30/04




SITE NUMBER



10/15/2001 23-06-101501 600373 4705549 23 0308030-09 Tetrachlorobiphenyls 5.14 µg/Kg 0.0642 µg/Kg10/15/2001 23-06-101501 600373 4705549 23 0308030-09 Pentachlorobiphenyls 10.8 µg/Kg 0.0740 µg/Kg10/15/2001 23-06-101501 600373 4705549 23 0308030-09 Hexachlorobiphenyls 14.7 µg/Kg 0.117 µg/Kg10/15/2001 23-06-101501 600373 4705549 23 0308030-09 Heptachlorobiphenyls 1.03 µg/Kg 0.0642 µg/Kg10/15/2001 23-06-101501 600373 4705549 23 0308030-09 Octachlorobiphenyls 0.0586 U µg/Kg 0.0586 µg/Kg10/15/2001 23-06-101501 600373 4705549 23 0308030-09 Nonachlorobiphenyls 4.20 µg/Kg 0.149 µg/Kg10/15/2001 23-06-101501 600373 4705549 23 0308030-09 Decachlorobiphenyl 3.24 µg/Kg 0.0698 µg/Kg10/15/2001 23-06-101501 600373 4705549 23 0308030-09 Total Homologs 51.1 µg/Kg 0.0698 µg/Kg10/15/2001 23-06-101501 600373 4705549 23 0308030-09 Percent Lipids 2.6 % 0.1 %10/15/2001 23-06-101501 600373 4705549 23 0308030-09 Percent Moisture 73.6 % 0.1 %10/16/2001 23-09-101601 600373 4705549 23 0308030-10 Cl2-BZ#8 0.106 U µg/Kg 0.106 µg/Kg10/16/2001 23-09-101601 600373 4705549 23 0308030-10 Cl3-BZ#18 0.236 U µg/Kg 0.236 µg/Kg10/16/2001 23-09-101601 600373 4705549 23 0308030-10 Cl3-BZ#31/#28 2.66 J µg/Kg 1.70 µg/Kg10/16/2001 23-09-101601 600373 4705549 23 0308030-10 Cl4-BZ#44 0.162 U µg/Kg 0.162 µg/Kg10/16/2001 23-09-101601 600373 4705549 23 0308030-10 Cl4-BZ#45 0.216 U µg/Kg 0.216 µg/Kg10/16/2001 23-09-101601 600373 4705549 23 0308030-10 Cl4-BZ#47 0.803 J µg/Kg 0.274 µg/Kg10/16/2001 23-09-101601 600373 4705549 23 0308030-10 Cl4-BZ#49 0.135 U µg/Kg 0.135 µg/Kg10/16/2001 23-09-101601 600373 4705549 23 0308030-10 Cl4-BZ#52 0.290 J µg/Kg 0.153 µg/Kg10/16/2001 23-09-101601 600373 4705549 23 0308030-10 Cl4-BZ#56 0.631 µg/Kg 0.0804 µg/Kg10/16/2001 23-09-101601 600373 4705549 23 0308030-10 Cl4-BZ#66 1.03 µg/Kg 0.108 µg/Kg10/16/2001 23-09-101601 600373 4705549 23 0308030-10 Cl4-BZ#70 0.562 µg/Kg 0.0940 µg/Kg10/16/2001 23-09-101601 600373 4705549 23 0308030-10 Cl4-BZ#74 0.501 J µg/Kg 0.166 µg/Kg10/16/2001 23-09-101601 600373 4705549 23 0308030-10 Cl4-BZ#77 0.148 U µg/Kg 0.148 µg/Kg10/16/2001 23-09-101601 600373 4705549 23 0308030-10 Cl4-BZ#81 0.147 U µg/Kg 0.147 µg/Kg10/16/2001 23-09-101601 600373 4705549 23 0308030-10 Cl5-BZ#87 0.377 µg/Kg 0.0655 µg/Kg10/16/2001 23-09-101601 600373 4705549 23 0308030-10 Cl5-BZ#95 0.0742 J µg/Kg 0.0507 µg/Kg10/16/2001 23-09-101601 600373 4705549 23 0308030-10 Cl5-BZ#99 1.53 µg/Kg 0.0346 µg/Kg10/16/2001 23-09-101601 600373 4705549 23 0308030-10 Cl5-BZ#101 0.284 J µg/Kg 0.0989 µg/Kg10/16/2001 23-09-101601 600373 4705549 23 0308030-10 Cl5-BZ#105 0.729 µg/Kg 0.0482 µg/Kg10/16/2001 23-09-101601 600373 4705549 23 0308030-10 Cl5-BZ#110 0.222 J µg/Kg 0.0940 µg/Kg10/16/2001 23-09-101601 600373 4705549 23 0308030-10 Cl5-BZ#114 0.0433 U µg/Kg 0.0433 µg/Kg10/16/2001 23-09-101601 600373 4705549 23 0308030-10 Cl5-BZ#118 2.10 µg/Kg 0.101 µg/Kg10/16/2001 23-09-101601 600373 4705549 23 0308030-10 Cl5-BZ#123 0.0853 U µg/Kg 0.0853 µg/Kg10/16/2001 23-09-101601 600373 4705549 23 0308030-10 Cl5-BZ#126 0.0754 U µg/Kg 0.0754 µg/Kg



Extracted 7/30/04




SITE NUMBER



10/16/2001 23-09-101601 600373 4705549 23 0308030-10 Cl6-BZ#128 0.266 J µg/Kg 0.0680 µg/Kg10/16/2001 23-09-101601 600373 4705549 23 0308030-10 Cl6-BZ#138 3.83 µg/Kg 0.0977 µg/Kg10/16/2001 23-09-101601 600373 4705549 23 0308030-10 Cl6-BZ#146 0.562 µg/Kg 0.0618 µg/Kg10/16/2001 23-09-101601 600373 4705549 23 0308030-10 Cl6-BZ#149 0.161 J µg/Kg 0.0791 µg/Kg10/16/2001 23-09-101601 600373 4705549 23 0308030-10 Cl6-BZ#151 0.131 U µg/Kg 0.131 µg/Kg10/16/2001 23-09-101601 600373 4705549 23 0308030-10 Cl6-BZ#153 3.54 µg/Kg 0.112 µg/Kg10/16/2001 23-09-101601 600373 4705549 23 0308030-10 Cl6-BZ#156 0.266 J µg/Kg 0.0804 µg/Kg10/16/2001 23-09-101601 600373 4705549 23 0308030-10 Cl6-BZ#157 0.0630 U µg/Kg 0.0630 µg/Kg10/16/2001 23-09-101601 600373 4705549 23 0308030-10 Cl6-BZ#158 0.0865 J µg/Kg 0.0532 µg/Kg10/16/2001 23-09-101601 600373 4705549 23 0308030-10 Cl6-BZ#167 0.130 J µg/Kg 0.0680 µg/Kg10/16/2001 23-09-101601 600373 4705549 23 0308030-10 Cl6-BZ#169 0.219 U µg/Kg 0.219 µg/Kg10/16/2001 23-09-101601 600373 4705549 23 0308030-10 Cl7-BZ#170 0.255 U µg/Kg 0.255 µg/Kg10/16/2001 23-09-101601 600373 4705549 23 0308030-10 Cl7-BZ#174 0.0519 U µg/Kg 0.0519 µg/Kg10/16/2001 23-09-101601 600373 4705549 23 0308030-10 Cl7-BZ#177 0.0729 U µg/Kg 0.0729 µg/Kg10/16/2001 23-09-101601 600373 4705549 23 0308030-10 Cl7-BZ#180 0.109 U µg/Kg 0.109 µg/Kg10/16/2001 23-09-101601 600373 4705549 23 0308030-10 Cl7-BZ#183 0.210 J µg/Kg 0.0494 µg/Kg10/16/2001 23-09-101601 600373 4705549 23 0308030-10 Cl7-BZ#187 0.995 µg/Kg 0.0544 µg/Kg10/16/2001 23-09-101601 600373 4705549 23 0308030-10 Cl7-BZ#189 0.0977 U µg/Kg 0.0977 µg/Kg10/16/2001 23-09-101601 600373 4705549 23 0308030-10 Cl8-BZ#194 0.114 U µg/Kg 0.114 µg/Kg10/16/2001 23-09-101601 600373 4705549 23 0308030-10 Cl8-BZ#195 0.112 U µg/Kg 0.112 µg/Kg10/16/2001 23-09-101601 600373 4705549 23 0308030-10 Cl8-BZ#201 0.241 J µg/Kg 0.0989 µg/Kg10/16/2001 23-09-101601 600373 4705549 23 0308030-10 Cl9-BZ#206 0.334 J µg/Kg 0.132 µg/Kg10/16/2001 23-09-101601 600373 4705549 23 0308030-10 Cl10-BZ#209 0.204 J µg/Kg 0.0618 µg/Kg10/16/2001 23-09-101601 600373 4705549 23 0308030-10 Monochlorobiphenyls 3.64 U µg/Kg 3.64 µg/Kg10/16/2001 23-09-101601 600373 4705549 23 0308030-10 Dichlorobiphenyls 0.106 U µg/Kg 0.106 µg/Kg10/16/2001 23-09-101601 600373 4705549 23 0308030-10 Trichlorobiphenyls 2.66 µg/Kg 0.365 µg/Kg10/16/2001 23-09-101601 600373 4705549 23 0308030-10 Tetrachlorobiphenyls 7.69 µg/Kg 0.0569 µg/Kg10/16/2001 23-09-101601 600373 4705549 23 0308030-10 Pentachlorobiphenyls 9.64 µg/Kg 0.0655 µg/Kg10/16/2001 23-09-101601 600373 4705549 23 0308030-10 Hexachlorobiphenyls 9.77 µg/Kg 0.104 µg/Kg10/16/2001 23-09-101601 600373 4705549 23 0308030-10 Heptachlorobiphenyls 1.19 µg/Kg 0.0569 µg/Kg10/16/2001 23-09-101601 600373 4705549 23 0308030-10 Octachlorobiphenyls 0.192 J µg/Kg 0.0519 µg/Kg10/16/2001 23-09-101601 600373 4705549 23 0308030-10 Nonachlorobiphenyls 0.352 J µg/Kg 0.132 µg/Kg10/16/2001 23-09-101601 600373 4705549 23 0308030-10 Decachlorobiphenyl 0.204 J µg/Kg 0.0618 µg/Kg10/16/2001 23-09-101601 600373 4705549 23 0308030-10 Total Homologs 31.7 µg/Kg 0.0618 µg/Kg



Extracted 7/30/04




SITE NUMBER



10/16/2001 23-09-101601 600373 4705549 23 0308030-10 Percent Lipids 2.0 % 0.1 %10/16/2001 23-09-101601 600373 4705549 23 0308030-10 Percent Moisture 70.6 % 0.1 %10/17/2001 23-11-101701 600373 4705549 23 0308030-11 Cl2-BZ#8 0.116 U µg/Kg 0.116 µg/Kg10/17/2001 23-11-101701 600373 4705549 23 0308030-11 Cl3-BZ#18 0.258 U µg/Kg 0.258 µg/Kg10/17/2001 23-11-101701 600373 4705549 23 0308030-11 Cl3-BZ#31/#28 6.70 J µg/Kg 1.86 µg/Kg10/17/2001 23-11-101701 600373 4705549 23 0308030-11 Cl4-BZ#44 0.177 U µg/Kg 0.177 µg/Kg10/17/2001 23-11-101701 600373 4705549 23 0308030-11 Cl4-BZ#45 0.236 U µg/Kg 0.236 µg/Kg10/17/2001 23-11-101701 600373 4705549 23 0308030-11 Cl4-BZ#47 1.35 J µg/Kg 0.300 µg/Kg10/17/2001 23-11-101701 600373 4705549 23 0308030-11 Cl4-BZ#49 0.147 U µg/Kg 0.147 µg/Kg10/17/2001 23-11-101701 600373 4705549 23 0308030-11 Cl4-BZ#52 0.223 J µg/Kg 0.167 µg/Kg10/17/2001 23-11-101701 600373 4705549 23 0308030-11 Cl4-BZ#56 0.803 µg/Kg 0.0878 µg/Kg10/17/2001 23-11-101701 600373 4705549 23 0308030-11 Cl4-BZ#66 1.66 µg/Kg 0.117 µg/Kg10/17/2001 23-11-101701 600373 4705549 23 0308030-11 Cl4-BZ#70 0.243 J µg/Kg 0.103 µg/Kg10/17/2001 23-11-101701 600373 4705549 23 0308030-11 Cl4-BZ#74 1.22 µg/Kg 0.181 µg/Kg10/17/2001 23-11-101701 600373 4705549 23 0308030-11 Cl4-BZ#77 0.162 U µg/Kg 0.162 µg/Kg10/17/2001 23-11-101701 600373 4705549 23 0308030-11 Cl4-BZ#81 0.161 U µg/Kg 0.161 µg/Kg10/17/2001 23-11-101701 600373 4705549 23 0308030-11 Cl5-BZ#87 0.952 µg/Kg 0.0716 µg/Kg10/17/2001 23-11-101701 600373 4705549 23 0308030-11 Cl5-BZ#95 0.0810 J µg/Kg 0.0554 µg/Kg10/17/2001 23-11-101701 600373 4705549 23 0308030-11 Cl5-BZ#99 3.23 µg/Kg 0.0378 µg/Kg10/17/2001 23-11-101701 600373 4705549 23 0308030-11 Cl5-BZ#101 0.203 J µg/Kg 0.108 µg/Kg10/17/2001 23-11-101701 600373 4705549 23 0308030-11 Cl5-BZ#105 2.09 µg/Kg 0.0527 µg/Kg10/17/2001 23-11-101701 600373 4705549 23 0308030-11 Cl5-BZ#110 0.103 U µg/Kg 0.103 µg/Kg10/17/2001 23-11-101701 600373 4705549 23 0308030-11 Cl5-BZ#114 0.223 J µg/Kg 0.0473 µg/Kg10/17/2001 23-11-101701 600373 4705549 23 0308030-11 Cl5-BZ#118 4.81 µg/Kg 0.111 µg/Kg10/17/2001 23-11-101701 600373 4705549 23 0308030-11 Cl5-BZ#123 0.0932 U µg/Kg 0.0932 µg/Kg10/17/2001 23-11-101701 600373 4705549 23 0308030-11 Cl5-BZ#126 0.0824 U µg/Kg 0.0824 µg/Kg10/17/2001 23-11-101701 600373 4705549 23 0308030-11 Cl6-BZ#128 0.959 µg/Kg 0.0743 µg/Kg10/17/2001 23-11-101701 600373 4705549 23 0308030-11 Cl6-BZ#138 14.3 µg/Kg 0.107 µg/Kg10/17/2001 23-11-101701 600373 4705549 23 0308030-11 Cl6-BZ#146 1.68 µg/Kg 0.0675 µg/Kg10/17/2001 23-11-101701 600373 4705549 23 0308030-11 Cl6-BZ#149 0.128 J µg/Kg 0.0864 µg/Kg10/17/2001 23-11-101701 600373 4705549 23 0308030-11 Cl6-BZ#151 0.143 U µg/Kg 0.143 µg/Kg10/17/2001 23-11-101701 600373 4705549 23 0308030-11 Cl6-BZ#153 14.2 µg/Kg 0.123 µg/Kg10/17/2001 23-11-101701 600373 4705549 23 0308030-11 Cl6-BZ#156 0.803 µg/Kg 0.0878 µg/Kg10/17/2001 23-11-101701 600373 4705549 23 0308030-11 Cl6-BZ#157 0.169 J µg/Kg 0.0689 µg/Kg



Extracted 7/30/04




SITE NUMBER



10/17/2001 23-11-101701 600373 4705549 23 0308030-11 Cl6-BZ#158 0.243 J µg/Kg 0.0581 µg/Kg10/17/2001 23-11-101701 600373 4705549 23 0308030-11 Cl6-BZ#167 0.500 µg/Kg 0.0743 µg/Kg10/17/2001 23-11-101701 600373 4705549 23 0308030-11 Cl6-BZ#169 0.239 U µg/Kg 0.239 µg/Kg10/17/2001 23-11-101701 600373 4705549 23 0308030-11 Cl7-BZ#170 0.278 U µg/Kg 0.278 µg/Kg10/17/2001 23-11-101701 600373 4705549 23 0308030-11 Cl7-BZ#174 0.0567 U µg/Kg 0.0567 µg/Kg10/17/2001 23-11-101701 600373 4705549 23 0308030-11 Cl7-BZ#177 0.0797 U µg/Kg 0.0797 µg/Kg10/17/2001 23-11-101701 600373 4705549 23 0308030-11 Cl7-BZ#180 0.119 U µg/Kg 0.119 µg/Kg10/17/2001 23-11-101701 600373 4705549 23 0308030-11 Cl7-BZ#183 0.628 µg/Kg 0.0540 µg/Kg10/17/2001 23-11-101701 600373 4705549 23 0308030-11 Cl7-BZ#187 1.32 µg/Kg 0.0594 µg/Kg10/17/2001 23-11-101701 600373 4705549 23 0308030-11 Cl7-BZ#189 0.107 U µg/Kg 0.107 µg/Kg10/17/2001 23-11-101701 600373 4705549 23 0308030-11 Cl8-BZ#194 0.124 U µg/Kg 0.124 µg/Kg10/17/2001 23-11-101701 600373 4705549 23 0308030-11 Cl8-BZ#195 0.331 J µg/Kg 0.123 µg/Kg10/17/2001 23-11-101701 600373 4705549 23 0308030-11 Cl8-BZ#201 0.830 µg/Kg 0.108 µg/Kg10/17/2001 23-11-101701 600373 4705549 23 0308030-11 Cl9-BZ#206 4.63 µg/Kg 0.145 µg/Kg10/17/2001 23-11-101701 600373 4705549 23 0308030-11 Cl10-BZ#209 2.60 µg/Kg 0.0675 µg/Kg10/17/2001 23-11-101701 600373 4705549 23 0308030-11 Monochlorobiphenyls 3.97 U µg/Kg 3.97 µg/Kg10/17/2001 23-11-101701 600373 4705549 23 0308030-11 Dichlorobiphenyls 0.116 U µg/Kg 0.116 µg/Kg10/17/2001 23-11-101701 600373 4705549 23 0308030-11 Trichlorobiphenyls 3.27 µg/Kg 0.398 µg/Kg10/17/2001 23-11-101701 600373 4705549 23 0308030-11 Tetrachlorobiphenyls 12.5 µg/Kg 0.0621 µg/Kg10/17/2001 23-11-101701 600373 4705549 23 0308030-11 Pentachlorobiphenyls 21.4 µg/Kg 0.0716 µg/Kg10/17/2001 23-11-101701 600373 4705549 23 0308030-11 Hexachlorobiphenyls 36.5 µg/Kg 0.113 µg/Kg10/17/2001 23-11-101701 600373 4705549 23 0308030-11 Heptachlorobiphenyls 1.75 µg/Kg 0.0621 µg/Kg10/17/2001 23-11-101701 600373 4705549 23 0308030-11 Octachlorobiphenyls 4.39 µg/Kg 0.0567 µg/Kg10/17/2001 23-11-101701 600373 4705549 23 0308030-11 Nonachlorobiphenyls 6.77 µg/Kg 0.145 µg/Kg10/17/2001 23-11-101701 600373 4705549 23 0308030-11 Decachlorobiphenyl 2.60 µg/Kg 0.0675 µg/Kg10/17/2001 23-11-101701 600373 4705549 23 0308030-11 Total Homologs 89.1 µg/Kg 0.0675 µg/Kg10/17/2001 23-11-101701 600373 4705549 23 0308030-11 Percent Lipids 2.8 % 0.1 %10/17/2001 23-11-101701 600373 4705549 23 0308030-11 Percent Moisture 71.7 % 0.1 %10/17/2001 23-12-101701 600373 4705549 23 0308030-12 Cl2-BZ#8 0.100 U µg/Kg 0.100 µg/Kg10/17/2001 23-12-101701 600373 4705549 23 0308030-12 Cl3-BZ#18 0.223 U µg/Kg 0.223 µg/Kg10/17/2001 23-12-101701 600373 4705549 23 0308030-12 Cl3-BZ#31/#28 9.00 µg/Kg 1.60 µg/Kg10/17/2001 23-12-101701 600373 4705549 23 0308030-12 Cl4-BZ#44 0.153 U µg/Kg 0.153 µg/Kg10/17/2001 23-12-101701 600373 4705549 23 0308030-12 Cl4-BZ#45 0.204 U µg/Kg 0.204 µg/Kg10/17/2001 23-12-101701 600373 4705549 23 0308030-12 Cl4-BZ#47 1.23 J µg/Kg 0.259 µg/Kg



Extracted 7/30/04




SITE NUMBER



10/17/2001 23-12-101701 600373 4705549 23 0308030-12 Cl4-BZ#49 0.127 U µg/Kg 0.127 µg/Kg10/17/2001 23-12-101701 600373 4705549 23 0308030-12 Cl4-BZ#52 0.186 J µg/Kg 0.145 µg/Kg10/17/2001 23-12-101701 600373 4705549 23 0308030-12 Cl4-BZ#56 0.664 µg/Kg 0.0758 µg/Kg10/17/2001 23-12-101701 600373 4705549 23 0308030-12 Cl4-BZ#66 1.43 µg/Kg 0.101 µg/Kg10/17/2001 23-12-101701 600373 4705549 23 0308030-12 Cl4-BZ#70 0.361 J µg/Kg 0.0886 µg/Kg10/17/2001 23-12-101701 600373 4705549 23 0308030-12 Cl4-BZ#74 0.717 J µg/Kg 0.156 µg/Kg10/17/2001 23-12-101701 600373 4705549 23 0308030-12 Cl4-BZ#77 0.140 U µg/Kg 0.140 µg/Kg10/17/2001 23-12-101701 600373 4705549 23 0308030-12 Cl4-BZ#81 0.139 U µg/Kg 0.139 µg/Kg10/17/2001 23-12-101701 600373 4705549 23 0308030-12 Cl5-BZ#87 0.548 µg/Kg 0.0618 µg/Kg10/17/2001 23-12-101701 600373 4705549 23 0308030-12 Cl5-BZ#95 0.0816 J µg/Kg 0.0478 µg/Kg10/17/2001 23-12-101701 600373 4705549 23 0308030-12 Cl5-BZ#99 1.85 µg/Kg 0.0326 µg/Kg10/17/2001 23-12-101701 600373 4705549 23 0308030-12 Cl5-BZ#101 0.274 J µg/Kg 0.0933 µg/Kg10/17/2001 23-12-101701 600373 4705549 23 0308030-12 Cl5-BZ#105 0.962 µg/Kg 0.0455 µg/Kg10/17/2001 23-12-101701 600373 4705549 23 0308030-12 Cl5-BZ#110 0.140 J µg/Kg 0.0886 µg/Kg10/17/2001 23-12-101701 600373 4705549 23 0308030-12 Cl5-BZ#114 0.0408 U µg/Kg 0.0408 µg/Kg10/17/2001 23-12-101701 600373 4705549 23 0308030-12 Cl5-BZ#118 1.97 µg/Kg 0.0956 µg/Kg10/17/2001 23-12-101701 600373 4705549 23 0308030-12 Cl5-BZ#123 0.0804 U µg/Kg 0.0804 µg/Kg10/17/2001 23-12-101701 600373 4705549 23 0308030-12 Cl5-BZ#126 0.0711 U µg/Kg 0.0711 µg/Kg10/17/2001 23-12-101701 600373 4705549 23 0308030-12 Cl6-BZ#128 0.595 µg/Kg 0.0641 µg/Kg10/17/2001 23-12-101701 600373 4705549 23 0308030-12 Cl6-BZ#138 8.57 µg/Kg 0.0921 µg/Kg10/17/2001 23-12-101701 600373 4705549 23 0308030-12 Cl6-BZ#146 1.11 µg/Kg 0.0583 µg/Kg10/17/2001 23-12-101701 600373 4705549 23 0308030-12 Cl6-BZ#149 0.210 J µg/Kg 0.0746 µg/Kg10/17/2001 23-12-101701 600373 4705549 23 0308030-12 Cl6-BZ#151 0.124 U µg/Kg 0.124 µg/Kg10/17/2001 23-12-101701 600373 4705549 23 0308030-12 Cl6-BZ#153 7.92 µg/Kg 0.106 µg/Kg10/17/2001 23-12-101701 600373 4705549 23 0308030-12 Cl6-BZ#156 0.350 J µg/Kg 0.0758 µg/Kg10/17/2001 23-12-101701 600373 4705549 23 0308030-12 Cl6-BZ#157 0.105 J µg/Kg 0.0595 µg/Kg10/17/2001 23-12-101701 600373 4705549 23 0308030-12 Cl6-BZ#158 0.163 J µg/Kg 0.0501 µg/Kg10/17/2001 23-12-101701 600373 4705549 23 0308030-12 Cl6-BZ#167 0.251 J µg/Kg 0.0641 µg/Kg10/17/2001 23-12-101701 600373 4705549 23 0308030-12 Cl6-BZ#169 0.206 U µg/Kg 0.206 µg/Kg10/17/2001 23-12-101701 600373 4705549 23 0308030-12 Cl7-BZ#170 0.240 U µg/Kg 0.240 µg/Kg10/17/2001 23-12-101701 600373 4705549 23 0308030-12 Cl7-BZ#174 0.0490 U µg/Kg 0.0490 µg/Kg10/17/2001 23-12-101701 600373 4705549 23 0308030-12 Cl7-BZ#177 0.0688 U µg/Kg 0.0688 µg/Kg10/17/2001 23-12-101701 600373 4705549 23 0308030-12 Cl7-BZ#180 0.103 U µg/Kg 0.103 µg/Kg10/17/2001 23-12-101701 600373 4705549 23 0308030-12 Cl7-BZ#183 0.635 µg/Kg 0.0466 µg/Kg



Extracted 7/30/04




SITE NUMBER



10/17/2001 23-12-101701 600373 4705549 23 0308030-12 Cl7-BZ#187 2.39 µg/Kg 0.0513 µg/Kg10/17/2001 23-12-101701 600373 4705549 23 0308030-12 Cl7-BZ#189 0.0921 U µg/Kg 0.0921 µg/Kg10/17/2001 23-12-101701 600373 4705549 23 0308030-12 Cl8-BZ#194 0.107 U µg/Kg 0.107 µg/Kg10/17/2001 23-12-101701 600373 4705549 23 0308030-12 Cl8-BZ#195 0.106 U µg/Kg 0.106 µg/Kg10/17/2001 23-12-101701 600373 4705549 23 0308030-12 Cl8-BZ#201 0.880 µg/Kg 0.0933 µg/Kg10/17/2001 23-12-101701 600373 4705549 23 0308030-12 Cl9-BZ#206 3.32 µg/Kg 0.125 µg/Kg10/17/2001 23-12-101701 600373 4705549 23 0308030-12 Cl10-BZ#209 2.03 µg/Kg 0.0583 µg/Kg10/17/2001 23-12-101701 600373 4705549 23 0308030-12 Monochlorobiphenyls 3.43 U µg/Kg 3.43 µg/Kg10/17/2001 23-12-101701 600373 4705549 23 0308030-12 Dichlorobiphenyls 0.100 U µg/Kg 0.100 µg/Kg10/17/2001 23-12-101701 600373 4705549 23 0308030-12 Trichlorobiphenyls 9.16 µg/Kg 0.344 µg/Kg10/17/2001 23-12-101701 600373 4705549 23 0308030-12 Tetrachlorobiphenyls 9.12 µg/Kg 0.0536 µg/Kg10/17/2001 23-12-101701 600373 4705549 23 0308030-12 Pentachlorobiphenyls 11.7 µg/Kg 0.0618 µg/Kg10/17/2001 23-12-101701 600373 4705549 23 0308030-12 Hexachlorobiphenyls 22.2 µg/Kg 0.0979 µg/Kg10/17/2001 23-12-101701 600373 4705549 23 0308030-12 Heptachlorobiphenyls 2.60 µg/Kg 0.0536 µg/Kg10/17/2001 23-12-101701 600373 4705549 23 0308030-12 Octachlorobiphenyls 0.565 µg/Kg 0.0490 µg/Kg10/17/2001 23-12-101701 600373 4705549 23 0308030-12 Nonachlorobiphenyls 4.98 µg/Kg 0.125 µg/Kg10/17/2001 23-12-101701 600373 4705549 23 0308030-12 Decachlorobiphenyl 2.03 µg/Kg 0.0583 µg/Kg10/17/2001 23-12-101701 600373 4705549 23 0308030-12 Total Homologs 62.3 µg/Kg 0.0583 µg/Kg10/17/2001 23-12-101701 600373 4705549 23 0308030-12 Percent Lipids 2.5 % 0.1 %10/17/2001 23-12-101701 600373 4705549 23 0308030-12 Percent Moisture 72.8 % 0.1 %10/18/2001 23-16-101801 600373 4705549 23 0308030-13 Cl2-BZ#8 0.0996 U µg/Kg 0.0996 µg/Kg10/18/2001 23-16-101801 600373 4705549 23 0308030-13 Cl3-BZ#18 0.221 U µg/Kg 0.221 µg/Kg10/18/2001 23-16-101801 600373 4705549 23 0308030-13 Cl3-BZ#31/#28 9.86 µg/Kg 1.60 µg/Kg10/18/2001 23-16-101801 600373 4705549 23 0308030-13 Cl4-BZ#44 0.152 U µg/Kg 0.152 µg/Kg10/18/2001 23-16-101801 600373 4705549 23 0308030-13 Cl4-BZ#45 0.203 U µg/Kg 0.203 µg/Kg10/18/2001 23-16-101801 600373 4705549 23 0308030-13 Cl4-BZ#47 0.672 J µg/Kg 0.257 µg/Kg10/18/2001 23-16-101801 600373 4705549 23 0308030-13 Cl4-BZ#49 0.126 U µg/Kg 0.126 µg/Kg10/18/2001 23-16-101801 600373 4705549 23 0308030-13 Cl4-BZ#52 0.185 J µg/Kg 0.144 µg/Kg10/18/2001 23-16-101801 600373 4705549 23 0308030-13 Cl4-BZ#56 0.515 µg/Kg 0.0753 µg/Kg10/18/2001 23-16-101801 600373 4705549 23 0308030-13 Cl4-BZ#66 0.938 µg/Kg 0.101 µg/Kg10/18/2001 23-16-101801 600373 4705549 23 0308030-13 Cl4-BZ#70 0.585 µg/Kg 0.0880 µg/Kg10/18/2001 23-16-101801 600373 4705549 23 0308030-13 Cl4-BZ#74 0.550 J µg/Kg 0.155 µg/Kg10/18/2001 23-16-101801 600373 4705549 23 0308030-13 Cl4-BZ#77 0.139 U µg/Kg 0.139 µg/Kg10/18/2001 23-16-101801 600373 4705549 23 0308030-13 Cl4-BZ#81 0.138 U µg/Kg 0.138 µg/Kg



Extracted 7/30/04




SITE NUMBER



10/18/2001 23-16-101801 600373 4705549 23 0308030-13 Cl5-BZ#87 0.371 µg/Kg 0.0614 µg/Kg10/18/2001 23-16-101801 600373 4705549 23 0308030-13 Cl5-BZ#95 0.0475 U µg/Kg 0.0475 µg/Kg10/18/2001 23-16-101801 600373 4705549 23 0308030-13 Cl5-BZ#99 1.26 µg/Kg 0.0324 µg/Kg10/18/2001 23-16-101801 600373 4705549 23 0308030-13 Cl5-BZ#101 0.168 J µg/Kg 0.0927 µg/Kg10/18/2001 23-16-101801 600373 4705549 23 0308030-13 Cl5-BZ#105 1.08 µg/Kg 0.0452 µg/Kg10/18/2001 23-16-101801 600373 4705549 23 0308030-13 Cl5-BZ#110 0.255 J µg/Kg 0.0880 µg/Kg10/18/2001 23-16-101801 600373 4705549 23 0308030-13 Cl5-BZ#114 0.145 J µg/Kg 0.0405 µg/Kg10/18/2001 23-16-101801 600373 4705549 23 0308030-13 Cl5-BZ#118 2.50 µg/Kg 0.0950 µg/Kg10/18/2001 23-16-101801 600373 4705549 23 0308030-13 Cl5-BZ#123 0.0799 U µg/Kg 0.0799 µg/Kg10/18/2001 23-16-101801 600373 4705549 23 0308030-13 Cl5-BZ#126 0.0706 U µg/Kg 0.0706 µg/Kg10/18/2001 23-16-101801 600373 4705549 23 0308030-13 Cl6-BZ#128 0.463 µg/Kg 0.0637 µg/Kg10/18/2001 23-16-101801 600373 4705549 23 0308030-13 Cl6-BZ#138 5.75 µg/Kg 0.0915 µg/Kg10/18/2001 23-16-101801 600373 4705549 23 0308030-13 Cl6-BZ#146 0.956 µg/Kg 0.0579 µg/Kg10/18/2001 23-16-101801 600373 4705549 23 0308030-13 Cl6-BZ#149 0.179 J µg/Kg 0.0741 µg/Kg10/18/2001 23-16-101801 600373 4705549 23 0308030-13 Cl6-BZ#151 0.123 U µg/Kg 0.123 µg/Kg10/18/2001 23-16-101801 600373 4705549 23 0308030-13 Cl6-BZ#153 6.40 µg/Kg 0.105 µg/Kg10/18/2001 23-16-101801 600373 4705549 23 0308030-13 Cl6-BZ#156 0.452 µg/Kg 0.0753 µg/Kg10/18/2001 23-16-101801 600373 4705549 23 0308030-13 Cl6-BZ#157 0.133 J µg/Kg 0.0591 µg/Kg10/18/2001 23-16-101801 600373 4705549 23 0308030-13 Cl6-BZ#158 0.122 J µg/Kg 0.0498 µg/Kg10/18/2001 23-16-101801 600373 4705549 23 0308030-13 Cl6-BZ#167 0.261 J µg/Kg 0.0637 µg/Kg10/18/2001 23-16-101801 600373 4705549 23 0308030-13 Cl6-BZ#169 0.205 U µg/Kg 0.205 µg/Kg10/18/2001 23-16-101801 600373 4705549 23 0308030-13 Cl7-BZ#170 0.239 U µg/Kg 0.239 µg/Kg10/18/2001 23-16-101801 600373 4705549 23 0308030-13 Cl7-BZ#174 0.0486 U µg/Kg 0.0486 µg/Kg10/18/2001 23-16-101801 600373 4705549 23 0308030-13 Cl7-BZ#177 0.0683 U µg/Kg 0.0683 µg/Kg10/18/2001 23-16-101801 600373 4705549 23 0308030-13 Cl7-BZ#180 0.102 U µg/Kg 0.102 µg/Kg10/18/2001 23-16-101801 600373 4705549 23 0308030-13 Cl7-BZ#183 0.347 µg/Kg 0.0463 µg/Kg10/18/2001 23-16-101801 600373 4705549 23 0308030-13 Cl7-BZ#187 1.77 µg/Kg 0.0510 µg/Kg10/18/2001 23-16-101801 600373 4705549 23 0308030-13 Cl7-BZ#189 0.0915 U µg/Kg 0.0915 µg/Kg10/18/2001 23-16-101801 600373 4705549 23 0308030-13 Cl8-BZ#194 0.106 U µg/Kg 0.106 µg/Kg10/18/2001 23-16-101801 600373 4705549 23 0308030-13 Cl8-BZ#195 0.105 U µg/Kg 0.105 µg/Kg10/18/2001 23-16-101801 600373 4705549 23 0308030-13 Cl8-BZ#201 0.567 µg/Kg 0.0927 µg/Kg10/18/2001 23-16-101801 600373 4705549 23 0308030-13 Cl9-BZ#206 0.735 µg/Kg 0.124 µg/Kg10/18/2001 23-16-101801 600373 4705549 23 0308030-13 Cl10-BZ#209 0.371 µg/Kg 0.0579 µg/Kg10/18/2001 23-16-101801 600373 4705549 23 0308030-13 Monochlorobiphenyls 3.40 U µg/Kg 3.40 µg/Kg



Extracted 7/30/04




SITE NUMBER



10/18/2001 23-16-101801 600373 4705549 23 0308030-13 Dichlorobiphenyls 0.0996 U µg/Kg 0.0996 µg/Kg10/18/2001 23-16-101801 600373 4705549 23 0308030-13 Trichlorobiphenyls 2.22 µg/Kg 0.342 µg/Kg10/18/2001 23-16-101801 600373 4705549 23 0308030-13 Tetrachlorobiphenyls 8.07 µg/Kg 0.0533 µg/Kg10/18/2001 23-16-101801 600373 4705549 23 0308030-13 Pentachlorobiphenyls 20.5 µg/Kg 0.0614 µg/Kg10/18/2001 23-16-101801 600373 4705549 23 0308030-13 Hexachlorobiphenyls 17.9 µg/Kg 0.0973 µg/Kg10/18/2001 23-16-101801 600373 4705549 23 0308030-13 Heptachlorobiphenyls 1.86 µg/Kg 0.0533 µg/Kg10/18/2001 23-16-101801 600373 4705549 23 0308030-13 Octachlorobiphenyls 0.458 µg/Kg 0.0486 µg/Kg10/18/2001 23-16-101801 600373 4705549 23 0308030-13 Nonachlorobiphenyls 2.40 µg/Kg 0.124 µg/Kg10/18/2001 23-16-101801 600373 4705549 23 0308030-13 Decachlorobiphenyl 0.371 µg/Kg 0.0579 µg/Kg10/18/2001 23-16-101801 600373 4705549 23 0308030-13 Total Homologs 53.8 µg/Kg 0.0579 µg/Kg10/18/2001 23-16-101801 600373 4705549 23 0308030-13 Percent Lipids 3.4 % 0.1 %10/18/2001 23-16-101801 600373 4705549 23 0308030-13 Percent Moisture 73.3 % 0.1 %10/18/2001 23-19-101801 600373 4705549 23 0308030-14 Cl2-BZ#8 0.117 U µg/Kg 0.117 µg/Kg10/18/2001 23-19-101801 600373 4705549 23 0308030-14 Cl3-BZ#18 0.259 U µg/Kg 0.259 µg/Kg10/18/2001 23-19-101801 600373 4705549 23 0308030-14 Cl3-BZ#31/#28 1.87 U µg/Kg 1.87 µg/Kg10/18/2001 23-19-101801 600373 4705549 23 0308030-14 Cl4-BZ#44 0.178 U µg/Kg 0.178 µg/Kg10/18/2001 23-19-101801 600373 4705549 23 0308030-14 Cl4-BZ#45 0.238 U µg/Kg 0.238 µg/Kg10/18/2001 23-19-101801 600373 4705549 23 0308030-14 Cl4-BZ#47 0.523 J µg/Kg 0.301 µg/Kg10/18/2001 23-19-101801 600373 4705549 23 0308030-14 Cl4-BZ#49 0.148 U µg/Kg 0.148 µg/Kg10/18/2001 23-19-101801 600373 4705549 23 0308030-14 Cl4-BZ#52 0.168 U µg/Kg 0.168 µg/Kg10/18/2001 23-19-101801 600373 4705549 23 0308030-14 Cl4-BZ#56 0.0883 U µg/Kg 0.0883 µg/Kg10/18/2001 23-19-101801 600373 4705549 23 0308030-14 Cl4-BZ#66 1.30 µg/Kg 0.118 µg/Kg10/18/2001 23-19-101801 600373 4705549 23 0308030-14 Cl4-BZ#70 0.224 J µg/Kg 0.103 µg/Kg10/18/2001 23-19-101801 600373 4705549 23 0308030-14 Cl4-BZ#74 0.312 J µg/Kg 0.182 µg/Kg10/18/2001 23-19-101801 600373 4705549 23 0308030-14 Cl4-BZ#77 0.163 U µg/Kg 0.163 µg/Kg10/18/2001 23-19-101801 600373 4705549 23 0308030-14 Cl4-BZ#81 0.162 U µg/Kg 0.162 µg/Kg10/18/2001 23-19-101801 600373 4705549 23 0308030-14 Cl5-BZ#87 0.312 J µg/Kg 0.0720 µg/Kg10/18/2001 23-19-101801 600373 4705549 23 0308030-14 Cl5-BZ#95 0.0557 U µg/Kg 0.0557 µg/Kg10/18/2001 23-19-101801 600373 4705549 23 0308030-14 Cl5-BZ#99 1.24 µg/Kg 0.0380 µg/Kg10/18/2001 23-19-101801 600373 4705549 23 0308030-14 Cl5-BZ#101 0.170 J µg/Kg 0.109 µg/Kg10/18/2001 23-19-101801 600373 4705549 23 0308030-14 Cl5-BZ#105 0.713 µg/Kg 0.0530 µg/Kg10/18/2001 23-19-101801 600373 4705549 23 0308030-14 Cl5-BZ#110 0.136 J µg/Kg 0.103 µg/Kg10/18/2001 23-19-101801 600373 4705549 23 0308030-14 Cl5-BZ#114 0.0475 U µg/Kg 0.0475 µg/Kg10/18/2001 23-19-101801 600373 4705549 23 0308030-14 Cl5-BZ#118 1.72 µg/Kg 0.111 µg/Kg



Extracted 7/30/04




SITE NUMBER



10/18/2001 23-19-101801 600373 4705549 23 0308030-14 Cl5-BZ#123 0.0937 U µg/Kg 0.0937 µg/Kg10/18/2001 23-19-101801 600373 4705549 23 0308030-14 Cl5-BZ#126 0.0828 U µg/Kg 0.0828 µg/Kg10/18/2001 23-19-101801 600373 4705549 23 0308030-14 Cl6-BZ#128 0.441 µg/Kg 0.0747 µg/Kg10/18/2001 23-19-101801 600373 4705549 23 0308030-14 Cl6-BZ#138 6.10 µg/Kg 0.107 µg/Kg10/18/2001 23-19-101801 600373 4705549 23 0308030-14 Cl6-BZ#146 0.699 µg/Kg 0.0679 µg/Kg10/18/2001 23-19-101801 600373 4705549 23 0308030-14 Cl6-BZ#149 0.156 J µg/Kg 0.0869 µg/Kg10/18/2001 23-19-101801 600373 4705549 23 0308030-14 Cl6-BZ#151 0.144 U µg/Kg 0.144 µg/Kg10/18/2001 23-19-101801 600373 4705549 23 0308030-14 Cl6-BZ#153 6.74 µg/Kg 0.124 µg/Kg10/18/2001 23-19-101801 600373 4705549 23 0308030-14 Cl6-BZ#156 0.326 J µg/Kg 0.0883 µg/Kg10/18/2001 23-19-101801 600373 4705549 23 0308030-14 Cl6-BZ#157 0.0693 U µg/Kg 0.0693 µg/Kg10/18/2001 23-19-101801 600373 4705549 23 0308030-14 Cl6-BZ#158 0.183 J µg/Kg 0.0584 µg/Kg10/18/2001 23-19-101801 600373 4705549 23 0308030-14 Cl6-BZ#167 0.156 J µg/Kg 0.0747 µg/Kg10/18/2001 23-19-101801 600373 4705549 23 0308030-14 Cl6-BZ#169 0.240 U µg/Kg 0.240 µg/Kg10/18/2001 23-19-101801 600373 4705549 23 0308030-14 Cl7-BZ#170 0.280 U µg/Kg 0.280 µg/Kg10/18/2001 23-19-101801 600373 4705549 23 0308030-14 Cl7-BZ#174 0.0570 U µg/Kg 0.0570 µg/Kg10/18/2001 23-19-101801 600373 4705549 23 0308030-14 Cl7-BZ#177 0.0801 U µg/Kg 0.0801 µg/Kg10/18/2001 23-19-101801 600373 4705549 23 0308030-14 Cl7-BZ#180 0.119 U µg/Kg 0.119 µg/Kg10/18/2001 23-19-101801 600373 4705549 23 0308030-14 Cl7-BZ#183 0.468 µg/Kg 0.0543 µg/Kg10/18/2001 23-19-101801 600373 4705549 23 0308030-14 Cl7-BZ#187 1.06 µg/Kg 0.0598 µg/Kg10/18/2001 23-19-101801 600373 4705549 23 0308030-14 Cl7-BZ#189 0.107 U µg/Kg 0.107 µg/Kg10/18/2001 23-19-101801 600373 4705549 23 0308030-14 Cl8-BZ#194 0.125 U µg/Kg 0.125 µg/Kg10/18/2001 23-19-101801 600373 4705549 23 0308030-14 Cl8-BZ#195 0.124 U µg/Kg 0.124 µg/Kg10/18/2001 23-19-101801 600373 4705549 23 0308030-14 Cl8-BZ#201 0.394 J µg/Kg 0.109 µg/Kg10/18/2001 23-19-101801 600373 4705549 23 0308030-14 Cl9-BZ#206 1.17 µg/Kg 0.145 µg/Kg10/18/2001 23-19-101801 600373 4705549 23 0308030-14 Cl10-BZ#209 0.869 µg/Kg 0.0679 µg/Kg10/18/2001 23-19-101801 600373 4705549 23 0308030-14 Monochlorobiphenyls 3.99 U µg/Kg 3.99 µg/Kg10/18/2001 23-19-101801 600373 4705549 23 0308030-14 Dichlorobiphenyls 0.117 U µg/Kg 0.117 µg/Kg10/18/2001 23-19-101801 600373 4705549 23 0308030-14 Trichlorobiphenyls 3.66 µg/Kg 0.401 µg/Kg10/18/2001 23-19-101801 600373 4705549 23 0308030-14 Tetrachlorobiphenyls 4.70 µg/Kg 0.0625 µg/Kg10/18/2001 23-19-101801 600373 4705549 23 0308030-14 Pentachlorobiphenyls 12.9 µg/Kg 0.0720 µg/Kg10/18/2001 23-19-101801 600373 4705549 23 0308030-14 Hexachlorobiphenyls 16.4 µg/Kg 0.114 µg/Kg10/18/2001 23-19-101801 600373 4705549 23 0308030-14 Heptachlorobiphenyls 1.45 µg/Kg 0.0625 µg/Kg10/18/2001 23-19-101801 600373 4705549 23 0308030-14 Octachlorobiphenyls 0.306 µg/Kg 0.0570 µg/Kg10/18/2001 23-19-101801 600373 4705549 23 0308030-14 Nonachlorobiphenyls 2.35 µg/Kg 0.145 µg/Kg



Extracted 7/30/04




SITE NUMBER



10/18/2001 23-19-101801 600373 4705549 23 0308030-14 Decachlorobiphenyl 0.869 µg/Kg 0.0679 µg/Kg10/18/2001 23-19-101801 600373 4705549 23 0308030-14 Total Homologs 42.6 µg/Kg 0.0679 µg/Kg10/18/2001 23-19-101801 600373 4705549 23 0308030-14 Percent Lipids 2.0 % 0.1 %10/18/2001 23-19-101801 600373 4705549 23 0308030-14 Percent Moisture 70.5 % 0.1 %10/18/2001 23-20-101801 600373 4705549 23 0308030-15 Cl2-BZ#8 0.107 U µg/Kg 0.107 µg/Kg10/18/2001 23-20-101801 600373 4705549 23 0308030-15 Cl3-BZ#18 0.238 U µg/Kg 0.238 µg/Kg10/18/2001 23-20-101801 600373 4705549 23 0308030-15 Cl3-BZ#31/#28 8.17 J µg/Kg 1.72 µg/Kg10/18/2001 23-20-101801 600373 4705549 23 0308030-15 Cl4-BZ#44 0.175 J µg/Kg 0.163 µg/Kg10/18/2001 23-20-101801 600373 4705549 23 0308030-15 Cl4-BZ#45 0.218 U µg/Kg 0.218 µg/Kg10/18/2001 23-20-101801 600373 4705549 23 0308030-15 Cl4-BZ#47 1.09 J µg/Kg 0.277 µg/Kg10/18/2001 23-20-101801 600373 4705549 23 0308030-15 Cl4-BZ#49 0.136 U µg/Kg 0.136 µg/Kg10/18/2001 23-20-101801 600373 4705549 23 0308030-15 Cl4-BZ#52 0.343 J µg/Kg 0.154 µg/Kg10/18/2001 23-20-101801 600373 4705549 23 0308030-15 Cl4-BZ#56 0.0810 U µg/Kg 0.0810 µg/Kg10/18/2001 23-20-101801 600373 4705549 23 0308030-15 Cl4-BZ#66 0.891 µg/Kg 0.108 µg/Kg10/18/2001 23-20-101801 600373 4705549 23 0308030-15 Cl4-BZ#70 0.567 µg/Kg 0.0947 µg/Kg10/18/2001 23-20-101801 600373 4705549 23 0308030-15 Cl4-BZ#74 0.442 J µg/Kg 0.167 µg/Kg10/18/2001 23-20-101801 600373 4705549 23 0308030-15 Cl4-BZ#77 0.150 U µg/Kg 0.150 µg/Kg10/18/2001 23-20-101801 600373 4705549 23 0308030-15 Cl4-BZ#81 0.148 U µg/Kg 0.148 µg/Kg10/18/2001 23-20-101801 600373 4705549 23 0308030-15 Cl5-BZ#87 0.0661 U µg/Kg 0.0661 µg/Kg10/18/2001 23-20-101801 600373 4705549 23 0308030-15 Cl5-BZ#95 0.143 J µg/Kg 0.0511 µg/Kg10/18/2001 23-20-101801 600373 4705549 23 0308030-15 Cl5-BZ#99 1.54 µg/Kg 0.0349 µg/Kg10/18/2001 23-20-101801 600373 4705549 23 0308030-15 Cl5-BZ#101 0.255 J µg/Kg 0.0997 µg/Kg10/18/2001 23-20-101801 600373 4705549 23 0308030-15 Cl5-BZ#105 0.735 µg/Kg 0.0486 µg/Kg10/18/2001 23-20-101801 600373 4705549 23 0308030-15 Cl5-BZ#110 0.249 J µg/Kg 0.0947 µg/Kg10/18/2001 23-20-101801 600373 4705549 23 0308030-15 Cl5-BZ#114 0.0436 U µg/Kg 0.0436 µg/Kg10/18/2001 23-20-101801 600373 4705549 23 0308030-15 Cl5-BZ#118 1.96 µg/Kg 0.102 µg/Kg10/18/2001 23-20-101801 600373 4705549 23 0308030-15 Cl5-BZ#123 0.0860 U µg/Kg 0.0860 µg/Kg10/18/2001 23-20-101801 600373 4705549 23 0308030-15 Cl5-BZ#126 0.0760 U µg/Kg 0.0760 µg/Kg10/18/2001 23-20-101801 600373 4705549 23 0308030-15 Cl6-BZ#128 0.617 µg/Kg 0.0685 µg/Kg10/18/2001 23-20-101801 600373 4705549 23 0308030-15 Cl6-BZ#138 5.96 µg/Kg 0.0985 µg/Kg10/18/2001 23-20-101801 600373 4705549 23 0308030-15 Cl6-BZ#146 1.17 µg/Kg 0.0623 µg/Kg10/18/2001 23-20-101801 600373 4705549 23 0308030-15 Cl6-BZ#149 0.224 J µg/Kg 0.0798 µg/Kg10/18/2001 23-20-101801 600373 4705549 23 0308030-15 Cl6-BZ#151 0.132 U µg/Kg 0.132 µg/Kg10/18/2001 23-20-101801 600373 4705549 23 0308030-15 Cl6-BZ#153 5.92 µg/Kg 0.113 µg/Kg



Extracted 7/30/04




SITE NUMBER



10/18/2001 23-20-101801 600373 4705549 23 0308030-15 Cl6-BZ#156 0.299 J µg/Kg 0.0810 µg/Kg10/18/2001 23-20-101801 600373 4705549 23 0308030-15 Cl6-BZ#157 0.0810 J µg/Kg 0.0636 µg/Kg10/18/2001 23-20-101801 600373 4705549 23 0308030-15 Cl6-BZ#158 0.181 J µg/Kg 0.0536 µg/Kg10/18/2001 23-20-101801 600373 4705549 23 0308030-15 Cl6-BZ#167 0.199 J µg/Kg 0.0685 µg/Kg10/18/2001 23-20-101801 600373 4705549 23 0308030-15 Cl6-BZ#169 0.221 U µg/Kg 0.221 µg/Kg10/18/2001 23-20-101801 600373 4705549 23 0308030-15 Cl7-BZ#170 0.257 U µg/Kg 0.257 µg/Kg10/18/2001 23-20-101801 600373 4705549 23 0308030-15 Cl7-BZ#174 0.0523 U µg/Kg 0.0523 µg/Kg10/18/2001 23-20-101801 600373 4705549 23 0308030-15 Cl7-BZ#177 0.0735 U µg/Kg 0.0735 µg/Kg10/18/2001 23-20-101801 600373 4705549 23 0308030-15 Cl7-BZ#180 0.110 U µg/Kg 0.110 µg/Kg10/18/2001 23-20-101801 600373 4705549 23 0308030-15 Cl7-BZ#183 0.424 µg/Kg 0.0499 µg/Kg10/18/2001 23-20-101801 600373 4705549 23 0308030-15 Cl7-BZ#187 1.88 µg/Kg 0.0548 µg/Kg10/18/2001 23-20-101801 600373 4705549 23 0308030-15 Cl7-BZ#189 0.0985 U µg/Kg 0.0985 µg/Kg10/18/2001 23-20-101801 600373 4705549 23 0308030-15 Cl8-BZ#194 0.115 U µg/Kg 0.115 µg/Kg10/18/2001 23-20-101801 600373 4705549 23 0308030-15 Cl8-BZ#195 0.113 U µg/Kg 0.113 µg/Kg10/18/2001 23-20-101801 600373 4705549 23 0308030-15 Cl8-BZ#201 0.953 µg/Kg 0.0997 µg/Kg10/18/2001 23-20-101801 600373 4705549 23 0308030-15 Cl9-BZ#206 0.854 µg/Kg 0.133 µg/Kg10/18/2001 23-20-101801 600373 4705549 23 0308030-15 Cl10-BZ#209 0.561 µg/Kg 0.0623 µg/Kg10/18/2001 23-20-101801 600373 4705549 23 0308030-15 Monochlorobiphenyls 3.66 U µg/Kg 3.66 µg/Kg10/18/2001 23-20-101801 600373 4705549 23 0308030-15 Dichlorobiphenyls 0.107 U µg/Kg 0.107 µg/Kg10/18/2001 23-20-101801 600373 4705549 23 0308030-15 Trichlorobiphenyls 6.38 µg/Kg 0.368 µg/Kg10/18/2001 23-20-101801 600373 4705549 23 0308030-15 Tetrachlorobiphenyls 6.01 µg/Kg 0.0573 µg/Kg10/18/2001 23-20-101801 600373 4705549 23 0308030-15 Pentachlorobiphenyls 19.6 µg/Kg 0.0661 µg/Kg10/18/2001 23-20-101801 600373 4705549 23 0308030-15 Hexachlorobiphenyls 16.4 µg/Kg 0.105 µg/Kg10/18/2001 23-20-101801 600373 4705549 23 0308030-15 Heptachlorobiphenyls 2.09 µg/Kg 0.0573 µg/Kg10/18/2001 23-20-101801 600373 4705549 23 0308030-15 Octachlorobiphenyls 0.723 µg/Kg 0.0523 µg/Kg10/18/2001 23-20-101801 600373 4705549 23 0308030-15 Nonachlorobiphenyls 2.25 µg/Kg 0.133 µg/Kg10/18/2001 23-20-101801 600373 4705549 23 0308030-15 Decachlorobiphenyl 0.561 µg/Kg 0.0623 µg/Kg10/18/2001 23-20-101801 600373 4705549 23 0308030-15 Total Homologs 54.0 µg/Kg 0.0623 µg/Kg10/18/2001 23-20-101801 600373 4705549 23 0308030-15 Percent Lipids 3.0 % 0.1 %10/18/2001 23-20-101801 600373 4705549 23 0308030-15 Percent Moisture 73.3 % 0.1 %10/18/2001 23-21-101801 600373 4705549 23 0308031-01 Cl2-BZ#8 0.137 U µg/Kg 0.137 µg/Kg10/18/2001 23-21-101801 600373 4705549 23 0308031-01 Cl3-BZ#18 0.303 U µg/Kg 0.303 µg/Kg10/18/2001 23-21-101801 600373 4705549 23 0308031-01 Cl3-BZ#31/#28 2.48 J µg/Kg 2.19 µg/Kg10/18/2001 23-21-101801 600373 4705549 23 0308031-01 Cl4-BZ#44 0.208 U µg/Kg 0.208 µg/Kg



Extracted 7/30/04




SITE NUMBER



10/18/2001 23-21-101801 600373 4705549 23 0308031-01 Cl4-BZ#45 0.278 U µg/Kg 0.278 µg/Kg10/18/2001 23-21-101801 600373 4705549 23 0308031-01 Cl4-BZ#47 0.461 J µg/Kg 0.353 µg/Kg10/18/2001 23-21-101801 600373 4705549 23 0308031-01 Cl4-BZ#49 0.173 U µg/Kg 0.173 µg/Kg10/18/2001 23-21-101801 600373 4705549 23 0308031-01 Cl4-BZ#52 0.197 U µg/Kg 0.197 µg/Kg10/18/2001 23-21-101801 600373 4705549 23 0308031-01 Cl4-BZ#56 0.103 U µg/Kg 0.103 µg/Kg10/18/2001 23-21-101801 600373 4705549 23 0308031-01 Cl4-BZ#66 0.524 J µg/Kg 0.138 µg/Kg10/18/2001 23-21-101801 600373 4705549 23 0308031-01 Cl4-BZ#70 0.302 J µg/Kg 0.121 µg/Kg10/18/2001 23-21-101801 600373 4705549 23 0308031-01 Cl4-BZ#74 0.366 J µg/Kg 0.213 µg/Kg10/18/2001 23-21-101801 600373 4705549 23 0308031-01 Cl4-BZ#77 0.191 U µg/Kg 0.191 µg/Kg10/18/2001 23-21-101801 600373 4705549 23 0308031-01 Cl4-BZ#81 0.189 U µg/Kg 0.189 µg/Kg10/18/2001 23-21-101801 600373 4705549 23 0308031-01 Cl5-BZ#87 0.270 J µg/Kg 0.0842 µg/Kg10/18/2001 23-21-101801 600373 4705549 23 0308031-01 Cl5-BZ#95 0.0795 J µg/Kg 0.0652 µg/Kg10/18/2001 23-21-101801 600373 4705549 23 0308031-01 Cl5-BZ#99 1.05 µg/Kg 0.0445 µg/Kg10/18/2001 23-21-101801 600373 4705549 23 0308031-01 Cl5-BZ#101 0.127 J µg/Kg 0.127 µg/Kg10/18/2001 23-21-101801 600373 4705549 23 0308031-01 Cl5-BZ#105 0.532 µg/Kg 0.0620 µg/Kg10/18/2001 23-21-101801 600373 4705549 23 0308031-01 Cl5-BZ#110 0.121 U µg/Kg 0.121 µg/Kg10/18/2001 23-21-101801 600373 4705549 23 0308031-01 Cl5-BZ#114 0.0795 J µg/Kg 0.0556 µg/Kg10/18/2001 23-21-101801 600373 4705549 23 0308031-01 Cl5-BZ#118 1.34 µg/Kg 0.130 µg/Kg10/18/2001 23-21-101801 600373 4705549 23 0308031-01 Cl5-BZ#123 0.110 U µg/Kg 0.110 µg/Kg10/18/2001 23-21-101801 600373 4705549 23 0308031-01 Cl5-BZ#126 0.0969 U µg/Kg 0.0969 µg/Kg10/18/2001 23-21-101801 600373 4705549 23 0308031-01 Cl6-BZ#128 0.342 J µg/Kg 0.0874 µg/Kg10/18/2001 23-21-101801 600373 4705549 23 0308031-01 Cl6-BZ#138 3.84 µg/Kg 0.125 µg/Kg10/18/2001 23-21-101801 600373 4705549 23 0308031-01 Cl6-BZ#146 0.437 µg/Kg 0.0795 µg/Kg10/18/2001 23-21-101801 600373 4705549 23 0308031-01 Cl6-BZ#149 0.119 J µg/Kg 0.102 µg/Kg10/18/2001 23-21-101801 600373 4705549 23 0308031-01 Cl6-BZ#151 0.168 U µg/Kg 0.168 µg/Kg10/18/2001 23-21-101801 600373 4705549 23 0308031-01 Cl6-BZ#153 4.01 µg/Kg 0.145 µg/Kg10/18/2001 23-21-101801 600373 4705549 23 0308031-01 Cl6-BZ#156 0.222 J µg/Kg 0.103 µg/Kg10/18/2001 23-21-101801 600373 4705549 23 0308031-01 Cl6-BZ#157 0.0810 U µg/Kg 0.0810 µg/Kg10/18/2001 23-21-101801 600373 4705549 23 0308031-01 Cl6-BZ#158 0.111 J µg/Kg 0.0683 µg/Kg10/18/2001 23-21-101801 600373 4705549 23 0308031-01 Cl6-BZ#167 0.151 J µg/Kg 0.0874 µg/Kg10/18/2001 23-21-101801 600373 4705549 23 0308031-01 Cl6-BZ#169 0.281 U µg/Kg 0.281 µg/Kg10/18/2001 23-21-101801 600373 4705549 23 0308031-01 Cl7-BZ#170 0.327 U µg/Kg 0.327 µg/Kg10/18/2001 23-21-101801 600373 4705549 23 0308031-01 Cl7-BZ#174 0.0667 U µg/Kg 0.0667 µg/Kg10/18/2001 23-21-101801 600373 4705549 23 0308031-01 Cl7-BZ#177 0.0938 U µg/Kg 0.0938 µg/Kg



Extracted 7/30/04




SITE NUMBER



10/18/2001 23-21-101801 600373 4705549 23 0308031-01 Cl7-BZ#180 0.140 U µg/Kg 0.140 µg/Kg10/18/2001 23-21-101801 600373 4705549 23 0308031-01 Cl7-BZ#183 0.318 µg/Kg 0.0636 µg/Kg10/18/2001 23-21-101801 600373 4705549 23 0308031-01 Cl7-BZ#187 0.683 µg/Kg 0.0699 µg/Kg10/18/2001 23-21-101801 600373 4705549 23 0308031-01 Cl7-BZ#189 0.125 U µg/Kg 0.125 µg/Kg10/18/2001 23-21-101801 600373 4705549 23 0308031-01 Cl8-BZ#194 0.146 U µg/Kg 0.146 µg/Kg10/18/2001 23-21-101801 600373 4705549 23 0308031-01 Cl8-BZ#195 0.145 U µg/Kg 0.145 µg/Kg10/18/2001 23-21-101801 600373 4705549 23 0308031-01 Cl8-BZ#201 0.302 J µg/Kg 0.127 µg/Kg10/18/2001 23-21-101801 600373 4705549 23 0308031-01 Cl9-BZ#206 1.10 µg/Kg 0.170 µg/Kg10/18/2001 23-21-101801 600373 4705549 23 0308031-01 Cl10-BZ#209 0.660 µg/Kg 0.0795 µg/Kg10/18/2001 23-21-101801 600373 4705549 23 0308031-01 Monochlorobiphenyls 4.67 U µg/Kg 4.67 µg/Kg10/18/2001 23-21-101801 600373 4705549 23 0308031-01 Dichlorobiphenyls 0.137 U µg/Kg 0.137 µg/Kg10/18/2001 23-21-101801 600373 4705549 23 0308031-01 Trichlorobiphenyls 2.85 µg/Kg 0.469 µg/Kg10/18/2001 23-21-101801 600373 4705549 23 0308031-01 Tetrachlorobiphenyls 3.15 µg/Kg 0.0731 µg/Kg10/18/2001 23-21-101801 600373 4705549 23 0308031-01 Pentachlorobiphenyls 7.73 µg/Kg 0.0842 µg/Kg10/18/2001 23-21-101801 600373 4705549 23 0308031-01 Hexachlorobiphenyls 10.5 µg/Kg 0.133 µg/Kg10/18/2001 23-21-101801 600373 4705549 23 0308031-01 Heptachlorobiphenyls 0.977 µg/Kg 0.0731 µg/Kg10/18/2001 23-21-101801 600373 4705549 23 0308031-01 Octachlorobiphenyls 0.278 J µg/Kg 0.0667 µg/Kg10/18/2001 23-21-101801 600373 4705549 23 0308031-01 Nonachlorobiphenyls 1.10 µg/Kg 0.170 µg/Kg10/18/2001 23-21-101801 600373 4705549 23 0308031-01 Decachlorobiphenyl 0.660 µg/Kg 0.0795 µg/Kg10/18/2001 23-21-101801 600373 4705549 23 0308031-01 Total Homologs 27.3 µg/Kg 0.0795 µg/Kg10/18/2001 23-21-101801 600373 4705549 23 0308031-01 Percent Lipids 2.3 % 0.1 %10/18/2001 23-21-101801 600373 4705549 23 0308031-01 Percent Moisture 72.7 % 0.1 %


Mouse (Peromyscus spp.) Tissue Hudson NRDA Floodplain DatabaseVersion 2.0

Extracted 7/30/04




SITE NUMBER LAB ID ANALYTE1

9/7/2001 Comp of Sta 1 611675 4758823 1 0308031-02 Cl2-BZ#8 0.130 U µg/Kg 0.130 µg/Kg9/7/2001 Comp of Sta 1 611675 4758823 1 0308031-02 Cl3-BZ#18 0.289 U µg/Kg 0.289 µg/Kg9/7/2001 Comp of Sta 1 611675 4758823 1 0308031-02 Cl3-BZ#31/#28 5.22 J µg/Kg 2.08 µg/Kg9/7/2001 Comp of Sta 1 611675 4758823 1 0308031-02 Cl4-BZ#44 0.212 J µg/Kg 0.198 µg/Kg9/7/2001 Comp of Sta 1 611675 4758823 1 0308031-02 Cl4-BZ#45 0.265 U µg/Kg 0.265 µg/Kg9/7/2001 Comp of Sta 1 611675 4758823 1 0308031-02 Cl4-BZ#47 3.69 µg/Kg 0.336 µg/Kg9/7/2001 Comp of Sta 1 611675 4758823 1 0308031-02 Cl4-BZ#49 0.606 J µg/Kg 0.165 µg/Kg9/7/2001 Comp of Sta 1 611675 4758823 1 0308031-02 Cl4-BZ#52 1.01 µg/Kg 0.188 µg/Kg9/7/2001 Comp of Sta 1 611675 4758823 1 0308031-02 Cl4-BZ#56 1.76 µg/Kg 0.0984 µg/Kg9/7/2001 Comp of Sta 1 611675 4758823 1 0308031-02 Cl4-BZ#66 1.63 µg/Kg 0.132 µg/Kg9/7/2001 Comp of Sta 1 611675 4758823 1 0308031-02 Cl4-BZ#70 0.961 µg/Kg 0.115 µg/Kg9/7/2001 Comp of Sta 1 611675 4758823 1 0308031-02 Cl4-BZ#74 2.70 µg/Kg 0.203 µg/Kg9/7/2001 Comp of Sta 1 611675 4758823 1 0308031-02 Cl4-BZ#77 0.182 U µg/Kg 0.182 µg/Kg9/7/2001 Comp of Sta 1 611675 4758823 1 0308031-02 Cl4-BZ#81 0.180 U µg/Kg 0.180 µg/Kg9/7/2001 Comp of Sta 1 611675 4758823 1 0308031-02 Cl5-BZ#87 3.43 J µg/Kg 0.0802 µg/Kg9/7/2001 Comp of Sta 1 611675 4758823 1 0308031-02 Cl5-BZ#95 0.250 J µg/Kg 0.0621 µg/Kg9/7/2001 Comp of Sta 1 611675 4758823 1 0308031-02 Cl5-BZ#99 15.0 µg/Kg 0.0424 µg/Kg9/7/2001 Comp of Sta 1 611675 4758823 1 0308031-02 Cl5-BZ#101 1.72 µg/Kg 0.121 µg/Kg9/7/2001 Comp of Sta 1 611675 4758823 1 0308031-02 Cl5-BZ#105 7.71 µg/Kg 0.0590 µg/Kg9/7/2001 Comp of Sta 1 611675 4758823 1 0308031-02 Cl5-BZ#110 0.500 J µg/Kg 0.115 µg/Kg9/7/2001 Comp of Sta 1 611675 4758823 1 0308031-02 Cl5-BZ#114 0.553 µg/Kg 0.0530 µg/Kg9/7/2001 Comp of Sta 1 611675 4758823 1 0308031-02 Cl5-BZ#118 16.2 µg/Kg 0.124 µg/Kg9/7/2001 Comp of Sta 1 611675 4758823 1 0308031-02 Cl5-BZ#123 0.105 U µg/Kg 0.105 µg/Kg9/7/2001 Comp of Sta 1 611675 4758823 1 0308031-02 Cl5-BZ#126 0.0924 U µg/Kg 0.0924 µg/Kg9/7/2001 Comp of Sta 1 611675 4758823 1 0308031-02 Cl6-BZ#128 1.17 µg/Kg 0.0833 µg/Kg9/7/2001 Comp of Sta 1 611675 4758823 1 0308031-02 Cl6-BZ#138 42.1 µg/Kg 0.120 µg/Kg9/7/2001 Comp of Sta 1 611675 4758823 1 0308031-02 Cl6-BZ#146 4.00 µg/Kg 0.0757 µg/Kg9/7/2001 Comp of Sta 1 611675 4758823 1 0308031-02 Cl6-BZ#149 1.15 µg/Kg 0.0969 µg/Kg9/7/2001 Comp of Sta 1 611675 4758823 1 0308031-02 Cl6-BZ#151 0.212 J µg/Kg 0.161 µg/Kg9/7/2001 Comp of Sta 1 611675 4758823 1 0308031-02 Cl6-BZ#153 28.5 µg/Kg 0.138 µg/Kg9/7/2001 Comp of Sta 1 611675 4758823 1 0308031-02 Cl6-BZ#156 4.00 µg/Kg 0.0984 µg/Kg9/7/2001 Comp of Sta 1 611675 4758823 1 0308031-02 Cl6-BZ#157 0.643 µg/Kg 0.0772 µg/Kg9/7/2001 Comp of Sta 1 611675 4758823 1 0308031-02 Cl6-BZ#158 0.961 µg/Kg 0.0651 µg/Kg9/7/2001 Comp of Sta 1 611675 4758823 1 0308031-02 Cl6-BZ#167 0.522 µg/Kg 0.0833 µg/Kg9/7/2001 Comp of Sta 1 611675 4758823 1 0308031-02 Cl6-BZ#169 0.268 U µg/Kg 0.268 µg/Kg

VALUE, INTERPRETIVE QUALIFIER2 AND

UNITS3 DETECTION LIMIT3



Extracted 7/30/04







9/7/2001 Comp of Sta 1 611675 4758823 1 0308031-02 Cl7-BZ#170 4.63 µg/Kg 0.312 µg/Kg9/7/2001 Comp of Sta 1 611675 4758823 1 0308031-02 Cl7-BZ#174 0.0908 J µg/Kg 0.0636 µg/Kg9/7/2001 Comp of Sta 1 611675 4758823 1 0308031-02 Cl7-BZ#177 0.863 µg/Kg 0.0893 µg/Kg9/7/2001 Comp of Sta 1 611675 4758823 1 0308031-02 Cl7-BZ#180 5.34 µg/Kg 0.133 µg/Kg9/7/2001 Comp of Sta 1 611675 4758823 1 0308031-02 Cl7-BZ#183 0.681 µg/Kg 0.0606 µg/Kg9/7/2001 Comp of Sta 1 611675 4758823 1 0308031-02 Cl7-BZ#187 10.0 µg/Kg 0.0666 µg/Kg9/7/2001 Comp of Sta 1 611675 4758823 1 0308031-02 Cl7-BZ#189 0.120 U µg/Kg 0.120 µg/Kg9/7/2001 Comp of Sta 1 611675 4758823 1 0308031-02 Cl8-BZ#194 1.10 µg/Kg 0.139 µg/Kg9/7/2001 Comp of Sta 1 611675 4758823 1 0308031-02 Cl8-BZ#195 0.386 J µg/Kg 0.138 µg/Kg9/7/2001 Comp of Sta 1 611675 4758823 1 0308031-02 Cl8-BZ#201 3.22 µg/Kg 0.121 µg/Kg9/7/2001 Comp of Sta 1 611675 4758823 1 0308031-02 Cl9-BZ#206 0.931 µg/Kg 0.162 µg/Kg9/7/2001 Comp of Sta 1 611675 4758823 1 0308031-02 Cl10-BZ#209 0.182 J µg/Kg 0.0757 µg/Kg9/7/2001 Comp of Sta 1 611675 4758823 1 0308031-02 Monochlorobiphenyls 4.45 U µg/Kg 4.45 µg/Kg9/7/2001 Comp of Sta 1 611675 4758823 1 0308031-02 Dichlorobiphenyls 0.130 U µg/Kg 0.130 µg/Kg9/7/2001 Comp of Sta 1 611675 4758823 1 0308031-02 Trichlorobiphenyls 5.12 µg/Kg 0.447 µg/Kg9/7/2001 Comp of Sta 1 611675 4758823 1 0308031-02 Tetrachlorobiphenyls 20.9 µg/Kg 0.0696 µg/Kg9/7/2001 Comp of Sta 1 611675 4758823 1 0308031-02 Pentachlorobiphenyls 76.9 µg/Kg 0.0802 µg/Kg9/7/2001 Comp of Sta 1 611675 4758823 1 0308031-02 Hexachlorobiphenyls 92.7 µg/Kg 0.127 µg/Kg9/7/2001 Comp of Sta 1 611675 4758823 1 0308031-02 Heptachlorobiphenyls 22.8 µg/Kg 0.0696 µg/Kg9/7/2001 Comp of Sta 1 611675 4758823 1 0308031-02 Octachlorobiphenyls 4.31 µg/Kg 0.0636 µg/Kg9/7/2001 Comp of Sta 1 611675 4758823 1 0308031-02 Nonachlorobiphenyls 5.33 µg/Kg 0.162 µg/Kg9/7/2001 Comp of Sta 1 611675 4758823 1 0308031-02 Decachlorobiphenyl 0.182 J µg/Kg 0.0757 µg/Kg9/7/2001 Comp of Sta 1 611675 4758823 1 0308031-02 Total Homologs 228 µg/Kg 0.0757 µg/Kg9/7/2001 Comp of Sta 1 611675 4758823 1 0308031-02 Percent Lipids 4.8 J % 0.1 %9/7/2001 Comp of Sta 1 611675 4758823 1 0308031-02 Percent Moisture 71.3 % 0.1 %9/9/2001 Comp of Sta 3 613916 4762429 3 0308031-03 Cl2-BZ#8 0.117 U µg/Kg 0.117 µg/Kg9/9/2001 Comp of Sta 3 613916 4762429 3 0308031-03 Cl3-BZ#18 0.261 U µg/Kg 0.261 µg/Kg9/9/2001 Comp of Sta 3 613916 4762429 3 0308031-03 Cl3-BZ#31/#28 1.88 U µg/Kg 1.88 µg/Kg9/9/2001 Comp of Sta 3 613916 4762429 3 0308031-03 Cl4-BZ#44 0.179 U µg/Kg 0.179 µg/Kg9/9/2001 Comp of Sta 3 613916 4762429 3 0308031-03 Cl4-BZ#45 0.239 U µg/Kg 0.239 µg/Kg9/9/2001 Comp of Sta 3 613916 4762429 3 0308031-03 Cl4-BZ#47 0.444 J µg/Kg 0.303 µg/Kg9/9/2001 Comp of Sta 3 613916 4762429 3 0308031-03 Cl4-BZ#49 0.149 U µg/Kg 0.149 µg/Kg9/9/2001 Comp of Sta 3 613916 4762429 3 0308031-03 Cl4-BZ#52 0.252 J µg/Kg 0.169 µg/Kg9/9/2001 Comp of Sta 3 613916 4762429 3 0308031-03 Cl4-BZ#56 0.0887 U µg/Kg 0.0887 µg/Kg9/9/2001 Comp of Sta 3 613916 4762429 3 0308031-03 Cl4-BZ#66 0.328 J µg/Kg 0.119 µg/Kg



Extracted 7/30/04







9/9/2001 Comp of Sta 3 613916 4762429 3 0308031-03 Cl4-BZ#70 0.104 U µg/Kg 0.104 µg/Kg9/9/2001 Comp of Sta 3 613916 4762429 3 0308031-03 Cl4-BZ#74 0.184 J µg/Kg 0.183 µg/Kg9/9/2001 Comp of Sta 3 613916 4762429 3 0308031-03 Cl4-BZ#77 0.164 U µg/Kg 0.164 µg/Kg9/9/2001 Comp of Sta 3 613916 4762429 3 0308031-03 Cl4-BZ#81 0.162 U µg/Kg 0.162 µg/Kg9/9/2001 Comp of Sta 3 613916 4762429 3 0308031-03 Cl5-BZ#87 0.307 J µg/Kg 0.0723 µg/Kg9/9/2001 Comp of Sta 3 613916 4762429 3 0308031-03 Cl5-BZ#95 0.0560 U µg/Kg 0.0560 µg/Kg9/9/2001 Comp of Sta 3 613916 4762429 3 0308031-03 Cl5-BZ#99 0.682 µg/Kg 0.0382 µg/Kg9/9/2001 Comp of Sta 3 613916 4762429 3 0308031-03 Cl5-BZ#101 0.184 J µg/Kg 0.109 µg/Kg9/9/2001 Comp of Sta 3 613916 4762429 3 0308031-03 Cl5-BZ#105 0.341 µg/Kg 0.0532 µg/Kg9/9/2001 Comp of Sta 3 613916 4762429 3 0308031-03 Cl5-BZ#110 0.104 U µg/Kg 0.104 µg/Kg9/9/2001 Comp of Sta 3 613916 4762429 3 0308031-03 Cl5-BZ#114 0.0478 U µg/Kg 0.0478 µg/Kg9/9/2001 Comp of Sta 3 613916 4762429 3 0308031-03 Cl5-BZ#118 0.853 µg/Kg 0.112 µg/Kg9/9/2001 Comp of Sta 3 613916 4762429 3 0308031-03 Cl5-BZ#123 0.0942 U µg/Kg 0.0942 µg/Kg9/9/2001 Comp of Sta 3 613916 4762429 3 0308031-03 Cl5-BZ#126 0.0833 U µg/Kg 0.0833 µg/Kg9/9/2001 Comp of Sta 3 613916 4762429 3 0308031-03 Cl6-BZ#128 0.0751 U µg/Kg 0.0751 µg/Kg9/9/2001 Comp of Sta 3 613916 4762429 3 0308031-03 Cl6-BZ#138 1.67 µg/Kg 0.108 µg/Kg9/9/2001 Comp of Sta 3 613916 4762429 3 0308031-03 Cl6-BZ#146 0.246 J µg/Kg 0.0682 µg/Kg9/9/2001 Comp of Sta 3 613916 4762429 3 0308031-03 Cl6-BZ#149 0.0873 U µg/Kg 0.0873 µg/Kg9/9/2001 Comp of Sta 3 613916 4762429 3 0308031-03 Cl6-BZ#151 0.145 U µg/Kg 0.145 µg/Kg9/9/2001 Comp of Sta 3 613916 4762429 3 0308031-03 Cl6-BZ#153 1.69 µg/Kg 0.124 µg/Kg9/9/2001 Comp of Sta 3 613916 4762429 3 0308031-03 Cl6-BZ#156 0.266 J µg/Kg 0.0887 µg/Kg9/9/2001 Comp of Sta 3 613916 4762429 3 0308031-03 Cl6-BZ#157 0.0696 U µg/Kg 0.0696 µg/Kg9/9/2001 Comp of Sta 3 613916 4762429 3 0308031-03 Cl6-BZ#158 0.0587 U µg/Kg 0.0587 µg/Kg9/9/2001 Comp of Sta 3 613916 4762429 3 0308031-03 Cl6-BZ#167 0.0751 U µg/Kg 0.0751 µg/Kg9/9/2001 Comp of Sta 3 613916 4762429 3 0308031-03 Cl6-BZ#169 0.242 U µg/Kg 0.242 µg/Kg9/9/2001 Comp of Sta 3 613916 4762429 3 0308031-03 Cl7-BZ#170 1.02 J µg/Kg 0.281 µg/Kg9/9/2001 Comp of Sta 3 613916 4762429 3 0308031-03 Cl7-BZ#174 0.0573 U µg/Kg 0.0573 µg/Kg9/9/2001 Comp of Sta 3 613916 4762429 3 0308031-03 Cl7-BZ#177 0.109 J µg/Kg 0.0805 µg/Kg9/9/2001 Comp of Sta 3 613916 4762429 3 0308031-03 Cl7-BZ#180 1.10 µg/Kg 0.120 µg/Kg9/9/2001 Comp of Sta 3 613916 4762429 3 0308031-03 Cl7-BZ#183 0.116 J µg/Kg 0.0546 µg/Kg9/9/2001 Comp of Sta 3 613916 4762429 3 0308031-03 Cl7-BZ#187 0.594 µg/Kg 0.0601 µg/Kg9/9/2001 Comp of Sta 3 613916 4762429 3 0308031-03 Cl7-BZ#189 0.108 U µg/Kg 0.108 µg/Kg9/9/2001 Comp of Sta 3 613916 4762429 3 0308031-03 Cl8-BZ#194 0.341 J µg/Kg 0.126 µg/Kg9/9/2001 Comp of Sta 3 613916 4762429 3 0308031-03 Cl8-BZ#195 0.124 U µg/Kg 0.124 µg/Kg9/9/2001 Comp of Sta 3 613916 4762429 3 0308031-03 Cl8-BZ#201 0.566 µg/Kg 0.109 µg/Kg



Extracted 7/30/04







9/9/2001 Comp of Sta 3 613916 4762429 3 0308031-03 Cl9-BZ#206 0.146 U µg/Kg 0.146 µg/Kg9/9/2001 Comp of Sta 3 613916 4762429 3 0308031-03 Cl10-BZ#209 0.0682 U µg/Kg 0.0682 µg/Kg9/9/2001 Comp of Sta 3 613916 4762429 3 0308031-03 Monochlorobiphenyls 4.01 U µg/Kg 4.01 µg/Kg9/9/2001 Comp of Sta 3 613916 4762429 3 0308031-03 Dichlorobiphenyls 0.117 U µg/Kg 0.117 µg/Kg9/9/2001 Comp of Sta 3 613916 4762429 3 0308031-03 Trichlorobiphenyls 1.26 J µg/Kg 0.403 µg/Kg9/9/2001 Comp of Sta 3 613916 4762429 3 0308031-03 Tetrachlorobiphenyls 3.46 µg/Kg 0.0628 µg/Kg9/9/2001 Comp of Sta 3 613916 4762429 3 0308031-03 Pentachlorobiphenyls 4.61 µg/Kg 0.0723 µg/Kg9/9/2001 Comp of Sta 3 613916 4762429 3 0308031-03 Hexachlorobiphenyls 4.61 µg/Kg 0.115 µg/Kg9/9/2001 Comp of Sta 3 613916 4762429 3 0308031-03 Heptachlorobiphenyls 3.64 µg/Kg 0.0628 µg/Kg9/9/2001 Comp of Sta 3 613916 4762429 3 0308031-03 Octachlorobiphenyls 0.914 µg/Kg 0.0573 µg/Kg9/9/2001 Comp of Sta 3 613916 4762429 3 0308031-03 Nonachlorobiphenyls 0.146 U µg/Kg 0.146 µg/Kg9/9/2001 Comp of Sta 3 613916 4762429 3 0308031-03 Decachlorobiphenyl 0.0682 U µg/Kg 0.0682 µg/Kg9/9/2001 Comp of Sta 3 613916 4762429 3 0308031-03 Total Homologs 18.5 µg/Kg 0.0682 µg/Kg9/9/2001 Comp of Sta 3 613916 4762429 3 0308031-03 Percent Lipids 1.2 % 0.1 %9/9/2001 Comp of Sta 3 613916 4762429 3 0308031-03 Percent Moisture 71.5 % 0.1 %

9/12/2001 Comp of Sta 4 614689 4765951 4 0308031-04 Cl2-BZ#8 0.140 U µg/Kg 0.140 µg/Kg9/12/2001 Comp of Sta 4 614689 4765951 4 0308031-04 Cl3-BZ#18 0.310 U µg/Kg 0.310 µg/Kg9/12/2001 Comp of Sta 4 614689 4765951 4 0308031-04 Cl3-BZ#31/#28 4.20 J µg/Kg 2.24 µg/Kg9/12/2001 Comp of Sta 4 614689 4765951 4 0308031-04 Cl4-BZ#44 0.213 U µg/Kg 0.213 µg/Kg9/12/2001 Comp of Sta 4 614689 4765951 4 0308031-04 Cl4-BZ#45 0.284 U µg/Kg 0.284 µg/Kg9/12/2001 Comp of Sta 4 614689 4765951 4 0308031-04 Cl4-BZ#47 2.88 µg/Kg 0.361 µg/Kg9/12/2001 Comp of Sta 4 614689 4765951 4 0308031-04 Cl4-BZ#49 0.552 J µg/Kg 0.177 µg/Kg9/12/2001 Comp of Sta 4 614689 4765951 4 0308031-04 Cl4-BZ#52 1.15 µg/Kg 0.201 µg/Kg9/12/2001 Comp of Sta 4 614689 4765951 4 0308031-04 Cl4-BZ#56 2.35 µg/Kg 0.106 µg/Kg9/12/2001 Comp of Sta 4 614689 4765951 4 0308031-04 Cl4-BZ#66 3.48 µg/Kg 0.141 µg/Kg9/12/2001 Comp of Sta 4 614689 4765951 4 0308031-04 Cl4-BZ#70 0.503 J µg/Kg 0.123 µg/Kg9/12/2001 Comp of Sta 4 614689 4765951 4 0308031-04 Cl4-BZ#74 5.57 µg/Kg 0.218 µg/Kg9/12/2001 Comp of Sta 4 614689 4765951 4 0308031-04 Cl4-BZ#77 0.195 U µg/Kg 0.195 µg/Kg9/12/2001 Comp of Sta 4 614689 4765951 4 0308031-04 Cl4-BZ#81 0.193 U µg/Kg 0.193 µg/Kg9/12/2001 Comp of Sta 4 614689 4765951 4 0308031-04 Cl5-BZ#87 2.75 µg/Kg 0.0861 µg/Kg9/12/2001 Comp of Sta 4 614689 4765951 4 0308031-04 Cl5-BZ#95 0.211 J µg/Kg 0.0666 µg/Kg9/12/2001 Comp of Sta 4 614689 4765951 4 0308031-04 Cl5-BZ#99 9.61 µg/Kg 0.0455 µg/Kg9/12/2001 Comp of Sta 4 614689 4765951 4 0308031-04 Cl5-BZ#101 1.32 µg/Kg 0.130 µg/Kg9/12/2001 Comp of Sta 4 614689 4765951 4 0308031-04 Cl5-BZ#105 9.65 µg/Kg 0.0633 µg/Kg9/12/2001 Comp of Sta 4 614689 4765951 4 0308031-04 Cl5-BZ#110 0.123 U µg/Kg 0.123 µg/Kg



Extracted 7/30/04







9/12/2001 Comp of Sta 4 614689 4765951 4 0308031-04 Cl5-BZ#114 0.731 µg/Kg 0.0568 µg/Kg9/12/2001 Comp of Sta 4 614689 4765951 4 0308031-04 Cl5-BZ#118 20.0 µg/Kg 0.133 µg/Kg9/12/2001 Comp of Sta 4 614689 4765951 4 0308031-04 Cl5-BZ#123 0.112 U µg/Kg 0.112 µg/Kg9/12/2001 Comp of Sta 4 614689 4765951 4 0308031-04 Cl5-BZ#126 0.0991 U µg/Kg 0.0991 µg/Kg9/12/2001 Comp of Sta 4 614689 4765951 4 0308031-04 Cl6-BZ#128 0.885 µg/Kg 0.0893 µg/Kg9/12/2001 Comp of Sta 4 614689 4765951 4 0308031-04 Cl6-BZ#138 16.6 µg/Kg 0.128 µg/Kg9/12/2001 Comp of Sta 4 614689 4765951 4 0308031-04 Cl6-BZ#146 2.13 µg/Kg 0.0812 µg/Kg9/12/2001 Comp of Sta 4 614689 4765951 4 0308031-04 Cl6-BZ#149 0.300 J µg/Kg 0.104 µg/Kg9/12/2001 Comp of Sta 4 614689 4765951 4 0308031-04 Cl6-BZ#151 0.308 J µg/Kg 0.172 µg/Kg9/12/2001 Comp of Sta 4 614689 4765951 4 0308031-04 Cl6-BZ#153 16.5 µg/Kg 0.148 µg/Kg9/12/2001 Comp of Sta 4 614689 4765951 4 0308031-04 Cl6-BZ#156 2.72 µg/Kg 0.106 µg/Kg9/12/2001 Comp of Sta 4 614689 4765951 4 0308031-04 Cl6-BZ#157 0.430 µg/Kg 0.0828 µg/Kg9/12/2001 Comp of Sta 4 614689 4765951 4 0308031-04 Cl6-BZ#158 0.503 µg/Kg 0.0698 µg/Kg9/12/2001 Comp of Sta 4 614689 4765951 4 0308031-04 Cl6-BZ#167 0.593 µg/Kg 0.0893 µg/Kg9/12/2001 Comp of Sta 4 614689 4765951 4 0308031-04 Cl6-BZ#169 0.287 U µg/Kg 0.287 µg/Kg9/12/2001 Comp of Sta 4 614689 4765951 4 0308031-04 Cl7-BZ#170 2.94 µg/Kg 0.335 µg/Kg9/12/2001 Comp of Sta 4 614689 4765951 4 0308031-04 Cl7-BZ#174 0.0682 U µg/Kg 0.0682 µg/Kg9/12/2001 Comp of Sta 4 614689 4765951 4 0308031-04 Cl7-BZ#177 0.438 J µg/Kg 0.0958 µg/Kg9/12/2001 Comp of Sta 4 614689 4765951 4 0308031-04 Cl7-BZ#180 3.73 µg/Kg 0.143 µg/Kg9/12/2001 Comp of Sta 4 614689 4765951 4 0308031-04 Cl7-BZ#183 0.341 µg/Kg 0.0650 µg/Kg9/12/2001 Comp of Sta 4 614689 4765951 4 0308031-04 Cl7-BZ#187 4.29 µg/Kg 0.0715 µg/Kg9/12/2001 Comp of Sta 4 614689 4765951 4 0308031-04 Cl7-BZ#189 0.128 U µg/Kg 0.128 µg/Kg9/12/2001 Comp of Sta 4 614689 4765951 4 0308031-04 Cl8-BZ#194 0.820 µg/Kg 0.149 µg/Kg9/12/2001 Comp of Sta 4 614689 4765951 4 0308031-04 Cl8-BZ#195 0.235 J µg/Kg 0.148 µg/Kg9/12/2001 Comp of Sta 4 614689 4765951 4 0308031-04 Cl8-BZ#201 1.84 µg/Kg 0.130 µg/Kg9/12/2001 Comp of Sta 4 614689 4765951 4 0308031-04 Cl9-BZ#206 0.625 J µg/Kg 0.174 µg/Kg9/12/2001 Comp of Sta 4 614689 4765951 4 0308031-04 Cl10-BZ#209 0.130 J µg/Kg 0.0812 µg/Kg9/12/2001 Comp of Sta 4 614689 4765951 4 0308031-04 Monochlorobiphenyls 4.77 U µg/Kg 4.77 µg/Kg9/12/2001 Comp of Sta 4 614689 4765951 4 0308031-04 Dichlorobiphenyls 0.140 U µg/Kg 0.140 µg/Kg9/12/2001 Comp of Sta 4 614689 4765951 4 0308031-04 Trichlorobiphenyls 4.21 µg/Kg 0.479 µg/Kg9/12/2001 Comp of Sta 4 614689 4765951 4 0308031-04 Tetrachlorobiphenyls 23.5 µg/Kg 0.0747 µg/Kg9/12/2001 Comp of Sta 4 614689 4765951 4 0308031-04 Pentachlorobiphenyls 75.4 µg/Kg 0.0861 µg/Kg9/12/2001 Comp of Sta 4 614689 4765951 4 0308031-04 Hexachlorobiphenyls 44.9 µg/Kg 0.136 µg/Kg9/12/2001 Comp of Sta 4 614689 4765951 4 0308031-04 Heptachlorobiphenyls 12.1 µg/Kg 0.0747 µg/Kg9/12/2001 Comp of Sta 4 614689 4765951 4 0308031-04 Octachlorobiphenyls 3.04 µg/Kg 0.0682 µg/Kg



Extracted 7/30/04







9/12/2001 Comp of Sta 4 614689 4765951 4 0308031-04 Nonachlorobiphenyls 6.69 µg/Kg 0.174 µg/Kg9/12/2001 Comp of Sta 4 614689 4765951 4 0308031-04 Decachlorobiphenyl 0.130 J µg/Kg 0.0812 µg/Kg9/12/2001 Comp of Sta 4 614689 4765951 4 0308031-04 Total Homologs 170 µg/Kg 0.0812 µg/Kg9/12/2001 Comp of Sta 4 614689 4765951 4 0308031-04 Percent Lipids 2.6 % 0.1 %9/12/2001 Comp of Sta 4 614689 4765951 4 0308031-04 Percent Moisture 70.9 % 0.1 %9/6/2001 Comp of Sta 5 615971 4768359 5 0308031-05 Cl2-BZ#8 0.139 U µg/Kg 0.139 µg/Kg9/6/2001 Comp of Sta 5 615971 4768359 5 0308031-05 Cl3-BZ#18 0.309 U µg/Kg 0.309 µg/Kg9/6/2001 Comp of Sta 5 615971 4768359 5 0308031-05 Cl3-BZ#31/#28 7.44 J µg/Kg 2.23 µg/Kg9/6/2001 Comp of Sta 5 615971 4768359 5 0308031-05 Cl4-BZ#44 1.68 µg/Kg 0.212 µg/Kg9/6/2001 Comp of Sta 5 615971 4768359 5 0308031-05 Cl4-BZ#45 0.283 U µg/Kg 0.283 µg/Kg9/6/2001 Comp of Sta 5 615971 4768359 5 0308031-05 Cl4-BZ#47 6.68 µg/Kg 0.359 µg/Kg9/6/2001 Comp of Sta 5 615971 4768359 5 0308031-05 Cl4-BZ#49 2.39 µg/Kg 0.176 µg/Kg9/6/2001 Comp of Sta 5 615971 4768359 5 0308031-05 Cl4-BZ#52 4.27 µg/Kg 0.201 µg/Kg9/6/2001 Comp of Sta 5 615971 4768359 5 0308031-05 Cl4-BZ#56 3.81 µg/Kg 0.105 µg/Kg9/6/2001 Comp of Sta 5 615971 4768359 5 0308031-05 Cl4-BZ#66 7.23 µg/Kg 0.141 µg/Kg9/6/2001 Comp of Sta 5 615971 4768359 5 0308031-05 Cl4-BZ#70 2.52 µg/Kg 0.123 µg/Kg9/6/2001 Comp of Sta 5 615971 4768359 5 0308031-05 Cl4-BZ#74 7.53 µg/Kg 0.217 µg/Kg9/6/2001 Comp of Sta 5 615971 4768359 5 0308031-05 Cl4-BZ#77 0.194 U µg/Kg 0.194 µg/Kg9/6/2001 Comp of Sta 5 615971 4768359 5 0308031-05 Cl4-BZ#81 0.192 U µg/Kg 0.192 µg/Kg9/6/2001 Comp of Sta 5 615971 4768359 5 0308031-05 Cl5-BZ#87 3.16 µg/Kg 0.0857 µg/Kg9/6/2001 Comp of Sta 5 615971 4768359 5 0308031-05 Cl5-BZ#95 1.12 µg/Kg 0.0663 µg/Kg9/6/2001 Comp of Sta 5 615971 4768359 5 0308031-05 Cl5-BZ#99 11.4 µg/Kg 0.0453 µg/Kg9/6/2001 Comp of Sta 5 615971 4768359 5 0308031-05 Cl5-BZ#101 2.90 µg/Kg 0.129 µg/Kg9/6/2001 Comp of Sta 5 615971 4768359 5 0308031-05 Cl5-BZ#105 7.33 µg/Kg 0.0631 µg/Kg9/6/2001 Comp of Sta 5 615971 4768359 5 0308031-05 Cl5-BZ#110 1.88 µg/Kg 0.123 µg/Kg9/6/2001 Comp of Sta 5 615971 4768359 5 0308031-05 Cl5-BZ#114 0.469 µg/Kg 0.0566 µg/Kg9/6/2001 Comp of Sta 5 615971 4768359 5 0308031-05 Cl5-BZ#118 14.0 µg/Kg 0.133 µg/Kg9/6/2001 Comp of Sta 5 615971 4768359 5 0308031-05 Cl5-BZ#123 0.112 U µg/Kg 0.112 µg/Kg9/6/2001 Comp of Sta 5 615971 4768359 5 0308031-05 Cl5-BZ#126 0.0987 U µg/Kg 0.0987 µg/Kg9/6/2001 Comp of Sta 5 615971 4768359 5 0308031-05 Cl6-BZ#128 0.817 µg/Kg 0.0890 µg/Kg9/6/2001 Comp of Sta 5 615971 4768359 5 0308031-05 Cl6-BZ#138 15.6 µg/Kg 0.128 µg/Kg9/6/2001 Comp of Sta 5 615971 4768359 5 0308031-05 Cl6-BZ#146 1.67 µg/Kg 0.0809 µg/Kg9/6/2001 Comp of Sta 5 615971 4768359 5 0308031-05 Cl6-BZ#149 1.34 µg/Kg 0.104 µg/Kg9/6/2001 Comp of Sta 5 615971 4768359 5 0308031-05 Cl6-BZ#151 0.388 J µg/Kg 0.171 µg/Kg9/6/2001 Comp of Sta 5 615971 4768359 5 0308031-05 Cl6-BZ#153 14.2 µg/Kg 0.147 µg/Kg



Extracted 7/30/04







9/6/2001 Comp of Sta 5 615971 4768359 5 0308031-05 Cl6-BZ#156 2.18 µg/Kg 0.105 µg/Kg9/6/2001 Comp of Sta 5 615971 4768359 5 0308031-05 Cl6-BZ#157 0.364 J µg/Kg 0.0825 µg/Kg9/6/2001 Comp of Sta 5 615971 4768359 5 0308031-05 Cl6-BZ#158 0.332 J µg/Kg 0.0696 µg/Kg9/6/2001 Comp of Sta 5 615971 4768359 5 0308031-05 Cl6-BZ#167 0.356 J µg/Kg 0.0890 µg/Kg9/6/2001 Comp of Sta 5 615971 4768359 5 0308031-05 Cl6-BZ#169 0.286 U µg/Kg 0.286 µg/Kg9/6/2001 Comp of Sta 5 615971 4768359 5 0308031-05 Cl7-BZ#170 3.24 µg/Kg 0.333 µg/Kg9/6/2001 Comp of Sta 5 615971 4768359 5 0308031-05 Cl7-BZ#174 0.113 J µg/Kg 0.0679 µg/Kg9/6/2001 Comp of Sta 5 615971 4768359 5 0308031-05 Cl7-BZ#177 0.324 J µg/Kg 0.0955 µg/Kg9/6/2001 Comp of Sta 5 615971 4768359 5 0308031-05 Cl7-BZ#180 5.09 µg/Kg 0.142 µg/Kg9/6/2001 Comp of Sta 5 615971 4768359 5 0308031-05 Cl7-BZ#183 0.510 µg/Kg 0.0647 µg/Kg9/6/2001 Comp of Sta 5 615971 4768359 5 0308031-05 Cl7-BZ#187 5.77 µg/Kg 0.0712 µg/Kg9/6/2001 Comp of Sta 5 615971 4768359 5 0308031-05 Cl7-BZ#189 0.128 U µg/Kg 0.128 µg/Kg9/6/2001 Comp of Sta 5 615971 4768359 5 0308031-05 Cl8-BZ#194 1.48 µg/Kg 0.149 µg/Kg9/6/2001 Comp of Sta 5 615971 4768359 5 0308031-05 Cl8-BZ#195 0.421 J µg/Kg 0.147 µg/Kg9/6/2001 Comp of Sta 5 615971 4768359 5 0308031-05 Cl8-BZ#201 2.79 µg/Kg 0.129 µg/Kg9/6/2001 Comp of Sta 5 615971 4768359 5 0308031-05 Cl9-BZ#206 1.81 µg/Kg 0.173 µg/Kg9/6/2001 Comp of Sta 5 615971 4768359 5 0308031-05 Cl10-BZ#209 0.251 J µg/Kg 0.0809 µg/Kg9/6/2001 Comp of Sta 5 615971 4768359 5 0308031-05 Monochlorobiphenyls 4.76 U µg/Kg 4.76 µg/Kg9/6/2001 Comp of Sta 5 615971 4768359 5 0308031-05 Dichlorobiphenyls 0.139 U µg/Kg 0.139 µg/Kg9/6/2001 Comp of Sta 5 615971 4768359 5 0308031-05 Trichlorobiphenyls 6.79 µg/Kg 0.477 µg/Kg9/6/2001 Comp of Sta 5 615971 4768359 5 0308031-05 Tetrachlorobiphenyls 46.9 µg/Kg 0.0744 µg/Kg9/6/2001 Comp of Sta 5 615971 4768359 5 0308031-05 Pentachlorobiphenyls 69.2 µg/Kg 0.0857 µg/Kg9/6/2001 Comp of Sta 5 615971 4768359 5 0308031-05 Hexachlorobiphenyls 43.2 µg/Kg 0.136 µg/Kg9/6/2001 Comp of Sta 5 615971 4768359 5 0308031-05 Heptachlorobiphenyls 14.6 µg/Kg 0.0744 µg/Kg9/6/2001 Comp of Sta 5 615971 4768359 5 0308031-05 Octachlorobiphenyls 5.36 µg/Kg 0.0679 µg/Kg9/6/2001 Comp of Sta 5 615971 4768359 5 0308031-05 Nonachlorobiphenyls 8.15 µg/Kg 0.173 µg/Kg9/6/2001 Comp of Sta 5 615971 4768359 5 0308031-05 Decachlorobiphenyl 0.251 J µg/Kg 0.0809 µg/Kg9/6/2001 Comp of Sta 5 615971 4768359 5 0308031-05 Total Homologs 194 µg/Kg 0.0809 µg/Kg9/6/2001 Comp of Sta 5 615971 4768359 5 0308031-05 Percent Lipids 2.6 % 0.1 %9/6/2001 Comp of Sta 5 615971 4768359 5 0308031-05 Percent Moisture 73.5 % 0.1 %9/9/2001 Comp of Sta 6 615670 4772192 6 0308031-06 Cl2-BZ#8 0.145 U µg/Kg 0.145 µg/Kg9/9/2001 Comp of Sta 6 615670 4772192 6 0308031-06 Cl3-BZ#18 0.322 U µg/Kg 0.322 µg/Kg9/9/2001 Comp of Sta 6 615670 4772192 6 0308031-06 Cl3-BZ#31/#28 6.92 J µg/Kg 2.32 µg/Kg9/9/2001 Comp of Sta 6 615670 4772192 6 0308031-06 Cl4-BZ#44 0.886 J µg/Kg 0.221 µg/Kg9/9/2001 Comp of Sta 6 615670 4772192 6 0308031-06 Cl4-BZ#45 0.295 U µg/Kg 0.295 µg/Kg



Extracted 7/30/04







9/9/2001 Comp of Sta 6 615670 4772192 6 0308031-06 Cl4-BZ#47 7.21 µg/Kg 0.375 µg/Kg9/9/2001 Comp of Sta 6 615670 4772192 6 0308031-06 Cl4-BZ#49 2.09 µg/Kg 0.184 µg/Kg9/9/2001 Comp of Sta 6 615670 4772192 6 0308031-06 Cl4-BZ#52 3.92 µg/Kg 0.209 µg/Kg9/9/2001 Comp of Sta 6 615670 4772192 6 0308031-06 Cl4-BZ#56 3.91 µg/Kg 0.110 µg/Kg9/9/2001 Comp of Sta 6 615670 4772192 6 0308031-06 Cl4-BZ#66 5.72 µg/Kg 0.147 µg/Kg9/9/2001 Comp of Sta 6 615670 4772192 6 0308031-06 Cl4-BZ#70 1.39 µg/Kg 0.128 µg/Kg9/9/2001 Comp of Sta 6 615670 4772192 6 0308031-06 Cl4-BZ#74 8.18 µg/Kg 0.226 µg/Kg9/9/2001 Comp of Sta 6 615670 4772192 6 0308031-06 Cl4-BZ#77 0.203 U µg/Kg 0.203 µg/Kg9/9/2001 Comp of Sta 6 615670 4772192 6 0308031-06 Cl4-BZ#81 0.201 U µg/Kg 0.201 µg/Kg9/9/2001 Comp of Sta 6 615670 4772192 6 0308031-06 Cl5-BZ#87 6.98 µg/Kg 0.0894 µg/Kg9/9/2001 Comp of Sta 6 615670 4772192 6 0308031-06 Cl5-BZ#95 0.675 µg/Kg 0.0692 µg/Kg9/9/2001 Comp of Sta 6 615670 4772192 6 0308031-06 Cl5-BZ#99 30.6 µg/Kg 0.0473 µg/Kg9/9/2001 Comp of Sta 6 615670 4772192 6 0308031-06 Cl5-BZ#101 5.07 µg/Kg 0.135 µg/Kg9/9/2001 Comp of Sta 6 615670 4772192 6 0308031-06 Cl5-BZ#105 15.8 µg/Kg 0.0658 µg/Kg9/9/2001 Comp of Sta 6 615670 4772192 6 0308031-06 Cl5-BZ#110 1.43 µg/Kg 0.128 µg/Kg9/9/2001 Comp of Sta 6 615670 4772192 6 0308031-06 Cl5-BZ#114 1.37 µg/Kg 0.0591 µg/Kg9/9/2001 Comp of Sta 6 615670 4772192 6 0308031-06 Cl5-BZ#118 43.8 µg/Kg 0.138 µg/Kg9/9/2001 Comp of Sta 6 615670 4772192 6 0308031-06 Cl5-BZ#123 0.116 U µg/Kg 0.116 µg/Kg9/9/2001 Comp of Sta 6 615670 4772192 6 0308031-06 Cl5-BZ#126 0.103 U µg/Kg 0.103 µg/Kg9/9/2001 Comp of Sta 6 615670 4772192 6 0308031-06 Cl6-BZ#128 2.70 µg/Kg 0.0928 µg/Kg9/9/2001 Comp of Sta 6 615670 4772192 6 0308031-06 Cl6-BZ#138 53.7 µg/Kg 0.133 µg/Kg9/9/2001 Comp of Sta 6 615670 4772192 6 0308031-06 Cl6-BZ#146 8.48 µg/Kg 0.0844 µg/Kg9/9/2001 Comp of Sta 6 615670 4772192 6 0308031-06 Cl6-BZ#149 2.02 µg/Kg 0.108 µg/Kg9/9/2001 Comp of Sta 6 615670 4772192 6 0308031-06 Cl6-BZ#151 0.304 J µg/Kg 0.179 µg/Kg9/9/2001 Comp of Sta 6 615670 4772192 6 0308031-06 Cl6-BZ#153 73.1 µg/Kg 0.154 µg/Kg9/9/2001 Comp of Sta 6 615670 4772192 6 0308031-06 Cl6-BZ#156 9.48 µg/Kg 0.110 µg/Kg9/9/2001 Comp of Sta 6 615670 4772192 6 0308031-06 Cl6-BZ#157 1.61 µg/Kg 0.0861 µg/Kg9/9/2001 Comp of Sta 6 615670 4772192 6 0308031-06 Cl6-BZ#158 1.07 µg/Kg 0.0726 µg/Kg9/9/2001 Comp of Sta 6 615670 4772192 6 0308031-06 Cl6-BZ#167 1.60 µg/Kg 0.0928 µg/Kg9/9/2001 Comp of Sta 6 615670 4772192 6 0308031-06 Cl6-BZ#169 0.299 U µg/Kg 0.299 µg/Kg9/9/2001 Comp of Sta 6 615670 4772192 6 0308031-06 Cl7-BZ#170 9.21 µg/Kg 0.348 µg/Kg9/9/2001 Comp of Sta 6 615670 4772192 6 0308031-06 Cl7-BZ#174 0.135 J µg/Kg 0.0709 µg/Kg9/9/2001 Comp of Sta 6 615670 4772192 6 0308031-06 Cl7-BZ#177 1.14 µg/Kg 0.0996 µg/Kg9/9/2001 Comp of Sta 6 615670 4772192 6 0308031-06 Cl7-BZ#180 22.3 µg/Kg 0.148 µg/Kg9/9/2001 Comp of Sta 6 615670 4772192 6 0308031-06 Cl7-BZ#183 2.27 µg/Kg 0.0675 µg/Kg



Extracted 7/30/04







9/9/2001 Comp of Sta 6 615670 4772192 6 0308031-06 Cl7-BZ#187 18.0 µg/Kg 0.0743 µg/Kg9/9/2001 Comp of Sta 6 615670 4772192 6 0308031-06 Cl7-BZ#189 0.133 U µg/Kg 0.133 µg/Kg9/9/2001 Comp of Sta 6 615670 4772192 6 0308031-06 Cl8-BZ#194 4.44 µg/Kg 0.155 µg/Kg9/9/2001 Comp of Sta 6 615670 4772192 6 0308031-06 Cl8-BZ#195 0.683 J µg/Kg 0.154 µg/Kg9/9/2001 Comp of Sta 6 615670 4772192 6 0308031-06 Cl8-BZ#201 4.64 µg/Kg 0.135 µg/Kg9/9/2001 Comp of Sta 6 615670 4772192 6 0308031-06 Cl9-BZ#206 2.38 µg/Kg 0.181 µg/Kg9/9/2001 Comp of Sta 6 615670 4772192 6 0308031-06 Cl10-BZ#209 0.354 J µg/Kg 0.0844 µg/Kg9/9/2001 Comp of Sta 6 615670 4772192 6 0308031-06 Monochlorobiphenyls 4.96 U µg/Kg 4.96 µg/Kg9/9/2001 Comp of Sta 6 615670 4772192 6 0308031-06 Dichlorobiphenyls 0.145 U µg/Kg 0.145 µg/Kg9/9/2001 Comp of Sta 6 615670 4772192 6 0308031-06 Trichlorobiphenyls 7.12 µg/Kg 0.498 µg/Kg9/9/2001 Comp of Sta 6 615670 4772192 6 0308031-06 Tetrachlorobiphenyls 43.1 µg/Kg 0.0776 µg/Kg9/9/2001 Comp of Sta 6 615670 4772192 6 0308031-06 Pentachlorobiphenyls 172 µg/Kg 0.0894 µg/Kg9/9/2001 Comp of Sta 6 615670 4772192 6 0308031-06 Hexachlorobiphenyls 167 µg/Kg 0.142 µg/Kg9/9/2001 Comp of Sta 6 615670 4772192 6 0308031-06 Heptachlorobiphenyls 51.3 µg/Kg 0.0776 µg/Kg9/9/2001 Comp of Sta 6 615670 4772192 6 0308031-06 Octachlorobiphenyls 11.0 µg/Kg 0.0709 µg/Kg9/9/2001 Comp of Sta 6 615670 4772192 6 0308031-06 Nonachlorobiphenyls 7.89 µg/Kg 0.181 µg/Kg9/9/2001 Comp of Sta 6 615670 4772192 6 0308031-06 Decachlorobiphenyl 0.354 J µg/Kg 0.0844 µg/Kg9/9/2001 Comp of Sta 6 615670 4772192 6 0308031-06 Total Homologs 460 µg/Kg 0.0844 µg/Kg9/9/2001 Comp of Sta 6 615670 4772192 6 0308031-06 Percent Lipids 2.0 % 0.1 %9/9/2001 Comp of Sta 6 615670 4772192 6 0308031-06 Percent Moisture 76.1 % 0.1 %

9/15/2001 Comp of Sta 7 614704 4781156 7 0308031-07 Cl2-BZ#8 0.158 U µg/Kg 0.158 µg/Kg9/15/2001 Comp of Sta 7 614704 4781156 7 0308031-07 Cl3-BZ#18 0.351 U µg/Kg 0.351 µg/Kg9/15/2001 Comp of Sta 7 614704 4781156 7 0308031-07 Cl3-BZ#31/#28 6.31 J µg/Kg 2.53 µg/Kg9/15/2001 Comp of Sta 7 614704 4781156 7 0308031-07 Cl4-BZ#44 1.23 µg/Kg 0.241 µg/Kg9/15/2001 Comp of Sta 7 614704 4781156 7 0308031-07 Cl4-BZ#45 0.377 J µg/Kg 0.322 µg/Kg9/15/2001 Comp of Sta 7 614704 4781156 7 0308031-07 Cl4-BZ#47 3.00 µg/Kg 0.408 µg/Kg9/15/2001 Comp of Sta 7 614704 4781156 7 0308031-07 Cl4-BZ#49 1.75 µg/Kg 0.200 µg/Kg9/15/2001 Comp of Sta 7 614704 4781156 7 0308031-07 Cl4-BZ#52 2.53 µg/Kg 0.228 µg/Kg9/15/2001 Comp of Sta 7 614704 4781156 7 0308031-07 Cl4-BZ#56 1.93 µg/Kg 0.120 µg/Kg9/15/2001 Comp of Sta 7 614704 4781156 7 0308031-07 Cl4-BZ#66 2.59 µg/Kg 0.160 µg/Kg9/15/2001 Comp of Sta 7 614704 4781156 7 0308031-07 Cl4-BZ#70 1.20 µg/Kg 0.140 µg/Kg9/15/2001 Comp of Sta 7 614704 4781156 7 0308031-07 Cl4-BZ#74 4.38 µg/Kg 0.247 µg/Kg9/15/2001 Comp of Sta 7 614704 4781156 7 0308031-07 Cl4-BZ#77 0.221 U µg/Kg 0.221 µg/Kg9/15/2001 Comp of Sta 7 614704 4781156 7 0308031-07 Cl4-BZ#81 0.219 U µg/Kg 0.219 µg/Kg9/15/2001 Comp of Sta 7 614704 4781156 7 0308031-07 Cl5-BZ#87 2.13 µg/Kg 0.0975 µg/Kg



Extracted 7/30/04







9/15/2001 Comp of Sta 7 614704 4781156 7 0308031-07 Cl5-BZ#95 0.506 µg/Kg 0.0754 µg/Kg9/15/2001 Comp of Sta 7 614704 4781156 7 0308031-07 Cl5-BZ#99 8.30 µg/Kg 0.0515 µg/Kg9/15/2001 Comp of Sta 7 614704 4781156 7 0308031-07 Cl5-BZ#101 1.29 µg/Kg 0.147 µg/Kg9/15/2001 Comp of Sta 7 614704 4781156 7 0308031-07 Cl5-BZ#105 3.94 µg/Kg 0.0717 µg/Kg9/15/2001 Comp of Sta 7 614704 4781156 7 0308031-07 Cl5-BZ#110 0.368 J µg/Kg 0.140 µg/Kg9/15/2001 Comp of Sta 7 614704 4781156 7 0308031-07 Cl5-BZ#114 0.350 µg/Kg 0.0644 µg/Kg9/15/2001 Comp of Sta 7 614704 4781156 7 0308031-07 Cl5-BZ#118 11.3 µg/Kg 0.151 µg/Kg9/15/2001 Comp of Sta 7 614704 4781156 7 0308031-07 Cl5-BZ#123 0.127 U µg/Kg 0.127 µg/Kg9/15/2001 Comp of Sta 7 614704 4781156 7 0308031-07 Cl5-BZ#126 0.112 U µg/Kg 0.112 µg/Kg9/15/2001 Comp of Sta 7 614704 4781156 7 0308031-07 Cl6-BZ#128 0.405 J µg/Kg 0.101 µg/Kg9/15/2001 Comp of Sta 7 614704 4781156 7 0308031-07 Cl6-BZ#138 16.4 µg/Kg 0.145 µg/Kg9/15/2001 Comp of Sta 7 614704 4781156 7 0308031-07 Cl6-BZ#146 2.15 µg/Kg 0.0920 µg/Kg9/15/2001 Comp of Sta 7 614704 4781156 7 0308031-07 Cl6-BZ#149 0.303 J µg/Kg 0.118 µg/Kg9/15/2001 Comp of Sta 7 614704 4781156 7 0308031-07 Cl6-BZ#151 0.195 U µg/Kg 0.195 µg/Kg9/15/2001 Comp of Sta 7 614704 4781156 7 0308031-07 Cl6-BZ#153 28.6 µg/Kg 0.167 µg/Kg9/15/2001 Comp of Sta 7 614704 4781156 7 0308031-07 Cl6-BZ#156 3.78 µg/Kg 0.120 µg/Kg9/15/2001 Comp of Sta 7 614704 4781156 7 0308031-07 Cl6-BZ#157 0.598 µg/Kg 0.0938 µg/Kg9/15/2001 Comp of Sta 7 614704 4781156 7 0308031-07 Cl6-BZ#158 0.248 J µg/Kg 0.0791 µg/Kg9/15/2001 Comp of Sta 7 614704 4781156 7 0308031-07 Cl6-BZ#167 0.396 J µg/Kg 0.101 µg/Kg9/15/2001 Comp of Sta 7 614704 4781156 7 0308031-07 Cl6-BZ#169 0.326 U µg/Kg 0.326 µg/Kg9/15/2001 Comp of Sta 7 614704 4781156 7 0308031-07 Cl7-BZ#170 4.11 µg/Kg 0.379 µg/Kg9/15/2001 Comp of Sta 7 614704 4781156 7 0308031-07 Cl7-BZ#174 0.0773 U µg/Kg 0.0773 µg/Kg9/15/2001 Comp of Sta 7 614704 4781156 7 0308031-07 Cl7-BZ#177 0.285 J µg/Kg 0.108 µg/Kg9/15/2001 Comp of Sta 7 614704 4781156 7 0308031-07 Cl7-BZ#180 8.75 µg/Kg 0.162 µg/Kg9/15/2001 Comp of Sta 7 614704 4781156 7 0308031-07 Cl7-BZ#183 0.451 µg/Kg 0.0736 µg/Kg9/15/2001 Comp of Sta 7 614704 4781156 7 0308031-07 Cl7-BZ#187 5.01 µg/Kg 0.0809 µg/Kg9/15/2001 Comp of Sta 7 614704 4781156 7 0308031-07 Cl7-BZ#189 0.145 U µg/Kg 0.145 µg/Kg9/15/2001 Comp of Sta 7 614704 4781156 7 0308031-07 Cl8-BZ#194 2.07 µg/Kg 0.169 µg/Kg9/15/2001 Comp of Sta 7 614704 4781156 7 0308031-07 Cl8-BZ#195 0.248 J µg/Kg 0.167 µg/Kg9/15/2001 Comp of Sta 7 614704 4781156 7 0308031-07 Cl8-BZ#201 2.19 µg/Kg 0.147 µg/Kg9/15/2001 Comp of Sta 7 614704 4781156 7 0308031-07 Cl9-BZ#206 1.00 µg/Kg 0.197 µg/Kg9/15/2001 Comp of Sta 7 614704 4781156 7 0308031-07 Cl10-BZ#209 0.166 J µg/Kg 0.0920 µg/Kg9/15/2001 Comp of Sta 7 614704 4781156 7 0308031-07 Monochlorobiphenyls 5.41 U µg/Kg 5.41 µg/Kg9/15/2001 Comp of Sta 7 614704 4781156 7 0308031-07 Dichlorobiphenyls 0.158 U µg/Kg 0.158 µg/Kg9/15/2001 Comp of Sta 7 614704 4781156 7 0308031-07 Trichlorobiphenyls 4.91 µg/Kg 0.543 µg/Kg



Extracted 7/30/04







9/15/2001 Comp of Sta 7 614704 4781156 7 0308031-07 Tetrachlorobiphenyls 27.6 µg/Kg 0.0846 µg/Kg9/15/2001 Comp of Sta 7 614704 4781156 7 0308031-07 Pentachlorobiphenyls 48.8 µg/Kg 0.0975 µg/Kg9/15/2001 Comp of Sta 7 614704 4781156 7 0308031-07 Hexachlorobiphenyls 56.8 µg/Kg 0.154 µg/Kg9/15/2001 Comp of Sta 7 614704 4781156 7 0308031-07 Heptachlorobiphenyls 17.4 µg/Kg 0.0846 µg/Kg9/15/2001 Comp of Sta 7 614704 4781156 7 0308031-07 Octachlorobiphenyls 4.86 µg/Kg 0.0773 µg/Kg9/15/2001 Comp of Sta 7 614704 4781156 7 0308031-07 Nonachlorobiphenyls 5.82 µg/Kg 0.197 µg/Kg9/15/2001 Comp of Sta 7 614704 4781156 7 0308031-07 Decachlorobiphenyl 0.166 J µg/Kg 0.0920 µg/Kg9/15/2001 Comp of Sta 7 614704 4781156 7 0308031-07 Total Homologs 166 µg/Kg 0.0920 µg/Kg9/15/2001 Comp of Sta 7 614704 4781156 7 0308031-07 Percent Lipids 2.4 % 0.1 %9/15/2001 Comp of Sta 7 614704 4781156 7 0308031-07 Percent Moisture 70.5 % 0.1 %9/14/2001 Comp of Sta 8 614814 4783340 8 0308031-08 Cl2-BZ#8 0.133 U µg/Kg 0.133 µg/Kg9/14/2001 Comp of Sta 8 614814 4783340 8 0308031-08 Cl3-BZ#18 0.295 U µg/Kg 0.295 µg/Kg9/14/2001 Comp of Sta 8 614814 4783340 8 0308031-08 Cl3-BZ#31/#28 10.8 µg/Kg 2.12 µg/Kg9/14/2001 Comp of Sta 8 614814 4783340 8 0308031-08 Cl4-BZ#44 2.32 µg/Kg 0.202 µg/Kg9/14/2001 Comp of Sta 8 614814 4783340 8 0308031-08 Cl4-BZ#45 0.386 J µg/Kg 0.270 µg/Kg9/14/2001 Comp of Sta 8 614814 4783340 8 0308031-08 Cl4-BZ#47 9.27 µg/Kg 0.342 µg/Kg9/14/2001 Comp of Sta 8 614814 4783340 8 0308031-08 Cl4-BZ#49 3.93 µg/Kg 0.168 µg/Kg9/14/2001 Comp of Sta 8 614814 4783340 8 0308031-08 Cl4-BZ#52 5.58 µg/Kg 0.191 µg/Kg9/14/2001 Comp of Sta 8 614814 4783340 8 0308031-08 Cl4-BZ#56 6.30 µg/Kg 0.100 µg/Kg9/14/2001 Comp of Sta 8 614814 4783340 8 0308031-08 Cl4-BZ#66 8.69 µg/Kg 0.134 µg/Kg9/14/2001 Comp of Sta 8 614814 4783340 8 0308031-08 Cl4-BZ#70 4.06 µg/Kg 0.117 µg/Kg9/14/2001 Comp of Sta 8 614814 4783340 8 0308031-08 Cl4-BZ#74 11.1 µg/Kg 0.207 µg/Kg9/14/2001 Comp of Sta 8 614814 4783340 8 0308031-08 Cl4-BZ#77 0.185 U µg/Kg 0.185 µg/Kg9/14/2001 Comp of Sta 8 614814 4783340 8 0308031-08 Cl4-BZ#81 0.184 U µg/Kg 0.184 µg/Kg9/14/2001 Comp of Sta 8 614814 4783340 8 0308031-08 Cl5-BZ#87 4.31 µg/Kg 0.0817 µg/Kg9/14/2001 Comp of Sta 8 614814 4783340 8 0308031-08 Cl5-BZ#95 1.26 µg/Kg 0.0632 µg/Kg9/14/2001 Comp of Sta 8 614814 4783340 8 0308031-08 Cl5-BZ#99 11.1 µg/Kg 0.0432 µg/Kg9/14/2001 Comp of Sta 8 614814 4783340 8 0308031-08 Cl5-BZ#101 3.69 µg/Kg 0.123 µg/Kg9/14/2001 Comp of Sta 8 614814 4783340 8 0308031-08 Cl5-BZ#105 7.34 µg/Kg 0.0602 µg/Kg9/14/2001 Comp of Sta 8 614814 4783340 8 0308031-08 Cl5-BZ#110 2.13 µg/Kg 0.117 µg/Kg9/14/2001 Comp of Sta 8 614814 4783340 8 0308031-08 Cl5-BZ#114 0.601 µg/Kg 0.0540 µg/Kg9/14/2001 Comp of Sta 8 614814 4783340 8 0308031-08 Cl5-BZ#118 14.5 µg/Kg 0.126 µg/Kg9/14/2001 Comp of Sta 8 614814 4783340 8 0308031-08 Cl5-BZ#123 0.106 U µg/Kg 0.106 µg/Kg9/14/2001 Comp of Sta 8 614814 4783340 8 0308031-08 Cl5-BZ#126 0.0941 U µg/Kg 0.0941 µg/Kg9/14/2001 Comp of Sta 8 614814 4783340 8 0308031-08 Cl6-BZ#128 0.779 µg/Kg 0.0848 µg/Kg



Extracted 7/30/04







9/14/2001 Comp of Sta 8 614814 4783340 8 0308031-08 Cl6-BZ#138 13.1 µg/Kg 0.122 µg/Kg9/14/2001 Comp of Sta 8 614814 4783340 8 0308031-08 Cl6-BZ#146 1.61 µg/Kg 0.0771 µg/Kg9/14/2001 Comp of Sta 8 614814 4783340 8 0308031-08 Cl6-BZ#149 0.941 µg/Kg 0.0987 µg/Kg9/14/2001 Comp of Sta 8 614814 4783340 8 0308031-08 Cl6-BZ#151 0.216 J µg/Kg 0.163 µg/Kg9/14/2001 Comp of Sta 8 614814 4783340 8 0308031-08 Cl6-BZ#153 12.7 µg/Kg 0.140 µg/Kg9/14/2001 Comp of Sta 8 614814 4783340 8 0308031-08 Cl6-BZ#156 1.90 µg/Kg 0.100 µg/Kg9/14/2001 Comp of Sta 8 614814 4783340 8 0308031-08 Cl6-BZ#157 0.324 J µg/Kg 0.0787 µg/Kg9/14/2001 Comp of Sta 8 614814 4783340 8 0308031-08 Cl6-BZ#158 0.347 µg/Kg 0.0663 µg/Kg9/14/2001 Comp of Sta 8 614814 4783340 8 0308031-08 Cl6-BZ#167 0.401 J µg/Kg 0.0848 µg/Kg9/14/2001 Comp of Sta 8 614814 4783340 8 0308031-08 Cl6-BZ#169 0.273 U µg/Kg 0.273 µg/Kg9/14/2001 Comp of Sta 8 614814 4783340 8 0308031-08 Cl7-BZ#170 2.69 µg/Kg 0.318 µg/Kg9/14/2001 Comp of Sta 8 614814 4783340 8 0308031-08 Cl7-BZ#174 0.0648 U µg/Kg 0.0648 µg/Kg9/14/2001 Comp of Sta 8 614814 4783340 8 0308031-08 Cl7-BZ#177 0.447 J µg/Kg 0.0910 µg/Kg9/14/2001 Comp of Sta 8 614814 4783340 8 0308031-08 Cl7-BZ#180 5.44 µg/Kg 0.136 µg/Kg9/14/2001 Comp of Sta 8 614814 4783340 8 0308031-08 Cl7-BZ#183 0.463 µg/Kg 0.0617 µg/Kg9/14/2001 Comp of Sta 8 614814 4783340 8 0308031-08 Cl7-BZ#187 4.70 µg/Kg 0.0679 µg/Kg9/14/2001 Comp of Sta 8 614814 4783340 8 0308031-08 Cl7-BZ#189 0.122 U µg/Kg 0.122 µg/Kg9/14/2001 Comp of Sta 8 614814 4783340 8 0308031-08 Cl8-BZ#194 1.23 µg/Kg 0.142 µg/Kg9/14/2001 Comp of Sta 8 614814 4783340 8 0308031-08 Cl8-BZ#195 0.278 J µg/Kg 0.140 µg/Kg9/14/2001 Comp of Sta 8 614814 4783340 8 0308031-08 Cl8-BZ#201 1.70 µg/Kg 0.123 µg/Kg9/14/2001 Comp of Sta 8 614814 4783340 8 0308031-08 Cl9-BZ#206 0.918 µg/Kg 0.165 µg/Kg9/14/2001 Comp of Sta 8 614814 4783340 8 0308031-08 Cl10-BZ#209 0.185 J µg/Kg 0.0771 µg/Kg9/14/2001 Comp of Sta 8 614814 4783340 8 0308031-08 Monochlorobiphenyls 4.54 U µg/Kg 4.54 µg/Kg9/14/2001 Comp of Sta 8 614814 4783340 8 0308031-08 Dichlorobiphenyls 0.308 J µg/Kg 0.133 µg/Kg9/14/2001 Comp of Sta 8 614814 4783340 8 0308031-08 Trichlorobiphenyls 10.8 µg/Kg 0.455 µg/Kg9/14/2001 Comp of Sta 8 614814 4783340 8 0308031-08 Tetrachlorobiphenyls 67.1 µg/Kg 0.0710 µg/Kg9/14/2001 Comp of Sta 8 614814 4783340 8 0308031-08 Pentachlorobiphenyls 76.0 µg/Kg 0.0817 µg/Kg9/14/2001 Comp of Sta 8 614814 4783340 8 0308031-08 Hexachlorobiphenyls 37.4 µg/Kg 0.130 µg/Kg9/14/2001 Comp of Sta 8 614814 4783340 8 0308031-08 Heptachlorobiphenyls 12.9 µg/Kg 0.0710 µg/Kg9/14/2001 Comp of Sta 8 614814 4783340 8 0308031-08 Octachlorobiphenyls 3.68 µg/Kg 0.0648 µg/Kg9/14/2001 Comp of Sta 8 614814 4783340 8 0308031-08 Nonachlorobiphenyls 5.41 µg/Kg 0.165 µg/Kg9/14/2001 Comp of Sta 8 614814 4783340 8 0308031-08 Decachlorobiphenyl 0.185 J µg/Kg 0.0771 µg/Kg9/14/2001 Comp of Sta 8 614814 4783340 8 0308031-08 Total Homologs 214 µg/Kg 0.0771 µg/Kg9/14/2001 Comp of Sta 8 614814 4783340 8 0308031-08 Percent Lipids 1.6 % 0.1 %9/14/2001 Comp of Sta 8 614814 4783340 8 0308031-08 Percent Moisture 69.0 % 0.1 %



Extracted 7/30/04







9/15/2001 Comp of Sta 10 614100 4788175 10 0308031-09 Cl2-BZ#8 0.128 U µg/Kg 0.128 µg/Kg9/15/2001 Comp of Sta 10 614100 4788175 10 0308031-09 Cl3-BZ#18 0.285 U µg/Kg 0.285 µg/Kg9/15/2001 Comp of Sta 10 614100 4788175 10 0308031-09 Cl3-BZ#31/#28 4.62 J µg/Kg 2.05 µg/Kg9/15/2001 Comp of Sta 10 614100 4788175 10 0308031-09 Cl4-BZ#44 0.195 U µg/Kg 0.195 µg/Kg9/15/2001 Comp of Sta 10 614100 4788175 10 0308031-09 Cl4-BZ#45 0.261 U µg/Kg 0.261 µg/Kg9/15/2001 Comp of Sta 10 614100 4788175 10 0308031-09 Cl4-BZ#47 1.26 J µg/Kg 0.331 µg/Kg9/15/2001 Comp of Sta 10 614100 4788175 10 0308031-09 Cl4-BZ#49 0.171 J µg/Kg 0.162 µg/Kg9/15/2001 Comp of Sta 10 614100 4788175 10 0308031-09 Cl4-BZ#52 0.350 J µg/Kg 0.185 µg/Kg9/15/2001 Comp of Sta 10 614100 4788175 10 0308031-09 Cl4-BZ#56 1.01 µg/Kg 0.0969 µg/Kg9/15/2001 Comp of Sta 10 614100 4788175 10 0308031-09 Cl4-BZ#66 1.13 µg/Kg 0.130 µg/Kg9/15/2001 Comp of Sta 10 614100 4788175 10 0308031-09 Cl4-BZ#70 0.276 J µg/Kg 0.113 µg/Kg9/15/2001 Comp of Sta 10 614100 4788175 10 0308031-09 Cl4-BZ#74 1.39 µg/Kg 0.200 µg/Kg9/15/2001 Comp of Sta 10 614100 4788175 10 0308031-09 Cl4-BZ#77 0.179 U µg/Kg 0.179 µg/Kg9/15/2001 Comp of Sta 10 614100 4788175 10 0308031-09 Cl4-BZ#81 0.177 U µg/Kg 0.177 µg/Kg9/15/2001 Comp of Sta 10 614100 4788175 10 0308031-09 Cl5-BZ#87 0.522 µg/Kg 0.0790 µg/Kg9/15/2001 Comp of Sta 10 614100 4788175 10 0308031-09 Cl5-BZ#95 0.0611 U µg/Kg 0.0611 µg/Kg9/15/2001 Comp of Sta 10 614100 4788175 10 0308031-09 Cl5-BZ#99 2.78 µg/Kg 0.0418 µg/Kg9/15/2001 Comp of Sta 10 614100 4788175 10 0308031-09 Cl5-BZ#101 0.425 J µg/Kg 0.119 µg/Kg9/15/2001 Comp of Sta 10 614100 4788175 10 0308031-09 Cl5-BZ#105 1.88 µg/Kg 0.0582 µg/Kg9/15/2001 Comp of Sta 10 614100 4788175 10 0308031-09 Cl5-BZ#110 0.113 U µg/Kg 0.113 µg/Kg9/15/2001 Comp of Sta 10 614100 4788175 10 0308031-09 Cl5-BZ#114 0.127 J µg/Kg 0.0522 µg/Kg9/15/2001 Comp of Sta 10 614100 4788175 10 0308031-09 Cl5-BZ#118 3.94 µg/Kg 0.122 µg/Kg9/15/2001 Comp of Sta 10 614100 4788175 10 0308031-09 Cl5-BZ#123 0.103 U µg/Kg 0.103 µg/Kg9/15/2001 Comp of Sta 10 614100 4788175 10 0308031-09 Cl5-BZ#126 0.0910 U µg/Kg 0.0910 µg/Kg9/15/2001 Comp of Sta 10 614100 4788175 10 0308031-09 Cl6-BZ#128 0.328 J µg/Kg 0.0820 µg/Kg9/15/2001 Comp of Sta 10 614100 4788175 10 0308031-09 Cl6-BZ#138 7.81 µg/Kg 0.118 µg/Kg9/15/2001 Comp of Sta 10 614100 4788175 10 0308031-09 Cl6-BZ#146 0.887 µg/Kg 0.0746 µg/Kg9/15/2001 Comp of Sta 10 614100 4788175 10 0308031-09 Cl6-BZ#149 0.194 J µg/Kg 0.0954 µg/Kg9/15/2001 Comp of Sta 10 614100 4788175 10 0308031-09 Cl6-BZ#151 0.158 U µg/Kg 0.158 µg/Kg9/15/2001 Comp of Sta 10 614100 4788175 10 0308031-09 Cl6-BZ#153 8.31 µg/Kg 0.136 µg/Kg9/15/2001 Comp of Sta 10 614100 4788175 10 0308031-09 Cl6-BZ#156 1.28 µg/Kg 0.0969 µg/Kg9/15/2001 Comp of Sta 10 614100 4788175 10 0308031-09 Cl6-BZ#157 0.246 J µg/Kg 0.0761 µg/Kg9/15/2001 Comp of Sta 10 614100 4788175 10 0308031-09 Cl6-BZ#158 0.194 J µg/Kg 0.0641 µg/Kg9/15/2001 Comp of Sta 10 614100 4788175 10 0308031-09 Cl6-BZ#167 0.194 J µg/Kg 0.0820 µg/Kg9/15/2001 Comp of Sta 10 614100 4788175 10 0308031-09 Cl6-BZ#169 0.264 U µg/Kg 0.264 µg/Kg



Extracted 7/30/04







9/15/2001 Comp of Sta 10 614100 4788175 10 0308031-09 Cl7-BZ#170 2.04 µg/Kg 0.307 µg/Kg9/15/2001 Comp of Sta 10 614100 4788175 10 0308031-09 Cl7-BZ#174 0.0626 U µg/Kg 0.0626 µg/Kg9/15/2001 Comp of Sta 10 614100 4788175 10 0308031-09 Cl7-BZ#177 0.201 J µg/Kg 0.0880 µg/Kg9/15/2001 Comp of Sta 10 614100 4788175 10 0308031-09 Cl7-BZ#180 3.71 µg/Kg 0.131 µg/Kg9/15/2001 Comp of Sta 10 614100 4788175 10 0308031-09 Cl7-BZ#183 0.298 µg/Kg 0.0596 µg/Kg9/15/2001 Comp of Sta 10 614100 4788175 10 0308031-09 Cl7-BZ#187 1.93 µg/Kg 0.0656 µg/Kg9/15/2001 Comp of Sta 10 614100 4788175 10 0308031-09 Cl7-BZ#189 0.118 U µg/Kg 0.118 µg/Kg9/15/2001 Comp of Sta 10 614100 4788175 10 0308031-09 Cl8-BZ#194 0.828 µg/Kg 0.137 µg/Kg9/15/2001 Comp of Sta 10 614100 4788175 10 0308031-09 Cl8-BZ#195 0.216 J µg/Kg 0.136 µg/Kg9/15/2001 Comp of Sta 10 614100 4788175 10 0308031-09 Cl8-BZ#201 1.12 µg/Kg 0.119 µg/Kg9/15/2001 Comp of Sta 10 614100 4788175 10 0308031-09 Cl9-BZ#206 0.552 J µg/Kg 0.160 µg/Kg9/15/2001 Comp of Sta 10 614100 4788175 10 0308031-09 Cl10-BZ#209 0.112 J µg/Kg 0.0746 µg/Kg9/15/2001 Comp of Sta 10 614100 4788175 10 0308031-09 Monochlorobiphenyls 4.38 U µg/Kg 4.38 µg/Kg9/15/2001 Comp of Sta 10 614100 4788175 10 0308031-09 Dichlorobiphenyls 0.128 U µg/Kg 0.128 µg/Kg9/15/2001 Comp of Sta 10 614100 4788175 10 0308031-09 Trichlorobiphenyls 4.21 µg/Kg 0.440 µg/Kg9/15/2001 Comp of Sta 10 614100 4788175 10 0308031-09 Tetrachlorobiphenyls 10.6 µg/Kg 0.0686 µg/Kg9/15/2001 Comp of Sta 10 614100 4788175 10 0308031-09 Pentachlorobiphenyls 17.3 µg/Kg 0.0790 µg/Kg9/15/2001 Comp of Sta 10 614100 4788175 10 0308031-09 Hexachlorobiphenyls 21.0 µg/Kg 0.125 µg/Kg9/15/2001 Comp of Sta 10 614100 4788175 10 0308031-09 Heptachlorobiphenyls 8.53 µg/Kg 0.0686 µg/Kg9/15/2001 Comp of Sta 10 614100 4788175 10 0308031-09 Octachlorobiphenyls 1.72 µg/Kg 0.0626 µg/Kg9/15/2001 Comp of Sta 10 614100 4788175 10 0308031-09 Nonachlorobiphenyls 4.26 µg/Kg 0.160 µg/Kg9/15/2001 Comp of Sta 10 614100 4788175 10 0308031-09 Decachlorobiphenyl 0.112 J µg/Kg 0.0746 µg/Kg9/15/2001 Comp of Sta 10 614100 4788175 10 0308031-09 Total Homologs 67.8 µg/Kg 0.0746 µg/Kg9/15/2001 Comp of Sta 10 614100 4788175 10 0308031-09 Percent Lipids 2.8 % 0.1 %9/15/2001 Comp of Sta 10 614100 4788175 10 0308031-09 Percent Moisture 70.5 % 0.1 %10/4/2001 Comp of Sta 11 614778 4791139 11 0308031-10 Cl2-BZ#8 0.145 U µg/Kg 0.145 µg/Kg10/4/2001 Comp of Sta 11 614778 4791139 11 0308031-10 Cl3-BZ#18 0.322 U µg/Kg 0.322 µg/Kg10/4/2001 Comp of Sta 11 614778 4791139 11 0308031-10 Cl3-BZ#31/#28 11.1 J µg/Kg 2.33 µg/Kg10/4/2001 Comp of Sta 11 614778 4791139 11 0308031-10 Cl4-BZ#44 0.946 J µg/Kg 0.221 µg/Kg10/4/2001 Comp of Sta 11 614778 4791139 11 0308031-10 Cl4-BZ#45 0.296 U µg/Kg 0.296 µg/Kg10/4/2001 Comp of Sta 11 614778 4791139 11 0308031-10 Cl4-BZ#47 14.8 µg/Kg 0.375 µg/Kg10/4/2001 Comp of Sta 11 614778 4791139 11 0308031-10 Cl4-BZ#49 1.73 µg/Kg 0.184 µg/Kg10/4/2001 Comp of Sta 11 614778 4791139 11 0308031-10 Cl4-BZ#52 5.17 µg/Kg 0.209 µg/Kg10/4/2001 Comp of Sta 11 614778 4791139 11 0308031-10 Cl4-BZ#56 5.28 µg/Kg 0.110 µg/Kg10/4/2001 Comp of Sta 11 614778 4791139 11 0308031-10 Cl4-BZ#66 7.87 µg/Kg 0.147 µg/Kg



Extracted 7/30/04







10/4/2001 Comp of Sta 11 614778 4791139 11 0308031-10 Cl4-BZ#70 1.33 µg/Kg 0.128 µg/Kg10/4/2001 Comp of Sta 11 614778 4791139 11 0308031-10 Cl4-BZ#74 12.3 µg/Kg 0.226 µg/Kg10/4/2001 Comp of Sta 11 614778 4791139 11 0308031-10 Cl4-BZ#77 0.203 U µg/Kg 0.203 µg/Kg10/4/2001 Comp of Sta 11 614778 4791139 11 0308031-10 Cl4-BZ#81 0.201 U µg/Kg 0.201 µg/Kg10/4/2001 Comp of Sta 11 614778 4791139 11 0308031-10 Cl5-BZ#87 6.83 µg/Kg 0.0895 µg/Kg10/4/2001 Comp of Sta 11 614778 4791139 11 0308031-10 Cl5-BZ#95 0.768 µg/Kg 0.0692 µg/Kg10/4/2001 Comp of Sta 11 614778 4791139 11 0308031-10 Cl5-BZ#99 58.6 µg/Kg 0.0473 µg/Kg10/4/2001 Comp of Sta 11 614778 4791139 11 0308031-10 Cl5-BZ#101 3.58 µg/Kg 0.135 µg/Kg10/4/2001 Comp of Sta 11 614778 4791139 11 0308031-10 Cl5-BZ#105 16.3 µg/Kg 0.0659 µg/Kg10/4/2001 Comp of Sta 11 614778 4791139 11 0308031-10 Cl5-BZ#110 0.929 µg/Kg 0.128 µg/Kg10/4/2001 Comp of Sta 11 614778 4791139 11 0308031-10 Cl5-BZ#114 0.937 µg/Kg 0.0591 µg/Kg10/4/2001 Comp of Sta 11 614778 4791139 11 0308031-10 Cl5-BZ#118 34.3 µg/Kg 0.139 µg/Kg10/4/2001 Comp of Sta 11 614778 4791139 11 0308031-10 Cl5-BZ#123 0.116 U µg/Kg 0.116 µg/Kg10/4/2001 Comp of Sta 11 614778 4791139 11 0308031-10 Cl5-BZ#126 0.103 U µg/Kg 0.103 µg/Kg10/4/2001 Comp of Sta 11 614778 4791139 11 0308031-10 Cl6-BZ#128 3.37 µg/Kg 0.0929 µg/Kg10/4/2001 Comp of Sta 11 614778 4791139 11 0308031-10 Cl6-BZ#138 93.6 µg/Kg 0.133 µg/Kg10/4/2001 Comp of Sta 11 614778 4791139 11 0308031-10 Cl6-BZ#146 8.72 µg/Kg 0.0844 µg/Kg10/4/2001 Comp of Sta 11 614778 4791139 11 0308031-10 Cl6-BZ#149 1.63 µg/Kg 0.108 µg/Kg10/4/2001 Comp of Sta 11 614778 4791139 11 0308031-10 Cl6-BZ#151 0.363 J µg/Kg 0.179 µg/Kg10/4/2001 Comp of Sta 11 614778 4791139 11 0308031-10 Cl6-BZ#153 145 µg/Kg 0.154 µg/Kg10/4/2001 Comp of Sta 11 614778 4791139 11 0308031-10 Cl6-BZ#156 11.8 µg/Kg 0.110 µg/Kg10/4/2001 Comp of Sta 11 614778 4791139 11 0308031-10 Cl6-BZ#157 2.15 µg/Kg 0.0861 µg/Kg10/4/2001 Comp of Sta 11 614778 4791139 11 0308031-10 Cl6-BZ#158 1.77 µg/Kg 0.0726 µg/Kg10/4/2001 Comp of Sta 11 614778 4791139 11 0308031-10 Cl6-BZ#167 0.971 µg/Kg 0.0929 µg/Kg10/4/2001 Comp of Sta 11 614778 4791139 11 0308031-10 Cl6-BZ#169 0.299 U µg/Kg 0.299 µg/Kg10/4/2001 Comp of Sta 11 614778 4791139 11 0308031-10 Cl7-BZ#170 14.0 µg/Kg 0.348 µg/Kg10/4/2001 Comp of Sta 11 614778 4791139 11 0308031-10 Cl7-BZ#174 0.0709 U µg/Kg 0.0709 µg/Kg10/4/2001 Comp of Sta 11 614778 4791139 11 0308031-10 Cl7-BZ#177 1.27 µg/Kg 0.0996 µg/Kg10/4/2001 Comp of Sta 11 614778 4791139 11 0308031-10 Cl7-BZ#180 28.9 µg/Kg 0.149 µg/Kg10/4/2001 Comp of Sta 11 614778 4791139 11 0308031-10 Cl7-BZ#183 2.13 µg/Kg 0.0675 µg/Kg10/4/2001 Comp of Sta 11 614778 4791139 11 0308031-10 Cl7-BZ#187 15.2 µg/Kg 0.0743 µg/Kg10/4/2001 Comp of Sta 11 614778 4791139 11 0308031-10 Cl7-BZ#189 0.133 U µg/Kg 0.133 µg/Kg10/4/2001 Comp of Sta 11 614778 4791139 11 0308031-10 Cl8-BZ#194 3.60 µg/Kg 0.155 µg/Kg10/4/2001 Comp of Sta 11 614778 4791139 11 0308031-10 Cl8-BZ#195 0.895 µg/Kg 0.154 µg/Kg10/4/2001 Comp of Sta 11 614778 4791139 11 0308031-10 Cl8-BZ#201 4.41 µg/Kg 0.135 µg/Kg



Extracted 7/30/04







10/4/2001 Comp of Sta 11 614778 4791139 11 0308031-10 Cl9-BZ#206 1.95 µg/Kg 0.181 µg/Kg10/4/2001 Comp of Sta 11 614778 4791139 11 0308031-10 Cl10-BZ#209 0.296 J µg/Kg 0.0844 µg/Kg10/4/2001 Comp of Sta 11 614778 4791139 11 0308031-10 Monochlorobiphenyls 4.96 U µg/Kg 4.96 µg/Kg10/4/2001 Comp of Sta 11 614778 4791139 11 0308031-10 Dichlorobiphenyls 0.145 U µg/Kg 0.145 µg/Kg10/4/2001 Comp of Sta 11 614778 4791139 11 0308031-10 Trichlorobiphenyls 8.67 µg/Kg 0.498 µg/Kg10/4/2001 Comp of Sta 11 614778 4791139 11 0308031-10 Tetrachlorobiphenyls 66.8 µg/Kg 0.0777 µg/Kg10/4/2001 Comp of Sta 11 614778 4791139 11 0308031-10 Pentachlorobiphenyls 197 µg/Kg 0.0895 µg/Kg10/4/2001 Comp of Sta 11 614778 4791139 11 0308031-10 Hexachlorobiphenyls 283 µg/Kg 0.142 µg/Kg10/4/2001 Comp of Sta 11 614778 4791139 11 0308031-10 Heptachlorobiphenyls 55.6 µg/Kg 0.0777 µg/Kg10/4/2001 Comp of Sta 11 614778 4791139 11 0308031-10 Octachlorobiphenyls 10.6 µg/Kg 0.0709 µg/Kg10/4/2001 Comp of Sta 11 614778 4791139 11 0308031-10 Nonachlorobiphenyls 7.02 µg/Kg 0.181 µg/Kg10/4/2001 Comp of Sta 11 614778 4791139 11 0308031-10 Decachlorobiphenyl 0.296 J µg/Kg 0.0844 µg/Kg10/4/2001 Comp of Sta 11 614778 4791139 11 0308031-10 Total Homologs 629 µg/Kg 0.0844 µg/Kg10/4/2001 Comp of Sta 11 614778 4791139 11 0308031-10 Percent Lipids 5.4 % 0.1 %10/4/2001 Comp of Sta 11 614778 4791139 11 0308031-10 Percent Moisture 69.2 % 0.1 %10/4/2001 Comp of Sta 12 (mouse 614851 4790327 12 0308031-11 Cl2-BZ#8 0.299 U µg/Kg 0.299 µg/Kg10/4/2001 Comp of Sta 12 (mouse 614851 4790327 12 0308031-11 Cl3-BZ#18 0.665 U µg/Kg 0.665 µg/Kg10/4/2001 Comp of Sta 12 (mouse 614851 4790327 12 0308031-11 Cl3-BZ#31/#28 24.6 µg/Kg 4.79 µg/Kg10/4/2001 Comp of Sta 12 (mouse 614851 4790327 12 0308031-11 Cl4-BZ#44 9.14 µg/Kg 0.456 µg/Kg10/4/2001 Comp of Sta 12 (mouse 614851 4790327 12 0308031-11 Cl4-BZ#45 0.609 U µg/Kg 0.609 µg/Kg10/4/2001 Comp of Sta 12 (mouse 614851 4790327 12 0308031-11 Cl4-BZ#47 62.4 µg/Kg 0.773 µg/Kg10/4/2001 Comp of Sta 12 (mouse 614851 4790327 12 0308031-11 Cl4-BZ#49 10.3 µg/Kg 0.379 µg/Kg10/4/2001 Comp of Sta 12 (mouse 614851 4790327 12 0308031-11 Cl4-BZ#52 23.0 µg/Kg 0.432 µg/Kg10/4/2001 Comp of Sta 12 (mouse 614851 4790327 12 0308031-11 Cl4-BZ#56 23.2 µg/Kg 0.226 µg/Kg10/4/2001 Comp of Sta 12 (mouse 614851 4790327 12 0308031-11 Cl4-BZ#66 35.0 µg/Kg 0.303 µg/Kg10/4/2001 Comp of Sta 12 (mouse 614851 4790327 12 0308031-11 Cl4-BZ#70 14.7 µg/Kg 0.264 µg/Kg10/4/2001 Comp of Sta 12 (mouse 614851 4790327 12 0308031-11 Cl4-BZ#74 60.7 µg/Kg 0.466 µg/Kg10/4/2001 Comp of Sta 12 (mouse 614851 4790327 12 0308031-11 Cl4-BZ#77 0.418 U µg/Kg 0.418 µg/Kg10/4/2001 Comp of Sta 12 (mouse 614851 4790327 12 0308031-11 Cl4-BZ#81 0.414 U µg/Kg 0.414 µg/Kg10/4/2001 Comp of Sta 12 (mouse 614851 4790327 12 0308031-11 Cl5-BZ#87 30.0 µg/Kg 0.184 µg/Kg10/4/2001 Comp of Sta 12 (mouse 614851 4790327 12 0308031-11 Cl5-BZ#95 5.93 µg/Kg 0.143 µg/Kg10/4/2001 Comp of Sta 12 (mouse 614851 4790327 12 0308031-11 Cl5-BZ#99 186 µg/Kg 0.0974 µg/Kg10/4/2001 Comp of Sta 12 (mouse 614851 4790327 12 0308031-11 Cl5-BZ#101 21.9 µg/Kg 0.278 µg/Kg10/4/2001 Comp of Sta 12 (mouse 614851 4790327 12 0308031-11 Cl5-BZ#105 60.9 µg/Kg 0.136 µg/Kg10/4/2001 Comp of Sta 12 (mouse 614851 4790327 12 0308031-11 Cl5-BZ#110 9.90 µg/Kg 0.264 µg/Kg



Extracted 7/30/04







10/4/2001 Comp of Sta 12 (mouse 614851 4790327 12 0308031-11 Cl5-BZ#114 5.17 µg/Kg 0.122 µg/Kg10/4/2001 Comp of Sta 12 (mouse 614851 4790327 12 0308031-11 Cl5-BZ#118 160 µg/Kg 0.285 µg/Kg10/4/2001 Comp of Sta 12 (mouse 614851 4790327 12 0308031-11 Cl5-BZ#123 0.240 U µg/Kg 0.240 µg/Kg10/4/2001 Comp of Sta 12 (mouse 614851 4790327 12 0308031-11 Cl5-BZ#126 0.212 U µg/Kg 0.212 µg/Kg10/4/2001 Comp of Sta 12 (mouse 614851 4790327 12 0308031-11 Cl6-BZ#128 10.4 µg/Kg 0.191 µg/Kg10/4/2001 Comp of Sta 12 (mouse 614851 4790327 12 0308031-11 Cl6-BZ#138 277 µg/Kg 0.275 µg/Kg10/4/2001 Comp of Sta 12 (mouse 614851 4790327 12 0308031-11 Cl6-BZ#146 30.4 µg/Kg 0.174 µg/Kg10/4/2001 Comp of Sta 12 (mouse 614851 4790327 12 0308031-11 Cl6-BZ#149 8.14 µg/Kg 0.223 µg/Kg10/4/2001 Comp of Sta 12 (mouse 614851 4790327 12 0308031-11 Cl6-BZ#151 0.369 U µg/Kg 0.369 µg/Kg10/4/2001 Comp of Sta 12 (mouse 614851 4790327 12 0308031-11 Cl6-BZ#153 365 µg/Kg 0.317 µg/Kg10/4/2001 Comp of Sta 12 (mouse 614851 4790327 12 0308031-11 Cl6-BZ#156 36.2 µg/Kg 0.226 µg/Kg10/4/2001 Comp of Sta 12 (mouse 614851 4790327 12 0308031-11 Cl6-BZ#157 6.61 µg/Kg 0.177 µg/Kg10/4/2001 Comp of Sta 12 (mouse 614851 4790327 12 0308031-11 Cl6-BZ#158 5.85 µg/Kg 0.150 µg/Kg10/4/2001 Comp of Sta 12 (mouse 614851 4790327 12 0308031-11 Cl6-BZ#167 5.48 µg/Kg 0.191 µg/Kg10/4/2001 Comp of Sta 12 (mouse 614851 4790327 12 0308031-11 Cl6-BZ#169 0.616 U µg/Kg 0.616 µg/Kg10/4/2001 Comp of Sta 12 (mouse 614851 4790327 12 0308031-11 Cl7-BZ#170 39.6 µg/Kg 0.717 µg/Kg10/4/2001 Comp of Sta 12 (mouse 614851 4790327 12 0308031-11 Cl7-BZ#174 0.539 J µg/Kg 0.146 µg/Kg10/4/2001 Comp of Sta 12 (mouse 614851 4790327 12 0308031-11 Cl7-BZ#177 3.72 µg/Kg 0.205 µg/Kg10/4/2001 Comp of Sta 12 (mouse 614851 4790327 12 0308031-11 Cl7-BZ#180 81.2 µg/Kg 0.306 µg/Kg10/4/2001 Comp of Sta 12 (mouse 614851 4790327 12 0308031-11 Cl7-BZ#183 8.28 µg/Kg 0.139 µg/Kg10/4/2001 Comp of Sta 12 (mouse 614851 4790327 12 0308031-11 Cl7-BZ#187 54.4 µg/Kg 0.153 µg/Kg10/4/2001 Comp of Sta 12 (mouse 614851 4790327 12 0308031-11 Cl7-BZ#189 0.275 U µg/Kg 0.275 µg/Kg10/4/2001 Comp of Sta 12 (mouse 614851 4790327 12 0308031-11 Cl8-BZ#194 12.3 µg/Kg 0.320 µg/Kg10/4/2001 Comp of Sta 12 (mouse 614851 4790327 12 0308031-11 Cl8-BZ#195 2.56 µg/Kg 0.317 µg/Kg10/4/2001 Comp of Sta 12 (mouse 614851 4790327 12 0308031-11 Cl8-BZ#201 14.9 µg/Kg 0.278 µg/Kg10/4/2001 Comp of Sta 12 (mouse 614851 4790327 12 0308031-11 Cl9-BZ#206 6.40 µg/Kg 0.372 µg/Kg10/4/2001 Comp of Sta 12 (mouse 614851 4790327 12 0308031-11 Cl10-BZ#209 0.870 J µg/Kg 0.174 µg/Kg10/4/2001 Comp of Sta 12 (mouse 614851 4790327 12 0308031-11 Monochlorobiphenyls 10.2 U µg/Kg 10.2 µg/Kg10/4/2001 Comp of Sta 12 (mouse 614851 4790327 12 0308031-11 Dichlorobiphenyls 0.299 U µg/Kg 0.299 µg/Kg10/4/2001 Comp of Sta 12 (mouse 614851 4790327 12 0308031-11 Trichlorobiphenyls 28.8 µg/Kg 1.03 µg/Kg10/4/2001 Comp of Sta 12 (mouse 614851 4790327 12 0308031-11 Tetrachlorobiphenyls 292 µg/Kg 0.160 µg/Kg10/4/2001 Comp of Sta 12 (mouse 614851 4790327 12 0308031-11 Pentachlorobiphenyls 769 µg/Kg 0.184 µg/Kg10/4/2001 Comp of Sta 12 (mouse 614851 4790327 12 0308031-11 Hexachlorobiphenyls 819 µg/Kg 0.292 µg/Kg10/4/2001 Comp of Sta 12 (mouse 614851 4790327 12 0308031-11 Heptachlorobiphenyls 175 µg/Kg 0.160 µg/Kg10/4/2001 Comp of Sta 12 (mouse 614851 4790327 12 0308031-11 Octachlorobiphenyls 32.4 µg/Kg 0.146 µg/Kg



Extracted 7/30/04







10/4/2001 Comp of Sta 12 (mouse 614851 4790327 12 0308031-11 Nonachlorobiphenyls 16.0 µg/Kg 0.372 µg/Kg10/4/2001 Comp of Sta 12 (mouse 614851 4790327 12 0308031-11 Decachlorobiphenyl 0.870 J µg/Kg 0.174 µg/Kg10/4/2001 Comp of Sta 12 (mouse 614851 4790327 12 0308031-11 Total Homologs 2130 µg/Kg 0.174 µg/Kg10/4/2001 Comp of Sta 12 (mouse 614851 4790327 12 0308031-11 Percent Lipids 4.1 % 0.1 %10/4/2001 Comp of Sta 12 (mouse 614851 4790327 12 0308031-11 Percent Moisture 69.9 % 0.1 %9/26/2001 Comp of Sta 13 611801 4757967 13 0308031-12 Cl2-BZ#8 0.137 U µg/Kg 0.137 µg/Kg9/26/2001 Comp of Sta 13 611801 4757967 13 0308031-12 Cl3-BZ#18 0.303 U µg/Kg 0.303 µg/Kg9/26/2001 Comp of Sta 13 611801 4757967 13 0308031-12 Cl3-BZ#31/#28 2.19 U µg/Kg 2.19 µg/Kg9/26/2001 Comp of Sta 13 611801 4757967 13 0308031-12 Cl4-BZ#44 0.208 U µg/Kg 0.208 µg/Kg9/26/2001 Comp of Sta 13 611801 4757967 13 0308031-12 Cl4-BZ#45 0.278 U µg/Kg 0.278 µg/Kg9/26/2001 Comp of Sta 13 611801 4757967 13 0308031-12 Cl4-BZ#47 0.381 J µg/Kg 0.353 µg/Kg9/26/2001 Comp of Sta 13 611801 4757967 13 0308031-12 Cl4-BZ#49 0.318 J µg/Kg 0.173 µg/Kg9/26/2001 Comp of Sta 13 611801 4757967 13 0308031-12 Cl4-BZ#52 0.349 J µg/Kg 0.197 µg/Kg9/26/2001 Comp of Sta 13 611801 4757967 13 0308031-12 Cl4-BZ#56 0.850 µg/Kg 0.103 µg/Kg9/26/2001 Comp of Sta 13 611801 4757967 13 0308031-12 Cl4-BZ#66 0.492 J µg/Kg 0.138 µg/Kg9/26/2001 Comp of Sta 13 611801 4757967 13 0308031-12 Cl4-BZ#70 0.230 J µg/Kg 0.121 µg/Kg9/26/2001 Comp of Sta 13 611801 4757967 13 0308031-12 Cl4-BZ#74 0.429 J µg/Kg 0.213 µg/Kg9/26/2001 Comp of Sta 13 611801 4757967 13 0308031-12 Cl4-BZ#77 0.191 U µg/Kg 0.191 µg/Kg9/26/2001 Comp of Sta 13 611801 4757967 13 0308031-12 Cl4-BZ#81 0.189 U µg/Kg 0.189 µg/Kg9/26/2001 Comp of Sta 13 611801 4757967 13 0308031-12 Cl5-BZ#87 0.342 J µg/Kg 0.0842 µg/Kg9/26/2001 Comp of Sta 13 611801 4757967 13 0308031-12 Cl5-BZ#95 0.0651 U µg/Kg 0.0651 µg/Kg9/26/2001 Comp of Sta 13 611801 4757967 13 0308031-12 Cl5-BZ#99 1.28 µg/Kg 0.0445 µg/Kg9/26/2001 Comp of Sta 13 611801 4757967 13 0308031-12 Cl5-BZ#101 0.238 J µg/Kg 0.127 µg/Kg9/26/2001 Comp of Sta 13 611801 4757967 13 0308031-12 Cl5-BZ#105 0.500 µg/Kg 0.0619 µg/Kg9/26/2001 Comp of Sta 13 611801 4757967 13 0308031-12 Cl5-BZ#110 0.121 U µg/Kg 0.121 µg/Kg9/26/2001 Comp of Sta 13 611801 4757967 13 0308031-12 Cl5-BZ#114 0.0556 U µg/Kg 0.0556 µg/Kg9/26/2001 Comp of Sta 13 611801 4757967 13 0308031-12 Cl5-BZ#118 1.29 µg/Kg 0.130 µg/Kg9/26/2001 Comp of Sta 13 611801 4757967 13 0308031-12 Cl5-BZ#123 0.110 U µg/Kg 0.110 µg/Kg9/26/2001 Comp of Sta 13 611801 4757967 13 0308031-12 Cl5-BZ#126 0.0969 U µg/Kg 0.0969 µg/Kg9/26/2001 Comp of Sta 13 611801 4757967 13 0308031-12 Cl6-BZ#128 0.0873 U µg/Kg 0.0873 µg/Kg9/26/2001 Comp of Sta 13 611801 4757967 13 0308031-12 Cl6-BZ#138 2.62 µg/Kg 0.125 µg/Kg9/26/2001 Comp of Sta 13 611801 4757967 13 0308031-12 Cl6-BZ#146 0.286 J µg/Kg 0.0794 µg/Kg9/26/2001 Comp of Sta 13 611801 4757967 13 0308031-12 Cl6-BZ#149 0.111 J µg/Kg 0.102 µg/Kg9/26/2001 Comp of Sta 13 611801 4757967 13 0308031-12 Cl6-BZ#151 0.168 U µg/Kg 0.168 µg/Kg9/26/2001 Comp of Sta 13 611801 4757967 13 0308031-12 Cl6-BZ#153 3.26 µg/Kg 0.145 µg/Kg



Extracted 7/30/04







9/26/2001 Comp of Sta 13 611801 4757967 13 0308031-12 Cl6-BZ#156 0.349 J µg/Kg 0.103 µg/Kg9/26/2001 Comp of Sta 13 611801 4757967 13 0308031-12 Cl6-BZ#157 0.0873 J µg/Kg 0.0810 µg/Kg9/26/2001 Comp of Sta 13 611801 4757967 13 0308031-12 Cl6-BZ#158 0.0794 J µg/Kg 0.0683 µg/Kg9/26/2001 Comp of Sta 13 611801 4757967 13 0308031-12 Cl6-BZ#167 0.0873 U µg/Kg 0.0873 µg/Kg9/26/2001 Comp of Sta 13 611801 4757967 13 0308031-12 Cl6-BZ#169 0.281 U µg/Kg 0.281 µg/Kg9/26/2001 Comp of Sta 13 611801 4757967 13 0308031-12 Cl7-BZ#170 0.327 U µg/Kg 0.327 µg/Kg9/26/2001 Comp of Sta 13 611801 4757967 13 0308031-12 Cl7-BZ#174 0.0667 U µg/Kg 0.0667 µg/Kg9/26/2001 Comp of Sta 13 611801 4757967 13 0308031-12 Cl7-BZ#177 0.0937 U µg/Kg 0.0937 µg/Kg9/26/2001 Comp of Sta 13 611801 4757967 13 0308031-12 Cl7-BZ#180 1.07 µg/Kg 0.140 µg/Kg9/26/2001 Comp of Sta 13 611801 4757967 13 0308031-12 Cl7-BZ#183 0.0873 J µg/Kg 0.0635 µg/Kg9/26/2001 Comp of Sta 13 611801 4757967 13 0308031-12 Cl7-BZ#187 0.659 µg/Kg 0.0699 µg/Kg9/26/2001 Comp of Sta 13 611801 4757967 13 0308031-12 Cl7-BZ#189 0.125 U µg/Kg 0.125 µg/Kg9/26/2001 Comp of Sta 13 611801 4757967 13 0308031-12 Cl8-BZ#194 0.310 J µg/Kg 0.146 µg/Kg9/26/2001 Comp of Sta 13 611801 4757967 13 0308031-12 Cl8-BZ#195 0.145 U µg/Kg 0.145 µg/Kg9/26/2001 Comp of Sta 13 611801 4757967 13 0308031-12 Cl8-BZ#201 0.619 J µg/Kg 0.127 µg/Kg9/26/2001 Comp of Sta 13 611801 4757967 13 0308031-12 Cl9-BZ#206 0.326 J µg/Kg 0.170 µg/Kg9/26/2001 Comp of Sta 13 611801 4757967 13 0308031-12 Cl10-BZ#209 0.0873 J µg/Kg 0.0794 µg/Kg9/26/2001 Comp of Sta 13 611801 4757967 13 0308031-12 Monochlorobiphenyls 4.67 U µg/Kg 4.67 µg/Kg9/26/2001 Comp of Sta 13 611801 4757967 13 0308031-12 Dichlorobiphenyls 0.137 U µg/Kg 0.137 µg/Kg9/26/2001 Comp of Sta 13 611801 4757967 13 0308031-12 Trichlorobiphenyls 1.45 J µg/Kg 0.468 µg/Kg9/26/2001 Comp of Sta 13 611801 4757967 13 0308031-12 Tetrachlorobiphenyls 8.83 µg/Kg 0.0731 µg/Kg9/26/2001 Comp of Sta 13 611801 4757967 13 0308031-12 Pentachlorobiphenyls 7.12 µg/Kg 0.0842 µg/Kg9/26/2001 Comp of Sta 13 611801 4757967 13 0308031-12 Hexachlorobiphenyls 9.20 µg/Kg 0.133 µg/Kg9/26/2001 Comp of Sta 13 611801 4757967 13 0308031-12 Heptachlorobiphenyls 2.01 µg/Kg 0.0731 µg/Kg9/26/2001 Comp of Sta 13 611801 4757967 13 0308031-12 Octachlorobiphenyls 0.897 µg/Kg 0.0667 µg/Kg9/26/2001 Comp of Sta 13 611801 4757967 13 0308031-12 Nonachlorobiphenyls 0.326 J µg/Kg 0.170 µg/Kg9/26/2001 Comp of Sta 13 611801 4757967 13 0308031-12 Decachlorobiphenyl 0.0873 J µg/Kg 0.0794 µg/Kg9/26/2001 Comp of Sta 13 611801 4757967 13 0308031-12 Total Homologs 29.9 µg/Kg 0.0794 µg/Kg9/26/2001 Comp of Sta 13 611801 4757967 13 0308031-12 Percent Lipids 2.2 % 0.1 %9/26/2001 Comp of Sta 13 611801 4757967 13 0308031-12 Percent Moisture 72.3 % 0.1 %9/20/2001 Comp of Sta 15 611552 4756404 15 0308031-13 Cl2-BZ#8 0.142 U µg/Kg 0.142 µg/Kg9/20/2001 Comp of Sta 15 611552 4756404 15 0308031-13 Cl3-BZ#18 0.315 U µg/Kg 0.315 µg/Kg9/20/2001 Comp of Sta 15 611552 4756404 15 0308031-13 Cl3-BZ#31/#28 2.27 U µg/Kg 2.27 µg/Kg9/20/2001 Comp of Sta 15 611552 4756404 15 0308031-13 Cl4-BZ#44 0.216 U µg/Kg 0.216 µg/Kg9/20/2001 Comp of Sta 15 611552 4756404 15 0308031-13 Cl4-BZ#45 0.289 U µg/Kg 0.289 µg/Kg



Extracted 7/30/04







9/20/2001 Comp of Sta 15 611552 4756404 15 0308031-13 Cl4-BZ#47 0.366 U µg/Kg 0.366 µg/Kg9/20/2001 Comp of Sta 15 611552 4756404 15 0308031-13 Cl4-BZ#49 0.256 J µg/Kg 0.180 µg/Kg9/20/2001 Comp of Sta 15 611552 4756404 15 0308031-13 Cl4-BZ#52 0.231 J µg/Kg 0.205 µg/Kg9/20/2001 Comp of Sta 15 611552 4756404 15 0308031-13 Cl4-BZ#56 0.528 J µg/Kg 0.107 µg/Kg9/20/2001 Comp of Sta 15 611552 4756404 15 0308031-13 Cl4-BZ#66 0.182 J µg/Kg 0.144 µg/Kg9/20/2001 Comp of Sta 15 611552 4756404 15 0308031-13 Cl4-BZ#70 0.125 U µg/Kg 0.125 µg/Kg9/20/2001 Comp of Sta 15 611552 4756404 15 0308031-13 Cl4-BZ#74 0.221 U µg/Kg 0.221 µg/Kg9/20/2001 Comp of Sta 15 611552 4756404 15 0308031-13 Cl4-BZ#77 0.198 U µg/Kg 0.198 µg/Kg9/20/2001 Comp of Sta 15 611552 4756404 15 0308031-13 Cl4-BZ#81 0.196 U µg/Kg 0.196 µg/Kg9/20/2001 Comp of Sta 15 611552 4756404 15 0308031-13 Cl5-BZ#87 0.231 J µg/Kg 0.0875 µg/Kg9/20/2001 Comp of Sta 15 611552 4756404 15 0308031-13 Cl5-BZ#95 0.0677 U µg/Kg 0.0677 µg/Kg9/20/2001 Comp of Sta 15 611552 4756404 15 0308031-13 Cl5-BZ#99 1.05 µg/Kg 0.0462 µg/Kg9/20/2001 Comp of Sta 15 611552 4756404 15 0308031-13 Cl5-BZ#101 0.140 J µg/Kg 0.132 µg/Kg9/20/2001 Comp of Sta 15 611552 4756404 15 0308031-13 Cl5-BZ#105 0.487 µg/Kg 0.0644 µg/Kg9/20/2001 Comp of Sta 15 611552 4756404 15 0308031-13 Cl5-BZ#110 0.125 U µg/Kg 0.125 µg/Kg9/20/2001 Comp of Sta 15 611552 4756404 15 0308031-13 Cl5-BZ#114 0.0578 U µg/Kg 0.0578 µg/Kg9/20/2001 Comp of Sta 15 611552 4756404 15 0308031-13 Cl5-BZ#118 1.23 µg/Kg 0.135 µg/Kg9/20/2001 Comp of Sta 15 611552 4756404 15 0308031-13 Cl5-BZ#123 0.114 U µg/Kg 0.114 µg/Kg9/20/2001 Comp of Sta 15 611552 4756404 15 0308031-13 Cl5-BZ#126 0.101 U µg/Kg 0.101 µg/Kg9/20/2001 Comp of Sta 15 611552 4756404 15 0308031-13 Cl6-BZ#128 0.0908 U µg/Kg 0.0908 µg/Kg9/20/2001 Comp of Sta 15 611552 4756404 15 0308031-13 Cl6-BZ#138 4.29 µg/Kg 0.130 µg/Kg9/20/2001 Comp of Sta 15 611552 4756404 15 0308031-13 Cl6-BZ#146 0.503 µg/Kg 0.0825 µg/Kg9/20/2001 Comp of Sta 15 611552 4756404 15 0308031-13 Cl6-BZ#149 0.106 U µg/Kg 0.106 µg/Kg9/20/2001 Comp of Sta 15 611552 4756404 15 0308031-13 Cl6-BZ#151 0.175 U µg/Kg 0.175 µg/Kg9/20/2001 Comp of Sta 15 611552 4756404 15 0308031-13 Cl6-BZ#153 6.89 µg/Kg 0.150 µg/Kg9/20/2001 Comp of Sta 15 611552 4756404 15 0308031-13 Cl6-BZ#156 0.809 µg/Kg 0.107 µg/Kg9/20/2001 Comp of Sta 15 611552 4756404 15 0308031-13 Cl6-BZ#157 0.190 J µg/Kg 0.0842 µg/Kg9/20/2001 Comp of Sta 15 611552 4756404 15 0308031-13 Cl6-BZ#158 0.0710 U µg/Kg 0.0710 µg/Kg9/20/2001 Comp of Sta 15 611552 4756404 15 0308031-13 Cl6-BZ#167 0.0908 U µg/Kg 0.0908 µg/Kg9/20/2001 Comp of Sta 15 611552 4756404 15 0308031-13 Cl6-BZ#169 0.292 U µg/Kg 0.292 µg/Kg9/20/2001 Comp of Sta 15 611552 4756404 15 0308031-13 Cl7-BZ#170 0.340 U µg/Kg 0.340 µg/Kg9/20/2001 Comp of Sta 15 611552 4756404 15 0308031-13 Cl7-BZ#174 0.0693 U µg/Kg 0.0693 µg/Kg9/20/2001 Comp of Sta 15 611552 4756404 15 0308031-13 Cl7-BZ#177 0.0974 U µg/Kg 0.0974 µg/Kg9/20/2001 Comp of Sta 15 611552 4756404 15 0308031-13 Cl7-BZ#180 3.44 µg/Kg 0.145 µg/Kg9/20/2001 Comp of Sta 15 611552 4756404 15 0308031-13 Cl7-BZ#183 0.190 J µg/Kg 0.0660 µg/Kg



Extracted 7/30/04







9/20/2001 Comp of Sta 15 611552 4756404 15 0308031-13 Cl7-BZ#187 0.875 µg/Kg 0.0726 µg/Kg9/20/2001 Comp of Sta 15 611552 4756404 15 0308031-13 Cl7-BZ#189 0.130 U µg/Kg 0.130 µg/Kg9/20/2001 Comp of Sta 15 611552 4756404 15 0308031-13 Cl8-BZ#194 1.40 µg/Kg 0.152 µg/Kg9/20/2001 Comp of Sta 15 611552 4756404 15 0308031-13 Cl8-BZ#195 0.150 U µg/Kg 0.150 µg/Kg9/20/2001 Comp of Sta 15 611552 4756404 15 0308031-13 Cl8-BZ#201 1.21 µg/Kg 0.132 µg/Kg9/20/2001 Comp of Sta 15 611552 4756404 15 0308031-13 Cl9-BZ#206 0.941 µg/Kg 0.177 µg/Kg9/20/2001 Comp of Sta 15 611552 4756404 15 0308031-13 Cl10-BZ#209 0.198 J µg/Kg 0.0825 µg/Kg9/20/2001 Comp of Sta 15 611552 4756404 15 0308031-13 Monochlorobiphenyls 4.85 U µg/Kg 4.85 µg/Kg9/20/2001 Comp of Sta 15 611552 4756404 15 0308031-13 Dichlorobiphenyls 0.142 U µg/Kg 0.142 µg/Kg9/20/2001 Comp of Sta 15 611552 4756404 15 0308031-13 Trichlorobiphenyls 1.30 J µg/Kg 0.487 µg/Kg9/20/2001 Comp of Sta 15 611552 4756404 15 0308031-13 Tetrachlorobiphenyls 7.04 µg/Kg 0.0759 µg/Kg9/20/2001 Comp of Sta 15 611552 4756404 15 0308031-13 Pentachlorobiphenyls 6.65 µg/Kg 0.0875 µg/Kg9/20/2001 Comp of Sta 15 611552 4756404 15 0308031-13 Hexachlorobiphenyls 11.5 µg/Kg 0.139 µg/Kg9/20/2001 Comp of Sta 15 611552 4756404 15 0308031-13 Heptachlorobiphenyls 6.71 µg/Kg 0.0759 µg/Kg9/20/2001 Comp of Sta 15 611552 4756404 15 0308031-13 Octachlorobiphenyls 2.82 µg/Kg 0.0693 µg/Kg9/20/2001 Comp of Sta 15 611552 4756404 15 0308031-13 Nonachlorobiphenyls 0.941 µg/Kg 0.177 µg/Kg9/20/2001 Comp of Sta 15 611552 4756404 15 0308031-13 Decachlorobiphenyl 0.198 J µg/Kg 0.0825 µg/Kg9/20/2001 Comp of Sta 15 611552 4756404 15 0308031-13 Total Homologs 37.1 µg/Kg 0.0825 µg/Kg9/20/2001 Comp of Sta 15 611552 4756404 15 0308031-13 Percent Lipids 3.0 % 0.1 %9/20/2001 Comp of Sta 15 611552 4756404 15 0308031-13 Percent Moisture 70.3 % 0.1 %9/20/2001 Comp of Sta 16 609620 4754219 16 0308031-14 Cl2-BZ#8 0.138 U µg/Kg 0.138 µg/Kg9/20/2001 Comp of Sta 16 609620 4754219 16 0308031-14 Cl3-BZ#18 0.307 U µg/Kg 0.307 µg/Kg9/20/2001 Comp of Sta 16 609620 4754219 16 0308031-14 Cl3-BZ#31/#28 3.46 J µg/Kg 2.21 µg/Kg9/20/2001 Comp of Sta 16 609620 4754219 16 0308031-14 Cl4-BZ#44 1.23 µg/Kg 0.211 µg/Kg9/20/2001 Comp of Sta 16 609620 4754219 16 0308031-14 Cl4-BZ#45 0.281 U µg/Kg 0.281 µg/Kg9/20/2001 Comp of Sta 16 609620 4754219 16 0308031-14 Cl4-BZ#47 4.21 µg/Kg 0.357 µg/Kg9/20/2001 Comp of Sta 16 609620 4754219 16 0308031-14 Cl4-BZ#49 1.60 µg/Kg 0.175 µg/Kg9/20/2001 Comp of Sta 16 609620 4754219 16 0308031-14 Cl4-BZ#52 2.81 µg/Kg 0.199 µg/Kg9/20/2001 Comp of Sta 16 609620 4754219 16 0308031-14 Cl4-BZ#56 2.31 µg/Kg 0.105 µg/Kg9/20/2001 Comp of Sta 16 609620 4754219 16 0308031-14 Cl4-BZ#66 3.54 µg/Kg 0.140 µg/Kg9/20/2001 Comp of Sta 16 609620 4754219 16 0308031-14 Cl4-BZ#70 2.43 µg/Kg 0.122 µg/Kg9/20/2001 Comp of Sta 16 609620 4754219 16 0308031-14 Cl4-BZ#74 3.02 µg/Kg 0.215 µg/Kg9/20/2001 Comp of Sta 16 609620 4754219 16 0308031-14 Cl4-BZ#77 0.193 U µg/Kg 0.193 µg/Kg9/20/2001 Comp of Sta 16 609620 4754219 16 0308031-14 Cl4-BZ#81 0.191 U µg/Kg 0.191 µg/Kg9/20/2001 Comp of Sta 16 609620 4754219 16 0308031-14 Cl5-BZ#87 3.62 µg/Kg 0.0852 µg/Kg



Extracted 7/30/04







9/20/2001 Comp of Sta 16 609620 4754219 16 0308031-14 Cl5-BZ#95 0.659 µg/Kg 0.0659 µg/Kg9/20/2001 Comp of Sta 16 609620 4754219 16 0308031-14 Cl5-BZ#99 22.9 µg/Kg 0.0450 µg/Kg9/20/2001 Comp of Sta 16 609620 4754219 16 0308031-14 Cl5-BZ#101 2.73 µg/Kg 0.129 µg/Kg9/20/2001 Comp of Sta 16 609620 4754219 16 0308031-14 Cl5-BZ#105 5.33 µg/Kg 0.0627 µg/Kg9/20/2001 Comp of Sta 16 609620 4754219 16 0308031-14 Cl5-BZ#110 1.25 µg/Kg 0.122 µg/Kg9/20/2001 Comp of Sta 16 609620 4754219 16 0308031-14 Cl5-BZ#114 0.0563 U µg/Kg 0.0563 µg/Kg9/20/2001 Comp of Sta 16 609620 4754219 16 0308031-14 Cl5-BZ#118 10.3 µg/Kg 0.132 µg/Kg9/20/2001 Comp of Sta 16 609620 4754219 16 0308031-14 Cl5-BZ#123 0.111 U µg/Kg 0.111 µg/Kg9/20/2001 Comp of Sta 16 609620 4754219 16 0308031-14 Cl5-BZ#126 0.0980 U µg/Kg 0.0980 µg/Kg9/20/2001 Comp of Sta 16 609620 4754219 16 0308031-14 Cl6-BZ#128 1.50 µg/Kg 0.0884 µg/Kg9/20/2001 Comp of Sta 16 609620 4754219 16 0308031-14 Cl6-BZ#138 41.7 µg/Kg 0.127 µg/Kg9/20/2001 Comp of Sta 16 609620 4754219 16 0308031-14 Cl6-BZ#146 3.96 µg/Kg 0.0804 µg/Kg9/20/2001 Comp of Sta 16 609620 4754219 16 0308031-14 Cl6-BZ#149 1.15 µg/Kg 0.103 µg/Kg9/20/2001 Comp of Sta 16 609620 4754219 16 0308031-14 Cl6-BZ#151 0.170 U µg/Kg 0.170 µg/Kg9/20/2001 Comp of Sta 16 609620 4754219 16 0308031-14 Cl6-BZ#153 52.9 µg/Kg 0.146 µg/Kg9/20/2001 Comp of Sta 16 609620 4754219 16 0308031-14 Cl6-BZ#156 6.58 µg/Kg 0.105 µg/Kg9/20/2001 Comp of Sta 16 609620 4754219 16 0308031-14 Cl6-BZ#157 1.25 µg/Kg 0.0820 µg/Kg9/20/2001 Comp of Sta 16 609620 4754219 16 0308031-14 Cl6-BZ#158 0.932 µg/Kg 0.0691 µg/Kg9/20/2001 Comp of Sta 16 609620 4754219 16 0308031-14 Cl6-BZ#167 0.587 µg/Kg 0.0884 µg/Kg9/20/2001 Comp of Sta 16 609620 4754219 16 0308031-14 Cl6-BZ#169 0.285 U µg/Kg 0.285 µg/Kg9/20/2001 Comp of Sta 16 609620 4754219 16 0308031-14 Cl7-BZ#170 11.0 µg/Kg 0.331 µg/Kg9/20/2001 Comp of Sta 16 609620 4754219 16 0308031-14 Cl7-BZ#174 0.0675 U µg/Kg 0.0675 µg/Kg9/20/2001 Comp of Sta 16 609620 4754219 16 0308031-14 Cl7-BZ#177 0.474 µg/Kg 0.0948 µg/Kg9/20/2001 Comp of Sta 16 609620 4754219 16 0308031-14 Cl7-BZ#180 22.6 µg/Kg 0.141 µg/Kg9/20/2001 Comp of Sta 16 609620 4754219 16 0308031-14 Cl7-BZ#183 1.34 µg/Kg 0.0643 µg/Kg9/20/2001 Comp of Sta 16 609620 4754219 16 0308031-14 Cl7-BZ#187 14.1 µg/Kg 0.0707 µg/Kg9/20/2001 Comp of Sta 16 609620 4754219 16 0308031-14 Cl7-BZ#189 0.127 U µg/Kg 0.127 µg/Kg9/20/2001 Comp of Sta 16 609620 4754219 16 0308031-14 Cl8-BZ#194 5.06 µg/Kg 0.148 µg/Kg9/20/2001 Comp of Sta 16 609620 4754219 16 0308031-14 Cl8-BZ#195 0.972 µg/Kg 0.146 µg/Kg9/20/2001 Comp of Sta 16 609620 4754219 16 0308031-14 Cl8-BZ#201 4.48 µg/Kg 0.129 µg/Kg9/20/2001 Comp of Sta 16 609620 4754219 16 0308031-14 Cl9-BZ#206 4.61 µg/Kg 0.172 µg/Kg9/20/2001 Comp of Sta 16 609620 4754219 16 0308031-14 Cl10-BZ#209 0.571 µg/Kg 0.0804 µg/Kg9/20/2001 Comp of Sta 16 609620 4754219 16 0308031-14 Monochlorobiphenyls 4.72 U µg/Kg 4.72 µg/Kg9/20/2001 Comp of Sta 16 609620 4754219 16 0308031-14 Dichlorobiphenyls 0.138 U µg/Kg 0.138 µg/Kg9/20/2001 Comp of Sta 16 609620 4754219 16 0308031-14 Trichlorobiphenyls 3.59 µg/Kg 0.474 µg/Kg



Extracted 7/30/04







9/20/2001 Comp of Sta 16 609620 4754219 16 0308031-14 Tetrachlorobiphenyls 31.0 µg/Kg 0.0739 µg/Kg9/20/2001 Comp of Sta 16 609620 4754219 16 0308031-14 Pentachlorobiphenyls 69.9 µg/Kg 0.0852 µg/Kg9/20/2001 Comp of Sta 16 609620 4754219 16 0308031-14 Hexachlorobiphenyls 123 µg/Kg 0.135 µg/Kg9/20/2001 Comp of Sta 16 609620 4754219 16 0308031-14 Heptachlorobiphenyls 46.3 µg/Kg 0.0739 µg/Kg9/20/2001 Comp of Sta 16 609620 4754219 16 0308031-14 Octachlorobiphenyls 14.4 µg/Kg 0.0675 µg/Kg9/20/2001 Comp of Sta 16 609620 4754219 16 0308031-14 Nonachlorobiphenyls 14.0 µg/Kg 0.172 µg/Kg9/20/2001 Comp of Sta 16 609620 4754219 16 0308031-14 Decachlorobiphenyl 0.571 µg/Kg 0.0804 µg/Kg9/20/2001 Comp of Sta 16 609620 4754219 16 0308031-14 Total Homologs 302 µg/Kg 0.0804 µg/Kg9/20/2001 Comp of Sta 16 609620 4754219 16 0308031-14 Percent Lipids 1.8 % 0.1 %9/20/2001 Comp of Sta 16 609620 4754219 16 0308031-14 Percent Moisture 72.0 % 0.1 %

10/15/2001 Comp of Sta 17 607475 4750334 17 0308031-15 Cl2-BZ#8 0.183 U µg/Kg 0.183 µg/Kg10/15/2001 Comp of Sta 17 607475 4750334 17 0308031-15 Cl3-BZ#18 0.405 U µg/Kg 0.405 µg/Kg10/15/2001 Comp of Sta 17 607475 4750334 17 0308031-15 Cl3-BZ#31/#28 5.36 J µg/Kg 2.92 µg/Kg10/15/2001 Comp of Sta 17 607475 4750334 17 0308031-15 Cl4-BZ#44 1.04 J µg/Kg 0.278 µg/Kg10/15/2001 Comp of Sta 17 607475 4750334 17 0308031-15 Cl4-BZ#45 0.372 U µg/Kg 0.372 µg/Kg10/15/2001 Comp of Sta 17 607475 4750334 17 0308031-15 Cl4-BZ#47 13.7 µg/Kg 0.471 µg/Kg10/15/2001 Comp of Sta 17 607475 4750334 17 0308031-15 Cl4-BZ#49 1.88 µg/Kg 0.231 µg/Kg10/15/2001 Comp of Sta 17 607475 4750334 17 0308031-15 Cl4-BZ#52 4.74 µg/Kg 0.263 µg/Kg10/15/2001 Comp of Sta 17 607475 4750334 17 0308031-15 Cl4-BZ#56 4.87 µg/Kg 0.138 µg/Kg10/15/2001 Comp of Sta 17 607475 4750334 17 0308031-15 Cl4-BZ#66 6.01 µg/Kg 0.185 µg/Kg10/15/2001 Comp of Sta 17 607475 4750334 17 0308031-15 Cl4-BZ#70 1.56 µg/Kg 0.161 µg/Kg10/15/2001 Comp of Sta 17 607475 4750334 17 0308031-15 Cl4-BZ#74 10.0 µg/Kg 0.285 µg/Kg10/15/2001 Comp of Sta 17 607475 4750334 17 0308031-15 Cl4-BZ#77 0.255 U µg/Kg 0.255 µg/Kg10/15/2001 Comp of Sta 17 607475 4750334 17 0308031-15 Cl4-BZ#81 0.253 U µg/Kg 0.253 µg/Kg10/15/2001 Comp of Sta 17 607475 4750334 17 0308031-15 Cl5-BZ#87 5.26 µg/Kg 0.112 µg/Kg10/15/2001 Comp of Sta 17 607475 4750334 17 0308031-15 Cl5-BZ#95 0.817 µg/Kg 0.0870 µg/Kg10/15/2001 Comp of Sta 17 607475 4750334 17 0308031-15 Cl5-BZ#99 35.5 µg/Kg 0.0594 µg/Kg10/15/2001 Comp of Sta 17 607475 4750334 17 0308031-15 Cl5-BZ#101 3.60 µg/Kg 0.170 µg/Kg10/15/2001 Comp of Sta 17 607475 4750334 17 0308031-15 Cl5-BZ#105 12.7 µg/Kg 0.0828 µg/Kg10/15/2001 Comp of Sta 17 607475 4750334 17 0308031-15 Cl5-BZ#110 1.42 µg/Kg 0.161 µg/Kg10/15/2001 Comp of Sta 17 607475 4750334 17 0308031-15 Cl5-BZ#114 0.764 µg/Kg 0.0743 µg/Kg10/15/2001 Comp of Sta 17 607475 4750334 17 0308031-15 Cl5-BZ#118 25.4 µg/Kg 0.174 µg/Kg10/15/2001 Comp of Sta 17 607475 4750334 17 0308031-15 Cl5-BZ#123 0.147 U µg/Kg 0.147 µg/Kg10/15/2001 Comp of Sta 17 607475 4750334 17 0308031-15 Cl5-BZ#126 0.130 U µg/Kg 0.130 µg/Kg10/15/2001 Comp of Sta 17 607475 4750334 17 0308031-15 Cl6-BZ#128 1.80 µg/Kg 0.117 µg/Kg



Extracted 7/30/04







10/15/2001 Comp of Sta 17 607475 4750334 17 0308031-15 Cl6-BZ#138 51.0 µg/Kg 0.168 µg/Kg10/15/2001 Comp of Sta 17 607475 4750334 17 0308031-15 Cl6-BZ#146 5.82 µg/Kg 0.106 µg/Kg10/15/2001 Comp of Sta 17 607475 4750334 17 0308031-15 Cl6-BZ#149 1.09 µg/Kg 0.136 µg/Kg10/15/2001 Comp of Sta 17 607475 4750334 17 0308031-15 Cl6-BZ#151 0.225 U µg/Kg 0.225 µg/Kg10/15/2001 Comp of Sta 17 607475 4750334 17 0308031-15 Cl6-BZ#153 69.5 µg/Kg 0.193 µg/Kg10/15/2001 Comp of Sta 17 607475 4750334 17 0308031-15 Cl6-BZ#156 7.50 µg/Kg 0.138 µg/Kg10/15/2001 Comp of Sta 17 607475 4750334 17 0308031-15 Cl6-BZ#157 1.35 µg/Kg 0.108 µg/Kg10/15/2001 Comp of Sta 17 607475 4750334 17 0308031-15 Cl6-BZ#158 0.913 µg/Kg 0.0913 µg/Kg10/15/2001 Comp of Sta 17 607475 4750334 17 0308031-15 Cl6-BZ#167 0.817 µg/Kg 0.117 µg/Kg10/15/2001 Comp of Sta 17 607475 4750334 17 0308031-15 Cl6-BZ#169 0.376 U µg/Kg 0.376 µg/Kg10/15/2001 Comp of Sta 17 607475 4750334 17 0308031-15 Cl7-BZ#170 10.1 µg/Kg 0.437 µg/Kg10/15/2001 Comp of Sta 17 607475 4750334 17 0308031-15 Cl7-BZ#174 0.0892 U µg/Kg 0.0892 µg/Kg10/15/2001 Comp of Sta 17 607475 4750334 17 0308031-15 Cl7-BZ#177 0.892 µg/Kg 0.125 µg/Kg10/15/2001 Comp of Sta 17 607475 4750334 17 0308031-15 Cl7-BZ#180 18.2 µg/Kg 0.187 µg/Kg10/15/2001 Comp of Sta 17 607475 4750334 17 0308031-15 Cl7-BZ#183 1.36 µg/Kg 0.0849 µg/Kg10/15/2001 Comp of Sta 17 607475 4750334 17 0308031-15 Cl7-BZ#187 9.17 µg/Kg 0.0934 µg/Kg10/15/2001 Comp of Sta 17 607475 4750334 17 0308031-15 Cl7-BZ#189 0.168 U µg/Kg 0.168 µg/Kg10/15/2001 Comp of Sta 17 607475 4750334 17 0308031-15 Cl8-BZ#194 5.12 µg/Kg 0.195 µg/Kg10/15/2001 Comp of Sta 17 607475 4750334 17 0308031-15 Cl8-BZ#195 0.945 J µg/Kg 0.193 µg/Kg10/15/2001 Comp of Sta 17 607475 4750334 17 0308031-15 Cl8-BZ#201 6.22 µg/Kg 0.170 µg/Kg10/15/2001 Comp of Sta 17 607475 4750334 17 0308031-15 Cl9-BZ#206 4.14 µg/Kg 0.227 µg/Kg10/15/2001 Comp of Sta 17 607475 4750334 17 0308031-15 Cl10-BZ#209 0.690 µg/Kg 0.106 µg/Kg10/15/2001 Comp of Sta 17 607475 4750334 17 0308031-15 Monochlorobiphenyls 6.24 U µg/Kg 6.24 µg/Kg10/15/2001 Comp of Sta 17 607475 4750334 17 0308031-15 Dichlorobiphenyls 0.183 U µg/Kg 0.183 µg/Kg10/15/2001 Comp of Sta 17 607475 4750334 17 0308031-15 Trichlorobiphenyls 5.21 µg/Kg 0.626 µg/Kg10/15/2001 Comp of Sta 17 607475 4750334 17 0308031-15 Tetrachlorobiphenyls 65.8 µg/Kg 0.0977 µg/Kg10/15/2001 Comp of Sta 17 607475 4750334 17 0308031-15 Pentachlorobiphenyls 138 µg/Kg 0.112 µg/Kg10/15/2001 Comp of Sta 17 607475 4750334 17 0308031-15 Hexachlorobiphenyls 151 µg/Kg 0.178 µg/Kg10/15/2001 Comp of Sta 17 607475 4750334 17 0308031-15 Heptachlorobiphenyls 36.6 µg/Kg 0.0977 µg/Kg10/15/2001 Comp of Sta 17 607475 4750334 17 0308031-15 Octachlorobiphenyls 12.2 µg/Kg 0.0892 µg/Kg10/15/2001 Comp of Sta 17 607475 4750334 17 0308031-15 Nonachlorobiphenyls 13.4 µg/Kg 0.227 µg/Kg10/15/2001 Comp of Sta 17 607475 4750334 17 0308031-15 Decachlorobiphenyl 0.690 µg/Kg 0.106 µg/Kg10/15/2001 Comp of Sta 17 607475 4750334 17 0308031-15 Total Homologs 423 µg/Kg 0.106 µg/Kg10/15/2001 Comp of Sta 17 607475 4750334 17 0308031-15 Percent Lipids 5.7 % 0.1 %10/15/2001 Comp of Sta 17 607475 4750334 17 0308031-15 Percent Moisture 62.6 % 0.1 %



Extracted 7/30/04







9/24/2001 Comp of Sta 18 608173 4747866 18 0308032-01 Cl2-BZ#8 0.132 U µg/Kg 0.132 µg/Kg9/24/2001 Comp of Sta 18 608173 4747866 18 0308032-01 Cl3-BZ#18 0.294 U µg/Kg 0.294 µg/Kg9/24/2001 Comp of Sta 18 608173 4747866 18 0308032-01 Cl3-BZ#31/#28 3.40 J µg/Kg 2.12 µg/Kg9/24/2001 Comp of Sta 18 608173 4747866 18 0308032-01 Cl4-BZ#44 0.231 J µg/Kg 0.201 µg/Kg9/24/2001 Comp of Sta 18 608173 4747866 18 0308032-01 Cl4-BZ#45 0.269 U µg/Kg 0.269 µg/Kg9/24/2001 Comp of Sta 18 608173 4747866 18 0308032-01 Cl4-BZ#47 0.845 J µg/Kg 0.341 µg/Kg9/24/2001 Comp of Sta 18 608173 4747866 18 0308032-01 Cl4-BZ#49 0.231 J µg/Kg 0.168 µg/Kg9/24/2001 Comp of Sta 18 608173 4747866 18 0308032-01 Cl4-BZ#52 0.191 U µg/Kg 0.191 µg/Kg9/24/2001 Comp of Sta 18 608173 4747866 18 0308032-01 Cl4-BZ#56 0.715 µg/Kg 0.0999 µg/Kg9/24/2001 Comp of Sta 18 608173 4747866 18 0308032-01 Cl4-BZ#66 0.984 µg/Kg 0.134 µg/Kg9/24/2001 Comp of Sta 18 608173 4747866 18 0308032-01 Cl4-BZ#70 0.223 J µg/Kg 0.117 µg/Kg9/24/2001 Comp of Sta 18 608173 4747866 18 0308032-01 Cl4-BZ#74 0.976 J µg/Kg 0.206 µg/Kg9/24/2001 Comp of Sta 18 608173 4747866 18 0308032-01 Cl4-BZ#77 0.184 U µg/Kg 0.184 µg/Kg9/24/2001 Comp of Sta 18 608173 4747866 18 0308032-01 Cl4-BZ#81 0.183 U µg/Kg 0.183 µg/Kg9/24/2001 Comp of Sta 18 608173 4747866 18 0308032-01 Cl5-BZ#87 0.507 µg/Kg 0.0815 µg/Kg9/24/2001 Comp of Sta 18 608173 4747866 18 0308032-01 Cl5-BZ#95 0.0630 U µg/Kg 0.0630 µg/Kg9/24/2001 Comp of Sta 18 608173 4747866 18 0308032-01 Cl5-BZ#99 3.84 µg/Kg 0.0430 µg/Kg9/24/2001 Comp of Sta 18 608173 4747866 18 0308032-01 Cl5-BZ#101 0.323 J µg/Kg 0.123 µg/Kg9/24/2001 Comp of Sta 18 608173 4747866 18 0308032-01 Cl5-BZ#105 1.68 µg/Kg 0.0599 µg/Kg9/24/2001 Comp of Sta 18 608173 4747866 18 0308032-01 Cl5-BZ#110 0.117 U µg/Kg 0.117 µg/Kg9/24/2001 Comp of Sta 18 608173 4747866 18 0308032-01 Cl5-BZ#114 0.131 J µg/Kg 0.0538 µg/Kg9/24/2001 Comp of Sta 18 608173 4747866 18 0308032-01 Cl5-BZ#118 3.94 µg/Kg 0.126 µg/Kg9/24/2001 Comp of Sta 18 608173 4747866 18 0308032-01 Cl5-BZ#123 0.106 U µg/Kg 0.106 µg/Kg9/24/2001 Comp of Sta 18 608173 4747866 18 0308032-01 Cl5-BZ#126 0.0938 U µg/Kg 0.0938 µg/Kg9/24/2001 Comp of Sta 18 608173 4747866 18 0308032-01 Cl6-BZ#128 0.207 J µg/Kg 0.0845 µg/Kg9/24/2001 Comp of Sta 18 608173 4747866 18 0308032-01 Cl6-BZ#138 10.5 µg/Kg 0.121 µg/Kg9/24/2001 Comp of Sta 18 608173 4747866 18 0308032-01 Cl6-BZ#146 1.11 µg/Kg 0.0769 µg/Kg9/24/2001 Comp of Sta 18 608173 4747866 18 0308032-01 Cl6-BZ#149 0.138 J µg/Kg 0.0984 µg/Kg9/24/2001 Comp of Sta 18 608173 4747866 18 0308032-01 Cl6-BZ#151 0.163 U µg/Kg 0.163 µg/Kg9/24/2001 Comp of Sta 18 608173 4747866 18 0308032-01 Cl6-BZ#153 12.9 µg/Kg 0.140 µg/Kg9/24/2001 Comp of Sta 18 608173 4747866 18 0308032-01 Cl6-BZ#156 1.75 µg/Kg 0.0999 µg/Kg9/24/2001 Comp of Sta 18 608173 4747866 18 0308032-01 Cl6-BZ#157 0.323 J µg/Kg 0.0784 µg/Kg9/24/2001 Comp of Sta 18 608173 4747866 18 0308032-01 Cl6-BZ#158 0.200 J µg/Kg 0.0661 µg/Kg9/24/2001 Comp of Sta 18 608173 4747866 18 0308032-01 Cl6-BZ#167 0.207 J µg/Kg 0.0845 µg/Kg9/24/2001 Comp of Sta 18 608173 4747866 18 0308032-01 Cl6-BZ#169 0.272 U µg/Kg 0.272 µg/Kg



Extracted 7/30/04







9/24/2001 Comp of Sta 18 608173 4747866 18 0308032-01 Cl7-BZ#170 3.80 µg/Kg 0.317 µg/Kg9/24/2001 Comp of Sta 18 608173 4747866 18 0308032-01 Cl7-BZ#174 0.0646 U µg/Kg 0.0646 µg/Kg9/24/2001 Comp of Sta 18 608173 4747866 18 0308032-01 Cl7-BZ#177 0.207 J µg/Kg 0.0907 µg/Kg9/24/2001 Comp of Sta 18 608173 4747866 18 0308032-01 Cl7-BZ#180 6.63 µg/Kg 0.135 µg/Kg9/24/2001 Comp of Sta 18 608173 4747866 18 0308032-01 Cl7-BZ#183 0.430 µg/Kg 0.0615 µg/Kg9/24/2001 Comp of Sta 18 608173 4747866 18 0308032-01 Cl7-BZ#187 3.36 µg/Kg 0.0676 µg/Kg9/24/2001 Comp of Sta 18 608173 4747866 18 0308032-01 Cl7-BZ#189 0.121 U µg/Kg 0.121 µg/Kg9/24/2001 Comp of Sta 18 608173 4747866 18 0308032-01 Cl8-BZ#194 2.61 µg/Kg 0.141 µg/Kg9/24/2001 Comp of Sta 18 608173 4747866 18 0308032-01 Cl8-BZ#195 0.354 J µg/Kg 0.140 µg/Kg9/24/2001 Comp of Sta 18 608173 4747866 18 0308032-01 Cl8-BZ#201 2.64 µg/Kg 0.123 µg/Kg9/24/2001 Comp of Sta 18 608173 4747866 18 0308032-01 Cl9-BZ#206 2.44 µg/Kg 0.164 µg/Kg9/24/2001 Comp of Sta 18 608173 4747866 18 0308032-01 Cl10-BZ#209 0.361 J µg/Kg 0.0769 µg/Kg9/24/2001 Comp of Sta 18 608173 4747866 18 0308032-01 Monochlorobiphenyls 4.52 U µg/Kg 4.52 µg/Kg9/24/2001 Comp of Sta 18 608173 4747866 18 0308032-01 Dichlorobiphenyls 0.132 U µg/Kg 0.132 µg/Kg9/24/2001 Comp of Sta 18 608173 4747866 18 0308032-01 Trichlorobiphenyls 3.08 µg/Kg 0.454 µg/Kg9/24/2001 Comp of Sta 18 608173 4747866 18 0308032-01 Tetrachlorobiphenyls 7.48 µg/Kg 0.0707 µg/Kg9/24/2001 Comp of Sta 18 608173 4747866 18 0308032-01 Pentachlorobiphenyls 20.0 µg/Kg 0.0815 µg/Kg9/24/2001 Comp of Sta 18 608173 4747866 18 0308032-01 Hexachlorobiphenyls 30.6 µg/Kg 0.129 µg/Kg9/24/2001 Comp of Sta 18 608173 4747866 18 0308032-01 Heptachlorobiphenyls 13.6 µg/Kg 0.0707 µg/Kg9/24/2001 Comp of Sta 18 608173 4747866 18 0308032-01 Octachlorobiphenyls 6.03 µg/Kg 0.0646 µg/Kg9/24/2001 Comp of Sta 18 608173 4747866 18 0308032-01 Nonachlorobiphenyls 5.82 µg/Kg 0.164 µg/Kg9/24/2001 Comp of Sta 18 608173 4747866 18 0308032-01 Decachlorobiphenyl 0.361 J µg/Kg 0.0769 µg/Kg9/24/2001 Comp of Sta 18 608173 4747866 18 0308032-01 Total Homologs 87.0 µg/Kg 0.0769 µg/Kg9/24/2001 Comp of Sta 18 608173 4747866 18 0308032-01 Percent Lipids 2.8 % 0.1 %9/24/2001 Comp of Sta 18 608173 4747866 18 0308032-01 Percent Moisture 70.4 % 0.1 %

10/11/2001 Comp of Sta 20 (mouse 609713 4741759 20 0308032-02 Cl2-BZ#8 0.134 U µg/Kg 0.134 µg/Kg10/11/2001 Comp of Sta 20 (mouse 609713 4741759 20 0308032-02 Cl3-BZ#18 0.297 U µg/Kg 0.297 µg/Kg10/11/2001 Comp of Sta 20 (mouse 609713 4741759 20 0308032-02 Cl3-BZ#31/#28 4.22 J µg/Kg 2.14 µg/Kg10/11/2001 Comp of Sta 20 (mouse 609713 4741759 20 0308032-02 Cl4-BZ#44 0.559 J µg/Kg 0.203 µg/Kg10/11/2001 Comp of Sta 20 (mouse 609713 4741759 20 0308032-02 Cl4-BZ#45 0.272 U µg/Kg 0.272 µg/Kg10/11/2001 Comp of Sta 20 (mouse 609713 4741759 20 0308032-02 Cl4-BZ#47 7.60 µg/Kg 0.345 µg/Kg10/11/2001 Comp of Sta 20 (mouse 609713 4741759 20 0308032-02 Cl4-BZ#49 0.885 µg/Kg 0.169 µg/Kg10/11/2001 Comp of Sta 20 (mouse 609713 4741759 20 0308032-02 Cl4-BZ#52 2.17 µg/Kg 0.193 µg/Kg10/11/2001 Comp of Sta 20 (mouse 609713 4741759 20 0308032-02 Cl4-BZ#56 2.52 µg/Kg 0.101 µg/Kg10/11/2001 Comp of Sta 20 (mouse 609713 4741759 20 0308032-02 Cl4-BZ#66 3.85 µg/Kg 0.135 µg/Kg



Extracted 7/30/04







10/11/2001 Comp of Sta 20 (mouse 609713 4741759 20 0308032-02 Cl4-BZ#70 0.986 µg/Kg 0.118 µg/Kg10/11/2001 Comp of Sta 20 (mouse 609713 4741759 20 0308032-02 Cl4-BZ#74 4.99 µg/Kg 0.208 µg/Kg10/11/2001 Comp of Sta 20 (mouse 609713 4741759 20 0308032-02 Cl4-BZ#77 0.186 U µg/Kg 0.186 µg/Kg10/11/2001 Comp of Sta 20 (mouse 609713 4741759 20 0308032-02 Cl4-BZ#81 0.185 U µg/Kg 0.185 µg/Kg10/11/2001 Comp of Sta 20 (mouse 609713 4741759 20 0308032-02 Cl5-BZ#87 2.24 µg/Kg 0.0823 µg/Kg10/11/2001 Comp of Sta 20 (mouse 609713 4741759 20 0308032-02 Cl5-BZ#95 0.388 µg/Kg 0.0637 µg/Kg10/11/2001 Comp of Sta 20 (mouse 609713 4741759 20 0308032-02 Cl5-BZ#99 16.6 J µg/Kg 0.0435 µg/Kg10/11/2001 Comp of Sta 20 (mouse 609713 4741759 20 0308032-02 Cl5-BZ#101 1.81 µg/Kg 0.124 µg/Kg10/11/2001 Comp of Sta 20 (mouse 609713 4741759 20 0308032-02 Cl5-BZ#105 5.94 J µg/Kg 0.0606 µg/Kg10/11/2001 Comp of Sta 20 (mouse 609713 4741759 20 0308032-02 Cl5-BZ#110 0.458 J µg/Kg 0.118 µg/Kg10/11/2001 Comp of Sta 20 (mouse 609713 4741759 20 0308032-02 Cl5-BZ#114 0.396 µg/Kg 0.0544 µg/Kg10/11/2001 Comp of Sta 20 (mouse 609713 4741759 20 0308032-02 Cl5-BZ#118 13.0 J µg/Kg 0.127 µg/Kg10/11/2001 Comp of Sta 20 (mouse 609713 4741759 20 0308032-02 Cl5-BZ#123 0.107 U µg/Kg 0.107 µg/Kg10/11/2001 Comp of Sta 20 (mouse 609713 4741759 20 0308032-02 Cl5-BZ#126 0.0947 U µg/Kg 0.0947 µg/Kg10/11/2001 Comp of Sta 20 (mouse 609713 4741759 20 0308032-02 Cl6-BZ#128 0.629 µg/Kg 0.0854 µg/Kg10/11/2001 Comp of Sta 20 (mouse 609713 4741759 20 0308032-02 Cl6-BZ#138 28.4 J µg/Kg 0.123 µg/Kg10/11/2001 Comp of Sta 20 (mouse 609713 4741759 20 0308032-02 Cl6-BZ#146 3.32 µg/Kg 0.0776 µg/Kg10/11/2001 Comp of Sta 20 (mouse 609713 4741759 20 0308032-02 Cl6-BZ#149 0.380 J µg/Kg 0.0994 µg/Kg10/11/2001 Comp of Sta 20 (mouse 609713 4741759 20 0308032-02 Cl6-BZ#151 0.165 U µg/Kg 0.165 µg/Kg10/11/2001 Comp of Sta 20 (mouse 609713 4741759 20 0308032-02 Cl6-BZ#153 41.8 J µg/Kg 0.141 µg/Kg10/11/2001 Comp of Sta 20 (mouse 609713 4741759 20 0308032-02 Cl6-BZ#156 4.20 µg/Kg 0.101 µg/Kg10/11/2001 Comp of Sta 20 (mouse 609713 4741759 20 0308032-02 Cl6-BZ#157 0.784 µg/Kg 0.0792 µg/Kg10/11/2001 Comp of Sta 20 (mouse 609713 4741759 20 0308032-02 Cl6-BZ#158 0.419 J µg/Kg 0.0668 µg/Kg10/11/2001 Comp of Sta 20 (mouse 609713 4741759 20 0308032-02 Cl6-BZ#167 0.412 J µg/Kg 0.0854 µg/Kg10/11/2001 Comp of Sta 20 (mouse 609713 4741759 20 0308032-02 Cl6-BZ#169 0.275 U µg/Kg 0.275 µg/Kg10/11/2001 Comp of Sta 20 (mouse 609713 4741759 20 0308032-02 Cl7-BZ#170 7.59 J µg/Kg 0.320 µg/Kg10/11/2001 Comp of Sta 20 (mouse 609713 4741759 20 0308032-02 Cl7-BZ#174 0.0652 U µg/Kg 0.0652 µg/Kg10/11/2001 Comp of Sta 20 (mouse 609713 4741759 20 0308032-02 Cl7-BZ#177 0.497 µg/Kg 0.0916 µg/Kg10/11/2001 Comp of Sta 20 (mouse 609713 4741759 20 0308032-02 Cl7-BZ#180 13.1 µg/Kg 0.137 µg/Kg10/11/2001 Comp of Sta 20 (mouse 609713 4741759 20 0308032-02 Cl7-BZ#183 0.637 µg/Kg 0.0621 µg/Kg10/11/2001 Comp of Sta 20 (mouse 609713 4741759 20 0308032-02 Cl7-BZ#187 5.50 µg/Kg 0.0683 µg/Kg10/11/2001 Comp of Sta 20 (mouse 609713 4741759 20 0308032-02 Cl7-BZ#189 0.123 U µg/Kg 0.123 µg/Kg10/11/2001 Comp of Sta 20 (mouse 609713 4741759 20 0308032-02 Cl8-BZ#194 4.34 µg/Kg 0.143 µg/Kg10/11/2001 Comp of Sta 20 (mouse 609713 4741759 20 0308032-02 Cl8-BZ#195 0.559 J µg/Kg 0.141 µg/Kg10/11/2001 Comp of Sta 20 (mouse 609713 4741759 20 0308032-02 Cl8-BZ#201 5.92 J µg/Kg 0.124 µg/Kg



Extracted 7/30/04







10/11/2001 Comp of Sta 20 (mouse 609713 4741759 20 0308032-02 Cl9-BZ#206 4.57 µg/Kg 0.166 µg/Kg10/11/2001 Comp of Sta 20 (mouse 609713 4741759 20 0308032-02 Cl10-BZ#209 0.714 µg/Kg 0.0776 µg/Kg10/11/2001 Comp of Sta 20 (mouse 609713 4741759 20 0308032-02 Monochlorobiphenyls 4.57 U µg/Kg 4.57 µg/Kg10/11/2001 Comp of Sta 20 (mouse 609713 4741759 20 0308032-02 Dichlorobiphenyls 0.134 U µg/Kg 0.134 µg/Kg10/11/2001 Comp of Sta 20 (mouse 609713 4741759 20 0308032-02 Trichlorobiphenyls 4.11 µg/Kg 0.458 µg/Kg10/11/2001 Comp of Sta 20 (mouse 609713 4741759 20 0308032-02 Tetrachlorobiphenyls 30.9 µg/Kg 0.0714 µg/Kg10/11/2001 Comp of Sta 20 (mouse 609713 4741759 20 0308032-02 Pentachlorobiphenyls 68.1 µg/Kg 0.0823 µg/Kg10/11/2001 Comp of Sta 20 (mouse 609713 4741759 20 0308032-02 Hexachlorobiphenyls 88.1 µg/Kg 0.130 µg/Kg10/11/2001 Comp of Sta 20 (mouse 609713 4741759 20 0308032-02 Heptachlorobiphenyls 26.3 µg/Kg 0.0714 µg/Kg10/11/2001 Comp of Sta 20 (mouse 609713 4741759 20 0308032-02 Octachlorobiphenyls 10.3 µg/Kg 0.0652 µg/Kg10/11/2001 Comp of Sta 20 (mouse 609713 4741759 20 0308032-02 Nonachlorobiphenyls 9.80 µg/Kg 0.166 µg/Kg10/11/2001 Comp of Sta 20 (mouse 609713 4741759 20 0308032-02 Decachlorobiphenyl 0.714 µg/Kg 0.0776 µg/Kg10/11/2001 Comp of Sta 20 (mouse 609713 4741759 20 0308032-02 Total Homologs 238 µg/Kg 0.0776 µg/Kg10/11/2001 Comp of Sta 20 (mouse 609713 4741759 20 0308032-02 Percent Lipids 5.0 % 0.1 %10/11/2001 Comp of Sta 20 (mouse 609713 4741759 20 0308032-02 Percent Moisture 68.1 % 0.1 %9/27/2001 Comp of Sta 21 609281 4740033 21 0308032-03 Cl2-BZ#8 0.137 U µg/Kg 0.137 µg/Kg9/27/2001 Comp of Sta 21 609281 4740033 21 0308032-03 Cl3-BZ#18 0.304 U µg/Kg 0.304 µg/Kg9/27/2001 Comp of Sta 21 609281 4740033 21 0308032-03 Cl3-BZ#31/#28 2.21 J µg/Kg 2.19 µg/Kg9/27/2001 Comp of Sta 21 609281 4740033 21 0308032-03 Cl4-BZ#44 0.209 U µg/Kg 0.209 µg/Kg9/27/2001 Comp of Sta 21 609281 4740033 21 0308032-03 Cl4-BZ#45 0.279 U µg/Kg 0.279 µg/Kg9/27/2001 Comp of Sta 21 609281 4740033 21 0308032-03 Cl4-BZ#47 0.773 J µg/Kg 0.354 µg/Kg9/27/2001 Comp of Sta 21 609281 4740033 21 0308032-03 Cl4-BZ#49 0.174 U µg/Kg 0.174 µg/Kg9/27/2001 Comp of Sta 21 609281 4740033 21 0308032-03 Cl4-BZ#52 0.198 U µg/Kg 0.198 µg/Kg9/27/2001 Comp of Sta 21 609281 4740033 21 0308032-03 Cl4-BZ#56 0.789 µg/Kg 0.104 µg/Kg9/27/2001 Comp of Sta 21 609281 4740033 21 0308032-03 Cl4-BZ#66 0.271 J µg/Kg 0.139 µg/Kg9/27/2001 Comp of Sta 21 609281 4740033 21 0308032-03 Cl4-BZ#70 0.121 U µg/Kg 0.121 µg/Kg9/27/2001 Comp of Sta 21 609281 4740033 21 0308032-03 Cl4-BZ#74 0.223 J µg/Kg 0.213 µg/Kg9/27/2001 Comp of Sta 21 609281 4740033 21 0308032-03 Cl4-BZ#77 0.191 U µg/Kg 0.191 µg/Kg9/27/2001 Comp of Sta 21 609281 4740033 21 0308032-03 Cl4-BZ#81 0.190 U µg/Kg 0.190 µg/Kg9/27/2001 Comp of Sta 21 609281 4740033 21 0308032-03 Cl5-BZ#87 0.0844 U µg/Kg 0.0844 µg/Kg9/27/2001 Comp of Sta 21 609281 4740033 21 0308032-03 Cl5-BZ#95 0.0653 U µg/Kg 0.0653 µg/Kg9/27/2001 Comp of Sta 21 609281 4740033 21 0308032-03 Cl5-BZ#99 2.24 µg/Kg 0.0446 µg/Kg9/27/2001 Comp of Sta 21 609281 4740033 21 0308032-03 Cl5-BZ#101 0.207 J µg/Kg 0.127 µg/Kg9/27/2001 Comp of Sta 21 609281 4740033 21 0308032-03 Cl5-BZ#105 1.43 µg/Kg 0.0621 µg/Kg9/27/2001 Comp of Sta 21 609281 4740033 21 0308032-03 Cl5-BZ#110 0.121 U µg/Kg 0.121 µg/Kg



Extracted 7/30/04







9/27/2001 Comp of Sta 21 609281 4740033 21 0308032-03 Cl5-BZ#114 0.0558 U µg/Kg 0.0558 µg/Kg9/27/2001 Comp of Sta 21 609281 4740033 21 0308032-03 Cl5-BZ#118 4.30 µg/Kg 0.131 µg/Kg9/27/2001 Comp of Sta 21 609281 4740033 21 0308032-03 Cl5-BZ#123 0.110 U µg/Kg 0.110 µg/Kg9/27/2001 Comp of Sta 21 609281 4740033 21 0308032-03 Cl5-BZ#126 0.0972 U µg/Kg 0.0972 µg/Kg9/27/2001 Comp of Sta 21 609281 4740033 21 0308032-03 Cl6-BZ#128 0.247 J µg/Kg 0.0876 µg/Kg9/27/2001 Comp of Sta 21 609281 4740033 21 0308032-03 Cl6-BZ#138 10.2 µg/Kg 0.126 µg/Kg9/27/2001 Comp of Sta 21 609281 4740033 21 0308032-03 Cl6-BZ#146 1.37 µg/Kg 0.0797 µg/Kg9/27/2001 Comp of Sta 21 609281 4740033 21 0308032-03 Cl6-BZ#149 0.102 U µg/Kg 0.102 µg/Kg9/27/2001 Comp of Sta 21 609281 4740033 21 0308032-03 Cl6-BZ#151 0.169 U µg/Kg 0.169 µg/Kg9/27/2001 Comp of Sta 21 609281 4740033 21 0308032-03 Cl6-BZ#153 16.2 µg/Kg 0.145 µg/Kg9/27/2001 Comp of Sta 21 609281 4740033 21 0308032-03 Cl6-BZ#156 1.55 µg/Kg 0.104 µg/Kg9/27/2001 Comp of Sta 21 609281 4740033 21 0308032-03 Cl6-BZ#157 0.311 J µg/Kg 0.0813 µg/Kg9/27/2001 Comp of Sta 21 609281 4740033 21 0308032-03 Cl6-BZ#158 0.207 J µg/Kg 0.0685 µg/Kg9/27/2001 Comp of Sta 21 609281 4740033 21 0308032-03 Cl6-BZ#167 0.287 J µg/Kg 0.0876 µg/Kg9/27/2001 Comp of Sta 21 609281 4740033 21 0308032-03 Cl6-BZ#169 0.282 U µg/Kg 0.282 µg/Kg9/27/2001 Comp of Sta 21 609281 4740033 21 0308032-03 Cl7-BZ#170 3.02 µg/Kg 0.328 µg/Kg9/27/2001 Comp of Sta 21 609281 4740033 21 0308032-03 Cl7-BZ#174 0.0669 U µg/Kg 0.0669 µg/Kg9/27/2001 Comp of Sta 21 609281 4740033 21 0308032-03 Cl7-BZ#177 0.0940 U µg/Kg 0.0940 µg/Kg9/27/2001 Comp of Sta 21 609281 4740033 21 0308032-03 Cl7-BZ#180 5.48 µg/Kg 0.140 µg/Kg9/27/2001 Comp of Sta 21 609281 4740033 21 0308032-03 Cl7-BZ#183 0.422 µg/Kg 0.0637 µg/Kg9/27/2001 Comp of Sta 21 609281 4740033 21 0308032-03 Cl7-BZ#187 2.65 µg/Kg 0.0701 µg/Kg9/27/2001 Comp of Sta 21 609281 4740033 21 0308032-03 Cl7-BZ#189 0.126 U µg/Kg 0.126 µg/Kg9/27/2001 Comp of Sta 21 609281 4740033 21 0308032-03 Cl8-BZ#194 1.58 µg/Kg 0.147 µg/Kg9/27/2001 Comp of Sta 21 609281 4740033 21 0308032-03 Cl8-BZ#195 0.145 U µg/Kg 0.145 µg/Kg9/27/2001 Comp of Sta 21 609281 4740033 21 0308032-03 Cl8-BZ#201 3.24 µg/Kg 0.127 µg/Kg9/27/2001 Comp of Sta 21 609281 4740033 21 0308032-03 Cl9-BZ#206 2.30 µg/Kg 0.170 µg/Kg9/27/2001 Comp of Sta 21 609281 4740033 21 0308032-03 Cl10-BZ#209 0.574 µg/Kg 0.0797 µg/Kg9/27/2001 Comp of Sta 21 609281 4740033 21 0308032-03 Monochlorobiphenyls 4.68 U µg/Kg 4.68 µg/Kg9/27/2001 Comp of Sta 21 609281 4740033 21 0308032-03 Dichlorobiphenyls 0.137 U µg/Kg 0.137 µg/Kg9/27/2001 Comp of Sta 21 609281 4740033 21 0308032-03 Trichlorobiphenyls 1.80 J µg/Kg 0.470 µg/Kg9/27/2001 Comp of Sta 21 609281 4740033 21 0308032-03 Tetrachlorobiphenyls 6.78 µg/Kg 0.0733 µg/Kg9/27/2001 Comp of Sta 21 609281 4740033 21 0308032-03 Pentachlorobiphenyls 23.0 µg/Kg 0.0844 µg/Kg9/27/2001 Comp of Sta 21 609281 4740033 21 0308032-03 Hexachlorobiphenyls 32.8 µg/Kg 0.134 µg/Kg9/27/2001 Comp of Sta 21 609281 4740033 21 0308032-03 Heptachlorobiphenyls 11.3 µg/Kg 0.0733 µg/Kg9/27/2001 Comp of Sta 21 609281 4740033 21 0308032-03 Octachlorobiphenyls 4.24 µg/Kg 0.0669 µg/Kg



Extracted 7/30/04







9/27/2001 Comp of Sta 21 609281 4740033 21 0308032-03 Nonachlorobiphenyls 9.65 µg/Kg 0.170 µg/Kg9/27/2001 Comp of Sta 21 609281 4740033 21 0308032-03 Decachlorobiphenyl 0.574 µg/Kg 0.0797 µg/Kg9/27/2001 Comp of Sta 21 609281 4740033 21 0308032-03 Total Homologs 90.2 µg/Kg 0.0797 µg/Kg9/27/2001 Comp of Sta 21 609281 4740033 21 0308032-03 Percent Lipids 3.5 % 0.1 %9/27/2001 Comp of Sta 21 609281 4740033 21 0308032-03 Percent Moisture 72.6 % 0.1 %

10/16/2001 Comp of Sta 22 602339 4715386 22 0308032-04 Cl2-BZ#8 0.122 U µg/Kg 0.122 µg/Kg10/16/2001 Comp of Sta 22 602339 4715386 22 0308032-04 Cl3-BZ#18 0.271 U µg/Kg 0.271 µg/Kg10/16/2001 Comp of Sta 22 602339 4715386 22 0308032-04 Cl3-BZ#31/#28 2.06 J µg/Kg 1.95 µg/Kg10/16/2001 Comp of Sta 22 602339 4715386 22 0308032-04 Cl4-BZ#44 0.186 U µg/Kg 0.186 µg/Kg10/16/2001 Comp of Sta 22 602339 4715386 22 0308032-04 Cl4-BZ#45 0.248 U µg/Kg 0.248 µg/Kg10/16/2001 Comp of Sta 22 602339 4715386 22 0308032-04 Cl4-BZ#47 0.333 J µg/Kg 0.315 µg/Kg10/16/2001 Comp of Sta 22 602339 4715386 22 0308032-04 Cl4-BZ#49 0.155 U µg/Kg 0.155 µg/Kg10/16/2001 Comp of Sta 22 602339 4715386 22 0308032-04 Cl4-BZ#52 0.255 J µg/Kg 0.176 µg/Kg10/16/2001 Comp of Sta 22 602339 4715386 22 0308032-04 Cl4-BZ#56 1.03 µg/Kg 0.0922 µg/Kg10/16/2001 Comp of Sta 22 602339 4715386 22 0308032-04 Cl4-BZ#66 0.123 U µg/Kg 0.123 µg/Kg10/16/2001 Comp of Sta 22 602339 4715386 22 0308032-04 Cl4-BZ#70 0.108 U µg/Kg 0.108 µg/Kg10/16/2001 Comp of Sta 22 602339 4715386 22 0308032-04 Cl4-BZ#74 0.190 U µg/Kg 0.190 µg/Kg10/16/2001 Comp of Sta 22 602339 4715386 22 0308032-04 Cl4-BZ#77 0.170 U µg/Kg 0.170 µg/Kg10/16/2001 Comp of Sta 22 602339 4715386 22 0308032-04 Cl4-BZ#81 0.169 U µg/Kg 0.169 µg/Kg10/16/2001 Comp of Sta 22 602339 4715386 22 0308032-04 Cl5-BZ#87 0.0752 U µg/Kg 0.0752 µg/Kg10/16/2001 Comp of Sta 22 602339 4715386 22 0308032-04 Cl5-BZ#95 0.0582 U µg/Kg 0.0582 µg/Kg10/16/2001 Comp of Sta 22 602339 4715386 22 0308032-04 Cl5-BZ#99 0.780 µg/Kg 0.0397 µg/Kg10/16/2001 Comp of Sta 22 602339 4715386 22 0308032-04 Cl5-BZ#101 0.128 J µg/Kg 0.113 µg/Kg10/16/2001 Comp of Sta 22 602339 4715386 22 0308032-04 Cl5-BZ#105 0.305 µg/Kg 0.0553 µg/Kg10/16/2001 Comp of Sta 22 602339 4715386 22 0308032-04 Cl5-BZ#110 0.108 U µg/Kg 0.108 µg/Kg10/16/2001 Comp of Sta 22 602339 4715386 22 0308032-04 Cl5-BZ#114 0.0496 U µg/Kg 0.0496 µg/Kg10/16/2001 Comp of Sta 22 602339 4715386 22 0308032-04 Cl5-BZ#118 0.723 µg/Kg 0.116 µg/Kg10/16/2001 Comp of Sta 22 602339 4715386 22 0308032-04 Cl5-BZ#123 0.0979 U µg/Kg 0.0979 µg/Kg10/16/2001 Comp of Sta 22 602339 4715386 22 0308032-04 Cl5-BZ#126 0.0865 U µg/Kg 0.0865 µg/Kg10/16/2001 Comp of Sta 22 602339 4715386 22 0308032-04 Cl6-BZ#128 0.0780 U µg/Kg 0.0780 µg/Kg10/16/2001 Comp of Sta 22 602339 4715386 22 0308032-04 Cl6-BZ#138 2.18 µg/Kg 0.112 µg/Kg10/16/2001 Comp of Sta 22 602339 4715386 22 0308032-04 Cl6-BZ#146 0.390 µg/Kg 0.0709 µg/Kg10/16/2001 Comp of Sta 22 602339 4715386 22 0308032-04 Cl6-BZ#149 0.0908 U µg/Kg 0.0908 µg/Kg10/16/2001 Comp of Sta 22 602339 4715386 22 0308032-04 Cl6-BZ#151 0.150 U µg/Kg 0.150 µg/Kg10/16/2001 Comp of Sta 22 602339 4715386 22 0308032-04 Cl6-BZ#153 3.72 µg/Kg 0.129 µg/Kg



Extracted 7/30/04







10/16/2001 Comp of Sta 22 602339 4715386 22 0308032-04 Cl6-BZ#156 0.284 J µg/Kg 0.0922 µg/Kg10/16/2001 Comp of Sta 22 602339 4715386 22 0308032-04 Cl6-BZ#157 0.0723 U µg/Kg 0.0723 µg/Kg10/16/2001 Comp of Sta 22 602339 4715386 22 0308032-04 Cl6-BZ#158 0.0610 UJ µg/Kg 0.0610 µg/Kg10/16/2001 Comp of Sta 22 602339 4715386 22 0308032-04 Cl6-BZ#167 0.0780 U µg/Kg 0.0780 µg/Kg10/16/2001 Comp of Sta 22 602339 4715386 22 0308032-04 Cl6-BZ#169 0.251 U µg/Kg 0.251 µg/Kg10/16/2001 Comp of Sta 22 602339 4715386 22 0308032-04 Cl7-BZ#170 1.06 J µg/Kg 0.292 µg/Kg10/16/2001 Comp of Sta 22 602339 4715386 22 0308032-04 Cl7-BZ#174 0.0596 U µg/Kg 0.0596 µg/Kg10/16/2001 Comp of Sta 22 602339 4715386 22 0308032-04 Cl7-BZ#177 0.121 J µg/Kg 0.0837 µg/Kg10/16/2001 Comp of Sta 22 602339 4715386 22 0308032-04 Cl7-BZ#180 1.92 µg/Kg 0.125 µg/Kg10/16/2001 Comp of Sta 22 602339 4715386 22 0308032-04 Cl7-BZ#183 0.184 J µg/Kg 0.0567 µg/Kg10/16/2001 Comp of Sta 22 602339 4715386 22 0308032-04 Cl7-BZ#187 0.681 µg/Kg 0.0624 µg/Kg10/16/2001 Comp of Sta 22 602339 4715386 22 0308032-04 Cl7-BZ#189 0.112 U µg/Kg 0.112 µg/Kg10/16/2001 Comp of Sta 22 602339 4715386 22 0308032-04 Cl8-BZ#194 1.09 µg/Kg 0.131 µg/Kg10/16/2001 Comp of Sta 22 602339 4715386 22 0308032-04 Cl8-BZ#195 0.129 U µg/Kg 0.129 µg/Kg10/16/2001 Comp of Sta 22 602339 4715386 22 0308032-04 Cl8-BZ#201 0.993 µg/Kg 0.113 µg/Kg10/16/2001 Comp of Sta 22 602339 4715386 22 0308032-04 Cl9-BZ#206 0.787 µg/Kg 0.152 µg/Kg10/16/2001 Comp of Sta 22 602339 4715386 22 0308032-04 Cl10-BZ#209 0.312 J µg/Kg 0.0709 µg/Kg10/16/2001 Comp of Sta 22 602339 4715386 22 0308032-04 Monochlorobiphenyls 4.17 U µg/Kg 4.17 µg/Kg10/16/2001 Comp of Sta 22 602339 4715386 22 0308032-04 Dichlorobiphenyls 0.122 U µg/Kg 0.122 µg/Kg10/16/2001 Comp of Sta 22 602339 4715386 22 0308032-04 Trichlorobiphenyls 2.48 µg/Kg 0.418 µg/Kg10/16/2001 Comp of Sta 22 602339 4715386 22 0308032-04 Tetrachlorobiphenyls 7.95 µg/Kg 0.0652 µg/Kg10/16/2001 Comp of Sta 22 602339 4715386 22 0308032-04 Pentachlorobiphenyls 6.97 µg/Kg 0.0752 µg/Kg10/16/2001 Comp of Sta 22 602339 4715386 22 0308032-04 Hexachlorobiphenyls 7.94 µg/Kg 0.119 µg/Kg10/16/2001 Comp of Sta 22 602339 4715386 22 0308032-04 Heptachlorobiphenyls 3.93 µg/Kg 0.0652 µg/Kg10/16/2001 Comp of Sta 22 602339 4715386 22 0308032-04 Octachlorobiphenyls 1.88 µg/Kg 0.0596 µg/Kg10/16/2001 Comp of Sta 22 602339 4715386 22 0308032-04 Nonachlorobiphenyls 5.49 µg/Kg 0.152 µg/Kg10/16/2001 Comp of Sta 22 602339 4715386 22 0308032-04 Decachlorobiphenyl 0.312 J µg/Kg 0.0709 µg/Kg10/16/2001 Comp of Sta 22 602339 4715386 22 0308032-04 Total Homologs 37.0 µg/Kg 0.0709 µg/Kg10/16/2001 Comp of Sta 22 602339 4715386 22 0308032-04 Percent Lipids 2.9 % 0.1 %10/16/2001 Comp of Sta 22 602339 4715386 22 0308032-04 Percent Moisture 71.8 % 0.1 %10/18/2001 Comp of Sta 23 600373 4705549 23 0308032-05 Cl2-BZ#8 0.115 U µg/Kg 0.115 µg/Kg10/18/2001 Comp of Sta 23 600373 4705549 23 0308032-05 Cl3-BZ#18 0.256 U µg/Kg 0.256 µg/Kg10/18/2001 Comp of Sta 23 600373 4705549 23 0308032-05 Cl3-BZ#31/#28 1.85 U µg/Kg 1.85 µg/Kg10/18/2001 Comp of Sta 23 600373 4705549 23 0308032-05 Cl4-BZ#44 0.176 U µg/Kg 0.176 µg/Kg10/18/2001 Comp of Sta 23 600373 4705549 23 0308032-05 Cl4-BZ#45 0.235 U µg/Kg 0.235 µg/Kg



Extracted 7/30/04







10/18/2001 Comp of Sta 23 600373 4705549 23 0308032-05 Cl4-BZ#47 0.375 J µg/Kg 0.298 µg/Kg10/18/2001 Comp of Sta 23 600373 4705549 23 0308032-05 Cl4-BZ#49 0.146 U µg/Kg 0.146 µg/Kg10/18/2001 Comp of Sta 23 600373 4705549 23 0308032-05 Cl4-BZ#52 0.166 U µg/Kg 0.166 µg/Kg10/18/2001 Comp of Sta 23 600373 4705549 23 0308032-05 Cl4-BZ#56 0.630 µg/Kg 0.0871 µg/Kg10/18/2001 Comp of Sta 23 600373 4705549 23 0308032-05 Cl4-BZ#66 0.117 U µg/Kg 0.117 µg/Kg10/18/2001 Comp of Sta 23 600373 4705549 23 0308032-05 Cl4-BZ#70 0.102 U µg/Kg 0.102 µg/Kg10/18/2001 Comp of Sta 23 600373 4705549 23 0308032-05 Cl4-BZ#74 0.180 U µg/Kg 0.180 µg/Kg10/18/2001 Comp of Sta 23 600373 4705549 23 0308032-05 Cl4-BZ#77 0.161 U µg/Kg 0.161 µg/Kg10/18/2001 Comp of Sta 23 600373 4705549 23 0308032-05 Cl4-BZ#81 0.160 U µg/Kg 0.160 µg/Kg10/18/2001 Comp of Sta 23 600373 4705549 23 0308032-05 Cl5-BZ#87 0.0710 U µg/Kg 0.0710 µg/Kg10/18/2001 Comp of Sta 23 600373 4705549 23 0308032-05 Cl5-BZ#95 0.0550 U µg/Kg 0.0550 µg/Kg10/18/2001 Comp of Sta 23 600373 4705549 23 0308032-05 Cl5-BZ#99 0.154 J µg/Kg 0.0375 µg/Kg10/18/2001 Comp of Sta 23 600373 4705549 23 0308032-05 Cl5-BZ#101 0.107 U µg/Kg 0.107 µg/Kg10/18/2001 Comp of Sta 23 600373 4705549 23 0308032-05 Cl5-BZ#105 0.0523 U µg/Kg 0.0523 µg/Kg10/18/2001 Comp of Sta 23 600373 4705549 23 0308032-05 Cl5-BZ#110 0.102 U µg/Kg 0.102 µg/Kg10/18/2001 Comp of Sta 23 600373 4705549 23 0308032-05 Cl5-BZ#114 0.0469 U µg/Kg 0.0469 µg/Kg10/18/2001 Comp of Sta 23 600373 4705549 23 0308032-05 Cl5-BZ#118 0.110 U µg/Kg 0.110 µg/Kg10/18/2001 Comp of Sta 23 600373 4705549 23 0308032-05 Cl5-BZ#123 0.0925 U µg/Kg 0.0925 µg/Kg10/18/2001 Comp of Sta 23 600373 4705549 23 0308032-05 Cl5-BZ#126 0.0818 U µg/Kg 0.0818 µg/Kg10/18/2001 Comp of Sta 23 600373 4705549 23 0308032-05 Cl6-BZ#128 0.0737 U µg/Kg 0.0737 µg/Kg10/18/2001 Comp of Sta 23 600373 4705549 23 0308032-05 Cl6-BZ#138 0.643 µg/Kg 0.106 µg/Kg10/18/2001 Comp of Sta 23 600373 4705549 23 0308032-05 Cl6-BZ#146 0.0670 U µg/Kg 0.0670 µg/Kg10/18/2001 Comp of Sta 23 600373 4705549 23 0308032-05 Cl6-BZ#149 0.0858 U µg/Kg 0.0858 µg/Kg10/18/2001 Comp of Sta 23 600373 4705549 23 0308032-05 Cl6-BZ#151 0.142 U µg/Kg 0.142 µg/Kg10/18/2001 Comp of Sta 23 600373 4705549 23 0308032-05 Cl6-BZ#153 1.42 µg/Kg 0.122 µg/Kg10/18/2001 Comp of Sta 23 600373 4705549 23 0308032-05 Cl6-BZ#156 0.0871 U µg/Kg 0.0871 µg/Kg10/18/2001 Comp of Sta 23 600373 4705549 23 0308032-05 Cl6-BZ#157 0.0684 U µg/Kg 0.0684 µg/Kg10/18/2001 Comp of Sta 23 600373 4705549 23 0308032-05 Cl6-BZ#158 0.0576 UJ µg/Kg 0.0576 µg/Kg10/18/2001 Comp of Sta 23 600373 4705549 23 0308032-05 Cl6-BZ#167 0.0737 U µg/Kg 0.0737 µg/Kg10/18/2001 Comp of Sta 23 600373 4705549 23 0308032-05 Cl6-BZ#169 0.237 U µg/Kg 0.237 µg/Kg10/18/2001 Comp of Sta 23 600373 4705549 23 0308032-05 Cl7-BZ#170 4.03 µg/Kg 0.276 µg/Kg10/18/2001 Comp of Sta 23 600373 4705549 23 0308032-05 Cl7-BZ#174 0.0563 U µg/Kg 0.0563 µg/Kg10/18/2001 Comp of Sta 23 600373 4705549 23 0308032-05 Cl7-BZ#177 0.0791 U µg/Kg 0.0791 µg/Kg10/18/2001 Comp of Sta 23 600373 4705549 23 0308032-05 Cl7-BZ#180 8.67 µg/Kg 0.118 µg/Kg10/18/2001 Comp of Sta 23 600373 4705549 23 0308032-05 Cl7-BZ#183 0.168 J µg/Kg 0.0536 µg/Kg



Extracted 7/30/04







10/18/2001 Comp of Sta 23 600373 4705549 23 0308032-05 Cl7-BZ#187 0.255 J µg/Kg 0.0590 µg/Kg10/18/2001 Comp of Sta 23 600373 4705549 23 0308032-05 Cl7-BZ#189 0.106 U µg/Kg 0.106 µg/Kg10/18/2001 Comp of Sta 23 600373 4705549 23 0308032-05 Cl8-BZ#194 6.72 µg/Kg 0.123 µg/Kg10/18/2001 Comp of Sta 23 600373 4705549 23 0308032-05 Cl8-BZ#195 0.617 µg/Kg 0.122 µg/Kg10/18/2001 Comp of Sta 23 600373 4705549 23 0308032-05 Cl8-BZ#201 2.47 µg/Kg 0.107 µg/Kg10/18/2001 Comp of Sta 23 600373 4705549 23 0308032-05 Cl9-BZ#206 2.37 µg/Kg 0.143 µg/Kg10/18/2001 Comp of Sta 23 600373 4705549 23 0308032-05 Cl10-BZ#209 0.308 J µg/Kg 0.0670 µg/Kg10/18/2001 Comp of Sta 23 600373 4705549 23 0308032-05 Monochlorobiphenyls 3.94 U µg/Kg 3.94 µg/Kg10/18/2001 Comp of Sta 23 600373 4705549 23 0308032-05 Dichlorobiphenyls 0.115 U µg/Kg 0.115 µg/Kg10/18/2001 Comp of Sta 23 600373 4705549 23 0308032-05 Trichlorobiphenyls 4.72 µg/Kg 0.395 µg/Kg10/18/2001 Comp of Sta 23 600373 4705549 23 0308032-05 Tetrachlorobiphenyls 6.53 µg/Kg 0.0617 µg/Kg10/18/2001 Comp of Sta 23 600373 4705549 23 0308032-05 Pentachlorobiphenyls 0.355 µg/Kg 0.0710 µg/Kg10/18/2001 Comp of Sta 23 600373 4705549 23 0308032-05 Hexachlorobiphenyls 2.74 µg/Kg 0.113 µg/Kg10/18/2001 Comp of Sta 23 600373 4705549 23 0308032-05 Heptachlorobiphenyls 11.8 µg/Kg 0.0617 µg/Kg10/18/2001 Comp of Sta 23 600373 4705549 23 0308032-05 Octachlorobiphenyls 9.46 µg/Kg 0.0563 µg/Kg10/18/2001 Comp of Sta 23 600373 4705549 23 0308032-05 Nonachlorobiphenyls 11.3 µg/Kg 0.143 µg/Kg10/18/2001 Comp of Sta 23 600373 4705549 23 0308032-05 Decachlorobiphenyl 0.308 J µg/Kg 0.0670 µg/Kg10/18/2001 Comp of Sta 23 600373 4705549 23 0308032-05 Total Homologs 47.2 µg/Kg 0.0670 µg/Kg10/18/2001 Comp of Sta 23 600373 4705549 23 0308032-05 Percent Lipids 2.8 % 0.1 %10/18/2001 Comp of Sta 23 600373 4705549 23 0308032-05 Percent Moisture 71.4 % 0.1 %


Meadow Vole (Microtus pennsylvanicus) Tissue Hudson NRDA Floodplain DatabaseVersion 2.0

Extracted 7/30/04





9/9/2001 Comp of Sta 2 613552 4761987 2 0308032-06 Cl2-BZ#8 0.118 U µg/Kg 0.118 µg/Kg9/9/2001 Comp of Sta 2 613552 4761987 2 0308032-06 Cl3-BZ#18 0.261 U µg/Kg 0.261 µg/Kg9/9/2001 Comp of Sta 2 613552 4761987 2 0308032-06 Cl3-BZ#31/#28 2.04 J µg/Kg 1.88 µg/Kg9/9/2001 Comp of Sta 2 613552 4761987 2 0308032-06 Cl4-BZ#44 0.179 U µg/Kg 0.179 µg/Kg9/9/2001 Comp of Sta 2 613552 4761987 2 0308032-06 Cl4-BZ#45 0.239 U µg/Kg 0.239 µg/Kg9/9/2001 Comp of Sta 2 613552 4761987 2 0308032-06 Cl4-BZ#47 0.520 J µg/Kg 0.303 µg/Kg9/9/2001 Comp of Sta 2 613552 4761987 2 0308032-06 Cl4-BZ#49 0.417 J µg/Kg 0.149 µg/Kg9/9/2001 Comp of Sta 2 613552 4761987 2 0308032-06 Cl4-BZ#52 0.615 J µg/Kg 0.169 µg/Kg9/9/2001 Comp of Sta 2 613552 4761987 2 0308032-06 Cl4-BZ#56 1.78 µg/Kg 0.0889 µg/Kg9/9/2001 Comp of Sta 2 613552 4761987 2 0308032-06 Cl4-BZ#66 4.05 µg/Kg 0.119 µg/Kg9/9/2001 Comp of Sta 2 613552 4761987 2 0308032-06 Cl4-BZ#70 1.03 µg/Kg 0.104 µg/Kg9/9/2001 Comp of Sta 2 613552 4761987 2 0308032-06 Cl4-BZ#74 1.80 µg/Kg 0.183 µg/Kg9/9/2001 Comp of Sta 2 613552 4761987 2 0308032-06 Cl4-BZ#77 0.164 U µg/Kg 0.164 µg/Kg9/9/2001 Comp of Sta 2 613552 4761987 2 0308032-06 Cl4-BZ#81 0.163 U µg/Kg 0.163 µg/Kg9/9/2001 Comp of Sta 2 613552 4761987 2 0308032-06 Cl5-BZ#87 0.588 µg/Kg 0.0725 µg/Kg9/9/2001 Comp of Sta 2 613552 4761987 2 0308032-06 Cl5-BZ#95 0.116 J µg/Kg 0.0561 µg/Kg9/9/2001 Comp of Sta 2 613552 4761987 2 0308032-06 Cl5-BZ#99 2.02 µg/Kg 0.0383 µg/Kg9/9/2001 Comp of Sta 2 613552 4761987 2 0308032-06 Cl5-BZ#101 0.492 J µg/Kg 0.109 µg/Kg9/9/2001 Comp of Sta 2 613552 4761987 2 0308032-06 Cl5-BZ#105 1.98 µg/Kg 0.0533 µg/Kg9/9/2001 Comp of Sta 2 613552 4761987 2 0308032-06 Cl5-BZ#110 0.342 J µg/Kg 0.104 µg/Kg9/9/2001 Comp of Sta 2 613552 4761987 2 0308032-06 Cl5-BZ#114 0.287 µg/Kg 0.0479 µg/Kg9/9/2001 Comp of Sta 2 613552 4761987 2 0308032-06 Cl5-BZ#118 4.07 µg/Kg 0.112 µg/Kg9/9/2001 Comp of Sta 2 613552 4761987 2 0308032-06 Cl5-BZ#123 0.0943 U µg/Kg 0.0943 µg/Kg9/9/2001 Comp of Sta 2 613552 4761987 2 0308032-06 Cl5-BZ#126 0.0834 U µg/Kg 0.0834 µg/Kg9/9/2001 Comp of Sta 2 613552 4761987 2 0308032-06 Cl6-BZ#128 0.356 J µg/Kg 0.0752 µg/Kg9/9/2001 Comp of Sta 2 613552 4761987 2 0308032-06 Cl6-BZ#138 1.71 µg/Kg 0.108 µg/Kg9/9/2001 Comp of Sta 2 613552 4761987 2 0308032-06 Cl6-BZ#146 0.349 µg/Kg 0.0684 µg/Kg9/9/2001 Comp of Sta 2 613552 4761987 2 0308032-06 Cl6-BZ#149 0.0889 J µg/Kg 0.0875 µg/Kg9/9/2001 Comp of Sta 2 613552 4761987 2 0308032-06 Cl6-BZ#151 0.145 U µg/Kg 0.145 µg/Kg9/9/2001 Comp of Sta 2 613552 4761987 2 0308032-06 Cl6-BZ#153 2.03 µg/Kg 0.124 µg/Kg9/9/2001 Comp of Sta 2 613552 4761987 2 0308032-06 Cl6-BZ#156 0.308 J µg/Kg 0.0889 µg/Kg9/9/2001 Comp of Sta 2 613552 4761987 2 0308032-06 Cl6-BZ#157 0.0697 U µg/Kg 0.0697 µg/Kg9/9/2001 Comp of Sta 2 613552 4761987 2 0308032-06 Cl6-BZ#158 0.0820 J µg/Kg 0.0588 µg/Kg9/9/2001 Comp of Sta 2 613552 4761987 2 0308032-06 Cl6-BZ#167 0.178 J µg/Kg 0.0752 µg/Kg





Extracted 7/30/04







9/9/2001 Comp of Sta 2 613552 4761987 2 0308032-06 Cl6-BZ#169 0.242 U µg/Kg 0.242 µg/Kg9/9/2001 Comp of Sta 2 613552 4761987 2 0308032-06 Cl7-BZ#170 0.827 J µg/Kg 0.282 µg/Kg9/9/2001 Comp of Sta 2 613552 4761987 2 0308032-06 Cl7-BZ#174 0.0574 U µg/Kg 0.0574 µg/Kg9/9/2001 Comp of Sta 2 613552 4761987 2 0308032-06 Cl7-BZ#177 0.0807 U µg/Kg 0.0807 µg/Kg9/9/2001 Comp of Sta 2 613552 4761987 2 0308032-06 Cl7-BZ#180 0.608 µg/Kg 0.120 µg/Kg9/9/2001 Comp of Sta 2 613552 4761987 2 0308032-06 Cl7-BZ#183 0.0752 J µg/Kg 0.0547 µg/Kg9/9/2001 Comp of Sta 2 613552 4761987 2 0308032-06 Cl7-BZ#187 0.479 µg/Kg 0.0602 µg/Kg9/9/2001 Comp of Sta 2 613552 4761987 2 0308032-06 Cl7-BZ#189 0.108 U µg/Kg 0.108 µg/Kg9/9/2001 Comp of Sta 2 613552 4761987 2 0308032-06 Cl8-BZ#194 0.164 J µg/Kg 0.126 µg/Kg9/9/2001 Comp of Sta 2 613552 4761987 2 0308032-06 Cl8-BZ#195 0.124 U µg/Kg 0.124 µg/Kg9/9/2001 Comp of Sta 2 613552 4761987 2 0308032-06 Cl8-BZ#201 0.109 U µg/Kg 0.109 µg/Kg9/9/2001 Comp of Sta 2 613552 4761987 2 0308032-06 Cl9-BZ#206 0.150 J µg/Kg 0.146 µg/Kg9/9/2001 Comp of Sta 2 613552 4761987 2 0308032-06 Cl10-BZ#209 0.0684 U µg/Kg 0.0684 µg/Kg9/9/2001 Comp of Sta 2 613552 4761987 2 0308032-06 Monochlorobiphenyls 4.02 U µg/Kg 4.02 µg/Kg9/9/2001 Comp of Sta 2 613552 4761987 2 0308032-06 Dichlorobiphenyls 0.118 U µg/Kg 0.118 µg/Kg9/9/2001 Comp of Sta 2 613552 4761987 2 0308032-06 Trichlorobiphenyls 2.47 µg/Kg 0.403 µg/Kg9/9/2001 Comp of Sta 2 613552 4761987 2 0308032-06 Tetrachlorobiphenyls 16.3 µg/Kg 0.0629 µg/Kg9/9/2001 Comp of Sta 2 613552 4761987 2 0308032-06 Pentachlorobiphenyls 23.4 µg/Kg 0.0725 µg/Kg9/9/2001 Comp of Sta 2 613552 4761987 2 0308032-06 Hexachlorobiphenyls 5.75 µg/Kg 0.115 µg/Kg9/9/2001 Comp of Sta 2 613552 4761987 2 0308032-06 Heptachlorobiphenyls 2.76 µg/Kg 0.0629 µg/Kg9/9/2001 Comp of Sta 2 613552 4761987 2 0308032-06 Octachlorobiphenyls 0.171 J µg/Kg 0.0574 µg/Kg9/9/2001 Comp of Sta 2 613552 4761987 2 0308032-06 Nonachlorobiphenyls 0.146 U µg/Kg 0.146 µg/Kg9/9/2001 Comp of Sta 2 613552 4761987 2 0308032-06 Decachlorobiphenyl 0.0684 U µg/Kg 0.0684 µg/Kg9/9/2001 Comp of Sta 2 613552 4761987 2 0308032-06 Total Homologs 51.0 µg/Kg 0.0684 µg/Kg9/9/2001 Comp of Sta 2 613552 4761987 2 0308032-06 Percent Lipids 1.3 % 0.1 %9/9/2001 Comp of Sta 2 613552 4761987 2 0308032-06 Percent Moisture 76.6 % 0.1 %

10/4/2001 Comp of Sta 12 (vole) 614851 4790327 12 0308032-07 Cl2-BZ#8 0.129 U µg/Kg 0.129 µg/Kg10/4/2001 Comp of Sta 12 (vole) 614851 4790327 12 0308032-07 Cl3-BZ#18 0.286 U µg/Kg 0.286 µg/Kg10/4/2001 Comp of Sta 12 (vole) 614851 4790327 12 0308032-07 Cl3-BZ#31/#28 20.9 µg/Kg 2.06 µg/Kg10/4/2001 Comp of Sta 12 (vole) 614851 4790327 12 0308032-07 Cl4-BZ#44 0.710 J µg/Kg 0.196 µg/Kg10/4/2001 Comp of Sta 12 (vole) 614851 4790327 12 0308032-07 Cl4-BZ#45 0.262 U µg/Kg 0.262 µg/Kg10/4/2001 Comp of Sta 12 (vole) 614851 4790327 12 0308032-07 Cl4-BZ#47 3.21 µg/Kg 0.332 µg/Kg10/4/2001 Comp of Sta 12 (vole) 614851 4790327 12 0308032-07 Cl4-BZ#49 1.40 µg/Kg 0.163 µg/Kg10/4/2001 Comp of Sta 12 (vole) 614851 4790327 12 0308032-07 Cl4-BZ#52 2.17 µg/Kg 0.185 µg/Kg



Extracted 7/30/04







10/4/2001 Comp of Sta 12 (vole) 614851 4790327 12 0308032-07 Cl4-BZ#56 9.29 µg/Kg 0.0972 µg/Kg10/4/2001 Comp of Sta 12 (vole) 614851 4790327 12 0308032-07 Cl4-BZ#66 19.1 µg/Kg 0.130 µg/Kg10/4/2001 Comp of Sta 12 (vole) 614851 4790327 12 0308032-07 Cl4-BZ#70 4.22 µg/Kg 0.114 µg/Kg10/4/2001 Comp of Sta 12 (vole) 614851 4790327 12 0308032-07 Cl4-BZ#74 16.8 µg/Kg 0.200 µg/Kg10/4/2001 Comp of Sta 12 (vole) 614851 4790327 12 0308032-07 Cl4-BZ#77 0.179 U µg/Kg 0.179 µg/Kg10/4/2001 Comp of Sta 12 (vole) 614851 4790327 12 0308032-07 Cl4-BZ#81 0.178 U µg/Kg 0.178 µg/Kg10/4/2001 Comp of Sta 12 (vole) 614851 4790327 12 0308032-07 Cl5-BZ#87 1.97 µg/Kg 0.0793 µg/Kg10/4/2001 Comp of Sta 12 (vole) 614851 4790327 12 0308032-07 Cl5-BZ#95 0.531 µg/Kg 0.0613 µg/Kg10/4/2001 Comp of Sta 12 (vole) 614851 4790327 12 0308032-07 Cl5-BZ#99 7.04 µg/Kg 0.0419 µg/Kg10/4/2001 Comp of Sta 12 (vole) 614851 4790327 12 0308032-07 Cl5-BZ#101 2.29 µg/Kg 0.120 µg/Kg10/4/2001 Comp of Sta 12 (vole) 614851 4790327 12 0308032-07 Cl5-BZ#105 10.1 µg/Kg 0.0583 µg/Kg10/4/2001 Comp of Sta 12 (vole) 614851 4790327 12 0308032-07 Cl5-BZ#110 1.22 µg/Kg 0.114 µg/Kg10/4/2001 Comp of Sta 12 (vole) 614851 4790327 12 0308032-07 Cl5-BZ#114 1.15 µg/Kg 0.0523 µg/Kg10/4/2001 Comp of Sta 12 (vole) 614851 4790327 12 0308032-07 Cl5-BZ#118 17.4 µg/Kg 0.123 µg/Kg10/4/2001 Comp of Sta 12 (vole) 614851 4790327 12 0308032-07 Cl5-BZ#123 0.103 U µg/Kg 0.103 µg/Kg10/4/2001 Comp of Sta 12 (vole) 614851 4790327 12 0308032-07 Cl5-BZ#126 0.0912 U µg/Kg 0.0912 µg/Kg10/4/2001 Comp of Sta 12 (vole) 614851 4790327 12 0308032-07 Cl6-BZ#128 1.03 µg/Kg 0.0823 µg/Kg10/4/2001 Comp of Sta 12 (vole) 614851 4790327 12 0308032-07 Cl6-BZ#138 5.29 µg/Kg 0.118 µg/Kg10/4/2001 Comp of Sta 12 (vole) 614851 4790327 12 0308032-07 Cl6-BZ#146 1.80 µg/Kg 0.0748 µg/Kg10/4/2001 Comp of Sta 12 (vole) 614851 4790327 12 0308032-07 Cl6-BZ#149 0.456 J µg/Kg 0.0957 µg/Kg10/4/2001 Comp of Sta 12 (vole) 614851 4790327 12 0308032-07 Cl6-BZ#151 0.172 J µg/Kg 0.159 µg/Kg10/4/2001 Comp of Sta 12 (vole) 614851 4790327 12 0308032-07 Cl6-BZ#153 5.12 µg/Kg 0.136 µg/Kg10/4/2001 Comp of Sta 12 (vole) 614851 4790327 12 0308032-07 Cl6-BZ#156 1.51 µg/Kg 0.0972 µg/Kg10/4/2001 Comp of Sta 12 (vole) 614851 4790327 12 0308032-07 Cl6-BZ#157 0.359 J µg/Kg 0.0763 µg/Kg10/4/2001 Comp of Sta 12 (vole) 614851 4790327 12 0308032-07 Cl6-BZ#158 0.179 J µg/Kg 0.0643 µg/Kg10/4/2001 Comp of Sta 12 (vole) 614851 4790327 12 0308032-07 Cl6-BZ#167 0.770 µg/Kg 0.0823 µg/Kg10/4/2001 Comp of Sta 12 (vole) 614851 4790327 12 0308032-07 Cl6-BZ#169 0.265 U µg/Kg 0.265 µg/Kg10/4/2001 Comp of Sta 12 (vole) 614851 4790327 12 0308032-07 Cl7-BZ#170 2.13 µg/Kg 0.308 µg/Kg10/4/2001 Comp of Sta 12 (vole) 614851 4790327 12 0308032-07 Cl7-BZ#174 0.0628 U µg/Kg 0.0628 µg/Kg10/4/2001 Comp of Sta 12 (vole) 614851 4790327 12 0308032-07 Cl7-BZ#177 0.479 µg/Kg 0.0882 µg/Kg10/4/2001 Comp of Sta 12 (vole) 614851 4790327 12 0308032-07 Cl7-BZ#180 2.59 µg/Kg 0.132 µg/Kg10/4/2001 Comp of Sta 12 (vole) 614851 4790327 12 0308032-07 Cl7-BZ#183 0.307 µg/Kg 0.0598 µg/Kg10/4/2001 Comp of Sta 12 (vole) 614851 4790327 12 0308032-07 Cl7-BZ#187 1.80 µg/Kg 0.0658 µg/Kg10/4/2001 Comp of Sta 12 (vole) 614851 4790327 12 0308032-07 Cl7-BZ#189 0.118 U µg/Kg 0.118 µg/Kg



Extracted 7/30/04







10/4/2001 Comp of Sta 12 (vole) 614851 4790327 12 0308032-07 Cl8-BZ#194 0.456 J µg/Kg 0.138 µg/Kg10/4/2001 Comp of Sta 12 (vole) 614851 4790327 12 0308032-07 Cl8-BZ#195 0.187 J µg/Kg 0.136 µg/Kg10/4/2001 Comp of Sta 12 (vole) 614851 4790327 12 0308032-07 Cl8-BZ#201 0.905 µg/Kg 0.120 µg/Kg10/4/2001 Comp of Sta 12 (vole) 614851 4790327 12 0308032-07 Cl9-BZ#206 0.232 J µg/Kg 0.160 µg/Kg10/4/2001 Comp of Sta 12 (vole) 614851 4790327 12 0308032-07 Cl10-BZ#209 0.0748 U µg/Kg 0.0748 µg/Kg10/4/2001 Comp of Sta 12 (vole) 614851 4790327 12 0308032-07 Monochlorobiphenyls 4.40 U µg/Kg 4.40 µg/Kg10/4/2001 Comp of Sta 12 (vole) 614851 4790327 12 0308032-07 Dichlorobiphenyls 0.129 U µg/Kg 0.129 µg/Kg10/4/2001 Comp of Sta 12 (vole) 614851 4790327 12 0308032-07 Trichlorobiphenyls 19.3 µg/Kg 0.441 µg/Kg10/4/2001 Comp of Sta 12 (vole) 614851 4790327 12 0308032-07 Tetrachlorobiphenyls 62.3 µg/Kg 0.0688 µg/Kg10/4/2001 Comp of Sta 12 (vole) 614851 4790327 12 0308032-07 Pentachlorobiphenyls 71.9 µg/Kg 0.0793 µg/Kg10/4/2001 Comp of Sta 12 (vole) 614851 4790327 12 0308032-07 Hexachlorobiphenyls 19.2 µg/Kg 0.126 µg/Kg10/4/2001 Comp of Sta 12 (vole) 614851 4790327 12 0308032-07 Heptachlorobiphenyls 8.00 µg/Kg 0.0688 µg/Kg10/4/2001 Comp of Sta 12 (vole) 614851 4790327 12 0308032-07 Octachlorobiphenyls 1.29 µg/Kg 0.0628 µg/Kg10/4/2001 Comp of Sta 12 (vole) 614851 4790327 12 0308032-07 Nonachlorobiphenyls 2.16 µg/Kg 0.160 µg/Kg10/4/2001 Comp of Sta 12 (vole) 614851 4790327 12 0308032-07 Decachlorobiphenyl 0.0748 U µg/Kg 0.0748 µg/Kg10/4/2001 Comp of Sta 12 (vole) 614851 4790327 12 0308032-07 Total Homologs 184 µg/Kg 0.0748 µg/Kg10/4/2001 Comp of Sta 12 (vole) 614851 4790327 12 0308032-07 Percent Lipids 1.8 % 0.1 %10/4/2001 Comp of Sta 12 (vole) 614851 4790327 12 0308032-07 Percent Moisture 74.1 % 0.1 %

10/10/2001 Comp of Sta 20 (vole) 609713 4741759 20 0308032-08 Cl2-BZ#8 0.122 U µg/Kg 0.122 µg/Kg10/10/2001 Comp of Sta 20 (vole) 609713 4741759 20 0308032-08 Cl3-BZ#18 0.271 U µg/Kg 0.271 µg/Kg10/10/2001 Comp of Sta 20 (vole) 609713 4741759 20 0308032-08 Cl3-BZ#31/#28 21.3 µg/Kg 1.95 µg/Kg10/10/2001 Comp of Sta 20 (vole) 609713 4741759 20 0308032-08 Cl4-BZ#44 1.69 µg/Kg 0.186 µg/Kg10/10/2001 Comp of Sta 20 (vole) 609713 4741759 20 0308032-08 Cl4-BZ#45 0.248 U µg/Kg 0.248 µg/Kg10/10/2001 Comp of Sta 20 (vole) 609713 4741759 20 0308032-08 Cl4-BZ#47 5.08 µg/Kg 0.315 µg/Kg10/10/2001 Comp of Sta 20 (vole) 609713 4741759 20 0308032-08 Cl4-BZ#49 3.15 µg/Kg 0.154 µg/Kg10/10/2001 Comp of Sta 20 (vole) 609713 4741759 20 0308032-08 Cl4-BZ#52 6.66 µg/Kg 0.176 µg/Kg10/10/2001 Comp of Sta 20 (vole) 609713 4741759 20 0308032-08 Cl4-BZ#56 6.44 µg/Kg 0.0921 µg/Kg10/10/2001 Comp of Sta 20 (vole) 609713 4741759 20 0308032-08 Cl4-BZ#66 15.7 µg/Kg 0.123 µg/Kg10/10/2001 Comp of Sta 20 (vole) 609713 4741759 20 0308032-08 Cl4-BZ#70 3.45 µg/Kg 0.108 µg/Kg10/10/2001 Comp of Sta 20 (vole) 609713 4741759 20 0308032-08 Cl4-BZ#74 11.3 µg/Kg 0.190 µg/Kg10/10/2001 Comp of Sta 20 (vole) 609713 4741759 20 0308032-08 Cl4-BZ#77 0.170 U µg/Kg 0.170 µg/Kg10/10/2001 Comp of Sta 20 (vole) 609713 4741759 20 0308032-08 Cl4-BZ#81 0.169 U µg/Kg 0.169 µg/Kg10/10/2001 Comp of Sta 20 (vole) 609713 4741759 20 0308032-08 Cl5-BZ#87 2.24 µg/Kg 0.0751 µg/Kg10/10/2001 Comp of Sta 20 (vole) 609713 4741759 20 0308032-08 Cl5-BZ#95 1.01 µg/Kg 0.0581 µg/Kg



Extracted 7/30/04







10/10/2001 Comp of Sta 20 (vole) 609713 4741759 20 0308032-08 Cl5-BZ#99 4.49 µg/Kg 0.0397 µg/Kg10/10/2001 Comp of Sta 20 (vole) 609713 4741759 20 0308032-08 Cl5-BZ#101 2.64 µg/Kg 0.113 µg/Kg10/10/2001 Comp of Sta 20 (vole) 609713 4741759 20 0308032-08 Cl5-BZ#105 4.37 µg/Kg 0.0553 µg/Kg10/10/2001 Comp of Sta 20 (vole) 609713 4741759 20 0308032-08 Cl5-BZ#110 1.25 µg/Kg 0.108 µg/Kg10/10/2001 Comp of Sta 20 (vole) 609713 4741759 20 0308032-08 Cl5-BZ#114 0.574 µg/Kg 0.0496 µg/Kg10/10/2001 Comp of Sta 20 (vole) 609713 4741759 20 0308032-08 Cl5-BZ#118 7.14 µg/Kg 0.116 µg/Kg10/10/2001 Comp of Sta 20 (vole) 609713 4741759 20 0308032-08 Cl5-BZ#123 0.0978 U µg/Kg 0.0978 µg/Kg10/10/2001 Comp of Sta 20 (vole) 609713 4741759 20 0308032-08 Cl5-BZ#126 0.0865 U µg/Kg 0.0865 µg/Kg10/10/2001 Comp of Sta 20 (vole) 609713 4741759 20 0308032-08 Cl6-BZ#128 0.489 µg/Kg 0.0780 µg/Kg10/10/2001 Comp of Sta 20 (vole) 609713 4741759 20 0308032-08 Cl6-BZ#138 2.47 µg/Kg 0.112 µg/Kg10/10/2001 Comp of Sta 20 (vole) 609713 4741759 20 0308032-08 Cl6-BZ#146 0.780 µg/Kg 0.0709 µg/Kg10/10/2001 Comp of Sta 20 (vole) 609713 4741759 20 0308032-08 Cl6-BZ#149 0.432 J µg/Kg 0.0907 µg/Kg10/10/2001 Comp of Sta 20 (vole) 609713 4741759 20 0308032-08 Cl6-BZ#151 0.262 J µg/Kg 0.150 µg/Kg10/10/2001 Comp of Sta 20 (vole) 609713 4741759 20 0308032-08 Cl6-BZ#153 2.40 µg/Kg 0.129 µg/Kg10/10/2001 Comp of Sta 20 (vole) 609713 4741759 20 0308032-08 Cl6-BZ#156 0.517 µg/Kg 0.0921 µg/Kg10/10/2001 Comp of Sta 20 (vole) 609713 4741759 20 0308032-08 Cl6-BZ#157 0.128 J µg/Kg 0.0723 µg/Kg10/10/2001 Comp of Sta 20 (vole) 609713 4741759 20 0308032-08 Cl6-BZ#158 0.128 J µg/Kg 0.0610 µg/Kg10/10/2001 Comp of Sta 20 (vole) 609713 4741759 20 0308032-08 Cl6-BZ#167 0.269 J µg/Kg 0.0780 µg/Kg10/10/2001 Comp of Sta 20 (vole) 609713 4741759 20 0308032-08 Cl6-BZ#169 0.251 U µg/Kg 0.251 µg/Kg10/10/2001 Comp of Sta 20 (vole) 609713 4741759 20 0308032-08 Cl7-BZ#170 0.292 U µg/Kg 0.292 µg/Kg10/10/2001 Comp of Sta 20 (vole) 609713 4741759 20 0308032-08 Cl7-BZ#174 0.0595 U µg/Kg 0.0595 µg/Kg10/10/2001 Comp of Sta 20 (vole) 609713 4741759 20 0308032-08 Cl7-BZ#177 0.368 J µg/Kg 0.0836 µg/Kg10/10/2001 Comp of Sta 20 (vole) 609713 4741759 20 0308032-08 Cl7-BZ#180 1.21 µg/Kg 0.125 µg/Kg10/10/2001 Comp of Sta 20 (vole) 609713 4741759 20 0308032-08 Cl7-BZ#183 0.149 J µg/Kg 0.0567 µg/Kg10/10/2001 Comp of Sta 20 (vole) 609713 4741759 20 0308032-08 Cl7-BZ#187 1.05 µg/Kg 0.0624 µg/Kg10/10/2001 Comp of Sta 20 (vole) 609713 4741759 20 0308032-08 Cl7-BZ#189 0.112 U µg/Kg 0.112 µg/Kg10/10/2001 Comp of Sta 20 (vole) 609713 4741759 20 0308032-08 Cl8-BZ#194 0.333 J µg/Kg 0.130 µg/Kg10/10/2001 Comp of Sta 20 (vole) 609713 4741759 20 0308032-08 Cl8-BZ#195 0.129 U µg/Kg 0.129 µg/Kg10/10/2001 Comp of Sta 20 (vole) 609713 4741759 20 0308032-08 Cl8-BZ#201 0.113 U µg/Kg 0.113 µg/Kg10/10/2001 Comp of Sta 20 (vole) 609713 4741759 20 0308032-08 Cl9-BZ#206 0.312 J µg/Kg 0.152 µg/Kg10/10/2001 Comp of Sta 20 (vole) 609713 4741759 20 0308032-08 Cl10-BZ#209 0.0709 U µg/Kg 0.0709 µg/Kg10/10/2001 Comp of Sta 20 (vole) 609713 4741759 20 0308032-08 Monochlorobiphenyls 4.17 U µg/Kg 4.17 µg/Kg10/10/2001 Comp of Sta 20 (vole) 609713 4741759 20 0308032-08 Dichlorobiphenyls 0.122 U µg/Kg 0.122 µg/Kg10/10/2001 Comp of Sta 20 (vole) 609713 4741759 20 0308032-08 Trichlorobiphenyls 17.8 µg/Kg 0.418 µg/Kg



Extracted 7/30/04







10/10/2001 Comp of Sta 20 (vole) 609713 4741759 20 0308032-08 Tetrachlorobiphenyls 65.4 µg/Kg 0.0652 µg/Kg10/10/2001 Comp of Sta 20 (vole) 609713 4741759 20 0308032-08 Pentachlorobiphenyls 44.5 µg/Kg 0.0751 µg/Kg10/10/2001 Comp of Sta 20 (vole) 609713 4741759 20 0308032-08 Hexachlorobiphenyls 9.68 µg/Kg 0.119 µg/Kg10/10/2001 Comp of Sta 20 (vole) 609713 4741759 20 0308032-08 Heptachlorobiphenyls 7.34 µg/Kg 0.0652 µg/Kg10/10/2001 Comp of Sta 20 (vole) 609713 4741759 20 0308032-08 Octachlorobiphenyls 0.206 J µg/Kg 0.0595 µg/Kg10/10/2001 Comp of Sta 20 (vole) 609713 4741759 20 0308032-08 Nonachlorobiphenyls 0.312 J µg/Kg 0.152 µg/Kg10/10/2001 Comp of Sta 20 (vole) 609713 4741759 20 0308032-08 Decachlorobiphenyl 0.0709 U µg/Kg 0.0709 µg/Kg10/10/2001 Comp of Sta 20 (vole) 609713 4741759 20 0308032-08 Total Homologs 145 µg/Kg 0.0709 µg/Kg10/10/2001 Comp of Sta 20 (vole) 609713 4741759 20 0308032-08 Percent Lipids 2.2 % 0.1 %10/10/2001 Comp of Sta 20 (vole) 609713 4741759 20 0308032-08 Percent Moisture 75.7 % 0.1 %


HUDSON RIVER



HU

DSO

N R

IVE

R DA

TA R

EP

OR

T: SM

AL

L MA

MM

AL

S AN

D A

ME

RIC

AN

WO

OD

CO

CK C

OL

LE

CT

ION

, AN

AL

YSIS O

F

FL

OO

DP

LA

IN E

AR

TH

WO

RM

S, AN

D R

E-AN

AL

YSIS O

F SE

LE

CT F

LO

OD

PL

AIN

SO

ILS A

ND

SM

AL

L MA

MM

AL

S

APPENDIX F

SOIL AND SHREW (2000) DATA SHEETS

F1: 2000 SOIL DATA SHEETS

F2: 2000 SHORT-TAILED SHREW TISSUE DATA SHEETS

HUDS

ON R

IVER



HU

DSO

N R

IVE

R D

AT

A R

EP

OR

T: S

MA

LL M

AM

MA

LS

AN

D A

ME

RIC

AN

WO

OD

CO

CK

CO

LL

EC

TIO

N, A

NA

LY

SIS

OF

FL

OO

DP

LA

IN E

AR

TH

WO

RM

S, A

ND

RE

-AN

AL

YSI

S O

F S

EL

EC

T F

LO

OD

PL

AIN

SO

ILS

AN

D S

MA

LL M

AM

MA

LS

2000 Soil Data Hudson NRDA Floodplain DatabaseVersion 2.0

Extracted 7/30/04





9/11/2000 7-1-A15 614711 4781148 7 0309086-01 Cl2-BZ#8 275 µg/Kg 6.13 µg/Kg9/11/2000 7-1-A15 614711 4781148 7 0309086-01 Cl3-BZ#18 168 J µg/Kg 4.37 µg/Kg9/11/2000 7-1-A15 614711 4781148 7 0309086-01 Cl3-BZ#31/#28 12400 J µg/Kg 2.07 µg/Kg9/11/2000 7-1-A15 614711 4781148 7 0309086-01 Cl4-BZ#44 6140 µg/Kg 2.64 µg/Kg9/11/2000 7-1-A15 614711 4781148 7 0309086-01 Cl4-BZ#45 1400 µg/Kg 1.03 µg/Kg9/11/2000 7-1-A15 614711 4781148 7 0309086-01 Cl4-BZ#47 3310 µg/Kg 1.68 µg/Kg9/11/2000 7-1-A15 614711 4781148 7 0309086-01 Cl4-BZ#49 7350 µg/Kg 2.95 µg/Kg9/11/2000 7-1-A15 614711 4781148 7 0309086-01 Cl4-BZ#52 9390 J µg/Kg 2.22 µg/Kg9/11/2000 7-1-A15 614711 4781148 7 0309086-01 Cl4-BZ#56 4810 µg/Kg 4.71 µg/Kg9/11/2000 7-1-A15 614711 4781148 7 0309086-01 Cl4-BZ#66 6360 µg/Kg 1.68 µg/Kg9/11/2000 7-1-A15 614711 4781148 7 0309086-01 Cl4-BZ#70 6290 µg/Kg 3.83 µg/Kg9/11/2000 7-1-A15 614711 4781148 7 0309086-01 Cl4-BZ#74 4530 µg/Kg 1.07 µg/Kg9/11/2000 7-1-A15 614711 4781148 7 0309086-01 Cl4-BZ#77 651 NJ µg/Kg 2.07 µg/Kg9/11/2000 7-1-A15 614711 4781148 7 0309086-01 Cl4-BZ#81 2.22 U µg/Kg 2.22 µg/Kg9/11/2000 7-1-A15 614711 4781148 7 0309086-01 Cl5-BZ#87 1650 µg/Kg 1.30 µg/Kg9/11/2000 7-1-A15 614711 4781148 7 0309086-01 Cl5-BZ#95 2330 µg/Kg 0.498 µg/Kg9/11/2000 7-1-A15 614711 4781148 7 0309086-01 Cl5-BZ#99 1850 µg/Kg 0.728 µg/Kg9/11/2000 7-1-A15 614711 4781148 7 0309086-01 Cl5-BZ#101 2190 µg/Kg 0.881 µg/Kg9/11/2000 7-1-A15 614711 4781148 7 0309086-01 Cl5-BZ#105 1390 J µg/Kg 1.30 µg/Kg9/11/2000 7-1-A15 614711 4781148 7 0309086-01 Cl5-BZ#110 2680 µg/Kg 0.881 µg/Kg9/11/2000 7-1-A15 614711 4781148 7 0309086-01 Cl5-BZ#114 122 µg/Kg 0.383 µg/Kg9/11/2000 7-1-A15 614711 4781148 7 0309086-01 Cl5-BZ#118 2540 J µg/Kg 2.34 µg/Kg9/11/2000 7-1-A15 614711 4781148 7 0309086-01 Cl5-BZ#123 1.30 UJ µg/Kg 1.30 µg/Kg9/11/2000 7-1-A15 614711 4781148 7 0309086-01 Cl5-BZ#126 0.996 U µg/Kg 0.996 µg/Kg9/11/2000 7-1-A15 614711 4781148 7 0309086-01 Cl6-BZ#128 162 J µg/Kg 3.45 µg/Kg9/11/2000 7-1-A15 614711 4781148 7 0309086-01 Cl6-BZ#138 915 J µg/Kg 1.84 µg/Kg9/11/2000 7-1-A15 614711 4781148 7 0309086-01 Cl6-BZ#146 143 µg/Kg 0.766 µg/Kg9/11/2000 7-1-A15 614711 4781148 7 0309086-01 Cl6-BZ#149 501 µg/Kg 1.23 µg/Kg9/11/2000 7-1-A15 614711 4781148 7 0309086-01 Cl6-BZ#151 149 µg/Kg 1.49 µg/Kg9/11/2000 7-1-A15 614711 4781148 7 0309086-01 Cl6-BZ#153 470 µg/Kg 2.22 µg/Kg9/11/2000 7-1-A15 614711 4781148 7 0309086-01 Cl6-BZ#156 104 µg/Kg 2.76 µg/Kg9/11/2000 7-1-A15 614711 4781148 7 0309086-01 Cl6-BZ#157 23.0 µg/Kg 2.68 µg/Kg9/11/2000 7-1-A15 614711 4781148 7 0309086-01 Cl6-BZ#158 132 µg/Kg 0.728 µg/Kg9/11/2000 7-1-A15 614711 4781148 7 0309086-01 Cl6-BZ#167 34.0 J µg/Kg 0.958 µg/Kg9/11/2000 7-1-A15 614711 4781148 7 0309086-01 Cl6-BZ#169 2.84 U µg/Kg 2.84 µg/Kg


DETECTION LIMIT3

1BZ#=PCB congener Ballschmiter & Zell number 2U=Non-detected result at the detection limit J/UJ=Estimated result or detection limit 3PCB results & detection limit reported on DRY weight basis 1 of 31


Extracted 7/30/04






DETECTION LIMIT3

9/11/2000 7-1-A15 614711 4781148 7 0309086-01 Cl7-BZ#170 109 µg/Kg 1.38 µg/Kg9/11/2000 7-1-A15 614711 4781148 7 0309086-01 Cl7-BZ#174 88.9 µg/Kg 0.919 µg/Kg9/11/2000 7-1-A15 614711 4781148 7 0309086-01 Cl7-BZ#177 44.6 µg/Kg 0.613 µg/Kg9/11/2000 7-1-A15 614711 4781148 7 0309086-01 Cl7-BZ#180 177 J µg/Kg 1.26 µg/Kg9/11/2000 7-1-A15 614711 4781148 7 0309086-01 Cl7-BZ#183 45.5 J µg/Kg 1.23 µg/Kg9/11/2000 7-1-A15 614711 4781148 7 0309086-01 Cl7-BZ#187 120 µg/Kg 1.26 µg/Kg9/11/2000 7-1-A15 614711 4781148 7 0309086-01 Cl7-BZ#189 6.44 J µg/Kg 1.46 µg/Kg9/11/2000 7-1-A15 614711 4781148 7 0309086-01 Cl8-BZ#194 3.06 J µg/Kg 1.38 µg/Kg9/11/2000 7-1-A15 614711 4781148 7 0309086-01 Cl8-BZ#195 35.4 J µg/Kg 1.38 µg/Kg9/11/2000 7-1-A15 614711 4781148 7 0309086-01 Cl8-BZ#201 41.1 µg/Kg 1.65 µg/Kg9/11/2000 7-1-A15 614711 4781148 7 0309086-01 Cl9-BZ#206 28.0 J µg/Kg 2.11 µg/Kg9/11/2000 7-1-A15 614711 4781148 7 0309086-01 Cl10-BZ#209 4.29 µg/Kg 0.575 µg/Kg9/11/2000 7-1-A15 614711 4781148 7 0309086-01 Monochlorobiphenyls 90.7 µg/Kg 0.996 µg/Kg9/11/2000 7-1-A15 614711 4781148 7 0309086-01 Dichlorobiphenyls 1740 µg/Kg 6.13 µg/Kg9/11/2000 7-1-A15 614711 4781148 7 0309086-01 Trichlorobiphenyls 18000 µg/Kg 1.72 µg/Kg9/11/2000 7-1-A15 614711 4781148 7 0309086-01 Tetrachlorobiphenyls 85000 µg/Kg 2.80 µg/Kg9/11/2000 7-1-A15 614711 4781148 7 0309086-01 Pentachlorobiphenyls 29200 µg/Kg 1.30 µg/Kg9/11/2000 7-1-A15 614711 4781148 7 0309086-01 Hexachlorobiphenyls 3830 µg/Kg 2.34 µg/Kg9/11/2000 7-1-A15 614711 4781148 7 0309086-01 Heptachlorobiphenyls 554 µg/Kg 0.804 µg/Kg9/11/2000 7-1-A15 614711 4781148 7 0309086-01 Octachlorobiphenyls 148 µg/Kg 1.15 µg/Kg9/11/2000 7-1-A15 614711 4781148 7 0309086-01 Nonachlorobiphenyls 80.4 µg/Kg 2.11 µg/Kg9/11/2000 7-1-A15 614711 4781148 7 0309086-01 Decachlorobiphenyl 4.29 µg/Kg 0.575 µg/Kg9/11/2000 7-1-A15 614711 4781148 7 0309086-01 Total Homologs 139000 µg/Kg 1.92 µg/Kg9/11/2000 7-1-A15 614711 4781148 7 0309086-01 Percent Moisture 42.0 % 0.1 %9/11/2000 7-1-B15 614704 4781153 7 0309086-02 Cl2-BZ#8 91.1 µg/Kg 2.53 µg/Kg9/11/2000 7-1-B15 614704 4781153 7 0309086-02 Cl3-BZ#18 89.0 J µg/Kg 1.80 µg/Kg9/11/2000 7-1-B15 614704 4781153 7 0309086-02 Cl3-BZ#31/#28 5290 J µg/Kg 0.854 µg/Kg9/11/2000 7-1-B15 614704 4781153 7 0309086-02 Cl4-BZ#44 1200 µg/Kg 1.09 µg/Kg9/11/2000 7-1-B15 614704 4781153 7 0309086-02 Cl4-BZ#45 156 µg/Kg 0.427 µg/Kg9/11/2000 7-1-B15 614704 4781153 7 0309086-02 Cl4-BZ#47 876 µg/Kg 0.696 µg/Kg9/11/2000 7-1-B15 614704 4781153 7 0309086-02 Cl4-BZ#49 1850 µg/Kg 1.22 µg/Kg9/11/2000 7-1-B15 614704 4781153 7 0309086-02 Cl4-BZ#52 2300 J µg/Kg 0.443 µg/Kg9/11/2000 7-1-B15 614704 4781153 7 0309086-02 Cl4-BZ#56 1650 µg/Kg 1.95 µg/Kg9/11/2000 7-1-B15 614704 4781153 7 0309086-02 Cl4-BZ#66 2260 µg/Kg 0.696 µg/Kg9/11/2000 7-1-B15 614704 4781153 7 0309086-02 Cl4-BZ#70 2280 µg/Kg 1.58 µg/Kg



Extracted 7/30/04






DETECTION LIMIT3

9/11/2000 7-1-B15 614704 4781153 7 0309086-02 Cl4-BZ#74 1800 µg/Kg 0.443 µg/Kg9/11/2000 7-1-B15 614704 4781153 7 0309086-02 Cl4-BZ#77 304 NJ µg/Kg 0.854 µg/Kg9/11/2000 7-1-B15 614704 4781153 7 0309086-02 Cl4-BZ#81 0.917 U µg/Kg 0.917 µg/Kg9/11/2000 7-1-B15 614704 4781153 7 0309086-02 Cl5-BZ#87 754 µg/Kg 0.538 µg/Kg9/11/2000 7-1-B15 614704 4781153 7 0309086-02 Cl5-BZ#95 819 µg/Kg 0.206 µg/Kg9/11/2000 7-1-B15 614704 4781153 7 0309086-02 Cl5-BZ#99 734 µg/Kg 0.301 µg/Kg9/11/2000 7-1-B15 614704 4781153 7 0309086-02 Cl5-BZ#101 1120 µg/Kg 0.364 µg/Kg9/11/2000 7-1-B15 614704 4781153 7 0309086-02 Cl5-BZ#105 866 J µg/Kg 0.538 µg/Kg9/11/2000 7-1-B15 614704 4781153 7 0309086-02 Cl5-BZ#110 1310 µg/Kg 0.364 µg/Kg9/11/2000 7-1-B15 614704 4781153 7 0309086-02 Cl5-BZ#114 72.4 µg/Kg 0.158 µg/Kg9/11/2000 7-1-B15 614704 4781153 7 0309086-02 Cl5-BZ#118 1470 J µg/Kg 0.965 µg/Kg9/11/2000 7-1-B15 614704 4781153 7 0309086-02 Cl5-BZ#123 R µg/Kg 0.538 µg/Kg9/11/2000 7-1-B15 614704 4781153 7 0309086-02 Cl5-BZ#126 0.411 U µg/Kg 0.411 µg/Kg9/11/2000 7-1-B15 614704 4781153 7 0309086-02 Cl6-BZ#128 150 J µg/Kg 1.42 µg/Kg9/11/2000 7-1-B15 614704 4781153 7 0309086-02 Cl6-BZ#138 821 J µg/Kg 0.759 µg/Kg9/11/2000 7-1-B15 614704 4781153 7 0309086-02 Cl6-BZ#146 108 µg/Kg 0.316 µg/Kg9/11/2000 7-1-B15 614704 4781153 7 0309086-02 Cl6-BZ#149 388 µg/Kg 0.506 µg/Kg9/11/2000 7-1-B15 614704 4781153 7 0309086-02 Cl6-BZ#151 99.2 µg/Kg 0.617 µg/Kg9/11/2000 7-1-B15 614704 4781153 7 0309086-02 Cl6-BZ#153 421 µg/Kg 0.917 µg/Kg9/11/2000 7-1-B15 614704 4781153 7 0309086-02 Cl6-BZ#156 101 µg/Kg 1.14 µg/Kg9/11/2000 7-1-B15 614704 4781153 7 0309086-02 Cl6-BZ#157 18.4 µg/Kg 1.11 µg/Kg9/11/2000 7-1-B15 614704 4781153 7 0309086-02 Cl6-BZ#158 105 µg/Kg 0.301 µg/Kg9/11/2000 7-1-B15 614704 4781153 7 0309086-02 Cl6-BZ#167 34.9 J µg/Kg 0.395 µg/Kg9/11/2000 7-1-B15 614704 4781153 7 0309086-02 Cl6-BZ#169 1.17 U µg/Kg 1.17 µg/Kg9/11/2000 7-1-B15 614704 4781153 7 0309086-02 Cl7-BZ#170 115 µg/Kg 0.569 µg/Kg9/11/2000 7-1-B15 614704 4781153 7 0309086-02 Cl7-BZ#174 66.7 µg/Kg 0.380 µg/Kg9/11/2000 7-1-B15 614704 4781153 7 0309086-02 Cl7-BZ#177 32.2 µg/Kg 0.253 µg/Kg9/11/2000 7-1-B15 614704 4781153 7 0309086-02 Cl7-BZ#180 132 J µg/Kg 0.522 µg/Kg9/11/2000 7-1-B15 614704 4781153 7 0309086-02 Cl7-BZ#183 27.3 J µg/Kg 0.506 µg/Kg9/11/2000 7-1-B15 614704 4781153 7 0309086-02 Cl7-BZ#187 79.0 µg/Kg 0.522 µg/Kg9/11/2000 7-1-B15 614704 4781153 7 0309086-02 Cl7-BZ#189 4.36 J µg/Kg 0.601 µg/Kg9/11/2000 7-1-B15 614704 4781153 7 0309086-02 Cl8-BZ#194 1.52 J µg/Kg 0.569 µg/Kg9/11/2000 7-1-B15 614704 4781153 7 0309086-02 Cl8-BZ#195 25.0 J µg/Kg 0.569 µg/Kg9/11/2000 7-1-B15 614704 4781153 7 0309086-02 Cl8-BZ#201 28.6 µg/Kg 0.680 µg/Kg9/11/2000 7-1-B15 614704 4781153 7 0309086-02 Cl9-BZ#206 18.4 J µg/Kg 0.870 µg/Kg



Extracted 7/30/04






DETECTION LIMIT3

9/11/2000 7-1-B15 614704 4781153 7 0309086-02 Cl10-BZ#209 4.24 µg/Kg 0.237 µg/Kg9/11/2000 7-1-B15 614704 4781153 7 0309086-02 Monochlorobiphenyls 22.9 µg/Kg 0.411 µg/Kg9/11/2000 7-1-B15 614704 4781153 7 0309086-02 Dichlorobiphenyls 727 µg/Kg 2.53 µg/Kg9/11/2000 7-1-B15 614704 4781153 7 0309086-02 Trichlorobiphenyls 6470 µg/Kg 0.712 µg/Kg9/11/2000 7-1-B15 614704 4781153 7 0309086-02 Tetrachlorobiphenyls 23600 µg/Kg 1.16 µg/Kg9/11/2000 7-1-B15 614704 4781153 7 0309086-02 Pentachlorobiphenyls 13200 µg/Kg 0.538 µg/Kg9/11/2000 7-1-B15 614704 4781153 7 0309086-02 Hexachlorobiphenyls 2800 µg/Kg 0.965 µg/Kg9/11/2000 7-1-B15 614704 4781153 7 0309086-02 Heptachlorobiphenyls 406 µg/Kg 0.332 µg/Kg9/11/2000 7-1-B15 614704 4781153 7 0309086-02 Octachlorobiphenyls 112 µg/Kg 0.475 µg/Kg9/11/2000 7-1-B15 614704 4781153 7 0309086-02 Nonachlorobiphenyls 48.0 µg/Kg 0.870 µg/Kg9/11/2000 7-1-B15 614704 4781153 7 0309086-02 Decachlorobiphenyl 4.24 µg/Kg 0.237 µg/Kg9/11/2000 7-1-B15 614704 4781153 7 0309086-02 Total Homologs 47400 µg/Kg 0.791 µg/Kg9/11/2000 7-1-B15 614704 4781153 7 0309086-02 Percent Moisture 26.6 % 0.1 %9/11/2000 7-1-B25 614704 4781153 7 0309086-03 Cl2-BZ#8 18.9 J µg/Kg 0.508 µg/Kg9/11/2000 7-1-B25 614704 4781153 7 0309086-03 Cl3-BZ#18 16.7 J µg/Kg 0.362 µg/Kg9/11/2000 7-1-B25 614704 4781153 7 0309086-03 Cl3-BZ#31/#28 731 J µg/Kg 0.172 µg/Kg9/11/2000 7-1-B25 614704 4781153 7 0309086-03 Cl4-BZ#44 168 J µg/Kg 0.219 µg/Kg9/11/2000 7-1-B25 614704 4781153 7 0309086-03 Cl4-BZ#45 17.4 J µg/Kg 0.0858 µg/Kg9/11/2000 7-1-B25 614704 4781153 7 0309086-03 Cl4-BZ#47 130 J µg/Kg 0.140 µg/Kg9/11/2000 7-1-B25 614704 4781153 7 0309086-03 Cl4-BZ#49 289 J µg/Kg 0.245 µg/Kg9/11/2000 7-1-B25 614704 4781153 7 0309086-03 Cl4-BZ#52 457 J µg/Kg 0.0890 µg/Kg9/11/2000 7-1-B25 614704 4781153 7 0309086-03 Cl4-BZ#56 311 J µg/Kg 0.391 µg/Kg9/11/2000 7-1-B25 614704 4781153 7 0309086-03 Cl4-BZ#66 435 J µg/Kg 0.140 µg/Kg9/11/2000 7-1-B25 614704 4781153 7 0309086-03 Cl4-BZ#70 504 J µg/Kg 0.318 µg/Kg9/11/2000 7-1-B25 614704 4781153 7 0309086-03 Cl4-BZ#74 355 J µg/Kg 0.0890 µg/Kg9/11/2000 7-1-B25 614704 4781153 7 0309086-03 Cl4-BZ#77 86.6 NJ µg/Kg 0.172 µg/Kg9/11/2000 7-1-B25 614704 4781153 7 0309086-03 Cl4-BZ#81 0.184 U µg/Kg 0.184 µg/Kg9/11/2000 7-1-B25 614704 4781153 7 0309086-03 Cl5-BZ#87 213 J µg/Kg 0.108 µg/Kg9/11/2000 7-1-B25 614704 4781153 7 0309086-03 Cl5-BZ#95 186 J µg/Kg 0.0413 µg/Kg9/11/2000 7-1-B25 614704 4781153 7 0309086-03 Cl5-BZ#99 143 J µg/Kg 0.0604 µg/Kg9/11/2000 7-1-B25 614704 4781153 7 0309086-03 Cl5-BZ#101 399 J µg/Kg 0.0731 µg/Kg9/11/2000 7-1-B25 614704 4781153 7 0309086-03 Cl5-BZ#105 185 J µg/Kg 0.108 µg/Kg9/11/2000 7-1-B25 614704 4781153 7 0309086-03 Cl5-BZ#110 394 J µg/Kg 0.0731 µg/Kg9/11/2000 7-1-B25 614704 4781153 7 0309086-03 Cl5-BZ#114 16.6 J µg/Kg 0.0318 µg/Kg9/11/2000 7-1-B25 614704 4781153 7 0309086-03 Cl5-BZ#118 384 J µg/Kg 0.194 µg/Kg



Extracted 7/30/04






DETECTION LIMIT3

9/11/2000 7-1-B25 614704 4781153 7 0309086-03 Cl5-BZ#123 0.108 U µg/Kg 0.108 µg/Kg9/11/2000 7-1-B25 614704 4781153 7 0309086-03 Cl5-BZ#126 0.0826 U µg/Kg 0.0826 µg/Kg9/11/2000 7-1-B25 614704 4781153 7 0309086-03 Cl6-BZ#128 38.0 J µg/Kg 0.286 µg/Kg9/11/2000 7-1-B25 614704 4781153 7 0309086-03 Cl6-BZ#138 391 J µg/Kg 0.153 µg/Kg9/11/2000 7-1-B25 614704 4781153 7 0309086-03 Cl6-BZ#146 31.9 J µg/Kg 0.0636 µg/Kg9/11/2000 7-1-B25 614704 4781153 7 0309086-03 Cl6-BZ#149 154 J µg/Kg 0.102 µg/Kg9/11/2000 7-1-B25 614704 4781153 7 0309086-03 Cl6-BZ#151 37.9 J µg/Kg 0.124 µg/Kg9/11/2000 7-1-B25 614704 4781153 7 0309086-03 Cl6-BZ#153 184 J µg/Kg 0.184 µg/Kg9/11/2000 7-1-B25 614704 4781153 7 0309086-03 Cl6-BZ#156 49.3 J µg/Kg 0.229 µg/Kg9/11/2000 7-1-B25 614704 4781153 7 0309086-03 Cl6-BZ#157 7.09 J µg/Kg 0.222 µg/Kg9/11/2000 7-1-B25 614704 4781153 7 0309086-03 Cl6-BZ#158 23.5 J µg/Kg 0.0604 µg/Kg9/11/2000 7-1-B25 614704 4781153 7 0309086-03 Cl6-BZ#167 16.6 J µg/Kg 0.0795 µg/Kg9/11/2000 7-1-B25 614704 4781153 7 0309086-03 Cl6-BZ#169 0.235 U µg/Kg 0.235 µg/Kg9/11/2000 7-1-B25 614704 4781153 7 0309086-03 Cl7-BZ#170 39.4 J µg/Kg 0.114 µg/Kg9/11/2000 7-1-B25 614704 4781153 7 0309086-03 Cl7-BZ#174 23.6 J µg/Kg 0.0763 µg/Kg9/11/2000 7-1-B25 614704 4781153 7 0309086-03 Cl7-BZ#177 15.7 J µg/Kg 0.0509 µg/Kg9/11/2000 7-1-B25 614704 4781153 7 0309086-03 Cl7-BZ#180 45.4 J µg/Kg 0.105 µg/Kg9/11/2000 7-1-B25 614704 4781153 7 0309086-03 Cl7-BZ#183 10.0 J µg/Kg 0.102 µg/Kg9/11/2000 7-1-B25 614704 4781153 7 0309086-03 Cl7-BZ#187 27.3 J µg/Kg 0.105 µg/Kg9/11/2000 7-1-B25 614704 4781153 7 0309086-03 Cl7-BZ#189 1.44 J µg/Kg 0.121 µg/Kg9/11/2000 7-1-B25 614704 4781153 7 0309086-03 Cl8-BZ#194 7.50 J µg/Kg 0.114 µg/Kg9/11/2000 7-1-B25 614704 4781153 7 0309086-03 Cl8-BZ#195 3.13 J µg/Kg 0.114 µg/Kg9/11/2000 7-1-B25 614704 4781153 7 0309086-03 Cl8-BZ#201 10.7 J µg/Kg 0.137 µg/Kg9/11/2000 7-1-B25 614704 4781153 7 0309086-03 Cl9-BZ#206 6.44 J µg/Kg 0.175 µg/Kg9/11/2000 7-1-B25 614704 4781153 7 0309086-03 Cl10-BZ#209 1.27 J µg/Kg 0.0477 µg/Kg9/11/2000 7-1-B25 614704 4781153 7 0309086-03 Monochlorobiphenyls 7.84 J µg/Kg 0.0826 µg/Kg9/11/2000 7-1-B25 614704 4781153 7 0309086-03 Dichlorobiphenyls 153 J µg/Kg 0.508 µg/Kg9/11/2000 7-1-B25 614704 4781153 7 0309086-03 Trichlorobiphenyls 1060 J µg/Kg 0.143 µg/Kg9/11/2000 7-1-B25 614704 4781153 7 0309086-03 Tetrachlorobiphenyls 3500 J µg/Kg 0.232 µg/Kg9/11/2000 7-1-B25 614704 4781153 7 0309086-03 Pentachlorobiphenyls 3470 J µg/Kg 0.108 µg/Kg9/11/2000 7-1-B25 614704 4781153 7 0309086-03 Hexachlorobiphenyls 1190 J µg/Kg 0.194 µg/Kg9/11/2000 7-1-B25 614704 4781153 7 0309086-03 Heptachlorobiphenyls 163 J µg/Kg 0.0667 µg/Kg9/11/2000 7-1-B25 614704 4781153 7 0309086-03 Octachlorobiphenyls 34.4 J µg/Kg 0.0953 µg/Kg9/11/2000 7-1-B25 614704 4781153 7 0309086-03 Nonachlorobiphenyls 36.3 J µg/Kg 0.175 µg/Kg9/11/2000 7-1-B25 614704 4781153 7 0309086-03 Decachlorobiphenyl 1.27 J µg/Kg 0.0477 µg/Kg



Extracted 7/30/04






DETECTION LIMIT3

9/11/2000 7-1-B25 614704 4781153 7 0309086-03 Total Homologs 9620 J µg/Kg 0.159 µg/Kg9/11/2000 7-1-B25 614704 4781153 7 0309086-03 Percent Moisture 23.2 % 0.1 %9/11/2000 7-1-C15 614698 4781158 7 0309086-04 Cl2-BZ#8 6.17 µg/Kg 0.181 µg/Kg9/11/2000 7-1-C15 614698 4781158 7 0309086-04 Cl3-BZ#18 2.43 J µg/Kg 0.129 µg/Kg9/11/2000 7-1-C15 614698 4781158 7 0309086-04 Cl3-BZ#31/#28 80.4 J µg/Kg 0.0611 µg/Kg9/11/2000 7-1-C15 614698 4781158 7 0309086-04 Cl4-BZ#44 6.52 µg/Kg 0.0781 µg/Kg9/11/2000 7-1-C15 614698 4781158 7 0309086-04 Cl4-BZ#45 0.752 µg/Kg 0.0306 µg/Kg9/11/2000 7-1-C15 614698 4781158 7 0309086-04 Cl4-BZ#47 7.90 µg/Kg 0.0498 µg/Kg9/11/2000 7-1-C15 614698 4781158 7 0309086-04 Cl4-BZ#49 33.8 µg/Kg 0.0872 µg/Kg9/11/2000 7-1-C15 614698 4781158 7 0309086-04 Cl4-BZ#52 46.8 J µg/Kg 0.0317 µg/Kg9/11/2000 7-1-C15 614698 4781158 7 0309086-04 Cl4-BZ#56 50.3 µg/Kg 0.139 µg/Kg9/11/2000 7-1-C15 614698 4781158 7 0309086-04 Cl4-BZ#66 87.8 µg/Kg 0.0498 µg/Kg9/11/2000 7-1-C15 614698 4781158 7 0309086-04 Cl4-BZ#70 74.9 µg/Kg 0.113 µg/Kg9/11/2000 7-1-C15 614698 4781158 7 0309086-04 Cl4-BZ#74 61.4 µg/Kg 0.0317 µg/Kg9/11/2000 7-1-C15 614698 4781158 7 0309086-04 Cl4-BZ#77 19.6 NJ µg/Kg 0.0611 µg/Kg9/11/2000 7-1-C15 614698 4781158 7 0309086-04 Cl4-BZ#81 1.30 NJ µg/Kg 0.0657 µg/Kg9/11/2000 7-1-C15 614698 4781158 7 0309086-04 Cl5-BZ#87 24.6 µg/Kg 0.0385 µg/Kg9/11/2000 7-1-C15 614698 4781158 7 0309086-04 Cl5-BZ#95 17.1 µg/Kg 0.0147 µg/Kg9/11/2000 7-1-C15 614698 4781158 7 0309086-04 Cl5-BZ#99 24.5 µg/Kg 0.0215 µg/Kg9/11/2000 7-1-C15 614698 4781158 7 0309086-04 Cl5-BZ#101 44.8 µg/Kg 0.0260 µg/Kg9/11/2000 7-1-C15 614698 4781158 7 0309086-04 Cl5-BZ#105 31.0 J µg/Kg 0.0385 µg/Kg9/11/2000 7-1-C15 614698 4781158 7 0309086-04 Cl5-BZ#110 46.7 µg/Kg 0.0260 µg/Kg9/11/2000 7-1-C15 614698 4781158 7 0309086-04 Cl5-BZ#114 2.02 µg/Kg 0.0113 µg/Kg9/11/2000 7-1-C15 614698 4781158 7 0309086-04 Cl5-BZ#118 54.5 J µg/Kg 0.0691 µg/Kg9/11/2000 7-1-C15 614698 4781158 7 0309086-04 Cl5-BZ#123 0.0385 U µg/Kg 0.0385 µg/Kg9/11/2000 7-1-C15 614698 4781158 7 0309086-04 Cl5-BZ#126 0.380 NJ µg/Kg 0.0294 µg/Kg9/11/2000 7-1-C15 614698 4781158 7 0309086-04 Cl6-BZ#128 2.91 J µg/Kg 0.102 µg/Kg9/11/2000 7-1-C15 614698 4781158 7 0309086-04 Cl6-BZ#138 36.9 J µg/Kg 0.0544 µg/Kg9/11/2000 7-1-C15 614698 4781158 7 0309086-04 Cl6-BZ#146 3.56 µg/Kg 0.0226 µg/Kg9/11/2000 7-1-C15 614698 4781158 7 0309086-04 Cl6-BZ#149 12.4 µg/Kg 0.0362 µg/Kg9/11/2000 7-1-C15 614698 4781158 7 0309086-04 Cl6-BZ#151 4.28 µg/Kg 0.0442 µg/Kg9/11/2000 7-1-C15 614698 4781158 7 0309086-04 Cl6-BZ#153 17.6 µg/Kg 0.0657 µg/Kg9/11/2000 7-1-C15 614698 4781158 7 0309086-04 Cl6-BZ#156 3.70 µg/Kg 0.0815 µg/Kg9/11/2000 7-1-C15 614698 4781158 7 0309086-04 Cl6-BZ#157 0.734 µg/Kg 0.0793 µg/Kg9/11/2000 7-1-C15 614698 4781158 7 0309086-04 Cl6-BZ#158 1.90 µg/Kg 0.0215 µg/Kg



Extracted 7/30/04






DETECTION LIMIT3

9/11/2000 7-1-C15 614698 4781158 7 0309086-04 Cl6-BZ#167 1.63 µg/Kg 0.0283 µg/Kg9/11/2000 7-1-C15 614698 4781158 7 0309086-04 Cl6-BZ#169 0.0838 U µg/Kg 0.0838 µg/Kg9/11/2000 7-1-C15 614698 4781158 7 0309086-04 Cl7-BZ#170 3.86 µg/Kg 0.0408 µg/Kg9/11/2000 7-1-C15 614698 4781158 7 0309086-04 Cl7-BZ#174 3.67 µg/Kg 0.0272 µg/Kg9/11/2000 7-1-C15 614698 4781158 7 0309086-04 Cl7-BZ#177 1.82 µg/Kg 0.0181 µg/Kg9/11/2000 7-1-C15 614698 4781158 7 0309086-04 Cl7-BZ#180 4.90 J µg/Kg 0.0374 µg/Kg9/11/2000 7-1-C15 614698 4781158 7 0309086-04 Cl7-BZ#183 0.775 J µg/Kg 0.0362 µg/Kg9/11/2000 7-1-C15 614698 4781158 7 0309086-04 Cl7-BZ#187 3.67 µg/Kg 0.0374 µg/Kg9/11/2000 7-1-C15 614698 4781158 7 0309086-04 Cl7-BZ#189 0.0430 U µg/Kg 0.0430 µg/Kg9/11/2000 7-1-C15 614698 4781158 7 0309086-04 Cl8-BZ#194 1.04 J µg/Kg 0.0408 µg/Kg9/11/2000 7-1-C15 614698 4781158 7 0309086-04 Cl8-BZ#195 0.471 J µg/Kg 0.0408 µg/Kg9/11/2000 7-1-C15 614698 4781158 7 0309086-04 Cl8-BZ#201 1.68 µg/Kg 0.0487 µg/Kg9/11/2000 7-1-C15 614698 4781158 7 0309086-04 Cl9-BZ#206 0.897 J µg/Kg 0.0623 µg/Kg9/11/2000 7-1-C15 614698 4781158 7 0309086-04 Cl10-BZ#209 0.199 J µg/Kg 0.0170 µg/Kg9/11/2000 7-1-C15 614698 4781158 7 0309086-04 Monochlorobiphenyls 4.07 µg/Kg 0.0294 µg/Kg9/11/2000 7-1-C15 614698 4781158 7 0309086-04 Dichlorobiphenyls 39.9 µg/Kg 0.181 µg/Kg9/11/2000 7-1-C15 614698 4781158 7 0309086-04 Trichlorobiphenyls 144 µg/Kg 0.0510 µg/Kg9/11/2000 7-1-C15 614698 4781158 7 0309086-04 Tetrachlorobiphenyls 484 µg/Kg 0.0827 µg/Kg9/11/2000 7-1-C15 614698 4781158 7 0309086-04 Pentachlorobiphenyls 483 µg/Kg 0.0385 µg/Kg9/11/2000 7-1-C15 614698 4781158 7 0309086-04 Hexachlorobiphenyls 108 µg/Kg 0.0691 µg/Kg9/11/2000 7-1-C15 614698 4781158 7 0309086-04 Heptachlorobiphenyls 18.8 µg/Kg 0.0238 µg/Kg9/11/2000 7-1-C15 614698 4781158 7 0309086-04 Octachlorobiphenyls 4.95 µg/Kg 0.0340 µg/Kg9/11/2000 7-1-C15 614698 4781158 7 0309086-04 Nonachlorobiphenyls 5.71 µg/Kg 0.0623 µg/Kg9/11/2000 7-1-C15 614698 4781158 7 0309086-04 Decachlorobiphenyl 0.199 J µg/Kg 0.0170 µg/Kg9/11/2000 7-1-C15 614698 4781158 7 0309086-04 Total Homologs 1290 µg/Kg 0.0566 µg/Kg9/11/2000 7-1-C15 614698 4781158 7 0309086-04 Percent Moisture 21.0 % 0.1 %9/11/2000 7-1-D15 614693 4781162 7 0309086-05 Cl2-BZ#8 8.40 µg/Kg 0.199 µg/Kg9/11/2000 7-1-D15 614693 4781162 7 0309086-05 Cl3-BZ#18 3.28 J µg/Kg 0.142 µg/Kg9/11/2000 7-1-D15 614693 4781162 7 0309086-05 Cl3-BZ#31/#28 44.8 J µg/Kg 0.0671 µg/Kg9/11/2000 7-1-D15 614693 4781162 7 0309086-05 Cl4-BZ#44 3.88 µg/Kg 0.0857 µg/Kg9/11/2000 7-1-D15 614693 4781162 7 0309086-05 Cl4-BZ#45 0.756 µg/Kg 0.0335 µg/Kg9/11/2000 7-1-D15 614693 4781162 7 0309086-05 Cl4-BZ#47 5.62 µg/Kg 0.0547 µg/Kg9/11/2000 7-1-D15 614693 4781162 7 0309086-05 Cl4-BZ#49 17.2 µg/Kg 0.0957 µg/Kg9/11/2000 7-1-D15 614693 4781162 7 0309086-05 Cl4-BZ#52 16.2 J µg/Kg 0.0348 µg/Kg9/11/2000 7-1-D15 614693 4781162 7 0309086-05 Cl4-BZ#56 29.1 µg/Kg 0.153 µg/Kg



Extracted 7/30/04






DETECTION LIMIT3

9/11/2000 7-1-D15 614693 4781162 7 0309086-05 Cl4-BZ#66 50.7 µg/Kg 0.0547 µg/Kg9/11/2000 7-1-D15 614693 4781162 7 0309086-05 Cl4-BZ#70 52.7 µg/Kg 0.124 µg/Kg9/11/2000 7-1-D15 614693 4781162 7 0309086-05 Cl4-BZ#74 33.2 µg/Kg 0.0348 µg/Kg9/11/2000 7-1-D15 614693 4781162 7 0309086-05 Cl4-BZ#77 13.8 NJ µg/Kg 0.0671 µg/Kg9/11/2000 7-1-D15 614693 4781162 7 0309086-05 Cl4-BZ#81 1.06 NJ µg/Kg 0.0721 µg/Kg9/11/2000 7-1-D15 614693 4781162 7 0309086-05 Cl5-BZ#87 15.4 µg/Kg 0.0422 µg/Kg9/11/2000 7-1-D15 614693 4781162 7 0309086-05 Cl5-BZ#95 6.57 µg/Kg 0.0162 µg/Kg9/11/2000 7-1-D15 614693 4781162 7 0309086-05 Cl5-BZ#99 16.5 µg/Kg 0.0236 µg/Kg9/11/2000 7-1-D15 614693 4781162 7 0309086-05 Cl5-BZ#101 27.7 µg/Kg 0.0286 µg/Kg9/11/2000 7-1-D15 614693 4781162 7 0309086-05 Cl5-BZ#105 26.4 J µg/Kg 0.0422 µg/Kg9/11/2000 7-1-D15 614693 4781162 7 0309086-05 Cl5-BZ#110 25.3 µg/Kg 0.0286 µg/Kg9/11/2000 7-1-D15 614693 4781162 7 0309086-05 Cl5-BZ#114 0.0124 U µg/Kg 0.0124 µg/Kg9/11/2000 7-1-D15 614693 4781162 7 0309086-05 Cl5-BZ#118 43.5 J µg/Kg 0.0758 µg/Kg9/11/2000 7-1-D15 614693 4781162 7 0309086-05 Cl5-BZ#123 0.0422 U µg/Kg 0.0422 µg/Kg9/11/2000 7-1-D15 614693 4781162 7 0309086-05 Cl5-BZ#126 0.0323 U µg/Kg 0.0323 µg/Kg9/11/2000 7-1-D15 614693 4781162 7 0309086-05 Cl6-BZ#128 2.76 J µg/Kg 0.112 µg/Kg9/11/2000 7-1-D15 614693 4781162 7 0309086-05 Cl6-BZ#138 30.9 J µg/Kg 0.0596 µg/Kg9/11/2000 7-1-D15 614693 4781162 7 0309086-05 Cl6-BZ#146 3.00 µg/Kg 0.0249 µg/Kg9/11/2000 7-1-D15 614693 4781162 7 0309086-05 Cl6-BZ#149 8.23 µg/Kg 0.0398 µg/Kg9/11/2000 7-1-D15 614693 4781162 7 0309086-05 Cl6-BZ#151 3.27 µg/Kg 0.0485 µg/Kg9/11/2000 7-1-D15 614693 4781162 7 0309086-05 Cl6-BZ#153 15.2 µg/Kg 0.0721 µg/Kg9/11/2000 7-1-D15 614693 4781162 7 0309086-05 Cl6-BZ#156 3.52 µg/Kg 0.0895 µg/Kg9/11/2000 7-1-D15 614693 4781162 7 0309086-05 Cl6-BZ#157 0.661 µg/Kg 0.0870 µg/Kg9/11/2000 7-1-D15 614693 4781162 7 0309086-05 Cl6-BZ#158 1.72 µg/Kg 0.0236 µg/Kg9/11/2000 7-1-D15 614693 4781162 7 0309086-05 Cl6-BZ#167 1.35 µg/Kg 0.0311 µg/Kg9/11/2000 7-1-D15 614693 4781162 7 0309086-05 Cl6-BZ#169 0.0920 U µg/Kg 0.0920 µg/Kg9/11/2000 7-1-D15 614693 4781162 7 0309086-05 Cl7-BZ#170 3.28 µg/Kg 0.0447 µg/Kg9/11/2000 7-1-D15 614693 4781162 7 0309086-05 Cl7-BZ#174 1.76 µg/Kg 0.0298 µg/Kg9/11/2000 7-1-D15 614693 4781162 7 0309086-05 Cl7-BZ#177 1.51 µg/Kg 0.0199 µg/Kg9/11/2000 7-1-D15 614693 4781162 7 0309086-05 Cl7-BZ#180 3.62 J µg/Kg 0.0410 µg/Kg9/11/2000 7-1-D15 614693 4781162 7 0309086-05 Cl7-BZ#183 0.542 J µg/Kg 0.0398 µg/Kg9/11/2000 7-1-D15 614693 4781162 7 0309086-05 Cl7-BZ#187 3.19 µg/Kg 0.0410 µg/Kg9/11/2000 7-1-D15 614693 4781162 7 0309086-05 Cl7-BZ#189 0.0472 U µg/Kg 0.0472 µg/Kg9/11/2000 7-1-D15 614693 4781162 7 0309086-05 Cl8-BZ#194 0.850 J µg/Kg 0.0447 µg/Kg9/11/2000 7-1-D15 614693 4781162 7 0309086-05 Cl8-BZ#195 0.398 J µg/Kg 0.0447 µg/Kg



Extracted 7/30/04






DETECTION LIMIT3

9/11/2000 7-1-D15 614693 4781162 7 0309086-05 Cl8-BZ#201 1.46 µg/Kg 0.0534 µg/Kg9/11/2000 7-1-D15 614693 4781162 7 0309086-05 Cl9-BZ#206 1.03 J µg/Kg 0.0683 µg/Kg9/11/2000 7-1-D15 614693 4781162 7 0309086-05 Cl10-BZ#209 0.214 J µg/Kg 0.0186 µg/Kg9/11/2000 7-1-D15 614693 4781162 7 0309086-05 Monochlorobiphenyls 5.35 µg/Kg 0.0323 µg/Kg9/11/2000 7-1-D15 614693 4781162 7 0309086-05 Dichlorobiphenyls 30.3 µg/Kg 0.199 µg/Kg9/11/2000 7-1-D15 614693 4781162 7 0309086-05 Trichlorobiphenyls 90.1 µg/Kg 0.0559 µg/Kg9/11/2000 7-1-D15 614693 4781162 7 0309086-05 Tetrachlorobiphenyls 272 µg/Kg 0.0907 µg/Kg9/11/2000 7-1-D15 614693 4781162 7 0309086-05 Pentachlorobiphenyls 306 µg/Kg 0.0422 µg/Kg9/11/2000 7-1-D15 614693 4781162 7 0309086-05 Hexachlorobiphenyls 86.9 µg/Kg 0.0758 µg/Kg9/11/2000 7-1-D15 614693 4781162 7 0309086-05 Heptachlorobiphenyls 13.8 µg/Kg 0.0261 µg/Kg9/11/2000 7-1-D15 614693 4781162 7 0309086-05 Octachlorobiphenyls 4.36 µg/Kg 0.0373 µg/Kg9/11/2000 7-1-D15 614693 4781162 7 0309086-05 Nonachlorobiphenyls 6.18 µg/Kg 0.0683 µg/Kg9/11/2000 7-1-D15 614693 4781162 7 0309086-05 Decachlorobiphenyl 0.214 J µg/Kg 0.0186 µg/Kg9/11/2000 7-1-D15 614693 4781162 7 0309086-05 Total Homologs 816 µg/Kg 0.0621 µg/Kg9/11/2000 7-1-D15 614693 4781162 7 0309086-05 Percent Moisture 25.3 % 0.1 %9/11/2000 7-1-F25 614680 4781172 7 0309086-06 Cl2-BZ#8 0.223 U µg/Kg 0.223 µg/Kg9/11/2000 7-1-F25 614680 4781172 7 0309086-06 Cl3-BZ#18 0.159 UJ µg/Kg 0.159 µg/Kg9/11/2000 7-1-F25 614680 4781172 7 0309086-06 Cl3-BZ#31/#28 0.0753 U µg/Kg 0.0753 µg/Kg9/11/2000 7-1-F25 614680 4781172 7 0309086-06 Cl4-BZ#44 0.485 J µg/Kg 0.0962 µg/Kg9/11/2000 7-1-F25 614680 4781172 7 0309086-06 Cl4-BZ#45 0.362 J µg/Kg 0.0376 µg/Kg9/11/2000 7-1-F25 614680 4781172 7 0309086-06 Cl4-BZ#47 0.658 J µg/Kg 0.0613 µg/Kg9/11/2000 7-1-F25 614680 4781172 7 0309086-06 Cl4-BZ#49 1.11 J µg/Kg 0.107 µg/Kg9/11/2000 7-1-F25 614680 4781172 7 0309086-06 Cl4-BZ#52 1.37 J µg/Kg 0.0390 µg/Kg9/11/2000 7-1-F25 614680 4781172 7 0309086-06 Cl4-BZ#56 1.59 J µg/Kg 0.171 µg/Kg9/11/2000 7-1-F25 614680 4781172 7 0309086-06 Cl4-BZ#66 2.22 J µg/Kg 0.0613 µg/Kg9/11/2000 7-1-F25 614680 4781172 7 0309086-06 Cl4-BZ#70 2.63 J µg/Kg 0.139 µg/Kg9/11/2000 7-1-F25 614680 4781172 7 0309086-06 Cl4-BZ#74 1.48 J µg/Kg 0.0390 µg/Kg9/11/2000 7-1-F25 614680 4781172 7 0309086-06 Cl4-BZ#77 0.0753 U µg/Kg 0.0753 µg/Kg9/11/2000 7-1-F25 614680 4781172 7 0309086-06 Cl4-BZ#81 0.0808 U µg/Kg 0.0808 µg/Kg9/11/2000 7-1-F25 614680 4781172 7 0309086-06 Cl5-BZ#87 0.0474 U µg/Kg 0.0474 µg/Kg9/11/2000 7-1-F25 614680 4781172 7 0309086-06 Cl5-BZ#95 0.0181 U µg/Kg 0.0181 µg/Kg9/11/2000 7-1-F25 614680 4781172 7 0309086-06 Cl5-BZ#99 1.06 J µg/Kg 0.0265 µg/Kg9/11/2000 7-1-F25 614680 4781172 7 0309086-06 Cl5-BZ#101 1.63 J µg/Kg 0.0321 µg/Kg9/11/2000 7-1-F25 614680 4781172 7 0309086-06 Cl5-BZ#105 2.41 J µg/Kg 0.0474 µg/Kg9/11/2000 7-1-F25 614680 4781172 7 0309086-06 Cl5-BZ#110 1.39 J µg/Kg 0.0321 µg/Kg



Extracted 7/30/04






DETECTION LIMIT3

9/11/2000 7-1-F25 614680 4781172 7 0309086-06 Cl5-BZ#114 0.0139 U µg/Kg 0.0139 µg/Kg9/11/2000 7-1-F25 614680 4781172 7 0309086-06 Cl5-BZ#118 3.68 J µg/Kg 0.0850 µg/Kg9/11/2000 7-1-F25 614680 4781172 7 0309086-06 Cl5-BZ#123 0.0474 U µg/Kg 0.0474 µg/Kg9/11/2000 7-1-F25 614680 4781172 7 0309086-06 Cl5-BZ#126 0.0362 U µg/Kg 0.0362 µg/Kg9/11/2000 7-1-F25 614680 4781172 7 0309086-06 Cl6-BZ#128 0.859 J µg/Kg 0.125 µg/Kg9/11/2000 7-1-F25 614680 4781172 7 0309086-06 Cl6-BZ#138 4.72 J µg/Kg 0.0669 µg/Kg9/11/2000 7-1-F25 614680 4781172 7 0309086-06 Cl6-BZ#146 0.418 J µg/Kg 0.0279 µg/Kg9/11/2000 7-1-F25 614680 4781172 7 0309086-06 Cl6-BZ#149 0.814 J µg/Kg 0.0446 µg/Kg9/11/2000 7-1-F25 614680 4781172 7 0309086-06 Cl6-BZ#151 0.814 J µg/Kg 0.0544 µg/Kg9/11/2000 7-1-F25 614680 4781172 7 0309086-06 Cl6-BZ#153 2.02 J µg/Kg 0.0808 µg/Kg9/11/2000 7-1-F25 614680 4781172 7 0309086-06 Cl6-BZ#156 2.43 J µg/Kg 0.100 µg/Kg9/11/2000 7-1-F25 614680 4781172 7 0309086-06 Cl6-BZ#157 0.0976 U µg/Kg 0.0976 µg/Kg9/11/2000 7-1-F25 614680 4781172 7 0309086-06 Cl6-BZ#158 0.268 J µg/Kg 0.0265 µg/Kg9/11/2000 7-1-F25 614680 4781172 7 0309086-06 Cl6-BZ#167 1.04 J µg/Kg 0.0348 µg/Kg9/11/2000 7-1-F25 614680 4781172 7 0309086-06 Cl6-BZ#169 0.103 U µg/Kg 0.103 µg/Kg9/11/2000 7-1-F25 614680 4781172 7 0309086-06 Cl7-BZ#170 0.881 J µg/Kg 0.0502 µg/Kg9/11/2000 7-1-F25 614680 4781172 7 0309086-06 Cl7-BZ#174 0.290 J µg/Kg 0.0334 µg/Kg9/11/2000 7-1-F25 614680 4781172 7 0309086-06 Cl7-BZ#177 0.485 J µg/Kg 0.0223 µg/Kg9/11/2000 7-1-F25 614680 4781172 7 0309086-06 Cl7-BZ#180 0.714 J µg/Kg 0.0460 µg/Kg9/11/2000 7-1-F25 614680 4781172 7 0309086-06 Cl7-BZ#183 0.139 J µg/Kg 0.0446 µg/Kg9/11/2000 7-1-F25 614680 4781172 7 0309086-06 Cl7-BZ#187 0.379 J µg/Kg 0.0460 µg/Kg9/11/2000 7-1-F25 614680 4781172 7 0309086-06 Cl7-BZ#189 0.0530 U µg/Kg 0.0530 µg/Kg9/11/2000 7-1-F25 614680 4781172 7 0309086-06 Cl8-BZ#194 0.0502 UJ µg/Kg 0.0502 µg/Kg9/11/2000 7-1-F25 614680 4781172 7 0309086-06 Cl8-BZ#195 0.0502 UJ µg/Kg 0.0502 µg/Kg9/11/2000 7-1-F25 614680 4781172 7 0309086-06 Cl8-BZ#201 0.0599 U µg/Kg 0.0599 µg/Kg9/11/2000 7-1-F25 614680 4781172 7 0309086-06 Cl9-BZ#206 0.0767 UJ µg/Kg 0.0767 µg/Kg9/11/2000 7-1-F25 614680 4781172 7 0309086-06 Cl10-BZ#209 0.0209 U µg/Kg 0.0209 µg/Kg9/11/2000 7-1-F25 614680 4781172 7 0309086-06 Monochlorobiphenyls 0.0362 U µg/Kg 0.0362 µg/Kg9/11/2000 7-1-F25 614680 4781172 7 0309086-06 Dichlorobiphenyls 0.223 U µg/Kg 0.223 µg/Kg9/11/2000 7-1-F25 614680 4781172 7 0309086-06 Trichlorobiphenyls 0.0627 U µg/Kg 0.0627 µg/Kg9/11/2000 7-1-F25 614680 4781172 7 0309086-06 Tetrachlorobiphenyls 17.9 J µg/Kg 0.102 µg/Kg9/11/2000 7-1-F25 614680 4781172 7 0309086-06 Pentachlorobiphenyls 57.4 J µg/Kg 0.0474 µg/Kg9/11/2000 7-1-F25 614680 4781172 7 0309086-06 Hexachlorobiphenyls 26.6 J µg/Kg 0.0850 µg/Kg9/11/2000 7-1-F25 614680 4781172 7 0309086-06 Heptachlorobiphenyls 4.56 J µg/Kg 0.0293 µg/Kg9/11/2000 7-1-F25 614680 4781172 7 0309086-06 Octachlorobiphenyls 0.0418 U µg/Kg 0.0418 µg/Kg



Extracted 7/30/04






DETECTION LIMIT3

9/11/2000 7-1-F25 614680 4781172 7 0309086-06 Nonachlorobiphenyls 0.0767 U µg/Kg 0.0767 µg/Kg9/11/2000 7-1-F25 614680 4781172 7 0309086-06 Decachlorobiphenyl 0.0209 U µg/Kg 0.0209 µg/Kg9/11/2000 7-1-F25 614680 4781172 7 0309086-06 Total Homologs 106 J µg/Kg 0.0697 µg/Kg9/11/2000 7-1-F25 614680 4781172 7 0309086-06 Percent Moisture 22.9 % 0.1 %9/11/2000 8-1-A15 614820 4783325 8 0309086-07 Cl2-BZ#8 158 J µg/Kg 2.64 µg/Kg9/11/2000 8-1-A15 614820 4783325 8 0309086-07 Cl3-BZ#18 89.2 J µg/Kg 1.88 µg/Kg9/11/2000 8-1-A15 614820 4783325 8 0309086-07 Cl3-BZ#31/#28 3140 J µg/Kg 0.891 µg/Kg9/11/2000 8-1-A15 614820 4783325 8 0309086-07 Cl4-BZ#44 924 µg/Kg 1.14 µg/Kg9/11/2000 8-1-A15 614820 4783325 8 0309086-07 Cl4-BZ#45 200 µg/Kg 0.446 µg/Kg9/11/2000 8-1-A15 614820 4783325 8 0309086-07 Cl4-BZ#47 673 µg/Kg 0.726 µg/Kg9/11/2000 8-1-A15 614820 4783325 8 0309086-07 Cl4-BZ#49 1270 µg/Kg 1.27 µg/Kg9/11/2000 8-1-A15 614820 4783325 8 0309086-07 Cl4-BZ#52 1440 J µg/Kg 0.462 µg/Kg9/11/2000 8-1-A15 614820 4783325 8 0309086-07 Cl4-BZ#56 1060 µg/Kg 2.03 µg/Kg9/11/2000 8-1-A15 614820 4783325 8 0309086-07 Cl4-BZ#66 1360 µg/Kg 0.726 µg/Kg9/11/2000 8-1-A15 614820 4783325 8 0309086-07 Cl4-BZ#70 1200 µg/Kg 1.65 µg/Kg9/11/2000 8-1-A15 614820 4783325 8 0309086-07 Cl4-BZ#74 1010 µg/Kg 0.462 µg/Kg9/11/2000 8-1-A15 614820 4783325 8 0309086-07 Cl4-BZ#77 149 NJ µg/Kg 0.891 µg/Kg9/11/2000 8-1-A15 614820 4783325 8 0309086-07 Cl4-BZ#81 0.957 U µg/Kg 0.957 µg/Kg9/11/2000 8-1-A15 614820 4783325 8 0309086-07 Cl5-BZ#87 321 µg/Kg 0.561 µg/Kg9/11/2000 8-1-A15 614820 4783325 8 0309086-07 Cl5-BZ#95 415 µg/Kg 0.215 µg/Kg9/11/2000 8-1-A15 614820 4783325 8 0309086-07 Cl5-BZ#99 370 µg/Kg 0.314 µg/Kg9/11/2000 8-1-A15 614820 4783325 8 0309086-07 Cl5-BZ#101 442 µg/Kg 0.380 µg/Kg9/11/2000 8-1-A15 614820 4783325 8 0309086-07 Cl5-BZ#105 278 J µg/Kg 0.561 µg/Kg9/11/2000 8-1-A15 614820 4783325 8 0309086-07 Cl5-BZ#110 532 µg/Kg 0.380 µg/Kg9/11/2000 8-1-A15 614820 4783325 8 0309086-07 Cl5-BZ#114 43.7 µg/Kg 0.165 µg/Kg9/11/2000 8-1-A15 614820 4783325 8 0309086-07 Cl5-BZ#118 526 J µg/Kg 1.01 µg/Kg9/11/2000 8-1-A15 614820 4783325 8 0309086-07 Cl5-BZ#123 0.561 UJ µg/Kg 0.561 µg/Kg9/11/2000 8-1-A15 614820 4783325 8 0309086-07 Cl5-BZ#126 0.429 U µg/Kg 0.429 µg/Kg9/11/2000 8-1-A15 614820 4783325 8 0309086-07 Cl6-BZ#128 31.4 J µg/Kg 1.48 µg/Kg9/11/2000 8-1-A15 614820 4783325 8 0309086-07 Cl6-BZ#138 179 J µg/Kg 0.792 µg/Kg9/11/2000 8-1-A15 614820 4783325 8 0309086-07 Cl6-BZ#146 30.5 µg/Kg 0.330 µg/Kg9/11/2000 8-1-A15 614820 4783325 8 0309086-07 Cl6-BZ#149 100 µg/Kg 0.528 µg/Kg9/11/2000 8-1-A15 614820 4783325 8 0309086-07 Cl6-BZ#151 32.9 µg/Kg 0.644 µg/Kg9/11/2000 8-1-A15 614820 4783325 8 0309086-07 Cl6-BZ#153 89.2 µg/Kg 0.957 µg/Kg9/11/2000 8-1-A15 614820 4783325 8 0309086-07 Cl6-BZ#156 23.0 µg/Kg 1.19 µg/Kg



Extracted 7/30/04






DETECTION LIMIT3

9/11/2000 8-1-A15 614820 4783325 8 0309086-07 Cl6-BZ#157 4.29 J µg/Kg 1.16 µg/Kg9/11/2000 8-1-A15 614820 4783325 8 0309086-07 Cl6-BZ#158 26.1 µg/Kg 0.314 µg/Kg9/11/2000 8-1-A15 614820 4783325 8 0309086-07 Cl6-BZ#167 7.20 J µg/Kg 0.413 µg/Kg9/11/2000 8-1-A15 614820 4783325 8 0309086-07 Cl6-BZ#169 1.22 U µg/Kg 1.22 µg/Kg9/11/2000 8-1-A15 614820 4783325 8 0309086-07 Cl7-BZ#170 28.1 µg/Kg 0.594 µg/Kg9/11/2000 8-1-A15 614820 4783325 8 0309086-07 Cl7-BZ#174 15.7 µg/Kg 0.396 µg/Kg9/11/2000 8-1-A15 614820 4783325 8 0309086-07 Cl7-BZ#177 10.4 µg/Kg 0.264 µg/Kg9/11/2000 8-1-A15 614820 4783325 8 0309086-07 Cl7-BZ#180 34.7 J µg/Kg 0.545 µg/Kg9/11/2000 8-1-A15 614820 4783325 8 0309086-07 Cl7-BZ#183 9.97 J µg/Kg 0.528 µg/Kg9/11/2000 8-1-A15 614820 4783325 8 0309086-07 Cl7-BZ#187 25.6 µg/Kg 0.545 µg/Kg9/11/2000 8-1-A15 614820 4783325 8 0309086-07 Cl7-BZ#189 1.85 J µg/Kg 0.627 µg/Kg9/11/2000 8-1-A15 614820 4783325 8 0309086-07 Cl8-BZ#194 0.594 UJ µg/Kg 0.594 µg/Kg9/11/2000 8-1-A15 614820 4783325 8 0309086-07 Cl8-BZ#195 8.45 J µg/Kg 0.594 µg/Kg9/11/2000 8-1-A15 614820 4783325 8 0309086-07 Cl8-BZ#201 9.24 µg/Kg 0.710 µg/Kg9/11/2000 8-1-A15 614820 4783325 8 0309086-07 Cl9-BZ#206 5.35 J µg/Kg 0.908 µg/Kg9/11/2000 8-1-A15 614820 4783325 8 0309086-07 Cl10-BZ#209 1.45 µg/Kg 0.248 µg/Kg9/11/2000 8-1-A15 614820 4783325 8 0309086-07 Monochlorobiphenyls 92.4 µg/Kg 0.429 µg/Kg9/11/2000 8-1-A15 614820 4783325 8 0309086-07 Dichlorobiphenyls 773 µg/Kg 2.64 µg/Kg9/11/2000 8-1-A15 614820 4783325 8 0309086-07 Trichlorobiphenyls 4680 µg/Kg 0.743 µg/Kg9/11/2000 8-1-A15 614820 4783325 8 0309086-07 Tetrachlorobiphenyls 16500 µg/Kg 1.20 µg/Kg9/11/2000 8-1-A15 614820 4783325 8 0309086-07 Pentachlorobiphenyls 5890 µg/Kg 0.561 µg/Kg9/11/2000 8-1-A15 614820 4783325 8 0309086-07 Hexachlorobiphenyls 721 µg/Kg 1.01 µg/Kg9/11/2000 8-1-A15 614820 4783325 8 0309086-07 Heptachlorobiphenyls 123 µg/Kg 0.347 µg/Kg9/11/2000 8-1-A15 614820 4783325 8 0309086-07 Octachlorobiphenyls 38.9 µg/Kg 0.495 µg/Kg9/11/2000 8-1-A15 614820 4783325 8 0309086-07 Nonachlorobiphenyls 20.9 µg/Kg 0.908 µg/Kg9/11/2000 8-1-A15 614820 4783325 8 0309086-07 Decachlorobiphenyl 1.45 µg/Kg 0.248 µg/Kg9/11/2000 8-1-A15 614820 4783325 8 0309086-07 Total Homologs 28800 µg/Kg 0.825 µg/Kg9/11/2000 8-1-A15 614820 4783325 8 0309086-07 Percent Moisture 35.0 % 0.1 %9/11/2000 8-1-B15 614813 4783327 8 0309086-08 Cl2-BZ#8 510 µg/Kg 2.74 µg/Kg9/11/2000 8-1-B15 614813 4783327 8 0309086-08 Cl3-BZ#18 132 J µg/Kg 1.95 µg/Kg9/11/2000 8-1-B15 614813 4783327 8 0309086-08 Cl3-BZ#31/#28 5830 J µg/Kg 0.925 µg/Kg9/11/2000 8-1-B15 614813 4783327 8 0309086-08 Cl4-BZ#44 1250 µg/Kg 1.18 µg/Kg9/11/2000 8-1-B15 614813 4783327 8 0309086-08 Cl4-BZ#45 227 µg/Kg 0.463 µg/Kg9/11/2000 8-1-B15 614813 4783327 8 0309086-08 Cl4-BZ#47 988 µg/Kg 0.754 µg/Kg9/11/2000 8-1-B15 614813 4783327 8 0309086-08 Cl4-BZ#49 1680 µg/Kg 1.32 µg/Kg



Extracted 7/30/04






DETECTION LIMIT3

9/11/2000 8-1-B15 614813 4783327 8 0309086-08 Cl4-BZ#52 2050 J µg/Kg 0.480 µg/Kg9/11/2000 8-1-B15 614813 4783327 8 0309086-08 Cl4-BZ#56 1530 µg/Kg 2.11 µg/Kg9/11/2000 8-1-B15 614813 4783327 8 0309086-08 Cl4-BZ#66 2000 µg/Kg 0.754 µg/Kg9/11/2000 8-1-B15 614813 4783327 8 0309086-08 Cl4-BZ#70 1920 µg/Kg 1.71 µg/Kg9/11/2000 8-1-B15 614813 4783327 8 0309086-08 Cl4-BZ#74 1620 µg/Kg 0.480 µg/Kg9/11/2000 8-1-B15 614813 4783327 8 0309086-08 Cl4-BZ#77 227 NJ µg/Kg 0.925 µg/Kg9/11/2000 8-1-B15 614813 4783327 8 0309086-08 Cl4-BZ#81 0.994 U µg/Kg 0.994 µg/Kg9/11/2000 8-1-B15 614813 4783327 8 0309086-08 Cl5-BZ#87 466 µg/Kg 0.582 µg/Kg9/11/2000 8-1-B15 614813 4783327 8 0309086-08 Cl5-BZ#95 631 µg/Kg 0.223 µg/Kg9/11/2000 8-1-B15 614813 4783327 8 0309086-08 Cl5-BZ#99 516 µg/Kg 0.326 µg/Kg9/11/2000 8-1-B15 614813 4783327 8 0309086-08 Cl5-BZ#101 649 µg/Kg 0.394 µg/Kg9/11/2000 8-1-B15 614813 4783327 8 0309086-08 Cl5-BZ#105 443 J µg/Kg 0.582 µg/Kg9/11/2000 8-1-B15 614813 4783327 8 0309086-08 Cl5-BZ#110 781 µg/Kg 0.394 µg/Kg9/11/2000 8-1-B15 614813 4783327 8 0309086-08 Cl5-BZ#114 71.5 µg/Kg 0.171 µg/Kg9/11/2000 8-1-B15 614813 4783327 8 0309086-08 Cl5-BZ#118 803 J µg/Kg 1.04 µg/Kg9/11/2000 8-1-B15 614813 4783327 8 0309086-08 Cl5-BZ#123 0.582 UJ µg/Kg 0.582 µg/Kg9/11/2000 8-1-B15 614813 4783327 8 0309086-08 Cl5-BZ#126 0.445 U µg/Kg 0.445 µg/Kg9/11/2000 8-1-B15 614813 4783327 8 0309086-08 Cl6-BZ#128 55.0 J µg/Kg 1.54 µg/Kg9/11/2000 8-1-B15 614813 4783327 8 0309086-08 Cl6-BZ#138 304 J µg/Kg 0.822 µg/Kg9/11/2000 8-1-B15 614813 4783327 8 0309086-08 Cl6-BZ#146 48.1 µg/Kg 0.343 µg/Kg9/11/2000 8-1-B15 614813 4783327 8 0309086-08 Cl6-BZ#149 170 µg/Kg 0.548 µg/Kg9/11/2000 8-1-B15 614813 4783327 8 0309086-08 Cl6-BZ#151 53.3 µg/Kg 0.668 µg/Kg9/11/2000 8-1-B15 614813 4783327 8 0309086-08 Cl6-BZ#153 155 µg/Kg 0.994 µg/Kg9/11/2000 8-1-B15 614813 4783327 8 0309086-08 Cl6-BZ#156 42.3 µg/Kg 1.23 µg/Kg9/11/2000 8-1-B15 614813 4783327 8 0309086-08 Cl6-BZ#157 6.78 µg/Kg 1.20 µg/Kg9/11/2000 8-1-B15 614813 4783327 8 0309086-08 Cl6-BZ#158 50.0 µg/Kg 0.326 µg/Kg9/11/2000 8-1-B15 614813 4783327 8 0309086-08 Cl6-BZ#167 12.9 J µg/Kg 0.428 µg/Kg9/11/2000 8-1-B15 614813 4783327 8 0309086-08 Cl6-BZ#169 1.27 U µg/Kg 1.27 µg/Kg9/11/2000 8-1-B15 614813 4783327 8 0309086-08 Cl7-BZ#170 44.1 µg/Kg 0.617 µg/Kg9/11/2000 8-1-B15 614813 4783327 8 0309086-08 Cl7-BZ#174 27.7 µg/Kg 0.411 µg/Kg9/11/2000 8-1-B15 614813 4783327 8 0309086-08 Cl7-BZ#177 15.3 µg/Kg 0.274 µg/Kg9/11/2000 8-1-B15 614813 4783327 8 0309086-08 Cl7-BZ#180 59.2 J µg/Kg 0.565 µg/Kg9/11/2000 8-1-B15 614813 4783327 8 0309086-08 Cl7-BZ#183 14.5 J µg/Kg 0.548 µg/Kg9/11/2000 8-1-B15 614813 4783327 8 0309086-08 Cl7-BZ#187 41.1 µg/Kg 0.565 µg/Kg9/11/2000 8-1-B15 614813 4783327 8 0309086-08 Cl7-BZ#189 3.29 µg/Kg 0.651 µg/Kg



Extracted 7/30/04






DETECTION LIMIT3

9/11/2000 8-1-B15 614813 4783327 8 0309086-08 Cl8-BZ#194 0.617 UJ µg/Kg 0.617 µg/Kg9/11/2000 8-1-B15 614813 4783327 8 0309086-08 Cl8-BZ#195 16.4 J µg/Kg 0.617 µg/Kg9/11/2000 8-1-B15 614813 4783327 8 0309086-08 Cl8-BZ#201 13.8 µg/Kg 0.737 µg/Kg9/11/2000 8-1-B15 614813 4783327 8 0309086-08 Cl9-BZ#206 9.12 J µg/Kg 0.942 µg/Kg9/11/2000 8-1-B15 614813 4783327 8 0309086-08 Cl10-BZ#209 2.26 µg/Kg 0.257 µg/Kg9/11/2000 8-1-B15 614813 4783327 8 0309086-08 Monochlorobiphenyls 176 µg/Kg 0.445 µg/Kg9/11/2000 8-1-B15 614813 4783327 8 0309086-08 Dichlorobiphenyls 1990 µg/Kg 2.74 µg/Kg9/11/2000 8-1-B15 614813 4783327 8 0309086-08 Trichlorobiphenyls 7780 µg/Kg 0.771 µg/Kg9/11/2000 8-1-B15 614813 4783327 8 0309086-08 Tetrachlorobiphenyls 22300 µg/Kg 1.25 µg/Kg9/11/2000 8-1-B15 614813 4783327 8 0309086-08 Pentachlorobiphenyls 8530 µg/Kg 0.582 µg/Kg9/11/2000 8-1-B15 614813 4783327 8 0309086-08 Hexachlorobiphenyls 1170 µg/Kg 1.04 µg/Kg9/11/2000 8-1-B15 614813 4783327 8 0309086-08 Heptachlorobiphenyls 190 µg/Kg 0.360 µg/Kg9/11/2000 8-1-B15 614813 4783327 8 0309086-08 Octachlorobiphenyls 56.5 µg/Kg 0.514 µg/Kg9/11/2000 8-1-B15 614813 4783327 8 0309086-08 Nonachlorobiphenyls 23.9 µg/Kg 0.942 µg/Kg9/11/2000 8-1-B15 614813 4783327 8 0309086-08 Decachlorobiphenyl 2.26 µg/Kg 0.257 µg/Kg9/11/2000 8-1-B15 614813 4783327 8 0309086-08 Total Homologs 42200 µg/Kg 0.857 µg/Kg9/11/2000 8-1-B15 614813 4783327 8 0309086-08 Percent Moisture 29.3 % 0.1 %9/11/2000 8-1-B25 614813 4783327 8 0309086-09 Cl2-BZ#8 1150 µg/Kg 10.0 µg/Kg9/11/2000 8-1-B25 614813 4783327 8 0309086-09 Cl3-BZ#18 301 J µg/Kg 7.16 µg/Kg9/11/2000 8-1-B25 614813 4783327 8 0309086-09 Cl3-BZ#31/#28 11400 J µg/Kg 3.39 µg/Kg9/11/2000 8-1-B25 614813 4783327 8 0309086-09 Cl4-BZ#44 2840 µg/Kg 4.33 µg/Kg9/11/2000 8-1-B25 614813 4783327 8 0309086-09 Cl4-BZ#45 730 µg/Kg 1.69 µg/Kg9/11/2000 8-1-B25 614813 4783327 8 0309086-09 Cl4-BZ#47 2450 µg/Kg 2.76 µg/Kg9/11/2000 8-1-B25 614813 4783327 8 0309086-09 Cl4-BZ#49 3530 µg/Kg 4.83 µg/Kg9/11/2000 8-1-B25 614813 4783327 8 0309086-09 Cl4-BZ#52 4890 J µg/Kg 1.76 µg/Kg9/11/2000 8-1-B25 614813 4783327 8 0309086-09 Cl4-BZ#56 2990 µg/Kg 7.72 µg/Kg9/11/2000 8-1-B25 614813 4783327 8 0309086-09 Cl4-BZ#66 3730 µg/Kg 2.76 µg/Kg9/11/2000 8-1-B25 614813 4783327 8 0309086-09 Cl4-BZ#70 4120 µg/Kg 6.28 µg/Kg9/11/2000 8-1-B25 614813 4783327 8 0309086-09 Cl4-BZ#74 2760 µg/Kg 1.76 µg/Kg9/11/2000 8-1-B25 614813 4783327 8 0309086-09 Cl4-BZ#77 400 NJ µg/Kg 3.39 µg/Kg9/11/2000 8-1-B25 614813 4783327 8 0309086-09 Cl4-BZ#81 3.64 U µg/Kg 3.64 µg/Kg9/11/2000 8-1-B25 614813 4783327 8 0309086-09 Cl5-BZ#87 860 µg/Kg 2.13 µg/Kg9/11/2000 8-1-B25 614813 4783327 8 0309086-09 Cl5-BZ#95 1300 µg/Kg 0.816 µg/Kg9/11/2000 8-1-B25 614813 4783327 8 0309086-09 Cl5-BZ#99 1070 µg/Kg 1.19 µg/Kg9/11/2000 8-1-B25 614813 4783327 8 0309086-09 Cl5-BZ#101 1210 µg/Kg 1.44 µg/Kg



Extracted 7/30/04






DETECTION LIMIT3

9/11/2000 8-1-B25 614813 4783327 8 0309086-09 Cl5-BZ#105 706 J µg/Kg 2.13 µg/Kg9/11/2000 8-1-B25 614813 4783327 8 0309086-09 Cl5-BZ#110 1480 µg/Kg 1.44 µg/Kg9/11/2000 8-1-B25 614813 4783327 8 0309086-09 Cl5-BZ#114 162 µg/Kg 0.628 µg/Kg9/11/2000 8-1-B25 614813 4783327 8 0309086-09 Cl5-BZ#118 1360 J µg/Kg 3.83 µg/Kg9/11/2000 8-1-B25 614813 4783327 8 0309086-09 Cl5-BZ#123 2.13 UJ µg/Kg 2.13 µg/Kg9/11/2000 8-1-B25 614813 4783327 8 0309086-09 Cl5-BZ#126 1.63 U µg/Kg 1.63 µg/Kg9/11/2000 8-1-B25 614813 4783327 8 0309086-09 Cl6-BZ#128 85.4 J µg/Kg 5.65 µg/Kg9/11/2000 8-1-B25 614813 4783327 8 0309086-09 Cl6-BZ#138 508 J µg/Kg 3.01 µg/Kg9/11/2000 8-1-B25 614813 4783327 8 0309086-09 Cl6-BZ#146 76.1 µg/Kg 1.25 µg/Kg9/11/2000 8-1-B25 614813 4783327 8 0309086-09 Cl6-BZ#149 309 µg/Kg 2.01 µg/Kg9/11/2000 8-1-B25 614813 4783327 8 0309086-09 Cl6-BZ#151 80.8 µg/Kg 2.45 µg/Kg9/11/2000 8-1-B25 614813 4783327 8 0309086-09 Cl6-BZ#153 256 µg/Kg 3.64 µg/Kg9/11/2000 8-1-B25 614813 4783327 8 0309086-09 Cl6-BZ#156 55.2 µg/Kg 4.52 µg/Kg9/11/2000 8-1-B25 614813 4783327 8 0309086-09 Cl6-BZ#157 11.3 J µg/Kg 4.39 µg/Kg9/11/2000 8-1-B25 614813 4783327 8 0309086-09 Cl6-BZ#158 73.6 µg/Kg 1.19 µg/Kg9/11/2000 8-1-B25 614813 4783327 8 0309086-09 Cl6-BZ#167 15.6 J µg/Kg 1.57 µg/Kg9/11/2000 8-1-B25 614813 4783327 8 0309086-09 Cl6-BZ#169 4.64 U µg/Kg 4.64 µg/Kg9/11/2000 8-1-B25 614813 4783327 8 0309086-09 Cl7-BZ#170 65.3 µg/Kg 2.26 µg/Kg9/11/2000 8-1-B25 614813 4783327 8 0309086-09 Cl7-BZ#174 44.2 µg/Kg 1.51 µg/Kg9/11/2000 8-1-B25 614813 4783327 8 0309086-09 Cl7-BZ#177 23.8 µg/Kg 1.00 µg/Kg9/11/2000 8-1-B25 614813 4783327 8 0309086-09 Cl7-BZ#180 97.4 J µg/Kg 2.07 µg/Kg9/11/2000 8-1-B25 614813 4783327 8 0309086-09 Cl7-BZ#183 29.6 J µg/Kg 2.01 µg/Kg9/11/2000 8-1-B25 614813 4783327 8 0309086-09 Cl7-BZ#187 61.8 µg/Kg 2.07 µg/Kg9/11/2000 8-1-B25 614813 4783327 8 0309086-09 Cl7-BZ#189 2.38 U µg/Kg 2.38 µg/Kg9/11/2000 8-1-B25 614813 4783327 8 0309086-09 Cl8-BZ#194 2.26 UJ µg/Kg 2.26 µg/Kg9/11/2000 8-1-B25 614813 4783327 8 0309086-09 Cl8-BZ#195 24.8 J µg/Kg 2.26 µg/Kg9/11/2000 8-1-B25 614813 4783327 8 0309086-09 Cl8-BZ#201 20.8 µg/Kg 2.70 µg/Kg9/11/2000 8-1-B25 614813 4783327 8 0309086-09 Cl9-BZ#206 14.3 J µg/Kg 3.45 µg/Kg9/11/2000 8-1-B25 614813 4783327 8 0309086-09 Cl10-BZ#209 3.51 J µg/Kg 0.941 µg/Kg9/11/2000 8-1-B25 614813 4783327 8 0309086-09 Monochlorobiphenyls 378 µg/Kg 1.63 µg/Kg9/11/2000 8-1-B25 614813 4783327 8 0309086-09 Dichlorobiphenyls 4100 µg/Kg 10.0 µg/Kg9/11/2000 8-1-B25 614813 4783327 8 0309086-09 Trichlorobiphenyls 17700 µg/Kg 2.82 µg/Kg9/11/2000 8-1-B25 614813 4783327 8 0309086-09 Tetrachlorobiphenyls 53100 µg/Kg 4.58 µg/Kg9/11/2000 8-1-B25 614813 4783327 8 0309086-09 Pentachlorobiphenyls 16800 µg/Kg 2.13 µg/Kg9/11/2000 8-1-B25 614813 4783327 8 0309086-09 Hexachlorobiphenyls 2000 µg/Kg 3.83 µg/Kg



Extracted 7/30/04






DETECTION LIMIT3

9/11/2000 8-1-B25 614813 4783327 8 0309086-09 Heptachlorobiphenyls 321 µg/Kg 1.32 µg/Kg9/11/2000 8-1-B25 614813 4783327 8 0309086-09 Octachlorobiphenyls 90.6 µg/Kg 1.88 µg/Kg9/11/2000 8-1-B25 614813 4783327 8 0309086-09 Nonachlorobiphenyls 55.7 µg/Kg 3.45 µg/Kg9/11/2000 8-1-B25 614813 4783327 8 0309086-09 Decachlorobiphenyl 3.51 J µg/Kg 0.941 µg/Kg9/11/2000 8-1-B25 614813 4783327 8 0309086-09 Total Homologs 94500 µg/Kg 3.14 µg/Kg9/11/2000 8-1-B25 614813 4783327 8 0309086-09 Percent Moisture 24.0 % 0.1 %9/11/2000 8-1-B35 614813 4783327 8 0309086-10 Cl2-BZ#8 1040 µg/Kg 65.8 µg/Kg9/11/2000 8-1-B35 614813 4783327 8 0309086-10 Cl3-BZ#18 2020 J µg/Kg 46.9 µg/Kg9/11/2000 8-1-B35 614813 4783327 8 0309086-10 Cl3-BZ#31/#28 84100 J µg/Kg 22.2 µg/Kg9/11/2000 8-1-B35 614813 4783327 8 0309086-10 Cl4-BZ#44 45600 µg/Kg 28.4 µg/Kg9/11/2000 8-1-B35 614813 4783327 8 0309086-10 Cl4-BZ#45 10800 µg/Kg 11.1 µg/Kg9/11/2000 8-1-B35 614813 4783327 8 0309086-10 Cl4-BZ#47 24300 µg/Kg 18.1 µg/Kg9/11/2000 8-1-B35 614813 4783327 8 0309086-10 Cl4-BZ#49 40100 µg/Kg 31.7 µg/Kg9/11/2000 8-1-B35 614813 4783327 8 0309086-10 Cl4-BZ#52 59800 J µg/Kg 11.5 µg/Kg9/11/2000 8-1-B35 614813 4783327 8 0309086-10 Cl4-BZ#56 42200 µg/Kg 50.6 µg/Kg9/11/2000 8-1-B35 614813 4783327 8 0309086-10 Cl4-BZ#66 48900 µg/Kg 18.1 µg/Kg9/11/2000 8-1-B35 614813 4783327 8 0309086-10 Cl4-BZ#70 32600 µg/Kg 41.1 µg/Kg9/11/2000 8-1-B35 614813 4783327 8 0309086-10 Cl4-BZ#74 32300 µg/Kg 11.5 µg/Kg9/11/2000 8-1-B35 614813 4783327 8 0309086-10 Cl4-BZ#77 4000 NJ µg/Kg 22.2 µg/Kg9/11/2000 8-1-B35 614813 4783327 8 0309086-10 Cl4-BZ#81 23.9 U µg/Kg 23.9 µg/Kg9/11/2000 8-1-B35 614813 4783327 8 0309086-10 Cl5-BZ#87 10800 µg/Kg 14.0 µg/Kg9/11/2000 8-1-B35 614813 4783327 8 0309086-10 Cl5-BZ#95 14200 µg/Kg 5.35 µg/Kg9/11/2000 8-1-B35 614813 4783327 8 0309086-10 Cl5-BZ#99 12600 µg/Kg 7.82 µg/Kg9/11/2000 8-1-B35 614813 4783327 8 0309086-10 Cl5-BZ#101 14500 µg/Kg 9.46 µg/Kg9/11/2000 8-1-B35 614813 4783327 8 0309086-10 Cl5-BZ#105 7060 J µg/Kg 14.0 µg/Kg9/11/2000 8-1-B35 614813 4783327 8 0309086-10 Cl5-BZ#110 16700 µg/Kg 9.46 µg/Kg9/11/2000 8-1-B35 614813 4783327 8 0309086-10 Cl5-BZ#114 1310 µg/Kg 4.11 µg/Kg9/11/2000 8-1-B35 614813 4783327 8 0309086-10 Cl5-BZ#118 14000 J µg/Kg 25.1 µg/Kg9/11/2000 8-1-B35 614813 4783327 8 0309086-10 Cl5-BZ#123 14.0 UJ µg/Kg 14.0 µg/Kg9/11/2000 8-1-B35 614813 4783327 8 0309086-10 Cl5-BZ#126 10.7 U µg/Kg 10.7 µg/Kg9/11/2000 8-1-B35 614813 4783327 8 0309086-10 Cl6-BZ#128 630 J µg/Kg 37.0 µg/Kg9/11/2000 8-1-B35 614813 4783327 8 0309086-10 Cl6-BZ#138 4170 J µg/Kg 19.7 µg/Kg9/11/2000 8-1-B35 614813 4783327 8 0309086-10 Cl6-BZ#146 655 µg/Kg 8.23 µg/Kg9/11/2000 8-1-B35 614813 4783327 8 0309086-10 Cl6-BZ#149 2950 µg/Kg 13.2 µg/Kg9/11/2000 8-1-B35 614813 4783327 8 0309086-10 Cl6-BZ#151 675 µg/Kg 16.0 µg/Kg



Extracted 7/30/04






DETECTION LIMIT3

9/11/2000 8-1-B35 614813 4783327 8 0309086-10 Cl6-BZ#153 2320 µg/Kg 23.9 µg/Kg9/11/2000 8-1-B35 614813 4783327 8 0309086-10 Cl6-BZ#156 502 µg/Kg 29.6 µg/Kg9/11/2000 8-1-B35 614813 4783327 8 0309086-10 Cl6-BZ#157 308 µg/Kg 28.8 µg/Kg9/11/2000 8-1-B35 614813 4783327 8 0309086-10 Cl6-BZ#158 852 µg/Kg 7.82 µg/Kg9/11/2000 8-1-B35 614813 4783327 8 0309086-10 Cl6-BZ#167 170 J µg/Kg 10.3 µg/Kg9/11/2000 8-1-B35 614813 4783327 8 0309086-10 Cl6-BZ#169 30.4 U µg/Kg 30.4 µg/Kg9/11/2000 8-1-B35 614813 4783327 8 0309086-10 Cl7-BZ#170 520 µg/Kg 14.8 µg/Kg9/11/2000 8-1-B35 614813 4783327 8 0309086-10 Cl7-BZ#174 420 µg/Kg 9.87 µg/Kg9/11/2000 8-1-B35 614813 4783327 8 0309086-10 Cl7-BZ#177 229 µg/Kg 6.58 µg/Kg9/11/2000 8-1-B35 614813 4783327 8 0309086-10 Cl7-BZ#180 912 J µg/Kg 13.6 µg/Kg9/11/2000 8-1-B35 614813 4783327 8 0309086-10 Cl7-BZ#183 267 J µg/Kg 13.2 µg/Kg9/11/2000 8-1-B35 614813 4783327 8 0309086-10 Cl7-BZ#187 528 µg/Kg 13.6 µg/Kg9/11/2000 8-1-B35 614813 4783327 8 0309086-10 Cl7-BZ#189 21.4 J µg/Kg 15.6 µg/Kg9/11/2000 8-1-B35 614813 4783327 8 0309086-10 Cl8-BZ#194 26.3 J µg/Kg 14.8 µg/Kg9/11/2000 8-1-B35 614813 4783327 8 0309086-10 Cl8-BZ#195 135 J µg/Kg 14.8 µg/Kg9/11/2000 8-1-B35 614813 4783327 8 0309086-10 Cl8-BZ#201 219 µg/Kg 17.7 µg/Kg9/11/2000 8-1-B35 614813 4783327 8 0309086-10 Cl9-BZ#206 92.1 J µg/Kg 22.6 µg/Kg9/11/2000 8-1-B35 614813 4783327 8 0309086-10 Cl10-BZ#209 19.7 J µg/Kg 6.17 µg/Kg9/11/2000 8-1-B35 614813 4783327 8 0309086-10 Monochlorobiphenyls 385 µg/Kg 10.7 µg/Kg9/11/2000 8-1-B35 614813 4783327 8 0309086-10 Dichlorobiphenyls 4860 µg/Kg 65.8 µg/Kg9/11/2000 8-1-B35 614813 4783327 8 0309086-10 Trichlorobiphenyls 121000 µg/Kg 18.5 µg/Kg9/11/2000 8-1-B35 614813 4783327 8 0309086-10 Tetrachlorobiphenyls 603000 µg/Kg 30.0 µg/Kg9/11/2000 8-1-B35 614813 4783327 8 0309086-10 Pentachlorobiphenyls 184000 µg/Kg 14.0 µg/Kg9/11/2000 8-1-B35 614813 4783327 8 0309086-10 Hexachlorobiphenyls 20300 µg/Kg 25.1 µg/Kg9/11/2000 8-1-B35 614813 4783327 8 0309086-10 Heptachlorobiphenyls 2880 µg/Kg 8.64 µg/Kg9/11/2000 8-1-B35 614813 4783327 8 0309086-10 Octachlorobiphenyls 660 µg/Kg 12.3 µg/Kg9/11/2000 8-1-B35 614813 4783327 8 0309086-10 Nonachlorobiphenyls 321 µg/Kg 22.6 µg/Kg9/11/2000 8-1-B35 614813 4783327 8 0309086-10 Decachlorobiphenyl 19.7 J µg/Kg 6.17 µg/Kg9/11/2000 8-1-B35 614813 4783327 8 0309086-10 Total Homologs 937000 µg/Kg 20.6 µg/Kg9/11/2000 8-1-B35 614813 4783327 8 0309086-10 Percent Moisture 42.9 % 0.1 %9/7/2000 1-1-A15 611699 4758797 1 0309086-11 Cl2-BZ#8 55.4 µg/Kg 3.43 µg/Kg9/7/2000 1-1-A15 611699 4758797 1 0309086-11 Cl3-BZ#18 159 J µg/Kg 2.44 µg/Kg9/7/2000 1-1-A15 611699 4758797 1 0309086-11 Cl3-BZ#31/#28 2530 J µg/Kg 1.16 µg/Kg9/7/2000 1-1-A15 611699 4758797 1 0309086-11 Cl4-BZ#44 681 µg/Kg 1.48 µg/Kg9/7/2000 1-1-A15 611699 4758797 1 0309086-11 Cl4-BZ#45 92.3 µg/Kg 0.579 µg/Kg



Extracted 7/30/04






DETECTION LIMIT3

9/7/2000 1-1-A15 611699 4758797 1 0309086-11 Cl4-BZ#47 552 µg/Kg 0.943 µg/Kg9/7/2000 1-1-A15 611699 4758797 1 0309086-11 Cl4-BZ#49 985 µg/Kg 1.65 µg/Kg9/7/2000 1-1-A15 611699 4758797 1 0309086-11 Cl4-BZ#52 1450 J µg/Kg 0.600 µg/Kg9/7/2000 1-1-A15 611699 4758797 1 0309086-11 Cl4-BZ#56 1110 µg/Kg 2.64 µg/Kg9/7/2000 1-1-A15 611699 4758797 1 0309086-11 Cl4-BZ#66 1530 µg/Kg 0.943 µg/Kg9/7/2000 1-1-A15 611699 4758797 1 0309086-11 Cl4-BZ#70 1440 µg/Kg 2.14 µg/Kg9/7/2000 1-1-A15 611699 4758797 1 0309086-11 Cl4-BZ#74 968 µg/Kg 0.600 µg/Kg9/7/2000 1-1-A15 611699 4758797 1 0309086-11 Cl4-BZ#77 226 NJ µg/Kg 1.16 µg/Kg9/7/2000 1-1-A15 611699 4758797 1 0309086-11 Cl4-BZ#81 1.24 U µg/Kg 1.24 µg/Kg9/7/2000 1-1-A15 611699 4758797 1 0309086-11 Cl5-BZ#87 657 µg/Kg 0.729 µg/Kg9/7/2000 1-1-A15 611699 4758797 1 0309086-11 Cl5-BZ#95 746 µg/Kg 0.279 µg/Kg9/7/2000 1-1-A15 611699 4758797 1 0309086-11 Cl5-BZ#99 648 µg/Kg 0.407 µg/Kg9/7/2000 1-1-A15 611699 4758797 1 0309086-11 Cl5-BZ#101 1100 µg/Kg 0.493 µg/Kg9/7/2000 1-1-A15 611699 4758797 1 0309086-11 Cl5-BZ#105 737 J µg/Kg 0.729 µg/Kg9/7/2000 1-1-A15 611699 4758797 1 0309086-11 Cl5-BZ#110 1270 µg/Kg 0.493 µg/Kg9/7/2000 1-1-A15 611699 4758797 1 0309086-11 Cl5-BZ#114 38.1 µg/Kg 0.214 µg/Kg9/7/2000 1-1-A15 611699 4758797 1 0309086-11 Cl5-BZ#118 1410 J µg/Kg 1.31 µg/Kg9/7/2000 1-1-A15 611699 4758797 1 0309086-11 Cl5-BZ#123 0.729 UJ µg/Kg 0.729 µg/Kg9/7/2000 1-1-A15 611699 4758797 1 0309086-11 Cl5-BZ#126 0.557 U µg/Kg 0.557 µg/Kg9/7/2000 1-1-A15 611699 4758797 1 0309086-11 Cl6-BZ#128 198 J µg/Kg 1.93 µg/Kg9/7/2000 1-1-A15 611699 4758797 1 0309086-11 Cl6-BZ#138 1070 J µg/Kg 1.03 µg/Kg9/7/2000 1-1-A15 611699 4758797 1 0309086-11 Cl6-BZ#146 120 µg/Kg 0.429 µg/Kg9/7/2000 1-1-A15 611699 4758797 1 0309086-11 Cl6-BZ#149 540 µg/Kg 0.686 µg/Kg9/7/2000 1-1-A15 611699 4758797 1 0309086-11 Cl6-BZ#151 116 µg/Kg 0.836 µg/Kg9/7/2000 1-1-A15 611699 4758797 1 0309086-11 Cl6-BZ#153 533 µg/Kg 1.24 µg/Kg9/7/2000 1-1-A15 611699 4758797 1 0309086-11 Cl6-BZ#156 128 µg/Kg 1.54 µg/Kg9/7/2000 1-1-A15 611699 4758797 1 0309086-11 Cl6-BZ#157 25.3 µg/Kg 1.50 µg/Kg9/7/2000 1-1-A15 611699 4758797 1 0309086-11 Cl6-BZ#158 154 µg/Kg 0.407 µg/Kg9/7/2000 1-1-A15 611699 4758797 1 0309086-11 Cl6-BZ#167 40.7 J µg/Kg 0.536 µg/Kg9/7/2000 1-1-A15 611699 4758797 1 0309086-11 Cl6-BZ#169 1.59 U µg/Kg 1.59 µg/Kg9/7/2000 1-1-A15 611699 4758797 1 0309086-11 Cl7-BZ#170 154 µg/Kg 0.772 µg/Kg9/7/2000 1-1-A15 611699 4758797 1 0309086-11 Cl7-BZ#174 90.2 µg/Kg 0.514 µg/Kg9/7/2000 1-1-A15 611699 4758797 1 0309086-11 Cl7-BZ#177 42.7 µg/Kg 0.343 µg/Kg9/7/2000 1-1-A15 611699 4758797 1 0309086-11 Cl7-BZ#180 169 J µg/Kg 0.707 µg/Kg9/7/2000 1-1-A15 611699 4758797 1 0309086-11 Cl7-BZ#183 42.1 J µg/Kg 0.686 µg/Kg



Extracted 7/30/04






DETECTION LIMIT3

9/7/2000 1-1-A15 611699 4758797 1 0309086-11 Cl7-BZ#187 85.0 µg/Kg 0.707 µg/Kg9/7/2000 1-1-A15 611699 4758797 1 0309086-11 Cl7-BZ#189 5.49 µg/Kg 0.814 µg/Kg9/7/2000 1-1-A15 611699 4758797 1 0309086-11 Cl8-BZ#194 2.92 J µg/Kg 0.772 µg/Kg9/7/2000 1-1-A15 611699 4758797 1 0309086-11 Cl8-BZ#195 27.8 J µg/Kg 0.772 µg/Kg9/7/2000 1-1-A15 611699 4758797 1 0309086-11 Cl8-BZ#201 33.7 µg/Kg 0.922 µg/Kg9/7/2000 1-1-A15 611699 4758797 1 0309086-11 Cl9-BZ#206 25.7 J µg/Kg 1.18 µg/Kg9/7/2000 1-1-A15 611699 4758797 1 0309086-11 Cl10-BZ#209 4.97 µg/Kg 0.322 µg/Kg9/7/2000 1-1-A15 611699 4758797 1 0309086-11 Monochlorobiphenyls 13.3 µg/Kg 0.557 µg/Kg9/7/2000 1-1-A15 611699 4758797 1 0309086-11 Dichlorobiphenyls 362 µg/Kg 3.43 µg/Kg9/7/2000 1-1-A15 611699 4758797 1 0309086-11 Trichlorobiphenyls 3940 µg/Kg 0.965 µg/Kg9/7/2000 1-1-A15 611699 4758797 1 0309086-11 Tetrachlorobiphenyls 15100 µg/Kg 1.56 µg/Kg9/7/2000 1-1-A15 611699 4758797 1 0309086-11 Pentachlorobiphenyls 12300 µg/Kg 0.729 µg/Kg9/7/2000 1-1-A15 611699 4758797 1 0309086-11 Hexachlorobiphenyls 3660 µg/Kg 1.31 µg/Kg9/7/2000 1-1-A15 611699 4758797 1 0309086-11 Heptachlorobiphenyls 519 µg/Kg 0.450 µg/Kg9/7/2000 1-1-A15 611699 4758797 1 0309086-11 Octachlorobiphenyls 118 µg/Kg 0.643 µg/Kg9/7/2000 1-1-A15 611699 4758797 1 0309086-11 Nonachlorobiphenyls 58.4 µg/Kg 1.18 µg/Kg9/7/2000 1-1-A15 611699 4758797 1 0309086-11 Decachlorobiphenyl 4.97 µg/Kg 0.322 µg/Kg9/7/2000 1-1-A15 611699 4758797 1 0309086-11 Total Homologs 36100 µg/Kg 1.07 µg/Kg9/7/2000 1-1-A15 611699 4758797 1 0309086-11 Percent Moisture 43.7 % 0.1 %9/7/2000 1-1-B15 611691 4758804 1 0309086-12 Cl2-BZ#8 30.4 µg/Kg 0.720 µg/Kg9/7/2000 1-1-B15 611691 4758804 1 0309086-12 Cl3-BZ#18 22.0 J µg/Kg 0.513 µg/Kg9/7/2000 1-1-B15 611691 4758804 1 0309086-12 Cl3-BZ#31/#28 1180 J µg/Kg 0.243 µg/Kg9/7/2000 1-1-B15 611691 4758804 1 0309086-12 Cl4-BZ#44 147 µg/Kg 0.310 µg/Kg9/7/2000 1-1-B15 611691 4758804 1 0309086-12 Cl4-BZ#45 11.6 µg/Kg 0.122 µg/Kg9/7/2000 1-1-B15 611691 4758804 1 0309086-12 Cl4-BZ#47 172 µg/Kg 0.198 µg/Kg9/7/2000 1-1-B15 611691 4758804 1 0309086-12 Cl4-BZ#49 338 µg/Kg 0.347 µg/Kg9/7/2000 1-1-B15 611691 4758804 1 0309086-12 Cl4-BZ#52 525 J µg/Kg 0.126 µg/Kg9/7/2000 1-1-B15 611691 4758804 1 0309086-12 Cl4-BZ#56 385 µg/Kg 0.553 µg/Kg9/7/2000 1-1-B15 611691 4758804 1 0309086-12 Cl4-BZ#66 565 µg/Kg 0.198 µg/Kg9/7/2000 1-1-B15 611691 4758804 1 0309086-12 Cl4-BZ#70 544 µg/Kg 0.450 µg/Kg9/7/2000 1-1-B15 611691 4758804 1 0309086-12 Cl4-BZ#74 454 µg/Kg 0.126 µg/Kg9/7/2000 1-1-B15 611691 4758804 1 0309086-12 Cl4-BZ#77 81.4 NJ µg/Kg 0.243 µg/Kg9/7/2000 1-1-B15 611691 4758804 1 0309086-12 Cl4-BZ#81 0.261 U µg/Kg 0.261 µg/Kg9/7/2000 1-1-B15 611691 4758804 1 0309086-12 Cl5-BZ#87 172 µg/Kg 0.153 µg/Kg9/7/2000 1-1-B15 611691 4758804 1 0309086-12 Cl5-BZ#95 151 µg/Kg 0.0585 µg/Kg



Extracted 7/30/04






DETECTION LIMIT3

9/7/2000 1-1-B15 611691 4758804 1 0309086-12 Cl5-BZ#99 141 µg/Kg 0.0855 µg/Kg9/7/2000 1-1-B15 611691 4758804 1 0309086-12 Cl5-BZ#101 259 µg/Kg 0.104 µg/Kg9/7/2000 1-1-B15 611691 4758804 1 0309086-12 Cl5-BZ#105 232 J µg/Kg 0.153 µg/Kg9/7/2000 1-1-B15 611691 4758804 1 0309086-12 Cl5-BZ#110 305 µg/Kg 0.104 µg/Kg9/7/2000 1-1-B15 611691 4758804 1 0309086-12 Cl5-BZ#114 24.3 µg/Kg 0.0450 µg/Kg9/7/2000 1-1-B15 611691 4758804 1 0309086-12 Cl5-BZ#118 395 J µg/Kg 0.275 µg/Kg9/7/2000 1-1-B15 611691 4758804 1 0309086-12 Cl5-BZ#123 0.153 UJ µg/Kg 0.153 µg/Kg9/7/2000 1-1-B15 611691 4758804 1 0309086-12 Cl5-BZ#126 0.117 U µg/Kg 0.117 µg/Kg9/7/2000 1-1-B15 611691 4758804 1 0309086-12 Cl6-BZ#128 42.7 J µg/Kg 0.405 µg/Kg9/7/2000 1-1-B15 611691 4758804 1 0309086-12 Cl6-BZ#138 230 J µg/Kg 0.216 µg/Kg9/7/2000 1-1-B15 611691 4758804 1 0309086-12 Cl6-BZ#146 22.9 µg/Kg 0.0900 µg/Kg9/7/2000 1-1-B15 611691 4758804 1 0309086-12 Cl6-BZ#149 95.9 µg/Kg 0.144 µg/Kg9/7/2000 1-1-B15 611691 4758804 1 0309086-12 Cl6-BZ#151 25.2 µg/Kg 0.176 µg/Kg9/7/2000 1-1-B15 611691 4758804 1 0309086-12 Cl6-BZ#153 109 µg/Kg 0.261 µg/Kg9/7/2000 1-1-B15 611691 4758804 1 0309086-12 Cl6-BZ#156 30.7 µg/Kg 0.324 µg/Kg9/7/2000 1-1-B15 611691 4758804 1 0309086-12 Cl6-BZ#157 6.03 µg/Kg 0.315 µg/Kg9/7/2000 1-1-B15 611691 4758804 1 0309086-12 Cl6-BZ#158 24.0 µg/Kg 0.0855 µg/Kg9/7/2000 1-1-B15 611691 4758804 1 0309086-12 Cl6-BZ#167 9.23 J µg/Kg 0.112 µg/Kg9/7/2000 1-1-B15 611691 4758804 1 0309086-12 Cl6-BZ#169 0.333 U µg/Kg 0.333 µg/Kg9/7/2000 1-1-B15 611691 4758804 1 0309086-12 Cl7-BZ#170 34.9 µg/Kg 0.162 µg/Kg9/7/2000 1-1-B15 611691 4758804 1 0309086-12 Cl7-BZ#174 18.2 µg/Kg 0.108 µg/Kg9/7/2000 1-1-B15 611691 4758804 1 0309086-12 Cl7-BZ#177 10.7 µg/Kg 0.0720 µg/Kg9/7/2000 1-1-B15 611691 4758804 1 0309086-12 Cl7-BZ#180 30.3 J µg/Kg 0.148 µg/Kg9/7/2000 1-1-B15 611691 4758804 1 0309086-12 Cl7-BZ#183 5.72 J µg/Kg 0.144 µg/Kg9/7/2000 1-1-B15 611691 4758804 1 0309086-12 Cl7-BZ#187 18.3 µg/Kg 0.148 µg/Kg9/7/2000 1-1-B15 611691 4758804 1 0309086-12 Cl7-BZ#189 2.14 µg/Kg 0.171 µg/Kg9/7/2000 1-1-B15 611691 4758804 1 0309086-12 Cl8-BZ#194 0.792 J µg/Kg 0.162 µg/Kg9/7/2000 1-1-B15 611691 4758804 1 0309086-12 Cl8-BZ#195 6.91 J µg/Kg 0.162 µg/Kg9/7/2000 1-1-B15 611691 4758804 1 0309086-12 Cl8-BZ#201 9.27 µg/Kg 0.193 µg/Kg9/7/2000 1-1-B15 611691 4758804 1 0309086-12 Cl9-BZ#206 8.62 J µg/Kg 0.248 µg/Kg9/7/2000 1-1-B15 611691 4758804 1 0309086-12 Cl10-BZ#209 1.87 µg/Kg 0.0675 µg/Kg9/7/2000 1-1-B15 611691 4758804 1 0309086-12 Monochlorobiphenyls 11.6 µg/Kg 0.117 µg/Kg9/7/2000 1-1-B15 611691 4758804 1 0309086-12 Dichlorobiphenyls 212 µg/Kg 0.720 µg/Kg9/7/2000 1-1-B15 611691 4758804 1 0309086-12 Trichlorobiphenyls 1460 µg/Kg 0.203 µg/Kg9/7/2000 1-1-B15 611691 4758804 1 0309086-12 Tetrachlorobiphenyls 4910 µg/Kg 0.329 µg/Kg



Extracted 7/30/04






DETECTION LIMIT3

9/7/2000 1-1-B15 611691 4758804 1 0309086-12 Pentachlorobiphenyls 3050 µg/Kg 0.153 µg/Kg9/7/2000 1-1-B15 611691 4758804 1 0309086-12 Hexachlorobiphenyls 723 µg/Kg 0.275 µg/Kg9/7/2000 1-1-B15 611691 4758804 1 0309086-12 Heptachlorobiphenyls 101 µg/Kg 0.0945 µg/Kg9/7/2000 1-1-B15 611691 4758804 1 0309086-12 Octachlorobiphenyls 33.8 µg/Kg 0.135 µg/Kg9/7/2000 1-1-B15 611691 4758804 1 0309086-12 Nonachlorobiphenyls 20.8 µg/Kg 0.248 µg/Kg9/7/2000 1-1-B15 611691 4758804 1 0309086-12 Decachlorobiphenyl 1.87 µg/Kg 0.0675 µg/Kg9/7/2000 1-1-B15 611691 4758804 1 0309086-12 Total Homologs 10500 µg/Kg 0.225 µg/Kg9/7/2000 1-1-B15 611691 4758804 1 0309086-12 Percent Moisture 46.8 % 0.1 %9/7/2000 1-1-B25 611691 4758804 1 0309086-13 Cl2-BZ#8 8.08 µg/Kg 0.381 µg/Kg9/7/2000 1-1-B25 611691 4758804 1 0309086-13 Cl3-BZ#18 17.9 J µg/Kg 0.271 µg/Kg9/7/2000 1-1-B25 611691 4758804 1 0309086-13 Cl3-BZ#31/#28 708 J µg/Kg 0.129 µg/Kg9/7/2000 1-1-B25 611691 4758804 1 0309086-13 Cl4-BZ#44 98.3 µg/Kg 0.164 µg/Kg9/7/2000 1-1-B25 611691 4758804 1 0309086-13 Cl4-BZ#45 9.33 µg/Kg 0.0643 µg/Kg9/7/2000 1-1-B25 611691 4758804 1 0309086-13 Cl4-BZ#47 75.0 µg/Kg 0.105 µg/Kg9/7/2000 1-1-B25 611691 4758804 1 0309086-13 Cl4-BZ#49 184 µg/Kg 0.183 µg/Kg9/7/2000 1-1-B25 611691 4758804 1 0309086-13 Cl4-BZ#52 316 J µg/Kg 0.0667 µg/Kg9/7/2000 1-1-B25 611691 4758804 1 0309086-13 Cl4-BZ#56 226 µg/Kg 0.293 µg/Kg9/7/2000 1-1-B25 611691 4758804 1 0309086-13 Cl4-BZ#66 283 µg/Kg 0.105 µg/Kg9/7/2000 1-1-B25 611691 4758804 1 0309086-13 Cl4-BZ#70 378 µg/Kg 0.238 µg/Kg9/7/2000 1-1-B25 611691 4758804 1 0309086-13 Cl4-BZ#74 211 µg/Kg 0.0667 µg/Kg9/7/2000 1-1-B25 611691 4758804 1 0309086-13 Cl4-BZ#77 49.0 NJ µg/Kg 0.129 µg/Kg9/7/2000 1-1-B25 611691 4758804 1 0309086-13 Cl4-BZ#81 0.138 U µg/Kg 0.138 µg/Kg9/7/2000 1-1-B25 611691 4758804 1 0309086-13 Cl5-BZ#87 118 µg/Kg 0.0810 µg/Kg9/7/2000 1-1-B25 611691 4758804 1 0309086-13 Cl5-BZ#95 101 µg/Kg 0.0310 µg/Kg9/7/2000 1-1-B25 611691 4758804 1 0309086-13 Cl5-BZ#99 83.7 µg/Kg 0.0452 µg/Kg9/7/2000 1-1-B25 611691 4758804 1 0309086-13 Cl5-BZ#101 193 µg/Kg 0.0548 µg/Kg9/7/2000 1-1-B25 611691 4758804 1 0309086-13 Cl5-BZ#105 164 J µg/Kg 0.0810 µg/Kg9/7/2000 1-1-B25 611691 4758804 1 0309086-13 Cl5-BZ#110 223 µg/Kg 0.0548 µg/Kg9/7/2000 1-1-B25 611691 4758804 1 0309086-13 Cl5-BZ#114 8.72 µg/Kg 0.0238 µg/Kg9/7/2000 1-1-B25 611691 4758804 1 0309086-13 Cl5-BZ#118 274 J µg/Kg 0.145 µg/Kg9/7/2000 1-1-B25 611691 4758804 1 0309086-13 Cl5-BZ#123 0.0810 U µg/Kg 0.0810 µg/Kg9/7/2000 1-1-B25 611691 4758804 1 0309086-13 Cl5-BZ#126 0.0619 U µg/Kg 0.0619 µg/Kg9/7/2000 1-1-B25 611691 4758804 1 0309086-13 Cl6-BZ#128 37.1 J µg/Kg 0.214 µg/Kg9/7/2000 1-1-B25 611691 4758804 1 0309086-13 Cl6-BZ#138 191 J µg/Kg 0.114 µg/Kg9/7/2000 1-1-B25 611691 4758804 1 0309086-13 Cl6-BZ#146 20.0 µg/Kg 0.0476 µg/Kg



Extracted 7/30/04






DETECTION LIMIT3

9/7/2000 1-1-B25 611691 4758804 1 0309086-13 Cl6-BZ#149 83.6 µg/Kg 0.0762 µg/Kg9/7/2000 1-1-B25 611691 4758804 1 0309086-13 Cl6-BZ#151 19.2 µg/Kg 0.0929 µg/Kg9/7/2000 1-1-B25 611691 4758804 1 0309086-13 Cl6-BZ#153 98.2 µg/Kg 0.138 µg/Kg9/7/2000 1-1-B25 611691 4758804 1 0309086-13 Cl6-BZ#156 26.0 µg/Kg 0.171 µg/Kg9/7/2000 1-1-B25 611691 4758804 1 0309086-13 Cl6-BZ#157 4.42 µg/Kg 0.167 µg/Kg9/7/2000 1-1-B25 611691 4758804 1 0309086-13 Cl6-BZ#158 24.7 µg/Kg 0.0452 µg/Kg9/7/2000 1-1-B25 611691 4758804 1 0309086-13 Cl6-BZ#167 8.65 J µg/Kg 0.0595 µg/Kg9/7/2000 1-1-B25 611691 4758804 1 0309086-13 Cl6-BZ#169 0.176 U µg/Kg 0.176 µg/Kg9/7/2000 1-1-B25 611691 4758804 1 0309086-13 Cl7-BZ#170 25.8 µg/Kg 0.0857 µg/Kg9/7/2000 1-1-B25 611691 4758804 1 0309086-13 Cl7-BZ#174 15.6 µg/Kg 0.0571 µg/Kg9/7/2000 1-1-B25 611691 4758804 1 0309086-13 Cl7-BZ#177 7.56 µg/Kg 0.0381 µg/Kg9/7/2000 1-1-B25 611691 4758804 1 0309086-13 Cl7-BZ#180 25.3 J µg/Kg 0.0786 µg/Kg9/7/2000 1-1-B25 611691 4758804 1 0309086-13 Cl7-BZ#183 5.52 J µg/Kg 0.0762 µg/Kg9/7/2000 1-1-B25 611691 4758804 1 0309086-13 Cl7-BZ#187 15.2 µg/Kg 0.0786 µg/Kg9/7/2000 1-1-B25 611691 4758804 1 0309086-13 Cl7-BZ#189 1.93 µg/Kg 0.0905 µg/Kg9/7/2000 1-1-B25 611691 4758804 1 0309086-13 Cl8-BZ#194 0.572 J µg/Kg 0.0857 µg/Kg9/7/2000 1-1-B25 611691 4758804 1 0309086-13 Cl8-BZ#195 5.20 J µg/Kg 0.0857 µg/Kg9/7/2000 1-1-B25 611691 4758804 1 0309086-13 Cl8-BZ#201 6.46 µg/Kg 0.102 µg/Kg9/7/2000 1-1-B25 611691 4758804 1 0309086-13 Cl9-BZ#206 5.08 J µg/Kg 0.131 µg/Kg9/7/2000 1-1-B25 611691 4758804 1 0309086-13 Cl10-BZ#209 1.13 µg/Kg 0.0357 µg/Kg9/7/2000 1-1-B25 611691 4758804 1 0309086-13 Monochlorobiphenyls 4.25 µg/Kg 0.0619 µg/Kg9/7/2000 1-1-B25 611691 4758804 1 0309086-13 Dichlorobiphenyls 92.2 µg/Kg 0.381 µg/Kg9/7/2000 1-1-B25 611691 4758804 1 0309086-13 Trichlorobiphenyls 830 µg/Kg 0.107 µg/Kg9/7/2000 1-1-B25 611691 4758804 1 0309086-13 Tetrachlorobiphenyls 2760 µg/Kg 0.174 µg/Kg9/7/2000 1-1-B25 611691 4758804 1 0309086-13 Pentachlorobiphenyls 2080 µg/Kg 0.0810 µg/Kg9/7/2000 1-1-B25 611691 4758804 1 0309086-13 Hexachlorobiphenyls 616 µg/Kg 0.145 µg/Kg9/7/2000 1-1-B25 611691 4758804 1 0309086-13 Heptachlorobiphenyls 91.5 µg/Kg 0.0500 µg/Kg9/7/2000 1-1-B25 611691 4758804 1 0309086-13 Octachlorobiphenyls 23.4 µg/Kg 0.0714 µg/Kg9/7/2000 1-1-B25 611691 4758804 1 0309086-13 Nonachlorobiphenyls 13.0 µg/Kg 0.131 µg/Kg9/7/2000 1-1-B25 611691 4758804 1 0309086-13 Decachlorobiphenyl 1.13 µg/Kg 0.0357 µg/Kg9/7/2000 1-1-B25 611691 4758804 1 0309086-13 Total Homologs 6520 µg/Kg 0.119 µg/Kg9/7/2000 1-1-B25 611691 4758804 1 0309086-13 Percent Moisture 40.6 % 0.1 %9/7/2000 1-1-B35 611691 4758804 1 0309086-14 Cl2-BZ#8 0.678 J µg/Kg 0.305 µg/Kg9/7/2000 1-1-B35 611691 4758804 1 0309086-14 Cl3-BZ#18 1.59 J µg/Kg 0.217 µg/Kg9/7/2000 1-1-B35 611691 4758804 1 0309086-14 Cl3-BZ#31/#28 62.8 J µg/Kg 0.103 µg/Kg



Extracted 7/30/04






DETECTION LIMIT3

9/7/2000 1-1-B35 611691 4758804 1 0309086-14 Cl4-BZ#44 6.53 µg/Kg 0.131 µg/Kg9/7/2000 1-1-B35 611691 4758804 1 0309086-14 Cl4-BZ#45 0.937 µg/Kg 0.0514 µg/Kg9/7/2000 1-1-B35 611691 4758804 1 0309086-14 Cl4-BZ#47 5.85 µg/Kg 0.0838 µg/Kg9/7/2000 1-1-B35 611691 4758804 1 0309086-14 Cl4-BZ#49 19.6 µg/Kg 0.147 µg/Kg9/7/2000 1-1-B35 611691 4758804 1 0309086-14 Cl4-BZ#52 31.4 J µg/Kg 0.0533 µg/Kg9/7/2000 1-1-B35 611691 4758804 1 0309086-14 Cl4-BZ#56 26.4 µg/Kg 0.234 µg/Kg9/7/2000 1-1-B35 611691 4758804 1 0309086-14 Cl4-BZ#66 37.3 µg/Kg 0.0838 µg/Kg9/7/2000 1-1-B35 611691 4758804 1 0309086-14 Cl4-BZ#70 49.5 µg/Kg 0.191 µg/Kg9/7/2000 1-1-B35 611691 4758804 1 0309086-14 Cl4-BZ#74 25.6 µg/Kg 0.0533 µg/Kg9/7/2000 1-1-B35 611691 4758804 1 0309086-14 Cl4-BZ#77 6.58 NJ µg/Kg 0.103 µg/Kg9/7/2000 1-1-B35 611691 4758804 1 0309086-14 Cl4-BZ#81 0.111 U µg/Kg 0.111 µg/Kg9/7/2000 1-1-B35 611691 4758804 1 0309086-14 Cl5-BZ#87 15.4 µg/Kg 0.0648 µg/Kg9/7/2000 1-1-B35 611691 4758804 1 0309086-14 Cl5-BZ#95 11.2 µg/Kg 0.0248 µg/Kg9/7/2000 1-1-B35 611691 4758804 1 0309086-14 Cl5-BZ#99 10.3 µg/Kg 0.0362 µg/Kg9/7/2000 1-1-B35 611691 4758804 1 0309086-14 Cl5-BZ#101 25.0 µg/Kg 0.0438 µg/Kg9/7/2000 1-1-B35 611691 4758804 1 0309086-14 Cl5-BZ#105 22.5 J µg/Kg 0.0648 µg/Kg9/7/2000 1-1-B35 611691 4758804 1 0309086-14 Cl5-BZ#110 34.4 µg/Kg 0.0438 µg/Kg9/7/2000 1-1-B35 611691 4758804 1 0309086-14 Cl5-BZ#114 1.17 µg/Kg 0.0190 µg/Kg9/7/2000 1-1-B35 611691 4758804 1 0309086-14 Cl5-BZ#118 43.3 J µg/Kg 0.116 µg/Kg9/7/2000 1-1-B35 611691 4758804 1 0309086-14 Cl5-BZ#123 0.0648 U µg/Kg 0.0648 µg/Kg9/7/2000 1-1-B35 611691 4758804 1 0309086-14 Cl5-BZ#126 0.0495 U µg/Kg 0.0495 µg/Kg9/7/2000 1-1-B35 611691 4758804 1 0309086-14 Cl6-BZ#128 6.07 J µg/Kg 0.171 µg/Kg9/7/2000 1-1-B35 611691 4758804 1 0309086-14 Cl6-BZ#138 35.8 J µg/Kg 0.0914 µg/Kg9/7/2000 1-1-B35 611691 4758804 1 0309086-14 Cl6-BZ#146 3.45 µg/Kg 0.0381 µg/Kg9/7/2000 1-1-B35 611691 4758804 1 0309086-14 Cl6-BZ#149 14.8 µg/Kg 0.0609 µg/Kg9/7/2000 1-1-B35 611691 4758804 1 0309086-14 Cl6-BZ#151 3.96 µg/Kg 0.0743 µg/Kg9/7/2000 1-1-B35 611691 4758804 1 0309086-14 Cl6-BZ#153 18.1 µg/Kg 0.111 µg/Kg9/7/2000 1-1-B35 611691 4758804 1 0309086-14 Cl6-BZ#156 4.40 µg/Kg 0.137 µg/Kg9/7/2000 1-1-B35 611691 4758804 1 0309086-14 Cl6-BZ#157 0.648 J µg/Kg 0.133 µg/Kg9/7/2000 1-1-B35 611691 4758804 1 0309086-14 Cl6-BZ#158 4.03 µg/Kg 0.0362 µg/Kg9/7/2000 1-1-B35 611691 4758804 1 0309086-14 Cl6-BZ#167 1.38 J µg/Kg 0.0476 µg/Kg9/7/2000 1-1-B35 611691 4758804 1 0309086-14 Cl6-BZ#169 0.141 U µg/Kg 0.141 µg/Kg9/7/2000 1-1-B35 611691 4758804 1 0309086-14 Cl7-BZ#170 5.22 µg/Kg 0.0686 µg/Kg9/7/2000 1-1-B35 611691 4758804 1 0309086-14 Cl7-BZ#174 2.76 µg/Kg 0.0457 µg/Kg9/7/2000 1-1-B35 611691 4758804 1 0309086-14 Cl7-BZ#177 1.60 µg/Kg 0.0305 µg/Kg



Extracted 7/30/04






DETECTION LIMIT3

9/7/2000 1-1-B35 611691 4758804 1 0309086-14 Cl7-BZ#180 4.88 J µg/Kg 0.0629 µg/Kg9/7/2000 1-1-B35 611691 4758804 1 0309086-14 Cl7-BZ#183 1.01 J µg/Kg 0.0609 µg/Kg9/7/2000 1-1-B35 611691 4758804 1 0309086-14 Cl7-BZ#187 2.83 µg/Kg 0.0629 µg/Kg9/7/2000 1-1-B35 611691 4758804 1 0309086-14 Cl7-BZ#189 0.0724 U µg/Kg 0.0724 µg/Kg9/7/2000 1-1-B35 611691 4758804 1 0309086-14 Cl8-BZ#194 0.107 J µg/Kg 0.0686 µg/Kg9/7/2000 1-1-B35 611691 4758804 1 0309086-14 Cl8-BZ#195 0.945 J µg/Kg 0.0686 µg/Kg9/7/2000 1-1-B35 611691 4758804 1 0309086-14 Cl8-BZ#201 0.937 µg/Kg 0.0819 µg/Kg9/7/2000 1-1-B35 611691 4758804 1 0309086-14 Cl9-BZ#206 0.907 J µg/Kg 0.105 µg/Kg9/7/2000 1-1-B35 611691 4758804 1 0309086-14 Cl10-BZ#209 0.228 µg/Kg 0.0286 µg/Kg9/7/2000 1-1-B35 611691 4758804 1 0309086-14 Monochlorobiphenyls 0.0495 U µg/Kg 0.0495 µg/Kg9/7/2000 1-1-B35 611691 4758804 1 0309086-14 Dichlorobiphenyls 1.04 J µg/Kg 0.305 µg/Kg9/7/2000 1-1-B35 611691 4758804 1 0309086-14 Trichlorobiphenyls 99.1 µg/Kg 0.0857 µg/Kg9/7/2000 1-1-B35 611691 4758804 1 0309086-14 Tetrachlorobiphenyls 319 µg/Kg 0.139 µg/Kg9/7/2000 1-1-B35 611691 4758804 1 0309086-14 Pentachlorobiphenyls 295 µg/Kg 0.0648 µg/Kg9/7/2000 1-1-B35 611691 4758804 1 0309086-14 Hexachlorobiphenyls 109 µg/Kg 0.116 µg/Kg9/7/2000 1-1-B35 611691 4758804 1 0309086-14 Heptachlorobiphenyls 16.4 µg/Kg 0.0400 µg/Kg9/7/2000 1-1-B35 611691 4758804 1 0309086-14 Octachlorobiphenyls 4.21 µg/Kg 0.0571 µg/Kg9/7/2000 1-1-B35 611691 4758804 1 0309086-14 Nonachlorobiphenyls 7.54 µg/Kg 0.105 µg/Kg9/7/2000 1-1-B35 611691 4758804 1 0309086-14 Decachlorobiphenyl 0.228 µg/Kg 0.0286 µg/Kg9/7/2000 1-1-B35 611691 4758804 1 0309086-14 Total Homologs 851 µg/Kg 0.0952 µg/Kg9/7/2000 1-1-B35 611691 4758804 1 0309086-14 Percent Moisture 29.8 % 0.1 %9/7/2000 1-1-C15 611683 4758811 1 0309086-15 Cl2-BZ#8 6.60 µg/Kg 0.299 µg/Kg9/7/2000 1-1-C15 611683 4758811 1 0309086-15 Cl3-BZ#18 10.5 J µg/Kg 0.213 µg/Kg9/7/2000 1-1-C15 611683 4758811 1 0309086-15 Cl3-BZ#31/#28 507 J µg/Kg 0.101 µg/Kg9/7/2000 1-1-C15 611683 4758811 1 0309086-15 Cl4-BZ#44 49.9 µg/Kg 0.129 µg/Kg9/7/2000 1-1-C15 611683 4758811 1 0309086-15 Cl4-BZ#45 5.38 µg/Kg 0.0504 µg/Kg9/7/2000 1-1-C15 611683 4758811 1 0309086-15 Cl4-BZ#47 67.5 µg/Kg 0.0822 µg/Kg9/7/2000 1-1-C15 611683 4758811 1 0309086-15 Cl4-BZ#49 140 µg/Kg 0.144 µg/Kg9/7/2000 1-1-C15 611683 4758811 1 0309086-15 Cl4-BZ#52 237 J µg/Kg 0.0523 µg/Kg9/7/2000 1-1-C15 611683 4758811 1 0309086-15 Cl4-BZ#56 143 µg/Kg 0.230 µg/Kg9/7/2000 1-1-C15 611683 4758811 1 0309086-15 Cl4-BZ#66 206 µg/Kg 0.0822 µg/Kg9/7/2000 1-1-C15 611683 4758811 1 0309086-15 Cl4-BZ#70 207 µg/Kg 0.187 µg/Kg9/7/2000 1-1-C15 611683 4758811 1 0309086-15 Cl4-BZ#74 158 µg/Kg 0.0523 µg/Kg9/7/2000 1-1-C15 611683 4758811 1 0309086-15 Cl4-BZ#77 25.7 NJ µg/Kg 0.101 µg/Kg9/7/2000 1-1-C15 611683 4758811 1 0309086-15 Cl4-BZ#81 0.108 U µg/Kg 0.108 µg/Kg



Extracted 7/30/04






DETECTION LIMIT3

9/7/2000 1-1-C15 611683 4758811 1 0309086-15 Cl5-BZ#87 63.0 µg/Kg 0.0635 µg/Kg9/7/2000 1-1-C15 611683 4758811 1 0309086-15 Cl5-BZ#95 65.6 µg/Kg 0.0243 µg/Kg9/7/2000 1-1-C15 611683 4758811 1 0309086-15 Cl5-BZ#99 66.1 µg/Kg 0.0355 µg/Kg9/7/2000 1-1-C15 611683 4758811 1 0309086-15 Cl5-BZ#101 119 µg/Kg 0.0430 µg/Kg9/7/2000 1-1-C15 611683 4758811 1 0309086-15 Cl5-BZ#105 98.9 J µg/Kg 0.0635 µg/Kg9/7/2000 1-1-C15 611683 4758811 1 0309086-15 Cl5-BZ#110 138 µg/Kg 0.0430 µg/Kg9/7/2000 1-1-C15 611683 4758811 1 0309086-15 Cl5-BZ#114 5.46 µg/Kg 0.0187 µg/Kg9/7/2000 1-1-C15 611683 4758811 1 0309086-15 Cl5-BZ#118 174 J µg/Kg 0.114 µg/Kg9/7/2000 1-1-C15 611683 4758811 1 0309086-15 Cl5-BZ#123 0.0635 U µg/Kg 0.0635 µg/Kg9/7/2000 1-1-C15 611683 4758811 1 0309086-15 Cl5-BZ#126 0.0486 U µg/Kg 0.0486 µg/Kg9/7/2000 1-1-C15 611683 4758811 1 0309086-15 Cl6-BZ#128 23.6 J µg/Kg 0.168 µg/Kg9/7/2000 1-1-C15 611683 4758811 1 0309086-15 Cl6-BZ#138 132 J µg/Kg 0.0897 µg/Kg9/7/2000 1-1-C15 611683 4758811 1 0309086-15 Cl6-BZ#146 13.1 µg/Kg 0.0374 µg/Kg9/7/2000 1-1-C15 611683 4758811 1 0309086-15 Cl6-BZ#149 52.5 µg/Kg 0.0598 µg/Kg9/7/2000 1-1-C15 611683 4758811 1 0309086-15 Cl6-BZ#151 12.8 µg/Kg 0.0729 µg/Kg9/7/2000 1-1-C15 611683 4758811 1 0309086-15 Cl6-BZ#153 62.8 µg/Kg 0.108 µg/Kg9/7/2000 1-1-C15 611683 4758811 1 0309086-15 Cl6-BZ#156 17.3 µg/Kg 0.134 µg/Kg9/7/2000 1-1-C15 611683 4758811 1 0309086-15 Cl6-BZ#157 2.98 µg/Kg 0.131 µg/Kg9/7/2000 1-1-C15 611683 4758811 1 0309086-15 Cl6-BZ#158 10.6 µg/Kg 0.0355 µg/Kg9/7/2000 1-1-C15 611683 4758811 1 0309086-15 Cl6-BZ#167 5.13 J µg/Kg 0.0467 µg/Kg9/7/2000 1-1-C15 611683 4758811 1 0309086-15 Cl6-BZ#169 0.138 U µg/Kg 0.138 µg/Kg9/7/2000 1-1-C15 611683 4758811 1 0309086-15 Cl7-BZ#170 17.7 µg/Kg 0.0673 µg/Kg9/7/2000 1-1-C15 611683 4758811 1 0309086-15 Cl7-BZ#174 9.75 µg/Kg 0.0448 µg/Kg9/7/2000 1-1-C15 611683 4758811 1 0309086-15 Cl7-BZ#177 5.47 µg/Kg 0.0299 µg/Kg9/7/2000 1-1-C15 611683 4758811 1 0309086-15 Cl7-BZ#180 18.0 J µg/Kg 0.0617 µg/Kg9/7/2000 1-1-C15 611683 4758811 1 0309086-15 Cl7-BZ#183 3.95 J µg/Kg 0.0598 µg/Kg9/7/2000 1-1-C15 611683 4758811 1 0309086-15 Cl7-BZ#187 10.3 µg/Kg 0.0617 µg/Kg9/7/2000 1-1-C15 611683 4758811 1 0309086-15 Cl7-BZ#189 0.0710 U µg/Kg 0.0710 µg/Kg9/7/2000 1-1-C15 611683 4758811 1 0309086-15 Cl8-BZ#194 0.523 J µg/Kg 0.0673 µg/Kg9/7/2000 1-1-C15 611683 4758811 1 0309086-15 Cl8-BZ#195 3.86 J µg/Kg 0.0673 µg/Kg9/7/2000 1-1-C15 611683 4758811 1 0309086-15 Cl8-BZ#201 5.13 µg/Kg 0.0803 µg/Kg9/7/2000 1-1-C15 611683 4758811 1 0309086-15 Cl9-BZ#206 4.74 J µg/Kg 0.103 µg/Kg9/7/2000 1-1-C15 611683 4758811 1 0309086-15 Cl10-BZ#209 1.03 µg/Kg 0.0280 µg/Kg9/7/2000 1-1-C15 611683 4758811 1 0309086-15 Monochlorobiphenyls 2.57 µg/Kg 0.0486 µg/Kg9/7/2000 1-1-C15 611683 4758811 1 0309086-15 Dichlorobiphenyls 51.1 µg/Kg 0.299 µg/Kg



Extracted 7/30/04






DETECTION LIMIT3

9/7/2000 1-1-C15 611683 4758811 1 0309086-15 Trichlorobiphenyls 578 µg/Kg 0.0841 µg/Kg9/7/2000 1-1-C15 611683 4758811 1 0309086-15 Tetrachlorobiphenyls 1850 µg/Kg 0.136 µg/Kg9/7/2000 1-1-C15 611683 4758811 1 0309086-15 Pentachlorobiphenyls 1300 µg/Kg 0.0635 µg/Kg9/7/2000 1-1-C15 611683 4758811 1 0309086-15 Hexachlorobiphenyls 388 µg/Kg 0.114 µg/Kg9/7/2000 1-1-C15 611683 4758811 1 0309086-15 Heptachlorobiphenyls 55.9 µg/Kg 0.0392 µg/Kg9/7/2000 1-1-C15 611683 4758811 1 0309086-15 Octachlorobiphenyls 30.1 µg/Kg 0.0561 µg/Kg9/7/2000 1-1-C15 611683 4758811 1 0309086-15 Nonachlorobiphenyls 11.6 µg/Kg 0.103 µg/Kg9/7/2000 1-1-C15 611683 4758811 1 0309086-15 Decachlorobiphenyl 1.03 µg/Kg 0.0280 µg/Kg9/7/2000 1-1-C15 611683 4758811 1 0309086-15 Total Homologs 4260 µg/Kg 0.0934 µg/Kg9/7/2000 1-1-C15 611683 4758811 1 0309086-15 Percent Moisture 44.3 % 0.1 %9/7/2000 1-1-D25 611675 4758816 1 0309086-16 Cl2-BZ#8 0.316 U µg/Kg 0.316 µg/Kg9/7/2000 1-1-D25 611675 4758816 1 0309086-16 Cl3-BZ#18 0.450 J µg/Kg 0.225 µg/Kg9/7/2000 1-1-D25 611675 4758816 1 0309086-16 Cl3-BZ#31/#28 9.48 J µg/Kg 0.107 µg/Kg9/7/2000 1-1-D25 611675 4758816 1 0309086-16 Cl4-BZ#44 1.08 µg/Kg 0.136 µg/Kg9/7/2000 1-1-D25 611675 4758816 1 0309086-16 Cl4-BZ#45 0.466 µg/Kg 0.0533 µg/Kg9/7/2000 1-1-D25 611675 4758816 1 0309086-16 Cl4-BZ#47 1.03 µg/Kg 0.0869 µg/Kg9/7/2000 1-1-D25 611675 4758816 1 0309086-16 Cl4-BZ#49 3.27 µg/Kg 0.152 µg/Kg9/7/2000 1-1-D25 611675 4758816 1 0309086-16 Cl4-BZ#52 3.82 J µg/Kg 0.0553 µg/Kg9/7/2000 1-1-D25 611675 4758816 1 0309086-16 Cl4-BZ#56 3.55 µg/Kg 0.243 µg/Kg9/7/2000 1-1-D25 611675 4758816 1 0309086-16 Cl4-BZ#66 6.21 µg/Kg 0.0869 µg/Kg9/7/2000 1-1-D25 611675 4758816 1 0309086-16 Cl4-BZ#70 9.11 µg/Kg 0.197 µg/Kg9/7/2000 1-1-D25 611675 4758816 1 0309086-16 Cl4-BZ#74 3.88 µg/Kg 0.0553 µg/Kg9/7/2000 1-1-D25 611675 4758816 1 0309086-16 Cl4-BZ#77 1.97 NJ µg/Kg 0.107 µg/Kg9/7/2000 1-1-D25 611675 4758816 1 0309086-16 Cl4-BZ#81 0.115 U µg/Kg 0.115 µg/Kg9/7/2000 1-1-D25 611675 4758816 1 0309086-16 Cl5-BZ#87 2.50 µg/Kg 0.0671 µg/Kg9/7/2000 1-1-D25 611675 4758816 1 0309086-16 Cl5-BZ#95 1.17 µg/Kg 0.0257 µg/Kg9/7/2000 1-1-D25 611675 4758816 1 0309086-16 Cl5-BZ#99 2.86 µg/Kg 0.0375 µg/Kg9/7/2000 1-1-D25 611675 4758816 1 0309086-16 Cl5-BZ#101 4.59 µg/Kg 0.0454 µg/Kg9/7/2000 1-1-D25 611675 4758816 1 0309086-16 Cl5-BZ#105 7.18 J µg/Kg 0.0671 µg/Kg9/7/2000 1-1-D25 611675 4758816 1 0309086-16 Cl5-BZ#110 7.95 µg/Kg 0.0454 µg/Kg9/7/2000 1-1-D25 611675 4758816 1 0309086-16 Cl5-BZ#114 0.0197 U µg/Kg 0.0197 µg/Kg9/7/2000 1-1-D25 611675 4758816 1 0309086-16 Cl5-BZ#118 14.9 J µg/Kg 0.120 µg/Kg9/7/2000 1-1-D25 611675 4758816 1 0309086-16 Cl5-BZ#123 0.0671 U µg/Kg 0.0671 µg/Kg9/7/2000 1-1-D25 611675 4758816 1 0309086-16 Cl5-BZ#126 0.0513 U µg/Kg 0.0513 µg/Kg9/7/2000 1-1-D25 611675 4758816 1 0309086-16 Cl6-BZ#128 3.15 J µg/Kg 0.178 µg/Kg



Extracted 7/30/04






DETECTION LIMIT3

9/7/2000 1-1-D25 611675 4758816 1 0309086-16 Cl6-BZ#138 17.8 J µg/Kg 0.0947 µg/Kg9/7/2000 1-1-D25 611675 4758816 1 0309086-16 Cl6-BZ#146 1.43 µg/Kg 0.0395 µg/Kg9/7/2000 1-1-D25 611675 4758816 1 0309086-16 Cl6-BZ#149 3.42 µg/Kg 0.0632 µg/Kg9/7/2000 1-1-D25 611675 4758816 1 0309086-16 Cl6-BZ#151 1.11 µg/Kg 0.0770 µg/Kg9/7/2000 1-1-D25 611675 4758816 1 0309086-16 Cl6-BZ#153 9.14 µg/Kg 0.115 µg/Kg9/7/2000 1-1-D25 611675 4758816 1 0309086-16 Cl6-BZ#156 1.71 µg/Kg 0.142 µg/Kg9/7/2000 1-1-D25 611675 4758816 1 0309086-16 Cl6-BZ#157 0.403 J µg/Kg 0.138 µg/Kg9/7/2000 1-1-D25 611675 4758816 1 0309086-16 Cl6-BZ#158 1.20 µg/Kg 0.0375 µg/Kg9/7/2000 1-1-D25 611675 4758816 1 0309086-16 Cl6-BZ#167 0.798 J µg/Kg 0.0493 µg/Kg9/7/2000 1-1-D25 611675 4758816 1 0309086-16 Cl6-BZ#169 0.146 U µg/Kg 0.146 µg/Kg9/7/2000 1-1-D25 611675 4758816 1 0309086-16 Cl7-BZ#170 2.84 µg/Kg 0.0711 µg/Kg9/7/2000 1-1-D25 611675 4758816 1 0309086-16 Cl7-BZ#174 1.18 µg/Kg 0.0474 µg/Kg9/7/2000 1-1-D25 611675 4758816 1 0309086-16 Cl7-BZ#177 0.624 µg/Kg 0.0316 µg/Kg9/7/2000 1-1-D25 611675 4758816 1 0309086-16 Cl7-BZ#180 2.12 J µg/Kg 0.0651 µg/Kg9/7/2000 1-1-D25 611675 4758816 1 0309086-16 Cl7-BZ#183 0.237 J µg/Kg 0.0632 µg/Kg9/7/2000 1-1-D25 611675 4758816 1 0309086-16 Cl7-BZ#187 1.44 µg/Kg 0.0651 µg/Kg9/7/2000 1-1-D25 611675 4758816 1 0309086-16 Cl7-BZ#189 0.0750 U µg/Kg 0.0750 µg/Kg9/7/2000 1-1-D25 611675 4758816 1 0309086-16 Cl8-BZ#194 0.0711 UJ µg/Kg 0.0711 µg/Kg9/7/2000 1-1-D25 611675 4758816 1 0309086-16 Cl8-BZ#195 0.379 J µg/Kg 0.0711 µg/Kg9/7/2000 1-1-D25 611675 4758816 1 0309086-16 Cl8-BZ#201 0.616 µg/Kg 0.0849 µg/Kg9/7/2000 1-1-D25 611675 4758816 1 0309086-16 Cl9-BZ#206 0.292 J µg/Kg 0.109 µg/Kg9/7/2000 1-1-D25 611675 4758816 1 0309086-16 Cl10-BZ#209 0.174 µg/Kg 0.0296 µg/Kg9/7/2000 1-1-D25 611675 4758816 1 0309086-16 Monochlorobiphenyls 0.0513 U µg/Kg 0.0513 µg/Kg9/7/2000 1-1-D25 611675 4758816 1 0309086-16 Dichlorobiphenyls 10.5 µg/Kg 0.316 µg/Kg9/7/2000 1-1-D25 611675 4758816 1 0309086-16 Trichlorobiphenyls 36.3 µg/Kg 0.0888 µg/Kg9/7/2000 1-1-D25 611675 4758816 1 0309086-16 Tetrachlorobiphenyls 58.8 µg/Kg 0.144 µg/Kg9/7/2000 1-1-D25 611675 4758816 1 0309086-16 Pentachlorobiphenyls 74.1 µg/Kg 0.0671 µg/Kg9/7/2000 1-1-D25 611675 4758816 1 0309086-16 Hexachlorobiphenyls 46.0 µg/Kg 0.120 µg/Kg9/7/2000 1-1-D25 611675 4758816 1 0309086-16 Heptachlorobiphenyls 7.63 µg/Kg 0.0415 µg/Kg9/7/2000 1-1-D25 611675 4758816 1 0309086-16 Octachlorobiphenyls 3.13 µg/Kg 0.0592 µg/Kg9/7/2000 1-1-D25 611675 4758816 1 0309086-16 Nonachlorobiphenyls 5.55 µg/Kg 0.109 µg/Kg9/7/2000 1-1-D25 611675 4758816 1 0309086-16 Decachlorobiphenyl 0.174 µg/Kg 0.0296 µg/Kg9/7/2000 1-1-D25 611675 4758816 1 0309086-16 Total Homologs 242 µg/Kg 0.0987 µg/Kg9/7/2000 1-1-D25 611675 4758816 1 0309086-16 Percent Moisture 31.9 % 0.1 %

9/12/2000 10-1-B15 614086 4788181 10 0309086-17 Cl2-BZ#8 136 µg/Kg 5.01 µg/Kg



Extracted 7/30/04






DETECTION LIMIT3

9/12/2000 10-1-B15 614086 4788181 10 0309086-17 Cl3-BZ#18 240 J µg/Kg 3.57 µg/Kg9/12/2000 10-1-B15 614086 4788181 10 0309086-17 Cl3-BZ#31/#28 10800 J µg/Kg 1.69 µg/Kg9/12/2000 10-1-B15 614086 4788181 10 0309086-17 Cl4-BZ#44 3890 µg/Kg 2.16 µg/Kg9/12/2000 10-1-B15 614086 4788181 10 0309086-17 Cl4-BZ#45 695 µg/Kg 0.846 µg/Kg9/12/2000 10-1-B15 614086 4788181 10 0309086-17 Cl4-BZ#47 2170 µg/Kg 1.38 µg/Kg9/12/2000 10-1-B15 614086 4788181 10 0309086-17 Cl4-BZ#49 4340 µg/Kg 2.41 µg/Kg9/12/2000 10-1-B15 614086 4788181 10 0309086-17 Cl4-BZ#52 5660 J µg/Kg 0.878 µg/Kg9/12/2000 10-1-B15 614086 4788181 10 0309086-17 Cl4-BZ#56 4560 µg/Kg 3.86 µg/Kg9/12/2000 10-1-B15 614086 4788181 10 0309086-17 Cl4-BZ#66 5810 µg/Kg 1.38 µg/Kg9/12/2000 10-1-B15 614086 4788181 10 0309086-17 Cl4-BZ#70 5420 µg/Kg 3.13 µg/Kg9/12/2000 10-1-B15 614086 4788181 10 0309086-17 Cl4-BZ#74 4710 µg/Kg 0.878 µg/Kg9/12/2000 10-1-B15 614086 4788181 10 0309086-17 Cl4-BZ#77 622 NJ µg/Kg 1.69 µg/Kg9/12/2000 10-1-B15 614086 4788181 10 0309086-17 Cl4-BZ#81 1.82 U µg/Kg 1.82 µg/Kg9/12/2000 10-1-B15 614086 4788181 10 0309086-17 Cl5-BZ#87 1570 µg/Kg 1.07 µg/Kg9/12/2000 10-1-B15 614086 4788181 10 0309086-17 Cl5-BZ#95 1920 µg/Kg 0.407 µg/Kg9/12/2000 10-1-B15 614086 4788181 10 0309086-17 Cl5-BZ#99 1640 µg/Kg 0.595 µg/Kg9/12/2000 10-1-B15 614086 4788181 10 0309086-17 Cl5-BZ#101 2240 µg/Kg 0.721 µg/Kg9/12/2000 10-1-B15 614086 4788181 10 0309086-17 Cl5-BZ#105 1310 J µg/Kg 1.07 µg/Kg9/12/2000 10-1-B15 614086 4788181 10 0309086-17 Cl5-BZ#110 2620 µg/Kg 0.721 µg/Kg9/12/2000 10-1-B15 614086 4788181 10 0309086-17 Cl5-BZ#114 237 µg/Kg 0.313 µg/Kg9/12/2000 10-1-B15 614086 4788181 10 0309086-17 Cl5-BZ#118 2580 J µg/Kg 1.91 µg/Kg9/12/2000 10-1-B15 614086 4788181 10 0309086-17 Cl5-BZ#123 1.07 UJ µg/Kg 1.07 µg/Kg9/12/2000 10-1-B15 614086 4788181 10 0309086-17 Cl5-BZ#126 0.815 U µg/Kg 0.815 µg/Kg9/12/2000 10-1-B15 614086 4788181 10 0309086-17 Cl6-BZ#128 229 J µg/Kg 2.82 µg/Kg9/12/2000 10-1-B15 614086 4788181 10 0309086-17 Cl6-BZ#138 1280 J µg/Kg 1.50 µg/Kg9/12/2000 10-1-B15 614086 4788181 10 0309086-17 Cl6-BZ#146 185 µg/Kg 0.627 µg/Kg9/12/2000 10-1-B15 614086 4788181 10 0309086-17 Cl6-BZ#149 735 µg/Kg 1.00 µg/Kg9/12/2000 10-1-B15 614086 4788181 10 0309086-17 Cl6-BZ#151 171 µg/Kg 1.22 µg/Kg9/12/2000 10-1-B15 614086 4788181 10 0309086-17 Cl6-BZ#153 672 µg/Kg 1.82 µg/Kg9/12/2000 10-1-B15 614086 4788181 10 0309086-17 Cl6-BZ#156 140 µg/Kg 2.26 µg/Kg9/12/2000 10-1-B15 614086 4788181 10 0309086-17 Cl6-BZ#157 28.8 µg/Kg 2.19 µg/Kg9/12/2000 10-1-B15 614086 4788181 10 0309086-17 Cl6-BZ#158 193 µg/Kg 0.595 µg/Kg9/12/2000 10-1-B15 614086 4788181 10 0309086-17 Cl6-BZ#167 48.0 J µg/Kg 0.784 µg/Kg9/12/2000 10-1-B15 614086 4788181 10 0309086-17 Cl6-BZ#169 2.32 U µg/Kg 2.32 µg/Kg9/12/2000 10-1-B15 614086 4788181 10 0309086-17 Cl7-BZ#170 174 µg/Kg 1.13 µg/Kg



Extracted 7/30/04






DETECTION LIMIT3

9/12/2000 10-1-B15 614086 4788181 10 0309086-17 Cl7-BZ#174 112 µg/Kg 0.752 µg/Kg9/12/2000 10-1-B15 614086 4788181 10 0309086-17 Cl7-BZ#177 52.9 µg/Kg 0.502 µg/Kg9/12/2000 10-1-B15 614086 4788181 10 0309086-17 Cl7-BZ#180 230 J µg/Kg 1.03 µg/Kg9/12/2000 10-1-B15 614086 4788181 10 0309086-17 Cl7-BZ#183 62.8 J µg/Kg 1.00 µg/Kg9/12/2000 10-1-B15 614086 4788181 10 0309086-17 Cl7-BZ#187 131 µg/Kg 1.03 µg/Kg9/12/2000 10-1-B15 614086 4788181 10 0309086-17 Cl7-BZ#189 5.64 J µg/Kg 1.19 µg/Kg9/12/2000 10-1-B15 614086 4788181 10 0309086-17 Cl8-BZ#194 3.76 J µg/Kg 1.13 µg/Kg9/12/2000 10-1-B15 614086 4788181 10 0309086-17 Cl8-BZ#195 37.2 J µg/Kg 1.13 µg/Kg9/12/2000 10-1-B15 614086 4788181 10 0309086-17 Cl8-BZ#201 44.6 µg/Kg 1.35 µg/Kg9/12/2000 10-1-B15 614086 4788181 10 0309086-17 Cl9-BZ#206 28.2 J µg/Kg 1.72 µg/Kg9/12/2000 10-1-B15 614086 4788181 10 0309086-17 Cl10-BZ#209 6.14 µg/Kg 0.470 µg/Kg9/12/2000 10-1-B15 614086 4788181 10 0309086-17 Monochlorobiphenyls 36.2 µg/Kg 0.815 µg/Kg9/12/2000 10-1-B15 614086 4788181 10 0309086-17 Dichlorobiphenyls 908 µg/Kg 5.01 µg/Kg9/12/2000 10-1-B15 614086 4788181 10 0309086-17 Trichlorobiphenyls 15900 µg/Kg 1.41 µg/Kg9/12/2000 10-1-B15 614086 4788181 10 0309086-17 Tetrachlorobiphenyls 64800 µg/Kg 2.29 µg/Kg9/12/2000 10-1-B15 614086 4788181 10 0309086-17 Pentachlorobiphenyls 27200 µg/Kg 1.07 µg/Kg9/12/2000 10-1-B15 614086 4788181 10 0309086-17 Hexachlorobiphenyls 4650 µg/Kg 1.91 µg/Kg9/12/2000 10-1-B15 614086 4788181 10 0309086-17 Heptachlorobiphenyls 698 µg/Kg 0.658 µg/Kg9/12/2000 10-1-B15 614086 4788181 10 0309086-17 Octachlorobiphenyls 161 µg/Kg 0.940 µg/Kg9/12/2000 10-1-B15 614086 4788181 10 0309086-17 Nonachlorobiphenyls 88.1 µg/Kg 1.72 µg/Kg9/12/2000 10-1-B15 614086 4788181 10 0309086-17 Decachlorobiphenyl 6.14 µg/Kg 0.470 µg/Kg9/12/2000 10-1-B15 614086 4788181 10 0309086-17 Total Homologs 114000 µg/Kg 1.57 µg/Kg9/12/2000 10-1-B15 614086 4788181 10 0309086-17 Percent Moisture 35.5 % 0.1 %9/12/2000 11-1-A25 614828 4791070 11 0309086-18 Cl2-BZ#8 114 µg/Kg 12.2 µg/Kg9/12/2000 11-1-A25 614828 4791070 11 0309086-18 Cl3-BZ#18 246 J µg/Kg 8.69 µg/Kg9/12/2000 11-1-A25 614828 4791070 11 0309086-18 Cl3-BZ#31/#28 8190 J µg/Kg 4.12 µg/Kg9/12/2000 11-1-A25 614828 4791070 11 0309086-18 Cl4-BZ#44 7640 µg/Kg 5.26 µg/Kg9/12/2000 11-1-A25 614828 4791070 11 0309086-18 Cl4-BZ#45 1450 µg/Kg 2.06 µg/Kg9/12/2000 11-1-A25 614828 4791070 11 0309086-18 Cl4-BZ#47 4430 µg/Kg 3.35 µg/Kg9/12/2000 11-1-A25 614828 4791070 11 0309086-18 Cl4-BZ#49 8670 µg/Kg 5.87 µg/Kg9/12/2000 11-1-A25 614828 4791070 11 0309086-18 Cl4-BZ#52 11100 J µg/Kg 2.13 µg/Kg9/12/2000 11-1-A25 614828 4791070 11 0309086-18 Cl4-BZ#56 8560 µg/Kg 9.37 µg/Kg9/12/2000 11-1-A25 614828 4791070 11 0309086-18 Cl4-BZ#66 10600 µg/Kg 3.35 µg/Kg9/12/2000 11-1-A25 614828 4791070 11 0309086-18 Cl4-BZ#70 8000 µg/Kg 7.62 µg/Kg9/12/2000 11-1-A25 614828 4791070 11 0309086-18 Cl4-BZ#74 7590 µg/Kg 2.13 µg/Kg



Extracted 7/30/04






DETECTION LIMIT3

9/12/2000 11-1-A25 614828 4791070 11 0309086-18 Cl4-BZ#77 1250 NJ µg/Kg 4.12 µg/Kg9/12/2000 11-1-A25 614828 4791070 11 0309086-18 Cl4-BZ#81 4.42 U µg/Kg 4.42 µg/Kg9/12/2000 11-1-A25 614828 4791070 11 0309086-18 Cl5-BZ#87 3270 µg/Kg 2.59 µg/Kg9/12/2000 11-1-A25 614828 4791070 11 0309086-18 Cl5-BZ#95 3750 µg/Kg 0.991 µg/Kg9/12/2000 11-1-A25 614828 4791070 11 0309086-18 Cl5-BZ#99 3480 µg/Kg 1.45 µg/Kg9/12/2000 11-1-A25 614828 4791070 11 0309086-18 Cl5-BZ#101 4920 µg/Kg 1.75 µg/Kg9/12/2000 11-1-A25 614828 4791070 11 0309086-18 Cl5-BZ#105 3020 J µg/Kg 2.59 µg/Kg9/12/2000 11-1-A25 614828 4791070 11 0309086-18 Cl5-BZ#110 5580 µg/Kg 1.75 µg/Kg9/12/2000 11-1-A25 614828 4791070 11 0309086-18 Cl5-BZ#114 224 µg/Kg 0.762 µg/Kg9/12/2000 11-1-A25 614828 4791070 11 0309086-18 Cl5-BZ#118 5950 J µg/Kg 4.65 µg/Kg9/12/2000 11-1-A25 614828 4791070 11 0309086-18 Cl5-BZ#123 2.59 UJ µg/Kg 2.59 µg/Kg9/12/2000 11-1-A25 614828 4791070 11 0309086-18 Cl5-BZ#126 1.98 U µg/Kg 1.98 µg/Kg9/12/2000 11-1-A25 614828 4791070 11 0309086-18 Cl6-BZ#128 524 J µg/Kg 6.86 µg/Kg9/12/2000 11-1-A25 614828 4791070 11 0309086-18 Cl6-BZ#138 3060 J µg/Kg 3.66 µg/Kg9/12/2000 11-1-A25 614828 4791070 11 0309086-18 Cl6-BZ#146 416 µg/Kg 1.52 µg/Kg9/12/2000 11-1-A25 614828 4791070 11 0309086-18 Cl6-BZ#149 1740 µg/Kg 2.44 µg/Kg9/12/2000 11-1-A25 614828 4791070 11 0309086-18 Cl6-BZ#151 380 µg/Kg 2.97 µg/Kg9/12/2000 11-1-A25 614828 4791070 11 0309086-18 Cl6-BZ#153 1630 µg/Kg 4.42 µg/Kg9/12/2000 11-1-A25 614828 4791070 11 0309086-18 Cl6-BZ#156 396 µg/Kg 5.49 µg/Kg9/12/2000 11-1-A25 614828 4791070 11 0309086-18 Cl6-BZ#157 68.6 µg/Kg 5.34 µg/Kg9/12/2000 11-1-A25 614828 4791070 11 0309086-18 Cl6-BZ#158 469 µg/Kg 1.45 µg/Kg9/12/2000 11-1-A25 614828 4791070 11 0309086-18 Cl6-BZ#167 125 J µg/Kg 1.90 µg/Kg9/12/2000 11-1-A25 614828 4791070 11 0309086-18 Cl6-BZ#169 5.64 U µg/Kg 5.64 µg/Kg9/12/2000 11-1-A25 614828 4791070 11 0309086-18 Cl7-BZ#170 419 µg/Kg 2.74 µg/Kg9/12/2000 11-1-A25 614828 4791070 11 0309086-18 Cl7-BZ#174 268 µg/Kg 1.83 µg/Kg9/12/2000 11-1-A25 614828 4791070 11 0309086-18 Cl7-BZ#177 133 µg/Kg 1.22 µg/Kg9/12/2000 11-1-A25 614828 4791070 11 0309086-18 Cl7-BZ#180 544 J µg/Kg 2.52 µg/Kg9/12/2000 11-1-A25 614828 4791070 11 0309086-18 Cl7-BZ#183 120 J µg/Kg 2.44 µg/Kg9/12/2000 11-1-A25 614828 4791070 11 0309086-18 Cl7-BZ#187 311 µg/Kg 2.52 µg/Kg9/12/2000 11-1-A25 614828 4791070 11 0309086-18 Cl7-BZ#189 14.0 J µg/Kg 2.90 µg/Kg9/12/2000 11-1-A25 614828 4791070 11 0309086-18 Cl8-BZ#194 8.23 J µg/Kg 2.74 µg/Kg9/12/2000 11-1-A25 614828 4791070 11 0309086-18 Cl8-BZ#195 77.1 J µg/Kg 2.74 µg/Kg9/12/2000 11-1-A25 614828 4791070 11 0309086-18 Cl8-BZ#201 97.2 µg/Kg 3.28 µg/Kg9/12/2000 11-1-A25 614828 4791070 11 0309086-18 Cl9-BZ#206 56.4 J µg/Kg 4.19 µg/Kg9/12/2000 11-1-A25 614828 4791070 11 0309086-18 Cl10-BZ#209 12.8 µg/Kg 1.14 µg/Kg



Extracted 7/30/04






DETECTION LIMIT3

9/12/2000 11-1-A25 614828 4791070 11 0309086-18 Monochlorobiphenyls 16.8 µg/Kg 1.98 µg/Kg9/12/2000 11-1-A25 614828 4791070 11 0309086-18 Dichlorobiphenyls 662 µg/Kg 12.2 µg/Kg9/12/2000 11-1-A25 614828 4791070 11 0309086-18 Trichlorobiphenyls 15800 µg/Kg 3.43 µg/Kg9/12/2000 11-1-A25 614828 4791070 11 0309086-18 Tetrachlorobiphenyls 117000 µg/Kg 5.56 µg/Kg9/12/2000 11-1-A25 614828 4791070 11 0309086-18 Pentachlorobiphenyls 56400 µg/Kg 2.59 µg/Kg9/12/2000 11-1-A25 614828 4791070 11 0309086-18 Hexachlorobiphenyls 12200 µg/Kg 4.65 µg/Kg9/12/2000 11-1-A25 614828 4791070 11 0309086-18 Heptachlorobiphenyls 1640 µg/Kg 1.60 µg/Kg9/12/2000 11-1-A25 614828 4791070 11 0309086-18 Octachlorobiphenyls 374 µg/Kg 2.29 µg/Kg9/12/2000 11-1-A25 614828 4791070 11 0309086-18 Nonachlorobiphenyls 130 µg/Kg 4.19 µg/Kg9/12/2000 11-1-A25 614828 4791070 11 0309086-18 Decachlorobiphenyl 12.8 µg/Kg 1.14 µg/Kg9/12/2000 11-1-A25 614828 4791070 11 0309086-18 Total Homologs 204000 µg/Kg 3.81 µg/Kg9/12/2000 11-1-A25 614828 4791070 11 0309086-18 Percent Moisture 11.3 % 0.1 %


2000 Short-Tailed Shrew (Blarina brevicauda) Tissue Hudson NRDA Floodplain DatabaseVersion 2.0

Extracted 7/30/04





9/10/2000 01-01-091000-10-S-STS 611675 4758823 1 0311027-01 Cl2-BZ#8 0.239 U µg/Kg 0.239 µg/Kg9/10/2000 01-01-091000-10-S-STS 611675 4758823 1 0311027-01 Cl3-BZ#18 0.531 U µg/Kg 0.531 µg/Kg9/10/2000 01-01-091000-10-S-STS 611675 4758823 1 0311027-01 Cl3-BZ#31/#28 306 µg/Kg 3.82 µg/Kg9/10/2000 01-01-091000-10-S-STS 611675 4758823 1 0311027-01 Cl4-BZ#44 4.76 µg/Kg 0.364 µg/Kg9/10/2000 01-01-091000-10-S-STS 611675 4758823 1 0311027-01 Cl4-BZ#45 0.486 U µg/Kg 0.486 µg/Kg9/10/2000 01-01-091000-10-S-STS 611675 4758823 1 0311027-01 Cl4-BZ#47 129 µg/Kg 0.617 µg/Kg9/10/2000 01-01-091000-10-S-STS 611675 4758823 1 0311027-01 Cl4-BZ#49 21.0 µg/Kg 0.303 µg/Kg9/10/2000 01-01-091000-10-S-STS 611675 4758823 1 0311027-01 Cl4-BZ#52 90.3 µg/Kg 0.344 µg/Kg9/10/2000 01-01-091000-10-S-STS 611675 4758823 1 0311027-01 Cl4-BZ#56 193 µg/Kg 0.181 µg/Kg9/10/2000 01-01-091000-10-S-STS 611675 4758823 1 0311027-01 Cl4-BZ#66 514 µg/Kg 0.242 µg/Kg9/10/2000 01-01-091000-10-S-STS 611675 4758823 1 0311027-01 Cl4-BZ#70 137 µg/Kg 0.211 µg/Kg9/10/2000 01-01-091000-10-S-STS 611675 4758823 1 0311027-01 Cl4-BZ#74 491 µg/Kg 0.372 µg/Kg9/10/2000 01-01-091000-10-S-STS 611675 4758823 1 0311027-01 Cl4-BZ#77 0.333 U µg/Kg 0.333 µg/Kg9/10/2000 01-01-091000-10-S-STS 611675 4758823 1 0311027-01 Cl4-BZ#81 0.331 U µg/Kg 0.331 µg/Kg9/10/2000 01-01-091000-10-S-STS 611675 4758823 1 0311027-01 Cl5-BZ#87 126 µg/Kg 0.147 µg/Kg9/10/2000 01-01-091000-10-S-STS 611675 4758823 1 0311027-01 Cl5-BZ#95 9.68 µg/Kg 0.114 µg/Kg9/10/2000 01-01-091000-10-S-STS 611675 4758823 1 0311027-01 Cl5-BZ#99 396 µg/Kg 0.0778 µg/Kg9/10/2000 01-01-091000-10-S-STS 611675 4758823 1 0311027-01 Cl5-BZ#101 74.6 µg/Kg 0.222 µg/Kg9/10/2000 01-01-091000-10-S-STS 611675 4758823 1 0311027-01 Cl5-BZ#105 249 µg/Kg 0.108 µg/Kg9/10/2000 01-01-091000-10-S-STS 611675 4758823 1 0311027-01 Cl5-BZ#110 47.9 µg/Kg 0.211 µg/Kg9/10/2000 01-01-091000-10-S-STS 611675 4758823 1 0311027-01 Cl5-BZ#114 20.9 µg/Kg 0.0972 µg/Kg9/10/2000 01-01-091000-10-S-STS 611675 4758823 1 0311027-01 Cl5-BZ#118 611 µg/Kg 0.228 µg/Kg9/10/2000 01-01-091000-10-S-STS 611675 4758823 1 0311027-01 Cl5-BZ#123 0.192 U µg/Kg 0.192 µg/Kg9/10/2000 01-01-091000-10-S-STS 611675 4758823 1 0311027-01 Cl5-BZ#126 0.169 U µg/Kg 0.169 µg/Kg9/10/2000 01-01-091000-10-S-STS 611675 4758823 1 0311027-01 Cl6-BZ#128 76.6 µg/Kg 0.153 µg/Kg9/10/2000 01-01-091000-10-S-STS 611675 4758823 1 0311027-01 Cl6-BZ#138 848 µg/Kg 0.496 µg/Kg9/10/2000 01-01-091000-10-S-STS 611675 4758823 1 0311027-01 Cl6-BZ#146 70.2 µg/Kg 0.139 µg/Kg9/10/2000 01-01-091000-10-S-STS 611675 4758823 1 0311027-01 Cl6-BZ#149 23.8 µg/Kg 0.178 µg/Kg9/10/2000 01-01-091000-10-S-STS 611675 4758823 1 0311027-01 Cl6-BZ#151 4.54 µg/Kg 0.294 µg/Kg9/10/2000 01-01-091000-10-S-STS 611675 4758823 1 0311027-01 Cl6-BZ#153 509 µg/Kg 0.253 µg/Kg9/10/2000 01-01-091000-10-S-STS 611675 4758823 1 0311027-01 Cl6-BZ#156 62.2 µg/Kg 0.181 µg/Kg9/10/2000 01-01-091000-10-S-STS 611675 4758823 1 0311027-01 Cl6-BZ#157 10.3 µg/Kg 0.142 µg/Kg9/10/2000 01-01-091000-10-S-STS 611675 4758823 1 0311027-01 Cl6-BZ#158 26.0 µg/Kg 0.119 µg/Kg9/10/2000 01-01-091000-10-S-STS 611675 4758823 1 0311027-01 Cl6-BZ#167 28.4 µg/Kg 0.153 µg/Kg9/10/2000 01-01-091000-10-S-STS 611675 4758823 1 0311027-01 Cl6-BZ#169 0.492 U µg/Kg 0.492 µg/Kg


DETECTION LIMIT3



Extracted 7/30/04






DETECTION LIMIT3

9/10/2000 01-01-091000-10-S-STS 611675 4758823 1 0311027-01 Cl7-BZ#170 75.5 µg/Kg 0.572 µg/Kg9/10/2000 01-01-091000-10-S-STS 611675 4758823 1 0311027-01 Cl7-BZ#174 0.117 U µg/Kg 0.117 µg/Kg9/10/2000 01-01-091000-10-S-STS 611675 4758823 1 0311027-01 Cl7-BZ#177 17.9 µg/Kg 0.164 µg/Kg9/10/2000 01-01-091000-10-S-STS 611675 4758823 1 0311027-01 Cl7-BZ#180 82.3 µg/Kg 0.244 µg/Kg9/10/2000 01-01-091000-10-S-STS 611675 4758823 1 0311027-01 Cl7-BZ#183 18.4 µg/Kg 0.111 µg/Kg9/10/2000 01-01-091000-10-S-STS 611675 4758823 1 0311027-01 Cl7-BZ#187 72.9 µg/Kg 0.122 µg/Kg9/10/2000 01-01-091000-10-S-STS 611675 4758823 1 0311027-01 Cl7-BZ#189 0.219 U µg/Kg 0.219 µg/Kg9/10/2000 01-01-091000-10-S-STS 611675 4758823 1 0311027-01 Cl8-BZ#194 0.256 U µg/Kg 0.256 µg/Kg9/10/2000 01-01-091000-10-S-STS 611675 4758823 1 0311027-01 Cl8-BZ#195 6.53 µg/Kg 0.253 µg/Kg9/10/2000 01-01-091000-10-S-STS 611675 4758823 1 0311027-01 Cl8-BZ#201 18.3 µg/Kg 0.222 µg/Kg9/10/2000 01-01-091000-10-S-STS 611675 4758823 1 0311027-01 Cl9-BZ#206 9.56 µg/Kg 0.297 µg/Kg9/10/2000 01-01-091000-10-S-STS 611675 4758823 1 0311027-01 Cl10-BZ#209 2.03 µg/Kg 0.139 µg/Kg9/10/2000 01-01-091000-10-S-STS 611675 4758823 1 0311027-01 Monochlorobiphenyls 8.17 U µg/Kg 8.17 µg/Kg9/10/2000 01-01-091000-10-S-STS 611675 4758823 1 0311027-01 Dichlorobiphenyls 0.239 U µg/Kg 0.239 µg/Kg9/10/2000 01-01-091000-10-S-STS 611675 4758823 1 0311027-01 Trichlorobiphenyls 307 µg/Kg 0.819 µg/Kg9/10/2000 01-01-091000-10-S-STS 611675 4758823 1 0311027-01 Tetrachlorobiphenyls 1820 µg/Kg 0.128 µg/Kg9/10/2000 01-01-091000-10-S-STS 611675 4758823 1 0311027-01 Pentachlorobiphenyls 2780 µg/Kg 0.147 µg/Kg9/10/2000 01-01-091000-10-S-STS 611675 4758823 1 0311027-01 Hexachlorobiphenyls 1710 µg/Kg 0.233 µg/Kg9/10/2000 01-01-091000-10-S-STS 611675 4758823 1 0311027-01 Heptachlorobiphenyls 250 µg/Kg 0.128 µg/Kg9/10/2000 01-01-091000-10-S-STS 611675 4758823 1 0311027-01 Octachlorobiphenyls 36.2 µg/Kg 0.117 µg/Kg9/10/2000 01-01-091000-10-S-STS 611675 4758823 1 0311027-01 Nonachlorobiphenyls 14.6 µg/Kg 0.297 µg/Kg9/10/2000 01-01-091000-10-S-STS 611675 4758823 1 0311027-01 Decachlorobiphenyl 2.03 µg/Kg 0.139 µg/Kg9/10/2000 01-01-091000-10-S-STS 611675 4758823 1 0311027-01 Total Homologs 6920 µg/Kg 0.139 µg/Kg9/10/2000 01-01-091000-10-S-STS 611675 4758823 1 0311027-01 Percent Lipids 3.3 % 0.1 %9/13/2000 01-02-091300-15-S-STS 611675 4758823 1 0311027-02 Cl2-BZ#8 0.357 U µg/Kg 0.357 µg/Kg9/13/2000 01-02-091300-15-S-STS 611675 4758823 1 0311027-02 Cl3-BZ#18 0.794 U µg/Kg 0.794 µg/Kg9/13/2000 01-02-091300-15-S-STS 611675 4758823 1 0311027-02 Cl3-BZ#31/#28 345 µg/Kg 5.72 µg/Kg9/13/2000 01-02-091300-15-S-STS 611675 4758823 1 0311027-02 Cl4-BZ#44 4.03 µg/Kg 0.544 µg/Kg9/13/2000 01-02-091300-15-S-STS 611675 4758823 1 0311027-02 Cl4-BZ#45 0.727 U µg/Kg 0.727 µg/Kg9/13/2000 01-02-091300-15-S-STS 611675 4758823 1 0311027-02 Cl4-BZ#47 131 µg/Kg 0.923 µg/Kg9/13/2000 01-02-091300-15-S-STS 611675 4758823 1 0311027-02 Cl4-BZ#49 18.6 µg/Kg 0.453 µg/Kg9/13/2000 01-02-091300-15-S-STS 611675 4758823 1 0311027-02 Cl4-BZ#52 65.6 µg/Kg 0.515 µg/Kg9/13/2000 01-02-091300-15-S-STS 611675 4758823 1 0311027-02 Cl4-BZ#56 217 µg/Kg 0.270 µg/Kg9/13/2000 01-02-091300-15-S-STS 611675 4758823 1 0311027-02 Cl4-BZ#66 694 µg/Kg 0.362 µg/Kg9/13/2000 01-02-091300-15-S-STS 611675 4758823 1 0311027-02 Cl4-BZ#70 152 µg/Kg 0.316 µg/Kg



Extracted 7/30/04






DETECTION LIMIT3

9/13/2000 01-02-091300-15-S-STS 611675 4758823 1 0311027-02 Cl4-BZ#74 634 µg/Kg 0.557 µg/Kg9/13/2000 01-02-091300-15-S-STS 611675 4758823 1 0311027-02 Cl4-BZ#77 0.499 U µg/Kg 0.499 µg/Kg9/13/2000 01-02-091300-15-S-STS 611675 4758823 1 0311027-02 Cl4-BZ#81 0.495 U µg/Kg 0.495 µg/Kg9/13/2000 01-02-091300-15-S-STS 611675 4758823 1 0311027-02 Cl5-BZ#87 125 µg/Kg 0.220 µg/Kg9/13/2000 01-02-091300-15-S-STS 611675 4758823 1 0311027-02 Cl5-BZ#95 7.46 µg/Kg 0.170 µg/Kg9/13/2000 01-02-091300-15-S-STS 611675 4758823 1 0311027-02 Cl5-BZ#99 419 µg/Kg 0.116 µg/Kg9/13/2000 01-02-091300-15-S-STS 611675 4758823 1 0311027-02 Cl5-BZ#101 57.1 µg/Kg 0.333 µg/Kg9/13/2000 01-02-091300-15-S-STS 611675 4758823 1 0311027-02 Cl5-BZ#105 272 µg/Kg 0.162 µg/Kg9/13/2000 01-02-091300-15-S-STS 611675 4758823 1 0311027-02 Cl5-BZ#110 29.8 µg/Kg 0.316 µg/Kg9/13/2000 01-02-091300-15-S-STS 611675 4758823 1 0311027-02 Cl5-BZ#114 24.8 µg/Kg 0.146 µg/Kg9/13/2000 01-02-091300-15-S-STS 611675 4758823 1 0311027-02 Cl5-BZ#118 730 µg/Kg 0.341 µg/Kg9/13/2000 01-02-091300-15-S-STS 611675 4758823 1 0311027-02 Cl5-BZ#123 0.287 U µg/Kg 0.287 µg/Kg9/13/2000 01-02-091300-15-S-STS 611675 4758823 1 0311027-02 Cl5-BZ#126 0.254 U µg/Kg 0.254 µg/Kg9/13/2000 01-02-091300-15-S-STS 611675 4758823 1 0311027-02 Cl6-BZ#128 33.9 µg/Kg 0.229 µg/Kg9/13/2000 01-02-091300-15-S-STS 611675 4758823 1 0311027-02 Cl6-BZ#138 702 µg/Kg 0.328 µg/Kg9/13/2000 01-02-091300-15-S-STS 611675 4758823 1 0311027-02 Cl6-BZ#146 58.0 µg/Kg 0.208 µg/Kg9/13/2000 01-02-091300-15-S-STS 611675 4758823 1 0311027-02 Cl6-BZ#149 15.3 µg/Kg 0.266 µg/Kg9/13/2000 01-02-091300-15-S-STS 611675 4758823 1 0311027-02 Cl6-BZ#151 3.72 µg/Kg 0.441 µg/Kg9/13/2000 01-02-091300-15-S-STS 611675 4758823 1 0311027-02 Cl6-BZ#153 472 µg/Kg 0.378 µg/Kg9/13/2000 01-02-091300-15-S-STS 611675 4758823 1 0311027-02 Cl6-BZ#156 62.2 µg/Kg 0.270 µg/Kg9/13/2000 01-02-091300-15-S-STS 611675 4758823 1 0311027-02 Cl6-BZ#157 10.3 µg/Kg 0.212 µg/Kg9/13/2000 01-02-091300-15-S-STS 611675 4758823 1 0311027-02 Cl6-BZ#158 18.6 µg/Kg 0.179 µg/Kg9/13/2000 01-02-091300-15-S-STS 611675 4758823 1 0311027-02 Cl6-BZ#167 22.8 µg/Kg 0.229 µg/Kg9/13/2000 01-02-091300-15-S-STS 611675 4758823 1 0311027-02 Cl6-BZ#169 0.736 U µg/Kg 0.736 µg/Kg9/13/2000 01-02-091300-15-S-STS 611675 4758823 1 0311027-02 Cl7-BZ#170 54.0 µg/Kg 0.856 µg/Kg9/13/2000 01-02-091300-15-S-STS 611675 4758823 1 0311027-02 Cl7-BZ#174 0.175 U µg/Kg 0.175 µg/Kg9/13/2000 01-02-091300-15-S-STS 611675 4758823 1 0311027-02 Cl7-BZ#177 0.245 U µg/Kg 0.245 µg/Kg9/13/2000 01-02-091300-15-S-STS 611675 4758823 1 0311027-02 Cl7-BZ#180 73.7 µg/Kg 0.366 µg/Kg9/13/2000 01-02-091300-15-S-STS 611675 4758823 1 0311027-02 Cl7-BZ#183 12.5 µg/Kg 0.166 µg/Kg9/13/2000 01-02-091300-15-S-STS 611675 4758823 1 0311027-02 Cl7-BZ#187 55.4 µg/Kg 0.183 µg/Kg9/13/2000 01-02-091300-15-S-STS 611675 4758823 1 0311027-02 Cl7-BZ#189 0.328 U µg/Kg 0.328 µg/Kg9/13/2000 01-02-091300-15-S-STS 611675 4758823 1 0311027-02 Cl8-BZ#194 0.382 U µg/Kg 0.382 µg/Kg9/13/2000 01-02-091300-15-S-STS 611675 4758823 1 0311027-02 Cl8-BZ#195 5.32 µg/Kg 0.378 µg/Kg9/13/2000 01-02-091300-15-S-STS 611675 4758823 1 0311027-02 Cl8-BZ#201 14.0 µg/Kg 0.333 µg/Kg9/13/2000 01-02-091300-15-S-STS 611675 4758823 1 0311027-02 Cl9-BZ#206 7.21 µg/Kg 0.445 µg/Kg



Extracted 7/30/04






DETECTION LIMIT3

9/13/2000 01-02-091300-15-S-STS 611675 4758823 1 0311027-02 Cl10-BZ#209 0.208 U µg/Kg 0.208 µg/Kg9/13/2000 01-02-091300-15-S-STS 611675 4758823 1 0311027-02 Monochlorobiphenyls 12.2 U µg/Kg 12.2 µg/Kg9/13/2000 01-02-091300-15-S-STS 611675 4758823 1 0311027-02 Dichlorobiphenyls 0.357 U µg/Kg 0.357 µg/Kg9/13/2000 01-02-091300-15-S-STS 611675 4758823 1 0311027-02 Trichlorobiphenyls 341 µg/Kg 1.23 µg/Kg9/13/2000 01-02-091300-15-S-STS 611675 4758823 1 0311027-02 Tetrachlorobiphenyls 2170 µg/Kg 0.191 µg/Kg9/13/2000 01-02-091300-15-S-STS 611675 4758823 1 0311027-02 Pentachlorobiphenyls 2990 µg/Kg 0.220 µg/Kg9/13/2000 01-02-091300-15-S-STS 611675 4758823 1 0311027-02 Hexachlorobiphenyls 1500 µg/Kg 0.349 µg/Kg9/13/2000 01-02-091300-15-S-STS 611675 4758823 1 0311027-02 Heptachlorobiphenyls 188 µg/Kg 0.191 µg/Kg9/13/2000 01-02-091300-15-S-STS 611675 4758823 1 0311027-02 Octachlorobiphenyls 10.8 µg/Kg 0.175 µg/Kg9/13/2000 01-02-091300-15-S-STS 611675 4758823 1 0311027-02 Nonachlorobiphenyls 13.0 µg/Kg 0.445 µg/Kg9/13/2000 01-02-091300-15-S-STS 611675 4758823 1 0311027-02 Decachlorobiphenyl 0.208 U µg/Kg 0.208 µg/Kg9/13/2000 01-02-091300-15-S-STS 611675 4758823 1 0311027-02 Total Homologs 7220 µg/Kg 0.208 µg/Kg9/13/2000 01-02-091300-15-S-STS 611675 4758823 1 0311027-02 Percent Lipids 3.3 % 0.1 %9/13/2000 01-03-091300-10-S-STS 611675 4758823 1 0311027-03 Cl2-BZ#8 0.154 U µg/Kg 0.154 µg/Kg9/13/2000 01-03-091300-10-S-STS 611675 4758823 1 0311027-03 Cl3-BZ#18 0.343 U µg/Kg 0.343 µg/Kg9/13/2000 01-03-091300-10-S-STS 611675 4758823 1 0311027-03 Cl3-BZ#31/#28 21.6 µg/Kg 2.47 µg/Kg9/13/2000 01-03-091300-10-S-STS 611675 4758823 1 0311027-03 Cl4-BZ#44 0.235 U µg/Kg 0.235 µg/Kg9/13/2000 01-03-091300-10-S-STS 611675 4758823 1 0311027-03 Cl4-BZ#45 0.314 U µg/Kg 0.314 µg/Kg9/13/2000 01-03-091300-10-S-STS 611675 4758823 1 0311027-03 Cl4-BZ#47 3.78 µg/Kg 0.398 µg/Kg9/13/2000 01-03-091300-10-S-STS 611675 4758823 1 0311027-03 Cl4-BZ#49 0.538 J µg/Kg 0.195 µg/Kg9/13/2000 01-03-091300-10-S-STS 611675 4758823 1 0311027-03 Cl4-BZ#52 1.42 µg/Kg 0.222 µg/Kg9/13/2000 01-03-091300-10-S-STS 611675 4758823 1 0311027-03 Cl4-BZ#56 8.26 µg/Kg 0.116 µg/Kg9/13/2000 01-03-091300-10-S-STS 611675 4758823 1 0311027-03 Cl4-BZ#66 23.8 µg/Kg 0.156 µg/Kg9/13/2000 01-03-091300-10-S-STS 611675 4758823 1 0311027-03 Cl4-BZ#70 13.0 µg/Kg 0.136 µg/Kg9/13/2000 01-03-091300-10-S-STS 611675 4758823 1 0311027-03 Cl4-BZ#74 16.6 µg/Kg 0.240 µg/Kg9/13/2000 01-03-091300-10-S-STS 611675 4758823 1 0311027-03 Cl4-BZ#77 0.215 U µg/Kg 0.215 µg/Kg9/13/2000 01-03-091300-10-S-STS 611675 4758823 1 0311027-03 Cl4-BZ#81 0.213 U µg/Kg 0.213 µg/Kg9/13/2000 01-03-091300-10-S-STS 611675 4758823 1 0311027-03 Cl5-BZ#87 4.15 µg/Kg 0.0950 µg/Kg9/13/2000 01-03-091300-10-S-STS 611675 4758823 1 0311027-03 Cl5-BZ#95 0.412 µg/Kg 0.0735 µg/Kg9/13/2000 01-03-091300-10-S-STS 611675 4758823 1 0311027-03 Cl5-BZ#99 11.6 µg/Kg 0.0502 µg/Kg9/13/2000 01-03-091300-10-S-STS 611675 4758823 1 0311027-03 Cl5-BZ#101 2.55 µg/Kg 0.143 µg/Kg9/13/2000 01-03-091300-10-S-STS 611675 4758823 1 0311027-03 Cl5-BZ#105 6.95 µg/Kg 0.0699 µg/Kg9/13/2000 01-03-091300-10-S-STS 611675 4758823 1 0311027-03 Cl5-BZ#110 3.38 µg/Kg 0.136 µg/Kg9/13/2000 01-03-091300-10-S-STS 611675 4758823 1 0311027-03 Cl5-BZ#114 0.646 µg/Kg 0.0628 µg/Kg9/13/2000 01-03-091300-10-S-STS 611675 4758823 1 0311027-03 Cl5-BZ#118 15.3 µg/Kg 0.147 µg/Kg



Extracted 7/30/04






DETECTION LIMIT3

9/13/2000 01-03-091300-10-S-STS 611675 4758823 1 0311027-03 Cl5-BZ#123 0.124 U µg/Kg 0.124 µg/Kg9/13/2000 01-03-091300-10-S-STS 611675 4758823 1 0311027-03 Cl5-BZ#126 0.109 U µg/Kg 0.109 µg/Kg9/13/2000 01-03-091300-10-S-STS 611675 4758823 1 0311027-03 Cl6-BZ#128 1.06 µg/Kg 0.0986 µg/Kg9/13/2000 01-03-091300-10-S-STS 611675 4758823 1 0311027-03 Cl6-BZ#138 24.2 µg/Kg 0.142 µg/Kg9/13/2000 01-03-091300-10-S-STS 611675 4758823 1 0311027-03 Cl6-BZ#146 2.65 µg/Kg 0.0896 µg/Kg9/13/2000 01-03-091300-10-S-STS 611675 4758823 1 0311027-03 Cl6-BZ#149 1.57 µg/Kg 0.115 µg/Kg9/13/2000 01-03-091300-10-S-STS 611675 4758823 1 0311027-03 Cl6-BZ#151 0.190 U µg/Kg 0.190 µg/Kg9/13/2000 01-03-091300-10-S-STS 611675 4758823 1 0311027-03 Cl6-BZ#153 12.7 µg/Kg 0.163 µg/Kg9/13/2000 01-03-091300-10-S-STS 611675 4758823 1 0311027-03 Cl6-BZ#156 1.08 µg/Kg 0.116 µg/Kg9/13/2000 01-03-091300-10-S-STS 611675 4758823 1 0311027-03 Cl6-BZ#157 0.251 J µg/Kg 0.0914 µg/Kg9/13/2000 01-03-091300-10-S-STS 611675 4758823 1 0311027-03 Cl6-BZ#158 1.00 µg/Kg 0.0771 µg/Kg9/13/2000 01-03-091300-10-S-STS 611675 4758823 1 0311027-03 Cl6-BZ#167 0.619 µg/Kg 0.0986 µg/Kg9/13/2000 01-03-091300-10-S-STS 611675 4758823 1 0311027-03 Cl6-BZ#169 0.317 U µg/Kg 0.317 µg/Kg9/13/2000 01-03-091300-10-S-STS 611675 4758823 1 0311027-03 Cl7-BZ#170 0.369 U µg/Kg 0.369 µg/Kg9/13/2000 01-03-091300-10-S-STS 611675 4758823 1 0311027-03 Cl7-BZ#174 0.0753 U µg/Kg 0.0753 µg/Kg9/13/2000 01-03-091300-10-S-STS 611675 4758823 1 0311027-03 Cl7-BZ#177 0.106 U µg/Kg 0.106 µg/Kg9/13/2000 01-03-091300-10-S-STS 611675 4758823 1 0311027-03 Cl7-BZ#180 0.158 U µg/Kg 0.158 µg/Kg9/13/2000 01-03-091300-10-S-STS 611675 4758823 1 0311027-03 Cl7-BZ#183 0.394 µg/Kg 0.0717 µg/Kg9/13/2000 01-03-091300-10-S-STS 611675 4758823 1 0311027-03 Cl7-BZ#187 5.28 µg/Kg 0.0789 µg/Kg9/13/2000 01-03-091300-10-S-STS 611675 4758823 1 0311027-03 Cl7-BZ#189 0.142 U µg/Kg 0.142 µg/Kg9/13/2000 01-03-091300-10-S-STS 611675 4758823 1 0311027-03 Cl8-BZ#194 0.165 U µg/Kg 0.165 µg/Kg9/13/2000 01-03-091300-10-S-STS 611675 4758823 1 0311027-03 Cl8-BZ#195 0.163 U µg/Kg 0.163 µg/Kg9/13/2000 01-03-091300-10-S-STS 611675 4758823 1 0311027-03 Cl8-BZ#201 1.07 µg/Kg 0.143 µg/Kg9/13/2000 01-03-091300-10-S-STS 611675 4758823 1 0311027-03 Cl9-BZ#206 0.192 U µg/Kg 0.192 µg/Kg9/13/2000 01-03-091300-10-S-STS 611675 4758823 1 0311027-03 Cl10-BZ#209 0.0896 U µg/Kg 0.0896 µg/Kg9/13/2000 01-03-091300-10-S-STS 611675 4758823 1 0311027-03 Monochlorobiphenyls 5.27 U µg/Kg 5.27 µg/Kg9/13/2000 01-03-091300-10-S-STS 611675 4758823 1 0311027-03 Dichlorobiphenyls 0.154 U µg/Kg 0.154 µg/Kg9/13/2000 01-03-091300-10-S-STS 611675 4758823 1 0311027-03 Trichlorobiphenyls 22.2 µg/Kg 0.529 µg/Kg9/13/2000 01-03-091300-10-S-STS 611675 4758823 1 0311027-03 Tetrachlorobiphenyls 80.0 µg/Kg 0.0825 µg/Kg9/13/2000 01-03-091300-10-S-STS 611675 4758823 1 0311027-03 Pentachlorobiphenyls 86.5 µg/Kg 0.0950 µg/Kg9/13/2000 01-03-091300-10-S-STS 611675 4758823 1 0311027-03 Hexachlorobiphenyls 50.2 µg/Kg 0.151 µg/Kg9/13/2000 01-03-091300-10-S-STS 611675 4758823 1 0311027-03 Heptachlorobiphenyls 15.0 µg/Kg 0.0825 µg/Kg9/13/2000 01-03-091300-10-S-STS 611675 4758823 1 0311027-03 Octachlorobiphenyls 0.726 µg/Kg 0.0753 µg/Kg9/13/2000 01-03-091300-10-S-STS 611675 4758823 1 0311027-03 Nonachlorobiphenyls 0.192 U µg/Kg 0.192 µg/Kg9/13/2000 01-03-091300-10-S-STS 611675 4758823 1 0311027-03 Decachlorobiphenyl 0.0896 U µg/Kg 0.0896 µg/Kg



Extracted 7/30/04






DETECTION LIMIT3

9/13/2000 01-03-091300-10-S-STS 611675 4758823 1 0311027-03 Total Homologs 255 µg/Kg 0.0896 µg/Kg9/13/2000 01-03-091300-10-S-STS 611675 4758823 1 0311027-03 Percent Lipids 5.1 % 0.1 %9/12/2000 07-01-091200-35-S-STS 614704 4781156 7 0311027-04 Cl2-BZ#8 0.150 U µg/Kg 0.150 µg/Kg9/12/2000 07-01-091200-35-S-STS 614704 4781156 7 0311027-04 Cl3-BZ#18 0.333 U µg/Kg 0.333 µg/Kg9/12/2000 07-01-091200-35-S-STS 614704 4781156 7 0311027-04 Cl3-BZ#31/#28 18.4 µg/Kg 2.40 µg/Kg9/12/2000 07-01-091200-35-S-STS 614704 4781156 7 0311027-04 Cl4-BZ#44 0.228 U µg/Kg 0.228 µg/Kg9/12/2000 07-01-091200-35-S-STS 614704 4781156 7 0311027-04 Cl4-BZ#45 0.305 U µg/Kg 0.305 µg/Kg9/12/2000 07-01-091200-35-S-STS 614704 4781156 7 0311027-04 Cl4-BZ#47 18.4 µg/Kg 0.387 µg/Kg9/12/2000 07-01-091200-35-S-STS 614704 4781156 7 0311027-04 Cl4-BZ#49 0.190 U µg/Kg 0.190 µg/Kg9/12/2000 07-01-091200-35-S-STS 614704 4781156 7 0311027-04 Cl4-BZ#52 1.01 J µg/Kg 0.216 µg/Kg9/12/2000 07-01-091200-35-S-STS 614704 4781156 7 0311027-04 Cl4-BZ#56 19.4 µg/Kg 0.113 µg/Kg9/12/2000 07-01-091200-35-S-STS 614704 4781156 7 0311027-04 Cl4-BZ#66 64.5 µg/Kg 0.152 µg/Kg9/12/2000 07-01-091200-35-S-STS 614704 4781156 7 0311027-04 Cl4-BZ#70 15.3 µg/Kg 0.132 µg/Kg9/12/2000 07-01-091200-35-S-STS 614704 4781156 7 0311027-04 Cl4-BZ#74 52.8 µg/Kg 0.234 µg/Kg9/12/2000 07-01-091200-35-S-STS 614704 4781156 7 0311027-04 Cl4-BZ#77 0.209 U µg/Kg 0.209 µg/Kg9/12/2000 07-01-091200-35-S-STS 614704 4781156 7 0311027-04 Cl4-BZ#81 0.207 U µg/Kg 0.207 µg/Kg9/12/2000 07-01-091200-35-S-STS 614704 4781156 7 0311027-04 Cl5-BZ#87 13.5 µg/Kg 0.0924 µg/Kg9/12/2000 07-01-091200-35-S-STS 614704 4781156 7 0311027-04 Cl5-BZ#95 0.0715 U µg/Kg 0.0715 µg/Kg9/12/2000 07-01-091200-35-S-STS 614704 4781156 7 0311027-04 Cl5-BZ#99 47.8 µg/Kg 0.0488 µg/Kg9/12/2000 07-01-091200-35-S-STS 614704 4781156 7 0311027-04 Cl5-BZ#101 5.28 µg/Kg 0.140 µg/Kg9/12/2000 07-01-091200-35-S-STS 614704 4781156 7 0311027-04 Cl5-BZ#105 30.8 µg/Kg 0.0680 µg/Kg9/12/2000 07-01-091200-35-S-STS 614704 4781156 7 0311027-04 Cl5-BZ#110 1.05 µg/Kg 0.132 µg/Kg9/12/2000 07-01-091200-35-S-STS 614704 4781156 7 0311027-04 Cl5-BZ#114 2.83 µg/Kg 0.0610 µg/Kg9/12/2000 07-01-091200-35-S-STS 614704 4781156 7 0311027-04 Cl5-BZ#118 67.8 µg/Kg 0.143 µg/Kg9/12/2000 07-01-091200-35-S-STS 614704 4781156 7 0311027-04 Cl5-BZ#123 0.120 U µg/Kg 0.120 µg/Kg9/12/2000 07-01-091200-35-S-STS 614704 4781156 7 0311027-04 Cl5-BZ#126 0.106 U µg/Kg 0.106 µg/Kg9/12/2000 07-01-091200-35-S-STS 614704 4781156 7 0311027-04 Cl6-BZ#128 5.77 µg/Kg 0.0959 µg/Kg9/12/2000 07-01-091200-35-S-STS 614704 4781156 7 0311027-04 Cl6-BZ#138 91.6 µg/Kg 0.138 µg/Kg9/12/2000 07-01-091200-35-S-STS 614704 4781156 7 0311027-04 Cl6-BZ#146 13.5 µg/Kg 0.0872 µg/Kg9/12/2000 07-01-091200-35-S-STS 614704 4781156 7 0311027-04 Cl6-BZ#149 1.14 µg/Kg 0.112 µg/Kg9/12/2000 07-01-091200-35-S-STS 614704 4781156 7 0311027-04 Cl6-BZ#151 0.185 U µg/Kg 0.185 µg/Kg9/12/2000 07-01-091200-35-S-STS 614704 4781156 7 0311027-04 Cl6-BZ#153 69.9 µg/Kg 0.159 µg/Kg9/12/2000 07-01-091200-35-S-STS 614704 4781156 7 0311027-04 Cl6-BZ#156 7.40 µg/Kg 0.113 µg/Kg9/12/2000 07-01-091200-35-S-STS 614704 4781156 7 0311027-04 Cl6-BZ#157 1.19 µg/Kg 0.0889 µg/Kg9/12/2000 07-01-091200-35-S-STS 614704 4781156 7 0311027-04 Cl6-BZ#158 2.99 µg/Kg 0.0750 µg/Kg



Extracted 7/30/04






DETECTION LIMIT3

9/12/2000 07-01-091200-35-S-STS 614704 4781156 7 0311027-04 Cl6-BZ#167 3.67 µg/Kg 0.0959 µg/Kg9/12/2000 07-01-091200-35-S-STS 614704 4781156 7 0311027-04 Cl6-BZ#169 0.309 U µg/Kg 0.309 µg/Kg9/12/2000 07-01-091200-35-S-STS 614704 4781156 7 0311027-04 Cl7-BZ#170 0.359 U µg/Kg 0.359 µg/Kg9/12/2000 07-01-091200-35-S-STS 614704 4781156 7 0311027-04 Cl7-BZ#174 0.0732 U µg/Kg 0.0732 µg/Kg9/12/2000 07-01-091200-35-S-STS 614704 4781156 7 0311027-04 Cl7-BZ#177 0.103 U µg/Kg 0.103 µg/Kg9/12/2000 07-01-091200-35-S-STS 614704 4781156 7 0311027-04 Cl7-BZ#180 0.154 U µg/Kg 0.154 µg/Kg9/12/2000 07-01-091200-35-S-STS 614704 4781156 7 0311027-04 Cl7-BZ#183 3.71 µg/Kg 0.0698 µg/Kg9/12/2000 07-01-091200-35-S-STS 614704 4781156 7 0311027-04 Cl7-BZ#187 17.1 µg/Kg 0.0767 µg/Kg9/12/2000 07-01-091200-35-S-STS 614704 4781156 7 0311027-04 Cl7-BZ#189 0.138 U µg/Kg 0.138 µg/Kg9/12/2000 07-01-091200-35-S-STS 614704 4781156 7 0311027-04 Cl8-BZ#194 0.161 U µg/Kg 0.161 µg/Kg9/12/2000 07-01-091200-35-S-STS 614704 4781156 7 0311027-04 Cl8-BZ#195 0.159 U µg/Kg 0.159 µg/Kg9/12/2000 07-01-091200-35-S-STS 614704 4781156 7 0311027-04 Cl8-BZ#201 3.03 µg/Kg 0.140 µg/Kg9/12/2000 07-01-091200-35-S-STS 614704 4781156 7 0311027-04 Cl9-BZ#206 0.187 U µg/Kg 0.187 µg/Kg9/12/2000 07-01-091200-35-S-STS 614704 4781156 7 0311027-04 Cl10-BZ#209 2.76 µg/Kg 0.0872 µg/Kg9/12/2000 07-01-091200-35-S-STS 614704 4781156 7 0311027-04 Monochlorobiphenyls 5.13 U µg/Kg 5.13 µg/Kg9/12/2000 07-01-091200-35-S-STS 614704 4781156 7 0311027-04 Dichlorobiphenyls 0.150 U µg/Kg 0.150 µg/Kg9/12/2000 07-01-091200-35-S-STS 614704 4781156 7 0311027-04 Trichlorobiphenyls 18.4 µg/Kg 0.515 µg/Kg9/12/2000 07-01-091200-35-S-STS 614704 4781156 7 0311027-04 Tetrachlorobiphenyls 201 µg/Kg 0.0802 µg/Kg9/12/2000 07-01-091200-35-S-STS 614704 4781156 7 0311027-04 Pentachlorobiphenyls 316 µg/Kg 0.0924 µg/Kg9/12/2000 07-01-091200-35-S-STS 614704 4781156 7 0311027-04 Hexachlorobiphenyls 203 µg/Kg 0.147 µg/Kg9/12/2000 07-01-091200-35-S-STS 614704 4781156 7 0311027-04 Heptachlorobiphenyls 40.4 µg/Kg 0.0802 µg/Kg9/12/2000 07-01-091200-35-S-STS 614704 4781156 7 0311027-04 Octachlorobiphenyls 2.93 µg/Kg 0.0732 µg/Kg9/12/2000 07-01-091200-35-S-STS 614704 4781156 7 0311027-04 Nonachlorobiphenyls 0.187 U µg/Kg 0.187 µg/Kg9/12/2000 07-01-091200-35-S-STS 614704 4781156 7 0311027-04 Decachlorobiphenyl 2.76 µg/Kg 0.0872 µg/Kg9/12/2000 07-01-091200-35-S-STS 614704 4781156 7 0311027-04 Total Homologs 785 µg/Kg 0.0872 µg/Kg9/12/2000 07-01-091200-35-S-STS 614704 4781156 7 0311027-04 Percent Lipids 5.1 % 0.1 %9/12/2000 07-02-091200-35-S-STS 614704 4781156 7 0311027-05 Cl2-BZ#8 0.168 U µg/Kg 0.168 µg/Kg9/12/2000 07-02-091200-35-S-STS 614704 4781156 7 0311027-05 Cl3-BZ#18 0.373 U µg/Kg 0.373 µg/Kg9/12/2000 07-02-091200-35-S-STS 614704 4781156 7 0311027-05 Cl3-BZ#31/#28 51.9 µg/Kg 2.69 µg/Kg9/12/2000 07-02-091200-35-S-STS 614704 4781156 7 0311027-05 Cl4-BZ#44 0.256 U µg/Kg 0.256 µg/Kg9/12/2000 07-02-091200-35-S-STS 614704 4781156 7 0311027-05 Cl4-BZ#45 0.342 U µg/Kg 0.342 µg/Kg9/12/2000 07-02-091200-35-S-STS 614704 4781156 7 0311027-05 Cl4-BZ#47 20.9 µg/Kg 0.434 µg/Kg9/12/2000 07-02-091200-35-S-STS 614704 4781156 7 0311027-05 Cl4-BZ#49 3.36 µg/Kg 0.213 µg/Kg9/12/2000 07-02-091200-35-S-STS 614704 4781156 7 0311027-05 Cl4-BZ#52 6.01 µg/Kg 0.242 µg/Kg9/12/2000 07-02-091200-35-S-STS 614704 4781156 7 0311027-05 Cl4-BZ#56 58.7 µg/Kg 0.127 µg/Kg



Extracted 7/30/04






DETECTION LIMIT3

9/12/2000 07-02-091200-35-S-STS 614704 4781156 7 0311027-05 Cl4-BZ#66 180 µg/Kg 0.170 µg/Kg9/12/2000 07-02-091200-35-S-STS 614704 4781156 7 0311027-05 Cl4-BZ#70 41.6 µg/Kg 0.148 µg/Kg9/12/2000 07-02-091200-35-S-STS 614704 4781156 7 0311027-05 Cl4-BZ#74 171 µg/Kg 0.262 µg/Kg9/12/2000 07-02-091200-35-S-STS 614704 4781156 7 0311027-05 Cl4-BZ#77 0.235 U µg/Kg 0.235 µg/Kg9/12/2000 07-02-091200-35-S-STS 614704 4781156 7 0311027-05 Cl4-BZ#81 0.233 U µg/Kg 0.233 µg/Kg9/12/2000 07-02-091200-35-S-STS 614704 4781156 7 0311027-05 Cl5-BZ#87 38.9 µg/Kg 0.104 µg/Kg9/12/2000 07-02-091200-35-S-STS 614704 4781156 7 0311027-05 Cl5-BZ#95 1.48 µg/Kg 0.0801 µg/Kg9/12/2000 07-02-091200-35-S-STS 614704 4781156 7 0311027-05 Cl5-BZ#99 155 µg/Kg 0.0547 µg/Kg9/12/2000 07-02-091200-35-S-STS 614704 4781156 7 0311027-05 Cl5-BZ#101 12.6 µg/Kg 0.156 µg/Kg9/12/2000 07-02-091200-35-S-STS 614704 4781156 7 0311027-05 Cl5-BZ#105 97.3 µg/Kg 0.0762 µg/Kg9/12/2000 07-02-091200-35-S-STS 614704 4781156 7 0311027-05 Cl5-BZ#110 7.39 µg/Kg 0.148 µg/Kg9/12/2000 07-02-091200-35-S-STS 614704 4781156 7 0311027-05 Cl5-BZ#114 9.11 µg/Kg 0.0684 µg/Kg9/12/2000 07-02-091200-35-S-STS 614704 4781156 7 0311027-05 Cl5-BZ#118 254 µg/Kg 0.160 µg/Kg9/12/2000 07-02-091200-35-S-STS 614704 4781156 7 0311027-05 Cl5-BZ#123 0.135 U µg/Kg 0.135 µg/Kg9/12/2000 07-02-091200-35-S-STS 614704 4781156 7 0311027-05 Cl5-BZ#126 0.119 U µg/Kg 0.119 µg/Kg9/12/2000 07-02-091200-35-S-STS 614704 4781156 7 0311027-05 Cl6-BZ#128 17.6 µg/Kg 0.108 µg/Kg9/12/2000 07-02-091200-35-S-STS 614704 4781156 7 0311027-05 Cl6-BZ#138 354 µg/Kg 0.154 µg/Kg9/12/2000 07-02-091200-35-S-STS 614704 4781156 7 0311027-05 Cl6-BZ#146 40.9 µg/Kg 0.0977 µg/Kg9/12/2000 07-02-091200-35-S-STS 614704 4781156 7 0311027-05 Cl6-BZ#149 3.88 µg/Kg 0.125 µg/Kg9/12/2000 07-02-091200-35-S-STS 614704 4781156 7 0311027-05 Cl6-BZ#151 1.06 µg/Kg 0.207 µg/Kg9/12/2000 07-02-091200-35-S-STS 614704 4781156 7 0311027-05 Cl6-BZ#153 269 µg/Kg 0.178 µg/Kg9/12/2000 07-02-091200-35-S-STS 614704 4781156 7 0311027-05 Cl6-BZ#156 25.3 µg/Kg 0.127 µg/Kg9/12/2000 07-02-091200-35-S-STS 614704 4781156 7 0311027-05 Cl6-BZ#157 3.80 µg/Kg 0.0997 µg/Kg9/12/2000 07-02-091200-35-S-STS 614704 4781156 7 0311027-05 Cl6-BZ#158 6.60 µg/Kg 0.0840 µg/Kg9/12/2000 07-02-091200-35-S-STS 614704 4781156 7 0311027-05 Cl6-BZ#167 12.4 µg/Kg 0.108 µg/Kg9/12/2000 07-02-091200-35-S-STS 614704 4781156 7 0311027-05 Cl6-BZ#169 0.346 U µg/Kg 0.346 µg/Kg9/12/2000 07-02-091200-35-S-STS 614704 4781156 7 0311027-05 Cl7-BZ#170 0.403 U µg/Kg 0.403 µg/Kg9/12/2000 07-02-091200-35-S-STS 614704 4781156 7 0311027-05 Cl7-BZ#174 0.0821 U µg/Kg 0.0821 µg/Kg9/12/2000 07-02-091200-35-S-STS 614704 4781156 7 0311027-05 Cl7-BZ#177 0.115 U µg/Kg 0.115 µg/Kg9/12/2000 07-02-091200-35-S-STS 614704 4781156 7 0311027-05 Cl7-BZ#180 42.2 µg/Kg 0.172 µg/Kg9/12/2000 07-02-091200-35-S-STS 614704 4781156 7 0311027-05 Cl7-BZ#183 5.74 µg/Kg 0.0782 µg/Kg9/12/2000 07-02-091200-35-S-STS 614704 4781156 7 0311027-05 Cl7-BZ#187 36.3 µg/Kg 0.0860 µg/Kg9/12/2000 07-02-091200-35-S-STS 614704 4781156 7 0311027-05 Cl7-BZ#189 19.1 µg/Kg 0.154 µg/Kg9/12/2000 07-02-091200-35-S-STS 614704 4781156 7 0311027-05 Cl8-BZ#194 0.180 U µg/Kg 0.180 µg/Kg9/12/2000 07-02-091200-35-S-STS 614704 4781156 7 0311027-05 Cl8-BZ#195 3.60 µg/Kg 0.178 µg/Kg



Extracted 7/30/04






DETECTION LIMIT3

9/12/2000 07-02-091200-35-S-STS 614704 4781156 7 0311027-05 Cl8-BZ#201 6.90 µg/Kg 0.156 µg/Kg9/12/2000 07-02-091200-35-S-STS 614704 4781156 7 0311027-05 Cl9-BZ#206 7.04 µg/Kg 0.209 µg/Kg9/12/2000 07-02-091200-35-S-STS 614704 4781156 7 0311027-05 Cl10-BZ#209 1.48 µg/Kg 0.0977 µg/Kg9/12/2000 07-02-091200-35-S-STS 614704 4781156 7 0311027-05 Monochlorobiphenyls 5.74 U µg/Kg 5.74 µg/Kg9/12/2000 07-02-091200-35-S-STS 614704 4781156 7 0311027-05 Dichlorobiphenyls 0.168 U µg/Kg 0.168 µg/Kg9/12/2000 07-02-091200-35-S-STS 614704 4781156 7 0311027-05 Trichlorobiphenyls 50.8 µg/Kg 0.576 µg/Kg9/12/2000 07-02-091200-35-S-STS 614704 4781156 7 0311027-05 Tetrachlorobiphenyls 536 µg/Kg 0.0899 µg/Kg9/12/2000 07-02-091200-35-S-STS 614704 4781156 7 0311027-05 Pentachlorobiphenyls 1040 µg/Kg 0.104 µg/Kg9/12/2000 07-02-091200-35-S-STS 614704 4781156 7 0311027-05 Hexachlorobiphenyls 749 µg/Kg 0.164 µg/Kg9/12/2000 07-02-091200-35-S-STS 614704 4781156 7 0311027-05 Heptachlorobiphenyls 133 µg/Kg 0.0899 µg/Kg9/12/2000 07-02-091200-35-S-STS 614704 4781156 7 0311027-05 Octachlorobiphenyls 6.05 µg/Kg 0.0821 µg/Kg9/12/2000 07-02-091200-35-S-STS 614704 4781156 7 0311027-05 Nonachlorobiphenyls 15.2 µg/Kg 0.209 µg/Kg9/12/2000 07-02-091200-35-S-STS 614704 4781156 7 0311027-05 Decachlorobiphenyl 1.48 µg/Kg 0.0977 µg/Kg9/12/2000 07-02-091200-35-S-STS 614704 4781156 7 0311027-05 Total Homologs 2530 µg/Kg 0.0977 µg/Kg9/12/2000 07-02-091200-35-S-STS 614704 4781156 7 0311027-05 Percent Lipids 5.7 % 0.1 %9/12/2000 07-03-091200-17-S-STS 614704 4781156 7 0311027-06 Cl2-BZ#8 0.333 U µg/Kg 0.333 µg/Kg9/12/2000 07-03-091200-17-S-STS 614704 4781156 7 0311027-06 Cl3-BZ#18 0.739 U µg/Kg 0.739 µg/Kg9/12/2000 07-03-091200-17-S-STS 614704 4781156 7 0311027-06 Cl3-BZ#31/#28 68.1 µg/Kg 5.33 µg/Kg9/12/2000 07-03-091200-17-S-STS 614704 4781156 7 0311027-06 Cl4-BZ#44 0.507 U µg/Kg 0.507 µg/Kg9/12/2000 07-03-091200-17-S-STS 614704 4781156 7 0311027-06 Cl4-BZ#45 0.677 U µg/Kg 0.677 µg/Kg9/12/2000 07-03-091200-17-S-STS 614704 4781156 7 0311027-06 Cl4-BZ#47 49.3 µg/Kg 0.859 µg/Kg9/12/2000 07-03-091200-17-S-STS 614704 4781156 7 0311027-06 Cl4-BZ#49 13.3 µg/Kg 0.422 µg/Kg9/12/2000 07-03-091200-17-S-STS 614704 4781156 7 0311027-06 Cl4-BZ#52 23.8 µg/Kg 0.480 µg/Kg9/12/2000 07-03-091200-17-S-STS 614704 4781156 7 0311027-06 Cl4-BZ#56 78.9 µg/Kg 0.252 µg/Kg9/12/2000 07-03-091200-17-S-STS 614704 4781156 7 0311027-06 Cl4-BZ#66 191 µg/Kg 0.337 µg/Kg9/12/2000 07-03-091200-17-S-STS 614704 4781156 7 0311027-06 Cl4-BZ#70 62.3 µg/Kg 0.294 µg/Kg9/12/2000 07-03-091200-17-S-STS 614704 4781156 7 0311027-06 Cl4-BZ#74 286 µg/Kg 0.519 µg/Kg9/12/2000 07-03-091200-17-S-STS 614704 4781156 7 0311027-06 Cl4-BZ#77 0.464 U µg/Kg 0.464 µg/Kg9/12/2000 07-03-091200-17-S-STS 614704 4781156 7 0311027-06 Cl4-BZ#81 0.461 U µg/Kg 0.461 µg/Kg9/12/2000 07-03-091200-17-S-STS 614704 4781156 7 0311027-06 Cl5-BZ#87 78.6 µg/Kg 0.205 µg/Kg9/12/2000 07-03-091200-17-S-STS 614704 4781156 7 0311027-06 Cl5-BZ#95 5.92 µg/Kg 0.159 µg/Kg9/12/2000 07-03-091200-17-S-STS 614704 4781156 7 0311027-06 Cl5-BZ#99 309 µg/Kg 0.108 µg/Kg9/12/2000 07-03-091200-17-S-STS 614704 4781156 7 0311027-06 Cl5-BZ#101 36.8 µg/Kg 0.310 µg/Kg9/12/2000 07-03-091200-17-S-STS 614704 4781156 7 0311027-06 Cl5-BZ#105 181 µg/Kg 0.151 µg/Kg9/12/2000 07-03-091200-17-S-STS 614704 4781156 7 0311027-06 Cl5-BZ#110 31.2 µg/Kg 0.294 µg/Kg



Extracted 7/30/04






DETECTION LIMIT3

9/12/2000 07-03-091200-17-S-STS 614704 4781156 7 0311027-06 Cl5-BZ#114 16.7 µg/Kg 0.135 µg/Kg9/12/2000 07-03-091200-17-S-STS 614704 4781156 7 0311027-06 Cl5-BZ#118 489 µg/Kg 0.317 µg/Kg9/12/2000 07-03-091200-17-S-STS 614704 4781156 7 0311027-06 Cl5-BZ#123 0.267 U µg/Kg 0.267 µg/Kg9/12/2000 07-03-091200-17-S-STS 614704 4781156 7 0311027-06 Cl5-BZ#126 0.236 U µg/Kg 0.236 µg/Kg9/12/2000 07-03-091200-17-S-STS 614704 4781156 7 0311027-06 Cl6-BZ#128 42.7 µg/Kg 0.213 µg/Kg9/12/2000 07-03-091200-17-S-STS 614704 4781156 7 0311027-06 Cl6-BZ#138 668 µg/Kg 0.306 µg/Kg9/12/2000 07-03-091200-17-S-STS 614704 4781156 7 0311027-06 Cl6-BZ#146 66.0 µg/Kg 0.193 µg/Kg9/12/2000 07-03-091200-17-S-STS 614704 4781156 7 0311027-06 Cl6-BZ#149 15.0 µg/Kg 0.248 µg/Kg9/12/2000 07-03-091200-17-S-STS 614704 4781156 7 0311027-06 Cl6-BZ#151 4.37 µg/Kg 0.410 µg/Kg9/12/2000 07-03-091200-17-S-STS 614704 4781156 7 0311027-06 Cl6-BZ#153 492 µg/Kg 0.352 µg/Kg9/12/2000 07-03-091200-17-S-STS 614704 4781156 7 0311027-06 Cl6-BZ#156 46.9 µg/Kg 0.252 µg/Kg9/12/2000 07-03-091200-17-S-STS 614704 4781156 7 0311027-06 Cl6-BZ#157 7.62 µg/Kg 0.197 µg/Kg9/12/2000 07-03-091200-17-S-STS 614704 4781156 7 0311027-06 Cl6-BZ#158 20.9 µg/Kg 0.166 µg/Kg9/12/2000 07-03-091200-17-S-STS 614704 4781156 7 0311027-06 Cl6-BZ#167 22.8 µg/Kg 0.213 µg/Kg9/12/2000 07-03-091200-17-S-STS 614704 4781156 7 0311027-06 Cl6-BZ#169 0.685 U µg/Kg 0.685 µg/Kg9/12/2000 07-03-091200-17-S-STS 614704 4781156 7 0311027-06 Cl7-BZ#170 63.2 µg/Kg 0.797 µg/Kg9/12/2000 07-03-091200-17-S-STS 614704 4781156 7 0311027-06 Cl7-BZ#174 0.162 U µg/Kg 0.162 µg/Kg9/12/2000 07-03-091200-17-S-STS 614704 4781156 7 0311027-06 Cl7-BZ#177 13.1 µg/Kg 0.228 µg/Kg9/12/2000 07-03-091200-17-S-STS 614704 4781156 7 0311027-06 Cl7-BZ#180 105 µg/Kg 0.341 µg/Kg9/12/2000 07-03-091200-17-S-STS 614704 4781156 7 0311027-06 Cl7-BZ#183 13.8 µg/Kg 0.155 µg/Kg9/12/2000 07-03-091200-17-S-STS 614704 4781156 7 0311027-06 Cl7-BZ#187 84.2 µg/Kg 0.170 µg/Kg9/12/2000 07-03-091200-17-S-STS 614704 4781156 7 0311027-06 Cl7-BZ#189 0.306 U µg/Kg 0.306 µg/Kg9/12/2000 07-03-091200-17-S-STS 614704 4781156 7 0311027-06 Cl8-BZ#194 0.356 U µg/Kg 0.356 µg/Kg9/12/2000 07-03-091200-17-S-STS 614704 4781156 7 0311027-06 Cl8-BZ#195 7.86 µg/Kg 0.352 µg/Kg9/12/2000 07-03-091200-17-S-STS 614704 4781156 7 0311027-06 Cl8-BZ#201 17.1 µg/Kg 0.310 µg/Kg9/12/2000 07-03-091200-17-S-STS 614704 4781156 7 0311027-06 Cl9-BZ#206 20.3 µg/Kg 0.414 µg/Kg9/12/2000 07-03-091200-17-S-STS 614704 4781156 7 0311027-06 Cl10-BZ#209 4.10 µg/Kg 0.193 µg/Kg9/12/2000 07-03-091200-17-S-STS 614704 4781156 7 0311027-06 Monochlorobiphenyls 11.4 U µg/Kg 11.4 µg/Kg9/12/2000 07-03-091200-17-S-STS 614704 4781156 7 0311027-06 Dichlorobiphenyls 0.333 U µg/Kg 0.333 µg/Kg9/12/2000 07-03-091200-17-S-STS 614704 4781156 7 0311027-06 Trichlorobiphenyls 71.0 µg/Kg 1.14 µg/Kg9/12/2000 07-03-091200-17-S-STS 614704 4781156 7 0311027-06 Tetrachlorobiphenyls 771 µg/Kg 0.178 µg/Kg9/12/2000 07-03-091200-17-S-STS 614704 4781156 7 0311027-06 Pentachlorobiphenyls 2060 µg/Kg 0.205 µg/Kg9/12/2000 07-03-091200-17-S-STS 614704 4781156 7 0311027-06 Hexachlorobiphenyls 1460 µg/Kg 0.325 µg/Kg9/12/2000 07-03-091200-17-S-STS 614704 4781156 7 0311027-06 Heptachlorobiphenyls 232 µg/Kg 0.178 µg/Kg9/12/2000 07-03-091200-17-S-STS 614704 4781156 7 0311027-06 Octachlorobiphenyls 54.3 µg/Kg 0.162 µg/Kg



Extracted 7/30/04






DETECTION LIMIT3

9/12/2000 07-03-091200-17-S-STS 614704 4781156 7 0311027-06 Nonachlorobiphenyls 30.3 µg/Kg 0.414 µg/Kg9/12/2000 07-03-091200-17-S-STS 614704 4781156 7 0311027-06 Decachlorobiphenyl 4.10 µg/Kg 0.193 µg/Kg9/12/2000 07-03-091200-17-S-STS 614704 4781156 7 0311027-06 Total Homologs 4680 µg/Kg 0.193 µg/Kg9/12/2000 07-03-091200-17-S-STS 614704 4781156 7 0311027-06 Percent Lipids 3.2 % 0.1 %9/12/2000 07-04-091200-8-S-STS 614704 4781156 7 0311027-07 Cl2-BZ#8 2.12 U µg/Kg 2.12 µg/Kg9/12/2000 07-04-091200-8-S-STS 614704 4781156 7 0311027-07 Cl3-BZ#18 4.70 U µg/Kg 4.70 µg/Kg9/12/2000 07-04-091200-8-S-STS 614704 4781156 7 0311027-07 Cl3-BZ#31/#28 245 µg/Kg 33.9 µg/Kg9/12/2000 07-04-091200-8-S-STS 614704 4781156 7 0311027-07 Cl4-BZ#44 61.8 µg/Kg 3.22 µg/Kg9/12/2000 07-04-091200-8-S-STS 614704 4781156 7 0311027-07 Cl4-BZ#45 4.31 U µg/Kg 4.31 µg/Kg9/12/2000 07-04-091200-8-S-STS 614704 4781156 7 0311027-07 Cl4-BZ#47 1710 µg/Kg 5.46 µg/Kg9/12/2000 07-04-091200-8-S-STS 614704 4781156 7 0311027-07 Cl4-BZ#49 135 µg/Kg 2.68 µg/Kg9/12/2000 07-04-091200-8-S-STS 614704 4781156 7 0311027-07 Cl4-BZ#52 501 µg/Kg 3.05 µg/Kg9/12/2000 07-04-091200-8-S-STS 614704 4781156 7 0311027-07 Cl4-BZ#56 217 µg/Kg 1.60 µg/Kg9/12/2000 07-04-091200-8-S-STS 614704 4781156 7 0311027-07 Cl4-BZ#66 414 µg/Kg 2.14 µg/Kg9/12/2000 07-04-091200-8-S-STS 614704 4781156 7 0311027-07 Cl4-BZ#70 251 µg/Kg 1.87 µg/Kg9/12/2000 07-04-091200-8-S-STS 614704 4781156 7 0311027-07 Cl4-BZ#74 1130 µg/Kg 3.30 µg/Kg9/12/2000 07-04-091200-8-S-STS 614704 4781156 7 0311027-07 Cl4-BZ#77 2.95 U µg/Kg 2.95 µg/Kg9/12/2000 07-04-091200-8-S-STS 614704 4781156 7 0311027-07 Cl4-BZ#81 2.93 U µg/Kg 2.93 µg/Kg9/12/2000 07-04-091200-8-S-STS 614704 4781156 7 0311027-07 Cl5-BZ#87 746 µg/Kg 1.30 µg/Kg9/12/2000 07-04-091200-8-S-STS 614704 4781156 7 0311027-07 Cl5-BZ#95 69.9 µg/Kg 1.01 µg/Kg9/12/2000 07-04-091200-8-S-STS 614704 4781156 7 0311027-07 Cl5-BZ#99 3280 µg/Kg 0.689 µg/Kg9/12/2000 07-04-091200-8-S-STS 614704 4781156 7 0311027-07 Cl5-BZ#101 395 µg/Kg 1.97 µg/Kg9/12/2000 07-04-091200-8-S-STS 614704 4781156 7 0311027-07 Cl5-BZ#105 1140 µg/Kg 0.960 µg/Kg9/12/2000 07-04-091200-8-S-STS 614704 4781156 7 0311027-07 Cl5-BZ#110 384 µg/Kg 1.87 µg/Kg9/12/2000 07-04-091200-8-S-STS 614704 4781156 7 0311027-07 Cl5-BZ#114 86.4 µg/Kg 0.862 µg/Kg9/12/2000 07-04-091200-8-S-STS 614704 4781156 7 0311027-07 Cl5-BZ#118 3590 µg/Kg 2.02 µg/Kg9/12/2000 07-04-091200-8-S-STS 614704 4781156 7 0311027-07 Cl5-BZ#123 1.70 U µg/Kg 1.70 µg/Kg9/12/2000 07-04-091200-8-S-STS 614704 4781156 7 0311027-07 Cl5-BZ#126 1.50 U µg/Kg 1.50 µg/Kg9/12/2000 07-04-091200-8-S-STS 614704 4781156 7 0311027-07 Cl6-BZ#128 217 µg/Kg 1.35 µg/Kg9/12/2000 07-04-091200-8-S-STS 614704 4781156 7 0311027-07 Cl6-BZ#138 4720 µg/Kg 1.94 µg/Kg9/12/2000 07-04-091200-8-S-STS 614704 4781156 7 0311027-07 Cl6-BZ#146 545 µg/Kg 1.23 µg/Kg9/12/2000 07-04-091200-8-S-STS 614704 4781156 7 0311027-07 Cl6-BZ#149 212 µg/Kg 1.58 µg/Kg9/12/2000 07-04-091200-8-S-STS 614704 4781156 7 0311027-07 Cl6-BZ#151 36.9 µg/Kg 2.61 µg/Kg9/12/2000 07-04-091200-8-S-STS 614704 4781156 7 0311027-07 Cl6-BZ#153 3010 µg/Kg 2.24 µg/Kg9/12/2000 07-04-091200-8-S-STS 614704 4781156 7 0311027-07 Cl6-BZ#156 322 µg/Kg 1.60 µg/Kg



Extracted 7/30/04






DETECTION LIMIT3

9/12/2000 07-04-091200-8-S-STS 614704 4781156 7 0311027-07 Cl6-BZ#157 54.6 µg/Kg 1.25 µg/Kg9/12/2000 07-04-091200-8-S-STS 614704 4781156 7 0311027-07 Cl6-BZ#158 211 µg/Kg 1.06 µg/Kg9/12/2000 07-04-091200-8-S-STS 614704 4781156 7 0311027-07 Cl6-BZ#167 84.8 µg/Kg 1.35 µg/Kg9/12/2000 07-04-091200-8-S-STS 614704 4781156 7 0311027-07 Cl6-BZ#169 4.36 U µg/Kg 4.36 µg/Kg9/12/2000 07-04-091200-8-S-STS 614704 4781156 7 0311027-07 Cl7-BZ#170 364 µg/Kg 5.07 µg/Kg9/12/2000 07-04-091200-8-S-STS 614704 4781156 7 0311027-07 Cl7-BZ#174 1.03 U µg/Kg 1.03 µg/Kg9/12/2000 07-04-091200-8-S-STS 614704 4781156 7 0311027-07 Cl7-BZ#177 146 µg/Kg 1.45 µg/Kg9/12/2000 07-04-091200-8-S-STS 614704 4781156 7 0311027-07 Cl7-BZ#180 648 µg/Kg 2.17 µg/Kg9/12/2000 07-04-091200-8-S-STS 614704 4781156 7 0311027-07 Cl7-BZ#183 143 µg/Kg 0.985 µg/Kg9/12/2000 07-04-091200-8-S-STS 614704 4781156 7 0311027-07 Cl7-BZ#187 1220 µg/Kg 1.08 µg/Kg9/12/2000 07-04-091200-8-S-STS 614704 4781156 7 0311027-07 Cl7-BZ#189 1.94 U µg/Kg 1.94 µg/Kg9/12/2000 07-04-091200-8-S-STS 614704 4781156 7 0311027-07 Cl8-BZ#194 130 µg/Kg 2.26 µg/Kg9/12/2000 07-04-091200-8-S-STS 614704 4781156 7 0311027-07 Cl8-BZ#195 41.4 µg/Kg 2.24 µg/Kg9/12/2000 07-04-091200-8-S-STS 614704 4781156 7 0311027-07 Cl8-BZ#201 179 µg/Kg 1.97 µg/Kg9/12/2000 07-04-091200-8-S-STS 614704 4781156 7 0311027-07 Cl9-BZ#206 70.0 µg/Kg 2.63 µg/Kg9/12/2000 07-04-091200-8-S-STS 614704 4781156 7 0311027-07 Cl10-BZ#209 1.23 U µg/Kg 1.23 µg/Kg9/12/2000 07-04-091200-8-S-STS 614704 4781156 7 0311027-07 Monochlorobiphenyls 72.4 U µg/Kg 72.4 µg/Kg9/12/2000 07-04-091200-8-S-STS 614704 4781156 7 0311027-07 Dichlorobiphenyls 2.12 U µg/Kg 2.12 µg/Kg9/12/2000 07-04-091200-8-S-STS 614704 4781156 7 0311027-07 Trichlorobiphenyls 296 µg/Kg 7.26 µg/Kg9/12/2000 07-04-091200-8-S-STS 614704 4781156 7 0311027-07 Tetrachlorobiphenyls 5290 µg/Kg 1.13 µg/Kg9/12/2000 07-04-091200-8-S-STS 614704 4781156 7 0311027-07 Pentachlorobiphenyls 18100 µg/Kg 1.30 µg/Kg9/12/2000 07-04-091200-8-S-STS 614704 4781156 7 0311027-07 Hexachlorobiphenyls 10200 µg/Kg 2.07 µg/Kg9/12/2000 07-04-091200-8-S-STS 614704 4781156 7 0311027-07 Heptachlorobiphenyls 2320 µg/Kg 1.13 µg/Kg9/12/2000 07-04-091200-8-S-STS 614704 4781156 7 0311027-07 Octachlorobiphenyls 383 µg/Kg 1.03 µg/Kg9/12/2000 07-04-091200-8-S-STS 614704 4781156 7 0311027-07 Nonachlorobiphenyls 99.8 µg/Kg 2.63 µg/Kg9/12/2000 07-04-091200-8-S-STS 614704 4781156 7 0311027-07 Decachlorobiphenyl 1.23 U µg/Kg 1.23 µg/Kg9/12/2000 07-04-091200-8-S-STS 614704 4781156 7 0311027-07 Total Homologs 36700 µg/Kg 1.23 µg/Kg9/12/2000 07-04-091200-8-S-STS 614704 4781156 7 0311027-07 Percent Lipids 4.6 % 0.1 %9/12/2000 08-01-091200-33-S-STS 614814 4783340 8 0311027-08 Cl2-BZ#8 0.822 U µg/Kg 0.822 µg/Kg9/12/2000 08-01-091200-33-S-STS 614814 4783340 8 0311027-08 Cl3-BZ#18 1.83 U µg/Kg 1.83 µg/Kg9/12/2000 08-01-091200-33-S-STS 614814 4783340 8 0311027-08 Cl3-BZ#31/#28 372 µg/Kg 13.2 µg/Kg9/12/2000 08-01-091200-33-S-STS 614814 4783340 8 0311027-08 Cl4-BZ#44 79.7 µg/Kg 1.25 µg/Kg9/12/2000 08-01-091200-33-S-STS 614814 4783340 8 0311027-08 Cl4-BZ#45 1.67 U µg/Kg 1.67 µg/Kg9/12/2000 08-01-091200-33-S-STS 614814 4783340 8 0311027-08 Cl4-BZ#47 914 µg/Kg 2.12 µg/Kg9/12/2000 08-01-091200-33-S-STS 614814 4783340 8 0311027-08 Cl4-BZ#49 70.4 µg/Kg 1.04 µg/Kg



Extracted 7/30/04






DETECTION LIMIT3

9/12/2000 08-01-091200-33-S-STS 614814 4783340 8 0311027-08 Cl4-BZ#52 341 µg/Kg 1.19 µg/Kg9/12/2000 08-01-091200-33-S-STS 614814 4783340 8 0311027-08 Cl4-BZ#56 226 µg/Kg 0.622 µg/Kg9/12/2000 08-01-091200-33-S-STS 614814 4783340 8 0311027-08 Cl4-BZ#66 498 µg/Kg 0.832 µg/Kg9/12/2000 08-01-091200-33-S-STS 614814 4783340 8 0311027-08 Cl4-BZ#70 212 µg/Kg 0.727 µg/Kg9/12/2000 08-01-091200-33-S-STS 614814 4783340 8 0311027-08 Cl4-BZ#74 791 µg/Kg 1.28 µg/Kg9/12/2000 08-01-091200-33-S-STS 614814 4783340 8 0311027-08 Cl4-BZ#77 1.15 U µg/Kg 1.15 µg/Kg9/12/2000 08-01-091200-33-S-STS 614814 4783340 8 0311027-08 Cl4-BZ#81 1.14 U µg/Kg 1.14 µg/Kg9/12/2000 08-01-091200-33-S-STS 614814 4783340 8 0311027-08 Cl5-BZ#87 294 µg/Kg 0.507 µg/Kg9/12/2000 08-01-091200-33-S-STS 614814 4783340 8 0311027-08 Cl5-BZ#95 49.8 µg/Kg 0.392 µg/Kg9/12/2000 08-01-091200-33-S-STS 614814 4783340 8 0311027-08 Cl5-BZ#99 896 µg/Kg 0.268 µg/Kg9/12/2000 08-01-091200-33-S-STS 614814 4783340 8 0311027-08 Cl5-BZ#101 151 µg/Kg 0.765 µg/Kg9/12/2000 08-01-091200-33-S-STS 614814 4783340 8 0311027-08 Cl5-BZ#105 396 µg/Kg 0.373 µg/Kg9/12/2000 08-01-091200-33-S-STS 614814 4783340 8 0311027-08 Cl5-BZ#110 180 µg/Kg 0.727 µg/Kg9/12/2000 08-01-091200-33-S-STS 614814 4783340 8 0311027-08 Cl5-BZ#114 38.9 µg/Kg 0.335 µg/Kg9/12/2000 08-01-091200-33-S-STS 614814 4783340 8 0311027-08 Cl5-BZ#118 1060 µg/Kg 0.784 µg/Kg9/12/2000 08-01-091200-33-S-STS 614814 4783340 8 0311027-08 Cl5-BZ#123 0.660 U µg/Kg 0.660 µg/Kg9/12/2000 08-01-091200-33-S-STS 614814 4783340 8 0311027-08 Cl5-BZ#126 0.583 U µg/Kg 0.583 µg/Kg9/12/2000 08-01-091200-33-S-STS 614814 4783340 8 0311027-08 Cl6-BZ#128 63.7 µg/Kg 0.526 µg/Kg9/12/2000 08-01-091200-33-S-STS 614814 4783340 8 0311027-08 Cl6-BZ#138 1350 µg/Kg 0.756 µg/Kg9/12/2000 08-01-091200-33-S-STS 614814 4783340 8 0311027-08 Cl6-BZ#146 172 µg/Kg 0.478 µg/Kg9/12/2000 08-01-091200-33-S-STS 614814 4783340 8 0311027-08 Cl6-BZ#149 67.2 µg/Kg 0.612 µg/Kg9/12/2000 08-01-091200-33-S-STS 614814 4783340 8 0311027-08 Cl6-BZ#151 12.7 µg/Kg 1.01 µg/Kg9/12/2000 08-01-091200-33-S-STS 614814 4783340 8 0311027-08 Cl6-BZ#153 929 µg/Kg 0.870 µg/Kg9/12/2000 08-01-091200-33-S-STS 614814 4783340 8 0311027-08 Cl6-BZ#156 81.2 µg/Kg 0.622 µg/Kg9/12/2000 08-01-091200-33-S-STS 614814 4783340 8 0311027-08 Cl6-BZ#157 15.5 µg/Kg 0.488 µg/Kg9/12/2000 08-01-091200-33-S-STS 614814 4783340 8 0311027-08 Cl6-BZ#158 55.7 µg/Kg 0.411 µg/Kg9/12/2000 08-01-091200-33-S-STS 614814 4783340 8 0311027-08 Cl6-BZ#167 44.5 µg/Kg 0.526 µg/Kg9/12/2000 08-01-091200-33-S-STS 614814 4783340 8 0311027-08 Cl6-BZ#169 1.69 U µg/Kg 1.69 µg/Kg9/12/2000 08-01-091200-33-S-STS 614814 4783340 8 0311027-08 Cl7-BZ#170 138 µg/Kg 1.97 µg/Kg9/12/2000 08-01-091200-33-S-STS 614814 4783340 8 0311027-08 Cl7-BZ#174 0.402 U µg/Kg 0.402 µg/Kg9/12/2000 08-01-091200-33-S-STS 614814 4783340 8 0311027-08 Cl7-BZ#177 40.0 µg/Kg 0.564 µg/Kg9/12/2000 08-01-091200-33-S-STS 614814 4783340 8 0311027-08 Cl7-BZ#180 317 µg/Kg 0.841 µg/Kg9/12/2000 08-01-091200-33-S-STS 614814 4783340 8 0311027-08 Cl7-BZ#183 69.2 µg/Kg 0.382 µg/Kg9/12/2000 08-01-091200-33-S-STS 614814 4783340 8 0311027-08 Cl7-BZ#187 528 µg/Kg 0.421 µg/Kg9/12/2000 08-01-091200-33-S-STS 614814 4783340 8 0311027-08 Cl7-BZ#189 0.756 U µg/Kg 0.756 µg/Kg



Extracted 7/30/04






DETECTION LIMIT3

9/12/2000 08-01-091200-33-S-STS 614814 4783340 8 0311027-08 Cl8-BZ#194 82.0 µg/Kg 0.880 µg/Kg9/12/2000 08-01-091200-33-S-STS 614814 4783340 8 0311027-08 Cl8-BZ#195 23.4 µg/Kg 0.870 µg/Kg9/12/2000 08-01-091200-33-S-STS 614814 4783340 8 0311027-08 Cl8-BZ#201 85.2 µg/Kg 0.765 µg/Kg9/12/2000 08-01-091200-33-S-STS 614814 4783340 8 0311027-08 Cl9-BZ#206 60.2 µg/Kg 1.02 µg/Kg9/12/2000 08-01-091200-33-S-STS 614814 4783340 8 0311027-08 Cl10-BZ#209 9.47 µg/Kg 0.478 µg/Kg9/12/2000 08-01-091200-33-S-STS 614814 4783340 8 0311027-08 Monochlorobiphenyls 28.1 U µg/Kg 28.1 µg/Kg9/12/2000 08-01-091200-33-S-STS 614814 4783340 8 0311027-08 Dichlorobiphenyls 0.822 U µg/Kg 0.822 µg/Kg9/12/2000 08-01-091200-33-S-STS 614814 4783340 8 0311027-08 Trichlorobiphenyls 355 µg/Kg 2.82 µg/Kg9/12/2000 08-01-091200-33-S-STS 614814 4783340 8 0311027-08 Tetrachlorobiphenyls 3580 µg/Kg 0.440 µg/Kg9/12/2000 08-01-091200-33-S-STS 614814 4783340 8 0311027-08 Pentachlorobiphenyls 5760 µg/Kg 0.507 µg/Kg9/12/2000 08-01-091200-33-S-STS 614814 4783340 8 0311027-08 Hexachlorobiphenyls 3060 µg/Kg 0.803 µg/Kg9/12/2000 08-01-091200-33-S-STS 614814 4783340 8 0311027-08 Heptachlorobiphenyls 1010 µg/Kg 0.440 µg/Kg9/12/2000 08-01-091200-33-S-STS 614814 4783340 8 0311027-08 Octachlorobiphenyls 236 µg/Kg 0.402 µg/Kg9/12/2000 08-01-091200-33-S-STS 614814 4783340 8 0311027-08 Nonachlorobiphenyls 79.6 µg/Kg 1.02 µg/Kg9/12/2000 08-01-091200-33-S-STS 614814 4783340 8 0311027-08 Decachlorobiphenyl 9.47 µg/Kg 0.478 µg/Kg9/12/2000 08-01-091200-33-S-STS 614814 4783340 8 0311027-08 Total Homologs 14100 µg/Kg 0.478 µg/Kg9/12/2000 08-01-091200-33-S-STS 614814 4783340 8 0311027-08 Percent Lipids 4.8 % 0.1 %9/12/2000 08-02-091200-6-S-STS 614814 4783340 8 0311027-09 Cl2-BZ#8 0.542 U µg/Kg 0.542 µg/Kg9/12/2000 08-02-091200-6-S-STS 614814 4783340 8 0311027-09 Cl3-BZ#18 1.20 U µg/Kg 1.20 µg/Kg9/12/2000 08-02-091200-6-S-STS 614814 4783340 8 0311027-09 Cl3-BZ#31/#28 1040 µg/Kg 8.68 µg/Kg9/12/2000 08-02-091200-6-S-STS 614814 4783340 8 0311027-09 Cl4-BZ#44 388 µg/Kg 0.826 µg/Kg9/12/2000 08-02-091200-6-S-STS 614814 4783340 8 0311027-09 Cl4-BZ#45 22.1 µg/Kg 1.10 µg/Kg9/12/2000 08-02-091200-6-S-STS 614814 4783340 8 0311027-09 Cl4-BZ#47 678 µg/Kg 1.40 µg/Kg9/12/2000 08-02-091200-6-S-STS 614814 4783340 8 0311027-09 Cl4-BZ#49 341 µg/Kg 0.687 µg/Kg9/12/2000 08-02-091200-6-S-STS 614814 4783340 8 0311027-09 Cl4-BZ#52 922 µg/Kg 0.782 µg/Kg9/12/2000 08-02-091200-6-S-STS 614814 4783340 8 0311027-09 Cl4-BZ#56 515 µg/Kg 0.410 µg/Kg9/12/2000 08-02-091200-6-S-STS 614814 4783340 8 0311027-09 Cl4-BZ#66 1060 µg/Kg 0.548 µg/Kg9/12/2000 08-02-091200-6-S-STS 614814 4783340 8 0311027-09 Cl4-BZ#70 597 µg/Kg 0.479 µg/Kg9/12/2000 08-02-091200-6-S-STS 614814 4783340 8 0311027-09 Cl4-BZ#74 944 µg/Kg 0.845 µg/Kg9/12/2000 08-02-091200-6-S-STS 614814 4783340 8 0311027-09 Cl4-BZ#77 0.756 U µg/Kg 0.756 µg/Kg9/12/2000 08-02-091200-6-S-STS 614814 4783340 8 0311027-09 Cl4-BZ#81 0.750 U µg/Kg 0.750 µg/Kg9/12/2000 08-02-091200-6-S-STS 614814 4783340 8 0311027-09 Cl5-BZ#87 310 µg/Kg 0.334 µg/Kg9/12/2000 08-02-091200-6-S-STS 614814 4783340 8 0311027-09 Cl5-BZ#95 188 µg/Kg 0.258 µg/Kg9/12/2000 08-02-091200-6-S-STS 614814 4783340 8 0311027-09 Cl5-BZ#99 387 µg/Kg 0.176 µg/Kg9/12/2000 08-02-091200-6-S-STS 614814 4783340 8 0311027-09 Cl5-BZ#101 316 µg/Kg 0.504 µg/Kg



Extracted 7/30/04






DETECTION LIMIT3

9/12/2000 08-02-091200-6-S-STS 614814 4783340 8 0311027-09 Cl5-BZ#105 255 µg/Kg 0.246 µg/Kg9/12/2000 08-02-091200-6-S-STS 614814 4783340 8 0311027-09 Cl5-BZ#110 485 µg/Kg 0.479 µg/Kg9/12/2000 08-02-091200-6-S-STS 614814 4783340 8 0311027-09 Cl5-BZ#114 23.0 µg/Kg 0.221 µg/Kg9/12/2000 08-02-091200-6-S-STS 614814 4783340 8 0311027-09 Cl5-BZ#118 491 µg/Kg 0.517 µg/Kg9/12/2000 08-02-091200-6-S-STS 614814 4783340 8 0311027-09 Cl5-BZ#123 0.435 U µg/Kg 0.435 µg/Kg9/12/2000 08-02-091200-6-S-STS 614814 4783340 8 0311027-09 Cl5-BZ#126 0.384 U µg/Kg 0.384 µg/Kg9/12/2000 08-02-091200-6-S-STS 614814 4783340 8 0311027-09 Cl6-BZ#128 27.5 µg/Kg 0.347 µg/Kg9/12/2000 08-02-091200-6-S-STS 614814 4783340 8 0311027-09 Cl6-BZ#138 451 µg/Kg 0.498 µg/Kg9/12/2000 08-02-091200-6-S-STS 614814 4783340 8 0311027-09 Cl6-BZ#146 49.0 µg/Kg 0.315 µg/Kg9/12/2000 08-02-091200-6-S-STS 614814 4783340 8 0311027-09 Cl6-BZ#149 121 µg/Kg 0.403 µg/Kg9/12/2000 08-02-091200-6-S-STS 614814 4783340 8 0311027-09 Cl6-BZ#151 34.6 µg/Kg 0.668 µg/Kg9/12/2000 08-02-091200-6-S-STS 614814 4783340 8 0311027-09 Cl6-BZ#153 229 µg/Kg 0.574 µg/Kg9/12/2000 08-02-091200-6-S-STS 614814 4783340 8 0311027-09 Cl6-BZ#156 27.4 µg/Kg 0.410 µg/Kg9/12/2000 08-02-091200-6-S-STS 614814 4783340 8 0311027-09 Cl6-BZ#157 5.11 µg/Kg 0.322 µg/Kg9/12/2000 08-02-091200-6-S-STS 614814 4783340 8 0311027-09 Cl6-BZ#158 15.6 µg/Kg 0.271 µg/Kg9/12/2000 08-02-091200-6-S-STS 614814 4783340 8 0311027-09 Cl6-BZ#167 10.6 µg/Kg 0.347 µg/Kg9/12/2000 08-02-091200-6-S-STS 614814 4783340 8 0311027-09 Cl6-BZ#169 1.12 U µg/Kg 1.12 µg/Kg9/12/2000 08-02-091200-6-S-STS 614814 4783340 8 0311027-09 Cl7-BZ#170 42.1 µg/Kg 1.30 µg/Kg9/12/2000 08-02-091200-6-S-STS 614814 4783340 8 0311027-09 Cl7-BZ#174 18.1 µg/Kg 0.265 µg/Kg9/12/2000 08-02-091200-6-S-STS 614814 4783340 8 0311027-09 Cl7-BZ#177 17.0 µg/Kg 0.372 µg/Kg9/12/2000 08-02-091200-6-S-STS 614814 4783340 8 0311027-09 Cl7-BZ#180 0.555 U µg/Kg 0.555 µg/Kg9/12/2000 08-02-091200-6-S-STS 614814 4783340 8 0311027-09 Cl7-BZ#183 15.8 µg/Kg 0.252 µg/Kg9/12/2000 08-02-091200-6-S-STS 614814 4783340 8 0311027-09 Cl7-BZ#187 170 µg/Kg 0.277 µg/Kg9/12/2000 08-02-091200-6-S-STS 614814 4783340 8 0311027-09 Cl7-BZ#189 0.498 U µg/Kg 0.498 µg/Kg9/12/2000 08-02-091200-6-S-STS 614814 4783340 8 0311027-09 Cl8-BZ#194 9.52 µg/Kg 0.580 µg/Kg9/12/2000 08-02-091200-6-S-STS 614814 4783340 8 0311027-09 Cl8-BZ#195 5.42 µg/Kg 0.574 µg/Kg9/12/2000 08-02-091200-6-S-STS 614814 4783340 8 0311027-09 Cl8-BZ#201 34.0 µg/Kg 0.504 µg/Kg9/12/2000 08-02-091200-6-S-STS 614814 4783340 8 0311027-09 Cl9-BZ#206 22.6 µg/Kg 0.674 µg/Kg9/12/2000 08-02-091200-6-S-STS 614814 4783340 8 0311027-09 Cl10-BZ#209 7.63 µg/Kg 0.315 µg/Kg9/12/2000 08-02-091200-6-S-STS 614814 4783340 8 0311027-09 Monochlorobiphenyls 18.5 U µg/Kg 18.5 µg/Kg9/12/2000 08-02-091200-6-S-STS 614814 4783340 8 0311027-09 Dichlorobiphenyls 7.85 µg/Kg 0.542 µg/Kg9/12/2000 08-02-091200-6-S-STS 614814 4783340 8 0311027-09 Trichlorobiphenyls 1120 µg/Kg 1.86 µg/Kg9/12/2000 08-02-091200-6-S-STS 614814 4783340 8 0311027-09 Tetrachlorobiphenyls 7030 µg/Kg 0.290 µg/Kg9/12/2000 08-02-091200-6-S-STS 614814 4783340 8 0311027-09 Pentachlorobiphenyls 4610 µg/Kg 0.334 µg/Kg9/12/2000 08-02-091200-6-S-STS 614814 4783340 8 0311027-09 Hexachlorobiphenyls 1120 µg/Kg 0.530 µg/Kg



Extracted 7/30/04






DETECTION LIMIT3

9/12/2000 08-02-091200-6-S-STS 614814 4783340 8 0311027-09 Heptachlorobiphenyls 323 µg/Kg 0.290 µg/Kg9/12/2000 08-02-091200-6-S-STS 614814 4783340 8 0311027-09 Octachlorobiphenyls 24.9 µg/Kg 0.265 µg/Kg9/12/2000 08-02-091200-6-S-STS 614814 4783340 8 0311027-09 Nonachlorobiphenyls 52.4 µg/Kg 0.674 µg/Kg9/12/2000 08-02-091200-6-S-STS 614814 4783340 8 0311027-09 Decachlorobiphenyl 7.63 µg/Kg 0.315 µg/Kg9/12/2000 08-02-091200-6-S-STS 614814 4783340 8 0311027-09 Total Homologs 14300 µg/Kg 0.315 µg/Kg9/12/2000 08-02-091200-6-S-STS 614814 4783340 8 0311027-09 Percent Lipids 12.0 % 0.1 %9/12/2000 08-03-091200-3-S-STS 614814 4783340 8 0311027-10 Cl2-BZ#8 0.146 U µg/Kg 0.146 µg/Kg9/12/2000 08-03-091200-3-S-STS 614814 4783340 8 0311027-10 Cl3-BZ#18 0.324 U µg/Kg 0.324 µg/Kg9/12/2000 08-03-091200-3-S-STS 614814 4783340 8 0311027-10 Cl3-BZ#31/#28 2.33 U µg/Kg 2.33 µg/Kg9/12/2000 08-03-091200-3-S-STS 614814 4783340 8 0311027-10 Cl4-BZ#44 0.222 U µg/Kg 0.222 µg/Kg9/12/2000 08-03-091200-3-S-STS 614814 4783340 8 0311027-10 Cl4-BZ#45 0.296 U µg/Kg 0.296 µg/Kg9/12/2000 08-03-091200-3-S-STS 614814 4783340 8 0311027-10 Cl4-BZ#47 4.77 µg/Kg 0.376 µg/Kg9/12/2000 08-03-091200-3-S-STS 614814 4783340 8 0311027-10 Cl4-BZ#49 1.20 µg/Kg 0.185 µg/Kg9/12/2000 08-03-091200-3-S-STS 614814 4783340 8 0311027-10 Cl4-BZ#52 3.76 µg/Kg 0.210 µg/Kg9/12/2000 08-03-091200-3-S-STS 614814 4783340 8 0311027-10 Cl4-BZ#56 7.68 µg/Kg 0.110 µg/Kg9/12/2000 08-03-091200-3-S-STS 614814 4783340 8 0311027-10 Cl4-BZ#66 17.6 µg/Kg 0.147 µg/Kg9/12/2000 08-03-091200-3-S-STS 614814 4783340 8 0311027-10 Cl4-BZ#70 8.17 µg/Kg 0.129 µg/Kg9/12/2000 08-03-091200-3-S-STS 614814 4783340 8 0311027-10 Cl4-BZ#74 11.1 µg/Kg 0.227 µg/Kg9/12/2000 08-03-091200-3-S-STS 614814 4783340 8 0311027-10 Cl4-BZ#77 0.203 U µg/Kg 0.203 µg/Kg9/12/2000 08-03-091200-3-S-STS 614814 4783340 8 0311027-10 Cl4-BZ#81 0.202 U µg/Kg 0.202 µg/Kg9/12/2000 08-03-091200-3-S-STS 614814 4783340 8 0311027-10 Cl5-BZ#87 3.73 µg/Kg 0.0898 µg/Kg9/12/2000 08-03-091200-3-S-STS 614814 4783340 8 0311027-10 Cl5-BZ#95 0.0695 U µg/Kg 0.0695 µg/Kg9/12/2000 08-03-091200-3-S-STS 614814 4783340 8 0311027-10 Cl5-BZ#99 8.45 µg/Kg 0.0474 µg/Kg9/12/2000 08-03-091200-3-S-STS 614814 4783340 8 0311027-10 Cl5-BZ#101 2.62 µg/Kg 0.135 µg/Kg9/12/2000 08-03-091200-3-S-STS 614814 4783340 8 0311027-10 Cl5-BZ#105 7.90 µg/Kg 0.0661 µg/Kg9/12/2000 08-03-091200-3-S-STS 614814 4783340 8 0311027-10 Cl5-BZ#110 0.129 U µg/Kg 0.129 µg/Kg9/12/2000 08-03-091200-3-S-STS 614814 4783340 8 0311027-10 Cl5-BZ#114 0.0593 U µg/Kg 0.0593 µg/Kg9/12/2000 08-03-091200-3-S-STS 614814 4783340 8 0311027-10 Cl5-BZ#118 16.0 µg/Kg 0.139 µg/Kg9/12/2000 08-03-091200-3-S-STS 614814 4783340 8 0311027-10 Cl5-BZ#123 0.117 U µg/Kg 0.117 µg/Kg9/12/2000 08-03-091200-3-S-STS 614814 4783340 8 0311027-10 Cl5-BZ#126 0.103 U µg/Kg 0.103 µg/Kg9/12/2000 08-03-091200-3-S-STS 614814 4783340 8 0311027-10 Cl6-BZ#128 0.0932 U µg/Kg 0.0932 µg/Kg9/12/2000 08-03-091200-3-S-STS 614814 4783340 8 0311027-10 Cl6-BZ#138 16.0 µg/Kg 0.134 µg/Kg9/12/2000 08-03-091200-3-S-STS 614814 4783340 8 0311027-10 Cl6-BZ#146 2.13 µg/Kg 0.0847 µg/Kg9/12/2000 08-03-091200-3-S-STS 614814 4783340 8 0311027-10 Cl6-BZ#149 0.108 U µg/Kg 0.108 µg/Kg9/12/2000 08-03-091200-3-S-STS 614814 4783340 8 0311027-10 Cl6-BZ#151 0.180 U µg/Kg 0.180 µg/Kg



Extracted 7/30/04






DETECTION LIMIT3

9/12/2000 08-03-091200-3-S-STS 614814 4783340 8 0311027-10 Cl6-BZ#153 12.0 µg/Kg 0.154 µg/Kg9/12/2000 08-03-091200-3-S-STS 614814 4783340 8 0311027-10 Cl6-BZ#156 1.39 µg/Kg 0.110 µg/Kg9/12/2000 08-03-091200-3-S-STS 614814 4783340 8 0311027-10 Cl6-BZ#157 0.0864 U µg/Kg 0.0864 µg/Kg9/12/2000 08-03-091200-3-S-STS 614814 4783340 8 0311027-10 Cl6-BZ#158 0.0729 U µg/Kg 0.0729 µg/Kg9/12/2000 08-03-091200-3-S-STS 614814 4783340 8 0311027-10 Cl6-BZ#167 0.0932 U µg/Kg 0.0932 µg/Kg9/12/2000 08-03-091200-3-S-STS 614814 4783340 8 0311027-10 Cl6-BZ#169 0.300 U µg/Kg 0.300 µg/Kg9/12/2000 08-03-091200-3-S-STS 614814 4783340 8 0311027-10 Cl7-BZ#170 0.349 U µg/Kg 0.349 µg/Kg9/12/2000 08-03-091200-3-S-STS 614814 4783340 8 0311027-10 Cl7-BZ#174 0.0712 U µg/Kg 0.0712 µg/Kg9/12/2000 08-03-091200-3-S-STS 614814 4783340 8 0311027-10 Cl7-BZ#177 0.100 U µg/Kg 0.100 µg/Kg9/12/2000 08-03-091200-3-S-STS 614814 4783340 8 0311027-10 Cl7-BZ#180 0.149 U µg/Kg 0.149 µg/Kg9/12/2000 08-03-091200-3-S-STS 614814 4783340 8 0311027-10 Cl7-BZ#183 0.0678 U µg/Kg 0.0678 µg/Kg9/12/2000 08-03-091200-3-S-STS 614814 4783340 8 0311027-10 Cl7-BZ#187 2.89 µg/Kg 0.0746 µg/Kg9/12/2000 08-03-091200-3-S-STS 614814 4783340 8 0311027-10 Cl7-BZ#189 0.134 U µg/Kg 0.134 µg/Kg9/12/2000 08-03-091200-3-S-STS 614814 4783340 8 0311027-10 Cl8-BZ#194 0.156 U µg/Kg 0.156 µg/Kg9/12/2000 08-03-091200-3-S-STS 614814 4783340 8 0311027-10 Cl8-BZ#195 0.154 U µg/Kg 0.154 µg/Kg9/12/2000 08-03-091200-3-S-STS 614814 4783340 8 0311027-10 Cl8-BZ#201 0.135 U µg/Kg 0.135 µg/Kg9/12/2000 08-03-091200-3-S-STS 614814 4783340 8 0311027-10 Cl9-BZ#206 0.181 U µg/Kg 0.181 µg/Kg9/12/2000 08-03-091200-3-S-STS 614814 4783340 8 0311027-10 Cl10-BZ#209 0.0847 U µg/Kg 0.0847 µg/Kg9/12/2000 08-03-091200-3-S-STS 614814 4783340 8 0311027-10 Monochlorobiphenyls 4.98 U µg/Kg 4.98 µg/Kg9/12/2000 08-03-091200-3-S-STS 614814 4783340 8 0311027-10 Dichlorobiphenyls 0.146 U µg/Kg 0.146 µg/Kg9/12/2000 08-03-091200-3-S-STS 614814 4783340 8 0311027-10 Trichlorobiphenyls 0.500 U µg/Kg 0.500 µg/Kg9/12/2000 08-03-091200-3-S-STS 614814 4783340 8 0311027-10 Tetrachlorobiphenyls 65.3 µg/Kg 0.0779 µg/Kg9/12/2000 08-03-091200-3-S-STS 614814 4783340 8 0311027-10 Pentachlorobiphenyls 81.1 µg/Kg 0.0898 µg/Kg9/12/2000 08-03-091200-3-S-STS 614814 4783340 8 0311027-10 Hexachlorobiphenyls 38.2 µg/Kg 0.142 µg/Kg9/12/2000 08-03-091200-3-S-STS 614814 4783340 8 0311027-10 Heptachlorobiphenyls 7.12 µg/Kg 0.0779 µg/Kg9/12/2000 08-03-091200-3-S-STS 614814 4783340 8 0311027-10 Octachlorobiphenyls 0.0712 U µg/Kg 0.0712 µg/Kg9/12/2000 08-03-091200-3-S-STS 614814 4783340 8 0311027-10 Nonachlorobiphenyls 0.181 U µg/Kg 0.181 µg/Kg9/12/2000 08-03-091200-3-S-STS 614814 4783340 8 0311027-10 Decachlorobiphenyl 0.0847 U µg/Kg 0.0847 µg/Kg9/12/2000 08-03-091200-3-S-STS 614814 4783340 8 0311027-10 Total Homologs 192 µg/Kg 0.0847 µg/Kg9/12/2000 08-03-091200-3-S-STS 614814 4783340 8 0311027-10 Percent Lipids 3.9 % 0.1 %9/13/2000 08-04-091300-33-S-STS 614814 4783340 8 0311027-11 Cl2-BZ#8 1.73 U µg/Kg 1.73 µg/Kg9/13/2000 08-04-091300-33-S-STS 614814 4783340 8 0311027-11 Cl3-BZ#18 3.84 U µg/Kg 3.84 µg/Kg9/13/2000 08-04-091300-33-S-STS 614814 4783340 8 0311027-11 Cl3-BZ#31/#28 536 µg/Kg 27.7 µg/Kg9/13/2000 08-04-091300-33-S-STS 614814 4783340 8 0311027-11 Cl4-BZ#44 136 µg/Kg 2.63 µg/Kg9/13/2000 08-04-091300-33-S-STS 614814 4783340 8 0311027-11 Cl4-BZ#45 3.52 U µg/Kg 3.52 µg/Kg



Extracted 7/30/04






DETECTION LIMIT3

9/13/2000 08-04-091300-33-S-STS 614814 4783340 8 0311027-11 Cl4-BZ#47 1480 µg/Kg 4.46 µg/Kg9/13/2000 08-04-091300-33-S-STS 614814 4783340 8 0311027-11 Cl4-BZ#49 225 µg/Kg 2.19 µg/Kg9/13/2000 08-04-091300-33-S-STS 614814 4783340 8 0311027-11 Cl4-BZ#52 942 µg/Kg 2.49 µg/Kg9/13/2000 08-04-091300-33-S-STS 614814 4783340 8 0311027-11 Cl4-BZ#56 383 µg/Kg 1.31 µg/Kg9/13/2000 08-04-091300-33-S-STS 614814 4783340 8 0311027-11 Cl4-BZ#66 776 µg/Kg 1.75 µg/Kg9/13/2000 08-04-091300-33-S-STS 614814 4783340 8 0311027-11 Cl4-BZ#70 337 µg/Kg 1.53 µg/Kg9/13/2000 08-04-091300-33-S-STS 614814 4783340 8 0311027-11 Cl4-BZ#74 1390 µg/Kg 2.69 µg/Kg9/13/2000 08-04-091300-33-S-STS 614814 4783340 8 0311027-11 Cl4-BZ#77 2.41 U µg/Kg 2.41 µg/Kg9/13/2000 08-04-091300-33-S-STS 614814 4783340 8 0311027-11 Cl4-BZ#81 2.39 U µg/Kg 2.39 µg/Kg9/13/2000 08-04-091300-33-S-STS 614814 4783340 8 0311027-11 Cl5-BZ#87 605 µg/Kg 1.06 µg/Kg9/13/2000 08-04-091300-33-S-STS 614814 4783340 8 0311027-11 Cl5-BZ#95 109 µg/Kg 0.824 µg/Kg9/13/2000 08-04-091300-33-S-STS 614814 4783340 8 0311027-11 Cl5-BZ#99 1890 µg/Kg 0.563 µg/Kg9/13/2000 08-04-091300-33-S-STS 614814 4783340 8 0311027-11 Cl5-BZ#101 374 µg/Kg 1.61 µg/Kg9/13/2000 08-04-091300-33-S-STS 614814 4783340 8 0311027-11 Cl5-BZ#105 857 µg/Kg 0.784 µg/Kg9/13/2000 08-04-091300-33-S-STS 614814 4783340 8 0311027-11 Cl5-BZ#110 376 µg/Kg 1.53 µg/Kg9/13/2000 08-04-091300-33-S-STS 614814 4783340 8 0311027-11 Cl5-BZ#114 72.2 µg/Kg 0.703 µg/Kg9/13/2000 08-04-091300-33-S-STS 614814 4783340 8 0311027-11 Cl5-BZ#118 2300 µg/Kg 1.65 µg/Kg9/13/2000 08-04-091300-33-S-STS 614814 4783340 8 0311027-11 Cl5-BZ#123 1.39 U µg/Kg 1.39 µg/Kg9/13/2000 08-04-091300-33-S-STS 614814 4783340 8 0311027-11 Cl5-BZ#126 1.23 U µg/Kg 1.23 µg/Kg9/13/2000 08-04-091300-33-S-STS 614814 4783340 8 0311027-11 Cl6-BZ#128 157 µg/Kg 1.10 µg/Kg9/13/2000 08-04-091300-33-S-STS 614814 4783340 8 0311027-11 Cl6-BZ#138 3020 µg/Kg 1.59 µg/Kg9/13/2000 08-04-091300-33-S-STS 614814 4783340 8 0311027-11 Cl6-BZ#146 309 µg/Kg 1.00 µg/Kg9/13/2000 08-04-091300-33-S-STS 614814 4783340 8 0311027-11 Cl6-BZ#149 156 µg/Kg 1.29 µg/Kg9/13/2000 08-04-091300-33-S-STS 614814 4783340 8 0311027-11 Cl6-BZ#151 28.4 µg/Kg 2.13 µg/Kg9/13/2000 08-04-091300-33-S-STS 614814 4783340 8 0311027-11 Cl6-BZ#153 2100 µg/Kg 1.83 µg/Kg9/13/2000 08-04-091300-33-S-STS 614814 4783340 8 0311027-11 Cl6-BZ#156 204 µg/Kg 1.31 µg/Kg9/13/2000 08-04-091300-33-S-STS 614814 4783340 8 0311027-11 Cl6-BZ#157 37.0 µg/Kg 1.02 µg/Kg9/13/2000 08-04-091300-33-S-STS 614814 4783340 8 0311027-11 Cl6-BZ#158 132 µg/Kg 0.864 µg/Kg9/13/2000 08-04-091300-33-S-STS 614814 4783340 8 0311027-11 Cl6-BZ#167 61.0 µg/Kg 1.10 µg/Kg9/13/2000 08-04-091300-33-S-STS 614814 4783340 8 0311027-11 Cl6-BZ#169 3.56 U µg/Kg 3.56 µg/Kg9/13/2000 08-04-091300-33-S-STS 614814 4783340 8 0311027-11 Cl7-BZ#170 270 µg/Kg 4.14 µg/Kg9/13/2000 08-04-091300-33-S-STS 614814 4783340 8 0311027-11 Cl7-BZ#174 0.844 U µg/Kg 0.844 µg/Kg9/13/2000 08-04-091300-33-S-STS 614814 4783340 8 0311027-11 Cl7-BZ#177 99.7 µg/Kg 1.19 µg/Kg9/13/2000 08-04-091300-33-S-STS 614814 4783340 8 0311027-11 Cl7-BZ#180 522 µg/Kg 1.77 µg/Kg9/13/2000 08-04-091300-33-S-STS 614814 4783340 8 0311027-11 Cl7-BZ#183 116 µg/Kg 0.804 µg/Kg



Extracted 7/30/04






DETECTION LIMIT3

9/13/2000 08-04-091300-33-S-STS 614814 4783340 8 0311027-11 Cl7-BZ#187 627 µg/Kg 0.884 µg/Kg9/13/2000 08-04-091300-33-S-STS 614814 4783340 8 0311027-11 Cl7-BZ#189 1.59 U µg/Kg 1.59 µg/Kg9/13/2000 08-04-091300-33-S-STS 614814 4783340 8 0311027-11 Cl8-BZ#194 113 µg/Kg 1.85 µg/Kg9/13/2000 08-04-091300-33-S-STS 614814 4783340 8 0311027-11 Cl8-BZ#195 39.6 µg/Kg 1.83 µg/Kg9/13/2000 08-04-091300-33-S-STS 614814 4783340 8 0311027-11 Cl8-BZ#201 113 µg/Kg 1.61 µg/Kg9/13/2000 08-04-091300-33-S-STS 614814 4783340 8 0311027-11 Cl9-BZ#206 61.1 µg/Kg 2.15 µg/Kg9/13/2000 08-04-091300-33-S-STS 614814 4783340 8 0311027-11 Cl10-BZ#209 1.00 U µg/Kg 1.00 µg/Kg9/13/2000 08-04-091300-33-S-STS 614814 4783340 8 0311027-11 Monochlorobiphenyls 59.1 U µg/Kg 59.1 µg/Kg9/13/2000 08-04-091300-33-S-STS 614814 4783340 8 0311027-11 Dichlorobiphenyls 1.73 U µg/Kg 1.73 µg/Kg9/13/2000 08-04-091300-33-S-STS 614814 4783340 8 0311027-11 Trichlorobiphenyls 555 µg/Kg 5.93 µg/Kg9/13/2000 08-04-091300-33-S-STS 614814 4783340 8 0311027-11 Tetrachlorobiphenyls 6710 µg/Kg 0.924 µg/Kg9/13/2000 08-04-091300-33-S-STS 614814 4783340 8 0311027-11 Pentachlorobiphenyls 12200 µg/Kg 1.06 µg/Kg9/13/2000 08-04-091300-33-S-STS 614814 4783340 8 0311027-11 Hexachlorobiphenyls 6750 µg/Kg 1.69 µg/Kg9/13/2000 08-04-091300-33-S-STS 614814 4783340 8 0311027-11 Heptachlorobiphenyls 1460 µg/Kg 0.924 µg/Kg9/13/2000 08-04-091300-33-S-STS 614814 4783340 8 0311027-11 Octachlorobiphenyls 308 µg/Kg 0.844 µg/Kg9/13/2000 08-04-091300-33-S-STS 614814 4783340 8 0311027-11 Nonachlorobiphenyls 78.7 µg/Kg 2.15 µg/Kg9/13/2000 08-04-091300-33-S-STS 614814 4783340 8 0311027-11 Decachlorobiphenyl 1.00 U µg/Kg 1.00 µg/Kg9/13/2000 08-04-091300-33-S-STS 614814 4783340 8 0311027-11 Total Homologs 28100 µg/Kg 1.00 µg/Kg9/13/2000 08-04-091300-33-S-STS 614814 4783340 8 0311027-11 Percent Lipids 3.6 % 0.1 %9/12/2000 08-05-091300-6-S-STS 614814 4783340 8 0311027-12 Cl2-BZ#8 0.667 U µg/Kg 0.667 µg/Kg9/12/2000 08-05-091300-6-S-STS 614814 4783340 8 0311027-12 Cl3-BZ#18 1.48 U µg/Kg 1.48 µg/Kg9/12/2000 08-05-091300-6-S-STS 614814 4783340 8 0311027-12 Cl3-BZ#31/#28 135 µg/Kg 10.7 µg/Kg9/12/2000 08-05-091300-6-S-STS 614814 4783340 8 0311027-12 Cl4-BZ#44 36.6 µg/Kg 1.02 µg/Kg9/12/2000 08-05-091300-6-S-STS 614814 4783340 8 0311027-12 Cl4-BZ#45 1.36 U µg/Kg 1.36 µg/Kg9/12/2000 08-05-091300-6-S-STS 614814 4783340 8 0311027-12 Cl4-BZ#47 989 µg/Kg 1.72 µg/Kg9/12/2000 08-05-091300-6-S-STS 614814 4783340 8 0311027-12 Cl4-BZ#49 36.9 µg/Kg 0.845 µg/Kg9/12/2000 08-05-091300-6-S-STS 614814 4783340 8 0311027-12 Cl4-BZ#52 184 µg/Kg 0.961 µg/Kg9/12/2000 08-05-091300-6-S-STS 614814 4783340 8 0311027-12 Cl4-BZ#56 71.2 µg/Kg 0.504 µg/Kg9/12/2000 08-05-091300-6-S-STS 614814 4783340 8 0311027-12 Cl4-BZ#66 127 µg/Kg 0.674 µg/Kg9/12/2000 08-05-091300-6-S-STS 614814 4783340 8 0311027-12 Cl4-BZ#70 74.5 µg/Kg 0.589 µg/Kg9/12/2000 08-05-091300-6-S-STS 614814 4783340 8 0311027-12 Cl4-BZ#74 318 µg/Kg 1.04 µg/Kg9/12/2000 08-05-091300-6-S-STS 614814 4783340 8 0311027-12 Cl4-BZ#77 0.930 U µg/Kg 0.930 µg/Kg9/12/2000 08-05-091300-6-S-STS 614814 4783340 8 0311027-12 Cl4-BZ#81 0.923 U µg/Kg 0.923 µg/Kg9/12/2000 08-05-091300-6-S-STS 614814 4783340 8 0311027-12 Cl5-BZ#87 150 µg/Kg 0.411 µg/Kg9/12/2000 08-05-091300-6-S-STS 614814 4783340 8 0311027-12 Cl5-BZ#95 24.3 µg/Kg 0.318 µg/Kg



Extracted 7/30/04






DETECTION LIMIT3

9/12/2000 08-05-091300-6-S-STS 614814 4783340 8 0311027-12 Cl5-BZ#99 712 µg/Kg 0.217 µg/Kg9/12/2000 08-05-091300-6-S-STS 614814 4783340 8 0311027-12 Cl5-BZ#101 69.1 µg/Kg 0.620 µg/Kg9/12/2000 08-05-091300-6-S-STS 614814 4783340 8 0311027-12 Cl5-BZ#105 202 µg/Kg 0.302 µg/Kg9/12/2000 08-05-091300-6-S-STS 614814 4783340 8 0311027-12 Cl5-BZ#110 66.6 µg/Kg 0.589 µg/Kg9/12/2000 08-05-091300-6-S-STS 614814 4783340 8 0311027-12 Cl5-BZ#114 19.0 µg/Kg 0.271 µg/Kg9/12/2000 08-05-091300-6-S-STS 614814 4783340 8 0311027-12 Cl5-BZ#118 633 µg/Kg 0.636 µg/Kg9/12/2000 08-05-091300-6-S-STS 614814 4783340 8 0311027-12 Cl5-BZ#123 0.535 U µg/Kg 0.535 µg/Kg9/12/2000 08-05-091300-6-S-STS 614814 4783340 8 0311027-12 Cl5-BZ#126 0.473 U µg/Kg 0.473 µg/Kg9/12/2000 08-05-091300-6-S-STS 614814 4783340 8 0311027-12 Cl6-BZ#128 43.6 µg/Kg 0.426 µg/Kg9/12/2000 08-05-091300-6-S-STS 614814 4783340 8 0311027-12 Cl6-BZ#138 979 µg/Kg 0.613 µg/Kg9/12/2000 08-05-091300-6-S-STS 614814 4783340 8 0311027-12 Cl6-BZ#146 99.7 µg/Kg 0.388 µg/Kg9/12/2000 08-05-091300-6-S-STS 614814 4783340 8 0311027-12 Cl6-BZ#149 32.4 µg/Kg 0.496 µg/Kg9/12/2000 08-05-091300-6-S-STS 614814 4783340 8 0311027-12 Cl6-BZ#151 6.20 µg/Kg 0.822 µg/Kg9/12/2000 08-05-091300-6-S-STS 614814 4783340 8 0311027-12 Cl6-BZ#153 696 µg/Kg 0.706 µg/Kg9/12/2000 08-05-091300-6-S-STS 614814 4783340 8 0311027-12 Cl6-BZ#156 71.3 µg/Kg 0.504 µg/Kg9/12/2000 08-05-091300-6-S-STS 614814 4783340 8 0311027-12 Cl6-BZ#157 11.8 µg/Kg 0.395 µg/Kg9/12/2000 08-05-091300-6-S-STS 614814 4783340 8 0311027-12 Cl6-BZ#158 41.7 µg/Kg 0.333 µg/Kg9/12/2000 08-05-091300-6-S-STS 614814 4783340 8 0311027-12 Cl6-BZ#167 14.8 µg/Kg 0.426 µg/Kg9/12/2000 08-05-091300-6-S-STS 614814 4783340 8 0311027-12 Cl6-BZ#169 1.37 U µg/Kg 1.37 µg/Kg9/12/2000 08-05-091300-6-S-STS 614814 4783340 8 0311027-12 Cl7-BZ#170 128 µg/Kg 1.60 µg/Kg9/12/2000 08-05-091300-6-S-STS 614814 4783340 8 0311027-12 Cl7-BZ#174 0.326 U µg/Kg 0.326 µg/Kg9/12/2000 08-05-091300-6-S-STS 614814 4783340 8 0311027-12 Cl7-BZ#177 30.9 µg/Kg 0.458 µg/Kg9/12/2000 08-05-091300-6-S-STS 614814 4783340 8 0311027-12 Cl7-BZ#180 260 µg/Kg 0.682 µg/Kg9/12/2000 08-05-091300-6-S-STS 614814 4783340 8 0311027-12 Cl7-BZ#183 54.7 µg/Kg 0.310 µg/Kg9/12/2000 08-05-091300-6-S-STS 614814 4783340 8 0311027-12 Cl7-BZ#187 220 µg/Kg 0.341 µg/Kg9/12/2000 08-05-091300-6-S-STS 614814 4783340 8 0311027-12 Cl7-BZ#189 0.613 U µg/Kg 0.613 µg/Kg9/12/2000 08-05-091300-6-S-STS 614814 4783340 8 0311027-12 Cl8-BZ#194 62.3 µg/Kg 0.713 µg/Kg9/12/2000 08-05-091300-6-S-STS 614814 4783340 8 0311027-12 Cl8-BZ#195 21.3 µg/Kg 0.706 µg/Kg9/12/2000 08-05-091300-6-S-STS 614814 4783340 8 0311027-12 Cl8-BZ#201 50.9 µg/Kg 0.620 µg/Kg9/12/2000 08-05-091300-6-S-STS 614814 4783340 8 0311027-12 Cl9-BZ#206 47.0 µg/Kg 0.830 µg/Kg9/12/2000 08-05-091300-6-S-STS 614814 4783340 8 0311027-12 Cl10-BZ#209 6.71 µg/Kg 0.388 µg/Kg9/12/2000 08-05-091300-6-S-STS 614814 4783340 8 0311027-12 Monochlorobiphenyls 22.8 U µg/Kg 22.8 µg/Kg9/12/2000 08-05-091300-6-S-STS 614814 4783340 8 0311027-12 Dichlorobiphenyls 0.667 U µg/Kg 0.667 µg/Kg9/12/2000 08-05-091300-6-S-STS 614814 4783340 8 0311027-12 Trichlorobiphenyls 171 µg/Kg 2.29 µg/Kg9/12/2000 08-05-091300-6-S-STS 614814 4783340 8 0311027-12 Tetrachlorobiphenyls 2260 µg/Kg 0.357 µg/Kg



Extracted 7/30/04






DETECTION LIMIT3

9/12/2000 08-05-091300-6-S-STS 614814 4783340 8 0311027-12 Pentachlorobiphenyls 3530 µg/Kg 0.411 µg/Kg9/12/2000 08-05-091300-6-S-STS 614814 4783340 8 0311027-12 Hexachlorobiphenyls 2180 µg/Kg 0.651 µg/Kg9/12/2000 08-05-091300-6-S-STS 614814 4783340 8 0311027-12 Heptachlorobiphenyls 630 µg/Kg 0.357 µg/Kg9/12/2000 08-05-091300-6-S-STS 614814 4783340 8 0311027-12 Octachlorobiphenyls 198 µg/Kg 0.326 µg/Kg9/12/2000 08-05-091300-6-S-STS 614814 4783340 8 0311027-12 Nonachlorobiphenyls 60.6 µg/Kg 0.830 µg/Kg9/12/2000 08-05-091300-6-S-STS 614814 4783340 8 0311027-12 Decachlorobiphenyl 6.71 µg/Kg 0.388 µg/Kg9/12/2000 08-05-091300-6-S-STS 614814 4783340 8 0311027-12 Total Homologs 9040 µg/Kg 0.388 µg/Kg9/12/2000 08-05-091300-6-S-STS 614814 4783340 8 0311027-12 Percent Lipids 3.7 % 0.1 %


Data Report for the Collection of Small Mammals and ... · hudson river hudson river data report: small mammals and american woodcock collection, analysis of floodplain earthworms,

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