Curriculum Vitae MUTHU KUMARAN GNANAMANI Senior Research Scientist Center for Applied Energy Research University of Kentucky Lexington, KY- 40511, USA Tel: +1-859-257-0240 (O) Fax: +1-859-257-0302 [email protected]https://scholar.google.com/citations?hl=en&user=wD4o1C8AAAAJ www.caer.uky.edu Personal details: First name: Muthu Kumaran Last name: Gnanamani Date of Birth: 01-01-1979 (mm/dd/yyyy) Citizenship: India US visa type: Green Card holder (US permanent resident) Married status: Married Carrier Objectives To pursue research in the field of heterogeneous catalysis, particularly energy conversions related to the production of liquid fuels and chemicals from syngas (Fischer-Tropsch synthesis), CO 2 conversion, Catalysis in various petroleum conversion processes which include hydrotreating, hydrocracking and reforming. Work Experience Senior Research Scientist August 2012-present Center for Applied Energy Research, University of Kentucky, USA Scientist-II September 2011-July 2012 Center for Applied Energy Research, University of Kentucky, USA Post Doctoral Fellow 2007- August 2011 Center for Applied Energy Research, University of Kentucky, USA
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Curriculum Vitae
MUTHU KUMARAN GNANAMANI
Senior Research Scientist Center for Applied Energy Research University of Kentucky Lexington, KY- 40511, USA Tel: +1-859-257-0240 (O) Fax: +1-859-257-0302 [email protected] https://scholar.google.com/citations?hl=en&user=wD4o1C8AAAAJ www.caer.uky.edu Personal details:
First name: Muthu Kumaran
Last name: Gnanamani
Date of Birth: 01-01-1979 (mm/dd/yyyy)
Citizenship: India
US visa type: Green Card holder (US permanent resident)
Married status: Married
Carrier Objectives
To pursue research in the field of heterogeneous catalysis, particularly energy conversions related to the production of liquid fuels and chemicals from syngas (Fischer-Tropsch synthesis), CO2 conversion, Catalysis in various petroleum conversion processes which include hydrotreating, hydrocracking and reforming.
National Eligibility Test (NET) for CSIR-JRF, 2002, India
Best paper award for the paper entitled “Deuterium labeled ethanol tracer studies on Iron
catalyzed Fischer-tropsch synthesis” in AICHE, spring meeting-2010, March 21-26, San Antonio, TX, USA.
Co-chaired two sessions “Production of Fuels and Chemicals from Fischer-Tropsch
Hydrocarbons-I &II” in AICHE, spring meeting-2011, March 13-17, Chicago, IL, USA. Chaired a session “Production of Fuels and Chemicals from Fischer-Tropsch Hydrocarbons”
in AICHE, spring meeting-2012, April 1-5, Houston, TX, USA. Chaired a session “Production of Fuels and Chemicals from Fischer-Tropsch Hydrocarbons”
in AICHE, spring meeting-2013, April 28-May 2, San Antonio, TX, USA.
Invited lecture
Delivered a invited lecture on the topic of “Catalysis in Petroleum Refining and Gas to
Liquid Technology” at D.K.M college for women, Department of Chemistry on December 17, 2014 in a state level colloquium on Recent Trends in Physical and Chemical Sciences, Vellore, Tamil Nadu, India.
Delivered a invited lecture on the topic of “Chemistry and Technology of Petroleum” at C.A.H. college, Department of Chemistry on December 19, 2014, Melvisharam, Tamil Nadu, India
Professional Affiliation
Life member of Catalysis Society of India
Tri-state Catalysis Society, USA
Kentucky Academy of Science
Journals reviewed:
1. Journal of Catalysis
2. Catalysis Communications
3. Materials Chemistry and Physics
4. Microporous and Mesoporous Materials
5. Applied Catalysis A: General
6. Topics on Catalysis
7. Industrial Engineering and Chemistry Research
Research Experience:
Projects:
At CAER, University of Kentucky, USA
Current projects
1. Selective conversion of carbon dioxide to higher alcohols using alkali promoted
transition metal carbides as catalysts (internal project). 2. Selectivie conversion of syngas to oxygenates using ceria supported cobalt catalysts (It is
a collaborative work between CAER and INT, Rio de janeiro, Brazil).
Completed projects
3. Fe-Co bimetallic catalysts for CO2 hydrogenation reaction. 4. Kinetics study and water addition effects on CO hydrogenation using Pt promoted
Co/Al2O3 catalysts funded by Chevron, Catalysis Research & Development, USA. (2007-2008)
5. Hydrogenation of Carbon dioxide using doubly promoted (K, Cu) Fe catalysts: The effect of process variables on Fischer-Tropsch synthesis activity and selectivity.
6. FT mechanisms study for CO and CO2 hydrogenation using Fe, and Co based catalysts: H2-D2 Kinetic Isotope Effect, funded by Naval Research Laboratory, Washington DC, USA. (2008-2009)
7. FT mechanisms study for CO hydrogenation using Fe, and Co catalysts: Isotopic tracer study of deuterium labeled linear 1-alkenes and alcohols co-feed to Iron and cobalt Fischer-Tropsch synthesis.
8. Deuterium Kinetic Isotope study: Hydrogenolysis of ethyl butyrate over alumina supported cobalt and iron based catalysts.
9. Synthesis of alcohols from syngas using CeO2 supported Pt-Co catalysts. 10. Effect of biomass impurities (H2S, CS2, COS, NH3, K, Cl, As, Na, etc) on cobalt FT
synthesis testing in a CSTR funded by TDA Inc. USA. (2011-2013) 11. Development of testing protocol for the selective conversion of phenol to diphenyl oxide
using two-stage fixed-bed reactor operates at high temperature and atmospheric pressure funded by Eastman Co. USA. (2013)
Doctorate work with Dr. G Murali Dhar, IIP Dehradun, India
Thesis title: Studies on Microporous and Mesoporous materials supported Hydrotreating catalysts
1. Synthesis and characterization of mesoporous molecular sieves like SBA-15, SBA-16,
KIT-6, FSM-16 and their Al, Ti, Zr substituted materials. 2. Acidity measurements using microcalorimetric ammonia adsorption and DRIFTS
pyridine adsorption methods. Evaluation of acidity of various supported metal sulfide catalysts using in situ microcalorimetric ammonia adsorption method.
3. Preparation of Mo, CoMo, NiMo, W, NiW, CoW catalysts by incipient-wetness impregnation method using different supports like microporous zeolite and mesoporous silica.
4. Evaluation of various hydrotreating catalytic functionalities like Hydrodesulfurization, hydrogenation, and hydrocracking in a fixed-bed glass micro reactor operating at atmospheric pressure using model compounds (Thiophene, cyclohexene, cumene)
Technical skills
Catalyst synthesis for the conversion of various heterogeneous catalytic reactions in
particular catalysis related to fossil fuels.
Experience in preparing various supported and nanoparticle based catalysts by IWI, solgel, CVD, reverse micelle techniques, and template methods.
Surface area and BJH pore size distribution analysis (ASAP-2010, Micromeritics, USA)
Static volumetric high vacuum adsorption unit for studying low temperature oxygen
chemisorptions.
Temperature programmed reduction (TPD/TPR 2900, Micromeritics, USA)
Identifying crystalline phases on catalytic surfaces using X-ray diffraction (XRD Rigaku D-
Max 111B).
Interpretation of data obtained from ESCA and solid state NMR especially Si and Al nuclei.
Hands on experiences to work with laboratory scale micro fixed-bed and CSTR reactors for testing of Fe and Co based Fischer-Tropsch catalysts at high temperatures and pressures.
Gas chromatographic analysis of Fischer-Tropsch synthesis products.
Estimation of deuterium contents in FT synthesis products using GC-MS.
Hands on experience with HR-TEM (Knowledge on HRTEM usage for the study of metal
particle dispersion)
Hands on experience with SEM (S4800, Hitachi) and EDX to study the morphology and elemental mapping for various Fe and cobalt FT catalysts.
Semi quantitative method of determining radio activity of 14C-labelled compounds using radio isotope detector.
B.H. Davis, “Hydrogenation of carbon dioxide over K-promoted FeCo bimetallic catalysts”
(ChemCatChem).
Accepted manuscript
2. Muthu Kumaran Gnanamani, G. Jacobs, W.D. Shafer, B.H. Davis, “Dehydration of 2-octanol over Ca-doped CeO2” ChemCatChem 2016.
Published articles 2016
3. Muthu Kumaran Gnanamani, H.H. Hamdeh, G. Jacobs, Q. Dali, F. Liu, S.D. Hopps, G.A. Thomas, W.D. Shafer, Q. Xial, Y. Hu, B.H. Davis, “Fischer-Tropsch synthesis: Effect of Cu, Mn and Zn addition on activity and product selectivity of cobalt ferrite” RSC Adv., 6 (2016) 62356-62367.
4. Muthu Kumaran Gnanamani, G. Jacobs, V.R.R. Pendyala, S.D. Hopps, G.A. Thomas, W.D. Shafer, D.E. Sparks, Q. Xiao, Y. Hu, B.H. Davis, “Fischer-Tropsch synthesis: anchoring of cobalt particles in phosphorus modified cobalt/silica catalysts” Appl. Catal. A: Gen. 523 (2016) 146-158.
5. Muthu Kumaran Gnanamani, W.D. Shafer, R.A. Keogh, B.H. Davis, “Dehydrocyclization of C6 hydrocarbon with and without oxygen containing substituent over Pt/(Na)-Al2O3 catalyst” Catal. Lett. 146 (2016) 424-432.
6. Muthu Kumaran Gnanamani, Gary Jacobs, H.H. Hamdeh, W.D. Shafer, F. Liu, S. Hopps, G.A. Thomas, B.H. Davis, “Hydrogenation of carbon dioxide over Co-Fe bimetallic catalysts” ACS Catal. 6 (2016) 913-927.
7. Muthu Kumaran Gnanamani, Gary Jacobs, U.M. Graham, M.C. Ribeiro, W.D. Shafer, B.H. Davis, “Influence of carbide formation on oxygenates selectivity during Fischer-Tropsch synthesis over Ce-containing Co catalysts,” Catal. Today 261 (2016) 40-47.
2015 8. Muthu Kumaran Gnanamani, Gary Jacobs, Robert A Keogh, Wilson D Shafer, Dennis E
Sparks, Shelley D Hopps, Gerald A Thomas, Burtron H Davis, “Fischer-Tropsch synthesis: Effect of pretreatment conditions of cobalt on activity and selectivity for hydrogenation of carbon dioxide”, Appl. Catal. A: Gen. 499 (2015) 39-46.
9. Muthu Kumaran Gnanamani, Wilson D Shafer, Venkat Ramana Rao Pendyala, Debanjan
Chakrabarti, Arno de Klerk, Robert A Keogh, Dennis E Sparks, Burtron H Davis, “14C-
Labeled Alcohol Tracer Study: Comparison of Reactivity of Alcohols over Cobalt and
Dennis E Sparks, Vinay Prasad, Arno de Klerk, Burtron H Davis, “Fischer-Tropsch mechanism: 13C18O tracer studies on a ceria-silica supported cobalt catalyst and a doubly promoted iron catalyst”, Ind. & Eng. Chem. Res. 54 (2015) 6438-6453.
11. Venkat Ramana Rao Pendyala, Gary Jacobs, Muthu Kumaran Gnanamani, Yongfeng Hu, Aimee MacLennan, Burtron H Davis, “Selectivity control of Cu promoted iron-based Fischer-Tropsch catalyst by tuning the oxidation state of Cu to mimic K”, Appl. Catal. A:
Gen. 495 (2015) 45-53. 12. Debanjan Chakrabarti, Arno de Klerk, Vinay Prasad, Muthu Kumaran Gnanamani, Wilson
D Shafer, Gary Jacobs, Dennis E Sparks, Burtron H Davis, “Conversion of CO2 over a Co-Based Fischer–Tropsch Catalyst” Ind. & Eng. Chem. Res. 54 (4) (2015) 1189-1196.
2014 13. Muthu Kumaran Gnanamani, Gary Jacobs, Wilson D. Shafer, Burtron H. Davis, “Low
temperature water-gas shift reaction over alkali-I metal promoted cobalt carbide catalysts”
Topics in Catalysis 57 (2014) 612-618. 14. Thani Jermwongratanachai, Gary Jacobs, Wilson D Shafer, Venkat Ramana Rao Pendyala,
Wenping Ma, Muthu Kumaran Gnanamani, Shelley Hopps, Gerald A Thomas, Boonyarach Kitiyanan, Syed Khalid, Burtron H Davis, “Fischer–Tropsch synthesis: TPR and XANES analysis of the impact of simulated regeneration cycles on the reducibility of Co/alumina catalysts with different promoters (Pt, Ru, Re, Ag, Au, Rh, Ir)” Catal. Today 228 (2014) 15-21.
15. Uschi M Graham, Gary Jacobs, Muthu Kumaran Gnanamani, Stephen M Lipka, Wilson D Shafer, Christopher R Swartz, Thani Jermwongratanachai, Rong Chen, Fon Rogers, Burtron H Davis,
“Fischer–Tropsch Synthesis: Higher Oxygenate Selectivity of Cobalt Catalysts Supported on Hydrothermal Carbons” ACS Catal. 4 (6) (2014) 1662-1672.
2013 16. Muthu Kumaran Gnanamani, Hussein H. Hamdeh, Wilson D. Shafer, Burtron H. Davis,
“Fischer-Tropsch Synthesis: Effect of potassium on activity and selectivity over oxide and
carbide Fe catalysts” Catalysis Letters 143(11) (2013) 1123-1131. 17. Muthu Kumaran Gnanamani, Gary Jacobs, Wilson D. Shafer, Burtron H. Davis, “Fischer-
Tropsch Synthesis: Activity of metallic phases of cobalt supported on silica” Catalysis Today
215 (2013) 13-17. 18. Muthu Kumaran Gnanamani, Gary Jacobs, Hussein H. Hamdeh, Wilson D. Shafer, and
Burtron H. Davis, “Fischer-Tropsch Synthesis: A Mössbauer investigation of Iron containing catalysts for Hydrogenation of Carbon Dioxide” Catalysis Today 207 (2013) 50-56.
19. M.C. Ribeiro, Muthu Kumaran Gnanamani, I.R. Azevedo, R.C. Rabelo-Neto, G. Jacobs, B.H. Davis, F.B. Noronha, Fischer-Tropsch synthesis: studies on the effect of support doping with Si, Mn and Cr on the selectivity to alcohols in ceria supported cobalt catalysts” Topics in Catalysis 57 (2014) 550-560.
20. Dennis E Sparks, G Jacobs, Muthu Kumaran Gnanamani, V.R.R. Pendyala, Wenping Ma,
J Kang, W.D. Shafer, R.A. Keogh, U.M. Graham, P. Gao, B.H. Davis, “Poisoning of cobalt
Wenping; Shafer, Wilson D.; Davis, Burtron H. “Fischer-Tropsch synthesis: effect of ammonia impurities in syngas feed over a cobalt/alumina catalyst” Applied Catalysis, A: General 468 (2013) 38-43.
22. Peters, E. E.; Chakraborty, A.; Crider, B. P.; Davis, B. H.; Gnanamani, M. K.; McEllistrem, M. T.; Prados-Estevez, F. M.; Vanhoy, J. R.; Yates, S. W. “Level lifetimes in the stable Zr nuclei: effects of chemical properties in Doppler-shift measurements” Physical Review C: Nuclear Physics (2013), 88(2), 024317/1-024317/10.
23. Wenping Ma, G Jacobs, J Kang, D.E. Sparks, Muthu Kumaran Gnanamani, V.R.R. Pendyala, W.D. Shafer, R.A. Keogh, U.M. Graham, G.A. Thomas, B.H. Davis, “Fischer–Tropsch synthesis. Effect of alkali, bicarbonate and chloride addition on activity and selectivity”Catalysis Today 215 (2013) 73-79.
24. Thani Jermwongratanachai, G Jacobs, Wenping Ma, W.D. Shafer, Muthu Kumaran Gnanamani, P. Gao, B. Kitiyanan, B.H. Davis, J.L.S. Klettlinger, C.H. Yen, D.C. Cronauer, A.J. Kropf, C.L. Marshall, “Fischer–Tropsch synthesis: Comparisons between Pt and Ag promoted Co/Al2O3 catalysts for reducibility, local atomic structure, catalytic activity, and oxidation– reduction (OR) cycles” Appl. Catal. A: Gen. 464 (2013) 165-180.
142 (2012) 1180. 26. Muthu Kumaran Gnanamani, Wilson D. Shafer and Burtron H. Davis, “Deuterium Exchange
Study for Hydrogenation of D5-1-Pentene (4,4,5,5,5) Over Conventional Cobalt Fischer-
Tropsch Catalyst” Catal. Lett. 142 (2012) 190. 27. Muthu Kumaran Gnanamani, Gary Jacobs, Wilson D. Shafer, Mauro C. Ribeiro, Venkat
Ramana Rao Pendyala, Wenping Ma, and Burtron H. Davis, “Fischer-Tropsch synthesis: Deuterium isotopic study for the formation of oxygenatges over CeO2 supported Pt-Co catalysts” Catal. Commun. 25 (2012) 12.
28. C.M. Masuku, W.D. Shafer, W. Ma, Muthu Kumaran Gnanamani, G. Jacobs, D. Hildebrandt, D. Glasser, and Burtron H. Davis, “Variation of residence time with chain length for products in a slurry-phase Fischer-Tropsch reactor” J. Catal. 287 (2012) 93.
2011 29. Muthu Kumaran Gnanamani, Wilson D. Shafer, Dennis E. Sparks, Burtron H. Davis,
“Effect of CO2 containing syngas over Pt promoted Co/γ-Al2O3 and K-promoted Fe catalysts” Catalysis Communications 12(11) (2011) 936.
30. Muthu Kumaran Gnanamani, Gary Jacobs, Dennis E. Sparks, Wilson D. Shafer, Burtron H. Davis, “Deuterium Kinetic Isotopic study for hydrogenation of carbon oxides over Fe and cobalt catalysts” Catalysis Letters 141 (2011) 1420.
31. Muthu Kumaran Gnanamani, Mauro Ribeiro, Weinping Ma, Wilson D. Shafer, Gary Jacobs,Uschi M. Graham, Burtron H. Davis, “Fischer Tropsch synthesis: metal-support interfacial contact governs oxygenates selectivity over CeO2 supported Pt-Co catalysts” Applied Catalysis A: Gen. 393 (2011) 17.
32. Muthu Kumaran Gnanamani, Bob R. Keogh, Wilson D. Shafer, Buchang Shi, Burtron H. Davis, “Deutero-1-pentene tracer studies for Iron and cobalt Fischer-tropsch synthesis” Applied Catalysis A: Gen. 393 (2011) 130.
33. Muthu Kumaran Gnanamani, Gary Jacobs, Bob R. Keogh, Burtron H. Davis, “Deuterium kinetic isotopic study for hydrogenolysis of ethyl butyrate” Journal of Catalysis 277(2011) 27.
34. Janet C. Mohandas, Muthu Kumaran Gnanamani, Gary Jacobs, Wenping Ma, Yaying Ji, Syed Khalid, Burtron H. Davis, “Fischer-Tropsch Synthesis: Characterization and reaction testing of cobalt carbide, ACS Catalysis 1(11) (2011) 1581.
35. Weinping Ma, Gary Jacobs, Dennis E Sparks, Muthu Kumaran Gnanamani, Venkat Ramana Rao Pendyala, Chia H. Yen, Jennifer L.S. Klettlinger, Thomas M. Tomsik, Burtron H. Davis, “Fischer–Tropsch synthesis: Support and cobalt cluster size effects on kinetics over Co/Al2O3 and Co/SiO2 catalysts”, Fuel, 90 (2) (2011) 756-765.
2010 36. Muthu Kumaran Gnanamani, Bob R. Keogh, Wilson D. Shafer, Buchang Shi, Burtron H.
Davis, “Deuterium labeled ethanol tracer studies on Iron catalyzed Fischer-tropsch synthesis”
Applied Catalysis. A: Gen. 385 (2010) 46. 37. Muthu Kumaran Gnanamani, Gary Jacobs, Uschi M. Graham, Weinping Ma, Venkat
Ramana Rao, Pendyala, Mauro Ribeiro, Burtron H. Davis, “Studies on KIT-6 supported cobalt catalyst for Fischer-tropsch synthesis”, Catalysis Letters 134 (2010) 37.
38. Muthu Kumaran Gnanamani, Bob R. Keogh, Wilson D. Shafer, Burtron H. Davis, “Deutero-1-pentene tracer studies for Iron and cobalt Fischer-tropsch synthesis” Prepr. Pap.-Am.Chem. Soc., Div. Fuel Chem. 55 (2) (2010) 449.
39. Venkat Ramana Rao, Pendyala; Gary Jacobs; Janet C Mohandas; Mingsheng Luo; Wenping Ma; Muthu Kumaran Gnanamani; Burtron H. Davis “Fischer-Tropsch Synthesis: Attempt to tune FTS and WGS by alkali promoting of iron catalysts” Appl. Catal. A: Gen. 389 (1-2) (2010) 131.
40. Muthu Kumaran Gnanamani, Wilson D Shaffer, Heather D Willauer, Dennis R Hardy, Frederick W Williams, Burtron H Davis, Prepr. Pap.-Am. Chem. Soc., Div. Fuel Chem. 2009 54(2) 935.
48. Kumaran, G. Muthu; Garg, Shelu; Soni, Kapil; Kumar, Manoj; Sharma, L. D.; Rao, K. S. Rama; Dhar, G. Murali. Industrial Engineering Chemistry Research 46(14) (2007) 4747-4754.
2006 49. Kumaran, G. Muthu; Garg, Shelu; Kumar, Manoj; Viswanatham, N.; Gupta, J. K.; Sharma,
L. D.; Dhar, G. Murali. Energy & Fuels 20(6) (2006) 2308-2313. 50. Kumaran, G. Muthu; Garg, Shelu; Soni, Kapil; Prasad, V. V. D. N.; Sharma, L. D.; Dhar,
G. Murali. Energy & Fuels 20(5) (2006) 1784-1790. 51. Kumaran, G. Muthu; Garg, Shelu; Soni, Kapil; Kumar, Manoj; Sharma, L. D.; Dhar, G.
Murali; Rao, K. S. Rama, Applied Catalysis A: Gen 305(2) (2006) 123-129. 52. Chiranjeevi, T.; Kumaran, G. Muthu; Gupta, J. K.; Dhar, G. Murali, Thermochimica Acta
443(1) (2006) 87-92. 53. Dhar, G. Murali; Kumaran, G. Muthu; Kumar, Manoj; Rawat, K. S.; Sharma, L. D.; Raju,
B. David; Rao, K. S. Rama. Catalysis Today 99(3-4) (2005) 309-314. 54. Chiranjeevi, T.; Kumaran, G. Muthu; Gupta, J. K.; Dhar, G. Murali. Catalsis
Communications 6(2) (2005) 101-106. Book chapters:
1. Muthu Kumaran Gnanamani, H.H. Hamdeh, G. Jacobs, W.D. Shafer, D.E. Sparks, B.H. Davis, “Fischer-Tropsch synthesis: activity and selectivity of -Fe5C2 and -Fe3C carbides,” in Fischer-Tropsch Synthesis, Catalysts and Catalysis: Advances and Applications, (eds. B.H. Davis, M.L. Occelli), CRC Press, Taylor & Francis Group, Boca Raton, FL, USA, 2016, Ch. 2, pp. 15-30.
of support composition on catalytic functionalities of Mo, CoMo, NiMo hydrotreating
catalysts”, presented in 17th
National Symposium on Catalysis, Jan. 18-20, 2005, CSMCRI
Bhavnagar, Gujarat.
40. Gnanamani, Muthu Kumaran, N.S. Rao, G. Prabhakar, L.D. Sharma, G. Murali
Dhar, “Physico-chemical characterization and catalysis on beta zeolite supported tungsten
hydrotreating catalysts”, presented in 17th
National Symposium on Catalysis, Jan. 18-20,
2005, CSMCRI Bhavnagar, Gujarat.
References:
1. Professor Burtron H. Davis
Associate Director, CAER 2540 Research Park Dr Center for Applied Energy Research University of Kentucky, Lexington, KY-40511, USA Phone: 001 859-257-0251 Fax: 859-257-0302 [email protected]
2. Professor Murali Dhar Gudimella
Senior professor Department of Chemical Engineering
Gayatri Vidya Parishad college of Engineering
Kakinada, Visakhapatnam, Andhra pradesh-530 041, India Phone: 011-91-9490451176 [email protected]
3. Professor S. Sivasanker
Chair Professor National Centre for Catalysis Research Department of Chemistry Indian Institute of Technology - Madras, Chennai - 600 036 Phone: 011-91-9840103865 [email protected]