Page 1
01890 Final ReportJanuary 31,1996
Appendix CPage17of43
COMPOUND IDENTIFIED
Nonane, 4-methyl
Octane, 3,6-dimethyl
Pentane, 2,2,4-trimethyl (Isooctane)
Pinene, a(2,6,6-Trimethyl-bicyclo[3.1.1 Jhept-2-ene1
Styrene
Toluene (Methylbenzene)
Unidentified
Xylene (para and/or meta)
Xylene, ortho
cis-I-Ethyl-3-methykyciohexane*
1.0 6.0 24.0 48.0 72.0 96.0
1.9
.2.3
1.6 0.7
3.4
7.0 3.1 5.5 5.5 4.2 6.5
9.2 0.7
1.5
4.8
2.0
4.0
%dicates best NISTIEPANH library match only.Individual compounds and TVOC (total volatile organic compounds) are calibrated relative to toluene.TVOC detection limit: 0.9 yg/m’. Individual detection limits may vary, depending on instrument response.
.
Page 2
Environmental Chamber,Product Loading:Test Conditions:
Test Period:
01890 Final ReportJanuary 31,1996
Appendix CPage18of43
Cushion C
SA30.42 m2/m31.00 ACH50.0% RH f 5.0% RH23.0 degs C f 2.0 degs C06/22/95 - 06126195
CHAMBER 7VOC CONCENTRATIONS FROM 0.000 TO 96.000 HOURS
ELAPSED T v o cEXPOSURE CONCENTRATION
HOUR ug/m3
0.000 0.0
1 .ooo 915.0
6.000 826.6
24.000 265.3 .
48.000 366.9
72.000 253.1
96.000 38.8
IVOC CONCENTtiTIONS (pg/m’) FROM 0.000 TO 96.000 HOURS
COMPOUND IDENTIFIED 1.0 6.0 24.0 48.0 72.0 96.0
1,3-Dioxolan-2-one, cl-methyl’ 5.9 4.8 11.0 9.1
l-Octanol, 3,7-dimethyl* 2.0 2.4
I-Pentanol, 2-methyl-’ 1.5
I-Pentanol, 4-methyl-2-propyl- (9CI)* 3.0
2,2,7,7-Tetmmethyloctane” 15.6 5.5
2,6-Diitert-butyWmethylphenol (BHT) 66.9 106.1 31.3 82.5 72.1 38.8
2-Hexanol, 5-methyl-* 4.5
2-Propanol (Isopropanol) 2.2
-I_.-__IL-. . . ..--- - -^__-_l”^
Page 3
01890 Final ReportJanuary 31,1996
Appendix CPage19of43
COMPOUND IDENTIFIED 1.0 6.0 24.0 48.0 7i.o 96.0
2-Propanol, 1 ,3-dichloro- 74.8 106.3 41.6 65.2 86.3
2.Propanone, I-(dimethylamino)-* 5.6
2i-k2,4a-Methanonaphthalene, 1.6 1.3 1.0 1.7 0.81,3,4,5,6,7-hexahydro-l , I ,5,5-tetramethyl-, (2s).’
4-Octanol, 4,7-dimethyl-* 1.2
A&amide, N,N-dimethyl- (8Cl9CI) 82.0 65.0 61.8
Acetone (2.Propanone) 11.2
Benzene, I-ethyl-4-methyl 2.6(IdEthyltofuene)
Benzene, I-methyl+(1-methylethyl) 2.2(p-Cymene; 4-lsopropyltoluene)*
Benzene,(l ,I-Dimethylethyl)- . 6.8 2.0(t-Butylbenzene)*
Butane, 1.52,2’-[methylenebis(oxy)]bis[2-methyl-*
Cyclohexane, propyl 1.7
Cyclohexanone, 4-methyl-* 1.4
Cyclohexasiloxane, dodecamethyl* 8.9 9.4 3.1 1.6
Cyclopentasiloxane, decamethyl* 145.4 123.7 7.3 0.8
Cyclotetrasiloxane, octamethyl 132.3 32.1
Decane, 2,5,9-trimethyl- (9CI) 5.0 4.6 0.7
Decane, 2-methyl’ 5.1 3.4
Decane, 3-methyl 16.8 5.1
Decane, 4-methyl 10.3 6.1
Dodecane 3.4 1.2
Ethane, III, I-trkhloro 2.8
Ethane, 1,2-dichloro 1.9 .
Ethane,l ,l’oxybis[2-chloro- 1.2(s-Dichloroethyl ether)
Ethanol 10.9
Page 4
01890 Final ReportJanuary 31,1996
Appendii CPage 20 of 43
COMPOUND IDENTIFIED 1.0 6.0 24.0 48.0 72.0 96.0
Ethene, 1,1,2,2-tetrachloro 2.7(Tetrachloroethylene)
Fomramide, N,N-dimethyl 2.8 78.9 13.5 6.1
Hepiane, 2,2,4,6,6-pentamethyl (8Cl9CI)” 6.8 1.9
Heptane, 2.2,6,6-tetramethyl* 11.2 1.3
Heptane, 4-ethyl-2,2,6,6-tetramethyl- 18.9 7.3(9Cl)
Hexanal (Hexaldehyde) 1.4
Hexane, 1 ,Y-Oxybis (Hexyl ether* 1.5
Hexane, 2,2,4-trimethyl 2.3
Isooctane, (ethenyloxy)- (9CI)* 1.3
Methanol 28.7 5.4
Methylene chloride (Dichloromethane) 5.1
N,N-Dimethyl-2-propenamide 5.0 100.9 70.9 126.8 82.6
Nonane 2.9
Nonane, 2,5-dimethyl-* 13.1 5.9
Nonane, 3,7-dimethyl’ 3.4
Nonane, 3-ethyl 1.9
Nonane, 3-methyl 1.5
Nonane, 4,5-dimethyl* 2.1 -
Octane, 2,2-dimethyl* 4.7
Octane, 2,3,6-trimethyl-* 2.7
Octane, 2,3-dimethyl* 2.3
Octane, 2,6-dimethyl 3.0
Oxetane, 2+dimethyl-, trans-* 5.9 1.2
Oxirane, (chloromethyl)-• 1.4
Pentane* 1.3
Pentane, 2,2,4-trimethyl (Isooctane) 9.2 1.4
Pentane, 2,3,4-trimethyl 3.4
Page 5
01890 Final ReportJanuary 31,1996
Appendix CPage 21 of 43
.
COMPOUND IDENTIFIED
Pentane, 3-ethyl-2,2-dimethyl- (8Cl9CI)”
Phenol
Propane,? ,2,3-trichloro
Toluene (Methylbenzene)
Undecane
Undecane, 6-methyl-’
Unidentified
Xylene (para and/or meta)
Xytene, ortho
a-Methylstyrene (iso-Propenylbenzene;(I-Methylethenyl)benzene)
1.0 6.0 24.0 48.0 72.0 96.0
2.8
.2.7 1.5 2.0
129.0 111.5 20.6 6.5
59.9 2.5
9.4 4.1
3.2 1.3
5.7 2.3
7.1
2.8
3.7 2.3
%dkates best NISTIEPAMH library match only.hdiidual compounds and TVOC (total volatile organic compounds) are calibrated relative to toluene.NDC detection limit: 0.9 pg/m’. Jndividual detection limits may vary, depending on instrument response.
Page 6
01890 Final ReportJanuary 31,1996
Appendix CPage 22 of 43
Environmental Chamber.Product Loading:T& Conditions:
TestPeriod:
Cushion D
SA40 40 m2/m3I:00 ACH50.0% RH f 5.0% RH23.0 degs C f 2.0 degs C06/26/95 - 06/30/95
CHAMBERTVOCCONCENTRATIONS FROM0.000TO96.000HOURS
ELAPSED TvocEXPOSURE CONCENTRATION
HOUR (pglm3)
0.000 0.0
1 .ooo 349.0
6.000 634.9
24.000 421.6
48.000 345.8
72.000 NA*
96.000 212.0 4
‘NA: data not available due to laboratory error.
lVOCCONCENTRAT10NS(pglm3)FROM0.000T096.000HOURS
COMPOUND IDENTIFIED
l&Dimethylpiperazine
I H-Cyclopropa[a]naphthaIene,la,2,3,5,6,7,7a,7b-octahydro-1,1,7,7a-te!ramethyl-,[laR-(laa,7a,7aa,7ba)J*
1.0 6.0 24.0 48.0 96.0
58.5 319.1 71.4 55.3
1.3 1.7 1.3
2,2,7,7-Tetramethyloctane* 0.8
2,6-Di-terkbutyl4methylphenol 23.5 108.1 149.9 122.1 100.9(WIT)
2-Butenal’ 2.1
Page 7
01890 Final ReportJanuary 31,1996
Appendii CPage 23 of 43
COMPOUND IDENTIFIED
2-Propanol (isopropanol)
44sobutylmorpholine*
Acetamide, N,N-dimethyl- (8Cl9CI)
Acetate, butyl
Acetic acid, hydroxy-•
Acetone (2,Propanone)
3enzene, l,2,4-trimethyl
Benzene, 1,2-dichloro
Benzene, ethyl
Benzene, propyl
Butane, 2-methyl (Isopentane)
Cyclohexasiloxane, dodecamethyl*
1.0 6.0 24.0 48.0 96.0
2.5
1.1
13.0 19.4 15.7 11.0 7.4
1.1
1.0
5.9
0.7
7.7 8.0 5.3 3.8 1.9
1.0
1.0
Ethane, 1, 1, I-trichloro
Ethanol, 2-butoxy
Page 8
01890 Final ReportJanuary 31,1996
Appendix CPage 24 of 43
COMPOUND IDENTIFIED 1.0 6.0 24.0 48.0 96.0I
Octane, 2,3-dimethyl
Pentane, 2,2,4-trimethyl (Isooctane)
Pentane, 2,3,4-trimethyl’
Phenol
Pinene, a(2,6,6-Trimethyl-bicyclo[3.1.l]hept-2-ene)
Styfene
1.2
2.11
0.6
1.0
1.1
40.6 40.3 23.1 12.2 4.2
Toluene (Methylbenzene) 16.9 4.0
Undecane 1.6 1.0
Unidentified 100.8 101.2 138.2 130.4 90.7IXyiene, ortho I 1.5 I I I I
Wtkates best NISTEPAINIH library match only.Individual compounds and TVOC (total volatile organic compounds) are calibrated relative to toluene.TVOC detection limit: 0.9 pg/m’. Individual detection limits may vary, depending on instrument response.
Page 9
01890 Final ReportJanuary 31,1996
Appendii CPage 25 of 43
Cushion E
Environmental Chamber:Product Loading:Test Conditions:
Test Period:
SA50.42 m2/m3I .OO ACH50.0% RH k 5.0% RH23.0 degs C f 2.0 degs C06/26/95 - 06/30/95
CHAMBER TVOC CONCENTRATIONS FROM 0.000 TO 96.000 HOURS
EXPOSURE CONCENTF$ATIONELH’+P;;D /;;)
0.000 0.0
1 .ooo 1447.1
6.000 1631.1
24.000 1260.0
48.000 856.1
72.900 572.9
96.000 177.7
IVOC CONCENTRATIONS &g/m’) FROM 0.000 TO 96.000 HOURS
COMPOUND IDENTIFIED 1.0 6.0 24.0 48.0 72.0 96.0
-1,2-Propanediol (Propylene 3.1 27.1 28.1 26.8 20.2glycol)
I ,3-Butanediol’ 4.2 44.9 40.4 41.5 30.6
1,3-Cyclohexadiene, 2.5 2.2I-methyl4(+methylethyl)-• I1 $I-Cyclohexadiene, 0.8I-methyl+(‘l-methylethyl)- (9CI)
I ,4-Dimethylpiperazine 2.1
1 +Dioxane, 3.12-methyl-3-methylene-*
1-Heptanol, 6-methyl* 1.7
Page 10
01890 Final ReportJanuary 31,1996
Appendix CPage 26 of 43
COMPOUND IDENTIFIED ‘1.0 6.0 24.0 48.0 72.0 96.0
IiUndecene, 8-methyl-* 6.5 5.3
2(3H)-Furanone,dihydro 3.3 3.5' 2.9 1.9(Butyrolactone)*
2,3-Butanediol 2.9 28.2 24.5 26.2 19.8
2,6-Octadien-I-01, 3,7-dimethyl-, 1.7(Z)-*
2-Butanone, 3-hydroxy-• 2.1
2-Decene, 4-methyl-, (Z)* 6.2
2-Decene, %methyl-, (Z)-” 5.7 2.7
2-Decene, 8-methyl-, (Z)-* 3.0 1.6
3-Cyclohexene-‘l-methanol, 43.7 69.1 49.8 54.7 35.7 20.2a,a,4-trimethyl-, acetate*
4-Dodecene” 8.0 6.9
4-Phenylcyclohexene 2.3 9.8 8.4 5.5 3.0 1.6
4-Undecene, (Z)-• 7.0 6.3
NJndecene, (E) 8.3 6.4
6-Dodecene, (E)- (8Cl9CI)” 3.1
Acetamide, N,N-dimethyl- 2.7 2.5 3.4 1.7(8Cl9CI)
Acetate, methyl (Acetic acid, 11.4 1.7Methyl ester)
Acetic acid 1170.4 1271.3 1004.@ 641.7 426.1 137.5
Acetic acid, phenylmethyl ester 8.4 3.9 2.1 1.2lBenzyl acetate)
Acetone (2.Propanone) 16.8 3.7
Benzaldehyde 8.1 4.1 2.8 1.7 2.2
Benzyl alcohol 7.1 4.4 6.0 3.8 1.6(Benzenemethanol)
Bicyclo[3.1 .l]heptane-2-methano 0.3I, 6,6-dimethyl-, acetate*
-“-- ..- --I-. -“.”
-_ - I . .I. --.-_l_---_l_.__ . . . _ _ _
___.
Page 11
01890 Final ReportJanuary 31,1996
Appendix CPage 27 of 43
COMPOUND IDENTIFIED
Biqrclo~.2.0]undec-4-ene,4J I,1 Wimethyl-8-methylene-,[IR-(1 R@,42,9S@)]-*
Cedrene, a*
Cyclohexane, 1, I’-oxybis*
Cyclohexanol
Cyclohexanol,I-methyl4(1-methylethenyl)-,acetate*
Cyclohexene,l-methyl-4-(I-methylethylidene)-•
Cyclopentasiloxane, decamethyl*
Cyclopropane, l-ethyl-2-heptyl-(9Cl)’
Cyclotetrasiioxane, octamethyl
Decane
Ethanol
Limonene (Dipentene;
j-Methyl4( 1 -methylethyl)cyciohexene)
Methanol
Nonane, 2,6-dimethyl’
Propanoic acid
Toluene (Methylbenzene)
1.0 6.0 24.0 48.0 72.0 96.0
1.2 1.4 1.3
5.0 5.3 5.7 2.5 4.8 1.7
2.5 2.1 1.2
1.8
1.2 1.3 0.9
22.3 20.1 9.0 2.7 1.0 0.9
21.4 2.4
7.3 4.7
1.3
1.4 1.9
3.1 1.8
25.9 35.0 31.0 13.9 6.0 6.6
24.6
2.0
-19.6 16.8 12.3 9.5 1.5
4.8
WI --._- . -- _- -_
---*,
Page 12
01890 Final ReportJanuary 31,1996
Appendix CPage 28 of 43
,1 COMPOUND IDENTIFIED 1.0 6.0 24.0 48.0 72.0 96.0
Tricyclo[5.4.0.02,8]undec-9-ene, 7.7 8.3 7.7 4.8 4.8 3.12,6,6,9-tetramethyl-•
Unidentified 14.7 4.4 5.0 1.1 1.3 0.9 4
Wckates best NISTIEPAINIH library match only.tndiiual compounds and TVOC (total volatile organic compounds) are calibrated relative to toluene.TVOC detection limit: 0.9 vg/m’. Individual detection limits may vary, depending on instrument response.
Page 13
01890 Final ReportJanuary 31,1996
Appendix CPage 29 of 43
Carpet B at Elevated Conditions (70 “C, 8% RH, high loading)
Environmentalchamber:Product Loading:Test Conditions:
TestPeriod:
SC41.64 m2/m3l.OOACH8.0% RH f 2.0% RH70.0 degsCk5.0degsC06121/95 - 06/21/95
CHAMBERTVOCCONCENTRATlONSFROM0.000TO99.000HOURS
t
ELAPSED T v o cEXPOSURE CONCENTRATION
HOUR @g/m3
-J
lVOCCONCENTRAT10NS(~g/m3)FROM 0.000T06.000 HOURS
COMPOUND IDENTIFIED 0.0 1.0 6.0
1,2-Ethanediol (Ethylene glycol) 98.3 466.0
1,3-Butanediol, (S)-' 4.3
l+Pentadien-3-01' 36.3 7.9
I-Butanol (N-Butylalcohol) 165.1 12.3
A-Decanol (N-Decyl alcohol) 60.6 21.6
I-Decene, 8-methyl 292.6 92.5
I-Dodecanol 766.5 63.4
I-Dodecene* i 51.8 17.5
'I-Heptanol,6-methyl* 1163.7 288.2
1-Hexene 4.5
I-Octanol, 2-butyl-(8Cl9CI)* 7.1 178.7
I-Octene, 2.6-dimethyl-* 74.6 22.5
Page 14
01890 Final ReportJanuary 31,1996
Appendix CPage 30 of 43
COMPOUND IDENTIFIED
I-Propanol (Propyl alcohol)
I-Propanol, 2-(2-hydroxypropoxy)*
1-Propene, 3-chloro-2-methyl-*
I-Tetradecanol’
2(1 i-i)-Naphthalenone,octahydro4a,7,74rimethyl-,trans-•
0.0 1.0 6.0
57.7 13.3
405.1 371.5
9.1 2.9
468.6 13.8
142.4 9.1
2,2/LTrimethyl-1,3-pentanediolmonoisobutyrate (Texanol)
2,2-Dimethyl-I-isopropyl-1,3-propanediol monoisobutyrate(Texanol)
2,6-Diitert-butyl+methyIphenolNJ-l
2,6-Octadien-l-01, 3,7-dimethyl-,acetate, (2).•
2,6-Octadien-1-ol,3,7-dimethyl, (E)- (Geraniol)’
2-Butanone (Methyl ethyl ketone,MEK)
2-Butenal, 2-ethenyf-•
2-Cyclohexen-l-one,2-methyl-5-( 1 -methylethenyl)-*
2-Decene, g-methyl-, (2).•
2-Decene, (Z)-•
2-Decene, 3-methyl-, (Z)-•
2-Decene, 5-methyt-, (Z)-*
2-Decene, 7-methyl-, (2)’
2-Dodecen-l-yl(-)succinicanhydride*
2-Dodecene, (E)’
’2-Naphthalenemethanol,a-meth+, (.+I-J-•
267.2 33.7
137.3 29.0
2351.0 328.3
78.8 6.3
* 10.4 6.4
5.0
2.4
14.3 6.9
217.8 44.4
327.7 79.0
387.6 173.0
220.0 35.8
1090.4
322.3
6.3
Page 15
01890 Final ReportJanuary 31,1996
Appendix CPage 31 of 43
COMPOUND IDENTIFIED
2-Octene, (E)-*
2-Octene, (z)-•
2-Octene, 4-ethyL*
2-Pentanone, 4hydroxy4methyl-(m9cI)*
2-Pentanone, 4-methyl (Methylisobutyl ketone, MIBK)*
2-Propanol (lsopropanol)
2-Propen-l-01, 2-methyl
2-Propenal’
2-Propenoic acid, methyl ester*
2 - U n d e c e n e , 2,5-dimethyl-”
2l-LBenzocyclohepten-2-one,decahydro-4a-methyl-, trans-•
3,5-Cyclohexadiene-I ,2-dione,3,5-bis(1, I-dimethyfethyl)-•
3-Buten-2-ol*
3-Cyclohexene-l-methanol,a,a,4-trimethyl-*
3Cyclohexene+methanol,a,a,lltrimethyl-, acetate*
3-Decene*
SDecene, 2-methyl-, (Z)-•
3-Dodecene, (E)*
SDodecene, (Z)- (8Cl9Cl)*
3-Ethyl-2-methyl-I-heptene’
3-Octene, 2,6-dimethyl-•
3-Undecene, 2-methyl-, (E)-•
IdDecene, 3-methyl-, (E)-•
4-Dodecene*
0.0 1.0 6.0
12.6
8.7
96.7
64.6 4.9
5.2
21.1 4.1
6.0 0.8
3.9
37.6 13.6
500.0 172.2
1214.1
11.5
3.9
82.8 29.5
61.5 9.4
273.3 106.1
985.6 281.6
527.3 158.6
63.6
3.1
99.1 18.2
1660.4 469.6
697.0
521.5 152.5
Page 16
01890 Final ReportJanuary 31,1996
Appendix CPage 32 of 43
COMPOUND IDENTIFIED 0.0 1.0 6.0.
4-Isobutylmorpholine > 1317.7** 547.3
4-Nonene, 3-methyl, (2) .551.7 126.6
4-Nonene, 5-methyl-* 56.0 34.0
4-Octene, (E)’ 35.0
4-Octene, 2,3&trimethyl-• 130.5
4-Phenylcyclohexene 58.7 10.2
4-Piperidinecarboxylic acid, 633.1 26.24-phenyl-, ethyl ester*
4-tert-Butylcyclohexyl acetate* 3.3
5-Dodecene, (E)* 191.6 49.5
5-Undecene, (E)” 1045.9 331 .I
5-Undecene, (z)- (8C19CI)’ 1789.0 403.0
6-Dodecene, (E)- (BCl9Cl) 816.4 348.0
A&amide, N,N-dimethyl- 404.3 60.5(BCl9Cl)
Acetamide, 264.1 28.2N-methyl-N-[4-[4-methoxy-I-hexahydropyridyll-2-butynyi]-•
Acetate, ethyl 4.0
Acetic acid 0.9 153.3
Acetone (2.Propanone) 78.0 23.1
Azulene, 7-ethyl-1,4-dimethyl-* 8.1
Benzene, I-ethyM-methyl 43.1(4-Ethyltoluene) .Benzene, ethyl 23.4
Benzene.1 ,I’-Oxybis- (Diphenyl 126.4 10.3ether)’
Benzoic acid, 2-hydroxy-, I - 399.7 53.63-methylbutyl ester”
Benzoic acid, 2-hydroxy-, pentyl 333.3 * 10.1ester*
Page 17
01890 Final ReportJanuary 31,1996
Appendix CPage 33 of 43
COMPOUND IDENTIFIED 0.0 1.0 6.0
Benzoic acid, 138.0 4.73-(5-hydroxy-I-pentenyl)-, methylester, (E)-*
Benzothiatole 8.8
Butane 6.7
Butanoic acid 10.3
Caryophyllene oxide* 464.7
Cyclohexane, (I-methylpropyl)-* 44.1 4.2
Cyclohexane, 1,1,2-trimethyl* 11.6 1.2
Cyclohexane, 278.0 163.01 ,I-dimethyl-Z-propyl-”
Cyclohexane, 2.0I-ethenyM-methylene-5-(l-propenylidene)-*
Cyclohexane, I-ethyl-2-methyl-, 17.5 3.9cis- (8Cl9CI)”
Cyclohexane, methyl 5.2
Cyclohexane, octyl’ 33.6
Cyclohexane, propyl 61.0
Cyclohexane, t-I-ethyM-methyl* 32.8
’Cyclohexanol, 52.6 15.1Z-methylene-3-(I-methylethyl)-, -acetate, cis-•
Cyclopentane, 1,2,4-trimethyl, 11.0 1.7(1 a,2&4a)*
Cyclopentasiloxane, decamethyl’ 99.5 25.9
Decane 910.6 . 46.7
Decane, 6-ethyl-2-methyl- (9CI)* 12.1
Dipropylene glycol 229.4 23.7
Disiloxane, pentamethyl-• 4.1 ‘
Dodecane 122.8 11.2
Page 18
01890 Final ReportJanuary 31,1998
Appendix CPage 34 of 43
COMPOUND IDENTIFIED 0.0 1.0 6.0
Ethane, 1 , 1,l -trichloro 4.7
Ethanol 210.4 4.7
Ethanol, 2-(2-butoxyethoxy) 224.8 105.2
Ethanol, 2-butoxy 35.6 3.7
Ethanol, 2-phenoxy- 84.4 36.6
Furantetrahydro; THF 2.0
Heptadecane* 2.4
Heptanal (Heptaldehyde)* 2.8
Heptane 15.6
Heptane, 2,4-dimethyl 25.0
Heptane, 2,5-dimethyl* 13.6
Heptane, 3-methyl 10.9
Heptane, 3-methylene- (9Cl)” 16.6
Heptane, 4-methyl 12.4
Hexadecane (Cetane) 235.7 10.5
Hexadecane, 2,6,10-trimethyl-* 10.0
Hexane, 2,2,5-trimethyl- (8Cl9CI)* 126.6 5.2
Hexane, 2,2-dimethyl 67.5
Hexane, 3-methyl 15.8
Hexanoic acid 77.6 66.4
lsobomyl acetate* 363.5
Methanesulfonyl chloride* 1.9
Morpholine, LGmethyl 6.6 3.4
Naphthalene 69.7 22.3
Naphthalene, 1,2-dimethyl-* 79.8 3.4
Naphthalene, t ,4,6-trimethyl* 120.2 8.2
Naphthalene, 1 +dimethyl’ 193.8 5.2
Naphthalene, 1,6-dimethyl* 199.9 10.7
Page 19
01890 Final ReportJanuary 31,1998
Appendix CPage 35 of 43
COMPOUND IDENTIFIED
Naphthalene,1,6-dimethyl(l-methylethyl)-’
Naphthalene, l-methyl
Naphthalene, 2,3,6-trimethyl-(8Cl9CI)*
Naphthalene, 2,7-dimethyl*
Naphthalene, 2-methyl
Naphthalene,6(3-ethylpropyl)-1,2,3,4-tetrahydrol
0.0 1.0 6.0
436.3
23.5 5.3
18.5
96.0 3.8
28.3 10.8
123.9 9.3
Naphthalene, 298.7 12.4decahydro-4a-methyl-l -methylene-7+methylethylidene)- (4aR-bans)-*
Nonane 84.8 2.0
Nonane, 3-methyl 73.1
Nonane, 4-methyl 31.7 3.3
Octane 23.1
Octane, 2,6-dimethyl 121.1 15.6
Octane, 2-methyl 17.7
Octane, 3-methyl 43.6 14.4
Octane, Idethyl* 75.8
Pentadecane, 469.92,6,10,14-tetramethyl-• aPentane, 2,2,4&imethyl 560.7(Isooctane)
Pentane, 2,3,4-trimethyl 61.6
Pentane, 2,3-dimethyl (8C19CI)* 11.8
Pentane, 2+dimethyl* 8.4
Pentanoic acid (Valeric acid) 30.1 20.2
Phenol 183.4 68.7
Page 20
01890 Final ReportJanuary 31,1996
Appendix CPage 36 of 43
COMPOUND IDENTIFIED
Phenol,4,6-di(l ,I-dimethylethyt)-2-methyl-l
0.0 1.0 6.0
79.6 2.0
Phenol, bis(1 ,l-dimethylethyI)-(9Cl)’
Propanedioic acid, diproyl-, diethylester*
8.0
747.7 59.4
Pyridine,l,2,3,6-tetrahydro-4~[4,5-dihydroxypheny!]-1 -methyl-*
TXIB(2,2,4-TrimethyI-1,3-pentanedioldiisobutyrate)
Terbutol*
Tetradecane
Toluene (Methylbenzene)
Tridecane
Trimethylamine(methanamine,N,N-dimethyl)*
Unidentified
Xylene (para and/or meta)
52.5
- 324.8 19.2
66.5
110.0 3.4
289.2
22.8
0.6
1840.9 30.8
52.9
‘Mites best NISTIEPAINIH library match only.“Values marked with l >. symbol were outside linear range of detector. Concentration value is a lower bound only.Individual compounds and TVOC (total volatile organic compounds) are calibrated relative to toluene.TVOC detection limit: 0.9 vg/rn’. Individual detection limits may vary, depending on insbument response.
I I.--“-^“.“l ̂ -e-P.-- _- -
- . . ..----.
Page 21
01890 Final ReportJanuary 31,1998
Appendix CPage 37 of 43
Cushion B at Elevated Conditions (70 “C, 8% RH, high loading)
Environmental Chamber:Product Loading:Test Conditions:
SC51.65 m2/m31.00 ACH8.0% RH f 2.0% RH
Test Period:70.0 degs C f 2.0 degs C06/21/95 - 06/21/95
CHAMBER IVOC CONCENTRATIONS FROM 0.000 TO 6.000 HOURS
ELAPSED T v o cEXPOSURE CONCENTl$ATION
HOtJR
p?jEzyj
IVOC CONCENTRATICNS (pg/m3) FROM 0.000 TO 6.000 HOURS
COMPOUND IDENTIFIED 1.0 6.0
(tert-Butoxymethyl)oxirane* 37.2
1,2-Ethanediol (Ethylene glycol) 30.9 39.4
1,2-Propanediol (Propylene glycol) 37.2 42.6
1 +Dimethylpiperatine 9.5
I-Acetoxy-2-propanol* 23.9
I-Butanol (N-Butyl alcohol) 471 .o 134.8
I-Dodecene 29.3
I-Hexanol, 2-ethyl 71.4 80.7
l-Nonene, 4,6&trimethyl- (9CI)* 8.8 8.0
I-Octanot 11.0
I-Octanol, 2-butyl- (8Cl9Cl) 14.7
I-Octene, 3-ethyl-* 26.5 4.9
- _ ^I--~P - .-...
Page 22
01890 Final ReportJanuary 31,1996
Appendix CPage 38 of 43
COMPOUND IDENTIFIED
I-Pentanol, 3-methyl
l-Phenyl-l-propyne
?-Propane! (PropyI alcohol)
l-Tetradecene
A-Undecene
I H-lndene,2,3-dihydro-I,? ,3-trimethyl-*
1 H-lndene,2,3-dihydro-l,2-dimethyl-”
1 H-lndene,2,3-dihydro-1,3-dimethyl*
1 H-lndene,2,3-dihydro-4,7-dimethyl-*
I H-lndene, 2,3-dihydro+methyl*
1 H-Phenanthro[9,10-dlimidazol-2-amine+
2,2,4&Tetramethyioctane*
2.2,~Trimethyl- ,3-pentanediolmonoisobutyrate (Texanol)
2,2-Dimethyl-l-isopropyl-1,3-propanediol monoisobutyrate (Texanol)
2,5-Cyclohexadiene-1 +dione,2,6-bis(1 ,I-dimethylethyl)- (9’
2,6-Di-tert-butyI4methylphenol(BHT)
2-Ethylhexanoic acid
2-Pentanone, 4-hydroxy4methyk(8C[9Cl)*
2-Pentanone, LGmethyI (Methylisobutyl ketone, MIBK)
2-Propanol (Isopropanol)
2-Propanol, 1,3=dichloro-
1.0 6.0
8.3 4.9
13.5
118.9 19.2
7.6
35.3
7.9
28.1 48.9
46.8 41.0
29.5 25.0
69.4 59.5
81.1 119.1
58.0 95.9
34.2 41.9
90.7 - 134.4
1823.6 2585.8
664.5 1210.1
447.3 303.9
13.7
7.7
53.9 41.3
Page 23
01890 Final ReportJanuary 31,1996
Appendix CPage 39 of 43
COMPOUND IDENTIFIED
2-Propanol,I-II-methyl-2-(2-propenyloxy)ethoxy
1.0 6.0
* 29.0
2-Propenal’
2-Propenal, 2-methyl*
2-Pyrrolidinone, l-methyl
2H-2,4a-Methanonaphthalene,I ,3,4,5,6,7-hexahydro-I, 1,5,5-tetramethyl-, (2S)-•
3-Carene”
3-Pentanol*
3-Penten-2-one, 4-methyl- (8Cl9CI)*
4kobutylmorpholine
Acetamide, N,N-dimethyl- (8Cl9CI)
Acetate, butyl
Acetic acid
Acetic acid, 2-ethylbutyl ester’
Acetic acid, phenylmethyl ester
Acetone (2-Propanone)
Benzaldehyde
Benzene, 1,2,4,5-tetramethyl*
Benzene, 1,2&trimethyl
Benzene, 1,4-dichloro
Benzene, I-ethyl-2,4-dimethyl-*
Benzene, I-ethyl-2-methyl(2.Ethyltoluene)
Benzene,l-methyl4(l-methylethyl)(p-Cymene; 4lsopropyltoluene)
Benzene, 4-ethyl-l &dimethyl*
Benzene, ethyl
12.3
4.5
14.4
40.1 37.9
63.4
6.8
18.0 13.9
> 1135.3** > 1534.1”’
337.8 362.7
10.2
69.7
14.8 11.7
39.8
226.4 94.5
20.0 10.6
37.3
90.9 35.4
37.2 24.5
48.9 34.5
38.9 9.5
48.6 22.0
21.6
9.8
Page 24
01890 Final ReportJanuary 31,1996
Appendix CPage 40 of 43
COMPOUND IDENTIFIED
Butanal (Butyraldehyde)
Butanoic acid
Camphene
Cedrene, a*
Cyclohexane, hexyl’
Cyclohexanone
Cyclohexene,3-methyl-6-(I-methylethylidene)-•
Cyclohexene, 4-(1 ,I-dimethylethyl)*
Cyclopentane,1 -methyl-3-(29methylpropyl)-•
Cyclopentanone’
Cyclopentasiloxane, decamethyl*
Decane
Decane, 2,2,4-trimethyl-’
Decane, 2,6,6-trimethyl-*
Decane, 2-methyl
Decane, 3,8-dimethyl
Decane, S-methyl*
Dodecane
.Dodecane, 2,6, IO-trimethyl-*
Dcdecane, 3-methyl- (8Cl9CI)
Ethane, 1 , 1, I-trichlom
Ethane, 1,2-dichloro
Ethanol
Ethanol, 2-(2.butoxyethoxy)
Ethanol, 2-butoxy
Ethanol, 2-chloro-•*
1.0 6.0
5.2
8.5
81.4 23.9
16.0 12.8
42.4 35.5
8.9 7.2
91.6 91.0
51.4
15.6
11.7 16.6
77.2 34.4
114.1 18.0
37.7
43.2
40.8
35.0
73.2
80.0 - 57.4
10.6
17.5 17.2
3.1
4.6 5.5
36.3 6.3
46.3
33.4 23.2
2.8
Page 25
01890 Final ReportJanuary 31,1996
Appendix CPage 41 of 43
COMPOUND IDENTIFIED
Ethene, 1 ,I ,2,2-tetrachloro(Tetrachloroethylene)
EthylI-methylcyclopropanecarboxylate*
Heptane, 2,2,6+tetramethyl
Heptane, 2,4,6-trimethyl
Hexane, 2,2,5-trimethyl- (8Cl9CI)’
Hexanoic acid
lsobomyl acetate*
Limonene (Dipentene;I-Methyl+ 1 -methylethyl)cyclohexene)
LinalooP
Morpholine, 4-ethyl-’
N,N-Dimethyl-2-propenamide
Naphthalene
Naphthalene,-l,2,3,5,6,8a-hexahydro-4,7-dimethyl-I-(I-methylethyl)-, (IS-cis)-*
Naphthalene, 1,4,6-trimethyl*
Naphthalene, ‘l,4-dimethyl
Naphthalene, 1 J-dimethyl-(8Cl9CI)’
Naphthalene,I$-dimethyl4(?-methylethyl)-*
Naphthalene, I-(2.propenyl)*
Naphthalene, I-methi
Naphthalene, 2,3,6-trimethyl-(8Cl9CI)’
Naphthalene, 2,6-dimethyl-*
Naphthalene, 2-ethyl*
1.0 6.0
6.0
60.2
8.1
8.9
10.2
27.5
848.2 906.5
224.6 75.9
71.2
18.0
12.3 14.4
115.0 95.3
13.8
52.4
10.5 10.2
-6.6
11.6
3.4 3.0 -
21.8 24.9
50.5
9.5
5.9
.- 1-..
Page 26
01890 Final ReportJanuary 31,1996
Appendix CPage 42 of 43
.
COMPOUND IDENTIFIED
Naphthalene, 2-methyl
Naphthalene,G-(1 ,l-dimethylethyl)-1,2,3+tetrahydro-*
Nonane
Nonane, 3,7-dimethyl’
Nonane, 3-methyl-5-propyl-•
Nonane, 4,5-dimethyl*
Nonane, 4-methyl
Octane, 2,2,6-trimethyl*
Octane, 3-ethyl-2,7-dimethyl- (9CI)”
Pentanal (Valeraldehyde)
Pentane, 2,2+trimethyl (Isooctane)
Phenol
Phenol,2,6-bis(1 ,I-dimethylethyl)+ethyl*
Phenol, 4-t-butyl(4-(1 ,I-Dimethylethyl)phenol)*
Pinene, a(2,6,6-Trimethyl-bicycloI3.1 .A Jhept-2-ene)
Propane, 2-methyl-2-nitro*
Propanoic acid
Propanoic acid, 2,2-dimethyl-’
Propanoic acid, 2-methyl- (9CI)*
Propanoic acid,2-methyl-2-f(trimethylsilyl)oxy]-,trimethyp
Styrene
Styrene, 2,5-dimethyl*
Tetradecane
1.0 6.0
63.4 69.7
.36.4
14.4
96.5 24.1
33.0
140.6
32.0
50.9 11.8
118.8
4.1
2.7
165.1 168.3
34.6
10.4
21.7
7.3
12.4
8.1
6.1
10.1 8.2
19.4 5.5
31.5 28.9
15.3 5.8
Page 27
01890 Final ReportJanuary 31,1996
Appendix CPage 43 of 43
COMPOUND IDENTIFIED 1.0 6.0
Thiophene, 17.12-buty&(2-methylpropg)- (9CI)’ 1 I~;~?fJlethylbenzene) / XL; 1 7.8
14.3
Undecane I 186.1 I 96.4I
Undecane, 2,3-dimethyl-’ - 34.1 25.5
Undecane, 2-methyl 27.6
Undecane, 3,9-dimethyl- (8CI)*
Undecane, 5-methyl- (8dl9Cl)*
42.8 I 42.0
30.6
Unidentified 374.8 503.3
Xylene (para and/or meta) 40.8
Xylene, ortho 28.9 9.4
‘Indicates best NISTEPANIH library match only.“Values marked with “pa symbol were outside Gnear range of detector. Concentration value is a lower bound only.Individual compounds and TVOC (total volatile organic, compounds) are calibrated relative to toluene.IVOC detection liiit: 0.9 yg/m’. Individual detection limits may vary, depending on instrument response.
-.----__ _-- - . ---_ _
Page 28
APPENDIX D
INDIVIDUAL VOC CONCENTRAIIONS DURING EXPOSURESTO SYNTHESIZED MIXTURES
----_ .” - ---~.
Page 29
61890 Flnet ReportJanuary 31,1996
Appendix 0Page 1 of 37
TABLE D-l
CONCENTRATION DATA FOR EXPOSURE TOPRIME URETHANE “A” TEST MIXTURE
Compound Concentration (mg/m3) Mean PrecisionConcentration
Sample 1 Sample 2 Sample(% RSD)
3(first IO minutes jmliidle IO minutes (!ast 90 minutes of
h4Jm
of exposure) of exposure) exposure)
2,6-Di-tert-butyl-4- 6.2 12.3 12.1 10.2 33.9methylphenol
1,4=Dimethylpiperarine 11.1 16.2 17.2 14.8 21.9
1 , 1, I -Trichloroethane 6.8 7.0 7.2’ 7.0 2.4
Adiponitrile 0.3 0.5 5.8 2.2 143
.Styrene 5.6 6.1 6.1 5.9 4.2
Octamethylcyclotetrasiloxane 3.0 3.2 3.3 3.2 3.5
Ether 0.8 1.3
Ethyl acetate* 0.5 0.8
Methanonaphthalene* 0.2 0.3 0.3
Isooctane* 0.2 0.2
Methanol* 0.1 0.2
Page 30
Oi 890 FM RepotIJanuary 31,1996
Appendix DPage 2 of 37
Compound
HexaM
1 ,I-Dichloroethene’
Hexamethylcyclotetrasiloxane*
Benzene*
Concentration (mg/m3) Mean PrecisionConcentration
Sample 1 Sample 2 Sample 3(% RSD)
(first 10 minutes (mlddle 10 minutes (last 10 minutes of h4m3)
of exposure) of exposure) exposure)
0.1 < 0.1
0.1
0.1.
Wuantftatfon felath to toluene response only.
Page 31
.
01890 Final ReportJanuary 31,1996
Appendix DPage 3 of 37
TABLE D-2
CONCENTRATION DATA FOR EXPOSURE TO. PRIME URETHANE “A” TEST MIXTURE WITH BHT REMOVEDI
Precision(% RSD)
Compound Concentration (mg/m’)
piz-I (first 10 minutes
of exposure)
Mean
Sample 2(middle IO minutes
of exposure)
- - C o n c e n t r a t i o nSample 3
(last 10 minutes of I Wm3)
exposure) I
nd ndnd2,6-Di-tert-butyl-4-methylphenol
1.4.Dimethylpiperazine
nd
13.8
--
15.8 I- 16.3 16.819.2
10.08.6 I 9.710.5I, I, I-Trichloroethane 10.0
Adiponitrile nd 1320.2 1.1 0.4
6.7 6.5 ' 4.4~~
6.7Styrene I 6.2
4.6 I 4.44.3 3.4Octamethylcyclotetrasiloxane
Methanol*
4.4
4.5 3.1 1.9
0.30.2Pyrazine*
Ether*
0.1
3.5 I1.7 I
--I ,I-Dkhloroethene”
Isooctane* 0.6 I
Page 32
01890 Final ReportJanuary 3 1,1998
Appendix DPage 4 of 37
Concentration
Ethyl acetate*
Acetone*
Hexane*
Benzene*
Qmtitatfon telative to toluene response onty,
Page 33
61890 FM ReportJanuary 31,1996
Appendix DPage 5 of 37
TABLE D-3
CONCENTRATION DATA FOR EXPOSURE TOPRIME URETHANE “A” TEST MIXTURE
WITH BHT AND 1,4=DIMETHYLPIPERAZINE REMOVED
TTCompound Concentration (mglm’) MeanConcentration
hm3;
Precision(% RSD)I
Sample 1 Sampie 2 ISampie 3
(first 10 (IO-30 (30 - 50mlnutes of minutes of minutes ofexposure) exposure) exposure)
Sample 4(last 10
minutes ofexposure)
ndI
ndI
nd nd nd
nd I nd I nd nd nd
2.9 I 2.7 I 2.5 2.5 2.7 8.0I, 1, I-Trichloroethane
Adiponitrile 6.4 3.3 89
4.9 4.7 7.6Styrene
1.4 0.9 51Octamethylcyclotetrasiloxane
Page 34
l Aluo esuodsal euanloj 01 wq]ep~ uo!pq~uen~,
.
3tmxwu
Page 35
LE lo L efieda xlpu=W9643 ‘18 henuerIJJodW P”!j 068 IO
Page 36
‘Aluo esuodsal euenlol 01 eh!jepJ uo!)eqjueno),
1’0.kw!wwn
1’0 >,wepoosI
2’01’0.eUeJ!XO-(I~~~aWOJO~~~)
+auan~o~
1’0daY13
1’0+auouedoJd-7;-oJopp 1
(aJnsodxa(aJnsodxa 40(aJnsodxa JO
(,wW40 swnww 0~ w)swnw oc ~IPP!Wsw-ww oc IsJ!l)
c awesz NwesL wJuw(asI4 %IUO!)t?J)lJCXWO~
UO!S!SaJdueaM(pp3lu) uo!)eJ)uatxlo~punodtuoa
Page 37
*Aluo asuodw auanlol 01 eA!lelaJ uo!lellueng.,l sls@ue Gu!Jnp jsol eldwes ‘elqellehe IOU f ~13,
Z’PZ
LO
P’9
02
t’6
1’P
-
(astr %IUO!S!NJd
1’0+VNS’O;,aueJ~xo-(~~y~awoJo~~~)
8’SP’CC*VNS-6louedoJd-Z-oJol43!a-E’ 1
L’963+VN83auexo(!seJ~aloprt~l~l(lawepg
03 � l8’S*VNv-9ap!we)a~el~~law!a-N’N
S’E6%+VNL’Cap!wewJollAt(law!a-N’N-
L’LZ’W+VNS’ZIeLied~jb~Joi4~~ji-e-l~’ i
8’91WZ+VN6’ZZap!wel~~el~~law!a-N’N
IouaydlAqlawPuPU+VNPU-tt-iWwwa-9’z
(aJnsodxa(aJnsodxa 40(aJnsodxa lo
@J/w40 wnuw 0~ w)swnw 01 HIPPY)swww oc )sJ!l)
c Wuwsz alduwc a1duJesuo~pgua3uo~
ueafq(,uJ/6w) uo!)leJ)ua3uo~punodwo3
a3AOW3tllHa HlIM EklfUXIW IS31 rrav 3NVHEiUn 3WlUd013klnSOdX3 tlO=1 VlVCl NOIlVtllN33N03
9-a 3iavl
L(: lo 6 e6eda muadv966 L 36 hnuerY=h lwlj 06810
Page 38
.*&a osuodseJ euenlo~ 01 @A()eleJ uolle\!iuont),
*Z‘OI’0
0’16’09’04aualeqlydeuoueq)aw
8’9fiL’ZL’CL’ZL’LIouedoJd-z-oJoly~!a-~’ 1
2’1I303l’P. I3auexol!seJlalol~~~lAy)awe~~o
8’829’05’08’05’0ap!wela~el~Y~aw!a-N’N
L’LL’OL’O *8’0LOap!wewJollrtY)aw!a-N’N
L’O93939-v8’Paued~,ldolaiy3!jI-~‘t1 c
8’011’90’96’99’5ap!wejl(l3elrtylaw!a-N’N
louaqdlhqlawL’693C’PL’Z-wWq-w-!a-9’i!
(aJnsodxa(amsodxa 40(amsodxa 4040wnw 01 asei)wnu!w 01 ww)www 01 IsJ!I) @Jlw
uopJptaziuo=)c aldwesz a1duJesc~ld~es
(am 54)UO!S!WJdueaw(,Lu/~uI) uogequawo3punodwo3
3tlnixiw1~31 #‘a,, 3Nvkuun 3witld ~0iitlkii~33N03 ~07 oi 3tInsodx3 uo=I viva N0ii~i~33~03
pa 3iavi
Page 39
6’tP’Z
6’01C’8
5’65’CL
1’0 >
1’0
5’Z
6-L
L’l4
G’O >
1’0
Z’Z
0’6
L’l4
,auazuaqln)ng
.auwwNkz
Jayla IAuaqd!a
auale414deul~L(law!a-~’ 1
awwdeWww-z
S;‘L
9’9
671
6X9
1’8t7
(astl%)UOlS!WJd
6-W6’218X1auazuaql~y~awyl=tr’Z‘ 1
O’OiL’81.6 ’eue3apuf-j
1’18’00’1auanlol
6’1O’G5’0ap!we~a~el~4~aw!a-N1N
5’0z-0COap!wewJol(~~law!a-N’N
(aJnsodxa(aJnsodxa 10(aJnsodxa JO40swwwocwi)swww01ww)wnww01FJ!l)
E Nwesz aldwes1 aldww
(,u~~6tu) uo!gequamo3punodwo3
3kHUXIW lS3l~3aaI-klEl9NOdS013tinSOdX3 24Oj VlVQ NOllV~lN33N03
8-a 3iavl
Page 40
Cl3AOW3kl3N31VHlHdVNlAH13W-Z HlIM 3~nlXIW IS31U3aafkl39NOdS 0133tinSOdX3 UOj VlVCl NOllV~lN33N03
6-a 3iaVl
LE Jo ZC eeeda w=Jdv
-9661 ‘re ken-rwW wld 068CO
Page 41
‘r(luo eeuodw euetqo~ 01 eh(jepr uollel!pten0,
0’61I
(as24 96)UO!S!WJd
~,wWuo!qwpJa3uo3
ueayy
Z’OIC'OI .1'0I
Pu -IIaual~4~Ydeul~lllaw!(7-t)’ 1
PuIPuIPuI
6’11IauazuaqlAy)aw!Jl-tT’Z’ 1
aue3apun
6’0 :auanlol
Iap!wela~el~4law!a-N’N
Iap!wewJollrtylaw!a-N’N
(amsodxa40 wnu!w 01 asei)
c QldWQ
(amsodxa 80wnw oc aw)
1 aldwes
&/SW) uo!)eJ)ua=luo=)punodwo3
Cl3AOW3U 3N31VHlHdVNlAH13Wla-P’C ClNV3N31VHlHdVNlAH13W-Z HlIM 33tlnlXIW lS31 kl3aafPl39NOdS
013tlfEOdX3 t;1Ozl VlVCl NOllVUlN33N03 AtiVWWfE
0 c-a 3iaVl
LE P EC efieda xrpueddv966 c ’ CE kenuerWhl Wld 068 LO
Page 42
bApo esUoctseJ auehlol 01 ehllepl uo~~e~!~Uon~,
(If) 0% . Cc3tlnlXlW IS31 ti388ntl39NOd~NOllVkUN3jNd3 MO1 013UnSOdX3 kJOrl VlVCl NOllV~lN33N03
cc-a 3iavl
~ww6eda wuaddv966 c ’ CE henuerWJ@fW!H68CO
Page 43
1’0L’O 7
too 71’0 71’01’0 7.auaWoMW3-2
S’OVP’OS’OP’O5’02’0JSl#0 IAual(d!a
P’fiPVlL’11’1O’ZLO *eualeq1~deulA~~aw!a-f 1
Z'P56’LP’ZZ’LL’E6’0~wwdeWwaw-7;
G’6L9’5L’5S’ttZ’L0’5auazuaqlAtjlawyL+z c
8’LC1VEIL’C19’21L’ttVZeue9apun
L'ZttE’OE’OI’05.0z.0‘auanlol
9l4CO5’0Pu5’0Puap!we)a~elA~~aw!a-N’N
ozcC’OL’OPuZ’OPuap!wewJo~l~~~aw!a-N’N
(aJnsodxa(aJnsodxa(aJnsodxa(aJnsodxa10 saanu!w40 saanu!w40 sapqw40 sqnu!w
(pmu01 aselIOS - oc)oc - 01)0 1 VJ!l)PI aidweE Nwesz aIdwec Nwes
(aski %Iuo!gwp4acWo3UO!S!WJdueaw(p/Gu~) uo!qeJquamo3punodwo3
(aL324nlxiw ‘y,t13MOl Oi 3tInSOdX3 kJO=I VlVCl NOllWlN333N03
zc-a 3iaVl
Page 44
‘Ap.to esuodm euenlot ol enflelal uoilel!yen&
1'0 7
1'0 7
(as24 56)UO!S!aaJd
@J/wuogwqua3uo3
ueaw
(aJnsodxaJO saanu!w
01 WI)v aldwes
I'0 7
(aJnsodxa(aJnsodxa40 saanu!wJO siqnujw
OS - oc)oc - 01)c +JJesz aldwes
(,w/6tu) uogeJquaauo=)
(aJnsodxa40 salnqw
01 PJ!4)c aidwes
+auazuag
,auepooq
.wwWww-t7-ibww~-!a-9’z
punodwoa
LE P 9 c e6eda xlpuddv966 c ' LE kmugrwfw wtd 068 10
.
Page 45
‘&o e9UOdSeJ elMlO) 01 OAllelaJ UOlp!)!~UtJh~~
Z’8EI’0~_~ ~~
IE'O - 1 E'O 1 1'0 1Jayja IAuaqd!a
PO1
8’99
1’11’0LOL’Z6’0aualeY1Ydeul~ylaw!a-tr’ 1
O’LZ’O0’18’11’1~uww@wQww-z
82Z’BI6’2IE’SI6’6I5’CIaUazuaqlAYlaw!Jl-tr’z’ 1
8’1ILO -1-- L’Z 1 Z’Z 1 Z’Z 1auempun
0’86
9’62
L’lL
1’0
S’O
8’0
1’0
LO
6’0
1’0
5’0
6’0
1’0 ’ z-0 ’
9’0P’O
L’OLO
(ask4 54)lJo!S!3Wd
Qm)uoI)wpamo3
uealry
(amsodxa(amsodxa(amsodxa(amsodxaJO sapmywJO sa)nu!w40 sap.qw40 saJnu!w
01 tsel)09 * oc)06 - 01)oc as441P aldwesc Mwesz dwes1 qdwes
(,w/fiw) uo!)equaauo3IIjunodwos
(3) 3unixiw TT‘.IS31 243aanU 39NOd~fi6ikhJ~~NO~-lS!lMOl-Ol3tfnSOdX3 80=1 VlVCl NOllWlN33N03
LE lo L 1 efleda xlr=ddv966b’t~ kmuerWht @‘Jlj 06810
Page 46
1’19
82
Z’CL
632
6’91
rst,
E’PC
(as24 54)UO!S!WJd
O’G
6’6
83
vi
0%
9’1
6'9
(p/Wuoy/w*uamo3
ueaw
P’ZL’Z1’6.aualeqlydeuoueqlayy
L’L8’09’08lXL
S-65’86’6ap!we)a~el~y~aw!a-N’N
6’18’1S’Laumaa
E’89’8Z’S ’aua3apyl
OILS;‘SL1;‘ZLaua3apun
Z’Z8’18’0ai!Jl!uod!Pv
louaqdlAqlaw82c-9L'C-tdMww!a=9'z
(ansodxa(amsodxa40(amsodxa4040 saanw 0~ asellsww oc ~~PPWsaanw 01 w!4)
c aldwwz aldwes1 aIdwe
(,w/6w) uolqequaauo3punodwo3
3mlxiw is31 3NvHl3tln a3aNoa013WlSOdX3 HO=I VlVa NOllVkflN33N03
Page 47
1'0.eue!pe)deH-9’ 1-a
L’O,wwe IN13
1’01’01’0.euhapoa-l
1’01’0C’O.aua!pexeL(-p’C-I~ll)ew!a-E’z
9’CCZ’P9’ZZ’SL’V81X1
031E-89'8P'66'9ep!we~e3ejAy)eur!~-N’N
L'81'2C'ZC'Z6'1eue3ea
L’S6 18'8L1Z'EZ6'LZZ'lleueaepyl
6'8E'OZ8'OZ -6'lZE-81wesepu,?\
L’PSE’Z8'00%6-Zei!Jt!uod!pv
IoueqdlAqlaw-PuPuPuPu-i4wwwa-9'z
(amsodxa(amsodxa 40(amsodxa 10
&VW40 svww 01 asel)swnw oc wP!W=wuw 01 w4)
(osu 54)c Ww. t aWes1 aldwtis
uo~)eJ)uaaJo~UO!Sl,CWJdut2aN(,uqSw) UO!)t?J)UZIUO=)punodwoa
Page 48
%luo esuodsal euanloj 01 eh!jepJ uo!jej!pn~,
(amsodxa(amsodxa 40(amsodxa 40
40 wnw ol aset)saanuw 0L ww)saanw 01 as441c WuwE WwesL WJJes
(,w/ljt.u) UO!)EJ)UXWO~punodwoa
Page 49
rn 5 9 * - P a - - - - -
2 E - 2 - .o a - 0 0 - P cd - l N - iti L
Page 51
-E’O1’0 >1’0,euexol!s~J~e)op~~lA~~ewe~~o
:.euexeyop~~(lrCuey~el~~~~w
2’02’01’01’0- lbl~uW3-E
L’S8’91’LO’L021’9eue3epun
9’PC63’E’9S’S6-t’6%louexeyopA3
-PuPuPuPuPuloueaapoa
1’1L’ZL’ZL’ZL’Z9-zeuezuaql/tdoJd
002 .2’1Pu8-PPuPuppt3 a!)e=>v~~-~ -- ~
8’91'2O'ZZ'Z ' * Z'Z6’1euel3oosl-
9’2LO1 -P’OC1’118‘069’0 1’WX!!O~
0’1C’9Z’9c-96’9z-9eueJ&
1%P'Z6’ZS’ZE’ZE’ZHC)A-DI
O’CZ0’8Z’6L’8L’8Z’SHad-V
(amsodxa(amsodxa(amsodxa(amsodxaJO saanuy40 saanuy40 sa~nupu40 sajnuy
(p/W. oc a=0OS; - 0s)oc - 01)01 aw)0 ~lduwE alduwt a1du-w1 alduw
Iastr %Iuopl~ua3uo~UO!SlNJdueaw(,wjfiur) uoge.quaauol)punodluo=) ’
Page 52
*AILJO asuodsu euan(o~ 01 eylepJ uo!legjuen&
IIII(amsodxa(amsodxa(aJnsodxae (aJnsodxa
(asu 74)UO!s!a;ud
(,wfwuo!)eJ~ua3uo~
ueaW
40 saanuyu01 asei)
0‘ widow
40 sapw!w40 saanu!urOS - oc)oc - 00
c alduwz a1duJes
(cw/6~) uo!gequacwo=)
40 saqnupuoc as44)
1 a1duJes
punodwo3
Page 53
I2'0I2'0I2'0Ipwwqnss.9I+VNIO’LIZ’9Iz-9Ieue3epun
1’EZ
SOL
1’9
Z’V
+VN
h/N
, II%
9’Zl
0’9
Pu
louexatjol3A3
louema
Z’Cl8’2III
I+VNIl’ZI9’2L’ZeuezuaqlhdoJd
EL12’0I+VNIPuIS’OIPuIppe 3ge3V~ ~ - ~~
L’ZZI63I+VNItr’lIO’ZI1’2Ieuel3oosl
8’91
L’91
Z-6 -
9’9
AfN
AfN
I
Ieuenjol
eueJA)S
Z’lZI1’2IwVNI9’1ICZIP’ZIHDA-P
8’PL
(as84 %IUo~s!CKBJd
C’8IAfINI6’8IZ’6I6’9IH3d-P
@J/wuo~)eJ)ua%Jo~
ueaw
I(amsodxa(amsodxa(amsodxa(amsodxa~0 saanu!w40 saanuy.u40 saanu!t.uJO saanqw
01 a=0OS - oc)oc-01)01 )SJ!l)P aWesc Mwesz aldu=S1 wduw
(,w/Sur) UO!)tZJ~Ui33UO~punodwo3
Page 54
*Aluo esuodsu euan~o~ 0~ eh!jelu uo!leglueno , ,qsheue Gupnp isol eldures ‘elqel!eAe IOU + VN,
(aski %IUO!S!WJd
@J/wuo!)eJ)lJaaJo~
ueaw
(amsodxa(amsodxaJO saanu!w40 saanuyu
oc asei)OS - oc)v 3lduwc aidwes
(amsodxa40 sa~nu!w
OE - 01)z Wwes
(amsodxa40 salnu!w
oc asm)L W-w
(,w/6w) uo!Jequamo3punodwo3
LE JO 82 e6eda xlpddv866 c ’ re hnuerWNJ lwd 068to
Page 56
*Aluo esuodsu euenlo) 0) e~lpp~ uo!ltqluen0,
(astl %IUO!S!WJd
@J/wuo!)w)ua3uo~
ueaw
1’0
(msodxa40 sa8ny.u
9 01 Mum WI)
1’01’0 >
2’0
1’01’0
(ansodxa(amsodxaJO sapwpu40 sapwpu
-6 OS mw3 0s)
oc - oc)2 wwes
(,uI/~uJ) uoi~eqmmo3 .
~eue~=>ooq
1’0,euqey)qdeuoueqla~
*JW3
E’O.auexol!se)uadol~~~l~~~~~e~~a
1’0$ueldaH
(amsodxa40 sa~nupu
01 W!4)c a1duJes
punodwo3
Page 58
*Aluo asuodsa, auanlol 01 a/gelaJ uo!ltq!yen~,,3ads ssew Jo a6ueJ Jeau!l Jo eplqno alaM punodwo:, slqj JOJ elep ‘pajeuqlsa uol\eJluawog,
m1’01’01’01’0..~U~XWWW-~
1’01’01’01’0,,~u~x~www-z
1’01’01’01’0~+~u~ad4-i
1’0 >1’0 >..~u~wuml-z
(amsodxa(amsodxa(amsodxa(amsodxa40 sa~nupu40 saqwpu40 sapwpu40 saanupu
Qv6~)01 WI)OS - oc)OE - 01)0 I W!4)
0 alduw(aski %I
c aldue2 aldumc alduwuo!)wquamo3
UO!S!ZlaJdueayll(,U@U) UO!~E?J~UXNlO~punodwo3
Page 60
‘&JO esuodsal euan[o~ 01 eh!telaJ uo(lepluen&
2’0,euempun
2’02’0V’O,we13oosl
1’0,leu==wwl-z
II1co i1P’O 1.JWEl
1’0 >1’0 >1’0+J~lj)~OJO(lj3!J~- 1’ 1’ 1
1’0 >+ue.mjozuaq!a
1’0 >1’0 >1’0 >1’0 >.~u~wvi~ww
1’0 >*auazuag
1’0.w=e 1h13
1’01’01’0+autmapun-s
1’0 >1’0 >1’0 >I’0 >,auhapun-l
(amsodxa(amsodxa(amsodxa(amsodxa40 sa~nuyJO sapwpu40 saqnqtu40 saanupu
&J/wOb WI)OS - 0s)oc - 00oc as441
v Mwes(astt %I
& a1duJes2 a1duJesI. Wuesuo!qequa=ruo3
UO!S!SaJdueaw&/6tu) uogequamo3punodwo3
Page 61
6’2
2’8
P’S
9’01
9tt
8’19
t’s-
(as24 56)UO!S!WJd
1'0
’ E’tt
9’81
6%
8’1
LO
Cl
0’2
Pu
(emsodxe40 salnupi
01 WI)0 ~ldum
9’06’0
C’O >G’O >
O'PZ’t,
8’09’8C
8X8%
9’1L’L
L’OPu
O’G0’1
9’101’1
PuPu
(amsodxe(msodxa40 se)nu!ur40 saanupu
OS - oc)oc - 01)c a1du-w2 elduw
(,w/Stu) uogequawog
zz-a 331avi
Page 62
l Aluo WJ0dSaJ euanloj 01 ehllepl uoljel!jueng,
,,euepoosl
2’11’1.eU~~~~-~OJOh~OUOwoJOly~!J~
VI@9’1*Jaw
1’01’0,auey)eoJoppp~-& ’ 1’ 1
2�01�01’0 >,ueJn~ozuaq!a
2�0P�OWWWD
9�0S'O.www uoqw
1'01'0&lazuag
(amsodxa(amsodxa(amsodxa(amsodxa40 sqnuy40 saanu!ur40 sa~nuyu40 sa~nqu.4
(pm01 WI)OS - oc)oc-01)01 W!4)
(aski 9-k)P a1duJesc w☺wes2 a1duJes1 alduw
uo!gequatwo3UO!S!3,aJdueayy(,w/6u() uo!ge.quaauof)punoduroa
LC JO w efieda xlm=W866 c ’ ts henuerW&l l=J!j 068 LO
Page 63
(amsodxa(amsodxa(amsodxa(amsodxa40 saanu!w40 sqnupu40 sqnuy40 saanu!w
(pww01 WI)OS - oc)oc - Ol)oc as441
o Mu-wE aldwesz wduwc aldwes(astr %Iuo!~wjua3uo3
UO!S!zWJduealry(,w~Stu) uo!gequamo3punodwo3
Page 64
CO
1’0
G’O
C’O
L’O
P’L
*-1’0l QulloydJoW
,euexeyol~r(~-(euep~I~~~~l~~~~w1’0-lh44laW-l
6X,au!loqdJowlrtlnqosl-b
VO,louelQO-1
.euampoa-l
1’0P’O1’2,eueydwe=)
PuPuPueu!weuey)e eu!loydJoyy-b
it48 HLIM 3unixiw is31 *‘a,, w3isAs iNividw03 oi3unsodx3 tio~ viva NOii~ti~~333~03
LE JO 9~ eseda xlpu=W866c ‘cc hnuermc&i mu omo
Page 65
,
*Aluo esuodsal euanloj 01 ah(lelaJ uollepyeng,
(aski 73UO!S!3aJd
&VWuogwJua3uo3
ueaw
(arnsodxa40 sa)nu!w
oc WI)P alduw
KO
P’O
1’0
1’0 >
(amsodxa(amsodxa40 sc3any.u40 sainugu
OS - oc)oc-01)c aldwesz alduw
(,w/~uJ) uo!ge.quamo3
1’0
(amsodxa40 sa)nu!w
0L as441c aldwes