www.anton-paar.com Critical Process Control Points Where, What, How and Why? 工艺控制关键点讨论 Daniel L. Gore Application Specialist – Process Instruments Brewer & Malter Anton Paar GmbH
www.anton-paar.com
Critical Process Control Points Where, What, How and Why?
工艺控制关键点讨论
Daniel L. Gore
Application Specialist – Process Instruments
Brewer & Malter
Anton Paar GmbH
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Create a Process Plan of YOUR Brewery
啤酒生产工艺流程
3
Ask a lot of questions and review your process thoroughly.
通过一些问题来回顾下生产过程
What is the difference between lab and process measurements?
Lab measurements are static snapshots of a dynamic process.
Process measurements are live streaming surveillance video.
实验室和在线测量的不同点是什么?
实验室测量是动态生产过程的静态定格拍照.
在线测量是连续的实况监视录像。
Lab and Process Instrument Basics.1
实验室及在线仪器基础1
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Ask more questions and review your process thoroughly.
通过一些问题来回顾下生产过程
Why both laboratory and process instruments?
A laboratory measurement is performed in a stable environment at a
stable temperature and is calibrated regularly with a verified standard.
A process measurement is performed under process conditions with
variable temperature, flow, pressure, and concentration and must be
verified with a representative lab sample.
为什么同时需要实验室和在线仪器呢?
实验室测量是在稳定的环境、稳定的温度和通过标准方法定期校准的仪器下完成的。
在线测量是在温度、流速、压力、浓度都在变化的生产条件下完成的,需要通过进行实验室样品测量进行校正。
Lab and Process Instrument Basics.2
实验室及在线仪器基础2
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Lab and Process Instrument Basics.3
实验室及在线仪器基础3
Ask more questions and keep reviewing your process.
通过更多问题来回顾下生产过程
What exactly do you need to measure?
• Temperature, extract, pH, alcohol, color, viscosity, etc.
什么是真正需要测量的?
• 温度、原浓、PH、酒精度、色度、粘度等
Where exactly do you need to measure it?
• Mash tun, lauter tun, kettle, blending, packaging, wastewater?
• Do you need a lab instrument? A portable, handheld instrument?
An inline instrument?
需要在什么点去测量?
• 糖化锅、过滤槽、煮沸锅、高浓稀释、包装、废水?
• 你需要实验室仪器吗?一个便携的手持仪器?一个在线仪器?
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Lab and Process Instrument Basics.4
实验室及在线仪器基础4
Ask more questions and keep reviewing your process.
通过更多问题来回顾下生产过程
What is the total cost of ownership (TCO)?
= Instrument price + installation cost + lifetime maintenance
+ consumables + training
- increased production - time, energy and resource savings
总共的购置成本是多少(TCO)?
= 仪器价格+ 安装费用 + 维护费用 + 消耗 + 培训
- 增加的生产价值-时间、能源、财力节约
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Lab and Process Instrument Basics.5
实验室及在线仪器基础5
Ask yet more questions to ensure you didn‘t miss anything.
再通过一些问题来确保没遗忘什么事情
What is the best method to use?
• Do you have an existing method already in use?
• What works best with YOUR existing systems and requirements?
• Do you have a preferred installation method?
• What are the pros and cons of available installation methods? ?
什么方法是最好的方法?
• 你现在已经有使用的方法吗?
• 什么能很好的满足你现在的系统和要求?
• 你有想要的安装方法吗?
• 什么才是有效的安装方法?
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Lab and Process Instrument Basics.6
实验室及在线仪器基础6
Ask yet more questions to ensure you didn‘t miss anything.
再通过一些问题来确保没遗忘什么事情
What do you want to do with the information (short and long term)?
• Quality control? Automation? Regulatory control? All of these?
• Do you need a dedicated lab instrument? A portable instrument?
• Do you need a portable or starter system to start your QA lab?
你计划做什么事情(短期和长期)?
• 质量管理? 自动化? 法规控制? 以上所有?
• 你需要一个专用的实验室仪器吗?一个便携的仪器?
• 你需要一个便携的或者系统启动器来启动你的QA实验室吗?
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Available Measuring Principles 各种测量方式
(there are a lot....)
Alcohol
酒精度
NIR, density and sound velocity, density
and refractive index, sound velocity and
refractive index, ATR...
近红外,密度声速,密度折光,声速折光,衰减全反射
Extract
麦汁浓度
Oscillating U-tube, sound velocity,
refractive index, ATR... U型震荡管,声速,折光,衰减全反射
Color
色度 430 nm absorbance measurement... 430 nm 吸光度
pH Potentiometric 电势电位测定
Turbidity 浊度
3-angle light scattering, ratio method,
optical... 3角度光散射,比例方法,光学
CO2 Multiple volume expansion method,
optical, Henry‘s law, membrane...
多体积膨胀法,光学,亨利定律,膜渗透
O2 Optical, membrane... 光学,膜渗透
Viscosity
粘度 Rolling-ball, rotation, vibration... 转球,旋转,震动
To name just a few.....
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Method Recommendations
方法推荐
Look for approved and recognized methods:
寻找一些被公认的方法:
MEBAK: 2.9.2.3, 2.9.6.1 – 2.9.6.3
EBC: 1.6, 9.2.6, 9.28.5, 9.43.2
ASBC: Beer-2B, Beer-4, Beer-5
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Congress Mash
糊化
What to measure?
测量什么?
• °Plato (extract yield), smell, iodine test,
filtration, clarity, viscosity, pH, wort color, boiled
wort color, nitrogen content, protein solubility
and diastatic power
• °Plato浓度、气味、碘液试验、过滤、净度、粘度、PH,麦汁色度、煮沸麦汁色度、含氮量、蛋白质溶解度和糖化力
Why measure it?
为什么测量?
• Monitor malt quality, how it responds
during the mash and its ability to
convert its contents.
• 控制麦芽质量,糊化过程中如何反应及转化力
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Lauter Tun/Mash Filter Outlet
过滤槽/麦汁过滤出口
What to measure?
测量什么?
• °Plato (extract), temperature, viscosity, pH
°Plato (麦汁), 温度,粘度, pH
Why measure it?
为什么测量?
• Monitor first runnings, main wort and
last runnings
监控生产开始,进程及结束
• Automate when to send wort to the kettle or last
runnings to wastewater
实现自动输送麦汁到煮沸锅或自动输送至废水回收。
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Lauter Tun/Mash Filter Outlet
过滤槽/麦汁过滤出口
Why measure it?
为什么测量?
• Save time and water, increase lauter tun
efficiency, reduce wastewater
节约时间和水,提高过滤槽效率,降低水耗
• Shorten boil time and increase kettle
efficiency
减少煮沸时间,增加煮沸效率
• Ensure further enzyme activity
确保更长的酶活性
• Ensure proper viscosity for optimal extract
and lauter time
确保适当的粘度来得到最佳的麦汁和过滤时间
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Lauter Tun/Mash Filter Outlet
过滤槽/麦汁过滤出口
To kettle →
There are many options... 有很多选择…
Volume
Meter
DPRn
SPRn
mPDS 1100 or mPDS 5
ESC
ENTER
TEMP +16.14 °C
DENS: 1.33317 g/cm3
:
PER-D: 2574.976 us
Ai-curr: 0.160 mA
mPDS 1100
L
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How and where to measure it?
怎样?在哪里测量?
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Kettle
煮沸锅
What to measure?
测量什么?
• Extract, temperature, viscosity, pH
麦汁浓度,温度,粘度,pH
Why measure it?
为什么测量?
• Reduce boil time and increase kettle
efficiency
减少煮沸时间,增加煮沸效率
• Save time and energy
节省时间和能源
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Kettle
煮沸锅
Why measure it?
为什么测量?
• Enable further automation for boil end
提高煮沸的自动化程度
• Ensure proper viscosity for filterability
确保合适的粘度以提高滤过率
• Monitor foam stability
监控泡沫稳定性
• Ensure proper hop isomerization
保证适当的异构化作用
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Hot water mPDS 1100 or mPDS 5
ESC
ENTER
TEMP +16.14 °C
DENS: 1.33317 g/cm3
:
PER-D: 2574.976 us
Ai-curr: 0.160 mA
mPDS 1100
L
06
Hot water
Kettle
煮沸锅
External
boiler
DPRn
SPRn
SP
Rn
There are many options... 有很多选择…
How and where to measure it?
怎样?在哪里测量?
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Production Increase Brewhouse ROI
生产增加酿酒厂的ROI
Example:
8 brews/day (3 hours/brew)
x 10 min saved/brew
= 80 min/day saved
80 min/day saved
x 7 days
= 3.1 extra brews/week
3.1 extra brews/week x 52 weeks/year
= 161 extra brews/year possible
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Cellar and Product Blending
发酵及高浓稀释
What to measure?
测量什么?
• Extract, alcohol, CO2, O2, pH, color, turbidity, viscosity, etc.
浓度、酒精度, CO2, O2, pH, 色度, 浊度, 粘度等
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Cellar and Product Blending
发酵及高浓稀释
Why measure it?
为什么测量?
• Monitor fermentation progress and avoid fermentation issues
控制发酵进程,避免发酵问题
• Proactively blend product to avoid production bottlenecks
混合产品,避免生产瓶颈
• Adjust CO2 content before packaging
包装之前校正CO2浓度
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Cellar and Product Blending
发酵及高浓稀释
Why measure it?
为什么测量?
• Avoid tax issues (gravity or alcohol and country specific)
避免税金事宜(比重或酒精度或政府明确的)
• Ensure product consistancy and quality
确保产品质量和一致性
• Increase production
增加产量
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Cellar and Product Blending
发酵及高浓稀释
Pressure and flow control
CO
2
H2O
Process pump
Blending
To BBT
and
carbonation
Measure Alcohol, Real and Original Extract and CO2
测量酒精度、真浓、原浓和CO2
How and where to measure it?
PLC
DSRn
Ca
rbo
51
0
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Production Increase: Blending ROI
产量增加:混合ROI
Real Example:
Target alcohol is 4.8%
200hl beer @ 4.9% alc blended with 4.17 hl H2O
= 204.17hl beer @ 4.8% alc
Every liter of water = additional beer
每多加一升水=多产的啤酒
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Packaged Product
成品包装
What to measure? 测量什么?
• Extract, alcohol, CO2, O2, TPO, pH, color, turbidity, viscosity, etc.
浓度、酒精度, CO2, O2, TPO, pH, 色度,浊度,粘度等
Why measure it? 为什么测量?
• This is the last QA check possible
这是最后的QA检查
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Packaged Product
成品包装
Why measure it? 为什么测量?
• Ensure product consistancy and quality
确保产品质量和一致性
• Verify process instrumentation
核实在线仪器的可靠性
• Avoid tax issues
避免税金事宜
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Possible Lab Measurements
可能的实验室测量
Wort / Fermentation
麦汁/发酵
% Alcohol (v/v, w/w)
°Plato
Color色度
Viscosity粘度
Degree of fermentation…
发酵度
Beer 啤酒
%v/v 酒精度
°Plato original extract原浓
Apparent, real and orginal
extract, calories…
表观浓度,真浓,原浓,卡路里
Options 选项
Color
色度
Turbidity
浊度
CO2
pH
O2
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Thank you!
Thank you
Prost! 乾杯! Cheers!