Chromatograms

GC CHROMATOGRAMS

GC Chromatograms by Column Phase Index . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .543-544

EPA Method Chart . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .544

Environmental . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .545-610Air, Brominated Flame Retardants, Chlorinated Disinfection Byproducts, Diesel Range Organics (DRO), Dioxins, Endocrine Disruptors, Explosives,Gasoline Range Organics (GRO), Glycols, Haloacetic Acids, Herbicides,

Organo Tins, PCB Mixtures, Pesticides, Semivolatiles, Volatiles

Foods, Flavors & Fragrances . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .611-641Antioxidants/Preservatives, Chiral Separations, Cholesterols, Essential Oils, FAMEs, Fatty Acids, Flavors, Food Contaminants, Food Testing, Fragrances, Sterols, Sugars, Triglycerides

Personal Care & Cleaning Products . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .642-643Cleaning Solvents

Petroleum & Petrochemicals . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .644-664Chlorofluorocarbon Gases, Fuels, Hydrocarbon Gases, Hydrocarbons, Hydrocarbons (Simulated Distillation), Hydrocarbons (High-Temperature), Permanent Gases, Sulfur Compounds

Clinical, Forensic & Toxicology . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .665-674Abused Inhalants, Alkyl Nitrates, Anesthetics, Arson Accelerants, Blood Alcohols, Cannabinoids, Cocaine, GHB/GBL, Glycols, Opiates, Solvents

Forensic/Pharmaceutical . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .675-683Acidic/Neutral Drugs, Barbiturates, Basic Drugs, Benzodiazepines, Cold Medications, Phenothiazines, Sympathomimetic Amines

Pharmaceutical . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .684-700Anesthetics, Antiepileptics, Basic Drugs, Chiral Analyses, Organic Volatile Impurities/Residual Solvents, Pesticides in Dietary Supplements, PGIs, Steroids

Solvents & Chemicals . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .701-707Alcohols, Aldehydes, Amines, Chlorides, Chlorofluorocarbons, Cresylic Acids, Ketones, Nitrosamines, Phenols, Solvents

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GC CHROMATOGRAMS

GC Chromatograms by Column Phase

Capillary ColumnsFAMEWAX

FAMEs . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .70, 620, 622MXT®-1 Sim Dist

hydrocarbons (high temp.) . . . . . . . . . . . . . . . . . . . .660MXT®-1HT Sim Dist

hydrocarbons (high temp.) . . . . . . . . . .78, 79, 658, 659MXT®-5

phenols . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .553MXT®-500 Sim Dist

hydrocarbons (high temp.) . . . . . . . . . . . . . . . . . . . .660MXT®-Biodiesel TG

biodiesel oils . . . . . . . . . . . . . . . . . . . . . . . . .81, 644, 645Rt®-2330

dioxins (TCDDs) . . . . . . . . . . . . . . . . . . . . . . . . . . . . .591FAMEs . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .621sugars . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .640Rt®-2560

FAMEs . . . . . . . . . . . . . . . . . . . . . . . . . .57, 69, 617 - 619Rt®-βDEXcst

flavors, fragrances . . . . . . . . . . . . . . . . . . . . . . . . . . . .613pharmaceuticals . . . . . . . . . . . . . . . . . . . . . . . . . .686, 687Rt®-βDEXsa

flavors, fragrances . . . . . . . . . . . . . . . . . . . . . . . .612, 613Rt®-βDEXse

fruit juices . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .614Rt®-βDEXsm

flavors, fragrances . . . . . . . . . . . . . . . . . . . . . . . . . . . .612pharmaceuticals . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .687Rt®-γDEXsa

fruit juices . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .614Rt®-TCEP

aromatics . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .655oxygenates . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .80Rtx®-1

air (Mass APH) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .610air (TO-14/TO-15 compounds) . . . .409, 606, 608, 609chlorofluorocarbons . . . . . . . . . . . . . . . . . . . . . . . . . .707essential oils . . . . . . . . . . . . . . . . . . . . . . . . . . . . .626, 627fatty acids (free) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .615flavor volatiles . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .628fragrances . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .641hydrocarbons . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .658hydrocarbons (gases) . . . . . . . . . . . . . . . . . . . . . . . . .650ozone precursors . . . . . . . . . . . . . . . . . . . . . . . . . . . . .606simulated distillation . . . . . . . . . . . . . . . . . . . . . . . . .661sulfur compounds . . . . . . . . . . . . . . . . . . . . . . . . . . . .664Rtx®-5

chlorinated disinfection byproducts . . . . . . . . . . . . .589chlorophenoxyacid herbicides . . . . . . . . . . . . . . . . . .580diesel range organics (DRO) . . . . . . . . . . . . . . . . . . .600drugs of abuse . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .673endocrine disruptors . . . . . . . . . . . . . . . . . . . . . . . . . .592essential oils . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .625gasoline range organics (GRO) . . . . . . . . .596, 597, 599haloacetic acids . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .603pharmaceuticals (basic) . . . . . . . . . . . . . . .677, 681, 682phenols . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .553steroids . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .687sterol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .623sympathomimetic amines . . . . . . . . . . . . . . . . . . . . .677Rtx®-5 Amine

amines . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .64, 703, 704amines, phenols . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .705cold medications . . . . . . . . . . . . . . . . . . . . . . . . . . . . .683pharmaceuticals (basic) . . . . . . . . . . . . . . .676, 683, 691sympathomimetic amines . . . . . . . . . . . . . . . . . . . . .676Rtx®-5MS

endocrine disruptors . . . . . . . . . . . . . . . . . . . . . . . . . .592food contaminants . . . . . . . . . . . . . . . . . . . . . . . . . . .638volatiles (food packaging) . . . . . . . . . . . . . . . . .633, 634

Rtx®-5Sil MS

phenols . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .560polycyclic aromatic hydrocarbons . . . . . . . . . . . . . . .555semivolatiles . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .560Rtx®-20

antiepileptics . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .692antioxidants . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .611Rtx®-35

barbiturates . . . . . . . . . . . . . . . . . . . . . . . . . . . . .678, 679endocrine disruptors . . . . . . . . . . . . . . . . . . . . . . . . . .592nitrogen herbicides . . . . . . . . . . . . . . . . . . . . . . . . . . .581organo tins . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .593pharmaceuticals (acidic, neutral) . . . . . . . . . . .678, 679pharmaceuticals (basic) . . . . . . . . . . . . . . . . . . . . . . .681Rtx®-35 Amine

amines . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .704cold medications . . . . . . . . . . . . . . . . . . . . . . . . . . . . .683pharmaceuticals (basic) . . . . . . . . . . . . . . . .65, 675, 683sympathomimetic amines . . . . . . . . . . . . . . . . . . . . .675Rtx®-50

antioxidants . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .611triazine herbicides . . . . . . . . . . . . . . . . . . . . . . . . . . . .581Rtx®-65TG

food testing . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .623triglycerides . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .72, 624Rtx®-200

benzodiazepines . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .682chlorinated disinfection byproducts . . . . . . . . . . . . .589chlorofluorocarbons . . . . . . . . . . . . . . . . . . . . . . . . . .707dietary supplements . . . . . . . . . . . . . . . . . . . . . . . . . .685explosives . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .593fatty acids (free) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .615glycols . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .601haloacetic acids . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .603pharmaceuticals (basic) . . . . . . . . . . . . . . .676, 680, 682phenols . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .553potential genotoxic impurities . . . . . . . . . . . . . . . . . .690solvents (organic volatile impurities) . . . . . . . . . . . .699sympathomimetic amines . . . . . . . . . . . . . . . . . . . . .676triazine herbicides . . . . . . . . . . . . . . . . . . . . . . . . . . . .581Rtx®-225

sugars . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .640Rtx®-440

cocaine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .672organochlorine pesticides . . . . . . . . . . . . . . . . . . . . . . .53Rtx®-502.2

air toxins . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .607gasoline range organics (GRO) . . . . . . . . . . . . .595, 597Rtx®-1301

chlorinated disinfection byproducts . . . . . . . . . . . . .590flavor volatiles . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .630solvents (organic volatile impurities) . . . . . . . . . . . .700Rtx®-1614

brominated flame retardants . . . . . . . . . . . . . . . .92, 588Rtx®-1701

antiepileptics . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .692barbiturates . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .678fragrances . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .641pharmaceuticals (basic) . . . . . . . . . . . . . . . . . . . . . . .691Rtx®-2887

simulated distillation . . . . . . . . . . . . . . . . . . . . . .77, 660Rtx®-BAC1/Rtx®-BAC2

alkyl nitrates . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .671anesthetics . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .671blood alcohol . . . . . . . . . . . . . . . . . . . . . . . . . . . . .82, 667butyrolactone, butanediol . . . . . . . . . . . . . . . . . . . . .669GHB, GBL . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .669glycols . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .602, 668inhalants (abused) . . . . . . . . . . . . . . . . . . . . . . . . . . . .670solvents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .672

Rtx®-Biodiesel TG

biodiesel oils . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .644Rtx®-CLPesticides/Rtx®-CLPesticides2

dibromoethane (EDB), dibromochloropropane(DBCP) . . . . . . . . . . . . . . . . . . . . . . . . . . . . .684 - 695

haloacetic acids . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .604herbicides . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .579nitrogen, phosphorus pesticides & herbicides . . . . .578organochlorine pesticides . . . . . . . . . . . . . . .89, 569, 570organophosphorus pesticides . . . . . . . . . . . . . .575 - 577PCBs . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .584, 585pesticides & herbicides . . . . . . . . . . . . . . . . . . . .571, 572Rtx®-DHA

hydrocarbons (detailed gasoline analysis) . . . . .75, 657Rtx®-Dioxin2

TCDD . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .96TCDF . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .96Rtx®-G27/Rtx®-G43

solvents (organic volatile impurities) . . . . . . . . .85, 700Rtx®-OPPesticides/Rtx®-OPPesticides2

organophosphorus pesticides . . . . . . . . . . .91, 573, 574triazine herbicides . . . . . . . . . . . . . . . . . . . . . . . . . . . .582Rtx®-PCB

PCBs . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .93, 586, 587Rtx®-TNT/Rtx®-TNT2

explosives . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .594Rtx®-VMS

solvents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .642, 643volatiles . . . . . . . . . . . . . . . . . . . . . . . .100, 467, 548 - 551Rtx®-Volatile Amines

amines . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .63Rtx®-VRX

volatiles . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .101Rtx®-WAX

FAMEs . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .619, 621glycols . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .601solvents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .58, 642solvents (organic volatile impurities) . . . . . . . . . . . .699Rtx®-XLB

PCBs . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .583semivolatiles . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .567Rxi®-1ms

diesel, motor oil . . . . . . . . . . . . . . . . . . . . . . . . . .598, 666fragrance allergens . . . . . . . . . . . . . . . . . . . . . . . . . . . . .61hydrocarbons (accelerants) . . . . . . . . . . . . . . . .665, 666microbial volatile organic compounds . . . . . . . . . . .605pesticides (Minnesota Ag List) . . . . . . . . . . . . . . . . . .497petroleum hydrocarbons . . . . . . . . . . . . . . . . . . . . . .598phthalate & adipate esters . . . . . . . . . . . . . . . . . . . . . .554steroids (sex hormones) . . . . . . . . . . . . . . . . . . . . . . .688sulfur compounds . . . . . . . . . . . . . . . . . . . . . . . . . . . .664Rxi®-5HT

bleed profile . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .47diesel . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .663gasoline range organics (GRO) . . . . . . . . . . . . . . . . .663hydrocarbons (accelerants) . . . . . . . . . . . . . . . . . . . .663hydrocarbons (crude oil) . . . . . . . . . . . . . . . . . .663, 664mineral oil & motor oil . . . . . . . . . . . . . . . . . . . . . . .663Rxi®-5ms

bleed profile . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .39cholesterols . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .625drugs (acidic, neutral) . . . . . . . . . . . . . . . . . . . . . . . . .679drugs (basic) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .680GBL . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .668local anesthetics . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .691pesticides (organochlorine & organophosphorus) .635polycyclic aromatic hydrocarbons . . . . . . . . . . . . . . .559pyridine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .38semivolatiles . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .568test mixes . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .39

GC Chromatograms by Column Phase (Alphabetical Order)


544 www.restek.com 800-356-1688 or 814-353-1300

GC CHROMATOGRAMS

GC Chromatograms by Column Phase, EPA Methods Chart

Rxi®-5Sil MS

amphetamines . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .675benzodiazepines . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .682cannabinoids . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .674cocaine & metabolites . . . . . . . . . . . . . . . . . . . . . . . . .673dietary supplements . . . . . . . . . . . . . . . . . . . . . .684, 685dioxins & furans . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .95opiates, extracted from blood . . . . . . . . . . . . . . . . . .674organochlorine pesticides . . . . . . . . . . . . . . . . . . . . . .639polycyclic aromatic hydrocarbons . . . .97, 555, 556, 636semivolatile organics . . . . . . . . . . . . . . .43, 87, 561 - 566sympathomimetic amines . . . . . . . . . . . . . . . . . . . . .675Rxi®-17

fragrance allergens . . . . . . . . . . . . . . . . . . . . . . . . . . . . .61Rxi®-17Sil MS

benzofluoranthenes . . . . . . . . . . . . . . . . . . . . . . . . . . .558polycyclic aromatic

hydrocarbons . . . . . . . .45, 73, 98, 557, 558, 637, 638Rxi®-624Sil MS

basic compounds . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .46potential genotoxic impurities (PGIs) . . . . . . .689, 690residual solvents . . . . . . . . . . . . . . . . . . . . . .83, 694, 695volatile organics . . . . . . . . . . . . . . . . . . . . . . . . . .103, 547Stabilwax®

acrylamide . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .639amines, alcohols, chlorides . . . . . . . . . . . . . . . . . . . . .706essential oils . . . . . . . . . . . . . . . . . . . . . . . . . . . . .626, 627FAMEs . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .59, 621, 646flavor volatiles . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .628glycols . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .602residual solvents . . . . . . . . . . . . . . . . . . . . . .84, 697, 698Stabilwax®-DA

cresylic acids . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .707fatty acids (free) . . . . . . . . . . . . . . . . . . . . . . . . .615, 616flavor volatiles . . . . . . . . . . . . . . . . . . . . . . . .67, 629, 631Stabilwax®-DB

amines . . . . . . . . . . . . . . . . . . . . . . . . . . . . .66, 704 - 706

Packed/Micropacked ColumnsCarboBlack B

blood alcohol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .667flavor volatiles . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .630D3606 Application Column

gasoline . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .128, 656HayeSep® Q

solvents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7025% Krytox®/CarboBlack B

chlorofluorocarbons . . . . . . . . . . . . . . . . . . . . . . . . . .706Molesieve 5A

permanent gases . . . . . . . . . . . . . . . . . . . . . . . . . . . . .647Molesieve 13X

permanent gases . . . . . . . . . . . . . . . . . . . . . . . . . . . . .647Refinery Gas Column Set

hydrocarbon gases . . . . . . . . . . . . . . . . . . . . . . . . . . . .129Res-Sil® C Packing

OPN . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .129n-Octane . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .129Rt®-1200/Bentone® 34

aromatics (BTEX) . . . . . . . . . . . . . . . . . . . . . . . . . . . .655Rt®-XLSulfur

sulfur compounds . . . . . . . . . . . . . . . . . . . . . . . .131, 664sulfurs in beverages . . . . . . . . . . . . . . . . . . . . . . . . . . .632Rtx®-1 on Chromosorb® WAW

hydrocarbons (motor oil, aviation gas) . . . . . . . . . .656Rtx®-1 SimDist 2887

simulated distillation . . . . . . . . . . . . . . . . . . . . .661, 662ShinCarbon ST

chlorofluorocarbons . . . . . . . . . . . . . . . . . . . . . . . . . .649hydrocarbon gases . . . . . . . . . . . . . . . . . . . . . . . .647, 652permanent gases . . . . . . . . . . . . . . . . . . . . . . . . .130, 64710% TCEP

aromatics, aliphatics . . . . . . . . . . . . . . . . . . . . . . . . . .65420% TCEP

hydrocarbons (motor oil, aviation gas) . . . . . . . . . .656

PLOT ColumnsRt®-Alumina BOND/CFC

chlorinated fluorocarbons . . . . . . . . . . . . . . . . . . . . . .74Rt®-Alumina BOND/KCl

hydrocarbon gases . . . . . . . . . . . . . . . . . . . .650, 651, 653Rt®-Alumina BOND/Na2SO4

hydrocarbon gases . . . . . . . . . . . . . . . . . . . .649, 652, 653natural gas . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .651Rt®-Msieve 5A PLOT

permanent gases . . . . . . . . . . . . . . . . . . . . . . . . .109, 648Rt®-Q-BOND

solvents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .111, 701Rt®-QS-BOND

hydrocarbon gases . . . . . . . . . . . . . . . . . . . . . . . .652, 654ketones . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .703solvents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .702Rt®-S-BOND

solvents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .701Rt®-U-BOND

aldehydes . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .703

GC Chromatograms by Column Phase (cont'd)

EPA Methods Chart

GC & HPLC Chromatograms

Compound Indexstarting on page 752

Method # Method Title ................................................................Page #

502.2 Volatile Organic Compounds ..................................................595504.1 1,2-dibromoethane & 1,2-dibromo-3-chloropropane ............552

505 Organohalide Pesticides & PCBs ..............................................571506 Semivolatile Organics................................................................554

508.1 Chlorinated Pesticides ..............................................................572524.2 Volatile Organics ......................................................................551525.2 Semivolatile Organics................................................................568

526 Semivolatile Organics (screening)............................................560528 Phenols ......................................................................................560

551.1 Chlorinated Disinfection Byproducts ..............................589, 590552.2 Haloacetic Acids ................................................................603, 604

604 Phenols ......................................................................................553610 Polycyclic Aromatic Hydrocarbons ..................................555-559615 Chlorophenoxyacid Herbicides ................................................580619 Nitrogen/Phosphorus Herbicides & Pesticides ..............578, 581624 Purgeable Halocarbons ............................................................467

1613 Dioxins..................................................................................................5911614 Brominated Flame Retardants ..........................................................5888021 Volatile Organics ......................................................................1018081 Chlorinated Pesticides ....................................................53, 569, 5708082 PCBs..............................................................................................584-5878095 Explosives ..................................................................................5948100 Polycyclic Aromatic Hydrocarbons ..........................................557

8140/8141/ 8141A Organophosphorus Pesticides ..........................................573-5758151A Chlorophenoxyacid Herbicides ................................................579

8260 Volatile Organics ................................................................547-5508270 Semivolatile Organics ........................................................561-567

8270 Appendix IX Semivolatile Organics ........................................................................566TO-14 ................................................................................606, 608TO-15 ................................................................................608, 609

Looking for more?Visit our online technical library for

chromatograms based on ASTM methods, USP procedures,

and other applications.

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GC CHROMATOGRAMS | ENVIRONMENTAL

Volatiles

Volatile Organic Compounds Retention Time Index: Rtx®-VMSData collected using a 60m, 0.25mm ID, 1.4µm Rtx®-VMS column; Oven: 40°C (hold 6 min.) to 230°C @ 14°C/min. (hold 11 min.); Carrier gas: helium; Regulation: constant pressure; Flow rate: 1mL/min.; Linear velocity: 21cm/sec.; Dead time: 4.90 min.

RRttxx®®--VVMMSSCCoommppoouunndd RReett.. TTiimmeedichlorodifluoromethane 5.52chloromethane 6.26vinyl chloride 6.54water 6.70bromomethane 7.61methanol 7.932-methylbutane 7.96chloroethane 8.00trichlorofluoromethane 8.41n-pentane 8.61diethylether 9.591,1-dichloroethene 9.64carbon disulfide 9.65Freon® 113 9.70ethanol 9.74iodomethane 9.993-chlorotrifluoropropane 10.45chloro-methyl-methylether 10.54acrolein 10.572-methylpentane 10.59allyl chloride 10.72methylene chloride 10.983-methylpentane 11.09acetone 11.24trans-1,2-dichloroethene 11.24methyl tert-butyl ether 11.422-propanol 11.52tert-butyl alcohol 11.56methyl acetate 11.63hexane 11.64acetonitrile 12.22chloroprene 12.301,1-dichloroethane 12.42acrylonitrile 12.60diisopropyl ether 12.622,4-dimethylpentane 12.68vinyl acetate 13.02ethyl-tert-buyl ether 13.081-propanol 13.18cis-1,2-dichloroethene 13.32allyl alcohol 13.352,2-dichloropropane 13.48bromochloromethane 13.62chloroform 13.75cyclohexane 13.84methyl acrylate 13.87carbon tetrachloride 13.94tetrahydrofuran 14.031,1,1-trichloroethane 14.06ethyl acetate 14.132-butanone 14.18dibromofluoromethane 14.181,1-dichloropropene 14.20propargyl alcohol 14.351-chlorobutane 14.512,2,4-trimethylpentane 14.53propionitrile 14.59benzene 14.60n-heptane (C7) 14.62methacrylonitrile 14.64

RRttxx®®--VVMMSSCCoommppoouunndd RReett.. TTiimmeebenzene-d6 14.72pentafluorobenzene 14.751,2-dichloroethane-d4 14.791,2-dichloroethane 14.90tert-amyl-methyl ether 15.00isobutyl alcohol 15.06fluorobenzene 15.16isopropyl acetate 15.34formic acid 15.37trichloroethene 15.391,4-difluorobenzene 15.58n-butanol 15.60methyl cyclohexane 15.78acetic acid 15.93dibromomethane 16.051,2-dichloropropane 16.17bromodichloromethane 16.23methyl methacrylate 16.28α,α,α-trifluorotoluene 16.451,4-dioxane 16.49n-propyl acetate 16.702-chloroethyl-vinyl-ether 16.922-chloroethanol 16.93cis-1,3-dichloropropene 17.041-bromo-2-chloroethane 17.05n-octane 17.17toluene-d8 17.28toluene 17.36propionic acid 17.61chloroacetonitrile 17.644-methyl-2-pentanone 17.762-bromo-1-chloropropane 17.812-nitropropane 17.83pyridine 17.861,1-dichloropropanone 17.88trans-1,3-dichloropropene 17.88tetrachloroethene 17.89ethyl methacrylate 17.921,1,2-trichloroethane 18.11dibromochloromethane 18.401,3-dichloropropane 18.49isobutyric acid 18.551,2-dibromoethane 18.78n-butyl acetate 18.802-hexanone 18.82butyric acid 19.171-chloro-3-fluorobenzene 19.17ethylbenzene 19.36chlorobenzene 19.391-chloro-4-fluorobenzene 19.39ethylbenzene-d10 19.401-chlorohexane 19.411,1,1,2-tetrachloroethane 19.44m-xylene 19.53p-xylene 19.54chlorobenzene-d5 19.551-chloro-2-fluorobenzene 19.67o-xylene 20.13stryrene 20.17isovaleric acid 20.18

RRttxx®®--VVMMSSCCoommppoouunndd RReett.. TTiimmeebromoform 20.30isopropylbenzene 20.511,2-butanediol 20.82valeric acid 20.891,4-dichlorobutane 20.90bromobenzene 20.914-bromo-1-fluorobenzene 20.95cis-1,4-dichloro-2-butene 20.97n-decane 21.04n-propylbenzene 21.071,1,2,2-tetrachloroethane 21.101,3,5-trimethylbenzene 21.301-ethyl-4-methylbenzene 21.331-ethyl-3-methylbenzene 21.341,2,3-trichloropropane 21.39trans-1,4-dichloro-2-butene 21.402-chlorotoluene 21.404-chlorotoluene 21.61cyclohexane 21.78tert-butylbenzene 21.811-ethyl-2-methylbenzene 21.821,2,4-trimethylbenzene 21.88pentachloroethane 21.921,3-dichloro-2-propanol 22.05sec-butylbenzene 22.06isocaproic acid 22.09p-isopropyltoluene 22.221,3-dichlorobenzene 22.53caproic acid 22.551,4-dichlorobenzene 22.64n-butylbenzene 22.88malononitrile 22.89benzyl chloride 23.231,2-dichlorobenzene-d4 23.361,2-dichlorobenzene 23.38hexachloroethane 23.631-octanol 23.70bis-(2-chloro-isopropyl) ether 24.064-bromo-1-chlorobenzene 24.09benzyl alcohol 24.23heptanoic acid 24.29n-dodecane 24.543-bromochlorobenzene 24.611,2-dibromo-3-chloropropane 24.782-bromochlorobenzene 25.54hexachlorobutadiene 25.99nitrobenzene 26.021,2,4-trichlorobenzene 26.19benzyl acetate 26.29n-tridecane 26.51naphthalene 27.011,2,3-trichlorobenzene 27.46n-tetradecane 28.832-methylnaphthalene 30.361-methylnaphthalene 30.96n-pentadecane 31.652-chloronaphthalene 33.36

for more infoSee pages 548–551 for Rtx®-VMS volatile organics chromatograms.


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Volatiles

RRxxii®®--662244SSiill MMSSCCoommppoouunndd RReett.. TTiimmeedichlorodifluoromethane 2.178chloromethane 2.438water 2.588vinyl chloride 2.63methanol 2.985ethylene oxide 3.127bromomethane 3.192chloroethane 3.395trichlorofluoromethane 3.834n-pentane 4.032ethanol 4.199diethylether 4.3872-methylbutane 4.501acrolein 4.6771,1-dichloroethene 4.848Freon 113 4.929acetone 4.971iodomethane 5.1352-propanol 5.323carbon disulfide 5.323acetonitrile 5.581methyl acetate 5.676allyl chloride 5.693methylene chloride 5.9392-methylpentane 6.01tert-butyl alcohol 6.19acrylonitrile 6.414methyl-d3-tert-butyl-ether 6.435methyl tert-butyl-ether 6.477trans-1,2-dichloroethene 6.483-methylpentane 6.503hexane 7.0231,1-dichloroethane 7.291allyl alcohol 7.309vinyl acetate 7.33diisopropyl ether 7.386chloroprene 7.4071-propanol 7.431ethyl tert-buyl ether 7.978TB(d9)A 8.133cis-1,2-dichloroethene 8.2042-butanone 8.2082,2-dichloropropane 8.208ethyl acetate 8.283propionitrile 8.297methyl acrylate 8.336methacrylonitrile 8.499bromochloromethane 8.528tetrahydrofuran 8.542chloroform 8.678dibromofluoromethane 8.8711,1,1-trichloroethane 8.872pentafluorobenzene 8.937

RRxxii®®--662244SSiill MMSSCCoommppoouunndd RReett.. TTiimmeecylcohexane 8.9591-chlorobutane 9.032carbon tetrachloride 9.0551,1-dichloropropene 9.067benzene-d6 9.2551,2-dichloroethane-d4 9.28benzene 9.2961,2-dichloroethane 9.365isopropyl acetate 9.3762,2,4-trimethylpentane 9.455isobutyl alcohol 9.456tert-amyl-methyl ether 9.457n-heptane 9.537fluorobenzene 9.6361,4-difluorobenzene 9.7841-butanol 9.911trichloroethene 10.013methyl cyclohexane 10.268tert-amyl ethyl ether 10.271,2-dichloropropane 10.28α,α,α-trifluorotoluene 10.325methyl methacrylate 10.3271,4-dioxane 10.379n-propyl acetate 10.383dibromomethane 10.443bromodichloromethane 10.5322-nitropropane 10.736chloroacetonitrile 10.7642-chloroethyl-vinyl-ether 10.7921-bromo-2-chloroethane 10.843epichlorhydrin 10.875cis-1,3-dichloropropene 10.9382,4-dimethylpentane 10.9614-methyl-2-pentanone 11.0621,1-dichloropropanone 11.105pyridine 11.135toluene-d8 11.185toluene 11.246n-octane 11.345trans-1,3-dichloropropene 11.441ethyl methacrylate 11.4712-bromo-1-chloropropane 11.4971,1,2-trichloroethane 11.619tetrachloroethene 11.6991,3-dichloropropane 11.761n-butyl acetate 11.792dibromochloromethane 11.821,2-dibromoethane 11.9341-chloro-3-fluorobenzene 12.1191-chloro-4-fluorobenzene 12.338chlorobenzene-D5 12.386chlorobenzene 12.415ethylbenzene-d10 12.44

RRxxii®®--662244SSiill MMSSCCoommppoouunndd RReett.. TTiimmee1-chlorohexane 12.4421,1,1,2-tetrachloroethane 12.503ethylbenzene 12.512m-xylene 12.636p-xylene 12.636n-nonane 12.6681-chloro-2-fluorobenzene 12.703o-xylene 12.99stryrene 13.01n-amyl acetate 13.148bromoform 13.177isopropylbenzene 13.327cis-1,4-dichloro-2-butene 13.3821,4-dichlorobutane 13.4394-bromo-1-fluorobenzene 13.4851,1,2,2-tetrachloroethane 13.6bromobenzene 13.612trans-1,4-dichloro-2-butene 13.6351,2,3-trichloropropane 13.655n-propylbenzene 13.6982-chlorotoluene 13.781,3,5-trimethylbenzene 13.858n-decane 13.8674-chlorotoluene 13.886tert-butylbenzene 14.131pentachloroethane 14.161,2,4-trimethylbenzene 14.182sec-butylbenzene 14.325n-butylcyclohexane 14.41,3-dichlorobenzene 14.431p-isopropyltoluene 14.4531,4-dichlorobenzene-d4 14.4971,4-dichlorobenzene 14.519n-butylbenzene 14.7961,2-dichlorobenzene-d4 14.8141,2-dichlorobenzene 14.823hexachloroethane 15.061-octanol 15.074-bromo-1-chlorobenzene 15.4671,2-dibromo-3-chloropropane 15.476nitrobenzene 15.638tetraethyl lead 15.6522-bromochlorobenzene 15.761n-tetradecane 15.783n-dodecane 15.7841,2,4-trichlorobenzene 16.176hexachlorobutadiene 16.293naphthalene 16.4181,2,3-trichlorobenzene 16.6082,5-dibromotoluene 17.4882-methylnaphthalene 17.5581-methyl-naphthalene 17.754

for more infoSee pages 547 for an Rxi®-624Sil MS volatile organics chromatogram.

Volatile Organic Compounds Retention Time Index: Rxi®-624Sil MS*Data collected using a 30 m x 0.25 mm x 1.400 µm Rxi®-624Sil MS column; Oven: 35°C (hold 5 min.) @ 11°C/min. to 60°C @ 20°C/min. to 220°C;Carrier gas: helium; Regulation: constant flow; Flow: 1.17 mL/min.; GC Temperature: 35°C; Inlet Pressure: 7.94 PSI; Outlet Pressure: 0.00 PSI;Dead Time: 1.780 min.; Linear Velocity: 32.68 cm/sec.; Detector 1: Mass Spectrometer*Modeled by Pro ezGC software.


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Volatiles

Volatiles by EPA Method 8260 on Rxi®-624Sil MS (30m, 0.25mm ID, 1.40μm)

Resolution of critical pairs, low

bleed, and high inertness make

this a great column for volatiles!

CCoolluummnn:: Rxi®-624Sil MS, 30 m, 0.25 mm ID, 1.40 µm (cat.# 13868)SSaammppllee:: 8260A Surrogate Mix (cat.# 30240)

8260A Internal Standard Mix (cat.# 30241)8260B MegaMix® Calibration Mix (cat.# 30633)VOA Calibration Mix #1 (ketones) (cat.# 30006)8260B Acetate Mix (revised) (cat.# 30489)California Oxygenates Mix (cat.# 30465)502.2 Calibration Mix #1 (gases) (cat.# 30042)

Conc.: 25 ppb in RO waterIInnjjeeccttiioonn purge and trap split (split ratio 30:1)Inj. Temp.: 225 °CPPuurrggee aanndd TTrraappInstrument: OI Analytical 4660Trap Type: 10 TrapPurge: 11 min. @ 20 °CDesorb Preheat Temp.: 180 °CDesorb: 0.5 min. @ 190 °CBake: 5 min. @ 210 °CInterface Connection: injection portOOvveennOven Temp: 35 °C (hold 5 min.) to 60 °C at 11 °C/min. to 220 °C

at 20 °C/min. (hold 2 min.)CCaarrrriieerr GGaass:: He, constant flowFlow Rate: 1.0 mL/min.DDeetteeccttoorr:: MSMode: ScanTransfer Line Temp.: 230 °CAnalyzer Type: QuadrupoleSource Temp.: 230 °CQuad Temp.: 150 °CElectron Energy: 70 eVSolvent Delay Time: 1.5 min.Tune Type: BFBIonization Mode: EIScan Range: 36-260 amuIInnssttrruummeenntt::Agilent 7890A GC & 5975C MSDNNootteessOther Purge and Trap Conditions:Sample Inlet: 40°CSample: 40°CWater Management: Purge 110°C, Desorb 0°C, Bake, 240°C

PPeeaakkss RRTT ((mmiinn..))1. Dichlorodifluoromethane

(CFC-12) 2.1982. Chloromethane 2.4593. Vinyl chloride 2.6594. Bromomethane 3.2265. Chloroethane 3.4346. Trichlorofluoromethane

(CFC-11) 3.8767. Diethyl ether (ethyl ether) 4.4408. 1,1-Dichloroethene 4.9099. 1,1,2-Trichlorotrifluoroethane

(CFC-113) 4.99810. Acetone 5.02911. Iodomethane 5.19512. Carbon disulfide 5.32313. Acetonitrile 5.63714. Allyl chloride 5.71515. Methyl acetate 5.72316. Methylene chloride 5.98117. tert-Butyl alcohol 6.23418. Acrylonitrile 6.45119. Methyl tert-butyl ether

(MTBE) 6.509

20. trans-1,2-Dichloroethene 6.51221. 1,1-Dichloroethane 7.31522. Vinyl acetate 7.35923. Diisopropyl ether (DIPE) 7.40724. Chloroprene 7.42925. Ethyl tert-butyl ether (ETBE) 7.97026. 2-Butanone (MEK) 8.19327. cis-1,2-Dichloroethene 8.19328. 2,2-Dichloropropane 8.19329. Ethyl acetate 8.26530. Propionitrile 8.27631. Methyl acrylate 8.31832. Methacrylonitrile 8.47633. Bromochloromethane 8.50734. Tetrahydrofuran 8.52135. Chloroform 8.65136. 1,1,1-Trichloroethane 8.84337. Dibromofluoromethane 8.84838. Carbon tetrachloride 9.02639. 1,1-Dichloropropene 9.03740. 1,2-Dichloroethane-d4 9.24641. Benzene 9.26242. 1,2-Dichloroethane 9.33443. Isopropyl acetate 9.340

44. Isobutyl alcohol 9.42145. tert-Amyl methyl ether

(TAME) 9.42146. Fluorobenzene 9.59847. Trichloroethene 9.97648. 1,2-Dichloropropane 10.24349. Methyl methacrylate 10.29050. 1,4-Dioxane (ND) 10.299*51. Dibromomethane 10.32652. Propyl acetate 10.34653. 2-Chloroethanol (ND) 10.368*54. Bromodichloromethane 10.49655. 2-Nitropropane 10.69856. cis-1,3-Dichloropropene 10.90457. 4-Methyl-2-pentanone

(MIBK) 11.02658. Toluene-D8 11.14859. Toluene 11.21060. trans-1,3-Dichloropropene 11.40761. Ethyl methacrylate 11.43562. 1,1,2-Trichloroethane 11.58563. Tetrachloroethene 11.66264. 1,3-Dichloropropane 11.72965. 2-Hexanone 11.749

66. Butyl acetate 11.83767. Dibromochloromethane 11.92168. 1,2-Dibromoethane (EDB) 12.03569. Chlorobenzene-d5 12.41270. Chlorobenzene 12.44071. Ethylbenzene 12.50772. 1,1,1,2-Tetrachloroethane 12.50773. m-Xylene 12.61274. p-Xylene 12.61275. o-Xylene 12.93576. Styrene 12.94977. n-Amyl acetate 13.01878. Bromoform 13.11879. Isopropylbenzene (cumene) 13.22680. cis-1,4-Dichloro-2-butene 13.26881. 4-Bromofluorobenzene 13.38582. 1,1,2,2-Tetrachloroethane 13.45683. trans-1,4-Dichloro-2-butene 13.49684. Bromobenzene 13.51585. 1,2,3-Trichloropropane 13.52686. n-Propylbenzene 13.56587. 2-Chlorotoluene 13.65788. 1,3,5-Trimethylbenzene 13.69989. 4-Chlorotoluene 13.751

90. tert-Butylbenzene 13.96591. Pentachloroethane 14.00792. 1,2,4-Trimethylbenzene 14.01093. sec-Butylbenzene 14.14094. 4-Isopropyltoluene

(p-cymene) 14.25495. 1,3-Dichlorobenzene 14.26396. 1,4-Dichlorobenzene-D4 14.32197. 1,4-Dichlorobenzene 14.34098. n-Butylbenzene 14.57999. 1,2-Dichlorobenzene 14.635

100. 1,2-Dibromo-3-chloropropane (DBCP) 15.252

101. Nitrobenzene 15.407102. 1,2,4-Trichlorobenzene 15.935103. Hexachloro-1,3-butadiene 16.040104. Naphthalene 16.196105. 1,2,3-Trichlorobenzene 16.396

* ND = not detected; retention timedetermined by wet needle injection

XIC — = m/z 43

— = m/z 72

GC_EV1169

NEW!

for more infowww.restek.com/cat006


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Volatiles

Volatile Organics

US EPA Method 8260 (80 ppb Standard)

Rtx®-VMS

GC_EV00685

Column: Rtx®-VMS, 30m, 0.25mm ID, 1.4µm (cat.# 19915)Sample: Calibration, internal standard, surrogate standard

mixes (cat.# 30475B, 30465, 30006, 30240, 30074)PPuurrggee aanndd ttrraapp ccoonnddiittiioonnss:: OO..II.. AAnnaallyyttiiccaall 44556600 wwiitthh 44555511AA AAuuttoossaammpplleerrTrap: #10 (Tenax®/silica gel/carbon molecular sieve)Purge time: 11 min.Purge flow rate: 38mL/min.Desorb flow rate: 32mL/min.Desorb time: 1.0 min.Bake time: 10 min.Sample size: 10mLWater management: 110°C purge, 0°C desorb, 240°C bakeSplit ratio: 1:25Temperatures:Sample: 40°CTrap: 20°C purge, 190°C desorb, 210°C bake

6-Port valve: 110°CTransfer line: 110°CSparge mount: 45°CDesorb preheat: 150°CValve manifold: 50°COther conditions: pre-purge, pre-heat, dry purge OFFCChhrroommaattooggrraapphhyy::Inj. temp.: 250°CCarrier gas: helium, constant flow Flow rate: 1.3 mL/min. Dead time: 1.47 min. @ 35°COven temp.: 35°C (hold 7 min.) to 90°C @ 4°C/min.(no hold)

to 220°C @ 45°C/min. (hold 1 min.). Det.: Agilent 5971A GC/MSTransfer line temp.: 280°CScan range: 35-260amuTune: PFTBA/BFB

*carbon dioxide 1. dichlorodifluoromethane 2. chloromethane3. vinyl chloride4. bromomethane5. chloroethane6. trichlorofluoromethane 7. diethylether8. 1,1-dichloroethene9. carbon disulfide

10. Freon® 11311. iodomethane12. allyl chloride13. methylene chloride14. acetone15. trans-1,2-dichloroethene16. methyl-d3-tert-butyl-ether17. methyl acetate18. methyl-tert-butyl-ether19. tert-butyl alcohol20. acetonitrile21. diisopropyl ether22. chloroprene23. 1,1-dichloroethane24. acrylonitrile25. ethyl-tert-butyl ether

26. cis-1,2-dichloroethene27. 2,2-dichloropropane28. bromochloromethane29. chloroform30. carbon tetrachloride31. tetrahydrofuran32. methyl acrylate33. 1,1,1-trichloroethane34. dibromofluoromethane35. 1,1-dichloropropene36. 2-butanone37. benzene38. propionitrile39. methacrylonitrile40. 1,2-dichloroethane-d441. pentafluorobenzene42. tert-amyl-methyl ether43. 1,2-dichloroethane44. isobutyl alcohol45. trichloroethene46. 1,4-difluorobenzene47. dibromomethane48. 1,2-dichloropropane49. bromodichloromethane50. methyl methacrylate51. cis-1,3-dichloropropene

52. 2-chloroethyl vinyl ether53. toluene-d854. toluene55. 2-nitropropane56. tetrachloroethene57. 2-bromo-1-chloropropane58. 4-methyl-2-pentanone59. trans-1,3-dichloropropene60. 1,1,2-trichloroethane61. ethyl methacrylate62. dibromochloromethane63. 1,3-dichloropropane64. 1,2-dibromoethane65. 2-hexanone66. chlorobenzene-d567. chlorobenzene68. ethylbenzene69. 1,1,1,2-tetrachloroethane70. m-xylene71. p-xylene72. o-xylene73. bromoform74. stryrene75. isopropylbenzene76. 4-bromo-1-fluorobenzene (SS)77. bromobenzene

78. cis-1,4-dichloro-2-butene79. 1,4-dichlorobutane80. n-propylbenzene81. 1,1,2,2-tetrachloroethane82. 2-chlorotoluene83. 1,2,3-trichloropropane84. 1,3,5-trimethylbenzene85. trans-1,4-dichloro-2-butene86. 4-chlorotoluene87. tert-butylbenzene88. pentachloroethane89. 1,2,4-trimethylbenzene90. sec-butylbenzene91. p-isopropyltoluene92. 1,3-dichlorobenzene93. 1,4-dichlorobenzene-d494. 1,4-dichlorobenzene95. n-butylbenzene96. 1,2-dichlorobenzene97. 1,2-dibromo-3-chloropropane98. nitrobenzene99. hexachlorobutadiene

100. 1,2,4-trichlorobenzene101. naphthalene102. 1,2,3-trichlorobenzene

GC_EV00686

Acknowledgments: Purge & trap courtesy of O.I. Analytical.

free literatureAnalysis of Trace Oxygenates

in Petroleum-Contaminated

Wastewater, Using Purge-and-

Trap/GC/MS (US EPA Methods

5030B & 8260)

This 8-page note describes apractical, effective approach tomonitoring oxygenates in wastewater. We evaluated theRtx®-VMS stationary phase foroxygenates recovery, adjustedpurge and trap conditions toincrease responses for oxy-genates, and optimized GC conditions to eliminate coelu-tions of ion-sharing analytes. The result is a sensitive, accurateanalysis for gasoline oxygenatesin wastewater, in the presence of much higher total gasolinecontent.

Download your free copy fromwww.restek.com

Applications Notelit. cat.# 59856

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Volatiles

Volatile Organics

US EPA Method 8260B

Rtx®-VMS

1. dichlorodifluoromethane2. chloromethane3. vinyl chloride4. bromomethane5. chloroethane6. trichlorofluoromethane7. ethanol (2500ppb)8. 1,1-dichloroethene9. carbon disulfide (40ppb)

10. allyl chloride11. methylene chloride12. acetone13. trans-1,2-dichloroethene14. tert-butyl alcohol (100ppb)15. methyl tert-butyl ether16. diisopropyl ether17. 1,1-dichloroethane18. acrylonitrile19. vinyl acetate*20. allyl alcohol (250ppb)21. ethyl-tert-butyl ether*22. cis-1,2-dichloroethene23. 2,2-dichloropropane24. bromochloromethane25. chloroform

26. ethyl acetate27. methyl acrylate28. propargyl alcohol (500ppb)29. dibromofluoromethane (SMC)30. tetrahydrofuran31. carbon tetrachloride32. 2-butanone33. 1,1,1-trichloroethane34. 1,1-dichloropropene35. pentafluorobenzene (IS)36. tert-amyl methyl ether37. benzene38. isobutyl alcohol (500ppb)39. 1,2-dichloroethane40. isopropyl acetate41. 1,4-difluorobenzene (SMC)42. trichloroethene43. dibromomethane44. bromodichloromethane45. 1,2-dichloropropane46. methyl methacrylate47. n-propyl acetate48. 2-chloroethanol (2500ppb)49. cis-1,3-dichloropropene50. toluene-d8 (SMC)

51. toluene52. 4-methyl-2-pentanone53. pyridine (250ppb)54. trans-1,3-dichloropropene55. ethyl methacrylate56. tetrachloroethene57. 1,1,2-trichloroethane58. dibromochloromethane59. 1,3-dichloropropane60. n-butyl acetate61. 1,2-dibromoethane62. 2-hexanone63. 2-picoline (250ppb)64. ethylbenzene65. chlorobenzene-D5 (IS)66. chlorobenzene67. 1,1,1,2-tetrachloroethane68. m-xylene69. p-xylene70. o-xylene71. styrene72. bromoform73. isopropylbenzene74. 4-bromo-1-fluorobenzene (SMC)75. n-propylbenzene

76. 1,1,2,2-tetrachloroethane77. bromobenzene78. 1,3,5-trimethylbenzene79. 2-chlorotoluene80. 1,2,3-trichloropropane81. 4-chlorotoluene82. tert-butylbenzene83. 1,2,4-trimethylbenzene84. pentachloroethane85. sec-butylbenzene86. p-isopropyltoluene87. 1,3-dichlorobenzene88. 1,4-dichlorobenzene-d4 (IS)89. 1,4-dichlorobenzene90. n-butylbenzene91. 1,2-dichlorobenzene92. 1,2-dibromo-3-chloropropane93. nitrobenzene (250ppb)94. hexachlorobutadiene95. 1,2,4-trichlorobenzene96. naphthalene97. 1,2,3-trichlorobenzene

min. 6 8 10 12 14 16

Column: Rtx®-VMS, 60m, 0.25mm ID, 1.40µm (cat.# 19916)Conc.: 10ppb in 5mL of RO water (unless noted);

ketones 2.5XConcentrator: Tekmar LSC-3100 Purge and TrapTrap: Vocarb 3000 (type K)Purge: 11 min. @ 40mL/min. (ambient temperature)Dry purge: 1 min. @ 40mL/min.Desorb preheat: 245°C Desorb: 250°C for 2 min., flow 26mL/min.Bake: 260°C for 8 min.Interface: 0.53mm ID Silcosteel® tubing transfer line

1:20 split at injection port. 1mm ID liner.Oven temp.: 60°C (hold 2 min.) to 180°C @ 12°C/min. (hold 0 min.) to

225°C @ 45°C/min. (hold 6 min.)Carrier gas: helium @ ~1.3mL/min. constant flow

Adjust dichlorodifluoromethane to a retention time of 4.03 min. @ 60°C.

Detector: Agilent 5973 MSDScan range: 35-300amu

1

2

3

4 5

6

7,8

9

10

11,12

13-15

16

17,1819-21

2223

24,25

28

29-3334

35

36-38

39,40

41,42

43

44-46

47

48

49

50

51

52,53

54

55-56

57

58

59

60

61

62

63

64-67

68,69

70

71

72

73

74

75

76,77

78

79,80

81

8283,84

8586

87

88,89

90

91

92

93,94

95

96

97

27

26

GC_EV00427

*Peaks 19 & 21 share an ion (43).

60°C starting temperature• fast analyses• fast cycles

Reduce starting temperature to best focusthe gases.

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Volatiles

Volatile Organics

US EPA Method 8260B

Rtx®-VMS

1. dichlorodifluoromethane2. chloromethane3. vinyl chloride4. bromomethane5. chloroethane6. trichlorofluoromethane7. ethanol (2500ppb)8. 1,1-dichloroethene9. carbon disulfide (40ppb)

10. allyl chloride11. methylene chloride12. acetone13. trans-1,2-dichloroethene14. methyl tert-butyl ether15. tert-butyl alcohol (100ppb)16. diisopropyl ether17. 1,1-dichloroethane18. acrylonitrile19. vinyl acetate20. allyl alcohol (250ppb)21. ethyl-tert-buyl ether22. cis-1,2-dichloroethene23. 2,2-dichloropropane24. bromochloromethane25. chloroform

26. ethyl acetate27. carbon tetrachloride28. methyl acrylate29. propargyl alcohol (500ppb)30. dibromofluoromethane (SMC)31. tetrahydrofuran32. 1,1,1-trichloroethane33. 2-butanone34. 1,1-dichloropropene35. benzene36. pentafluorobenzene (IS)37. tert-amyl-methyl ether38. 1,2-dichloroethane39. isobutyl alcohol (500ppb)40. isopropyl acetate41. trichloroethene42. 1,4-difluorobenzene (SMC)43. dibromomethane44. 1,2-dichloropropane45. bromodichloromethane46. methyl methacrylate47. n-propyl acetate48. 2-chloroethanol (2500ppb)49. cis-1,3-dichloropropene50. toluene-d8 (SMC)

51. toluene52. pyridine (250ppb)53. tetrachloroethene54. 4-methyl-2-pentanone55. trans-1,3-dichloropropene56. 1,1,2-trichloroethane57. ethyl methacrylate58. dibromochloromethane59. 1,3-dichloropropane60. 1,2-dibromoethane61. n-butyl acetate62. 2-hexanone63. 2-picoline (250ppb)64. chlorobenzene-D5 (IS)65. chlorobenzene66. ethylbenzene67. 1,1,1,2-tetrachloroethane68. m-xylene69. p-xylene70. o-xylene71. stryrene72. bromoform73. isopropylbenzene74. 4-bromo-1-fluorobenzene (SMC)75. bromobenzene

76. n-propylbenzene77. 1,1,2,2-tetrachloroethane78. 2-chlorotoluene79. 1,3,5-trimethylbenzene80. 1,2,3-trichloropropane81. 4-chlorotoluene82. tert-butylbenzene83. pentachloroethane84. 1,2,4-trimethylbenzene85. sec-butylbenzene86. p-isopropyltoluene87. 1,3-dichlorobenzene88. 1,4-dichlorobenzene-d4 (IS)89. 1,4-dichlorobenzene90. n-butylbenzene91. 1,2-dichlorobenzene92. 1,2-dibromo-3-chloropropane93. nitrobenzene (250ppb)94. hexachlorobutadiene95. 1,2,4-trichlorobenzene96. naphthalene97. 1,2,3-trichlorobenzene

Column: Rtx®-VMS, 20m, 0.18mm ID, 1.00µm (cat.# 49914)Conc.: 10ppb in 5mL of RO water

unless otherwise noted; ketones at 2.5XConcentrator: Tekmar LSC-3100 Purge and TrapTrap: Vocarb 3000 (type K)Purge: 11 min. @ 40mL/min. (ambient temperature)Dry purge: 1 min. @ 40mL/min.Desorb preheat: 245°C Desorb: 250°C for 2 min., flow 40mL/min.Bake: 260°C for 8 min.Interface: 0.53mm ID Silcosteel® tubing transfer line

1:40 split at injection port. 1mm ID liner.Oven temp.: 50°C (hold 4 min.) to 100°C @ 18°C/min. (hold 0 min.)

to 230°C @ 40°C/min. (hold 3 min.)Carrier gas: helium @ ~1.0mL/min. constant flow

Adjust dichlorodifluoromethane to a retention time of 1.03 min. @ 50°C.Detector: Agilent 5973 MSDScan range: 35-300amu

min. 2 4 6 8 10

2

13

45

6

7

8

9 10

1113

1415

16

17

18

19-212223

24

25

26-2829-32

33,34

35

36 37

38

39

40

41

42

43

4445

46 4748

49

50

51

52

53

54,55

56

57

58

59

6061

62,63

64,65

66,67

68,69

70

71,72

73

74

75

76

77

78

79,80

81

82,83

8485

86

87

88,8990

91

92

93

94

95

96

97

GC_EV00428

12

• First choice for use with dual purge & traps¹• EPA recommended surrogate used.

¹A.L. Hilling and G. Smith, Environmental Testing & Analysis, 10(3), 15-19, 2001.

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Volatiles

Volatile Organics

US EPA Method 524.2 Revision IV

Rtx®-VMS

PPuurrggee aanndd TTrraapp CCoonnddiittiioonnss:: Concentrator: Tekmar LSC-3100 purge and trapTrap: Vocarb 3000 (type K) Purge: 11 min. @ 40mL/min. @ ambient temperature. Dry purge: 1 min. @ 40mL/min. (MCS bypassed using Silcosteel® tubing)Desorb preheat: 245°C Desorb: 250°C for 2 min., flow 33mL/min.Bake: 260°C for 8 min.Interface: Silcosteel® transfer line

1:30 split at injection port. 1mm ID split inlet liner (cat.# 20972)

Column: Rtx®-VMS, 30m, 0.25mm ID, 1.4µm (cat.# 19915)Sample: 502.2 Calibration Mix #1 (cat.# 30042)

Drinking Water VOA MegaMix®, 524.2 Rev 4 (cat.# 30601)524 Internal Standard/Surrogate Mix (cat.# 30201)Ketone Mix, EPA Method 524.2 Rev 4.1 (cat.# 30602)Compounds at 20 ppb each in 5mL RO water(ketones at 50ppb; internal standards at 40ppb)

Inj. temp.: 250°CCarrier gas: helium, constant flow Flow rate: 1.1mL/min. Dead time: 1.48 min. @ 40°COven temp.: 40°C (hold 2 min.) to 85°C @ 14°C/min. (hold 2 min.) to

220°C @ 30°C/min. (hold 4 min.). Det: Agilent 5971A GC/MSTransfer line temp.: 280°CScan range: 35-300amuTune PFTBA/BFBIonization: EI

1. dichlorodifluoromethane2. chloromethane3. vinyl chloride4. bromomethane5. chloroethane6. trichlorofluoromethane7. diethyl ether8. 1,1-dichloroethene9. carbon disulfide

10. iodomethane11. allyl chloride12. methylene chloride13. acetone14. trans-1,2-dichloroethene15. methyl tert-butyl ether16. 1,1-dichloroethane17. acrylonitrile18. cis-1,2-dichloroethene

19. 2,2-dichloropropane20. bromochloromethane21. chloroform22. methyl acrylate23. carbon tetrachloride24. tetrahydrofuran25. 1,1,1-trichloroethane26. 2-butanone27. 1,1-dichloropropene28. 1-chlorobutane29. propionitrile30. methacrylonitrile31. benzene32. 1,2-dichloroethane33. fluorobenzene34. trichloroethene35. dibromomethane36. 1,2-dichloropropane

37. bromodichloromethane38. methyl methacrylate39. cis-1,3-dichloropropene40. toluene41. chloroacetonitrile42. 2-nitropropane43. 1,1-dichloropropanone44. 4-methyl-2-pentanone45. tetrachloroethene46. trans-1,3-dichloropropene47. 1,1,2-trichloroethane48. ethyl methacrylate49. dibromochloromethane50. 1,3-dichloropropane51. 1,2-dibromoethane52. 2-hexanone53. chlorobenzene54. ethylbenzene

55. 1,1,1,2-tetrachloroethane56. m-xylene57. p-xylene58. o-xylene59. styrrene60. bromoform61. isopropylbenzene62. 4-bromofluorobenzene 63. bromobenzene64. n-propylbenzene65. 1,1,2,2-tetrachloroethane66. 2-chlorotoluene67. 1,2,3-trichloropropane68. 1,3,5-trimethylbenzene69. trans-1,4-dichloro-2-butene70. 4-chlorotoluene71. tert-butylbenzene72. pentachloroethane

73. 1,2,4-trimethylbenzene74. sec-butylbenzene75. p-isopropyltoluene76. 1,3-dichlorobenzene77. 1,4-dichlorobenzene78. n-butylbenzene79. hexachloroethane80. 1,2-dichlorobenzene-d481. 1,2-dichlorobenzene82. 1,2-dibromo-3-chloropropane83. nitrobenzene84. hexachlorobutadiene85. 1,2,4-trichlorobenzene86. naphthalene87. 1,2,3-trichlorobenzene

GC_EV00718

*Peaks 42 & 43 share an ion (43).

Chromatogram Search ToolSearch by compound name, synonym,CAS # or keywordwww.restek.com/chromatograms


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Volatiles

EDB/DBCP

US EPA Method 504.1

Rtx®-CLPesticides & Rtx®-CLPesticides2

1. chloroform2. bromodichloromethane3. chlorodibromomethane4. 1,2-dibromoethane (EDB)5. 1,1,1,2-tetrachloroethane6. bromoform7. 1,2,3-trichloropropane8. 1,2-dibromo-3-chloropropane (DBCP)

Columns: Rtx®-CLPesticides, 30m, 0.32mm ID, 0.50µm (cat.# 11139),Rtx®-CLPesticides2, 30m, 0.32mm ID, 0.25µm (cat.# 11324), 0.32mm ID guard column (cat.# 10044), universal angled “Y” Press-Tight® connector (cat.# 20403)

Inj. Direct injection using a Uniliner® inlet liner (cat.#20335)On-column conc.: 10pg each compound. Oven temp.: 35°C (hold 2 min.) to 300°C @ 12°C/min. Inj./det. temp.: 200°C/300°C Carrier gas: helium, 12psi constant pressure

Rtx®-CLPesticides

Rtx®-CLPesticides2

min. 3 4 5 6 7 8 9 10

1

2

3

4

5

6

7

8

1

2

3

4

5

6

7

8

min. 3 4 5 6 7 8 9 10

GC_EV00020

• Dual-column analysis

free literatureGC Analysis of US EPA Method 504.1

Organochlorine Pesticides, Using

the Rtx®-CLPesticides and

Rtx®-CLPesticides2 Columns

A versatile column pair for analyzing organochlorine pesticides, herbicides, or PCBs

Analysts following Method 504.1 in monitoring 1,2-dibromoethane (EDB), 1,2-dibromo-3-chloropropane (DBCP), and1,2,3-trichloropropane (TCP) in drinkingwater will value Rtx®-CLPesticides and Rtx®-CLPesticides2 columns because thissame primary column/confirmation columnpair can be used to perform numerous related analyses: organochlorine pesticides(e.g., by EPA Method 608 or 8081), herbicides, or polychlorinated biphenyls(PCBs). Details in this 2-page note show EDB,DBCP, and TCP are fully resolved from common interference compounds, perrequirements of Method 504.1.


Rtx®-CLPesticides and Rtx®-CLPesticides2

columns also are ideal for:

• Triazine herbicides (lit. cat.# 59101)

• PCBs (lit. cat.# 59120)

• Chlorinated pesticides (lit. cat.# EVAN1197)

• Chlorinated pesticides, PCBs, & chlorinatedherbicides (lit. cat.# EVFL1013)

Download your free copy of the literature listed here from www.restek.com

No chromatographic influence

from trihalomethane compounds.


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Semivolatiles

Phenols

US EPA Method 604

MXT®-5

1

2 3

4

5

6

7

8

910

11

min. 4 8 12 16

604 Phenols Mix (cat.# 31029)1. phenol2. 2-chlorophenol3. 2-nitrophenol4. 2,4-dimethylphenol5. 2,4-dichlorophenol6. 4-chloro-3-methylphenol7. 2,4,6-trichlorophenol8. 2,4-dinitrophenol9. 4-nitrophenol

10. 2-methyl-4,6-dinitrophenol11. pentachlorophenol

GC_EV00027

Column: MXT®-5, 30m, 0.28mm ID, 0.25µm (cat.# 70224)Inj.: 1.0µL splitless injection of phenolsConc.: 25ng/µL per componentOven temp.: 40°C to 250°C @ 10°C/min.Inj./det. temp.: 280°C/300°CCarrier gas: hydrogenLinear velocity: 50cm/sec. set @ 40°CFID sensitivity: 2.56 x 10-10 AFS

Phenols

US EPA Method 604

Rtx®-200

Column: Rtx®-200, 30m, 0.32mm ID, 0.25µm (cat.# 15024)Inj.: 1.0µL split injection of a 200ng standardOven temp.: 50°C (hold 4 min.) to 250°C @ 6°C/min.Inj./det. temp.: 250°CCarrier gas: heliumLinear velocity: 20cm/sec. FID sensitivity: 4 x 10-11 AFSSplit ratio: 40:1

11

109

8

6

54

2

1

min. 4 8 12 16 20 24 28

7

3

GC_EV00028

604 Phenols Mix (cat.# 31029)1. phenol2. 2-chlorophenol3. 2,4-dimethylphenol4. 2,4-dichlorophenol5. 2-nitrophenol6. 4-chloro-3-methylphenol7. 2,4,6-trichlorophenol8. 4-nitrophenol9. pentachlorophenol

10. 2,4-dinitrophenol11. 2-methyl-4,6-dinitrophenol

Phenols

US EPA Method 604

Rtx®-5

Column: Rtx®-5, 30m, 0.25mm ID, 0.25µm (cat.# 10223)Inj.: 1.0µL split injection of phenols.Conc.: 3-5ng/µL per component.Oven temp.: 50°C (hold 4 min.) to 250°C

@ 8°C/min.Inj./det. temp.: 250°CCarrier gas: hydrogenLinear velocity: 40cm/sec. set @ 110°CFID sensitivity: 8 x 10-11 AFSSplit ratio: 40:1

min. 4 8 12 16 20 24

1

2

35

6

78

9

10

11

4

GC_EV00030

604 Phenols Mix (cat.# 31029)1. phenol2. 2-chlorophenol3. 2-nitrophenol4. 2,4-dimethylphenol5. 2,4-dichlorophenol6. 4-chloro-3-methylphenol7. 2,4,6-trichlorophenol8. 2,4-dinitrophenol9. 4-nitrophenol

10. 2-methyl-4,6-dinitrophenol11. pentachlorophenol

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Solutions Online

www.restek.com/enviro

553-568_GCappSemivol.qxp 11/22/2010 9:03 PM Page 553

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Semivolatiles

1

2

3

45

6

7

8

9 10 11

12

13

14

15

16

4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50 11.00 min.

Phthalate & Adipate Esters

US EPA Method 506

Rxi®-1ms

GC_EV00832

Column: Rxi®-1ms, 30m, 0.25mm ID, 0.25µm (cat.# 13323)Sample: US EPA Method 506 mix:

506 Calibration Mix (cat.# 31845), SV Internal Standard Mix (cat.# 31206), B/N Surrogate Mix (4/89 SOW) (cat.# 31024)

Inj.: 1.0µL, 5µg/mL each analyte (internal standards 25µg/mL), split (10:1)4mm Drilled Uniliner® inlet liner (hole on bottom) (cat.# 20771)

Instrument: Agilent 6890Inj. temp.: 250°CCarrier gas: helium, constant flowFlow rate: 1.2mL/min.Oven temp.: 50°C (hold 1 min.) to 330°C @ 30°C/min. (hold 2 min.)Det.: Agilent 5973 MSDTransfer line

temp.: 280°CScan range: 35-550amuSolvent delay: 3.75 min.Tune: DFTPPIonization: EI

1. 1,4-dichlorobenzene-d4 (IS)2. nitrobenzene-d5 (SS)3. naphthalene-d8 (IS)4. 2-fluorobiphenyl (SS)5. dimethylphthalate6. acenaphthene-d10 (IS)7. diethylphthalate8. phenanthrene-d10 (IS)9. di-n-butylphthalate

10. p-terphenyl-d14 (SS)11. benzyl butyl phthalate12. bis(2-ethylhexyl)adipate13. chrysene-d12 (IS)14. bis(2-ethylhexyl)phthalate15. di-n-octylphthalate16. perylene-d12 (IS)

Rxi® Technology!Exceptionally inert,

ultra low- bleed capillary columns.



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Semivolatiles

Column: Rtx®-5Sil MS, 30m, 0.25mm ID, 0.25µm (cat.# 12723)Sample: 50µg/mL 610 PAH Mix (cat.# 31011)

in methylene chloride Inj.: 1.0µL splitless (hold 2 min.),

2mm splitless inlet liner w/wool (cat.# 20829)Inj. temp.: 330°CCarrier gas: hydrogen, 4mL/min. constant flow Oven temp.: 40°C (hold 2 min.) to 250°C @ 25°C/min. to 265°C @ 5°C/min.

to 300°C (hold 4 min.) @ 25°C/min.Det.: FID @ 350°C

1. naphthalene2. acenaphthylene3. acenaphthene4. fluorene5. phenanthrene6. anthracene7. fluoranthene8. pyrene9. benzo(a)anthracene

10. chrysene11. benzo(b)fluoranthene12. benzo(k)fluoranthene13. benzo(a)pyrene14. indeno(1,2,3-cd)pyrene15. dibenzo(a,h)anthracene16. benzo(ghi)perylene

GC_EV00595

Polycyclic Aromatic Hydrocarbons

US EPA Method 610

Rtx®-5Sil MS

PAHs resolved in

less than 16 min.!

1. 0 2. 0 3. 0 4. 0 5. 0 6. 0 7. 0 8. 0 9. 0 10. 0

1. naphthalene2. acenaphthylene3. acenaphthene4. fluorene5. phenanthrene6. anthracene7. fluoranthene8. pyrene

9. benzo(a)anthracene10. chrysene11. benzo(b)fluoranthene12. benzo(k)fluoranthene13. benzo(a)pyrene14. indeno(1,2,3-cd)pyrene15. dibenzo(a,h)anthracene16. benzo(ghi)perylene


US EPA Method 610

Rxi®-5Sil MS (20m x 0.18 mm x 0.18 μm)

Column: Rxi®-5Sil MS, 20m, 0.18mm ID, 0.18µm (cat.# 43602)Sample: 610 PAH Mix, 10ppm (cat.# 31011) Instrument: PerkinElmer Clarus 600Inj.: 0.5µL splitless (hold 1.75 min.), 2mm split/splitless liner w/ wool (cat.# 21718)Inj. temp.: 320°CCarrier gas: helium, constant flow Linear velocity: 37cm/sec. @ 45°COven temp.: 45°C (hold 0.5 min.) to 150°C @ 95°C/min. to 270°C @ 45°C/min. to 300°C @ 7°C/min. Det.: FID @ 320°C

GC_EV01037

1 2 34

5 6

78

910

1211

13

1415

16

min.

NEW!

PAHs resolved in

less than 10 min.!


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Semivolatiles

Peak List Retention Time1. naphthalene 4.932. 2-methylnaphthalene 5.583. 1-methylnaphthalene 5.684. 2-fluorobiphenyl (SS) 5.935. acenaphthylene 6.456. acenaphthene 6.627. fluorene 7.128. phenanthrene 8.069. anthracene 8.11

10. fluoranthene 9.2311. pyrene 9.4512. p-terphenyl-d14 (IS) 9.6113. benzo(a)anthracene 10.6514. chrysene 10.6915. benzo(b)fluoranthene 11.9616. benzo(k)fluoranthene 12.0017. benzo(a)pyrene 12.4218. perylene-d12 (IS) 12.5119. indeno(1,2,3-cd)pyrene 14.1920. dibenzo(a,h)anthracene 14.2321. benzo(ghi)perylene 14.65

Column: Rxi®-5Sil MS, 30m, 0.25mm ID, 0.25µm (cat.# 13623) Sample: PAH mix, 1µL of 0.005µg/mL (IS 2µg/mL)

SV Calibration Mix #5 (cat.# 31011)1-methylnaphthalene (cat.# 31283)2-methylnaphthalene (cat.# 31285)2-fluorobiphenyl (cat.# 31091)

Inj.: 1.0µL (5pg on-column concentration), 4mm Drilled Uniliner® (hole near top) inlet liner w/wool (cat.# 21055-200.5),pulsed splitless: pulse 20psi @ 0.2 min., 60mL/min. @ 0.15 min.

Inj. temp.: 300°CCarrier gas: helium, constant flowFlow rate: 1.4mL/min.Oven temp.: 50°C (hold 0.5 min.) to 290°C @ 25°C/min. to 320°C @ 5°C/min. Det.: MSTransfer line

temp: 290°CIonization: EIMode: SIM

SSiinnggllee IIoonn MMoonniittoorriinngg PPrrooggrraammGGrroouupp TTiimmee IIoonn((ss)) DDwweellll ((mmss))1 4.00 128 1002 5.25 142 1003 5.80 172 1004 6.25 152 1005 6.90 166 1006 7.60 178 1007 8.75 202, 244 1008 10.2 228 1009 11.5 252, 264 100

10 13.5 276, 278 100


Rxi®-5Sil MS

GC_EV00970

Full ScaleOutstanding response at5pg on-column!



free literatureAccurately Quantify PAHs Down to 5 pg On-Column: GC/MS Sim Analysis with the New Rxi®-5Sil MS Column

Polycyclic aromatic hydrocarbons (PAHs) are common environmental pollutants, affecting air, water, and soil quality.Although naturally occurring, human impact has created a steady increase in environmental levels of PAHs and theirbyproducts. PAHs are typically formed through the incomplete combustion of organic materials, such as wood, coal,and oil, but are also used in manufacturing of some medicines, plastics, and pesticides. Many PAHs are known or suspected carcinogens. The United States Environmental Protection Agency currently lists and mandates testing ofthe 16 PAHs they deem most hazardous.

Download your free copy from www.restek.com

Applications Notelit. cat.# EVAN1284


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Semivolatiles

Restek Customer ServiceIn the U.S.Call: 800-356-1688 (ext. 3) or 814-353-1300(ext. 3)

Monday–Friday 8:00 a.m.–6:00 p.m. ET

Fax: 814-353-1309—24-hours a day

Online: www.restek.com—24-hours a day

Outside the U.S.Contact your Restek representative:Refer to our list on pages 4-5 or visit our website at www.restek.com

Mike Shuey, Customer Service

GC_EV1160

1. Naphthalene2. 2-Methylnaphthalene3. 1-Methylnaphthalene4. Acenaphthylene5. Acenaphthene6. Fluorene7. Phenanthrene8. Anthracene9. Fluoranthene

10. Pyrene11. Benz[a]anthracene12. Chrysene13. Triphenylene14. Benzo[b]fluoranthene

15. Benzo[k]fluoranthene16. Benzo(j)fluoranthene17. Benzo[a]pyrene18. 3-Methylcholanthrene19. Dibenz(a,h)acridine20. Dibenz[a,j]acridine21. Indeno[1,2,3-cd]pyrene22. Dibenz[a,h]anthracene23. Benzo[ghi]perylene24. 7H-Dibenzo[c,g]carbazole25. Dibenzo[a,e]pyrene26. Dibenzo(a,i)pyrene27. Dibenzo(a,h)pyrene

CCoolluummnn Rxi®-17Sil MS, 30 m, 0.25 mm ID, 0.25 µm (cat.# 14123)SSaammppllee SV Calibration Mix #5 / 610 PAH Mix (cat.# 31011)

EPA Method 8310 PAH Mixture (cat.# 31841)Diluent: dichloromethaneConc.: 10 ppmIInnjjeeccttiioonnInj. Vol.: 0.5 µL splitless (hold 1.75 min.)Liner: Auto SYS XL PSS Split/Splitless w/Wool (cat.# 21718)Inj. Temp.: 320 °CPurge Flow: 75 mL/min.OOvveennOven Temp: 65 °C (hold 0.5 min.) to 220 °C at 15 °C/min. to 330 °C at 4 °C/min. (hold 15 min.)CCaarrrriieerr GGaass He, constant flowFlow Rate: 2.0 mL/min.DDeetteeccttoorr FID @ 320 °CIInnssttrruummeenntt PE Clarus 600 GCAAcckknnoowwlleeddggeemmeenntt Instrument provided by PerkinElmer


US EPA Method 8100

Rxi®-17Sil MSNEW!


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Semivolatiles

GC_EV1186


Rxi®-17Sil MS (15 m x 0.25 mm x 0.25 μm)

PPeeaakkss1. Naphthalene2. 2-Methylnaphthalene3. 1-Methylnaphthalene4. Acenaphthylene5. Acenaphthene6. Fluorene7. Phenanthrene8. Anthracene9. Fluoranthene

10. Pyrene11. Benzo(a)anthracene12. Chrysene13. Triphenylene14. Benzo(b)fluoranthene15 Benzo(k)fluoranthene16. Benzo(j)fluoranthene17. Benzo(a)pyrene18. Indeno(1,2,3-cd)pyrene19. Dibenz(a,h)anthracene20. Benzo(ghi)perylene

CCoolluummnn Rxi®-17Sil MS, 15 m, 0.25 mm ID, 0.25 µm (cat.# 14120)SSaammpplleeDiluent: Methylene chlorideConc.: 20 ng/µLIInnjjeeccttiioonnInj. Vol.: 1 µL split (split ratio 20:1)Liner: 4mm Split Precision® Liner w/Wool (cat.# 21022)Inj. Temp.: 275 °CSplit VentFlow Rate: 42 mL/min.OOvveennOven Temp: 80 °C (hold 1 min.) to 320 °C at 15 °C/min. (hold 2 min.)CCaarrrriieerr GGaass H2, constant flowFlow Rate: 2 mL/min.DDeetteeccttoorr FID @ 340 °CConstant Column +Constant Make-up: 50 mL/min.Make-upGas Type: N2

Data Rate: 20 HzIInnssttrruummeenntt Agilent/HP6890 GC

NEW!

GC_EV1189

BenzofluoranthenesRxi®-17Sil MS (15 m x 0.25 mm x 0.25 μm)

PPeeaakkss1. Benzo(b)fluoranthene2. Benzo(k)fluoranthene3. Benzo(j)fluoranthene

PPeeaakkss1. Phenanthrene2. Anthracene

GC_EV1188

Phenanthrene and AnthraceneRxi®-17Sil MS (15 m x 0.25 mm x 0.25 μm)


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Semivolatiles


US EPA Method 610

Rxi®-5ms

1. naphthalene2. acenaphthylene3. acenaphthene4. fluorene5. phenanthrene6. anthracene7. fluoranthene8. pyrene

9. benzo(a)anthracene10. chrysene11. benzo(b)fluoranthene12. benzo(k)fluoranthene13. benzo(a)pyrene14. indeno(1,2,3-cd)pyrene15. dibenzo(a,h)anthracene16. benzo(ghi)perylene

GC_EV00824

Column: Rxi®-5ms, 30m, 0.25mm ID, 0.25µm (cat.# 13423)

Sample: SV Calibration Mix #5/610 PAH Mix (cat.# 31011)

Inj.: 1.0µL, 10ppm each analyte (10ng on column), splitless (hold 0.1 min.)4mm Drilled Uniliner® inlet liner (hole near bottom) (cat.# 20771)

Instrument: Agilent 6890Inj. temp.: 275°CCarrier gas: helium, constant flow

Flow rate: 1.2mL/min.Oven temp.: 75°C (hold 0.5 min.) to 245°C @ 25°C/min.,

to 330°C @ 4°C/min. (hold 1 min.)Det.: Agilent 5973 GC/MSTransfer line

temp.: 280°CScan range: 35-550amuSolvent delay: 2 min.Tune: DFTPPIonization: EI

14.75 15.00 15.25 15.50 15.75

benzo(b)fluoranthene benzo(k)fluoranthenePolycyclic Aromatic Hydrocarbons

US EPA Method 610 (with Internal Standards & Surrogates)Rxi®-5ms

GC_EV00825

1. 2-fluorophenol2. phenol-d63. 1,4-dichlorobenzene-d44. nitrobenzene-d55. naphthalene-d86. naphthalene7. 2-fluorobiphenyl8. acenaphthylene9. acenaphthene-d10

10. acenaphthene11. fluorene12. 2,4,6-tribromophenol13. phenanthrene-d1014. phenanthrene

15. anthracene16. fluoranthene17. pyrene18. p-terphenyl-d1419. benzo(a)anthracene20. chrysene-d1221. chrysene22. benzo(b)fluoranthene23. benzo(k)fluoranthene24. benzo(a)pyrene25. perylene-d1226. indeno(1,2,3-cd)pyrene27. dibenzo(a,h)anthracene28. benzo(ghi)perylene

Column: Rxi®-5ms, 30m, 0.25mm ID, 0.25µm (cat.# 13423)Sample: SV Calibration Mix #5/610 PAH Mix

(cat.# 31011), Acid Surrogate Mix (4/89 SOW) (cat.# 31025), B/N Surrogate Mix (4/89 SOW) (cat.# 31024), SV Internal Standard Mix (cat.# 31206)

Inj.: 1.0µL, 10ppm each analyte (10ng on column; 40ng each internal standard), splitless (hold 0.1 min.)4mm Drilled Uniliner® inlet liner (hole near bottom) (cat.# 20771)

Instrument: Agilent 6890

Inj. temp.: 275°CCarrier gas: helium, constant flowFlow rate: 1.2mL/min.Oven temp.: 75°C (hold 0.5 min.) to 245°C @ 25°C/min.,

to 330°C @ 4°C/min. (hold 1 min.)Det.: Agilent 5973 GC/MSTransfer line

temp.: 280°CScan range: 35-550amuSolvent delay:2 min.Tune: DFTPPIonization: EI






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Semivolatiles

Semivolatile Organics

US EPA Method 526 (Screening)

Rtx®-5Sil MS

GC_EV00656

Column: Rtx®-5Sil MS, 30m, 0.25mm ID, 0.25µm (cat.# 12723)Sample: US EPA Method 526 Mix 1µL 10ppm (20ppm IS)

Primary Dilution Standard/Semivolatiles/EPA 526 (cat.# 31691)Surrogate Standard/Method 526 (cat.# 31693)Internal Standard/Method 526 (cat.# 31692)

Inj.: 1.0µL splitless (hold 0.3 min.), 4mm Drilled Uniliner® inlet liner (cat.# 21055)

GC Agilent 6890 Inj. temp.: 300°CCarrier gas: helium, constant flowFlow rate: 0.8mL/min.Oven temp.: 50°C (hold 1 min.) to 200°C @ 20°C/min. (hold 5 min.)

to 310°C @ 30°/min. (hold 3 min.)Det: Agilent 5973 GC/MSTransfer line temp.: 280°CScan range: 35-550amuSolvent delay: 5.5 min.Tune: DFTPPIonization: EI

1. nitrobenzene2. 2,4-dichlorophenol3. 1,3-dimethyl-2-nitrobenzene (SS)4. 2,4,6-trichlorophenol5. acenaphthene-d10 (IS#1)6. azobenzene*7. prometon8. terbufos9. diazinon

10. fonofos

11. phenanthrene-d10 (IS#2)12. disulfoton13. acetochlor14. cyanazine15. triphenylphosphate (SS)16. chrysene-d12* Compound listed in method,

1,2-diphenylhydrazine, decomposes toazobenzene.

Column: Rtx®-5Sil MS, 30m, 0.25mm ID, 0.25µm (cat.# 12723)Sample: US EPA Method 528 Mix 1µL 5ppm standard

Phenol Stock Calibration Solution (cat.# 31694)Internal Standard Phenols Method 528 (cat.# 31696)Surrogate Fortification Standard/Phenols (cat.# 31692)5ng each analyte on-column

Inj.: 1.0µL pulsed splitless (hold 0.5 min.),4mm Drilled Uniliner® inlet liner (cat.# 21055), pulsed pressure 50psi for 0.5 min.

GC: Agilent 6890 Inj. temp.: 220°CCarrier gas: helium, constant flow Flow rate: 1.3mL/min. Oven temp.: 40°C (hold 1 min.) to 220°C @ 12°C/min.

(hold 0 min.) to 300°C @ 30°C/min. (hold 1 min.) Det: Agilent 5973 GC/MSTransfer line temp.: 280°CScan range: 35-550amuSolvent delay: 5.5 min.Tune: DFTPPIonization: EI

Phenols

US EPA Method 528

Rtx®-5Sil MS

GC_EV00664

1. phenol2. 2-chlorophenol-3,4,5,6-d4 (SS)3. 2-chlorophenol4. 2-methylphenol5. 2-nitrophenol6. 2,4-dimethylphenol-3,5,6-d3 (SS)7. 2,4-dimethylphenol8. 2,4-dichlorophenol9. 4-chloro-3-methylphenol

10. 1,2-dimethyl-3-nitrobenzene (IS#1)11. 2,4,6-trichlorophenol12. 2,4-dinitrophenol13. 4-nitrophenol14. 2,3,4,5-tetrachlorophenol (IS#2)15. 2-methyl-4,6-dinitrophenol16. 2,4,6-tribromophenol (SS)17. pentachlorophenol

Optimized

resolution!

Excellent sensitivity

and peak shape

at 5ng on-column.


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Semivolatiles

1. 1,4-dioxane2. N-nitrosodimethylamine3. pyridine4. 2-fluorophenol (SS)5. phenol-d6 (SS)6. phenol7. aniline8. bis(2-chloroethyl) ether9. 2-chlorophenol

10. 1,3-dichlorobenzene11. 1,4-dichlorobenzene-d4 (IS)12. 1,4-dichlorobenzene13. benzyl alcohol14. 1,2-dichlorobenzene 15. 2-methylphenol16. bis(2-chloroisopropyl) ether17. 4-methylphenol/3-methylphenol18. N-nitroso-di-n-propylamine19. hexachloroethane20. nitrobenzene-d5 (SS)

21. nitrobenzene22. isophorone23. 2-nitrophenol 24. 2,4-dimethylphenol25. benzoic acid26. bis(2-chloroethoxy)methane27. 2,4-dichlorophenol28. 1,2,4-trichlorobenzene29. naphthalene-d8 (IS)30. naphthalene31. 4-chloroaniline32. hexachlorobutadiene33. 4-chloro-3-methylphenol34. 2-methylnaphthalene35. 1-methylnaphthalene36. hexachlorocyclopentadiene37. 2,4,6-trichlorophenol38. 2,4,5-trichlorophenol39. 2-fluorobiphenyl (SS)40. 2-chloronaphthalene

41. 2-nitroaniline42. 1,4-dinitrobenzene43. dimethyl phthalate44. 1,3-dinitrobenzene45. 2,6-dinitrotoluene46. 1,2-dinitrobenzene 47. acenaphthylene48. 3-nitroaniline49. acenaphthene-d10 (IS)50. acenaphthene 51. 2,4-dinitrophenol52. 4-nitrophenol53. 2,4-dinitrotoluene54. dibenzofuran55. 2,3,5,6-tetrachlorophenol56. 2,3,4,6-tetrachlorophenol57. diethyl phthalate58. 4-chlorophenyl phenyl ether59. fluorene60. 4-nitroanaline

61. 4,6-dinitro-2-methylphenol62. N-nitrosodiphenylamine

(diphenylamine)63. 1,2-diphenylhydrazine

(as azobenzene)64. 2,4,6-tribromophenol (SS)65. 4-bromophenyl phenyl ether66. hexachlorobenzene67. pentachlorophenol68. phenanthrene-d10 (IS)69. phenanthrene70. anthracene71. carbazole72. di-n-butyl phthalate73. fluoranthene74. benzidine75. pyrene-d10 (SS)76. pyrene77. p-terphenyl-d14 (SS)78. 3,3-dimethylbenzidine

79. butyl benzyl phthalate80. bis(2-ethylhexyl) adipate81. 3,3'-dichlorobenzidine82. benzo(a)anthracene83. bis(2-ethylhexyl) phthalate84. chrysene-d12 (IS)85. chrysene86. di-n-octyl phthalate87. benzo(b)fluoranthene88. benzo(k)fluoranthene89. benzo(a)pyrene90. perylene-d12 (IS)91. dibenzo(a,h)anthracene92. indeno(1,2,3-cd)pyrene93. benzo(ghi)perylene

c = toluene


US EPA Method 8270

Rxi®-5Sil MS

GC_EV01129

Restek's New Semivolatiles Wool

High 2,4-DNP response (RF = 0.269).

Column: Rxi®-5Sil MS, 30m, 0.25mm ID,0.25µm (cat.# 13623)

Sample: 8270 MegaMix® (cat.# 31850),Benzoic Acid (cat.# 31879)8270 Benzidines Mix (cat.# 31852),Acid Surrogate Mix (4/89 SOW) (cat.# 31025),Revised B/N Surrogate Mix (cat.# 31887),1,4-dioxane (cat.# 31853),SV Internal Standard Mix (cat.# 31206) in methylene chloride, 10ng on column

Inj.: 1.0µL pulsed splitless,pulse 25psi @ 0.3min., 60mL/min. @ 0.25min,4mm single gooseneck liner with semivolatiles wool (cat.# 20798-231.1)

Inj. temp.: 250°CCarrier gas: helium, constant flow Flow rate: 1.2mL/min. Oven temp.: 40°C (hold 1.0 min.) to 280°C @ 25°C/min. to

320°C @ 5°C/min. (hold 1.0 min.)Det: MSTransfer line

temp.: 280°CScan range: 35-550 amuIonization: EIMode: scan Instrument: Agilent 7890A/5975 GC/MS

Symmetric

pyridine peak

shape.

Excellent

resolution

of PAHs.

NEW!


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Semivolatiles

GC_EV1182

Semivolatiles

EPA Method 8270

Rxi®-5Sil MS (Split Injection)

PPeeaakkss1. 1,4-Dioxane2. N-Nitrosodimethylamine3. Pyridine4. 2-Fluorophenol (SS)5. Phenol-d6 (SS)6. Phenol7. Aniline8. Bis(2-chloroethyl) ether9. 2-Chlorophenol

10. 1,3-Dichlorobenzene11. 1,4-Dichlorobenzene-D4 (IS)12. 1,4-Dichlorobenzene13. Benzyl Alcohol14. 1,2-Dichlorobenzene15. 2-Methylphenol16. Bis(2-chloroisopropyl) ether17. 4-Methylphenol/3-Methylphenol18. N-Nitrosodi-N-propylamine19. Hexachloroethane20. Nitrobenzene-D5 (SS)21. Nitrobenzene22. Isophorone23. 2-Nitrophenol

24. 2,4-Dimethylphenol25. Benzoic acid26. Bis(2-chloroethoxy)methane27. 2,4-Dichlorophenol28. 1,2,4-Trichlorobenzene29. Naphthalene-D8 (IS)30. Naphthalene31. 4-Chloroaniline32. Hexachlorobutadiene33. 4-Chloro-3-methylphenol34. 2-Methylnaphthalene35. 1-Methylnaphthalene36. Hexachlorocyclopentadiene37. 2,4,6-Trichlorophenol38. 2,4,5-Trichlorophenol39. 2-Fluorobiphenyl (SS)40. 2-Chloronaphthalene41. 2-Nitroaniline42. 1,4-Dinitrobenzene43. Dimethyl phthalate44. 1,3-Dinitrobenzene45. 2,6-Dinitrotoluene46. 1,2-Dinitrobenzene47. Acenaphthylene

48. 3-Nitroaniline49. Acenaphthene-d10 (IS)50. Acenaphthene51. 2,4-Dinitrophenol52. 4-Nitrophenol53. 2,4-Dinitrotoluene54. Dibenzofuran55. 2,3,5,6-Tetrachlorophenol56. 2,3,4,6-Tetrachlorophenol57. Diethyl Phthalate58. 4-Chlorophenyl phenyl ether59. Fluorene60. 4-Nitroaniline61. 4,6-Dinitro-2-methylphenol62. N-Nitrosodiphenylamine

(Diphenylamine)63. 1,2-Diphenylhydrazine (as Azobenzene)64. 2,4,6-Tribromophenol (SS)65. 4-Bromophenyl phenyl ether66. Hexachlorobenzene67. Pentachlorophenol68. Phenanthrene-D10 (IS)69. Phenanthrene70. Anthracene

71. Carbazole72. di-n-Butyl phthalate73. Fluoranthene74. Benzidine75. Pyrene-d10 (SS)76. Pyrene77. p-Terphenyl-d14 (SS)78. 3,3'-Dimethylbenzidine79. Butyl benzyl phthalate80. Bis(2-ethylhexyl) adipate81. 3,3'-Dichlorobenzidine82. Benz[a]anthracene83. Bis(2-ethylhexyl)phthalate84. Chrysene-D12 (IS)85. Chrysene86. Di-n-octyl phthalate87. Benzo[b]fluoranthene88. Benzo[k]fluoranthene89. Benzo[a]pyrene90. Perylene-D12 (IS)91. Dibenz[a,h]anthracene92. Indeno[1,2,3-cd]pyrene93. Benzo[ghi]perylene

CCoolluummnn Rxi®-5Sil MS, 30 m, 0.25 mm ID, 0.25 µm (cat.# 13623)SSaammppllee 8270 MegaMix® (cat.# 31850)

Benzoic acid (cat.# 31879)8270 Benzidines Mix (cat.# 31852)Acid Surrogate Mix (4/89 SOW) (cat.# 31025)1,4-dioxane (cat.# 31853)Revised B/N Surrogate Mix (cat.# 31887)SV Internal Standard Mix (cat.# 31206)

Diluent: Methylene chlorideConc.: 40 µg/mL (4 ng on-column)IInnjjeeccttiioonnInj. Vol.: 1.0 µL split (split ratio 10:1)Liner: 4mm Split Precision® Liner w/ Semivolatiles Wool (cat.# 21023-231.5)Inj. Temp.: 270 °CSplit VentFlow Rate: 60 mL/min.

OOvveennOven Temp: 80 °C (hold 1 min.) to 280 °C at 25 °C/min. to 320 °C at 5 °C/min.CCaarrrriieerr GGaass He, constant flowFlow Rate: 1.2 mL/min.DDeetteeccttoorr MSMode: ScanTransferLine Temp.: 280 °CAnalyzer Type: QuadrupoleSource Temp.: 250 °CQuad Temp.: 150 °CTune Type: DFTPPIonization Mode: EIScan Range: 35-400 amuIInnssttrruummeenntt Agilent 7890A GC & 5975C MSD

Analyze more samples per shift with fast split injection

• Faster analyses than with typical splitless conditions.• Good resolution of late eluting compounds.

NEW!

Great peak shape for early eluters—

even with 80°C initial oven temp!


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Column: Rxi®-5Sil MS, 30m, 0.25mm ID, 0.25µm (cat.# 13623)

Sample: US EPA Method 8270D Mix, 1µL of 10µg/mL (IS 40µg/mL)8270 MegaMix® (cat.# 31850)Benzoic Acid (cat.# 31879)8270 Benzidines Mix (cat.# 31852)Acid Surrogate Mix (4/89 SOW) (cat.# 31025)Revised B/N Surrogate Mix (cat.# 31887)1,4-Dioxane (cat.# 31853)SV Internal Standard Mix (cat.# 31206)

Inj.: 1.0µL (10ng on-column concentration), 4mm Drilled Uniliner® (hole near bottom) inlet liner (cat.# 20756),pulsed splitless: pulse 25psi @ 0.2 min., 60mL/min. @ 0.15 min.

Inj. temp.: 250°CCarrier gas: helium, constant flowFlow rate: 1.2mL/min.Oven temp.: 40°C (hold 1.0 min.) to 280°C @ 25°C/min.

to 320°C @ 5°C/min. (hold 1 min.) Det.: MSTransfer line

temp: 280°CScan range: 35-550amuIonization: EIMode: scan


US EPA Method 8270

Rxi®-5Sil MS

1. 1,4-dioxane2. n-nitrosodimethylamine3. pyridinec. toluene4. 2-fluorophenol (SS)5. phenol-d6 (SS)6. phenol7. aniline8. bis(2-chloroethyl) ether9. 2-chlorophenol

10. 1,3-dichlorobenzene11. 1,4-dichlorobenzene-d4 (IS)12. 1,4-dichlorobenzene13. benzyl alcohol14. 1,2-dichlorobenzene 15. 2-methylphenol16. bis(2-chloroisopropyl) ether

17. 4-methylphenol/3-methylphenol18. n-nitroso-di-n-propylamine19. hexachloroethane20. nitrobenzene-d5 (SS)21. nitrobenzene22. isophorone23. 2-nitrophenol 24. 2,4-dimethylphenol25. benzoic acid26. bis(2-chloroethoxy)methane27. 2,4-dichlorophenol28. 1,2,4-trichlorobenzene29. naphthalene-d8 (IS)30. naphthalene31. 4-chloroaniline32. hexachlorobutadiene33. 4-chloro-3-methylphenol

34. 2-methylnaphthalene35. 1-methylnaphthalene36. hexachlorocyclopentadiene37. 2,4,6-trichlorophenol38. 2,4,5-trichlorophenol39. 2-fluorobiphenyl (SS)40. 2-chloronaphthalene41. 2-nitroaniline42. 1,4-dinitrobenzene43. dimethyl phthalate44. 1,3-dinitrobenzene45. 2,6-dinitrotoluene46. 1,2-dinitrobenzene 47. acenaphthylene48. 3-nitroaniline49. acenaphthene-d10 (IS)50. acenaphthene

51. 2,4-dinitrophenol52. 4-nitrophenol53. 2,4-dinitrotoluene54. dibenzofuran55. 2,3,5,6-tetrachlorophenol56. 2,3,4,6-tetrachlorophenol57. diethyl phthalate58. 4-chlorophenyl phenyl ether59. fluorene60. 4-nitroanaline61. 4,6-dinitro-2-methylphenol62. n-nitrosodiphenylamine

(diphenylamine)63. 1,2-diphenylhydrazine (as

azobenzene)64. 2,4,6-tribromophenol (SS)65. 4-bromophenyl phenyl ether

66. hexachlorobenzene67. pentachlorophenol68. phenanthrene-d10 (IS)69. phenanthrene70. anthracene71. carbazole72. di-n-butyl phthalate73. fluoranthene74. benzidine75. pyrene-d10 (SS)76. pyrene77. p-terphenyl-d14 (SS)78. 3,3'-dimethylbenzidine79. butyl benzyl phthalate80. bis(2-ethylhexyl) adipate81. 3,3'-dichlorobenzidine82. benzo(a)anthracene

83. bis(2-ethylhexyl) phthalate84. chrysene-d12 (IS)85. chrysene86. di-n-octyl phthalate87. benzo(b)fluoranthene88. benzo(k)fluoranthene89. benzo(a)pyrene90. perylene-d12 (IS)91. indeno(1,2,3-cd)pyrene92. dibenzo(a,h)anthracene93. benzo(ghi)perylene

c = contaminant

GC_EV00943

EIC

88,74,79m/z

EIC

252m/z

Excellent

resolution

of PAHs

Excellent

peak shape

of pyridine

Excellent

response for

2,4-dinitrophenol

RF=0.245

EIC 184m/z

• Drilled Uniliner® liner,• 10ng each compound• Silarylene phase• 0.25μm film thickness


564 www.restek.com 800-356-1688 or 814-353-1300


Semivolatiles

GC_EV00944

Column: Rxi®-5Sil MS, 30m, 0.25mm ID, 0.5µm (cat.# 13638) Sample: US EPA Method 8270D Mix, 1µL of 10µg/mL (IS 40µg/mL)

8270 MegaMix® (cat.# 31850)Benzoic Acid (cat.# 31879)8270 Benzidines Mix (cat.# 31852)Acid Surrogate Mix (4/89 SOW) (cat.# 31025)Revised B/N Surrogate Mix (cat.# 31887)1,4-Dioxane (cat.# 31853)SV Internal Standard Mix (cat.# 31206)


Inj. temp.: 250°CCarrier gas: helium, constant flowFlow rate: 1.2mL/min.Oven temp.: 40°C (hold 1.0 min.) to 280°C @ 25°C/min. to 320°C @ 5°C/min. (hold 3.5 min.) Det.: MSTransfer line



US EPA Method 8270

Rxi®-5Sil MS

1. 1,4-dioxane2. n-nitrosodimethylamine3. pyridine4. 2-fluorophenol (SS)5. phenol-d6 (SS)6. phenol7. aniline8. bis(2-chloroethyl) ether9. 2-chlorophenol

10. 1,3-dichlorobenzene11. 1,4-dichlorobenzene-d4 (IS)12. 1,4-dichlorobenzene13. benzyl alcohol14. 2-methylphenol15. 1,2-dichlorobenzene 16. bis(2-chloroisopropyl) ether17. 4-methylphenol/

3-methylphenol

18. n-nitroso-di-n-propylamine19. hexachloroethane20. nitrobenzene-d5 (SS)21. nitrobenzene22. isophorone23. 2,4-dimethylphenol 24. benzoic acid25. 2-nitrophenol26. bis(2-chloroethoxy)methane27. 2,4-dichlorophenol28. 1,2,4-trichlorobenzene29. naphthalene-d8 (IS)30. naphthalene31. 4-chloroaniline32. hexachlorobutadiene33. 4-chloro-3-methylphenol34. 2-methylnaphthalene35. 1-methylnaphthalene

36. hexachlorocyclopentadiene37. 2,4,6-trichlorophenol38. 2,4,5-trichlorophenol39. 2-fluorobiphenyl (SS)40. 2-chloronaphthalene41. 2-nitroaniline42. 1,4-dinitrobenzene43. dimethyl phthalate44. 1,3-dinitrobenzene45. 2,6-dinitrotoluene46. 1,2-dinitrobenzene 47. acenaphthylene48. 3-nitroaniline49. acenaphthene-d10 (IS)50. 2,4-dinitrophenol 51. acenaphthene52. 4-nitrophenol53. 2,4-dinitrotoluene

54. dibenzofuran55. 2,3,5,6-tetrachlorophenol56. 2,3,4,6-tetrachlorophenol57. diethyl phthalate58. 4-chlorophenyl phenyl ether59. 4-nitroanaline60. fluorene 61. 4,6-dinitro-2-methylphenol62. n-nitrosodiphenylamine


(as azobenzene)64. 2,4,6-tribromophenol (SS)65. 4-bromophenyl phenyl ether66. hexachlorobenzene67. pentachlorophenol68. phenanthrene-d10 (IS)69. phenanthrene

70. anthracene71. carbazole72. di-n-butyl phthalate73. fluoranthene74. benzidine75. pyrene-d10 (SS)76. 3,3'-dimethylbenzidine 77. pyrene 78. p-terphenyl-d14 (SS)79. butyl benzyl phthalate 80. bis(2-ethylhexyl) adipate81. bis(2-ethylhexyl) phthalate 82. 3,3'-dichlorobenzidine83. benzo(a)anthracene84. chrysene-d12 (IS)85. chrysene86. di-n-octyl phthalate 87. benzo(b)fluoranthene

88. benzo(k)fluoranthene89. benzo(a)pyrene90. perylene-d12 (IS)91. indeno(1,2,3-cd)pyrene92. dibenzo(a,h)anthracene93. benzo(ghi)perylene

EIC

EIC

• Drilled Uniliner® liner• 10ng each compound• Silarylene phase• 0.5μm film thickness




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Semivolatiles


US EPA Method 8270

Rxi®-5Sil MS

1. 1,4-dioxane2. n-nitrosodimethylamine3. pyridine4. 2-fluorophenol (SS)5. phenol-d6 (SS)6. phenol7. aniline8. bis(2-chloroethyl) ether9. 2-chlorophenol

10. 1,3-dichlorobenzene11. 1,4-dichlorobenzene-d4 (IS)12. 1,4-dichlorobenzene13. benzyl alcohol14. 1,2-dichlorobenzene 15. 2-methylphenol16. bis(2-chloroisopropyl) ether17. 4-methylphenol/

3-methylphenol

18. n-nitroso-di-n-propylamine19. hexachloroethane20. nitrobenzene-d5 (SS)21. nitrobenzene22. isophorone23. 2-nitrophenol 24. 2,4-dimethylphenol25. bis(2-chloroethoxy)methane 26. benzoic acid27. 2,4-dichlorophenol28. 1,2,4-trichlorobenzene29. naphthalene-d8 (IS)30. naphthalene31. 4-chloroaniline32. hexachlorobutadiene33. 4-chloro-3-methylphenol34. 2-methylnaphthalene35. 1-methylnaphthalene

36. hexachlorocyclopentadiene37. 2,4,6-trichlorophenol38. 2,4,5-trichlorophenol39. 2-fluorobiphenyl (SS)40. 2-chloronaphthalene41. 2-nitroaniline42. 1,4-dinitrobenzene43. dimethyl phthalate44. 1,3-dinitrobenzene45. 2,6-dinitrotoluene46. 1,2-dinitrobenzene 47. acenaphthylene48. 3-nitroaniline49. acenaphthene-d10 (IS)50. acenaphthene 51. 2,4-dinitrophenol52. 4-nitrophenol53. dibenzofuran

54. 2,4-dinitrotoluene55. 2,3,5,6-tetrachlorophenol56. 2,3,4,6-tetrachlorophenol57. diethyl phthalate58. fluorene59. 4-chlorophenyl phenyl ether 60. 4-nitroanaline61. 4,6-dinitro-2-methylphenol62. n-nitrosodiphenylamine


(as azobenzene)64. 2,4,6-tribromophenol (SS)65. 4-bromophenyl phenyl ether66. hexachlorobenzene67. pentachlorophenol68. phenanthrene-d10 (IS)69. phenanthrene

70. anthracene71. carbazole72. di-n-butyl phthalate73. fluoranthene74. benzidine75. pyrene-d10 (SS)76. pyrene77. p-terphenyl-d14 (SS)78. 3,3'-dimethylbenzidine79. butyl benzyl phthalate80. bis(2-ethylhexyl) adipate81. benzo(a)anthracene 82. 3,3'-dichlorobenzidine83. chrysene-d12 (IS)84. chrysene 85. bis(2-ethylhexyl) phthalate86. di-n-octyl phthalate87. benzo(b)fluoranthene

88. benzo(k)fluoranthene89. benzo(a)pyrene90. perylene-d12 (IS)91. indeno(1,2,3-cd)pyrene92. dibenzo(a,h)anthracene93. benzo(ghi)perylene

Column: Rxi®-5Sil MS, 20m, 0.18mm ID, 0.18µm (cat.# 43602)

Sample: US EPA Method 8270D Mix, 1µL of 10µg/mL (IS 40µg/mL)8270 MegaMix® (cat.# 31850)Benzoic Acid (cat.# 31879)8270 Benzidines Mix (cat.# 31852)Acid Surrogate Mix (4/89 SOW) (cat.# 31025)Revised B/N Surrogate Mix (cat.# 31887)1,4-Dioxane (cat.# 31853)SV Internal Standard Mix (cat.# 31206)


Inj. temp.: 250°CCarrier gas: helium, constant flowFlow rate: 1.0mL/min.Oven temp.: 50°C (hold 0.5 min.) to 260°C @ 20°C/min.

to 280°C @ 5°C/min. to 330°C @ 20°C/min.(hold 1.0 min.)

Det.: MSTransfer line


GC_EV00945

EIC

EIC

• Drilled Uniliner® liner• 10ng each compound• Silarylene phase• 20m x 0.18mm ID x 0.18μm




93. 1,3,5-trinitrobenzene 94. phenacetin 95. 4-bromophenyl phenyl ether 96. hexachlorobenzene 97. atrazine 98. 4-aminobiphenyl 99. pentachlorophenol

100. pentachloronitrobenzene 101. propyzamide 102. phenanthrene 103. anthracene 104. carbazole 105. di-n-butylphthalate 106. 4-nitroquinoline-1-oxide 107. methapyriline 108. isodrin 109. fluoranthene 110. benzidine111. pyrene 112. Aramite (isomer) 113. p-terphenyl-d14 (SS) 114. Aramite (isomer) 115. dimethylaminoazobenzene

116. dichlorobenzilate 117. 3,3'-dimethylbenzidine 118. benzyl butyl phthalate 119. Kepone 120. bis(2-ethylhexyl)adipate 121. 2-acetylaminofluorene 122. 3,3'-dichlorobenzidine123. chrysene 124. benzo(a)anthracene 125. bis(2-ethylhexyl)phthalate 126. di-n-octyl phthalate 127. benzo(b)fluoranthene 128. 7,12-dimethylbenzo(a)anthracene 129. benzo(k)fluoranthene 130. benzo(a)pyrene 131. 3-methylcholanthrene 132. dibenzo(a,j)acridine 133. indeno(1,2,3-cd)pyrene 134. dibenzo(a,h)anthracene 135. benzo(ghi)perylene

566 www.restek.com 800-356-1688 or 814-353-1300


Semivolatiles


US EPA Method 8270-Appendix IX

Rxi®-5Sil MS

1. 1,4-dioxane 2. N-nitrosodimethylamine3. pyridine4. ethyl methacrylate 5. 2-picoline 6. N-nitrosomethylethylamine 7. methyl methanesulfonate 8. 2-fluorophenol 9. N-nitrosodiethylamine

10. ethyl methanesulfonate 11. benzaldehyde12. phenol13. aniline14. bis(2-chloroethyl)ether 15. pentachloroethane 16. 2-chlorophenol 17. 1,3-dichlorobenzene 18. 1,4-dichlorobenzene 19. benzyl alcohol 20. 1,2-dichlorobenzene 21. 2-methylphenol 22. bis(2-chloroisopropyl)ether 23. 4-methylphenol

Column: Rxi®-5Sil MS, 30m, 0.25mm ID, 0.25µm, w/10m Integra-Guard™ (cat.# 13623-127)

Sample: 8270 MegaMix® (cat.# 31850), Appendix IX Mix #1 (cat.# 31625), Appendix IX Mix #2 (cat.# 31806), Revised B/N Surrogate Mix (cat.# 31887), Acid Surrogate Mix (4/89 SOW) (cat.# 31025), 8270 Benzidines Mix (cat.# 31852)in methylene chloride, 10ng on-column

Inj.: 1.0µL pulsed splitless, pulse 20psi @ 0.3 min., 60mL/min. @ 0.25 min. 4mm single gooseneck inlet liner w/wool (cat.# 22405)

Inj. temp.: 275°CCarrier gas: helium, constant flow Flow rate: 1.2mL/min. Oven temp.: 50°C (hold 0.5 min.) to 260°C @ 20°C/min. to

280°C @ 5°C/min. to 340°C (hold 2 min.) @ 18°C/min.

Det: MSTransfer line temp.: 280°CScan range: 35-550Ionization: EIMode: scan

24. 3-methylphenol25. acetophenone 26. N-nitroso-di-n-propylamine 27. nitrosopyrrolydine 28. 4-nitrosomorpholine 29. o-toluidine 30. hexachloroethane 31. nitrobenzene-d5 (SS) 32. nitrobenzene 33. N-nitrosopiperidine 34. isophorone 35. 2-nitrophenol 36. 2,4-dimethylphenol 37. bis(2-chloroethoxy)methane 38. 2,4-dichlorophenol 39. α,α-dimethylphenylamine 40. 1,2,4-trichlorobenzene 41. naphthalene 42. 2,6-dichlorophenol 43. 4-chloroaniline 44. hexachloropropene 45. hexachlorobutadiene46. N-nitroso-n-butylamine

47. caprolactam48. 1,4-phenylenediamine 49. 4-chloro-3-methylphenol 50. isosafrole 51. 2-methylnaphthalene 52. 1-methylnaphthalene 53. hexachlorocyclopentadiene 54. 1,2,4,5-tetrachlorobenzene 55. isosafrole 56. 2,4,6-trichlorophenol 57. 2,4,5-trichlorophenol 58. 2-fluorobiphenyl (SS) 59. safrole 60. biphenyl 61. 2-chloronaphthalene 62. 1-chloronaphthalene 63. diphenyl ether 64. 2-nitroaniline 65. 1,4-naphthoquinone 66. 1,4-dinitrobenzene 67. dimethylphthalate 68. 1,3-dinitrobenzene 69. 2,6-dinitrotoluene

70. acenaphthylene 71. 1,2-dinitrobenzene 72. 3-nitroaniline 73. acenaphthene 74. 2,4-dinitrophenol 75. 4-nitrophenol 76. pentachlorobenzene 77. dibenzofuran 78. 2,4-dinitrotoluene 79. 1-naphthalamine 80. 2,3,4,6-tetrachlorophenol 81. 2,3,5,6-tetrachlorophenol 82. 2-naphthylamine 83. diethyl phthalate 84. fluorene 85. 4-chlorophenyl phenyl ether 86. 2-methyl-5-nitroaniline 87. 4-nitroaniline 88. 4,6-dinitro-2-methylphenol 89. diphenylamine 90. azobenzene 91. 2,4,6-tribromophenol (SS) 92. diallate

GC_EV01077



• Single gooseneck liner w/wool• 10ng on-column• Silarylene phase• 0.25mm ID, 10m Integra-Guard®


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Semivolatiles

• Splitless injection, 2.5ng each component• XLB phase• 0.18μm film thicknessColumn: Rtx®-XLB, 20m, 0.18mm ID, 0.18µm

(cat.# 42802)Sample: US EPA Method 8270D mix:

8270 MegaMix® (cat.# 31850), benzoic acid (cat.# 31415), benzidine (cat.# 31441),2,4-dinitrophenol (cat.# 31291), Acid Surrogate Mix (4/89 SOW) (cat.# 31063), B/N Surrogate Mix (4/89 SOW) (cat.# 31062)

Inj.: 0.5µL, 5ppm each analyte (2.5ng on column) (2.5ppm/1.25ng on column for 3-methylphenol and 4-methylphenol)2mm splitless cyclo double gooseneck inlet liner (cat.# 20907);splitless hold time 0.15 min.;pressure pulse: 0.20 min. @ 30psi

GC: Agilent 6890Inj. temp.: 270°CCarrier gas: heliumFlow rate: 1.2mL/min., constant flowOven temp.: 40°C (hold 0.5 min.) to 90°C @

14°C/min. (no hold) to 330°C @ 22°C/min. (hold 1 min.)

Det.: Agilent 5973 GC/MSTransfer line

temp.: 280°CScan range: 35–550amuSolvent delay: 1 min.Tune: DFTPPIonization: EI

1. pyridine2. N-nitrosodimethylamine3. 2-fluorophenol4. phenol-d65. phenol6. aniline7. 2-chlorophenol8. bis(2-chloroethyl)ether9. 1,3-dichlorobenzene

10. 1,4-dichlorobenzene-d411. 1,4-dichlorobenzene12. 1,2-dichlorobenzene13. benzyl alcohol14. 2-methylphenol15. bis(2-chloroisopropyl)ether16. hexachloroethane17a.4-methylphenol17b.3-methylphenol18. N-nitroso-di-n-propylamine

19. nitrobenzene-d520. nitrobenzene21. isophorone22. 2,4-dimethylphenol23. 2-nitrophenol24. benzoic acid25. bis(2-chloroethoxy)methane26. 2,4-dichlorophenol27. 1,2,4-trichlorobenzene28. naphthalene-d829. naphthalene30. hexachlorobutadiene31. 4-chloroanaline32. 4-chloro-3-methylphenol33. 2-methylnaphthalene34. hexachlorocyclopentadiene35. 1-methylnaphthalene36. 2,4,6-trichlorophenol37. 2,4,5-trichlorophenol

38. 2-fluorobiphenyl39. 2-chloronaphthalene40. 2-nitroaniline41. dimethylphthalate42. acenaphthylene43. 2,6-dinitrotoluene44. acenaphthene-d1045. 1,4-dinitrobenzene46. acenaphthene47. 1,3-dinitrobenzene48. 3-nitroaniline49. 1,2-dinitrobenzene50. 4-nitrophenol51. dibenzofuran52. 2,3,4,6-tetrachlorophenol53. 2,3,5,6-tetrachlorophenol54. 2,4-dinitrophenol55. diethyl phthalate56. 2,4-dinitrotoluene

57. 4-chlorophenyl phenyl ether58. fluorene59. diphenylamine60. 4-nitroaniline61. azobenzene62. 2,4,6-tribromophenol63. 4,6-dinitro-2-methylphenol64. 4-bromophenyl phenyl ether65. hexachlorobenzene66. pentachlorophenol67. phenanthrene-d1068. phenanthrene69. anthracene70. carbazole71. di-n-butylphthalate72. fluoranthene73. benzidine74. pyrene75. p-terphenyl-d14

76. benzyl butyl phthalate77. bis(2-ethylhexyl)adipate78. bis(2-ethylhexyl)phthalate79. benzo(a)anthracene80. chrysene-d1281. chrysene82. di-n-octyl phthalate83. benzo(b)fluoranthene84. benzo(k)fluoranthene85. benzo(a)pyrene86. perylene-d1287. indeno(1,2,3-cd)pyrene88. dibenzo(a,h)anthracene89. benzo(ghi)perylene


US EPA Method 8270D by GC/MS

Rtx®-XLB

GC_EV00747


568 www.restek.com 800-356-1688 or 814-353-1300


Semivolatiles

Column: Rxi®-5ms, 30m, 0.25mm ID, 0.25µm (cat.# 13423)Sample: US EPA Method 525.2 mix, 10µg/mL each analyte,

25µg/mL each internal standard and surrogate: Method 525.2 Semivolatile Mix (cat.# 31899), Organonitrogen Pesticide Mix #1 (cat.# 33012), Organonitrogen Pesticide Mix #2 (cat.# 33011), Organophosphate Pesticide Mix #1 (cat.# 33013), Nitrogen/Phosphorous Pesticide Mix #2 (cat.# 32423), Method 525.2 Internal Standard Mix (cat.# 31825), Method 525.2 Surrogate Standard Mix (cat.# 31826)

Instrument: Agilent 6890Inj.: 1.0µL, pulsed splitless injection: 50psi (0.3 min.), 80mL/min. (0.15 min.), gas saver 15mL/min. (1 min.),

4mm Drilled Uniliner® inlet liner, hole near bottom (cat.# 20771)Inj. temp.: 250°CCarrier gas: helium, constant flowFlow rate: 1.2mL/min.Oven temp.: 90°C (1 min.) to 270°C @ 20°C/min., to 315°C @ 6°C/min.Det.: Agilent 5973 MSDInterface line temp.: 280°CScan range: 35-550amuSolvent delay: 3.00 min.Tune: DFTPPIonization: EI

1. isophorone2. 2-nitro-m-xylene (SS)3. naphthalene4. dichlorvos (DDVP)5. hexachlorocyclopentadiene6. EPTC7. mevinphos8. butylate9. vernolate

10. dimethyl phthalate11. pebulate12. etridiazole (Terrazole®)13. 2,6-dinitrotoluene14. acenaphthylene15. acenaphthene-d10 (IS)16. chlorneb17. tebuthiuron18. 2,4-dinitrotoluene19. molinate20. diethyl phthalate21. fluorene22. propachlor23. ethoprop (ethoprophos)24. cycloate25. chlorpropham26. trifluralin27. atraton28. hexachlorobenzene29. prometon30. simazine31. atrazine32. propazine33. pentachlorophenol34. terbufos35. pronamide (propyzamide)36. diazinon37. phenanthrene-d10 (IS)38. phenanthrene39. disulfoton40. methyl paraoxon41. anthracene42. terbacil43. chlorothalonil44. metribuzin45. simetryn46. ametryn47. alachlor48. prometryn49. terbutryn50. di-n-butyl phthalate51. bromacil52. cyanazine (Bladex)53. metolochlor54. chlorpyrifos (Dursban®)55. triademefon56. Dacthal® (DCPA)57. MGK-264 (isomer A)58. diphenamid59. MGK-264 (isomer B)60. merphos61. heptachlor epoxide62. fluoranthene63. stirofos64. disulfoton sulfone65. butachlor66. pyrene-d10 (SS)67. fenamiphos68. pyrene69. napropamide (Devrinol®)70. trans-nonachlor71. merphos oxide72. tricyclazole (Beam)73. carboxin74. chlorobenzilate75. benzyl butyl phthalate76. norflurazon77. bis(2-ethylhexyl) adipate78. hexazinone (Velpar®)79. triphenylphosphate (SS)80. benzo(a)anthracene81. chrysene-d12 (IS)82. chrysene83. bis(2-ethylhexyl) phthalate84. fenarimol85. cis-permethrin86. trans-permethrin87. di-n-octyl phthalate88. benzo(b)fluoranthene89. benzo(k)fluoranthene90. benzo(a)pyrene91. fluridone (Sonar®)92. perylene-d12 (SS)93. indeno(1,2,3-cd)pyrene94. dibenzo(a,h)anthracene95. benzo(ghi)perylene

GC_EV00859

Semivolatile

Organics

US EPA

Method 525.2

Rxi®-5ms

Low bleed

at 315°C!

• Drilled Uniliner® liner• 10ng each compound• diphenyl phase• 0.25μm film thickness




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Pesticides

Organochlorine Pesticide Mix AB #2

US EPA Method 8081

Rtx®-CLPesticides and Rtx®-CLPesticides2 (0.53mm ID Column Set)

Columns: Rtx®-CLPesticides, 30m, 0.53mm ID, 0.50µm (cat.# 11140) andRtx®-CLPesticides2, 30m, 0.53mm ID, 0.42µm (cat.# 11340) with5m x 0.53mm ID Rxi® deactivated guard tubing (cat.# 10054), connected using Siltek® Treated Universal “Y” Press-Tight® connector (cat.# 20486)

Sample: Organochlorine Pesticide Mix AB #2, 8-80µg/mL each component in hexane/toluene (cat.# 32292), Pesticide Surrogate Mix, 200µg/mL each component in acetone (cat.# 32000)

Inj.: 1.0µL splitless (hold 0.3 min.), 4mm single gooseneck inlet liner (cat.# 20799)Inj. temp.: 250°CCarrier gas: helium, constant flow Linear velocity: 45cm/sec. @ 120°COven temp.: 120°C to 200°C @ 45°C/min. to 230°C @ 12.5°C/min. to

320°C (hold 2 min.) @ 20°C/min.Det.: µ-ECD @ 330°C

1. 2,4,5,6-tetrachloro-m-xylene (SS)2. α-BHC3. γ-BHC4. β-BHC5. δ-BHC6. heptachlor7. aldrin8. heptachlor epoxide (isomer B)9. γ-chlordane

10. α-chlordane11. endosulfan I

12. 4,4'-DDE13. dieldrin14. endrin15. 4,4'-DDD16. endosulfan II17. 4,4'-DDT18. endrin aldehyde19. endosulfan sulfate20. methoxychlor21. endrin ketone22. decachlorobiphenyl (SS)

GC_EV00937GC_EV00936

Rtx®-CLPesticides2Rtx®-CLPesticides


US EPA Method 8081

Rtx®-CLPesticides and Rtx®-CLPesticides2 (0.32mm ID Column Set)

Columns: Rtx®-CLPesticides, 30m, 0.32mm ID, 0.32µm (cat.# 11141) and Rtx®-CLPesticides2, 30m, 0.32mm ID, 0.25µm (cat.# 11324) with5m x 0.32mm ID Rxi® deactivated guard tubing (cat.# 10039), connected using Deactivated Universal “Y” Press-Tight® connector (cat.# 20405-261)

Sample: Organochlorine Pesticide Mix AB #2, 8-80µg/mL each component in hexane/toluene (cat.# 32292), Pesticide Surrogate Mix, 200µg/mL each component in acetone (cat.# 32000)

Inj.: 1.0µL splitless (hold 0.3 min.), 4mm single gooseneck inlet liner (cat.# 20799)Inj. temp.: 250°CCarrier gas: helium, constant flow Linear velocity: 60cm/sec. @ 120°COven temp.: 120°C to 200°C @ 45°C/min. to 230°C @ 15°C/min. to 330°C (hold 2 min.)

@ 30°C/min.Det.: µ-ECD @ 330°C




GC_EV00933 GC_EV00933A

Rtx®-CLPesticides2Rtx®-CLPesticides

0.53mm ID column analysis

performed in less than 9 min.

0.32mm ID column analysis

performed in less than 7 min.

569-582_GCappPest.qxp 11/22/2010 9:05 PM Page 569

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Pesticides


US EPA Method 8081

Rtx®-CLPesticides and Rtx®-CLPesticides2 (0.25mm ID column set)

Columns: Rtx®-CLPesticides, 30m, 0.25mm ID, 0.25µm (cat.# 11123) and Rtx®-CLPesticides2, 30m, 0.25mm ID, 0.20µm (cat.# 11323) with 5m x 0.25mm ID Rxi® deactivated guard tubing (cat.# 10029), connected using Siltek®-treated Universal “Y” Press-Tight® Connector (cat.# 20486)

Sample: Organochlorine Pesticide Mix AB #2, 8–80µg/mL each component in hexane/toluene (cat.# 32292), Pesticide Surrogate Mix, 200µg/mL each component in acetone (cat.# 32000)

Inj.: 0.5µL splitless (hold 0.5 min.), 2mm Cyclo Double Gooseneck inlet liner (cat.# 20908)Inj. temp.: 250°CCarrier gas: helium, constant flowLinear velocity: 41cm/sec. @ 125°COven temp.: 125°C to 200°C @ 45°C/min. to 230°C @ 12.5°C/min. to

330°C (hold 2 min.) @ 30°C/min.Det.: µ-ECD @ 330°C




GC_EV00940 GC_EV00941

Rtx®-CLPesticides Rtx®-CLPesticides2

GC_EV00892 GC_EV00893

Columns: Rtx®-CLPesticides, 20m, 0.18mm ID, 0.18µm (cat.# 42102) andRtx®-CLPesticides2, 20m, 0.18mm ID, 0.14µm (cat.# 42302) with 5m x 0.53mm ID intermediate-polarity deactivated guard tubing (cat.# 10045), connected using SeCure® “Y” Connector Kit (cat.# 20276) with Universal “Y” Press-Tight® Connector

Sample: Organochlorine Pesticide Mix AB #2 (cat.# 32292), 8-80µg/mL each component in hexane/toluene, Pesticide Surrogate Mix (cat.# 32000), 200µg/mL each component in acetone

Inj.: 0.5µL splitless (hold 0.75 min.), 2mm single gooseneck inlet liner (cat.# 20796)Inj. temp.: 250°CCarrier gas: helium, constant flowLinear velocity: 20cm/sec. @ 140°COven temp.: 140°C (hold 1 min.) to 250°C @ 35°C/min. (hold 1 min.) to 330°C @

35°C/min. (hold 3 min.)Det.: µ-ECD @ 350°C

Organochlorine Pesticides

US EPA Method 8081

Rtx®-CLPesticides and Rtx®-CLPesticides2 (0.18mm ID column set)

1. 2,4,5,6-tetrachloro-m-xylene (SS)2. α-BHC3. γ-BHC4. β-BHC5. δ-BHC6. heptachlor7. aldrin8. heptachlor epoxide9. γ-chlordane



Rtx®-CLPesticides Rtx®-CLPesticides2

Dual column

analysis in less

than 8 minutes!


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Pesticides

Pesticides & Herbicides

US EPA Method 505


1. hexachlorocyclopentadiene2. hexachlorobenzene3. simazine4. atrazine5. γ-BHC6. heptachlor7. alachlor8. aldrin9. heptachlor epoxide

10. γ-chlordane11. trans-nonachlor12. α-chlordane13. dieldrin14. endrin15. cis-nonachlor16. methoxychlor

Column: Rtx®-CLPesticides2, 30m, 0.32mm ID, 0.25µm (cat.# 11324) andRtx®-CLPesticides, 30m, 0.32mm ID, 0.32µm (cat.# 11141) with5m x 0.32mm ID Rxi® deactivated guard tubing (cat.# 10039), connected using Universal “Y” Press-Tight® Connector (cat.# 20405-261)

Sample: 200ng/mL 505 Organohalide Pesticide Mix (cat.# 32024), 4.2µg/mL Simazine (cat.# 32236), 4.2µg/mL Atrazine (cat.# 32208) in methanol

Inj.: 2µL splitless (hold 0.75 min.), 4mm cyclo double gooseneck liner (cat.# 20896)Inj. temp.: 250°CCarrier gas: helium, constant flowLinear velocity: 40cm/sec. @ 90°COven temp.: 90°C (hold 1 min.) to 310°C (hold 5 min.) @ 10°C/min. Det. temp.: µ-ECD @ 325°C

GC_EV01004

GC_EV01005

Rtx®-CLPesticides

Rtx®-CLPesticides2


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Pesticides

GC_EV01023

GC_EV01022

1. hexachlorocyclopentadiene2. etridiazole3. chloroneb4. propachlor5. trifluralin6. hexachlorobenzene7. α-BHC8. simazine9. atrazine

10. pentachloronitrobenzene (IS)11. γ-BHC12. β-BHC13. δ-BHC14. heptachlor15. chlorothalonil16. metribuzin17. alachlor18. aldrin19. 4,4'-dibromobiphenyl (SS)20. metachlor21. DCPA22. heptachlor epoxide23. γ-chlordane24. cyanazine25. α-chlordane26. endosulfan I27. 4,4'-DDE28. dieldrin29. endrin30. chlorobenzilate31. 4,4'-DDD32. endosulfan II33. 4,4'-DDT34. endrin aldehyde35. endosulfan sulfate36. methoxychlor37. cis-permethrin38. trans-permethrin

Column: Rtx®-CLPesticides2, 30m, 0.32mm ID, 0.25µm (cat.# 11324) and Rtx®-CLPesticides, 30m, 0.32mm ID, 0.32µm (cat.# 11141) with 5m x 0.32mm ID Rxi® deactivated guard tubing (cat.# 10039), connected using Universal “Y” Press-Tight® Connector (cat.# 20405-261)

Sample: 50ng/mL 508.1 Calibration Mix #1 (cat.# 32094), 100ng/mL 508.1 Calibration Mix #2 (cat.# 32095), 100ng/mL 508.1 Calibration Mix #3 (cat.# 32096), 50ng/mL 508.1 Internal Standard (cat.# 32091), 250ng/mL 508.1 Surrogate (cat.# 32092), 500ng/mL Atrazine (cat.# 32208), 500ng/mL Simazine (cat.# 32236) in ethyl acetate

Inj.: 2µL splitless (hold 0.75 min.), 4mm cyclo double gooseneck liner (cat.# 20896)

Inj. temp.: 250°CCarrier gas: helium, constant flowLinear velocity: 26cm/sec. @ 80°COven temp.: 80°C (hold 0.5 min.) to 155°C (hold 1 min.) @

19°C/min. to 210°C @ 4°C/min. to 310°C (hold 0.5 min.) @ 25°C/min.

Detector temp.: µ-ECD @ 325°C

Rtx®-CLPesticides

Rtx®-CLPesticides2

Pesticides & Herbicides

US EPA Method 508.1



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Pesticides

Organophosphorus Pesticides

US EPA Method 8141A

Rtx®-OPPesticides2

GC_EV00602

1. dichlorvos2. hexamethylphosphoramide3. mevinphos4. trichlorfon5. TEPP6. demeton-O7. thionazin8. tributyl phosphate (IS)9. ethoprop

10. naled11. sulfotepp12. phorate13. dicrotophos14. demeton-S15. monocrotophos16. terbufos17. dimethoate18. dioxathion

19. fonophos20. diazinon21. disulfoton22. phosphamidon isomer 23. dichlorofenthion24. chlorpyrifos methyl25. phosphamidon26. parathion-methyl27. ronnel28. fenitrothion29. aspon30. malathion31. chlorpyrifos32. trichloronate33. parathion-ethyl34. fenthion35. merphos36. chlorfenvinphos

37. crotoxyphos38. stirofos39. tokuthion40. merphos oxone

(breakdown product) 41. ethion42. fensulfothion43 bolstar44. carbophenothion45. famphur46. triphenyl phosphate (SS)47. EPN48. phosmet49. leptophos50. tri-o-cresyl phosphate51. azinphos-methyl52. azinphos-ethyl 53. coumaphos

Column: Rtx®-OPPesticides2, 30m, 0.25mm ID, 0.25µm (cat.# 11243)Sample: US EPA Method 8141A Custom Standard Mix 1µL 100ppm

(100ng on column) Triphenylphosphate Standard (cat.# 32281)Tributylphosphate Standard (cat.# 32280)8140/8141 OP Pesticides Calibration Mix A (cat.# 32277)8141 OP Pesticides Calibration Mix B (cat.# 32278)Custom Mixes: Call Restek for Information

Inj.: 1.0µL splitless (hold 0.4 min.), 4mm doublegooseneck inlet liner (cat.# 20785)

Inj. temp.: 250°CCarrier gas: helium, constant flow Flow rate: 1.0mL/min. Oven temp.: 80°C (hold 0.5 min.) to 140°C @ 20°C/min.

to 210°C @ 4°C/min. (hold 1 min.) to 280°C @ 30°C (hold 5 min.)

Det: MSTransfer line temp.: 280°CScan range: 35-400amuIonization: EI

Best column for most

resolved compounds

for Method 8141A.



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Pesticides

GC: splitless, purge on 1.0 min. constant pressureOven temp.: 80°C (hold 0.5 min.) to 280°C

@ 12°C/min. (hold 10 min.)Injector: 200°CInlet liner: 4mm Siltek® single gooseneck inlet linerDetector: FPD @ 250°CDead time: 1.03 min. @ 80°CInjection: 1µL US EPA Method 8141A Custom

Standard Mixes (100ng/mL)Triphenylphosphate Standard (cat.# 32281)Tributylphosphate Standard (cat.# 32280)8140/8141 OP Pesticides Calibration Mix A (cat.# 32277)8141 OP Pesticides Calibration Mix B (cat.# 32278)

Dual-column injector


US EPA Method 8141A

Rtx®-OPPesticides &

Rtx®-OPPesticides2

1. dichlorvos2. hexamethylphosphoramide3. mevinphos4. trichlorfon5. TEPP6. demeton-O7. tributyl phosphate (SS)8. thionazin9. ethoprop

10. naled11. sulfotepp12. phorate13. dicrotophos14. monocrotophos15. demeton-S16. terbufos17. dimethoate18. diazinon19. dioxathion20. fonophos21. disulfoton22. phosphamidon isomer

(breakdown product)23. dichlorofenthion24. phosphamidon25. chlorpyrifos methyl26. parathion-methyl27. ronnel28. aspon29. fenitrothion30. malathion31. chlorpyrifos32. trichloronate33. parathion-ethyl34. fenthion35. merphos36. chlorfenvinphos37. crotoxyphos38. stirofos39. tokuthion40. merphos oxone

(breakdown product)41. ethion42. fensulfothion43. bolstar44. carbophenothion45. famphur46. triphenyl phosphate (SS)47. EPN48. phosmet49. leptophos50. tri-o-cresyl phosphate51. azinphos-methyl52. azinphos-ethyl53. coumaphos

1

2

3

4

5

6

7

8

9

10

11

12

13

14

15

16

1718

19,20

21

22

23

24

25

26

27

28

29

31

32,33

5352

5150

49

4847

46

45

44

43

42

41

40

39

38

37

36

35

34

30

1

2 4

3

6

8

9

12

10,11

7

18

16

5,20

19,21

15

13,14

31

28

32

26,30

29

22

23

25

17

27,35

34

39

24

36,33

40

3837

43

44,41

46

4942

50

47,48

45

51

52

53

min. 8 10 12 14 16 18 20 22

min. 6 8 10 12 14 16 18 20

Rtx®-OPPesticides30m, 0.32mm ID, 0.50μm(cat.# 11239)

Rtx®-OPPesticides230m, 0.32mm ID, 0.32μm(cat.# 11241)

GC_EV00394


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Pesticides


US EPA Method 8140/8141/8141A

Rtx®-CLPesticides

Column: Rtx®-CLPesticides, 30m, 0.32mm ID, 0.50µm (cat.# 11139)Sample: 1µL US EPA Method 8141A custom standard mixes (200ng/mL)

Triphenylphosphate Standard (cat.# 32281)Tributylphosphate Standard (cat.# 32280)8140/8141 OP Pesticides Calibration Mix A (cat.# 32277)8141 OP Pesticides Calibration Mix B (cat.# 32278)

Splitless hold time: 1 min.Oven temp.: 100°C to 180°C @ 10°C/min.

(hold 2 min.), to 300°C @18°C/min. (hold 3 min.)

Inj./det. temp.: 250°C/280°C FPD

min. 2 4 6 8 10 12 14 16 18

1

2

3

4

5

6

7

8

9

10, 11, 12

13,14,15

16,17,18

19,20,21 2223

24

25

26

27

28

29,30

3132

3334

35

36

37

38

39,40

41

42

43

44,45

46

4748

49

50

51 52

53

1. dichlorvos2. hexamethylphosphoramide3. trichlorfon4. mevinphos5. demeton-O6. thionazin7. ethoprop8. phorate9. naled

10. tributyl phosphate (SS)11. TEPP

12. sulfotepp13. demeton-S14. terbufos15. fonophos16. dicrotophos17. diazinon18. disulfoton19. dioxathion20. monocrotophos21. dimethoate22. dichlorofenthion

23. chlorpyrifos methyl24. ronnel25. phosphamidon isomer26. merphos27. chlorpyrifos28. fenthion29. aspon30. parathion-methyl31. trichloronate32. malathion33. fenitrothion

34. phosphamidon35. parathion-ethyl36. chlorfenvinphos37. tokuthion38. merphos oxone39. crotoxyphos40. stirofos41. bolstar42. famphur43. carbophenothion44. fensulfothion

45. triphenyl phosphate (SS)46. leptophos47. ethion48. phosmet49. EPN50. tri-o-cresyl phosphate51. azinphos-methyl52. azinphos-ethyl53. coumaphos

GC_EV00413


US EPA Method 8140/8141/8141A

Rtx®-CLPesticides2

2 4 6 8 10 12 14 16 18 min.

1

2

3

4

5

6

7

8,9

10

11

12

13,14,15

16

17

1819

20,21

22

23

2425

26

27

2829,30

31

32,33,34

35

3637 38

39,40

41

42

43

44

45,46

47

48,49

51 5253

1. dichlorvos2. hexamethylphosphoramide3. mevinphos4. trichlorfon5. demeton-O6. thionazin7. tributyl phosphate (SS)8. ethoprop9. TEPP

10. naled11. phorate

12. sulfotepp13. demeton-S14. dicrotophos15. dioxathion16. terbufos17. monocrotophos18. fonophos19. diazinon20. disulfoton21. dimethoate22. dichlorofenthion

23. phosphamidon isomer24. chlorpyrifos methyl25. ronnel26. parathion-methyl27. phosphamidon28. aspon29. chlorpyrifos30. trichloronate31. merphos32. fenitrothion33. fenthion

34. malathion35. parathion-ethyl36. chlorfenvinphos37. crotoxyphos38. tokuthion39. merphos oxone40. stirofos41. famphur42. bolstar43. carbophenothion44. fensulfothion

45. triphenyl phosphate (SS)46. ethion47. EPN48. phosmet49. leptophos50. tri-o-cresyl phosphate51. azinphos-methyl52. azinphos-ethyl53. coumaphos

Column: Rtx®-CLPesticides2, 30m, 0.32mm ID, 0.25µm (cat.# 11324)

Sample: 1µL US EPA Method 8141A custom standard mixes (200ng/mL)Triphenylphosphate Standard (cat.# 32281)Tributylphosphate Standard (cat.# 32280)8140/8141 OP Pesticides Calibration Mix A (cat.# 32277)8141 OP Pesticides Calibration Mix B (cat.# 32278)

Splitless hold time: 1 min.Oven temp.: 100°C to 180°C @

10°C/min. (hold 2 min.), to 300°C @ 18°C/min. (hold 3 min.)

Inj./det. temp.: 250°C/280°C FPD

GC_EV00414

50


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Pesticides

GC_EV00676

Column: Rtx®-CLPesticides, 30m, 0.32mm ID, 0.50µm (cat.# 11139)Sample: European OPP Mix (cat.# 32418)

100–1000µg/mL in acetone Inj.: 0.5µL direct, open-top Siltek® Drilled Uniliner®

inlet liner (cat.# 21055-214.5)Inj. temp.: 250°CCarrier gas: helium, constant pressure Linear velocity: 35cm/sec. @ 80°COven temp.: 80°C (hold 1 min.) to 150°C @ 7°C/min.

to 280°C @ 15°C/min. (hold 10 min.)Det.: FPD @ 280°C

CCoonncceennttrraattiioonnoonn--ccoolluummnn ((nngg))

1. methamidophos 1.252. dichlorvos 1.253. acephate 0.504. demeton-S-methyl 0.505. tributylphosphate (IS) 1.256. omethoate 2.507. dimethoate 0.508. tolclofos-methyl 0.259. pirimiphos methyl 0.25

10. chlorpyriphos 0.2511. malathion 0.5012. tokuthion 0.5013. methidathion 0.5014. profenfos 0.5015. ethion 0.5016. triphenylphosphate (SS) 1.2517. azinphos-methyl 1.0018. pyrazophos 1.25

Organophosphorus Pesticides (European)

Rtx®-CLPesticides


Solutions Online



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Pesticides

Organophosphorus Pesticides (European)

Rtx®-CLPesticides

GC_EV00648

Column: Rtx®-CLPesticides, 30m, 0.25mm ID, 0.25µm (cat.# 11123)Sample: Custom European Mix

1-bromo-2-nitrobenzene (cat.# 32279)4-chloro-3-nitrobenzotrifluoride (cat.# 32282)tributylphosphate (cat.# 32280)triphenylphosphate (cat.# 32281)

Inj.: 1.0µL splitless (hold 0.4 min.)4mm double gooseneck inlet liner (cat.# 20785)

Inj. temp.: 250°CCarrier gas: helium, constant flow, 6psi head pressure Flow rate: 0.75mL/min.Linear velocity: 28cm/sec.* Dead time: 1.82 min. @ 80°C Oven temp.: 80°C (hold 1.0 min.) to 150°C @ 7°C/min. (no hold)

to 280°C @ 15°C/min. (hold 7 min.) Det.: Agilent 5971A GC/MSTransfer line temp.: 280°CScan range: 35–400amuSolvent Delay 5 min.Tune PFTBAIonization: EI

*This mix was prepared for FPD analyses. Peaks will be equivalent height with FPDdetection if linear velocity is set at 28cm/sec. (0.32mm ID column).

CCoommppoouunndd CCoonncc.. oonn--ccoolluummnn ((nngg))1. 4-chloro-3-nitro-trifluoride 1002. methamidophos 503. dichlorvos 504. 1-bromo-2-nitrobenzene 1005. acephate 206. demeton-S-methyl 207. TBP (IS) 1008. omethoate 1009. dimethoate 20

10. tolclofos-methyl 1011. pirimiphos methyl 1012. chlorpyrifos 1013. malathion 2014. quinalphos 1015. tokuthion (prothiofos) 2016. methidathion 2017. profenfos 2018. ethion 2019. TPP (SS) 10020. azinphos-methyl 4021. pyrazophos 50



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Pesticides/Herbicides

1

2

34

5

7

6

Columns: Rtx®-CLPesticides, 30m, 0.32mm ID, 0.50µm (cat.# 11139) andRtx®-CLPesticides2, 30m, 0.32mm ID, 0.25µm (cat.# 11324)with a 5m, 0.32mm ID guard column (cat.# 10044) and a “Y” Press-Tight® connector (cat.# 20403)

Inj.: Direct injection using a Uniliner® inlet liner (cat.# 20964) and adaptor for an Agilent 5890 (cat.#21303)Conc.: On-column, 50pg each compoundOven temp.: 100°C (hold 0 min.) to 250°C @ 4°C/min. (hold 5 min.)Inj./det. temp.: 250°C/275°CCarrier gas: hydrogen, 9.65psi constant pressureGC: Agilent 6890 with purged packed injection portDet: NPD

Rtx®-CLPesticides

8

min. 18 19 20 21 22 23

9 10 11

CAS No.1. prometon 1610-18-0 2. simazine 122-34-93. atraton 1610-17-94. propazine 139-40-25. atrazine 1912-24-96. terbuthylazine 5915-41-37. secbumeton 26259-45-08. simetryne 1014-70-69. ametryne 834-12-8

10. prometryne 7287-19-611. terbutryne 886-50-0

Nitrogen/Phosphorus Pesticides & Herbicides

US EPA Method 619

Rtx®-CLPesticides & Rtx®-CLPesticides2 (dual column analysis)

1

2

3

4

5

7

6

8

min. 18 19 20 21 22 23

9

10 11

Rtx®-CLPesticides2

GC_EV00056


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Herbicides

Column: Rtx®-CLPesticides2, 30m, 0.32mm ID, 0.25µm (cat.# 11324) andRtx®-CLPesticides, 30m, 0.32mm ID, 0.32µm (cat.# 11141), with5m x 0.32mm ID Rxi® deactivated guard tubing (cat.# 10039),connected using Deactivated Universal “Y” Press-Tight® Connector (cat.# 20405-261)

Sample: 200ng/mL Herbicide Mix #1 (cat.# 32055) in hexane1,000ng/mL Herbicide Mix #2 (cat.# 32057) in hexane20,000ng/mL Herbicide Mix #3 (cat.# 32059) in hexane 200ng/mL Herbicide Mix #4 (cat.# 32062) in hexane 250ng/mL Herbicide Internal Standard (cat.# 32053) in hexane 400ng/mL Herbicide Surrogate (cat.# 32050) in hexane

Inj.: 1.0µL splitless (hold 0.75 min.), 4mm Cyclo Double Gooseneck inlet liner (cat.# 20895)

Inj. temp.: 250°CCarrier gas: helium, constant pressureFlow rate: 36cm/sec. @ 70°COven temp.: 70°C (hold 0.5 min.) to 190°C @ 25°C/min. (hold 1 min.) to 300°C @ 11°C/min. (hold 5 min.)Det.: µ-ECD @ 325°C

Rtx®-CLPesticides

Rtx®-CLPesticides2

1. dalapon methyl ester2. 3,5-dichlorobenzoic acid methyl ester (SS)3. 4-nitroanisole 4. DCAA methyl ester (SS)5. dicamba methyl ester6. MCPP methyl ester7. MCPA methyl ester8. dichlorprop methyl ester9. 4,4'-DBOB (IS)

10. 2,4-D methyl ester11. pentachloroanisole12. 2,4,5-TP methyl ester13. 2,4,5-T methyl ester14. chloramben methyl ester15. 2,4-DB methyl ester16. dinoseb methyl ester17. bentazon methyl ester18. DCPA 19. picloram methyl ester20. acifluorfen methyl esterC. contaminant

Herbicides

US EPA Method 8151A


GC_EV00971

GC_EV00971A

<13 min.

chlorophenoxyacid

herbicide analysis!

Fully resolve bentazon and

picloram methyl esters


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Herbicides

Chlorophenoxyacid Herbicides

US EPA Method 615

Rtx®-5

min. 5 10 15 20 25 30GC_EV00095

Column: Rtx®-5, 30m, 0.53mm ID, 0.50µm (cat.# 10240)Sample: 0.5µL direct injection of chlorophenoxy herbicides,

on-column concentration 10–10,000µg/mLOven temp.: 60°C to 150°C @ 8°C/min. (hold 5 min.),

to 210°C @ 4°C/min.Inj./det. temp.: 250°C/275°CCarrier gas: heliumLinear velocity: 35cm/sec. set @ 60°CDet.: ECD w/anode purge

1 2

3

4

5

7

8 6

910

12

11

1. dalapon2. DCAA (SS)3. dicamba4. MCPP5. MCPA6. DBOB (IS)7. dichlorprop8. 2,4-D9. 2,4,5-TP

10. 2,4,5-T11. dinoseb12. 2,4-DB

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Increase productivity by improving separations and shortening analysis time with opti-mized temperature and carrier gas programs. Pro ezGC software for Windows® operat-ing systems accurately models analyses when using guard columns and capillary restric-tors, even when their IDs differ from the analytical column. The power of Pro ezGCsoftware is especially helpful when modeling two columns connected in series or twocolumns connected in parallel to two separate detectors.

Pro ezGC includes a master set of retention index libraries at no extra charge! Theselibraries contain more than 3,000 compounds analyzed on the most commonly usedstationary phases, in ten application areas, including pesticides, PCBs, dioxins/furans,flavor and fragrance compounds, drugs of abuse, FAMEs, semivolatile and volatile pol-lutants, petroleum hydrocarbons, and solvents and chemicals. The libraries permitcomputer simulation without entering actual laboratory data.

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Herbicides

Triazine Herbicides

US EPA Method 619

Rtx®-50, Rtx®-200

min. 10 12 14 16

GC_EV00058

1

11

10

9

7

8

6

5

43

2

1. atraton2. prometon3. terbutylazine4. atrazine5. simazine6. propazine7. secbumeton8. terbutryne9. ametryne

10. simetryne11. prometryne

Sample: 0.5µL direct injection of EPA Method 619 - triazine herbicides.

Conc.: on-column, 50ngOven temp.: 150°C to 250°C

@ 4°C/min. (hold 5 min.)Inj./det. temp.: 250°C/275°CDetector: TSDCarrier gas: heliumLinear velocity: 40cm/sec. set @ 150°C

Rtx®-50

30m, 0.53mm ID, 0.50μm (cat.# 10540)

Rtx®-200

30m, 0.53mm ID, 0.50μm(cat.# 15040)

10

9,11

8

6

54

3,7

2

1

GC_EV00059min. 4 6 8 10

Nitrogen-Containing Herbicides

Rtx®-35

GC_EV00088

min. 2 4 6 8 10 12 14 16 18 20

1 2 34 5

6

89

10 1112

1314

15

16

17

18,19

20 21 22

Column: Rtx®-35, 30m, 0.53mm ID, 0.50µm (cat.# 10440)Inj.: 0.2µL direct injection, Uniliner® inlet liner,

approximately 10ng per component.Oven temp.: 60°C (hold 1 min.) to 290°C

@ 15°C/min. (hold 5 min.)Inj./det. temp.: 290°CCarrier gas: heliumLinear velocity: 40cm/sec. (flow rate: 5.2cc/min.) FID sensitivity: 16 x 10-11 AFS

1. Eptam®

2. Sutan®

3. Vernam4. Tillam5. Ordram®

6. Treflan®

7. Balan®

8. Ro-Neet9. propachlor

10. Tolban11. propazine

12. atrazine13. simazine14. terbacil15. Sencor®

16. Dual®

17. Paarlan18. Prowl19. bromacil20. oxadiazon21. GOAL®

22. hexazinone7


582 www.restek.com 800-356-1688 or 814-353-1300


Herbicides

Triazine Herbicides (French) & Degradation Products

Rtx®-OPPesticides2

GC_EV00626

PPeeaakk LLiisstt:: CCAASS##1. trifluralin 1582-09-82. desisopropylatrazine 1007-28-93. desethyl-atrazine 6190-65-4 4. desethyl-terbuthylazine —5. simazine 122-34-96. atrazine 1912-24-97. terbumeton 33693-04-88. terbuthylazine 5915-41-39. secbumeton 26259-45-0

10. cyanazine 21725-46-2

Column: Rtx®-OPPesticides2, 30m, 0.25mm ID, 0.25µm (cat.# 11243)Sample: custom standard, 100ng/µL each componentInj.: 1.0µL splitless (hold 0.5 min.), 4mm single gooseneck inlet liner (cat.# 20904)Inj. temp.: 300°CCarrier gas: helium, constant pressure Flow rate: 1.0mL/min. @ 80°C (27.22cm/sec.) Oven temp.: 80°C (hold 1 min.) to 140°C @ 25°C/min. (hold 5 min.) to 165°C @

1°C/min. to 300°C @ 15°C (hold 1 min.) Det: Agilent 5971A GC/MSTransfer line temp.: 280°CScan range: 35-360amuIonization: EI

Technical ServiceDo you have a technical question? Restek’s Technical Service group hasanswers! Drawing from our extensive libraries of technical information and many years of collective chromatography experience, the experts inTechnical Service can help you from set-up to method development.

Contact us:

For quick answers to commonly asked questions any time of the day, visitwww.restek.com/answers or contact us directly:

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PCB Mixtures

PCB Congeners

Rtx®-XLB

Column: Rtx®-XLB, 30m, 0.32mm ID, 0.50µm (cat.# 12839)Sample: 200ppb each PCB congener in hexane (cat.# 32416), 200ppb

2,4,5,6-tetrachloro-m-xylene (SS) (cat.# 32027), 100ppb decachlorobiphenyl (IS) (cat.# 32289)

Inj.: 1.0µL splitless (hold 0.75 min.), 4mm Drilled Uniliner® inlet liner (cat.# 21055)Inj. temp.: 220°CCarrier gas: hydrogen, constant pressureLinear velocity: 66cm/sec. @ 120°COven temp.: 120°C (hold 0.5 min.) to 260°C @ 29°C/min. (hold 2.5 min.), to 330°C @

28°C/min. (hold 5 min.)Det.: ECD @ 320°C

CCoommppoouunndd RRTT ((mmiinn..))1. 2-chlorobiphenyl (BZ #1) 3.862. 2,4,5,6 tetrachloro-m-xylene (SS) 4.533. 2,3-dichlorobiphenyl (BZ #5) 4.834. 2,2',5-trichlorobiphenyl (BZ #18) 5.175. 2,4',5-trichlorobiphenyl (BZ #31) 5.636. 2,2',5,5'-tetrachlorobiphenyl (BZ #52) 5.897. 2,2',3,5'-tetrachlorobiphenyl (BZ #44) 6.098. 2,3',4,4'-tetrachlorobiphenyl (BZ #66) 6.649. 2,2',4,5,5'-pentachlorobiphenyl (BZ #101) 6.84

10. 2,2',3,4,5'-pentachlorobiphenyl (BZ #87) 7.2411. 2,3,3',4',6-pentachlorobiphenyl (BZ #110) 7.3912. 2,2',3,5,5',6-hexachlorobiphenyl (BZ #151) 7.5113. 2,2',4,4',5,5'-hexachlorobiphenyl (BZ #153) 8.1514. 2,2',3,4,5,5'-hexachlorobiphenyl (BZ #141) 8.3515. 2,2',3,4,4',5'-hexachlorobiphenyl (BZ #138) 8.6116. 2,2',3,4',5,5',6-heptachlorobiphenyl (BZ #187) 8.7617. 2,2',3,4,4',5',6-heptachlorobiphenyl (BZ #183) 8.8418. 2,2',3,4,4',5,5'-heptachlorobiphenyl (BZ #180) 9.5019. 2,2',3,3',4,4',5-heptachlorobiphenyl (BZ #170) 9.8620. 2,2',3,3',4,4',5,5',6-nonachlorobiphenyl (BZ #206) 10.8721. decachlorobiphenyl (SS) 11.17

GC_EV00730

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583-594_GCappPcbs.qxp 11/22/2010 9:08 PM Page 583

584 www.restek.com 800-356-1688 or 814-353-1300


PCB Mixtures

GC_EV00992

GC_EV00994

GC_EV00993

GC_EV00997

GC_EV00996

GC_EV00995

GC_EV00998

Aroclor 1221

Aroclor 1232

Aroclor 1016

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260

Rtx®-CLPesticides30m, 0.32mm ID, 0.32μm (cat.# 11141)

1

1

1

1

1

1

1

1. decachlorobiphenyl (DCB)

Column: Rtx®-CLPesticides, 30m, 0.32mm ID, 0.32µm (cat.# 11141) Sample: 1,000µg/mL each Aroclor compound in hexane diluted to 1,000ppb,

decachlorobiphenyl (BZ #209) 200µg/mL in acetone (cat.# 32029) diluted to 100ppb

Inj.: 1.0µL pulsed splitless @ 30psi (hold 0.3 min.), 4mm cyclo double gooseneck inlet liner (cat.# 20895)

Inj. temp.: 250°CCarrier gas: helium, constant flowLinear velocity: 60cm/sec. @ 120°COven temp.: 120°C to 200°C @ 45°C/min. to 230°C @ 15°C/min.

to 330°C (hold 2 min.) @ 30°C/min.Det.: µ-ECD @ 330°C

Aroclor PCBs

US EPA Method 8082

Rtx®-CLPesticides


800-356-1688 or 814-353-1300 www.restek.com 585


PCB Mixtures

GC_EV00992A

GC_EV00994A

GC_EV00993A

GC_EV00997A

GC_EV00996A

GC_EV00995A

Aroclor 1221

Aroclor 1232

Aroclor 1016

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260

Rtx®-CLPesticides230m, 0.32mm ID, 0.25μm (cat.# 11324)

1

1

1

1

1

1

1

1. decachlorobiphenyl (DCB)

Column: Rtx®-CLPesticides2, 30m, 0.32mm ID, 0.25µm (cat.# 11324) Sample: 1,000µg/mL each Aroclor compound in hexane diluted to 1,000ppb,

decachlorobiphenyl (BZ #209) 200µg/mL in acetone (cat.# 32029) diluted to 100ppb

Inj.: 1.0µL pulsed splitless @ 30psi (hold 0.3 min.), 4mm cyclo double gooseneck inlet liner (cat.# 20895)

Inj. temp.: 250°CCarrier gas: helium, constant flowLinear velocity: 60cm/sec. @ 120°COven temp.: 120°C to 200°C @ 45°C/min. to 230°C @ 15°C/min.

to 330°C (hold 2 min.) @ 30°C/min.Det.: µ-ECD @ 330°C

Aroclor PCBs

US EPA Method 8082

Rtx®-CLPesticides2

GC_EV00998A


586 www.restek.com 800-356-1688 or 814-353-1300


PCB Mixtures

Aroclor 1242/1254/1262 PCBs

US EPA Method 8082

Rtx®-PCB

Column: Rtx®-PCB, 40m, 0.18mm ID, 0.18µm (cat.# 41303)Sample: 300ng/mL Aroclor 1242/1254/1262 in hexane: Aroclor 1242 (cat.# 32009),

Aroclor 1254 (cat.# 32011), Aroclor 1262 (cat.# 32409)Inj.: 1.0µL splitless (hold 0.75 min.), 4mm single gooseneck inlet liner (cat.# 20983)Inj. temp.: 230°CCarrier gas: hydrogen, constant pressureLinear velocity: 40cm/sec. @ 100°COven temp.: 100°C (hold 1 min.) to 200°C @ 30°C/min., to 320°C @ 2°C/min. (hold 1 min.)Det.: ECD @ 330°C

GC_EV00768

2826 32 34 36 38 42 44 46

5

restekinnovation!The Rtx®-PCB column offersexcellent resolution forPCB congeners.



800-356-1688 or 814-353-1300 www.restek.com 587


PCB Mixtures

Sample: 200ng/mL Aroclor 1242 (cat.# 32009)

GC_EV00752

Sample: 200ng/mL Aroclor 1254 (cat.# 32011)Column: Rtx®-PCB, 30m, 0.25mm ID, 0.25µm

(cat.# 13223)Inj.: 1.0µL splitless (hold 0.75 min.), 3.5mm ID

single gooseneck inlet liner (cat.# 20962)Inj. temp.: 250°CCarrier gas: hydrogen, constant pressureLinear velocity: 71cm/sec. @ 110°COven temp.: 100°C (hold 1.0 min.) to 300°C @ 10°C/min.

(hold 4 min.)Det.: ECD @ 310°C

Aroclor 1254 PCBs

Rtx®-PCB

GC_EV00753

Sample: 200ng/mL Aroclor 1260 (cat.# 32012)

Aroclor 1260 PCBs

Rtx®-PCB

GC_EV00754

Aroclor 1242 PCBs

Rtx®-PCB

Aroclor 1242/1254/1262 PCBs

US EPA Method 8082

Rtx®-PCB

GC_EV00767Column: Rtx®-PCB, 60m, 0.25mm ID, 0.25µm (cat.# 13226)Sample: Aroclor 1242 (cat.# 32009), 1254 (cat.# 32011), 1262 (cat.# 32409), 333ppm eachInj.: 1.0µL splitless (hold 0.75 min.), 4mm single gooseneck inlet liner w/wool (cat.# 22405)Inj. temp.: 280°CCarrier gas: helium, constant flowFlow rate: 1.1mL/min.Oven temp.: 100°C (hold 1 min.) to 200°C @ 30°C/min., to 320°C @ 2°C/min. (hold 1 min.)Det.: MSTransfer line

temp.: 280°CScan range: 50 to 550amuIonization: EIMode: scan

European indicator

PCB congeners

resolved from

other congeners

when using GC/MS.


588 www.restek.com 800-356-1688 or 814-353-1300


Brominated Flame Retardants

1. BDE-102. BDE-73. BDE-84. BDE-115. BDE-126. BDE-137. BDE-158. BDE-309. BDE-32

10. BDE-1711. BDE-2512. BDE-2813. BDE-3314. BDE-3515. BDE-3716. BDE-7517. BDE-4918. BDE-7119. BDE-4720. BDE-6621. BDE-7722. BDE-10023. BDE-11924. BDE-9925. BDE-11626. BDE-11827. BDE-8528. BDE-15529. BDE-12630. BDE-15431. BDE-15332. BDE-13833. BDE-16634. BDE-18335. BDE-18136. BDE-19037. BDE-20838. BDE-20739. BDE-20640. BDE-209

Column: Rtx®-1614, 15m, 0.25mm ID, 0.10µm (cat.# 10296)Sample: 100-300ppb PBDE PAR Solution (cat.# EO-5113, Cambridge

Isotope Laboratories Inc.), 500ppb decabromodiphenyl ether (cat.# BDE-209, Wellington Laboratories)

Inj.: 1µL splitless (hold 1 min.), 4mm cyclo double gooseneck liner (cat.# 20896)

Inj. temp.: 340°CCarrier gas: helium, constant flowLinear velocity: 60cm/sec. @ 120°COven temp.: 120°C (hold 1 min.) to 275°C @ 15°C/min. to 300°C @

5°C/min. (hold 5 min.) Detector temp.: µ-ECD @ 345°C


Rtx®-1614

GC_EV01025

1. BDE-102. BDE-73. BDE-84. BDE-115. BDE-126. BDE-137. BDE-158. BDE-309. BDE-32

10. BDE-1711. BDE-2512. BDE-2813. BDE-3314. BDE-3515. BDE-3716. BDE-7517. BDE-4918. BDE-7119. BDE-4720. BDE-6621. BDE-7722. BDE-10023. BDE-11924. BDE-9925. BDE-11626. BDE-11827. BDE-8528. BDE-15529. BDE-12630. BDE-15431. BDE-15332. BDE-13833. BDE-16634. BDE-18335. BDE-18136. BDE-19037. BDE-20838. BDE-20739. BDE-20640. BDE-209

Column: Rtx®-1614, 30m, 0.25mm ID, 0.10µm (cat.# 10295)Sample: 100-300ppb PBDE PAR Solution (cat.# EO-5113, Cambridge

Isotope Laboratories Inc.), 500ppb decabromodiphenyl ether (cat.# BDE-209, Wellington Laboratories)

Inj.: 1µL splitless (hold 1 min.), 4mm cyclo double gooseneck liner (cat.# 20896)

Inj. temp.: 300°CCarrier gas: helium, constant flowLinear velocity: 20cm/sec. @ 100°COven temp.: 100°C (hold 3 min.) to 320°C @ 5°C/min. (hold 15 min.) Detector temp.: µ-ECD @ 340°C

GC_EV01019


Rtx®-1614

Get results 3 times

faster with a short

column method!

Great peak shape

for BDE 209!


800-356-1688 or 814-353-1300 www.restek.com 589


Chlorinated Disinfection Byproducts


US EPA Method 551.1

Rtx®-5

1. chloroform2. 1,1,1-trichloroethane3. carbon tetrachloride4. trichloroacetonitrile5. trichloroethylene6. bromodichloromethane7. chloral hydrate8. dichloroacetonitrile9. 1,1-dichloro-2-propanone

10. 1,1,2-trichloroethane11. chloropicrin12. dibromochloromethane13. 1,2-dibromoethane (EDB)14. tetrachloroethylene15. bromochloroacetonitrile16. 1,1,1-trichloro-2-propanone17. bromoform18. dibromoacetonitrile19. 1,2,3-trichloropropane20. 4-bromofluorobenzene (IS)21. 1,2-dibromo-3-chloropropane

(DBCP)

Column: Rtx®-5, 30m, 0.25mm ID, 1.0µm (cat.# 10253)Inj.: 1.0µL split injection, 1ng on-column concentrationOven temp.: 35°C (hold 22 min.) to 200°C @ 10°C/min.Inj./det. temp.: 200°C/290°CCarrier gas: heliumLinear velocity: 30cm/sec. @ 50°CECD sensitivity: 20kHz full scaleSplit ratio: 10:1

1

min. 10 20 30

2

3

4

5

6

7

8

9

10

11

1213

14

15

16

17

18

19

20

21

GC_EV00023


US EPA Method 551.1

Rtx®-200


1

min. 10 20 30

2

3

4

5/6

7 9

10

1213/11

14/8

15

16

17

19/18

20

21

GC_EV00024


590 www.restek.com 800-356-1688 or 814-353-1300



Chlorinated Disinfection Byproducts, Chlorinated Solvents, and Halogenated Pesticides

US EPA Method 551.1

Rtx®-1301

Column: Rtx®-1301, 30m, 0.25mm ID, 1.0µm (cat.# 16053)Sample: 5-10µg/mL each analyte (Method 551.1 Pesticide/Herbicide Mix (cat.# 32438) and Disinfection

Byproducts & Chlorinated Solvents Mix (cat.# 30615) Inj.: 1.0µL splitless (hold 0.5 min.), 4mm split injection liner w/wool (cat.# 20781)Inj. temp.: 200°CCarrier gas: helium, constant pressure Linear velocity: 30cm/sec. @ 35°COven temp.: 35°C (hold 22 min.) to 145°C @ 10°C/min. (hold 2 min.)

to 225° @ 20°C/min. (hold 15 min.) to 260° @ 10°C/min. (hold 30 min.)Det.: ECD @ 290°C

GC_EV00758

1. chloroform2. 1,1,1-trichloroethane3. carbon tetrachloride4. trichloroacetonitrile5. trichloroethylene6. bromodichloromethane7. 1,1-dichloropropanone8. chloropicrin9. tetrachloroethylene

10. 1,1,2-trichloroethane11. dichloroacetonitrile12. dibromochloromethane13. 1,2-dibromoethane14. 1,1,1-trichloropropanone15. bromochloroacetonitrile16. bromoform17. 1,2,3-trichloropropane18. dibromoacetonitrile

19. 1,2-dibromo-3-chloropropane20. hexachlorocyclopentadiene21. trifluralin22. hexachlorobenzene23. atrazine24. simazine25. γ-BHC (lindane)26. heptachlor27. alachlor28. metolachlor29. heptachlor epoxide (B)30. bromacil31. cyanazine32. endrin33. endrin aldehyde34. endrin ketone35. methoxychlor

min.



Fax: 814-353-1309—24-hours a day



Mike Shuey, Customer Service


800-356-1688 or 814-353-1300 www.restek.com 591


Dioxins

TCDD Isomers

Rt®-2330

Column: Rt®-2330, 60m, 0.25mm ID, 0.20µm (cat.# 10726)Sample: 2.0µL splitless injection of TCDD isomers,

approximately 0.5ng each isomerSplitless hold: 0.45 min.Oven temp.: 200°C (hold 1 min.) to 250°C @ 8°C/min. (hold 15

min.), to 275°C @ 15°C/min. (hold 5 min.)Inj./det. temp.: 275°CCarrier gas: hydrogenLinear velocity: 40cm/sec.ECD sensitivity: 21 kHz full scale

1. 1,4,7,8-TCDD2. 2,3,7,8-TCDD3. 1,2,3,4-TCDD4. 1,2,3,7-TCDD5. 1,2,3,8-TCDD6. 1,2,7,8-TCDD7. 1,2,6,7-TCDD

GC_EV00108

min. 2 4 6 8 10 12 14 16 18 20

1

2

3

4, 5

6 7

also availableFor Rtx®-Dioxin2 columns,designed specifically for dioxin/furan analysis, seepage 96.


Solutions Online



592 www.restek.com 800-356-1688 or 814-353-1300


Endocrine Disruptors

Endocrine Disruptors: Alkyl Phenols

Rtx®-5MS

Column: Rtx®-5MS, 30m, 0.25mm ID, 0.25µm (cat.# 12623) Conc.: 5–10ng on-column Inj.: splitless, purge on @ 1 min.Oven temp.: 35°C (hold 1 min.) to 300°C @ 10°C/min. (hold 15 min.)Inj./det. temp.: 275°C/310°C Carrier gas: helium

1. tert-butyl phenol2. n-pentyl phenol3. n-hexyl phenol4. n-heptyl phenol5. tert-octyl phenol6. n-octyl phenol7. n-nonyl phenol8. bisphenol A

min. 12 14 16 18 20 22 24

1

2

3

4

5 6

7

8

GC_EV00046

Endocrine Disruptors: Phthalate Esters

Rtx®-5MS

Column: Rtx®-5MS, 30m, 0.25mm ID, 0.50µm (cat #12638)Conc.: 100pg on-column injection MS-SIM Oven temp.: 35°C (hold 1 min.) to 285°C @ 10°C/min.Pressure: 7.5psi constant pressure

1. dimethyl phthalate2. diethyl phthalate3. isobutyl phthalate4. dibutyl phthalate5. dipentyl phthalate6. dihexyl phthalate

7. benzylethyl phthalate8. diheptyl phthalate9. 2-ethylhexyl phthalate

10. cyclohexyl phthalate11. dioctyl phthalate

GC_EV00049min.18 20 22 24 26 28 30 32

12

34

5

6

7

8

9

10

11

Endocrine Disruptors:

Butyl Tins (hexyl derivatives)

Rtx®-5

min. 6 8 10 12 14

1

2

34

5

6

Column: Rtx®-5, 30m, 0.32mm ID, 0.50µm (cat.# 10239)Conc.: 500pg on-column direct injectionOven temp.: 100°C (hold 1 min.) to 285°C

@ 10°C/min.Inj./det. temp.: 250°CCarrier gas: heliumLinear velocity: 45cm/sec.Detector: FPD with 610nm filter

1. tetrapropyltin2. tetrabutyltin3. tributyltin4. dibutyltin5. tripentyltin6. monobutyltin

GC_EV00047

Endocrine Disruptors:

Butyl Tins (hexyl derivatives)

Rtx®-35

min. 6 8 10 12 14

1

2

34

56

1. tetrapropyltin2. tetrabutyltin3. tributyltin4. dibutyltin5. tripentyltin6. monobutyltin

GC_EV00048also availableButyl tin reference materials—see page 496.

Column: Rtx®-35, 30m, 0.32mm ID, 0.50µm (cat.# 10439)Conc.: 500pg on-column direct injectionOven temp.: 100°C (hold 1 min.) to 285°C

@ 10°C/min.Inj./det. temp.: 250°CCarrier gas: heliumLinear velocity: 45cm/sec.Detector: FPD with 610nm filter


800-356-1688 or 814-353-1300 www.restek.com 593


Organo Tins, Explosives

Explosives

Rtx®-200

3

1

24

5

6

7

89

10

11,12

13

17

21

23

1416

15

18,19

20

22

min. 10 15 20 25 30 35 40 45 50 55

Column: Rtx®-200, 30m, 0.25mm ID, 0.25µm (cat.# 15023)Inj.: 1.0µL splitless injectionConc.: 20ng/µLOven temp.: 80°C (hold 2 min.) to 260°C @

3°C/min. (hold 2 min.)Inj. temp.: 280°CDet.: MS, 300°CCarrier gas: heliumLinear velocity: 20cm/sec. set @ 80°CSplitless hold time: 0.6 min.

1. 2-nitrotoluene2. 3-nitrotoluene3. 4-nitrotoluene4. 2,3-diaminotoluene5. 2,6-diaminotoluene6. 2,4-diaminotoluene7. 1,4-dinitrobenzene8. 2,6-dinitrotoluene9. 2-amino-6-nitrotoluene

10. 1,3-dinitrobenzene11. 2,4-dinitrotoluene12. 2-amino-4-nitrotoluene

13. 2,3-dinitrotoluene14. 3,4-dinitrotoluene15. 3-nitrobiphenyl16. 2,4,6-trinitrotoluene17. 2,4,5-trinitrotoluene18. 4-amino-2,6-dinitrotoluene19. 2,3,4-trinitrotoluene20. 1,3-dinitronaphthalene21. 2,6-diamino-4-nitrotoluene22. 2-amino-4,6-dinitrotoluene23. 2,2-dinitrobiphenyl

GC_EV00060

Column: Rtx®-35, 30m, 0.32mm ID, 1.0µm (cat.# 10454)Inj.: direct injection using a Uniliner® inlet liner (cat.# 20335)Conc.: 5pg on-column Head pressure: 15psi, constantOven temp.: 100°C (hold 1 min.) to 285°C @ 10°C/min. (hold 10 min.)Detector: PFPD* Model 5380 courtesy of O.I. Analytical Corp., College Station, TX

min. 8 10 12 14 16 18

1. tetrapropyl tin2. tetrabutyl tin3. tributyl tin4. dibutyl tin5. monobutyl tin

1

2

3

4

5

*Peak tailing is a function of this detector.

GC_EV00788

did you know?PFPD increases sensitivityby 100 times when analyz-ing organo tin com-pounds by this method.

Organo Tins

Rtx®-35

5pg on-column

concentration


594 www.restek.com 800-356-1688 or 814-353-1300


Explosives

Explosives

US EPA Method 8095

Rtx®-TNT & Rtx®-TNT2

1. nitrobenzene2. 2-nitrotoluene3. 3-nitrotoluene4. 4-nitrotoluene5. nitroglycerine6. 1,3-dinitrobenzene7. 2,6-dinitrotoluene8. 2,4-dinitrotoluene9. 3,4-dinitrotoluene (IS)

10. 1,3,5-trinitrobenzene11. trinitrotoluene12. PETN13. RDX14. 4-amino-2,6-dinitrotoluene15. 3,5-dinitroaniline16. 2-amino-4,6-dinitrotoluene17. tetryl

Column: Rtx®-TNT, 6m, 0.53mm ID, 1.50µm (cat.# 12998) Inj.: direct injection using a 1mm Siltek® Uniliner® inlet liner (cat.# 21052-214.1)On-column conc.: est. 200-1,000pg/compound. 8095 Calibration Mix A (cat.# 31607),

8095 Calibration Mix B (cat.# 31608), and 3,4-dinitrotoluene (cat.# 31452) Oven temp.: 80°C (hold 1 min.) to 180°C @ 10°C/min. to 300°C @

30°C/min. (hold 3 min.)Inj. temp.: 250°CDet.: ECD @ 330°C with anode purgeDead time: 4.4 sec.Head pressure: helium @ 3psi (20.7 KPa)Flow rate: helium @ 17mL/min. @ 80°C

1 2 3

7

8

9

13

15

16

45

610

11

12

17

14

min. 2 4 6 8 10

GC_EV00406

Improved resolution ofnitroaromatic compoundssuch as those listed in USEPA Method 8095.

Column: Rtx®-TNT2, 6m, 0.53mm ID, 1.50µm (cat.# 12999) Inj.: direct injection using a 1mm Siltek® Uniliner® (cat.# 21052-214.1)On-column conc.: est. 200-1,000pg/compound. 8095 Calibration Mix A (cat.# 31607),

8095 Calibration Mix B (cat.# 31608), and 3,4-dinitrotoluene (cat.# 31452) Oven temp.: 80°C (hold 1 min.) to 180°C @ 10°C/min. to 300°C @

30°C/min. (hold 3 min.)Inj. temp.: 250°CDet.: ECD @ 330°C with anode purgeDead time: 4.4 sec.Head pressure: helium @ 3psi (20.7 KPa)Flow rate: helium @ 17mL/min. @ 80°C

1 2 35

8

9

16

15,13

4

11

10

12,14

17

7

6

min. 2 4 6 8 10 12

GC_EV00407

Rtx®-TNT2

Rtx®-TNT

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Gasoline Range Organics (GRO)

Volatile Petroleum Hydrocarbons (VPH)

Massachusetts Department of Environmental Protection

Rtx®-502.2

PID

min. 4 8 12 16 20 24 28 32

1. methanol2. methyl tert-butyl ether (60ng)3. benzene (20ng)4. toluene5. ethylbenzene (20ng)6. p+m-xylene (40ng ea.)7. o-xylene (40ng)8. 1,2,4-trimethylbenzene (40ng)9. naphthalene (40ng)

10. 2,5-dibromotoluene (SS)

2

1 3

4

5

6

7

8

910

Column: Rtx®-502.2, 105m, 0.53mm ID, 3.0µm (cat.# 10910) Conc.: on-column at levels listed Oven temp: 45°C to 90°C @ 3°C/min., to 140° @ 5°C/min.,

to 230°C @ 45°C/min. (hold 8 min.)Carrier gas: helium @ 15mL/min. Tekmar Model LSC 2000 Trap: BTEX Purge: helium @ 40mL/min. for 11 min.Dry purge: 2 min. Desorb preheat: 245°CDesorb: 2 min. @ 250°CBake: 6 min. @ 260°C

Chromatograms courtesy of Severn Trent Laboratories, Burlington, VT.

1. methanol2. n-pentane (40ng)3. 2-methylpentane (60ng)4. methyl tert-butyl ether (60ng)5. 2,2,4-trimethylpentane (60ng)6. benzene (20ng)7. toluene (60ng)8. n-nonane (40ng)9. ethylbenzene (20ng)

10. p+m-xylene (40ng ea.)11. o-xylene (40ng)12. 1,2,4-trimethylbenzene (40ng)13. naphthalene (40ng)14. 2,5-dibromotoluene (SS)

FID

GC_EV00063

For VPH analysis on an Rtx®-502.2 column, use PID for aromatic

compounds and FID for aliphatic compounds.

21

3

4

56

7

8 9

10

11

12

13

14

min. 4 8 12 16 20 24 28 32

free literatureOptimizing Massachusetts Volatile Petroleum

Hydrocarbon GC Analysis

Massachusetts VPH affords more reliable quantification of volatile petroleum hydrocarbons, relative to older “analytical window” methods, and has been adopted by other states and in Canada. This 2-page note offers valuable tips for selecting a trap and a capillary GC column compatible with the methodology. Referencemixes specifically designed for MA VPH are described.

Download your free copy from www.restek.com


595-610_GCappGro.qxp 11/22/2010 9:10 PM Page 595

Texas UST: Alternate Boiling Point/Carbon Number Distribution Marker

Rtx®-5

Column: Rtx®-5, 15m, 0.25 ID, 0.25µm (cat.# 10220)Sample: 200µg/mL Alternate BP/CN Distribution Marker Stock

Solution (cat.# 31639) in pentaneInj.: 0.5µL splitless (hold 0.2 min.), 4mm drilled Uniliner®

inlet liner (hole near bottom) (cat.# 20756)Inj. temp.: 285°CCarrier gas: helium, constant pressure Linear velocity: 27cm/sec. @ 30°COven temp.: 30°C (hold 1 min.) to 330°C @ 60°C/min. (hold 6

min.) with GC Racer for Agilent 5890 Series II GCDet.: FID @ 330°C

1. hexane (C6)2. octane (C8)3. decane (C10)4. dodecane (C12)5. hexadecane (C16)6. heneicosane (C21)7. octacosane (C28)8. pentatriacontane (C35)9. hexatriacontane (C36)

GC_EV00690

Column: Rtx®-5, 15m, 0.25mm ID, 0.25µm (cat.# 10220)Sample: 1,000µg/mL unleaded gas and diesel fuel #2 composites

standard (cat.# 31483) in pentane250µg/mL 2-fluorobiphenyl standard (cat.# 31096) in dichloromethane250µg/mL 1-chlorooctane (cat.# 30084) in P&T methanol

Inj.: 0.5µL splitless (hold 0.2 min.), 4mm drilled Uniliner® inlet liner(hole near bottom) (cat.# 20756)

Inj. temp.: 285°CCarrier gas: helium, constant pressure Linear velocity: 27cm/sec. @ 30°COven temp.: 30°C (hold 1 min.) to 330°C @ 60°C/min. (hold 6 min.) with GC

Racer for Agilent 5890 Series II GCDet.: FID @ 330°C

1. 1-chlorooctane (SS)2. 2-fluorobiphenyl (SS)

GC_EV00692

Texas UST: diesel/gas composites

Rtx®-5

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Texas UST: Alternate Boiling Point/Carbon Number Distribution Marker

Rtx®-5

1. n-hexane(C6)2. n-octane(C8)3. n-decane(C10)4. n-dodecane(C12)5. n-hexadecane(C16)6. n-heneicosane(C21)7. n-octacosane(C28)8. n-pentatriacontane9. n-hexatriacontane(C36)

Column: Rtx®-5, 30m, 0.25mm ID, 0.50µm (cat.# 10238)Sample: 1µL Alternate Boiling Point/Carbon Number Distribution Marker Stock

Solution (cat.# 31639), 200µg/mL each component in pentaneCarrier gas: hydrogen @ 40cm/sec.Oven temp.: 40°C (hold 2 min.) to 330°C @ 10°C/min. (hold 5 min.)Inj. temp.: 250°C Det. temp.: 330°CDet.: FID

GC_EV00691

Wisconsin GRO Mix, plus C12

Rtx®-502.26

1

2

3

4 7

9

105

8

min. 10 20 30

1. 3-methylpentane2. 2,2,4-trimethylpentane (isooctane)3. benzene4. toluene5. ethylbenzene6. m-xylene7. o-xylene8. 1,2,4-trimethylbenzene9. dodecane

10. naphthalene

FID

Column: Rtx®-502.2, 105m, 0.53mm ID, 3.0µm (cat.# 10910)Sample: GRO Mix (WISC) + C12 (cat.# 30069)Conc.: 200ppb each in 5mL of H2O.Oven temp.: 40°C (hold 1 min.) to 100°C @ 5°C/min. to

240°C @ 8°C/min. (hold 8 min.)Inj./det. temp.: 200°C/250°CCarrier gas: helium Flow rate: 10mL/min.Trap: Tenax®, silica gel, charcoalPurge: 12 min. @ 40mL/min.Desorb preheat: 175°CDesorb temp.: 180°CDesorb time: 2 min.Desorb flow: 10mL/min.FID sensitivity: 16 x 10-11 AFS

10

9

8

76

5

4

3

GC_EV00071

PID

min. 10 20 30


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GC_EV00887

Column: Rxi®-1ms, 20m, 0.18mm ID, 0.18µm (cat.# 13302)Sample: Diesel #2/Motor Oil (cat.# 31682) 5,000µg/mL each component in hexaneInj.: 0.5µL, split, split ratio 20:1, 3.5mm Precision® inlet liner (cat.# 21021)Instrument: Shimadzu GC-2010Inj. temp.: 275°CCarrier gas: hydrogen, constant pressureLinear velocity: 55cm/sec. @ 40°COven temp.: 40°C (hold 1 min.) to 330°C @ 20°C/min. (hold 10 min.)Det.: FID @ 350°C

1. diesel fuel #2 composite2. motor oil

Lubrication Range Organics

Diesel Fuel #2/Motor Oil

Rxi®-1ms

GC_EV00886

Column: Rxi®-1ms, 20m, 0.18mm ID, 0.18µm (cat.# 13302)Sample: Florida TRPH Standard (cat.# 31266), 500µg/mL each component in hexaneInj.: 0.5µL, split, split ratio 20:1, 3.5mm Precision® inlet liner (cat.# 21021)Instrument: Shimadzu GC-2010*Inj. temp.: 275°CCarrier gas: hydrogen, constant pressureLinear velocity: 55cm/sec. @ 40°COven temp.: 40°C (hold 1 min.) to 330°C @ 20°C/min. (hold 10 min.)Det.: FID @ 350°C

*GC courtesy of Shimadzu Scientific.

Petroleum Hydrocarbons (TPH)

Rxi®-1ms1. C82. C103. C124. C145. C166. C187. C208. C229. C24

10. C2611. C2812. C3013. C3214. C3415. C3616. C3817. C40






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Column: Rtx®-5, 15m, 0.25mm ID, 0.25µm (cat.# 10220)

Sample: 500µg/mL Unleaded Gasoline Standard (unweathered) (cat.# 30096) in methylene chloride

Inj.: 1.0µL splitless (hold 0.5 min.), 4mm single gooseneck inlet liner (cat.# 20904)

Inj. temp.: 260°CCarrier gas: helium, constant pressure Linear velocity: 76cm/sec. @ 50°COven temp.: 35°C (2 min.) to 330°C

@ 60°C/min. using GC RacerDet.: FID @ 330°C

Unleaded Gasoline

Rtx®-5

GC_EV00671


Sample: 500µg/mL Jet Fuel A standard (cat.# 31215) in methylene chloride

Inj.: 1.0µL splitless (hold 0.5 min.), 4mm single gooseneck inlet liner (cat.# 22405)

Inj. temp.: 260°CCarrier gas: helium, constant pressure Linear velocity: 76cm/sec. @ 50°COven temp.: 50°C (1 min.) to 330°C @

60°C/min. (hold 0.5 min.)using GC Racer

Det.: FID @ 330°C

Jet Fuel

Rtx®-5

GC_EV00670


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Diesel Range Organics (DRO)

Column: Rtx®-5, 15m, 0.25mm ID, 0.25µm (cat.# 10220)Sample: 500µg/mL Diesel Fuel Composite standard (cat.# 31093) in methylene chlorideInj.: 1.0µL splitless (hold 0.5 min.), 4mm single gooseneck inlet liner (cat.# 20904)Inj. temp.: 260°CCarrier gas: helium, constant pressure Linear velocity: 76cm/sec. @ 50°COven temp.: 50°C (1 min.) to 330°C @ 20°C/min.Det.: FID @ 330°C

Diesel Fuel

Rtx®-5

GC_EV00669

conventional

20°C/min. temperature program

DRO Mix

Rtx®-5

1. C102. C123. C144. C165. C186. C207. C228. C249. C26

10. C28

12 3

4

10987

6

5

Column: Rtx®-5, 30m, 0.53mm ID, 1.0µm (cat.# 10255)Sample: Direct injection of DRO Mix (cat.# 31064) Conc.: 50ng/µLOven temp.: 40°C (hold 2 min.) to 310°C

@ 12°C/min. (hold 10 min.)Inj./det. temp.: 280°C/310°CCarrier gas: helium @ 65cm/sec.FID sensitivity: 8 x 10-11 AFS

min. 5 10 15 20 25GC_EV00069

For Biodiesel chromatograms,

see pages 644–646.


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Glycols

Glycols

Rtx®-Wax

min. 1.00 1.50 2.00 2.50 3.00 3.50 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00

1

2

1. propylene glycol2. ethylene glycol

Column: Rtx®-Wax, 30m, 0.53mm ID, 1.0µm (cat.# 12455)Inj.: directInj./det. temp.: 220°C/270°COven temp.: 80°C (hold 1 min.) to 120°C

@ 8°C/min. (hold 3 min.)10psi pressureStd. = 100µg/mL

GC_EV00444

Glycols

Rtx®-200

min. 0.20 0.40 0.60 0.80 1.00 1.20 1.40 1.60 1.80 2.00 2.20 2.40 2.60 2.80 3.00 3.20 3.40 3.60 3.80 4.00

1

2

1. ethylene glycol2. propylene glycol

Column: Rtx®-200, 30m, 0.53mm ID, 1.0µm (cat.# 15055)Inj.: directInj./det. temp.: 220°C/270°COven temp.: 80°C (hold 1 min.) to 200°C

@ 8°C/min. (hold 3 min.)10psi pressureStd. = 100µg/mL

GC_EV00445


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Glycols

Glycols

Stabilwax®

Column: Stabilwax®, 30m, 0.53mmID, 1.0µm (cat.# 10655)Inj.: 1.0µL direct injection, open-top Uniliner® inlet liner

without wool (cat.# 20843-205)Conc.: 150ppmSolvent: water/methanol (50:50)Oven temp.: 80°C to 200°C @ 8°C/min. (hold 10 min.)Septa purge: 5.0cc/min.Carrier gas: heliumLinear velocity: 50cm/sec.Column flow rate: 6.9mL/min.Det.: FID @ 270°CMake up gas flow: 45cc/min.

1. 1,2-propylene glycol2. ethylene glycol3. 1,3-butylene glycol4. 1,3-propylene glycol5. 1,4-butylene glycol6. diethylene glycol7. glycerol

GC_EV00476

Column: Stabilwax®, 30m, 0.53mm ID, 1.0µm (cat.# 10655)

Inj.: 1.0µL of direct injection of glycols in water. Open-top Uniliner® inlet liner without wool (cat.# 20843-205)

Conc.: 100ppmOven temp.: 80°C (hold 1 min.) to 200°C @

8°C/min. (hold 5 min.)Inj./det. temp.: 225°C/250°CCarrier gas: heliumLinear velocity: 50cm/sec.Det.: FIDSeptum Purge: 5.0cc/min.

min.8.0 9.0 10.0 11.0

~~

1. propylene glycol2. ethylene glycol

1

2

GC_EV00546

Glycols

Stabilwax®

Glycols

Rtx®-BAC1 & Rtx®-BAC2


Rtx®-BAC1 Rtx®-BAC2

Columns: Rtx®-BAC1, 30m, 0.32mm ID, 1.8µm (cat.# 18003)Rtx®-BAC2, 30m, 0.32mm ID, 1.2µm (cat.# 18002)

Inj.: 0.5µL split injectionConc.: 1%Solvent: methanolOven temp.: 100°C to 240°C @ 5°C/min. (hold 5 min.)Inj. temp.: 240°CInj. mode: 100:1 splitInlet liner: 4mm single gooseneck (cat.# 20798)Septa purge: 5.0cc/min.Carrier gas: helium, constant pressurePressure: 12psiLinear velocity: 37cm/sec.Column flow rate: 2.1mL/min.Det.: FID @ 240°CMake-up gas flow: 40cc/min.

GC_EV00474


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Haloacetic Acids

Haloacetic Acids

US EPA Method 552.2

Rtx®-5

1

min. 10 12 14 16 18 20 22 24 26

23

4

56/7

8

9

10

11

12

1. monochloroacetic acid (MCAA)2. monobromoacetic acid (MBAA)3. dichloroacetic acid (DCAA)4. dalapon5. 1,2,3-trichloropropane (IS)6. bromochloroacetic acid (BCAA)7. trichloroacetic acid (TCAA)8. dibromoacetic acid (DBAA)9. bromodichloroacetic acid (BDCAA)

10. 2,3-dibromopropionic acid (SS)11. chlorodibromoacetic acid (CDBAA)12. tribromoacetic acid (TBAA)

(All compounds derivatized)

GC_EV00025

Haloacetic Acids

US EPA Method 552.2

Rtx®-200


1

min. 10 12 14 16 18 20 22 24 26

2/3

4

5

6

8

9

10

11

12

7

GC_EV00026



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Haloacetic Acids

Haloacetic Acids & Dalapon

US EPA Method 552.2


PPeeaakk LLiisstt CCoonncc..((µµgg//mmLL))1. methyl monochloroacetate 1.22. methyl monobromoacetate 0.83. methyl dichloroacetate 1.24. dalapon methyl ester 25. methyl trichloroacetate 0.4 6. 1,2,3-trichloropropane (IS) 47. methyl bromochloroacetate 0.88. methyl bromodichloroacetate 0.89. methyl dibromoacetate 0.4

10. methyl chlorodibromoacetate 211. methyl 2,3-dibromopropionate (SS) 212. methyl tribromoacetate 4

GC_EV01006

GC_EV01007

Column: Rtx®-CLPesticides2, 30m, 0.32mm ID, 0.25µm (cat.# 11324) andRtx®-CLPesticides, 30m, 0.32mm ID, 0.32µm (cat.# 11141) with5m x 0.32mm ID Rxi® deactivated guard tubing (cat.# 10039), connected using Universal “Y” Press-Tight® Connector (cat.# 20405-261)

Sample: Haloacetic Acid Methyl Ester Mix #2 (cat.# 31647), Dalapon Methyl Ester (cat.# 32057), Methyl-2,3-dibromopropionate (cat.# 31656), 552.2 Internal Standard (cat.# 31648), diluted in methyl tert-butyl ether (MTBE)

Inj.: 1µL splitless (hold 0.75 min.), 4mm cyclo double gooseneck liner (cat.# 20896)Inj. temp.: 250°CCarrier gas: helium, constant flowLinear velocity: 25cm/sec. @ 35°COven temp.: 35°C (hold 4 min.) to 250°C (hold 5 min.) @ 15°C/min. Detector temp.: µ-ECD @ 300°C

Rtx®-CLPesticides

Rtx®-CLPesticides2


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Air

Microbial Volatile Organic Compounds (MVOCs)

Rxi®-1ms

CCoommppoouunndd RRtt ((mmiinn..))1. 2-butanone 9.0472. 2-methyl-furan 9.6403. 3-methyl-furan 9.9624. 2-methyl-1-propanol 10.4055. 2-methyl-2-butanol 10.7916. 1-butanol 11.5067. 3-methyl-2-butanol 12.0928. 2-pentanol 12.5929. 2-methyl-1-butanol 13.779

10. dimethyl-disulfide 13.97911. 3-hexanone 14.99412. 2-hexanone 15.08013. 2-heptanone 17.76714. 1-octen-3-ol 20.01915. 3-octanone 20.13316. 3-octanol 20.43317. 2-pentyl-furan 20.47618. 2-ethyl-1-hexanol 21.16319. 1-octanol 22.01320. 2-isopropyl-3-methoxypyrazine 22.62821. isoborneol 24.37922. α-terpineol 24.84423. geosmin 28.347

Column: Rxi®-1ms, 60m, 0.25mm ID, 1.00µm (cat.# 13356)Sample: Microbial volatile organic compounds, 2ppbv, 60% RHInj.: 1.0µL split (split ratio 1:1),

1mm split inlet liner (cat.# 20972)Inj. temp.: 200°CCarrier gas: helium, constant flow Flow rate: 1.5mL/min. Oven temp.: 10°C (hold 1 min.) to 235°C @ 8°C/min. Det: Agilent 6890/5973 GC/MS

5 min. solvent delayTransfer line temp.: 260°CScan range: 35 to 350amuIonization: EIMode: scan Other: Nutech 8900DS Preconcentrator

Conditions:Sample = 200mL from canisterCryotrap1 = -160°CDesorb = 20°CCryotrap2 = 20°CDesorb = 200°CCryofocuser = 200°CDesorb = 200°C

GC_AR01030

Early detection of MVOCs

allows faster treatment!

ChromaBLOGraphyTopical and timely insights from top chromatographers.

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Air

US EPA TO-14 Compounds

Rtx®-1

1. dichlorodifluoromethane2. chloromethane3. 1,2-dichlorotetrafluoroethane4. vinyl chloride5. bromomethane6. chloroethane7. trichlorofluoromethane8. 1,1-dichloroethene9. methylene chloride

10. 3-chloropropene11. 1,1,2-trichloro-1,2,2-trifluoroethane12. 1,1-dichloroethane13. cis-1,2-dichloroethene14. chloroform15. 1,2-dichloroethane16. 1,1,1-trichloroethane17. benzene18. carbon tetrachloride19. 1,2-dichloropropane20. trichloroethene

21. cis-1,3-dichloropropene22. trans-1,3-dichloropropene23. 1,1,2-trichloroethane24. toluene25. 1,2-dibromoethane26. tetrachloroethene27. chlorobenzene28. ethylbenzene29. m-xylene30. p-xylene31. styrene32. o-xylene33. 1,1,2,2-tetrachloroethane34. 4-methyltoluene35. 1,3,5-trimethylbenzene36. 1,2,4-trimethylbenzene37. 1,3-dichlorobenzene38. 1,4-dichlorobenzene39. 1,2-dichlorobenzene40. 1,2,4-trichlorobenzene41. hexachlorobutadiene

1

2

3

4

5

6

7

8

910

12

13

14

11

16

1517

18

19

20

21

22

23

24

25

41

40

39

38

37

3635

34

32,33

31

29,30

28

27

26

min. 10 15 20 25 30 35

Column: Rtx®-1, 60m, 0.32mm ID, 3.0µm (cat.# 10187)Sample: 5mL of 2ppmv TO-14 standard.Oven temp.: 30°C (hold 4 min.) to 250°C @ 7°C/min. (hold 15 min.)Detector: MSDet. temp.: 250°CCarrier gas: heliumLinear velocity: 21cm/sec. set @ 30°CIonization: EIScan range: 34-280amu

Preconcentrator conditions:Nutech 3550 A PreconcentratorCryotrap temp.: -160°CCryotrap desorb temp.: 150°CCryofocusing unit temp.: -190°CCryofocusing desorb temp.: 150°C

GC_EV00018

Ozone Precursors

Rtx®-1

min. 5 10 15 20 25 30 35

321

54

6

78

910

1112

1314

1615

17

18 19 20 21 22

2423

25 26 27 2829

30

31,32

3334 35

36,37

38

1. ethylene2. acetylene3. ethane4. propylene5. propane6. isobutane7. 1-butene8. n-butane9. trans-2-butene

10. cis-2-butene11. isopentane12. 2-methyl-1-butene13. n-pentane14. trans-2-pentene15. cis-2-pentene16. cyclopentane17. isohexane18. 3-methylpentane19. n-hexane20. methylcyclopentane21. benzene22. isoheptane23. 2,3-dimethylpentane

24. 3-methylhexane25. 2,2,4-trimethylpentane26. n-heptane27. methylcyclohexane28. 2,2,3-trimethylpentane29. toluene30. ethylbenzene31. m-xylene32. p-xylene33. o-xylene34. n-nonane35. n-propylbenzene36. p-ethyltoluene37. 1,3,5-trimethylbenzene38. 1,2,4-trimethylbenzene

Column: Rtx®-1, 60m, 0.32mm ID, 3.0µm (cat.# 10187)Sample: 0.5L of C2-C9 gas standard cryogenically concentrated;

15nL/component desorbed onto column.Oven temp.: -60°C (hold 5 min.) to 100°C @ 8°C/min., to

150°C @ 6°C/min., then to 240°C @ 8°C/min.Carrier gas: heliumLinear velocity: 30cm/sec. (flow rate: 1.8cc/min.)FID sensitivity: 64 x 10-12 AFS

GC_EV00019Permission to publish this chromatogram granted by Radian Corporation.


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Air

Air Toxins

Rtx®-502.2

Permission to publish this chromatogram granted by Tekmar Company.

Column: Rtx®-502.2, 60m, 0.32mm ID, 1.8µm (cat.# 10920)Sample: 500mL of 10ppbv standard concentrated on an AEROCAN 6000 using a glass

bead trap at 165°C then desorbed at 200°C for 4 min. @ 1mL/min., cryofocused @ -175°C then desorbed @ 150°C

Oven temp.: 35°C (hold 6 min.) to 120°C @ 15°C/min., then to 200°C @ 5°C/min., then to 220°C @ 25°C/min. (hold 10 min.)

Det. & det. temp.: Agilent-5971A GC/MS, 280°CCarrier gas: helium @ 1mL/min.Linear velocity: 20cm/sec.Scan range: 28-260amuSolvent delay: 4 min.

1. chlorodifluoromethane2. dichlorodifluoromethane3. dichlorotetrafluoroethane4. chloromethane5. butane6. vinyl chloride7. 1,3-butadiene8. acetaldehyde9. bromomethane

10. chloroethane11. trichlorofluoromethane12. isopropanol13. acetone14. 1,1-dichloroethene15. acetonitrile16. dichloromethane17. acrylonitrile18. 1-propanol

19. trans-1,2-dichloroethene20. 1,1-dichloroethane21. methyl ethyl ketone22. cis-1,2-dichloroethene23. methacrylonitrile24. chloroform25. bromochloromethane26. tetrahydrofuran27. 1,1,1-trichloroethane28. n-butanol29. heptane30. 1,2-dichloroethane31. benzene32. 1,4-difluorobenzene33. trichloroethene34. ethyl methacrylate35. 1,2-dichloropropane36. 1,4-dioxane

37. bromodichloromethane38. 4-methyl-2-pentanone39. octane40. toluene41. 2-hexanone42. 1,1,2-trichloroethane43. tetrachloroethene44. dibromochloromethane45. 1,2-dibromoethane46. chlorobenzene-d547. chlorobenzene48. m-xylene49. p-xylene50. 2-heptanone51. styrene52. o-xylene53. isopropylbenzene54. bromoform

55. 1,1,1,2-tetrachloroethane56. 4-bromofluoromethane57. n-propylbenzene58. 1,3,5-trimethylbenzene59. α-methylstyrene60. tert-butylbenzene61. 1,2,4-trimethylbenzene62. sec-butylbenzene63. 1,3-dichlorobenzene64. 1,4-dichlorobenzene65. butylbenzene66. 1,2-dichlorobenzene67. dodecane68. dibromochloropropane69. 1,2,4-trichlorobenzene70. hexachlorobutadiene71. naphthalene

min. 5 10 15 20 25 30

1

2

3

4

5

76

8 9

10

11

13

12

14

1518

19

2021

1617

22,23

24

25,26

27

28

29

31

30

32

33

35

34

38

39

40 41

42

43

44

36,37

45

46

47

48,49

50

71

7069

68

67

6665

63

64

6260

59

58

57

56

5554

53

51,52

61

GC_EV00022


608 www.restek.com 800-356-1688 or 814-353-1300


Air

Column: Rtx®-1, 60m, 0.32mm ID, 1.0µm (cat.# 10157)Sample: 200mL of 10ppbv TO-15 standard, injected into TO-Can® canister and

humidified to 70% RH. Concentrator: Nutech 3550 Preconcentrator

200mL of sample concentrated at -160°C, thermally desorbed at 150°C, and cryofocused at -185°C

Oven temp.: 30°C (hold 4 min.) to 175°C @ 9°C/min. to 220°C @ 40°C/min.Carrier gas: helium @ 1.2mL/min.Det.: Agilent 5971 MSScan range: 35-265amu

4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 min.

1

3

45

6

7

8

9/10

11

12

1314

15

16

1718

1920

21

22/2324

25

26

27

28

29

30

31

32

333435/36

37

38

39

40

41 42

4344

45

46

47

48

49

50

51

52

53

54

55

56

5758

59

60 61

62

63

BFB

GC_EV00379

2

Chromatogram courtesy of Gina Maio, Severn Trent Laboratories, Inc., Burlington, VT.

1. dichlorofluoromethane2. chloromethane3. dichlorotetrafluoroethane4. vinyl chloride5. 1,3-butadiene6. bromomethane7. chloroethane8. bromoethene9. acetone

10. trichlorofluoromethane11. isopropyl alcohol12. 1,1-dichloroethene13. methylene chloride14. 3-chloropropene15. carbon disulfide16. Freon® TF17. trans-1,2-dichloroethene18. 1,1-dichloroethane19. methyl tert-butyl ether20. methyl ethyl ketone21. cis-1,2-dichloroethene22. bromochloromethane (IS)

23. n-hexane24. chloroform25. tetrahydrofuran26. 1,2-dichloroethane27. 1,1,1-trichloroethane28. benzene29. carbon tetrachloride30. cyclohexane31. 1,4-difluorobenzene (IS)32. 1,2-dichloropropane33. bromodichloromethane34. trichloroethene35. 1,4-dioxane36. 2,2,4-trimethylpentane37. n-heptane38. cis-1,3-dichloropropene39. methyl isobutyl ketone40. trans-1,3-dichloropropene41. 1,1,2-trichloroethane42. toluene43. methyl butyl ketone44. dibromochloromethane

45. 1,2-dibromoethane46. tetrachloroethene47. chlorobenzene-d5 (IS)48. chlorobenzene49. ethylbenzene

50a. m-xylene50b. p-xylene51. bromoform52. styrene53. 1,1,2,2-tetrachloroethane54. o-xylene55. 2-chlorotoluene56. 4-ethyltoluene57. 1,3,5-trimethylbenzene58. 1,2,4-trimethylbenzene59. 1,3-dichlorobenzene60. 1,4-dichlorobenzene61. 1,2-dichlorobenzene62. 1,2,4-trichlorobenzene63. hexachlorobutadiene

US EPA TO-14/TO-15 Compounds

Rtx®-1


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Air

US EPA TO-15 Compounds

Rtx®-1

Column: Rtx®-1, 60m, 0.32mm ID, 1.0µm (cat.# 10157)Sample: TO-15 standard (cat.# 34436) humidified to 33% RH in a 6L SilcoCan®

canister (cat.# 24182)Concentrator: Nutech 3550A Preconcentrator; 300mL sample concentrated at

-160°C, thermally desorbed at 150°C, cryofocused at -185°C, thermally desorbed to column at 150°C

Carrier gas: helium, constant flowFlow rate: 1.2mL/min.Oven temp.: 30°C (hold 4 min.) to 175°C @ 8°C/min., to 220°C @

20°C/min. (hold 2 min.)Det.: MSTransfer line

temp.: 150°CScan range: 35–280amuIonization: EIMode: scan

1. propylene2. Freon®-12 (dichlorodifluoromethane)3. chloromethane4. Freon®-114 (dichlorotetrafluoroethane)5. vinyl chloride6. 1,3-butadiene7. bromomethane8. chloroethane9. carbon disulfide

10. acetone11. Freon®-11 (trichlorofluoromethane)12. isopropyl alcohol13. 1,1-dichloroethene14. methylene chloride15. Freon®-113 (1,1,2-trichloro-1,2,2-trifluoroethane)16. trans-1,2-dichloroethene17. 1,1-dichloroethane18. methyl tert-butyl ether19. vinyl acetate20. methyl ethyl ketone21. cis-1,2-dichloroethene

22. hexane23. chloroform24. ethyl acetate25. tetrahydrofuran26. 1,2-dichloroethane27. 1,1,1-trichloroethane28. benzene29. carbon tetrachloride30. cyclohexane31. 1,2-dichloropropane32. trichloroethylene33. bromodichloromethane34. 1,4-dioxane35. heptane36. cis-1,3-dichloropropene37. methyl isobutyl ketone38. trans-1,3-dichloropropene39. 1,1,2-trichloroethane40. toluene41. methyl butyl ketone42. dibromochloromethane

43. 1,2-dibromoethane44. tetrachloroethylene45. chlorobenzene46. ethylbenzene47. p-xylene48. m-xylene49. bromoform50. styrene51. o-xylene52. 1,1,2,2-tetrachloroethane53. 4-ethyltoluene54. 1,3,5-trimethylbenzene55. 1,2,4-trimethylbenzene56. 1,3-dichlorobenzene57. benzyl chloride58. 1,4-dichlorobenzene59. 1,2-dichlorobenzene60. 1,2,4-trichlorobenzene61. hexachloro-1,3-butadiene

GC_AR00748



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Air

Massachusetts APH Mix

Rtx®-1

Column: Rtx®-1, 60m, 0.32mm ID, 1.0µm (cat.# 10157)Sample: Massachusetts APH Mix, (cat.# 34540)Concentrator: Nutech 3550A Air Preconcentrator, 100mL of a 40ppbv standard

concentrated at -160°C, thermally desorbed at 150°C and cryofocused at -185°C

Carrier gas: helium Flow rate: 1mL/min. Oven temp.: 35°C (hold 1 min.) to 220°C @ 8°C/min. Det: MS, Agilent 5971Transfer line temp.: 250°CScan range: 35-280amuIonization: EIMode: scan

1. 1,3-butadiene2. isopentane3. methyl tert-butyl ether4. hexane5. benzene6. cyclohexane7. 2,3-dimethylpentane8. heptane9. toluene-D8

10. toluene11. octane12. ethylbenzene13. 2,3-dimethylheptane

14a. m-xylene 14b. p-xylene15. o-xylene16. nonane17. isopropylbenzene18. 1-methyl-3-ethylbenzene19. 1,3,5-trimethylbenzene20. decane21. 1,2,3-trimethylbenzene22. p-isopropyltoluene23. butylcyclohexane24. undecane25. dodecane

GC_AR00697

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GC CHROMATOGRAMS | FOODS, FLAVORS & FRAGRANCES

Antioxidants/Preservatives

Column: Rtx®-50, 30m, 0.53mm ID, 0.50µm (cat.# 10540)Sample: 50ppm each in methanol Inj.: 1.0µL direct, gooseneck splitless inlet liner, 4mm (cat.# 20798)Inj. temp.: 280°CCarrier gas: helium, constant pressure Linear velocity: 60cm/sec. @ 50°COven temp.: 50°C to 240°C @15°C/min. (hold 3 min.)Det.: FID @ 280°C

BHA and BHT

Rtx®-50

GC_FF00630

1. butylated hydroxyanisole (BHA)2. butylated hydroxytoluene (BHT)

Column: Rtx®-20, 30m, 0.53mm ID, 0.5µm (cat.# 10340)Sample: 1mg/mL each component in isooctane Inj.: 1.0µL split (split ratio 20:1), 4mm inlet liner (cat.# 20814)Inj. temp.: 320°CCarrier gas: hydrogen, constant flow Flow rate: 5.2mL/min.Oven temp.: 270°C to 290°C @ 2°C/min.

290°C to 320°C @ 10°C/min. (1 min. hold)Det.: FID @ 320°C

Tocopherols and Tocotrienols

Rtx®-20

GC_FF00634

1. δ-tocopherol2. β-tocopherol3. γ-tocopherol4. dl-δ-tocotrienol5. α-tocopherol6. dl-β-tocotrienol7. dl-γ-tocotrienol8. hexadecyl hexadecanoate9. dl-α-tocotrienol

ChromatogramSearch Tool

Search by compound name, synonym,CAS # or keyword


611-622_GCappChiral.qxp 11/22/2010 9:12 PM Page 611

Rosemary Oil

Rt®-βDEXsm

1. (-/+)α-pinene2. (+/-)camphene3. (+/-)β-pinene4. (-/+)limonene5. eucalyptol (1,8-cineole)6. (-/+)linalool7. (+/-)camphor8. (-/+)terpinen-4-ol9. (+/-)isoborneol

10. (+/-)borneol11. (+/-)α-terpineol

Column: Rt®-βDEXsm, 30m, 0.32mm ID, 0.25µm(cat.# 13104)

Oven temp.: 40°C (hold 1 min.) to 200°C@ 2°C/min. (hold 3 min.)

Carrier gas: hydrogenLinear velocity: 80cm/sec.Det.: FID @ 220°C

min. 0 10 20 30 40

1

2

3

3

4

4

5

6

7

8

9

10

1111109

GC_FF00147

Geranium Oil (Commercial)

Rt®-βDEXsa

1a. (+)-(2R,4S)-cis-rose oxide1b. (-)-(2S,4R)-cis-rose oxide2a. (-)-(2R,4R)-trans-rose oxide2b. (+)-(2S,4S)-trans-rose oxide3. isomenthone4. menthone5a. (-)-(R)-linalool5b. (+)-(S)-linalool6a. (-)-(S)-β-citronellol6b. (+)-(R)-β-citronellol7. geraniol8. citronellyl formate

Column: Rt®-βDEXsa, 30m, 0.25mm ID, 0.25µm (cat.# 13109)

Oven temp.: 60°C to 110°C @ 1°C/min. (hold 30 min.) Carrier gas: hydrogenLinear velocity: 40cm/sec. set @ 60°CDet.: FID @ 220°C

min. 20 30 40 50 60

1a1b

2a

2b

3

4

5a 5b

6a 6b

7

8

GC_FF00148

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Chiral Separations


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Chiral Separations

Irone Isomers - Rt®-βDEXcst

1. (-)-(2R,6R)-trans-α-irone2. (+)-(2S,6S)-trans-α-irone3. (+)-(2R,6R)-trans-γ-irone4. (-)-(2S,6S)-trans-γ-irone5. (+)-(2R,6S)-cis-α-irone6. (+)-(2R,6S)-cis-γ-irone7. (-)-(2S,6R)-cis-γ-irone8. (-)-(2S,6R)-cis-α-irone9. (+)-(2R)-β-irone

10. (-)-(2R)-β-irone

Column: Rt®-βDEXcst, 30m, 0.32mm ID, 0.25µm (cat.# 13102)

Oven temp.: 40°C (hold 1 min.) to 230°C @ 2°C/min. (hold 3 min.)

Carrier gas: hydrogenLinear velocity: 80cm/sec. set @ 40°C Det.: FID @ 220°C

1 2

3

4

5

6

7

8

910

min. 40

GC_FF00150

1-octen-3-ol and carvone - Rt®-βDEXsa




1

min. 20 30 40

21. (+/-)1-octen-3-ol2. (-)carvone3. (+)carvone

3

GC_FF00151

γ-lactones - Rt®-βDEXcst

1. (+/-)γ-heptalactone2. (+/-)γ-octalactone3. (+/-)γ-nonalactone4. (+/-)γ-decalactone5. (+/-)γ-dodecalactone


Oven temp.: 60°C (hold 1 min.) to 200°C @ 1°C/min.


min. 100 120 140

1

2

3

4

5

GC_FF00152

β-citronellol - Rt®-βDEXsa



Carrier gas: hydrogenLinear velocity: 80cm/sec. set @ 40°CDet.: FID @ 220°C

min. 51 52 53

1 2

1. (-)-(S)-β-citronellol2. (+)-(R)-β-citronellol

GC_FF00153

δ-lactones - Rt®-βDEXcst

1. (+/-)δ-pentalactone2. (+/-)δ-hexalactone3. (+/-)δ-heptalactone4. (+/-)δ-octalactone5. (+/-)δ-nonalactone6. (+/-)δ-decalactone7. (+/-)δ-dodecalactone


Oven temp.:60°C (hold 1 min.) to 200°C @ 1°C/min.

Carrier gas:hydrogen

Linear velocity: 40cm/sec. set @ 60°C

Det.:FID @ 220°C

1

2

34

5

6

7

min. 100 120 140

GC_FF00154




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Chiral Separations

Apple Juice with Standards

Rt®-βDEXse

1

2

3

4

min. 8 10 12 14

Column: Rt®-βDEXse, 30m, 0.32mm ID, 0.25µm (cat.# 13106)Inj.: 1.0µL split injectionOn-column conc.

(standards): ~50ngOven temp.: 40°C (hold 1 min.) to 220°C @ 2°C/min.Inj./det. temp.: 220°CCarrier gas: hydrogenLinear velocity: 80cm/sec.

1. (R)-ethyl 2-methylbutyrate2. (S)-ethyl 2-methylbutyrate3. (R)-2-methylbutyrate4. (S)-2-methylbutyrate

GC_FF00157

Apple Juice

Rt®-βDEXse

2

3

min. 8 10 12 14

GC_FF00158

Grape Juice Extract

Rt®-γDEXsa

1. methyl (S)-(+)-3-hydroxybutyrate2. methyl (R)-(+)-3-hydroxybutyrate3. ethyl (S)-(+)-3-hydroxybutyrate4. ethyl (R)-(+)-3-hydroxybutyrate

Column: Rt®-γDEXsa, 30m, 0.32mm ID, 0.25µm (cat.# 13112)Inj.: 1.0µL split injectionOn-column conc.: ~150ng/enantiomerOven temp.: 40°C (hold 1 min.) to 200°C @ 2°C/min.Inj./det. temp.: 220°C/230°CCarrier gas: hydrogenLinear velocity: 80cm/sec. set @ 40°CSplit ratio: 25:1

min. 20 22 24 26 28

1

2

4

3

GC_FF00159

Bergamot Flavor

Rt®-βDEXse

Column: Rt®-βDEXse, 30m, 0.32mm ID, 0.25µm (cat.# 13106) Oven temp.: 40°C (hold 1 min.) to 200°C @ 4°C/min. Carrier gas: helium, 60cm/sec. set @ 40°CDet.: MS @ 220°C

1. (S)-limonene 2. (R)-limonene 3. (R)-linalool 4. (S)-linalool 5. (R)-linalyl acetate 6. (S)-linalyl acetate

min. 8 13 18

1

2

34

5 6

GC_FF00163


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Fatty Acids

Fatty Acids (Free)

Rtx®-200

1

2

34

5

67 8

9

min. 1 2 3 4GC_CH00282

Column: Rtx®-200, 30m, 0.25mm ID, 0.25µm (cat.# 15023)Sample: 0.8µL split injection of a free fatty acid standardConc.: approximately 10 to 20ng/µLOven temp.: 90°CInj./det. temp.: 250°CCarrier gas: hydrogenLinear velocity: 40cm/sec. (flow rate: 1.4cc/min.)FID sensitivity: 4 x 10-11 AFSSplit vent: 40cc/min.

1. acetic acid2. propionic acid3. isobutyric acid4. n-butyric acid5. isovaleric acid6. n-valeric acid7. isocaproic acid8. caproic acid9. heptanoic acid

Fatty Acids (Free)

Stabilwax®-DA

Column: Stabilwax®-DA, 30m, 0.25mm ID, 0.25µm (cat.# 11023)

Sample: 1.0µL split injection of a free acid standardConc.: approximately 10 to 20ng/µLOven temp.: 145°CInj./det. temp.: 250°CCarrier gas: hydrogenLinear velocity: 40cm/sec.FID sensitivity: 2 x 10-11 AFSSplit ratio: 50:1

GC_CH00280

min. 4 8 12

9

87

6

5

4

1

3

2


Fatty Acids (Free)

Rtx®-1

GC_CH00281min. 4 8

1

2

3 4

56

7 8 9

Column: Rtx®-1, 30m, 0.53mm ID, 5.0µm (cat.# 10179)Sample: 0.2µL injection of a 10–20ng/µL free fatty acid

standard in water.Inj.: direct injection using a Uniliner® inlet linerOven temp.: 60°C to 180°C @ 15°C/min.Inj./det. temp.: 250°CCarrier gas: hydrogenLinear velocity: 50cm/sec. (flow rate: 6cc/min.)FID sensitivity: 4 x 10-11 AFS


No derivatization

needed!

No derivatization

needed!

No derivatization

needed!

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Fax: 814-353-1309—24-hours a day


Outside the U.S.Contact your Restek representative:Refer to our list on pages 4-5 or visit our website atwww.restek.com

Paula Zuchowski, Customer Service


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Fatty Acids

Fatty Acids (Free)

Stabilwax®-DA

GC_FF00653

Column: Stabilwax®-DA, 30m, 0.32mm ID, 0.25µm (cat.# 11024)Sample: 1.0µL free fatty acid mixSolvent: methanolConc.: 100ppm in methanolInj.: splitless/250°CSplitless hold time: 0.25min.Carrier gas: hydrogen (constant flow)Flow rate: 6.0mL/min. Split flow: 75mL/min.Det.: FID @ 250°CInlet liner: laminar cup splitter Oven temp.: 40°C to 250°C @ 10°C/min. (hold 15 min.)

1. C4:0 - butyric acid2. C6:0 - caproic acid3. C8:0 - caprylic acid4. C10:0 - capric acid5. C12:0 - lauric acid6. C14:0 - myristic acid7. C16:0 - palmitic acid8. C18:0 - stearic acid9. C18:1 - oleic acid

10. C18:2 - linoleic acid11. C18:3 - linolenic acid12. C20:0 - arachidic acid13. C22:0 - behenic acid

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FAMEs

GC_FF00649

FAMEs (AOAC 996.06 Standard)

Rt®-2560

Column: Rt®-2560, 100m, 0.25mm ID, 0.2µm (cat.# 13199)Sample: Food Industry FAME Mix (cat.# 35077),

30mg/mL total FAMEs in methylene chloride Inj.: 2.0µL split (split ratio 200:1), 4mm inlet liner (cat.# 20814)Inj. temp.: 225°CCarrier gas: hydrogen, constant flow Flow rate: 1.2mL/min.Oven temp.: 100°C (4 min. hold) to 240°C @ 3°C/min. (10 min. hold) Det.: FID @ 250°C

CCoommppoouunndd %% iinn MMiixx1. C4:0 methyl butyrate 4.02. C6:0 methyl hexanoate 4.03. C8:0 methyl octanoate 4.04. C10:0 methyl decanoate 4.05. C11:0 methyl undecanoate 2.06. C12:0 methyl laurate 4.07. C13:0 methyl tridecanoate 2.08. C14:0 methyl myristate 4.09. C14:1 methyl myristoleate (cis-9) 2.0

10. C15:0 methyl pentadecanoate 2.011. C15:1 methyl pentadecenoate (cis-10) 2.012. C16:0 methyl palmitate 6.013. C16:1 methyl palmitoleate (cis-9) 2.014. C17:0 methyl heptadecanoate 2.015. C17:1 methyl heptadecenoate (cis-10) 2.016. C18:0 methyl stearate 4.017. C18:1 methyl elaidate (trans-9) 2.018. C18:1 methyl oleate (cis-9) 4.019. C18:2 methyl linoleaidate (trans-9,12) 2.020. C18:2 methyl linoleate (cis-9,12) 2.021. C20:0 methyl arachidate 4.022. C18:3 methyl γ-linolenate (cis-6,9,12) 2.023. C20:1 methyl eicosenoate (cis-11) 2.024. C18:3 methyl linolenate (cis-9,12,15) 2.025. C21:0 methyl heneicosanoate 2.026. C20:2 methyl eicosadienoate (cis-11,14) 2.027. C22:0 methyl behenate 4.028. C20:3 methyl eicosatrienoate (cis-8,11,14) 2.029. C22:1 methyl erucate (cis-13) 2.030. C20:3 methyl eicosatrienoate (cis-11,14,17) 2.031. C20:4 methyl arachidonate (cis-5,8,11,14) 2.032. C23:0 methyl tricosanoate 2.033. C22:2 methyl docosadienoate (cis-13,16) 2.034. C24:0 methyl lignocerate 4.035. C20:5 methyl eicosapentaenoate (cis-5,8,11,14,17) 2.036. C24:1 methyl nervonate (cis-15) 2.037. C22:6 methyl docosahexaenoate (cis-4,7,10,13,16,19) 2.0

Food Industry FAME Mixcat.# 35077

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FAMEs

FAMEs (NLEA Mix)

Rt®-2560

Column: Rt®-2560, 100m, 0.25mm ID, 0.20µm (cat.# 13199)Sample: NLEA FAME Mix (cat.# 35078), 30mg/mL

total FAMEs in methylene chloride Inj.: 1.0µL split (split ratio 100:1),

4mm inlet liner (cat.# 20814)Inj. temp.: 225°CCarrier gas: hydrogen, constant flow Flow rate: 1.2mL/min.Oven temp.: 100°C (4 min. hold) to 240°C @ 3°C/min. (10 min. hold) Det.: FID @ 250°C

1. C4:0 methyl butyrate2. C6:0 methyl hexanoate3. C8:0 methyl octanoate4. C10:0 methyl decanoate5. C11:0 methyl undecanoate6. C12:0 methyl laurate7. C13:0 methyl tridecanoate8. C14:0 methyl myristate9. C14:1 methyl myristoleate (cis-9)

10. C15:0 methyl pentadecanoate

11. C16:0 methyl palmitate12. C16:1 methyl palmitoleate (cis-9)13. C17:0 methyl heptadecanoate14. C18:0 methyl stearate15. C18:1 methyl elaidate (trans-9)16. C18:1 methyl oleate (cis-9)17. C18:2 methyl linoelaidate (trans-9,12)18. C18:2 methyl linoleate (cis-9,12)19. C20:0 methyl arachidate20. C20:1 methyl eicosenoate (cis-11)

21. C18:3 methyl linolenate (cis-9,12,15)22. C22:0 methyl behenate23. C22:1 methyl erucate (cis-13)24. C23:0 methyl tricosanoate25. C24:0 methyl lignocerate26. C20:5 methyl eicosapentaenoate (cis-5,8,11,14,17)27. C24:1 methyl nervonate (cis-15)28. C22:6 methyl docosahexaenoate (cis-4,7,10,13,16,19)

GC_FF00651

NLEA FAME Mixcat.# 35078

An Rt®-2560 column providesthe resolution of cis & transFAMEs needed for AOACMethod 996.06.

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FAMEs

GC_FF00652

FAMEs (cis/trans isomers)

Rt®-2560

Column: Rt®-2560, 100m, 0.25mm ID, 0.2µm (cat.# 13199)Sample: cis/trans FAME Mix (cat.# 35079), 10mg/mL total FAMEs in methylene chloride Inj.: 1.0µL split (split ratio 20:1), 4mm inlet liner (cat.# 20814)Inj. temp.: 225°CCarrier gas: hydrogen, constant flow Flow rate: 1.2mL/min.Oven temp.: 100°C (4 min. hold) to 240°C @ 3°C/min. (10 min. hold) Det.: FID @ 250°C

CCoommppoouunndd %% iinn MMiixx1. C18:0 methyl stearate 20.02. C18:1 methyl petroselaidate (trans-6) 8.03. C18:1 methyl elaidate (trans-9) 10.04. C18:1 methyl transvaccenate (trans-11) 12.05. C18:1 methyl petroselinate (cis-6) 8.06. C18:1 methyl oleate (cis-9) 10.07. C18:1 methyl vaccenate (cis-11) 12.08. C18:2 methyl linoleate (cis-9,12) 20.0

cis/trans FAME Mixcat.# 35079

Excellent resolution of

cis & trans isomers!

5,6

FAMEs (cis/trans isomers)

Rtx®-Wax

Column: Rtx®-Wax, 60m, 0.25mm ID, 0.25µm (cat.#12426)On-column conc.: 40–75ngOven temp.: 165°C to 250°C @ 2°C/min. Inj./det. temp.: 220°C/250°CCarrier gas: heliumLinear velocity: 20cm/sec. set @ 165°CSplit ratio: 50:1

1

3

2

4

7

8

9

10

12

11

13

14

1. C14:02. C14:1n5 cis3. C14:1n5 trans4. C16:05. C16:1n7 cis6. C16:1n7 trans7. C18:08. C18:1 cis isomers

(n12, n9, n7)

9. C18:1 trans isomers(n12, n9, n7)

10. C18:2n6 cis11. C18:2n6 trans12. C20:013. C20:1n9 cis14. C20:1n9 trans

min. 12 14 16 18 20 22 24 26 28 30 32 34 36GC_FF00121


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FAMEs

FAMEs (Marine Oil Standard)

FAMEWAX

GC_FF00568

1. C14:02. C15:03. C16:04. C16:15. C16:26. C17:07. C17:18. C16:49. C18:0

10. C18:1 (oleate)11. C18:1 (vaccenate)12. C18:2n6cis13. C18:3n314. C18:4n6

15. C18:4n316. C20:017. C20:1n718. C20:1n919. C20:4n620. C20:4n321. C20:5n322. C22:1n723. C21:5n324. C23:0 (IS)25. C22:5n626. C22:5n327. C22:6n328. C24:1

Column: FAMEWAX, 30m, 0.32mm ID, 0.25µm (cat.# 12498)Sample: 12mg/mL total FAMEsInj.: 0.5µL, split (150:1), 3mm ID split liner for TRACE Series GCs, packed

with glass wool (cat.# 20936-202.1)Inj. temp.: 250°CCarrier gas: hydrogen, constant flowLinear velocity: 62cm/sec.Oven temp.: 195°C to 240°C @ 5°C/min. (hold 1 min.)Det.: FID @ 250°C

FAST analysis!

PPeeaakk LLiisstt CCoonncc.. ((µµgg//mmLL))1. C14:0 6002. C14:1 1003. C16:0 1,6004. C16:1 5005. C18:0 8006. C18:1 (oleate) 1,3007. C18:1 (vaccenate) 4008. C18:2 2009. C18:3 200

10. C20:0 10011. C20:1 90012. C20:2 10013. C20:4 30014. C20:3 10015. C20:5 1,00016. C22:0 10017. C22:1 30018. C24:0 10019. C22:6 1,20020. C24:1 100

FAMEs (Marine Oil Standard)

FAMEWAX

Column: FAMEWAX, 30m, 0.32mm ID, 0.25µm (cat.# 12498)Inj.: 1µLConc.: 10,000µg/mL in isooctane (total FAMES; see breakdown in peak list)Oven temp.: 195–240°C at 5°C/min., 1 min. holdInj./det. temp.: 250°C/275°CCarrier gas: hydrogenFlow rate: 3mL/min. (constant flow)Split ratio: 100:1

GC_FF00499

Column engineered

for optimal resolution.


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FAMEs

FAMEs (Cocoa Butter)

Stabilwax®

Column: Stabilwax®, 30m, 0.25mm ID, 0.25µm (cat.# 10623)Sample: 1.0µL split injection of a FAME reference standard for

cocoa butter.Oven temp.: 200°C to 250°C @ 8°C/min. (hold 3 min.)Inj./det. temp.: 250°CCarrier gas: hydrogenLinear velocity: 31.4cm/sec. set @ 200°CFID sensitivity: 8 x 10-11 AFSSplit ratio: 45:1

1. C14:02. C16:03. C16:1n74. C17:05. C18:06. C18:1n97. C18:2n68. C18:3n39. C20:0

10. C20:1n911. C22:0

GC_FF00120

1

3

2 6

7

5

9

10114

min. 2 4 6 8

8

GC_FF00538

Column: Rtx®-Wax, 30m, 0.25mm, 0.25µm (cat.# 12423)Sample: 1µL split injection of saw palmetto standardConc.: see peak listOven temp.: 120°C (hold 3 min.) to 220°C

at 20°C/min. (hold 12 min.)Inj./det. temp.: 250°C/300°CCarrier gas: heliumLinear velocity: 1mL/min. (34 cm/sec.)Split ratio: 100:1

FAMEs (Saw Palmetto)

Rtx®-Wax PPeeaakk LLiisstt CCoonncc.. ((mmgg//mmLL))1. methyl caproate (C6:0) 0.42. methyl caprylate (C8:0) 0.43. methyl nonanoate (C9:0) 2.04. methyl caprate (C10:0) 0.45. methyl laurate (C12:0) 5.06. methyl myristate (C14:0) 2.07. methyl palmitate (C16:0) 2.08. methyl palmitoleate (C16:1) 0.49. methyl stearate (C18:0) 0.4

10. methyl oleate (C18:1) 5.011. methyl linoleate (C18:2) 1.012. methyl linolenate (C18:3) 0.4

5

FAMEs (PUFA, animal source)

Rt®-2330

1. C14:02. C16:03. C16:1n74. C18:05. C18:1n96. C18:1n77. C18:2n68. C18:3n69. C18:3n3

10. C20:3n611. C20:4n612. C20:5n313. C22:4n614. C22:5n315. C22:6n3

Column: Rt®-2330, 30m, 0.32mm ID, 0.20µm (cat.# 10724)

Sample: 0.1µL split injection of PUFA 2 mixOven temp.: 160°C to 250°C @ 2°C/min. (hold 10 min.)Inj./det. temp.: 260°CCarrier gas: hydrogenLinear velocity: 40cm/sec. FID sensitivity: 8 x 10-11 AFSSplit ratio: 20:1

min. 4 8 12 16 20 24 28

1

2

3

4

6

7

8

9

10

11

12

13

14

15

GC_FF00119

87

13

FAMEs (PUFA, marine source)

Rt®-2330

Column: Rt®-2330, 30m, 0.25mm ID, 0.20µm (cat.# 10723)

Sample: 0.5µL split injection of a PUFA mixOven temp.: 160°C to 225°C @ 2°C/min. Inj./det. temp.: 225°C/250°CCarrier gas: hydrogenLinear velocity: 45cm/sec. set @ 160°CFID sensitivity: 8 x 10-11 AFSSplit ratio: 35:1

1

2

3 4

65

9

11

10

12

14

15

1617

18

min. 5 10 15 20GC_FF00118

1. C14:02. C16:03. C16:1n74. C18:1n95. C18:1n76. C18:2n67. C18:3n38. C20:1n119. C20:1n9

10. C20:1n7 11. C18:4n3 12. C22:1n11 13. C22:1n9 14. C20:4n3 15. C20:5n316. C21:5n3 17. C22:5n3 18. C22:6n3


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FAMEs

FAMEs (Evening Primrose Oil)

FAMEWAX

1

2

3

4

5

min. 20 40

1. C16:02. C18:03. C18:1n94. C18:2n65. C18:3n6

GC_FF00363

FAMEs (Flax Seed Oil)

FAMEWAX

min. 20 40

1

2

3

4

61. C16:02. C18:03. C18:1n94. C18:2n65. C18:3n66. C18:3n3

GC_FF00364

FAMEs (Black Currant Seed Oil)

FAMEWAX

min. 20 40

1

2

3

4

5

6

GC_FF00365

1. C16:02. C18:03. C18:1n94. C18:2n65. C18:3n66. C18:3n3

FAMEs (Borage Seed Oil)

FAMEWAX

CCoolluummnn aanndd ccoonnddiittiioonnss ffoorr aallll ffoouurr ooiillss aannaallyysseess::Column: FAMEWAX, 30m, 0.25mm ID, 0.25µm (cat.# 12497)Oven temp.: 165°C (hold 30 min.) to 220°C @

1.5°C/min. (hold 15 min.) Inj. temp.: 225°CDet. temp.: 230°CCarrier gas: helium @ 40cm/sec.

min. 20 40

1

2

3

4

5

GC_FF00366

1. C16:02. C18:03. C18:1n94. C18:2n65. C18:3n6


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Sterols, Food Testing

Phytosterols (Saw Palmetto)

Rtx®-5

1. cholesterol2. brassicasterol3. campesterol4. stigmasterol5. β-sitosterol

Column: Rtx®-5, 60m, 0.25mm ID, 0.25µm (cat.# 10226)Inj.: 1µL splitless injection*Oven temp.: 200°C (hold 1 min.) to 340°C @ 15°C/min. (hold 10 min.)Inj./FID temp.: 345°C/355°C

*Split injection may be used, but results can have greater variability. Asplit flow of 112mL/min. is suggested.

1

2

3

4

5

min. 5 10GC_FF00368

Chromatogram provided by the Institute for Nutraceutical Advancement (INA)

GC_FF01046

Egg Pasta: Sterols & Glycerides

Rtx®-65TG

1. squalene (IS)2. cholesterol3. β-sitosterol4. diglycerides5. triglycerids

Column: Rtx®-65TG, 30m, 0.25mm ID, 0.10µm (cat.# 17008)Sample: 50µg/mL fat extract from egg pasta in diethyl ether solution with 3,000ppm squalene (IS)Inj.: 0.5µL, split (1:80), 70°C (hold 12 sec.) at 99°C up to 370°C (hold 5 min.)Carrier gas: hydrogen Flow rate: 1.5mL/min. Oven temp.: 220°C (hold 2.0 min.) to 360°C @ 5°C/min. (hold 5 min.) Det: FID @ 370°C



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Triglycerides

Triglycerides (Butter)

Rtx®-65TG

min. 0 10 20 30 40

T26 T28 T32 T34 T36 T38 T40 T42 T44 T46 T48 T50 T54T52

Column: Rtx®-65TG, 30m, 0.25mm ID, 0.10µm (cat.# 17008)Sample: 0.2µL cold on-column injection of 1% butterfat in isooctaneOven temp.: 80°C (hold 1 min.) to 240°C @ 30°C/min.

to 360°C @ 4°C/min. (hold 5 min.)Det. temp.: 380°CCarrier gas: hydrogenLinear velocity: 70cm/sec. FID sensitivity: 16 x 10-11 AFSSPI injector: high performance capillary insert 60°C,

300°C/min. to 400°C (hold 5 min.)

GC_FF00137

Technical ServiceDo you have a technical question? Restek’s Technical Service group hasanswers! Drawing from our extensive libraries of technical informationand many years of collective chromatography experience, the experts inTechnical Service can help you from set-up to method development.

Contact us:

For quick answers to commonly asked questions any time of the day,visit www.restek.com/answers or contact us directly:

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Outside the U.S.Contact your Restek representative.

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Cholesterols, Essential Oils

Underivatized Cholesterol

Rxi®-5ms

GC_FF00881

GC_FF00882

B. Isothermal conditions will maximize sample throughput.

Oven temp.: 300°C (hold 10 min.)

A. Temperature program conditions.

Oven temp.: 200°C (hold 1 min.) to 330°C @ 20°C/min. (hold 7.5 min.)

Column: Rxi®-5ms, 15m, 0.25mm ID, 0.25µm (cat.# 13420)Sample: 1,000µg/mL cholesterol in DMF, 1000µg/mL 5-α-cholestane in hexane;

25ng cholesterol, 150ng 5-α-cholestane on columnInj.: 1.0µL, split (20:1), single gooseneck inlet liner w/wool (cat.# 22405)Inj. temp.: 250°CCarrier gas: helium, constant pressure (9.7psi @ 200°C)Linear velocity: 24cm/sec.Oven temp.: see aboveDet.: FID @ 340°C

1. 5-α-cholestane (IS)2. cholesterol

Derivatized Cholesterol

Rxi®-5ms

B. Isothermal conditions will maximize

sample throughput.

Oven temp.: 300°C (hold 10 min.)

A. Temperature program conditions.

Oven temp.: 200°C (hold 1 min.) to 330°C @ 20°C/min. (hold 7.5 min.)

Column: Rxi®-5ms, 15m, 0.25mm ID, 0.25µm (cat.# 13420)Sample: 1,000µg/mL cholesterol in hexane, 1000µg/mL 5-α-cholestane in hexane;

50ng derivatized cholesterol, 150ng 5-α-cholestane on columnInj.: 1.0µL, split (20:1), single gooseneck inlet liner w/wool (cat.# 22405)Inj. temp.: 250°CCarrier gas: helium, constant pressure (9.7psi @ 200°C)Linear velocity: 24cm/sec.Oven temp.: see aboveDet.: FID @ 340°C

1. 5-α-cholestane (IS)2. cholesterol

GC_FF00883

GC_FF00884

One column, many

cholesterol methods.

2 3 5

19

Lemon Oil

Rtx®-5

GC_FF00138

min. 2 4 6 8 10 12 14 16 18 20 22 24 26 28

1

4

6

9

7,8

1110

12

13

1415

16

17

18

2021 22

2324

25

26

27,28

29

3031

32

33

34

35

36

38

37

1. heptanol2. α-thujene3. α-pinene4. camphene5. sabinene6. β-pinene7. 6-methyl-5-hepten-2-one8. myrcene9. octanal

10. α-phellandrene11. 3-carene12. α-terpinene13. p-cymene14. limonene15. γ-terpinene16. octanol17. terpinolene18. linalool19. nonanal20. citronellal21. terpinene-4-ol22. α-terpineol23. decanol24. octyl acetate25. nerol26. neral27. carvone28. geraniol29. geranial30. nonyl acetate31. citronellyl acetate32. neryl acetate33. geranyl acetate34. dodecanal35. β-caryophyllene36. trans-α-bergamotene37. α-humulene38. β-bisabolene

Column: Rtx®-5, 30m, 0.32mm ID, 0.25µm (cat.# 10224)Sample: Wet needle split injection of a neat lemon oilOven temp.: 75°C (hold 8 min.) to 250°C @ 4°C/min.Inj./det. temp.: 250°CCarrier gas: hydrogenLinear velocity: 40cm/sec. (flow rate: 3.2cc/min.) FID sensitivity: 2 x 10-11 AFSSplit ratio: 100:1


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Essential Oils

Spearmint Oil (Native )

Stabilwax®

1 2

3

4

5

6 7

8

912

1011

13

14

15

16

17

18

19

20

21

22

23

24

26 27

28

29

30

25

GC_FF00140

1. α-pinene2. β-pinene3. sabinene4. myrcene5. α-terpinene6. l-limonene7. 1,8-cineole8. cis-ocimene9. γ-terpinene

10. p-cymene

11. terpinolene12. 3-octyl acetate13. 3-octanol14. l-menthone15. trans-sabinenehydrate16. β-bourbonene17. linalool18. terpinene-4-ol19. β-caryophyllene20. dihydrocarvone

21. trans-dihydrocarvyl acetate22. β-farnesene23. α-terpineol24. germacrene-Δ25. carvone26. cis-carvyl acetate27. trans-carveol28. cis-carveol29. cis-jasmone30. viridiflorol


Sample: 0.2µL split injection of a neat spearmint oil


Inj./det. temp.: 250°CCarrier gas: hydrogenLinear velocity: 40cm/sec. set @ 160°C FID sensitivity: 4 x 10-11 AFSSplit ratio: 100:1

min. 4 6 8 10 12 14 16 18 20 22 24 26 28 30 32

Synthetic Essential Oil Mixture

Rtx®-11. ethyl butyrate2. trans-2-hexenol3. α-pinene4. benzaldehyde5. camphene6. octanol7. β-myrcene8. β-pinene9. α-phellandrene

10. p-cymene11. l-limonene12. camphor13. trans-sabinene hydrate14. linalool15. citronellal16. l-menthone17. menthofuran18. l-menthol19. α-terpineol20. linalyl acetate21. β-citronellol22. nerol23. carveol

24. anisaldehyde25. carvone26. geraniol27. anethole28. cinnamic alcohol29. eugenol30. neryl acetate31. geranyl acetate32. vanillin33. coumarin34. α-ionone35. ethyl vanillin36. β-caryophyllene37. α-caryophyllene38. β-ionone39. valencene40. ethyl laurate41. amyl cinnamic aldehyde42. nootketone

Column: Rtx®-1, 60m, 0.25mm ID, 0.25µm (cat.# 10126)Sample: 1.0µL split injection of 42 flavor componentsOven temp.: 100°C to 260°C @ 4°C/min. (hold 1 min.)Inj./det. temp.: 250°C/280°CDet. type: MSDCarrier gas: heliumLinear velocity: 30cm/sec. set @ 50°CFID sensitivity: 2 x 10-11 AFSSplit vent: 100cc/min.

min. 10 15 20 25 30GC_FF00534

1

2

3,4

5

6,7

58

910

11,12

913

14

15

16

17

18

20,21

23,24

22

25

26

27

28

29

30

31

32,33

1919

34

35

36

37

38

39

40

41

42


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Essential Oils

min. 6 8 10 12 14 16 18 20 22 24 26 28

1

3

8

13

4

16

912

6

5

117

15

14102

Citronella Java Oil

Rtx®-1

Column: Rtx®-1, 60m, 0.25mm ID, 0.25µm (cat.# 10126)Sample: 1.0µL split injection of citronella Java oilOven temp.: 100°C to 260°C @ 4°C/min. (hold 1 min.)Inj./det. temp.: 250°C/280°CDet. type: MSDCarrier gas: heliumLinear velocity: 30cm/sec. set @ 50°CSplit vent: 100cc/min.

GC_FF00144

Citronella Java Oil

Stabilwax®

Column: Stabilwax®, 60m, 0.25mm ID, 0.25µm (cat.# 10626)Sample: 1.0µL split injection of citronella Java oilOven temp.: 100°C to 260°C @ 4°C/min. (hold 1 min.)Inj./det. temp.: 250°C/280°CDet. type: MSDCarrier gas: heliumLinear velocity: 30cm/sec. set @ 50°CSplit vent: 100cc/min.

min. 5 10 15 20 25

15

16

9

12

13

8

7

6

5

4

3

1 10,11 142

GC_FF00145

1. limonene2. citronellal3. linalool4. borneol5. γ-elemene6. β-caryophyllene7. neryl acetate8. α-terpineol9. germancrene-Δ

10. β-citronellol11. geranyl acetate12. δ-cadenene13. nerol14. geraniol15. eugenol16. α-bergamotene


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Flavors

Flavor Volatiles

Rtx®-1

1. methanol2. acetaldehyde3. ethanol4. acetone5. isopropyl alcohol6. methylene chloride7. hexane8. ethyl acetate9. ethyl propionate

10. n-hexanal

11. ethyl butyrate12. furfural13. trans-2-hexenal14. α-thujene15. α-pinene16. camphene17. sabinene18. β-pinene19. octanal20. myrcene

21. α-phellandrene22. α-terpinene23. p-cymene24. δ-limonene25. γ-terpinene26. octanol27. terpinolene28. nonanal29. linalool30. cis-limonene monoxide

31. trans-limonene monoxide32. citronellal33. terpinene-4-ol34. α-terpineol35. decanal36. d & l carveol37. neral38. carvone39. geranial40. neryl acetate

41. geranyl acetate42. α-ionone43. β-caryophyllene44. trans-α-bergamotene45. BHA46. β-ionone47. valencene48. γ-elemene49. β-bisabolene50. nootketone

Column: Rtx®-1, 60m, 0.53mm ID, 0.50µm (cat.# 10143)Sample: 0.8µL split injection of a flavor volatiles test mixOven temp.: 70° (hold 15 min.) to 190°C @ 2°C/min. (hold 5 min.)Inj./det. temp.: 220°C/260°CCarrier gas: heliumLinear velocity: 20cm/sec. set @ 70°CFID sensitivity: 64 x 10-11 AFSSplit ratio: 20:1

50

49

47

48

4645

44

43

4241

40

39

38

37

36

35

34

33

32

3130

28,29

27262524

23

22

21

19,201817

16

151413121011

9

7,8

6

1,23 4,5

min. 4 8 12 16 20 24 28 32 36 40 44 48 52 56 60 64 68 72 76 80GC_FF00536

min. 4 8 12 16 20 24 28 32 36 40 44 48 52 56 60 64 68 72

1. hexane2. acetaldehyde3. acetone4. methanol5. ethyl acetate6. isopropyl alcohol7. ethanol8. methylene chloride9. ethyl propionate

10. α-pinene11. ethylbutyrate12. n-hexanal13. β-pinene14. sabinene15. myrcene16. δ-limonene17. 1,8-cineole18. trans-2-hexenal

19. γ-terpinene20. p-cymene21. terpinolene22. octanal23. nonanal24. cis-limonene monoxide25. trans-limonene26. furfural27. citronellal

28. decanal29. linalool30. octanol31. trans-α-bergamotene32. β-caryophyllene33. terpinene-4-ol34. neral35. α-terpineol36. neryl acetate

37. valencene38. geranial39. carvone40. geranyl acetate41. d/l carveol42. α-ionone43. d/l carveol44. β-ionone

Column: Stabilwax®, 60m, 053mm ID, 0.50µm (cat.# 10643)Sample: 0.8µL split injection of a flavor volatiles test mixOven temp.: 70°C (hold 15 min.) to 190°C @ 2°C/min. (hold 5 min.)Inj./det. temp.: 220°C/260°CCarrier gas: heliumLinear velocity: 20cm/sec. set @ 70°CFID sensitivity: 64 x 10-11 AFSSplit ratio: 20:1

Flavor Volatiles

Stabilwax®

4443

424140

38

3937

36

35

34

33

32

31

30

29

28

27

26

2524

23

22

2120

19

18

1716151413

121110

9

7,84,5

3

21

6

GC_FF00537


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Flavors: Beverage Analysis

Malt Whiskey

Stabilwax®-DA

Column: Stabilwax®-DA, 30m, 0.18mm ID, 0.18µm (cat.# 550752)Inj.: 10µL large volume injection (splitless),

at 10µL/min.Std. conc.: neatGerstel CIS Injector: 35°C (hold 2 min.), to 300°C @

10°C/sec. (hold 5 min.)Helium vent flow: 600mL/min. with 1.8 min. vent end timeCarrier gas: heliumLinear velocity: 45cm/sec.Oven temp.: 60°C (hold 2 min.) to 100°C @

20°C/min., to 240°C @ 5°C/min.(hold 10 min.)

Det.: MSDTransfer line temp.: 240°CQuadrupole temp.: 150°CMS source temp.: 230°CScan range: 30–400amuIonization: 70eVMode: EI

Chromatogram courtesy of Kevin MacNamara, Ph.D., Irish Distilleries, Ltd.

1. ethyl octanoate2. acetic acid3. siloxane4. 1-hydroxy-2,3-butadione5. 1-hydroxy-2-propanone acetate6. furfural7. formic acid8. propionic acid9. isobutyric acid

10. dimethyl sulfoxide11. 5-methyl furfural12. methyl decanoate + unknown13. butyric acid14. siloxane15. ethyl decanoate16. furfuryl alcohol17. isoamyl octanoate18. isovaleric acid19. 2-methylbutyric acid20. diethyl succinate21. 3-methyl-2(5H)-furanone (possible)22. valeric acid

23. ethyl undecanoate24. isobutyl decanoate25. 2(5H)-furanone26. unknown27. di(ethyleneglycol) butyl ether28. siloxane29. methyl dodecanoate30. 2-phenylethyl acetate31. methylcyclopentenolone32. hexanoic acid33. ethyl dodecanoate34. isoamyl decanoate35. guaiacol36. dodecyl acetate (possible)37. whiskey lactone (1)38. 2-phenylethanol39. heptanoic acid40. siloxane41. dimethoxybenzene or 4-methyl-

guaiacol42. whiskey lactone (2)43. dodecanol

44. unknown45. phenol46. methyl tetradecanoate47. nerolidol48. diethyl malate49. ethyl tetradecanoate50. octanoic acid51. unknown52. p-cresol53. siloxane54. diethyl octanedioate55. monomethyl succinate (possible)56. 3,5-dimethyl-2,4(5H)furandione57. nonanoic acid58. diethyl 2-hydroxyglutarate59 unknown60. tetradecanol61. 4-vinylguaiacol62. diethyl nonanedioate63. methyl hexadecanoate64. ethyl γ-lactone 2-hydroxyglutarate65. ethyl hexadecanoate

66. decanoic acid67. ethyl 9-hexadecanoate68. triacosan69. unknown70. phthalide71. diethyl phthalate72. hexadecanol73. 4-hydroxycinnamic acid (decomp.)74. methyl stearate75. benzoic acid76. methyl 8-octadecenoate77. ethyl stearate78. dodecanoic acid79. hydroxymethylfurfural80. ethyl linoleate81. 4-allyl-2,6-dimethoxyphenol82. diisobutyl phthalate83. vanillin84. sinapic acid (decomp.)85. 2-phenylethyl decanoate

+2 unknowns86. 4-propenyl-2,6-dimethoxyphenol

87. ethyl vanillate88. acetovanillone89. vanillin methyl ketone90. tetradecanoic acid91. ethyl homovanillate92. propiovanillone93. fatty acid ester94. (similar to 4-allyl-2,6-

dimethoxyphenol)95. unknown96. hexadecanoic acid97. syringealdehyde

GC_FF00603


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Rum

Rtx®-13011. acetaldehyde2. methanol3. ethanol4. acetone5. ethyl formate6. isopropanol7. n-propanol8. ethyl acetate

9. sec-butanol10. isobutanol11. isoamyl alcohol12. active amyl alcohol13. n-amyl alcohol

Column: Rtx®-1301, 60m, 0.25mm ID, 1.4µm (cat.# 16016)Inj.: 1.0µL split injection using a Cyclosplitter® inlet liner (cat.# 20706)Conc.: neatOven temp.: 35°C (hold 5 min.) to 100°C @ 1°C/min.Inj./det. temp.: 150°C/200°CCarrier gas: hydrogen @ 40cm/sec.Split ratio: 100:1

min. 5 10 15 20 25

1

2

4

5

6

7

8

3

9

1011

12

13

GC_FF00110

Rum

CarboBlack B

Column: 5% Carbowax® 20M 80/120 CarboBlack B, 2m, 1/8" OD, 2mm ID SilcoSmooth® tubing(cat.# 80105)

Inj.: 0.5µL on-column injection, neatOven temp.: 65°C (hold 5 min.) to 150°C @

4°C/min.Inj./det. temp.: 200°C/250°CDet.: FIDCarrier gas: nitrogenColumn flow rate: 20mL/min.FID sensitivity: 1.28 x 10-10 AFS

1

2

3

4

5

6

7

8

9

12

11

10

min. 10 20GC_FF00111

1. acetaldehyde2. methanol3. acetone4. ethyl formate5. ethanol6. ethyl acetate7. n-propanol8. sec-butanol9. isobutanol

10. active amyl alcohol11. isoamyl alcohol12. n-amyl alcohol

Scotch

CarboBlack B

Column: 5% Carbowax® 20M 80/120 CarboBlack B, 2m, 1/8" OD, 2mm ID SilcoSmooth® tubing (cat.# 80105)

Inj.: 0.5µL on-column injection, neatOven temp.: 70°C to 150°C @ 4°C/min.Inj./det. temp.: 200°C/250°CDet.: FIDCarrier gas: nitrogenColumn flow rate: 20mL/min.FID sensitivity: 1.28 x 10-10 AFS

1. acetaldehyde2. methanol3. ethanol4. ethyl acetate5. n-propanol6. isobutanol7. acetic acid8. active amyl alcohol9. isoamyl alcohol

12

4

5

6

9

8

7

min. 5 10 15

3

GC_FF00113

Scotch

Rtx®-1301

Column: Rtx®-1301, 60m, 0.25mm ID, 1.4µm (cat.# 16016)Inj.: 1.0µL split injection using a Cyclosplitter® inlet liner (cat.# 20706)Conc.: neatOven temp.: 35°C (hold 5 min.) to 100°C @ 1°C/min.Inj./det. temp.: 150°C/200°CCarrier gas: hydrogen @ 40cm/sec.Split ratio: 100:1

1

2

3

4

6

7

5

min. 5 10 15 20 25

8

9

10 11

1. acetaldehyde2. methanol3. ethanol4. acetone5. isopropanol6. n-propanol

7. ethyl acetate8. isobutanol9. acetic acid

10. isoamyl alcohol11. active amyl alcohol

aceticacid

GC_FF00112


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Alcoholic Beverage Standard: Acids and Esters

Stabilwax®-DA

PPeeaakk LLiisstt CCoonncc.. ((ppppmm))1. ethyl octanoate 1002. acetic acid 1003. propionic acid 1004. isobutyric acid 1005. 3-decanol 506. ethyl decanoate 507. ethyl laurate 508. cis-lactone 1009. 2-phenylethanol 50

10. trans-lactone 10011. methyl myristate 5012. ethyl myristate 5013. octanoic acid 10014. ethyl palmitate 5015. decanoic acid 10016. dodecanoic acid 10017. vanillin 100

Column: Stabilwax®-DA, 30m, 0.18mm ID, 0.18µm (cat.# 550752)Inj.: 1µL splitless (hold 0.5 min.) at conc. shown in

peak list, in ethyl acetate, 4mm ID splitless liner w/wool (cat.# 20814-202.1)

Inj. temp.: 240°CCarrier gas: hydrogenMake-up gas: nitrogenLinear velocity: 28psi @ 240°COven temp.: 70°C to 240°C at 12°C/min. (hold 3 min.)Det.: FID

GC_FF00500

free literatureAnalyzing Alcoholic Beverages by Gas Chromatography

Selectivity, sensitivity, and minimal sample preparation make GC a powerful tool for monitoringalcoholic beverage composition

Volatile component profiles of alcoholic beverages reveal a wide range of compounds:acids, alcohols, aldehydes, and others. This 16-page guide describes packed column GCand capillary GC approaches to monitoring these complex mixtures of analytes. A separatesection is devoted to detailed information about quantifying trace sulfur compounds in beer.

Technical Guidelit. cat.# 59462

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Food Contaminants

Column: Rt®-XLSulfur, 100/120 mesh, 1m, 0.75mm ID Sulfinert® tubing (cat.# 19806)

Conc.: sulfur standard @ 20ppb each in CO2

Inj.: 1cc sample loop, 6-port Valco® valveCarrier gas: heliumFlow rate: 10mL/min. @ ambient temp.Oven temp.: 60°C to 260°C @ 15°C/min. (hold 5 min.) Det. sensitivity: SCD, attn. x 1Det. temp.: 800°C

GC_FF00491

Sulfur Compounds in Beverage Grade CO2

Rt®-XLSulfur

1. hydrogen sulfide2. carbonyl sulfide3. methyl mercaptan4. ethyl mercaptan and/or

dimethyl sulfide5. dimethyl disulfide

GC_FF00494

Column: Rt®-XLSulfur, 100/120 mesh, 1m, 0.75mm ID Sulfinert® tubing (cat.# 19806)

Conc.: headspace of a domestic (US) beer sampleInj.: 1cc sample loop, 6-port Valco® valveCarrier gas: heliumFlow rate: 10mL/min. @ ambient temp.Oven temp.: 60°C to 260°C @ 15°C/min. (hold 5 min.) Det. sensitivity: SCD, attn. x 1Det. temp.: 800°C

1. hydrogen sulfide2. methyl mercaptan3. dimethyl sulfide and/or

ethyl mercaptan4. unknown

Sulfur Compounds in Beer

Rt®-XLSulfur(Headspace/GC)



GC_FF00487

Column: Rt®-XLSulfur, 100/120 mesh, 1m, 0.75mm ID Sulfinert® tubing(cat.# 19806)

Conc.: headspace of an imported((CCaannaaddaa)) beer sample

Inj.: 1cc sample loop,6-port Valco® valve

Carrier gas: heliumFlow rate: 10mL/min. @ ambient temp.Oven temp.: 60°C to 260°C @

15°C/min. (hold 5 min.)Det. sensitivity: SCD, attn. x 1Det temp: 800°C

1. hydrogen sulfide2. methyl mercaptan3. dimethyl sulfide and/or

ethyl mercaptan4. unknown



GC_FF00483

Column: Rt®-XLSulfur, 100/120 mesh, 1m, 0.75mm ID Sulfinert® tubing(cat.# 19806)

Conc.: headspace of an imported((MMeexxiiccoo)) beer sample

Inj.: 1cc sample loop,6-port Valco® valve

Carrier gas: heliumFlow rate: 10mL/min. @ ambient temp.Oven temp.: 60°C to 260°C @

15°C/min. (hold 5 min.)Det. sensitivity: SCD, attn. x 1Det temp: 800°C


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Food Contaminants

1

2

9

34

5

6 78 10

11

12

0 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21

VVoollaattiilleess SSttaannddaarrdd1. isopropanol2. methylene chloride3. 2-methyl-1-propanol4. tetrahydrofuran5. benzene6. toluene7. hexanal8. furfural9. 4-heptanone (IS)

10. butyl ether11. styrene12. dodecane

Column: Rtx®-5MS, 30m, 0.25mm ID, 1µm (cat.# 12653)Concentrator: Tekmar LSC-3100 purge & trapTrap: Vocarb 3000, type KPurge: 10 min. @ 40mL/min. @ 60°CDry purge: 3 min. @ 40mL/min.Desorb preheat: 220°CDesorb: 245°C, 2 min., 40mL/min.Bake: 230°C, 6 min.Interface: 1:20 split at injection port with 1mm ID linerTransfer line: 0.53mm ID Silcosteel® MXT® tubing (cat.# 20591)Oven temp.: 50°C to 92°C @ 3°C/min., to 220°C @

20°C/min., hold 1 min. Inj. temp.: 250°CCarrier gas: heliumLinear velocity: 36cm/sec. (1mL/min.)Split ratio: 20:1Det.: MSDDet. temp.: 280°CScan range: 35–260amuIonization: EI @ 70 eV

Food Packaging Volatiles

Rtx®-5MS

GC_FF00457

1. tetrahydrofuran2. 1-butanol3. toluene4. hexanal5. ethylbenzene6. 4-heptanone7. butyl ether8. styrene9. 1-methylethylbenzene

10. propylbenzene11. benzaldehyde12. benzeneacetaldehyde13. acetophenone14. benzoic acid, methyl ester15. decanal

Column: Rtx®-5MS, 30m, 0.25mm ID, 1µm (cat.# 12653)Concentrator: Tekmar LSC-3100 purge & trapTrap: Vocarb 3000, type KPurge: 10 min. @ 40mL/min. @ 60°CDry purge: 3 min. @ 40mL/min.Desorb preheat: 220°CDesorb: 245°C, 2 min., 40mL/min.Bake: 230°C, 6 min.Interface: 1:20 split at injection with 1mm ID linerTransfer line: 0.53mm ID Silcosteel® MXT® tubing (cat.# 20591)Inj. temp.: 250°CCarrier gas: heliumLinear velocity: 36cm/sec. (1mL/min.)Split ratio: 20:1Oven temp.: 50°C to 92°C @ 3°C/min., to 220°C @

20°C/min, hold for 1 min.Det. : MSD (Agilent 5973)Det. temp.: 280°CScan range: 35-260amuIonization: EI @ 70eV

GC_FF00459

Food Packaging Volatiles

Rtx®-5MS


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Food Contaminants

1 2

3

4

56

0 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21

Food Packaging Volatiles by Purge & Trap GC/MS

Rtx®-5MS(Purge & Trap GC/MS)

1. ethyl acetate2. toluene3. 4-heptanone4. n-butyl ether5. styrene6. alkanes

Column: Rtx®-5MS, 30m, 0.25mm ID, 1µm (cat.# 12653)GC: Agilent 6890Oven temp.: 50°C to 92°C @ 3°C/min., to 220°C @

20°C/min. (hold 1 min.) Injector temp.: 250°CCarrier gas: heliumLinear velocity: 36cm/sec. (1mL/min.)Det. sensitivity: NASplit ratio: 20:1Det.: MSD (Agilent 5973)Det. temp.: 280°CScan range: 35-260amuIonization: EI @ 70eVMode:

Sample Conditions:Sample: Overwrap, inner bowlConcentrator: Tekmar LSC-3100 purge & trapTrap: Vocarb 3000, type KPurge: 10 min. @ 40mL/min., at 60°CDry purge: 3 min. @ 40mL/min.Desorb preheat: 220°CDesorb: 245°C, 2 min., 40mL/min.Bake: 230°C, 6 min.Interface: 1:20 split at injection port with 1mm ID inlet linerTransfer line: 0.53mm ID Silcosteel® MXT® tubing (cat.# 22501)

GC_FF00462

1 2 3

4

5

6 7 8

0 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21

Food Packaging Volatiles by Purge & Trap GC/MS

Rtx®-5MS(Purge & Trap GC/MS)

GC_FF00461

1. tetrahydrofuran2. ethylbenzene3. 4-heptanone4. styrene5. benzaldehyde6. nonanal7. decanal8. cinnamaldehyde

Column: Rtx®-5MS, 30m, 0.25mm ID, 1µm (cat.# 12653)GC: Agilent 6890Oven temp.: 50°C to 92°C @ 3°C/min., to 220°C @

20°C/min. (hold 1 min.)Inj. temp.: 250°CCarrier gas: heliumLinear velocity: 36cm/sec. (1mL/min.)Det. sensitivity: NASplit ratio: 20:1Det.: MSD (Agilent 5973)Det. temp.: 280°CScan range: 35-260amuIonization: EI @ 70eVMode:

Sample Conditions:Sample: Overwrap, lid of bowlConcentrator: Tekmar LSC-3100 purge & trapTrap: Vocarb 3000, type KPurge: 10 min. @ 40mL/min., at 60°CDry purge: 3 min. @ 40mL/min.Desorb preheat: 220°CDesorb: 245°C, 2 min., 40mL/min.Bake: 230°C, 6 min.Interface: 1:20 split at injection port with 1mm ID inlet linerTransfer line: 0.53mm ID Silcosteel® MXT® tubing (cat.# 22501)


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Food Contaminants

Organochlorine and Organophosphorus Pesticides

FAPAS® Proficiency Testing

Rxi®-5ms

GC_FF00826

1. dichlorvos2. methacrifos3. α-BHC4. hexachlorobenzene5. δ-BHC (lindane)6. β-BHC7. diazinon8. etrimphos9. phosphamidon

10. chlorpyrifos-methyl11. heptachlor12. fenitrothion13. pirimiphos methyl14. malathion15. aldrin

16. chlorpyrifos17. heptachlor epoxide18. oxychlordane19. trans-chlordane20. endosulfan I21. cis-chlordane22. 2,4'-DDT23. dieldrin24. endrin25. endosulfan II26. 4,4'-DDE27. 4,4'-DDD28. endosulfan sulfate29. 4,4'-DDT


Sample: FAPAS Series 5 OC Pesticide Mix 1 (cat.# 32412), FAPAS Series 9 OP Pesticide Mix 1 (cat.# 32413)

Inj.: 1.0µL, 10ppm each analyte, split (10:1)4mm Drilled Uniliner® inlet liner (hole near bottom) (cat.# 20771)

Instrument: Agilent 6890Inj. temp.: 290°CCarrier gas: helium, constant flowFlow rate: 1.2mL/min.Oven temp.: 100°C (hold 0.5 min.) to 300°C @ 7°C/min.

(hold 1 min.)Det.: Agilent 5973 GC/MSTransfer line


Organochlorine and Organophosphorus Pesticides

FAPAS® Proficiency Testing

Rxi®-5ms1. naphthalene-d82. dichlorvos3. acenaphthene-d104. methacrifos5. α-BHC6. hexachlorobenzene7. δ-BHC (lindane)8. β-BHC9. phenanthrene-d10

10. diazinon11. etrimphos12. phosphamidon13. chlorpyrifos-methyl14. heptachlor15. fenitrothion16. pirimiphos methyl17. malathion

18. aldrin19. chlorpyrifos20. heptachlor epoxide21. oxychlordane22. trans-chlordane23. endosulfan I24. cis-chlordane25. 2,4'-DDT26. dieldrin27. endrin28. endosulfan II29. 4,4'-DDE30. 4,4'-DDD31. endosulfan sulfate32. 4,4'-DDT33. chrysene-d1234. perylene-d12


Sample: FAPAS Series 5 OC Pesticide Mix 1 (cat.# 32412), FAPAS Series 9 OP Pesticide Mix 1 (cat.# 32413), SV Internal Standard Mix (cat.# 31206)

Inj.: 1.0µL, 10ppm each analyte, split (10:1)4mm Drilled Uniliner® inlet liner (hole near bottom) (cat.# 20771)

Instrument: Agilent 6890Inj. temp.: 290°CCarrier gas: helium, constant flowFlow rate: 1.2mL/min.Oven temp.: 100°C (hold 0.5 min.) to 300°C @ 7°C/min.

(hold 1 min.)Det.: Agilent 5973 GC/MSTransfer line


GC_FF00827






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Food Contaminants

Polycyclic Aromatic Hydrocarbons in

Infant Formula with and without QuEChERS dSPE Clean-up

Rxi®-5Sil MS

CCoommppoouunndd lliisstt aanndd iioonnss mmoonniittoorreedd ((SSIIMM mmooddee))Compound m/z

1. decafluorobiphenyl (SS) 2652. naphthalene 1283. 2-methylnaphthalene 1424. 1-methylnaphthalene 1425. acenaphthylene 1526. acenaphthene 1527. fluorine 1668. phenanthrene-d10 (IS) 1889. phenanthrene 178

10. anthracene 17811. fluoranthene 20212. pyrene 20213. benzo(a)anthracene 22814. chrysene 22815. benzo(b)fluoranthene 25216. benzo(k)fluoranthene 25217. benzo(a)pyrene 25218. indeno(1,2,3-cd)pyrene 27619. dibenzo(a,h)anthracene 27820. benzo(ghi)perylene 276

Column: Rxi®-5Sil MS, 30m, 0.25mm ID, 0.25µm (cat.# 13623)Sample: liquid infant formula spiked at 1µg/mL with decafluorobiphenyl (cat.# 31842) and EPA Method 8310 PAH Mixture (cat.# 31841) and at 0.5µg/mL with

internal standard phenanthrene-d10 (cat.# 31045), then extracted with acetonitrile and Q-sep™ Q110 QuEChERS extraction tube (cat.# 26213)A. extract with clean-up using Q-sep™ Q210 QuEChERS dSPE clean-up tube (cat.# 26215)B. extract without clean-up

Inj.: 1.0µL splitless (hold 0.15 min.),3.5mm single gooseneck liner with w/wool (cat.# 22286-200.1)

Inj. temp.: 300°CCarrier gas: helium, constant flow Flow rate: 1.4mL/min. Oven temp.: 50°C (hold 0.5 min.) to 290°C @ 25°C/min. to 320°C @ 5°C/min. (hold 5 min.)Det: MSMode: scan (SIM shown below)Transfer line temp.: 290°CAnalyzer Type: QuadrupoleScan range: 100-350amuIonization: EIInstrument: Shimadzu 2010 GC & QP2010 Plus MS

GC_FF01122

Q-sep™ Q250QuEChERS clean-upSIM Mode

Scan Mode

GC_FF01123

NEW!


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Food Contaminants

GC_EV1160

1. Naphthalene2. 2-Methylnaphthalene3. 1-Methylnaphthalene4. Acenaphthylene5. Acenaphthene6. Fluorene7. Phenanthrene8. Anthracene9. Fluoranthene

10. Pyrene11. Benz[a]anthracene12. Chrysene13. Triphenylene14. Benzo[b]fluoranthene

15. Benzo[k]fluoranthene16. Benzo(j)fluoranthene17. Benzo[a]pyrene18. 3-Methylcholanthrene19. Dibenz(a,h)acridine20. Dibenz[a,j]acridine21. Indeno[1,2,3-cd]pyrene22. Dibenz[a,h]anthracene23. Benzo[ghi]perylene24. 7H-Dibenzo[c,g]carbazole25. Dibenzo[a,e]pyrene26. Dibenzo(a,i)pyrene27. Dibenzo(a,h)pyrene

CCoolluummnn Rxi®-17Sil MS, 30 m, 0.25 mm ID, 0.25 µm (cat.# 14123)SSaammppllee SV Calibration Mix #5 / 610 PAH Mix (cat.# 31011)

EPA Method 8310 PAH Mixture (cat.# 31841)Diluent: dichloromethaneConc.: 10 ppmIInnjjeeccttiioonnInj. Vol.: 0.5 µL splitless (hold 1.75 min.)Liner: Auto SYS XL PSS Split/Splitless w/Wool (cat.# 21718)Inj. Temp.: 320 °CPurge Flow: 75 mL/min.OOvveennOven Temp: 65 °C (hold 0.5 min.) to 220 °C at 15 °C/min. to 330 °C at 4 °C/min. (hold 15 min.)CCaarrrriieerr GGaass He, constant flowFlow Rate: 2.0 mL/min.DDeetteeccttoorr FID @ 320 °CIInnssttrruummeenntt PE Clarus 600 GCAAcckknnoowwlleeddggeemmeenntt Instrument provided by PerkinElmer


Rxi®-17Sil MS NEW!


Excellent column for

PAH residues in food!


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Food Contaminants

GC_FF00977

Column: Rtx®-5MS, 30m, 0.25mm ID, 0.25µm (cat.# 12623)Sample: melamine, cyanuric acid, ammelide, ammeline, benzoguanamine

in dry cat food (10µg/mL prederivatized)Inj.: 1µL, splitless (hold 1 min.), 3.5mm splitless inlet liner (cat.# 22286)Inj. temp.: 280°CCarrier gas: helium, constant flow Flow rate: 1mL/min. Oven temp.: 75°C to 320°C @ 15°C/min. (hold 4 min.)Det: MSTransfer line temp.: 290°CIonization: EIMode: SIM

1. cyanuric acid2. ammelide3. ammeline4. melamine5. benzoguanamine

Melamine Spike in Cat Food

Rtx®-5MS

Reliable

identifications

in matrix.

QuEChERS Extract of NIST SRM 2974a Freeze-Dried Mussel Tissue (GCxGC contour plot)

GC_FF1197

CCoolluummnn Rxi®-17Sil MS 30 m, 0.25 mm ID, 0.25 µm (cat.# 14123)Rxi®-1ms 1.2 m, 0.15 mm ID, 0.15 µm (cat.# custom)

SSaammppllee NIST SRM 2974a freeze-dried mussel tissue with incurred residues

Diluent: AcetonitrileIInnjjeeccttiioonnInj. Vol.: 1 µL splitless (hold 1 min.)Liner: Gooseneck Splitless (4mm)

w/Semivolatiles Wool (cat.# 20798-231.1)

Inj. Temp.: 250 °CPurge Flow: 40 mL/min.OOvveennOven Temp: Rxi®-17Sil MS: 90 °C (hold 1

min.) to 320 °C at 3.75 °C/min. (hold 2.67 min.)Rxi®-1ms: 95 °C (hold 1 min.) to 325 °C at 3.75 °C/min. (hold 2.67 min.)

CCaarrrriieerr GGaass HeMMoodduullaattiioonnModulatorTemp. Offset: 20 °CSecond DimensionSeparation Time: 3 sec.Hot Pulse Time: 0.9 sec.Cool Timebetween Stages: 0.6 sec.DDeetteeccttoorr TOFMSTransferLine Temp.: 300 °CAnalyzer Type: TOFSource Temp.: 250 °CElectron Energy: 70 eVMass Defect: -20 mu/100 uSolvent DelayTime: 5 min.Tune Type: PFTBAIonization Mode: EIAcquisition Range: 45 to 550 amuSpectralAcquisition Rate: 100 spectra/secIInnssttrruummeenntt LECO Pegasus 4D

GCxGC-TOFMSNNootteess PAHs (shown in box) elute in a relativelynarrow band and are identified by the white peakmarker dots.

PPeeaakkss1. Naphthalene2. 2-Methylnaphthalene3. 1-Methylnaphthalene4. Biphenyl5. 2,6-Dimethylnaphthalene6. Acenaphthylene

7. Acenaphthene8. 2,3,5-Trimethylnaphthalene9. Fluorene

10. Phenanthrene11. Anthracene12. 1-Methylphenanthrene13. Fluoranthene

14. Pyrene15. Benzo(a)anthracene16. Chrysene17. Benzo(b)fluoranthene18. Benzo(k)fluoranthene19. Benzo(j)fluoranthene20. Benzo(e)pyrene

21. Benzo(a)pyrene22. Perylene23. Dibenz(a,h)anthracene24. Indeno(1,2,3-cd)pyrene25. Benzo(ghi)perylene

NEW!

Get More!High Sensitivity

Melamine GC/MS Analysis of Cat Food

Modified Conditions Save Costs and Reduce Maintenance

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Food Contaminants

Organochlorine Pesticides

Rxi®-5Sil MS

CCoommppoouunndd QQuuaanntt.. iioonn QQ11 QQ33*1. α-BHC 219 181 109

2. γ-BHC 219 181 1093. β-BHC 219 181 1094. δ-BHC 219 181 1095. heptachlor 272 237 1006. aldrin 263 293 2207. heptachlor epoxide 263 237 818. γ-chlordane 272 237 659. α-chlordane 272 237 65

10. endosulfan I 195 207 24111. 4,4'-DDE 246 318 17612. dieldrin 79 263 27713. endrin 263 281 8114. 4,4'-DDD 235 165 19915. endosulfan II 195 207 -16. 4,4'-DDT 235 165 19917. endrin aldehyde 67 250 34518. endosulfan sulfate 272 229 23919. methoxychlor 227 274 -20. endrin ketone 67 317 281* not present

Column: Rxi®-5Sil MS, 30m, 0.25mm ID, 0.25µm (cat.# 13623)Sample: 10µg/mL Organochlorine Pesticide Mix AB # 3

(cat.# 32415) in olive oilInj.: 1µL, splitless (hold 0.5 min.),

3.5mm single gooseneck liner (cat.# 20962) packed with wool

Inj. temp.: 225°CCarrier gas: helium, constant flow Flow rate: 1mL/min. Oven temp.: 130°C to 330°C @ 5°C/min.Det: MSTransfer line temp.: 320°CIonization: EIMode: SIM

GC_FF01044

NEW!

Acrylamide (Reference Standard)

Stabilwax®

Column: Stabilwax®, 15m, 0.53mm ID, 0.50µm (cat.# 10637)Sample: 25µg/mL acrylamide standard in waterInj.: 1.0µL, 0.5 min holdLiner: 2mm splitless with wool (cat.# 20830)Inj. temp.: 260°CCarrier gas: helium, constant pressureLinear velocity: 62cm/sec. @ 100°COven temp.: 100°C (hold 0.5 min.) to 200°C @ 15°C/min.Det.: FID @ 260°C

GC_FF00642

1. acrylamide

Acrylamide (Potato Chip Extract)

Stabilwax®

GC_FF00643

Column: Stabilwax®, 15m, 0.53mm ID, 0.50µm (cat.# 10637)Sample: 1g of potato chips spiked with 100µg acrylamideInj.: 1.0µL, 0.5 min. holdLiner: 2mm splitless with wool (cat.# 20830)Inj. temp.: 260°CCarrier gas: helium, constant pressureLinear velocity: 62cm/sec. @ 100°COven temp.: 100°C (hold 0.5 min.) to 200°C @ 15°C/min.Det.: FID @ 260°C

1. acrylamide

blank


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Sugars

3 4 6 8

Column: Rt®-2330, 15m, 0.32mm ID, 0.20µm (cat.# 10721)Inj.: 0.6µL split injectionOven temp.: 175°C (hold 2 min.) to 240°C @ 8°C/min. (hold 1

min.) to 265°C @ 8°C/min. (hold 12 min.)Inj./det. temp.: 275°CCarrier gas: heliumLinear velocity: 80cm/sec. (flow rate: 10cc/min.)FID sensitivity: 2 x 10-11 AFSSplit ratio: 20:1

Sugars (Alditol Acetates)

Rt®-2330

GC_FF00127

1 2 5 7 9 10

11

12 13

14

15

16

min. 2 4 6 8 10 12 14 16 18 20 22

1. glyceraldehyde2. deoxyribitol3. rhamnitol4. fucitol5. ribitol6. arabinitol7. xylitol8. deoxyglucitol9. mannitol

10. galactitol11. glucitol12. inositol13. glucoheptitol14. n-acetyl galactose amine15. n-acetyl glucose amine16. 2-keto-3-deoxyoctanate

5

Sugars (Alditol Acetates)

Rtx®-225

GC_FF00128

87

64

3

21

1. rhamnitol2. fucitol3. ribitol4. arabinitol5. mannitol6. galactitol7. glucitol8. inositol


Inj.: 0.5µL split injectionOven temp.: 190°C (hold 5 min.) to 250°C

@ 8°C/min. (hold 5 min.)Inj./det. temp.: 260°CCarrier gas: hydrogenLinear velocity: 42cm/sec. set @ 40°CFID sensitivity: 16 x 10-11 AFSSplit ratio: 50:1

min. 2.5 5 7.5 10 12.5


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Fragrances

GC_FF00657

5% Fragrance Materials Association Mix

Rtx®-1


Sample: 5% FMA mix in acetone (cat.# 31807) Inj.: 1.0µL split (split ratio 40:1),

4mm inlet liner (cat.# 20814)Inj. temp.: 285°CCarrier gas: helium, constant flow Flow rate: 0.6mL/min.Oven temp.: 50°C to 270°C @ 3°C/min. Det.: FID @ 300°C

CCoommppoouunndd %% iinn tthhee FFMMAA mmiixx1. ethyl butyrate 35.72. limonene 20.03. eucalyptol 0.54. benzoic acid 1.05. cinnamic aldehyde 0.56. geraniol 0.67. hydroxycitronellal 5.08. thymol 0.39. cinnamyl alcohol 0.3

10. vanillin 0.111. cinnamyl acetate 0.312. benzyl salicylate 35.7

FMA Reference Mixcat.# 31807

5% Fragrance Materials Association Mix

Rtx®-1701

GC_FF00658

Column: Rtx®-1701, 60m, 0.25mm ID, 0.25µm (cat.# 12026)Sample: 5% FMA mix in acetone Inj.: 1.0µL split (split ratio 40:1), 4mm inlet liner (cat.# 20814)Inj. temp.: 285°CCarrier gas: helium, constant flow Flow rate: 0.6mL/min.Oven temp.: 50°C to 270°C @ 3°C/min. Det.: FID @ 300°C

CCoommppoouunndd %% iinn FFMMAA MMiixx1. ethyl butyrate 35.72. limonene 20.03. eucalyptol 0.54. geraniol 0.65. benzoic acid 1.06. cinnamic aldehyde 0.57. hydroxycitronellal 5.08. thymol 0.39. cinnamyl alcohol 0.3

10. cinnamyl acetate 0.311. vanillin 0.112. benzyl salicylate 35.7


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GC CHROMATOGRAMS | PERSONAL CARE & CLEANING PRODUCTS

Cleaning Solvents

Cleaning Solvents

Rtx®-Wax

Column: Rtx®-Wax, 30m, 0.32mm ID, 0.25µm (cat.# 12424)Sample: 1% each solvent in methanolInj.: 1.0µL split (split ratio 100:1), 4mm inlet liner (cat.# 20814)Inj. temp.: 250°CCarrier gas: hydrogen, constant flow Flow rate: 3.0mL/min.Oven temp.: 35°C (4 min. hold) to 85°C @ 3°C/min., to 200°C @ 15°C/min. (2 min. hold)Det.: FID @ 250°C

1. methanol2. iso-propanol3. ethanol4. n-propanol5. iso-butanol6. n-butanol7. methyl Cellosolve®

8. limonene9. Cellosolve®

10. butyl Cellosolve®

11. dipropylene glycol monomethyl ether (DPGMME)12. diethylene glycol ethyl ether (DEGEE)13. ethylene glycol14. tripropylene glycol monomethyl ether (TPGMME)15. phenyl Cellosolve®

GC_FF00644

Cleaning Solvents

Rtx®-VMSColumn: Rtx®-VMS, 60m, 0.25mm ID, 1.4µm (cat.# 19916)Sample: 1% each solvent in methanolInj.: 1.0µL split (split ratio 100:1), 4mm inlet liner (cat.# 20814)Inj. temp.: 250°CCarrier gas: hydrogen, constant flow Flow rate: 1.5mL/min.Oven temp.: 60°C (1 min. hold) to 138°C @ 4°C/min.,

to 145°C @ 2°C/min., to 210°C @ 15°C/min., to 230°C @ 5°C/min.

Det.: FID @ 250°C

1. methanol2. ethanol3. iso-propanol4. tert-butanol5. n-propanol6. iso-butanol7. methyl Cellosolve®

8. n-butanol9. Cellosolve®

10. ethylene glycol11. butyl Cellosolve®

12. limonene13. dipropylene glycol monomethyl ether (DPGMME)14. diethylene glycol ethyl ether (DEGEE)15. phenyl Cellosolve®

16. tripropylene glycol monomethyl ether (TPGMME)

GC_FF00645

642-664_GCapppetro.qxp 11/22/2010 9:19 PM Page 642

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GC CHROMATOGRAMS | PERSONAL CARE & CLEANING PRODUCTS

Cleaning Solvents

Cleaning Solvents (All-Purpose Cleaner)

Rtx®-VMS

Column: Rtx®-VMS, 60m, 0.25mm ID, 1.4µm (cat.# 19916)Sample: approx. 5% cleaner in methanolInj.: 1.0µL split (split ratio 100:1), 4mm inlet liner (cat.# 20814)Inj. temp.: 250°CCarrier gas: hydrogen, constant flow Flow rate: 1.5mL/min.Oven temp.: 60°C (1 min. hold) to 138°C @ 4°C/min. to 145°C @ 2°C/min. to 210°C

@ 15°C/min. to 230°C @ 5°C/min.Det.: FID @ 250°C

1. butyl Cellosolve®

2. limonene

GC_FF00646

Cleaning Solvents (Glass Cleaner)

Rtx®-VMS

Column: Rtx®-VMS, 60m, 0.25mm ID, 1.4µm (cat.# 19916)Sample: approx. 5% cleaner in methanolInj.: 1.0µL split (split ratio 100:1), 4mm inlet liner (cat.# 20814)Inj. temp.: 250°CCarrier gas: hydrogen, constant flow Flow rate: 1.5mL/min.Oven temp.: 60°C (1 min. hold) to 138°C @ 4°C/min. to 145°C @ 2°C/min. to 210°C

@ 15°C/min. to 230°C @ 5°C/min.Det.: FID @ 250°C

1. iso-propanol2. butyl Cellosolve®

GC_FF00647





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GC CHROMATOGRAMS | PETROLEUM & PETROCHEMICAL

Fuels

• built-in retention gap

• eliminates connector

Retention Gap Liquid Phase

Total Glycerin in Biodiesel

MXT®-Biodiesel TG

0 10 20Time (min)

Column: MXT®-Biodiesel TG, 14m, 0.53mm ID, 0.16µm (cat.# 70289) witha 2m x 0.53mm Integra-Gap® retention gap (16m total length)

Sample: biodiesel (B100), derivatizedInj.: cool on-column injection

1µL in heptane Inj. temp.: oven trackCarrier gas: hydrogen, constant flowFlow rate: 4mL/min.Oven temp.: 50°C (hold 1 min.) to 180°C @ 15°C/min. to 230°C @ 7°C/min. to

430°C @ 30°C/min. (hold 5 min.)Det.: FID @ 430°C

GC_PC00969

glycerin

monoglycerides monoglycerides diglycerides triglycerides

buta

netr

iol (

IS)

tric

aprin

(IS)

The best solution

for analyzing total

glycerin in biodiesel!

Biodiesel Oil (B100)

Rtx®-Biodiesel TG

B. Rtx®-Biodiesel TG

with Universal Press-Tight®Connector and

2 meters of 0.53mm ID Hydroguard® tubing

A. Rtx®-Biodiesel TG

with Alumaseal® connector and

2 meters of 0.53mm ID Hydroguard® tubing

GC_PC00905

Columns: A. Rtx®-Biodiesel TG, 10m, 0.32mm ID, 0.10µm connected to 2m x 0.53mm Hydroguard® tubing using Alumaseal® connectorB. Rtx®-Biodiesel TG, 10m, 0.32mm ID, 0.10µm connected to 2m x 0.53mm Hydroguard® tubing using Universal Press-Tight® connector

Sample: biodiesel (B100) with butanetriol at 12.5ppm (12.5ng on-column)Inj.: 1µL, cool on-column injectionInj. temp.: oven track modeCarrier gas: hydrogen, constant flow 4cc/min.Linear velocity: 79cm/sec.Oven temp.: 50°C (hold 1min.) to 180°C @ 15°C/min. to 230°C @ 7°C/min. to 380°C

@ 30°C/min. (hold 5 min.)Det.: FID @ 380°C

Butanetriol AAssyymmmmeettrryy == 11..1144

Butanetriol AAssyymmmmeettrryy == 11..0000

Integra-Gap® technology.


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Fuels

Derivatized B100 and Internal Standards

MXT®-Biodiesel TG with 2m x 0.53mm ID Retention Gap

GC_PC00935

monoglycerides

triglycerides

Column: MXT®-Biodiesel TG, 10m, 0.32mm ID, 0.1µm with 2m x 0.53mm retention gap (cat.# 70290)

Sample: B100 + IS butanetriol & tricaprin derivatized with MSTFA as per ASTM D-6584

Inj.: 1.0µL cool on-columnInj. temp.: oven trackCarrier gas: hydrogen, constant flowFlow rate: 4mL/min.Oven temp.: 50°C (hold 1 min.) to 180°C @ 15°C/min.,

to 230°C @ 7°C/min., to 430°C @ 30°C/min. (hold 5 min.)Det.: FID @ 430°C

butanetriol (IS)

glycerin

tricaprin (IS)

diglycerides

Note perfect solvent

peak shape!

B100

MXT®-Biodiesel TG

Column: MXT®-Biodiesel TG, 15m, 0.32mm ID, 0.10µm (cat.# 70291) witha 2m x 0.53mm MXT® retention gap connected with a MXT® low-dead-volume connector (17m total length)

Sample: biodiesel (B100), derivatizedInj.: cool on-column injection

1µL in heptane Inj. temp.: oven trackCarrier gas: hydrogen, constant flowFlow rate: 3mL/min.Oven temp.: 50°C (hold 1 min.) to 180°C @ 15°C/min. to 230°C @ 7°C/min. to 430°C @

30°C/min. (hold 5 min.)Det.: FID @ 430°C

GC_PC00968

glycerin

buta

netr

iol (

IS)

tric

aprin

(IS)

monoglycerides monoglycerides diglycerides triglycerides

Get More!

Biodiesel Solutions

Online

www.restek.com/biodiesel


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Fuels

Column: Stabilwax®, 30m, 0.32mm ID, 0.25µm (cat.# 10624)Sample: various sources of biodiesel (B100), prepared according to European Method EN 14103Inj.: 1.0µL split (split ratio 100:1), Cyclosplitter® inlet liner (cat.# 20706)Inj. temp.: 250°CCarrier gas: hydrogen, constant flow, 3mL/min.Linear velocity: 60cm/sec.Oven temp.: 210°C (hold 5 min.) to 230°C @ 20°C/min. (hold 5 min.)Det.: FID @ 250°C

Yellow Grease FAMEs on Stabilwax®

Tallow FAMEs on Stabilwax®

Rapeseed FAMEs on Stabilwax®

Soy FAMEs on Stabilwax®

1. myristic acid C14:02. palmitic acid C16:03. palmitoleic acid C16:1

IS methyl heptadecanoate4. stearic acid C18:05. oleic acid C18:1

6. linoleic acid C18:27. linolenic acid C18:38. arachidic acid C20:09. gadoleic acid C20:1

10. behenic acid C22:011. lignoceric acid C24:0

GC_PC00915


IS methyl heptadecanoate4. stearic acid C18:05. oleic acid C18:1

6. linoleic acid C18:27. linolenic acid C18:38. arachidic acid C20:09. gadoleic acid C20:1

10. lignoceric acid C24:011. nervonic acid C24:1

GC_PC00916


IS methyl heptadecanoate4. stearic acid C18:05. oleic acid C18:16. linoleic acid C18:2

7. linolenic acid C18:38. arachidic acid C20:09. gadoleic acid C20:1

10. behenic acid C22:011. erucic acid C22:112. lignoceric acid C24:013. nervonic acid C24:1

GC_PC00917


IS methyl heptadecanoate4. stearic acid C18:05. oleic acid C18:16. linoleic acid C18:2

7. linolenic acid C18:38. arachidic acid C20:09. gadoleic acid C20:1

10. behenic acid C22:011. erucic acid C22:112. lignoceric acid C24:0

GC_PC00918

FAMEs in Biodiesel Oils

Stabilwax®


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Permanent Gases

Column: ShinCarbon ST, 100/120 mesh, 2m, 1mm ID micropacked (cat.# 19808)

Sample: 5µL permanent gases mix, approx. 5 mole % each

Inj. temp.: 100°CCarrier gas: heliumFlow rate: 10mL/min.Oven temp.: 40°C (hold 3 min.) to 250°

@ 8°/min. (hold 10 min.)Det. HID @ 200°C

Permanent Gases

ShinCarbon ST(micropacked)

1. hydrogen2. oxygen3. nitrogen4. carbon monoxide5. methane6. carbon dioxide

GC_PC00666

Column: ShinCarbon ST, 100/120 mesh 2m, 1mm ID micropacked (cat.# 19808)

Sample: permanent gases-C1+C2 hydrocarbons Sample size: 5µLInj. temp.: 100°CCarrier gas: heliumFlow rate: 10mL/min.Oven temp.: 40°C (hold 3 min.) to 250°

@ 8°/min. (hold 10 min.)Det. HID @ 200°C

Permanent Gases, C1+C2 hydrocarbons


1. oxygen2. nitrogen3. carbon monoxide4. methane5. carbon dioxide6. acetylene7. ethylene8. ethane

GC_PC00665

Permanent Gases

Molecular Sieve 5A and Molecular Sieve 13X(packed)

Molecular Sieve 5A:

excellent resolution of oxygen, nitrogen,methane, and carbon monoxide.

1. oxygen2. nitrogen3. methane4. carbon monoxide

10µL helium, 5–10% each componentOven temp.: 50°CInj./det. temp.: 150°C/200°CCarrier gas: hydrogenFlow: 30mL/min. Det.: TCD

1 2

3 4

min.0 2 4

Molecular Sieve 13X:

rapid analysis and excellent peaksymmetry for carbon monoxide.

GC_PC00166

1

2

3

4

min.0 2 4

Molecular Sieve 5A 80/100 mesh1m x 1/8" x 2mm ID SilcoSmooth® tubing (cat.# 80440-800)

Molecular Sieve 13X 80/100 mesh2m x 1/8" x 2mm (ID) SilcoSmooth® tubing (cat.# 80439-800)

Excellent

peak shape.


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Permanent Gases

Permanent Gases

Rt®-MSieve 5A (PLOT)

Column: Rt®-Msieve 5A, 30m, 0.53mm ID, 50µm (cat.# 19723)

Sample: 0.5mL (sample loop injection) Column temp.: 27°C Carrier gas: helium Linear velocity: 34cm/sec.Det.: Valco® HID

1. hydrogen, 29.1 ppm2. argon, 53.4 ppm3. oxygen, 31.3 ppm

1

2

3

min. 1 2 3

Chromatogram courtesy of Larry McElmurry, Mobile Analytical Labs.

GC_PC00170

Permanent Gases

Rt®-Msieve 5A(PLOT)

GC_PC00898

1. hydrogen 40ppm2. argon 30ppm3. oxygen 50ppm4. nitrogen 50ppm5. methane 40ppm6. carbon monoxide 50ppm

Column: Rt®-Msieve 5A, 30m, 0.53mm ID, 50µm (cat.# 19723)Sample: permanent gases (ppm)Inj.: 5µL sample loop, 6-port Valco® valve, valve temp.: ambientInj. temp.: 200°CCarrier gas: helium, constant flowFlow: 5mL/min.Oven temp.: 27°C (hold 5 min.) to 100°C @ 10°C/min. (hold 5 min.)Det.: Valco® helium ionization detector @ 150°C

Argon

resolved

from oxygen.Excellent

peak shape

for carbon

monoxide.

Peak List1. helium2. hydrogen

Column: Rt®-Msieve 5A, 30m, 0.53mm ID, 50.0µm (cat.# 19723)Sample: helium/hydrogen gas mixtureInj.: 25µL split (split ratio 1:10), 40mL/min. split vent flow rate

2mm split Precision® liner w/wool (cat.# 20823)Inj. temp.: 200°CCarrier gas: nitrogen, constant pressure (7.0psi, 48.3kPa)Linear velocity: 38cm/sec. @ 30°COven temp.: 30°CDet.: TCD @ 200°CInstrument: Agilent 5890

Helium/Hydrogen

Rt®-Msieve 5A(PLOT)

GC_MS01136

NEW!


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Chlorofluorocarbon & Hydrocarbon Gases

Column: ShinCarbon ST, 100/120 mesh, 1m, 1mm IDSilcosteel® micropacked column (cat.# 19809)

Sample: fluorocarbon blend, 5µL ~1-3% eachInj. temp.: 200°CDet.: FID @ 250°CCarrier gas: helium Linear velocity: 10mL/min. Oven temp.: 125°C to 320°C @ 16°C/min.

PPeeaakk RReett.. TTiimmee ((mmiinn..))1. Freon® 134a/22 4.952. Freon® 12 7.113. Freon® 133a 9.194. Freon® 114 10.85

Chlorofluorocarbon Gases


GC_PC00673

for more infosee pages 706 & 707 for more chlorofluorocarbon chromatograms.

NEW!

1. methane2. ethane3. propane4. isobutane5. n-butane6. trans-2-butene7. 1-butene8. isobutylene

0 2 4 6 8 10 12 14 16 18Time (min)

Butane Lighter Fluid

Rt®-Alumina BOND/Na2SO4

(PLOT)

Column: Rt®-Alumina BOND/Na2SO4, 50m, 0.53mm ID, 10µm (cat.# 19756)

Sample: butane lighter fluidInj.: 100µL sample loop on gas sampling

valve, split (split vent flow 400mL/min.),2mm single gooseneck liner (cat.# 20795)

Inj. temp.: 200°CCarrier gas: hydrogen, constant pressure, 8.0psiLinear velocity: 74cm/sec. @ 45°COven temp.: 45°C (hold 1 min.) to 200°C @

10°C/min. (hold 3.5 min.)Det.: FID @ 200°C

GC_PC01083

12

3

4 5

6

7 8

min.

NEW!

1. methane2. ethane3. ethylene4. propane5. propylene6. isobutane7. n-butane

Column: Rt®-Alumina BOND/Na2SO4, 50m, 0.53mm ID, 10µm (cat.# 19756)

Sample: propane camping fuelInj.: 100µL sample loop on gas sampling

valve, split (split vent flow 400mL/min.),2mm single gooseneck liner (cat.# 20795)

Inj. temp.: 200°CCarrier gas: hydrogen, constant pressure, 8.0psiLinear velocity: 74cm/sec. @ 45°COven temp.: 45°C (hold 1 min.) to 200°C @

10°C/min. (hold 3.5 min.)Det.: FID @ 200°C

Propane Camping Fuel


(PLOT)

0 2 4 6 8 10 12 14 16 18Time (min)

1 2

3

4

5

6

7

GC_PC01084

min.




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Hydrocarbon Gases

Ethylene and C1-C5 Hydrocarbons

ASTM D6159-97

Rt®-Alumina BOND/KCI, Rtx®-1 (PLOT)

Column: Rt®-Alumina BOND/KCl, 50m, 0.53mm ID, 10.0µm (cat.# 19760) in series with Rtx®-1, 30m, 0.53mm ID, 5.0µm (cat.# 10179), connected using a Universal Press-Tight® Connector (cat.# 20401)

Sample: ethylene and C1-C5 hydrocarbonsInj.: 1µL split, 60mL/min. split vent flow rate

2mm splitless liner (cat.# 20712)Inj. temp.: 200°CCarrier gas: helium, constant pressure (8.0psi, 55.2kPa)Linear velocity: 25.4cm/sec. @ 35°COven temp.: 35°C (hold 2 min.) to 190°C @ 4°C/min. (hold 15 min.)

(conditions as per ASTM D6159-97)Det.: FID @ 200°CInstrument: Agilent 5890

Peak List1. methane2. ethane3. ethylene4. propane5. cyclopropane6. propylene7. acetylene8. isobutane9. propadiene

10 n-butane11. trans-2-butene12. 1-butene13. isobutylene14. cis-2-butene15. isopentane16. methyl acetylene17. n-pentane18. 1,3-butadiene

GC_PC01110

NEW!


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Hydrocarbon Gases

Natural Gas


(PLOT)

Column Rt®-Alumina BOND/Na2SO4, 50 m, 0.53 mm ID, 10 µm (cat.# 19756)Sample natural gas

IInnjjeeccttiioonnInj. Vol.: 500 µL splitLiner: Gooseneck Splitless (2mm) (cat.# 20795)Inj. Temp.: 200 °CSplit Vent

Flow Rate: 50 mL/min.

OOvveennOven Temp: 45 °C (hold 1 min.) to 200 °C at 10 °C/min. (hold 8.5 min.)

CCaarrrriieerr GGaass H2, constant pressure (8.0 psi, 55.2kPa)Linear Velocity: 45 cm/sec. @ 45 °C

DDeetteeccttoorr FID @ 200 °CMake-up

Gas Type: N2

Data Rate: 20 Hz

IInnssttrruummeenntt HP5890 GC

1. Methane2. Ethane3. Propane4. Isobutane5. n-Butane6. neo-Pentane7. Isopentane8. n-Pentane9. Hexane Isomers

10. Heptane Isomers11. Benzene12. C7+

Natural Gas

Rt®-Alumina BOND/KCl(PLOT)

GC_PC01091

1. Methane2. Ethane3. Propane4. Isobutane5. n-Butane6. neo-Pentane7. Isopentane8. n-Pentane9. Hexane Isomers

10. Heptane Isomers11. Benzene12. C7+

Column Rt®-Alumina BOND/KCl, 50 m, 0.53 mm ID, 10 µm (cat.# 19760)Sample natural gas

IInnjjeeccttiioonnInj. Vol.: 500 µL splitLiner: Gooseneck Splitless (2mm) (cat.# 20795)Inj. Temp.: 200 °CSplit Vent

Flow Rate: 50 mL/min.

OOvveennOven Temp: 45 °C (hold 1 min.) to 200 °C at 10 °C/min. (hold 8.5 min.)

CCaarrrriieerr GGaass H2, constant pressure (8.0 psi, 55.2kPa)Linear Velocity: 45 cm/sec. @ 45 °C

DDeetteeccttoorr FID @ 200 °CMake-up

Gas Type: N2

Data Rate: 20 Hz


NEW!

NEW!

GC_PC01092


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Hydrocarbon Gases

Column: ShinCarbon ST, 100/120 mesh 1m, 1mm ID Silcosteel® micropacked column (cat.# 19809)

Sample: 0.5-8% varied, C1-C6 hydrocarbonsInj. temp.: 200°CDet.: FID @ 250°CCarrier gas: helium (constant flow)Linear velocity: 10mL/min. Oven temp.: 125°C to 250°C @ 16°C/min.

1. C12. C23. C34. iC4-isobutane5. C46. iC5-isopentane7. nC58. hexanes

Natural Gas


GC_PC00672

Natural Gas #2

Rt®-QS-BOND(PLOT)

Column: Rt®-QS-BOND, 30m, 0.53mm ID (cat.# 19738)Sample: natural gas mix (mole%)Inj.: 20µL split (split ratio 10:1), 4mm Siltek® single

gooseneck liner (cat.# 20798-214.1)Inj. temp.: 240°CCarrier gas: helium, constant flow Flow rate: 5.7mL/min. @ 40°COven temp.: 40°C (hold 2 min.) to 225°C @ 20°C/min. (hold 5 min.)Det.: FID @ 240°C

GC_PC01013

1. methane2. ethane3. propane4. isobutane5. n-butane6. isopentane7. n-pentane8. hexanes & hexenes

Propylene and C1-C5 Hydrocarbons


(PLOT)

Column: Rt®-Alumina BOND/Na2SO4, 50m, 0.53mm ID, 10.0µm (cat.# 19756) Sample: propylene and C1-C5 hydrocarbonsInj.: 10µL split, 35mL/min. split vent flow rate

2mm splitless liner (cat.# 20712)Inj. temp.: 200°CCarrier gas: helium, constant pressure (10.0psi, 68.9kPa)Linear velocity: 47cm/sec. @ 50°COven temp.: 50°C to 150°C @ 6°C/min.Det.: FID @ 200°CInstrument: Agilent 5890

Peak List1. methane2. ethane3. ethylene4. propane5. cyclopropane6. propylene7. isobutane8. n-butane9. propadiene

10. acetylene11. trans-2-butene12. 1-butene13. isobutylene14. cis-2-butene15. isopentane16. n-pentane17. 1,3-butadiene18. methyl acetylene

GC_PC01142

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Hydrocarbon Gases

Refinery Gas


(PLOT)

1. methane2. ethane3. ethylene4. propane5. propylene6. isobutane7. n-butane8. propadiene9. acetylene

10. trans-2-butene11. 1-butene

12. isobutylene13. cis-2-butene14. isopentane15. n-pentane16. 1,3-butadiene17. trans-2-pentene18. 2-methyl-2-butene19. 1-pentene20. cis-2-pentene21. hexanes

Column: Rt®-Alumina BOND/Na2SO4, 50m, 0.53mm ID, 10µm (cat.# 19756)Sample: refinery gasInj.: 10µL split (split vent flow 80mL/min.), 2mm single gooseneck liner

(cat.# 20795)Inj. temp.: 200°CCarrier gas: hydrogen, constant pressure, 8.0psiLinear velocity: 74cm/sec. @ 45°COven temp.: 45°C (hold 1 min.) to 200°C @ 10°C/min. (hold 3.5 min.)Det.: FID @ 200°C

GC_PC01085

NEW!

0 2 4 6 8 10 12 14 16 18Time (min)

Refinery Gas

Rt®-Alumina BOND/KCl(PLOT)

Column: Rt®-Alumina BOND/KCl, 50m, 0.53mm ID, 10µm (cat.# 19760)Sample: refinery gasInj.: 10µL split (split vent flow 80mL/min.),

2mm single gooseneck liner (cat.# 20795)Inj. temp.: 200°CCarrier gas: hydrogen, constant pressure, 8.0psiLinear velocity: 74cm/sec. @ 45°COven temp.: 45°C (hold 1 min.) to 200°C @ 10°C/min. (hold 3.5 min.)Det.: FID @ 200°C

1. methane2. ethane3. ethylene4. propane5. propylene6. isobutane7. n-butane8. propadiene9. acetylene

10. trans-2-butene11. 1-butene12. isobutylene13. cis-2-butene14. isopentane15. n-pentane16. 1,3-butadiene17. trans-2-pentene18. 2-methyl-2-butene19. 1-pentene20. cis-2-pentene21. hexanes

12 3 4

5

6

7,8

9

10

11

12

13

14

15

16

17

18 19

20 21

GC_PC01088

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Hydrocarbon Gases, Hydrocarbons

Aromatics, Aliphatics

10% TCEP 100/120 Chromosorb® PAW(packed)

Column: 10% TCEP on 100/120 Chromosorb® PAW, 2.5m, 1/8" OD, 2mm ID SilcoSmooth® tubing (cat.# 80126)

Sample size: 0.1mL neatOven temp.: 80°CInj./det. temp.: 200°C/250°CCarrier gas: nitrogenFlow rate: 20mL/min.FID sensitivity: 128 x 10-10 AFS

1. n-hexane2. n-heptane3. n-octane4. n-nonane5. n-decane6. benzene7. toluene8. ethylbenzene

9a. m-xylene9b. p-xylene10. isopropylbenzene11. o-xylene

1 2 3 4

5

6

7

8

9

1011

min. 2 4 6 8 10 12 14 16GC_PC00217

NEW!

0 2 4 6 8 10 12 14 16 18Time (min)

CCoolluummnn Rt®-QS-BOND, 30 m, 0.53 mm ID, 20 µm (cat.# 19738)SSaammppllee refinery gas standard

IInnjjeeccttiioonnInj. Vol.: 20 µL splitLiner: 2mm Splitless (cat.# 20712)Inj. Temp.: 200 °CSplit Vent FlowRate: 35 mL/min.

OOvveennOven Temp: 40 °C (hold 2 min.) to 225 °C at 15 °C/min. (hold 5 min.)

CCaarrrriieerr GGaass He, constant pressure (11.5 psi, 79.3kPa)Linear Velocity: 68 cm/sec. @ 40 °C

DDeetteeccttoorr TCD @ 225 °CMake-up Gas Type: HeData Rate: 20 HzSensitivity Mode: He/H2


Peaks1. Air2. Methane3. Carbon dioxide4. Ethylene5. Acetylene6. Ethane7. Propylene8. Propane9. Propadiene

10. Isobutane11. Isobutylene/1-Butene12. 1,3-Butadiene13. n-Butane/cis-2-Butene14. trans-2-Butene15. Isopentane16. 1-Pentene17. 2-Methyl-2-butene18. n-Pentane/cis-2-Pentene19. n-Hexane

Refinery Gas Mixture

Rt®-QS-BOND(PLOT)

GC_PC1143

1 2

3

4

5

6

7

9

8

10

11

12

14

13

15

1617

18

19





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Hydrocarbons

Aromatics (Xylene Isomers plus Cumene)

5% Rt®-1200/1.75% Bentone® 34(packed)

1 2

3

4

56

7 8

9 10

11

min. 2 4 6 8 10 12 14

1. hexane2. benzene3. n-octane4. toluene5. n-nonane6. ethylbenzene7. p-xylene8. m-xylene9. o-xylene

10. cumene11. n-decane

Column: 5% Rt®-1200/1.75% Bentone® 34 on 100/120 Silcoport®, 1.8m, 1/8" OD, 2mm ID SilcoSmooth® tubing (cat.# 80125)

Sample size: 0.1µLConc.: 0.5µg/µL in hexaneOven temp.: 75°CInj./det. temp.: 200°CCarrier gas: nitrogenFlow rate: 20mL/min.FID sensitivity: 32 x 10-11 AFS

GC_PC00192

Aromatics (Xylene Isomers /BTEX)

5% Rt®-1200/5% Bentone® 34(packed)

1

2

34 5

6

1. benzene2. toluene3. ethylbenzene4. p-xylene5. m-xylene6. o-xylene

Column: 5% Rt®-1200/5% Bentone® 34 100/120 Silcoport®, 2m, 1/8" OD, 2mm ID SilcoSmooth® tubing (cat.# 80129)

Sample size: 0.1µLConc.: 0.5µg/µL in hexaneOven temp.: 100°CInj./det. temp.: 200°CCarrier gas: nitrogenFlow rate: 20mL/min.FID sensitivity: 32 x 10-11 AFS

GC_PC00193

min. 1 2 3 4 5 6 7

Aromatics

Rt®-TCEP

min. 0 2 4 6 8 10 12 14 16 18GC_PC00211

15

14

13

12

119

1087

6

5

421

3

1. n-undecane2. benzene3. n-dodecane4. toluene5. ethylbenzene6. p-xylene7. m-xylene8. cumene9. n-propylbenzene

10. o-xylene11. mesitylene12. 1-ethyl-2-methylbenzene13. m-diethylbenzene14. p-diethylbenzene15. o-diethylbenzene

Column: Rt®-TCEP, 60m, 0.25mm ID, 0.40µm (cat.# 10999)

Inj.: 1.0µL split injection, components @ 500ppm (ethylbenzene @ 1000ppm)


Inj./det. temp.: 200°CCarrier gas: heliumLinear velocity: 30cm/sec. set @ 80°CFID sensitivity: 6.4 x 10-11 AFSSplit flow: 46mL/min.


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Hydrocarbons

1. nonaromatics2. benzene3. methyl ethyl ketone (IS)4. toluene

Motor Oil & Aviation Gas

ASTM Method D3606-99

10% Rtx®-1 & 20% TCEP(micropacked)

Column:A: 10% Rtx®-1 on 60/80 Chromosorb® WAW, 0.8m, 1/16 inch, 1mm ID Silcosteel® tubing

B: 20% TCEP on 80/100 Chromosorb® PAW, 4.0m, 1/16 inch, 1mmID Silcosteel® tubing connected in series and using MicropackedColumn On-Column Injection Kit

Sample: benzene, toluene, methyl ethyl ketone in pentaneInj.: 1.0µL, on-column, 4mm ID splitless inlet liner

(cat.# 20772)Carrier gas: hydrogen,

constant flowFlow rate: 9.0mL/min.Inj. temp.: 200°COven temp.: 145°CDet.: FID @ 200°C

GC_PC00775

NEW!

Gasoline

ASTM D3606 Modified (for Gasoline Containing Ethanol)(packed)

1. ethanol2. benzene3. 2-butanol4. toluene

Column: D3606 Application Column (2 column set, cat.# 83606-800) Column 1: nonpolar Rtx®-1, 6' (1.8m), 1/8" OD, 2.0mm IDColumn 2: proprietary packing material, 16' (4.9m), 1/8" OD, 2.0mm ID

Sample: 1.5µL gasoline with internal standardInj.: 200°CBackflush: 3 min.Carrier gas: helium, constant flowFlow rate: 20mL/min.Oven temp.: 135°C, isothermal Det.: TCD @ 200°C

GC_PC01079

Chromatogram courtesy of Boguslaw Dudek, Conoco Phillips, Linden, NJ.


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Hydrocarbons

1

2

3

4

9 10 11 12 min

Column: Rtx®-DHA-100, 100m, 0.25mm ID, 0.5µm (cat.# 10148) plus Rtx®-5 DHA tuning column, 2.62m, 0.25mm ID, 1.0µm, connected via Press-Tight® connector (cat.# 20446)

Sample: custom detailed hydrocarbons analysis (DHA) mix, neat

Inj.: 0.01µL, split (split ratio 150:1),4mm cup inlet liner (cat.# 20709)

Inj. temp.: 200°CCarrier gas: helium, constant flowLinear velocity: 28cm/sec. (2.3mL/min.)Oven temp.: 35°CDet.: FID @ 250°C

1. ethanol2. C53. tert-butanol4. 2-methylbutene-2

C5 efficiency: 613,596 total theoretical platesk' (C5): 0.489tert-butanol skewness: 1.25Resolution (tert-butanol/2-methylbutene-2): 5.60

GC_PC00743A

Detailed Hydrocarbons Analysis (DHA)

Rtx®-DHA-100/Rtx®-5 DHA Tuning Column

Fast Detailed Hydrocarbons Analysis (DHA)

Rtx®-DHA-100/Rtx®-5 DHA Tuning Column

AA:: FFrroonntt eenndd ooff DDHHAA//ooxxyyggeennaatteess sseettuupp bblleennddC5 efficiency: 586,825 platesC5 k': 0.476tert-butanol skew: 2.10Resolution tert-butanol/2-methylbutene-2: R = 5.39

BB:: DDHHAA//ooxxyyggeennaatteess sseettuupp bblleenndd1. ethanol2. C53. tert-butanol4. 2-methylbutene-25. 2,3-dimethylbutane6. methyl tert-butyl ether (MTBE)7. C68. 1-methylcyclopentene9. benzene

10. cyclohexane11. 3-ethylpentane

12. 1,2-dimethylcyclopentane13. C714. 2,2,3-trimethylpentane15. 2,3,3-trimethylpentane16. toluene17. C818. ethylbenzene19. p-xylene20. 2,3-dimethylheptane21. C922. 5-methylnonane23. 1,2-methylethylbenzene24. C1025. C1126. 1,2,3,5-tetramethylbenzene27. naphthalene28. C1229. 1-methylnaphthalene30. C13

Column: Rtx®-DHA-100 100m, 0.25mm ID, 0.5µm (cat.# 10148) plus Rtx®-5 DHA tuning column (cat.# 10165), connected via angled Press-Tight® connector (cat.# 20446)

Sample: DHA/oxygenates setup blendInj.: 0.01µL, split (split ratio 150:1), 4mm ID cup inlet liner

(cat.# 20709)A: front slice of DHA/oxygenates setup blendB: DHA/oxygenates setup blend

Carrier gas: hydrogen, constant flow (3.62cc/min.)Linear velocity: 55cm/sec.Inj. temp.: 250°COven temp.: A: 35°C

B: 5°C (hold 8.32 min.) (elute C5) to 48°C @ 22°C/min. (hold 26.32 min.) (elute ethylbenzene) to 141°C @ 3.20°C/min. (no hold) (elute C12) to 300°C @ 1°C/min.

Det.: FID @ 300°C

GC_PC00774

Chromatogram courtesy of Neil Johansen, Inc., Aztec, New Mexico, in association withEnvantage Analytical Software, Inc., Cleveland, Ohio.

conditions and peak identifications shown below

Excellent peak

shape for alcohols.

AB


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Hydrocarbons

Hydrocarbons, C7-C42

Rtx®-1

min. 4 8 12 16 20 24 28 32 36 40 44 48 52 56 60

12

3

4

5

79 11

12

13

14

1516

6 8 10 17 20

19

21

22

23

24

2526

27

Column: Rtx®-1, 30m, 0.53mm ID, 0.25µm (cat.# 10125)Sample: 0.2µL injection of a synthetic hydrocarbon mix,

~ 0.1mg/mL per component Inj.: Direct injection using a Uniliner® inlet linerOven temp.: 40°C to 340°C @ 5°C/min.Inj./det. temp.: 340°CCarrier gas: hydrogenLinear velocity: 40cm/sec. set @ 40°CFID sensitivity: 64 x 10-11 AFS

18

GC_PC00216

1. C72. C83. C94. C105. C116. C127. C138. C149. C15

10. C1611. C1712. C1813. C1914. C2015. C22

16. C2317. C2418. C2519. C2620. C2821. C3022. C3223. C3424. C3625. C3826. C4027. C42

GC_PC1165

C5-C106 Hydrocarbons on MXT®-1HT SimDist at 430 °CPPeeaakkss RRTT ((mmiinn..))

1. C5 —2. C6 —3. C7 —4. C8 —5. C9 —6. C10 —7. C11 —8. C12 0.9889. C13 1.677

10. C14 2.54411. C15 3.50312. C16 4.48413. C17 5.45114. C18 6.38615. C20 8.1516. C22 9.76417. C24 11.25918. C26 12.64519. C28 13.92020. C30 15.134

PPeeaakkss RRTT ((mmiinn..))21. C32 16.28022. C34 17.36423. C36 18.39224. C38 19.37125. C40 20.36326. C42 21.19927. C44 22.04128. C46 22.84329. C48 23.60930. C50 24.34031. C52 25.04132. C54 25.71233. C56 26.36534. C58 26.99035. C60 27.59436. C62 28.17337. C64 28.73338. C66 29.27439. C68 29.79740. C70 30.303

PPeeaakkss RRTT ((mmiinn..))41. C72 30.78942. C74 31.26543. C76 31.72544. C78 32.17345. C80 32.60946. C82 33.03347. C84 33.45448. C86 33.85849. C88 34.25650. C90 34.64351. C92 35.02452. C94 35.39553. C96 35.75854. C98 36.11555. C100 36.46056. C102 36.80357. C104 37.13958. C106 37.465

CCoolluummnn MXT®-1HT SimDist, 5 m, 0.53 mm ID, 0.10 µm (cat.# 70112)SSaammppllee custom C5-C106 hydrocarbon standardDiluent: carbon disulfideConc.: 1%IInnjjeeccttiioonnInj. Vol.: 0.5 µL cold on-columnTemp. Program: 53°C to 430°C at 10°C/min. (hold 5 min.)OOvveennOven Temp: 50 °C to 430 °C at 10 °C/min. (hold 5 min.)CCaarrrriieerr GGaass He, constant flowFlow Rate: 18 mL/min.DDeetteeccttoorr FID @ 430 °CMake-up GasFlow Rate: 24 mL/min.Constant Column + Constant Make-up: 42 mL/min.Make-upGas Type: N2

Data Rate: 20 HzIInnssttrruummeenntt Shimadzu 2010 GC

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on the market!


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Hydrocarbons

5 10 15 20 25 min.

C9

C10

C11

C14

C12

C16

C18

C20

C24

C28

C32

C36

C40

C44

Column: MXT®-1HT Sim Dist, 5m, 0.53mm ID, 0.10µm (cat.# 70100)

Sample: 0.2µL hydrocarbon standard (cat.# 31222)Solvent: carbon disulfideOven temp.: 40°C to 430°C @ 10°C/min. (hold 30 min.)Injector: on-column (track oven)Carrier gas: helium (constant pressure)Head pressure: 1.0psiLinear velocity: 60cm/sec.Flow rate: 7.8mL/min.Det.: FID @ 430°CMake-up gas flow: 40cc/min.

GC_PC00529

Hydrocarbons (C10-C44)

MXT®-1HT Sim Dist

GC_PC1164

C5-C106 Hydrocarbons on MXT®-1HT SimDist at 450 °C

CCoolluummnn MXT®-1HT SimDist, 5 m, 0.53 mm ID, 0.10 µm (cat.# 70112)SSaammppllee custom C5-C106 hydrocarbon standardDiluent: carbon disulfideConc.: 1%IInnjjeeccttiioonnInj. Vol.: 0.5 µL cold on-columnTemp. Program: 53°C to 450°C at 10°C/min. (hold 5 min.)OOvveennOven Temp: 50 °C to 450 °C at 10 °C/min. (hold 5 min.)CCaarrrriieerr GGaass He, constant flowFlow Rate: 18 mL/min.DDeetteeccttoorr FID @ 450 °CMake-upGas Flow Rate: 24 mL/min.Constant Column + Constant Make-up: 42 mL/min.Make-upGas Type: N2

Data Rate: 20 HzIInnssttrruummeenntt Shimadzu 2010 GC

PPeeaakkss RRTT ((mmiinn..))1. C5 —2. C6 —3. C7 —4. C8 —5. C9 —6. C10 —7. C11 —8. C12 0.9389. C13 1.586

10. C14 2.42511. C15 3.36512. C16 4.33213. C17 5.29014. C18 6.21715. C20 7.96616. C22 9.56617. C24 11.05118. C26 12.42619. C28 13.68920. C30 14.897

PPeeaakkss RRTT ((mmiinn..))21. C32 16.03522. C34 17.11023. C36 18.13324. C38 19.10825. C40 20.09626. C42 20.92327. C44 21.75928. C46 22.55629. C48 23.31730. C50 24.05131. C52 24.75232. C54 25.42233. C56 26.07934. C58 26.70135. C60 27.30536. C62 27.87837. C64 28.43938. C66 28.97539. C68 29.49940. C70 30.002

PPeeaakkss RRTT ((mmiinn..))41. C72 30.48942. C74 30.90643. C76 31.41444. C78 31.86245. C80 32.29446. C82 32.71947. C84 33.13248. C86 33.52949. C88 33.92750. C90 34.31051. C92 34.68952. C94 35.05953. C96 35.42354. C98 35.77355. C100 36.12056. C102 36.46357. C104 36.79358. C106 37.118

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Hydrocarbons (Simulated Distillation)

Simulated Distillation

(Standard Calibration)

MXT®-1 Sim Dist

3

2

5

4

67

8

9

10

11 12

13 1415

1617

min. 4 8 12 16 20 24

1. C62. C73. C84. C95. C106. C117. C128. C149. C16

10. C1811. C2012. C2413. C2814. C3215. C3616. C4017. C44

1

GC_PC00224

Column: MXT®-1 Sim Dist, 6m, 0.53mm ID, 0.15µm (cat.# 70101)Sample: wet needle on-column injection of ASTM D2887 standardOven temp.: -12°C to 430°C @ 20°C/min. Inj./det. temp.: -17°C to 433°C/430°CCarrier gas: hydrogenLinear velocity: 40cm/sec. FID sensitivity: 128 x 10-11 AFS


(High-Temperature)

MXT®-500 Sim Dist

Column: MXT®-500 Sim Dist, 6m, 0.53mm ID, 0.15µm (cat.# 70104)Sample: cold on-column injection of Polywax® 655 in CS2

Oven temp.: 40°C to 430°C @ 6°C/min.Carrier gas: heliumLinear velocity: 40cm/sec.FID sensitivity: 2 x 10-11AFS

20 24 28 32 36 40 44 48 52 56 60 64 68min.

GC_PC00225

GC_PC00750


Rtx®-2887

Column: Rtx®-2887, 10m, 0.53mm ID, 2.65µm (cat.# 10199)Sample: 1µL direct injection of 0.01-0.1 wt. % C5 to C44 hydrocarbon standard

in carbon disulfide Inj. temp.: 360°CDet. temp: 360°CCarrier gas: helium (constant flow)Linear velocity: 15mL/min. (112cm/sec.)Oven temp.: 35°C to 360°C @ 15°C/min. (hold 5 min.)

1. C52. C63. C74. C85. C96. C107. C118. C129. C14

10. C1611. C1812. C2013. C2414. C2815. C3216. C3617. C4018. C44


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1. pentane2. hexane3. heptane4. octane5. nonane6. decane7. undecane8. dodecane9. tetradecane

10. hexadecane11. octadecane12. eicosane13. tetracosane14. octacosane15. dotricontane16. hexatriacontane17. tetracontane18. tetratetracontane

Simulated Distillation (ASTM D-2887)

Rtx®-1 SimDist 2887(packed)

1 2 3 4 5 6 7 8 9 10 11

1213

14 15 16 17 18

min. 0 10 20 30

GC_PC00228

Column: Rtx®-1 SimDist 2887, SilcoSmooth® stainless steel, 25", 1/8", 2mm ID (cat.# 80000)

Inj.: 1.0µL direct injection, 1–12% (w/w) each componentOven temp.: 35°C to 350°C @ 10°C/min. (hold 5 min.)Inj./det. temp.: 350°CCarrier gas: helium @ 25mL/min.FID sensitivity: 256 x 10-11 AFS

cat.# 31674 (1% each listed analyte in CS2) and cat.# 31675 (5% each, neat) meet requirements of ASTM D2887-01.

GC_PC00852

Column: Rtx®-1, 30m, 0.53mm ID, 5.0µm (cat.# 10179)Sample: custom paraffin mix, neat, 2.7-12.9% each componentInj.: 0.1µL splitless (hold 1 min.), 4mm single gooseneck inlet liner (cat.# 20904)Inj. temp.: 250°CCarrier gas: hydrogen, constant flow (Parker ChromGas® hydrogen generator)Linear velocity: 184cm/sec. @ 40°COven temp.: 40°C (1 min.) to 265°C @ 25°C/min. (hold 4 min.)Det.: FID @ 280°C

1. ethanol2. isopentane3. n-pentane4. 2-methylpentane5. n-hexane6. 2,4-dimethylpentane7. n-heptane8. toluene9. n-octane

10. p-xylene11. n-propylbenzene12. n-decane13. butylbenzene14. n-dodecane15. n-tridecane16. n-tetradecane17. n-pentadecane18. n-hexadecane


Rtx®-1 (Hydrogen Carrier Gas)


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Simulated Distillation (ASTM D-3710 Calibration)



Sample: D-3710 Calibration Mix, C3, C4, C16, & C17 addedOven temp: -30°C to 250°C @ 10°C/min.Inj./det. temp.: 250°C/300°CCarrier gas: helium @ 25mL/min.FID sensitivity: 256 x 10-11 AFS

1. n-propane2. 2-methyl propane3. n-butane4. 2-methylbutane5. n-pentane6. 2-methylpentane7. n-hexane8. 2,4-dimethylpentane9. n-heptane

10. toluene11. n-octane12. p-xylene13. n-propylbenzene14. n-decane15. n-butylbenzene16. n-dodecane17. n-tridecane18. n-tetradecane19. n-pentadecane20. n-hexadecane21. n-heptadecane2

3

1

min. 0 5 10 15 20

4 5 6 7 8 9 10 11 12 13

14

15

16

17 18 19 20 21

GC_PC00229

Simulated Distillation (ASTM D-3710, Gasoline)



Sample: 1.0µL direct injection of unleaded gasoline (ASTM D-2887)Oven temp: -30°C to 250°C @ 10°C/min.Inj./det. temp.: 250°C/300°CCarrier gas: helium @ 25mL/min.FID sensitivity: 256 x 10-11 AFS

1. n-propane2. 2-methyl propane3. n-butane4. 2-methylbutane5. n-pentane6. 2-methylpentane7. n-hexane8. 2,4-dimethylpentane9. n-heptane

10. toluene11. p-xylene12. n-propylbenzene13. n-decane14. n-butylbenzene

min. 0 5 10 15

4

6

5

2

1

7

89

10 11

12

1413

GC_PC00230

3


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Hydrocarbons (High-Temperature)

GC_PC1159

Crude Oil on Rxi®-5HT

CCoolluummnn Rxi®-5HT, 30 m, 0.32 mm ID, 0.25 µm (cat.# 13924)using Rxi® Guard Column 2 m, 0.53 mm ID (cat.# 10054)

SSaammppllee System Performance Test Standard Mixture of n-Alkanes (cat.# 31678)

Diluent: HexaneConc.: 50 µg/mLIInnjjeeccttiioonnInj. Vol.: 1 µL cold on-columnTemp. Program: 53°C to 300°C at 10°C/min. (hold 20 min.)OOvveennOven Temp: 50 °C to 300 °C at 10 °C/min. (hold 20 min.)CCaarrrriieerr GGaass H2, constant flowLinear Velocity: 40 cm/sec. @ 50 °CDead Time: 1.25 min. @ 50 °CDDeetteeccttoorr FID @ 330 °CMake-up GasFlow Rate: 30 mL/min.Make-upGas Type: N2

Data Rate: 20 HzIInnssttrruummeenntt Agilent/HP6890 GC

GC_PC1160

Diesel on Rxi®-5HT

GC_PC1161

Gasoline on Rxi®-5HT

NEW!

GC_PC1162

Kerosene on Rxi®-5HT

CCoolluummnn Rxi®-5HT, 30 m, 0.32 mm ID, 0.25 µm (cat.# 13924)using Rxi® guard column 2 m, 0.53 mm ID (cat.# 10054)

SSaammppllee diesel fuel #2 composite (cat.# 31258)Diluent: methylene chlorideConc.: 50,000 µg/mL diluted to 500 ppm and spiked with C10 & C40


SSaammppllee unleaded gasoline composite (cat.# 30081)Diluent: methanolConc.: 2,500 µg/mL diluted to 500 ppm and spiked with C10 & C40


SSaammppllee kerosene composite (cat.# 31094)Diluent: methylene chlorideConc.: 500 µg/mL spiked with C10 & C40

GC_PC1163

Mineral Oil & Motor Oil on Rxi®-5HT

CCoolluummnn Rxi®-5HT, 30 m, 0.32 mm ID, 0.25 µm (cat.# 13924)using Rxi® Guard Column 2 m, 0.53 mm ID (cat.# 10054)

SSaammppllee custom mineral oil and motor oil standardDiluent: hexaneConc.: 500 µg/mL

NEW! NEW!

NEW! NEW!

(See GC_PC1159 above for conditions.) (See GC_PC1159 above for conditions.)

(See GC_PC1159 above for conditions.) (See GC_PC1159 above for conditions.)


min. 4 8 12 16 20 24 28

1 23

4

5

6

7

8

1. thiophene2. 2-methylthiophene3. 3-methylthiophene4. 2-ethylthiophene5. alkylthiophenes6. benzothiophene7. methylbenzothiophenes8. dimethylbenzothiophenes

Sulfur in Gasoline

Rtx®-1

GC_PC00198

Column: Rtx®-1, 30m, 0.32mm ID, 4.0µm (cat.# 10198)Sample: 1.0µL split injection of gasoline containing 300ppm

total sulfurOven temp.: 40°C (hold 3 min.) to 275°C @ 10°C/min.

(hold 5 min.)Inj./det. temp.: 275°CDet.: SCD Carrier gas: heliumLinear velocity: 70cm/sec. (flow rate: 2.5mL/min.)Split ratio: 10:1

Column: Rt®-XLSulfur micropacked column, 1m, 0.75mm ID (cat.# 19806)

Conc.: 50ppb eachOven temp.: 60°C to 230°C @ 15°C/min. Carrier gas: heliumFlow rate: 9mL/min.Det.: SCD/FID

Sulfur standards courtesy of DCG Partnership 1 Ltd., Pearland, TX.

Sulfur Compounds

Rt®-XLSulfur(micropacked)

ssuullffuurrss1. hydrogen sulfide2. carbonyl sulfide3. methyl mercaptan4. ethyl mercaptan5. dimethyl sulfide6. dimethyl disulfide

hhyyddrrooccaarrbboonnssA. methaneB. ethaneC. propyleneD. propaneE. isobutaneF. butaneG. isopentaneH. pentaneI. hexane

1

23

4/5

6

min. 2 4 6 8 10GC_PC00436

A B

C

D

E

F

GH

I

Sulfur Compounds

Rxi®-1ms

GC_AR00861

Column: Rxi®-1ms, 30m, 0.32mm ID, 4.00µm (cat.# 13396)Sample: hydrogen sulfide, carbonyl sulfide, methyl mercaptan,

ethyl mercaptan, dimethyl sulfide, 100 ppbv each in heliumInj.: 1mL splitless, directSample loop temp.: 30°CCarrier gas: helium, constant pressureLinear velocity: 48cm/sec. @ 30°COven temp.: 30°CDet.: sulfur chemiluminescence detectorDet. temp.: 800°C

Sample storage & transfer:SilcoCan® air monitoring canister with Siltek® treated 1/4" valve (cat.# 24182-650);Sulfinert® treated gas sample loop, 1cc (cat.# 22848); Sulfinert® treated gas sample loop,10cc (custom order)

1. hydrogen sulfide2. carbonyl sulfide3. methyl mercaptan4. ethyl mercaptan5. dimethyl sulfide



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Hydrocarbons (High-Temperature), Sulfur Compounds

GC_PC1172

Midrange Crude on Rxi®-5HT

PPeeaakkss1. C172. Pristane3. C184. Phytane

CCoolluummnn Rxi®-5HT, 30 m, 0.32 mm ID, 0.10 µm (cat.# 13909)using retention gap 2 m, 0.53 mm ID,

SSaammppllee Midrange crudeConc.: 500 µg/mLIInnjjeeccttiioonnInj. Vol.: 1.0 µL cold on-columnOOvveennOven Temp: 50 °C to 300 °C at 10 °C/min. (hold 10 min.)CCaarrrriieerr GGaass H2, constant flowLinear Velocity: 40 cm/sec.DDeetteeccttoorr FID @ 330 °CIInnssttrruummeenntt Agilent/HP6890 GCAAcckknnoowwlleeddggeemmeenntt Sample courtesy of Exxon Mobil Corporation

NEW!


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GC CHROMATOGRAMS | CLINICAL, FORENSIC & TOXICOLOGY

Arson Accelerants

Unleaded Gasoline

Rxi®-1ms

Column: Rxi®-1ms, 30m, 0.25mm ID, 0.25µm (cat.# 13323)Sample: 5,000µg/mL unleaded gasoline, unweathered, in methanol

(cat.# 30096)Inj.: 1µL split (split ratio 20:1), 4mm single gooseneck liner w/ wool

(cat.# 22405)Inj. temp.: 250°CCarrier gas: helium, constant flow Linear velocity: 28cm/sec. @ 50°COven temp.: 50°C (hold 2 min.) to 75°C @ 10°C/min. to 300°C @ 20°C/min.

(hold 5 min.)Det.: FID @ 300°C

GC_PC01071

99% Weathered Unleaded Gasoline

Rxi®-1ms

Column: Rxi®-1ms, 30m, 0.25mm ID, 0.25µm (cat.# 13323)Sample: 5,000µg/mL unleaded gasoline, 99% weathered, in methanol

(cat.# 30436)Inj.: 1µL split (split ratio 20:1), 4mm single gooseneck liner w/ wool

(cat.# 22405)Inj. temp.: 250°CCarrier gas: helium, constant flow Linear velocity: 28cm/sec. @ 50°COven temp.: 50°C (hold 2 min.) to 75°C @ 10°C/min. to 300°C @ 20°C/min.

(hold 5 min.)Det.: FID @ 300°

GC_PC01070

Unweathered Kerosene

Rxi®-1ms

GC_PC01060

Column: Rxi®-1ms, 30m, 0.25mm ID, 0.25µm (cat.# 13323)Sample: 5,000µg/mL kerosene, unweathered, in methylene chloride (cat.# 31229)Inj.: 1µL split (split ratio 20:1), 4mm single gooseneck liner w/ wool (cat.# 22405)Inj. temp.: 250°CCarrier gas: helium, constant flow Linear velocity: 28cm/sec. @ 50°COven temp.: 50°C (hold 2 min.) to 75°C @ 10°C/min. to 300°C @ 20°C/min. (hold 5 min.)Det.: FID @ 300°C

665-674_GCappforensic.qxp 11/22/2010 9:28 PM Page 665

50% Weathered Diesel Fuel #2

Rxi®-1ms

GC_PC00921

Column: Rxi®-1ms, 30m, 0.25mm ID, 0.50µm (cat.# 13338) Sample: 5,000µg/mL diesel fuel #2, 50% weathered (cat.# 31235)

in methylene chlorideInj.: 1.0µL split (split ratio 20:1), 4mm single gooseneck

w/wool inlet liner (cat.# 22405)Inj. temp.: 250°CCarrier gas: helium, constant flowLinear velocity: 28cm/sec. @ 50°COven temp.: 50°C (hold 2 min.) to 75°C @ 10°C/min.,


Unweathered Diesel Fuel #2

Rxi®-1ms

GC_PC00922

Column: Rxi®-1ms, 30m, 0.25mm ID, 0.50µm (cat.# 13338) Sample: 5,000µg/mL diesel fuel #2, unweathered (cat.# 31233) in

methylene chlorideInj.: 1.0µL split (split ratio 20:1),

4mm single gooseneck w/wool inlet liner (cat.# 22405)Inj. temp.: 250°CCarrier gas: helium, constant flowLinear velocity: 28cm/sec. @ 50°COven temp.: 50°C (hold 2 min.) to 75°C @ 10°C/min.,


Column: Rxi®-1ms, 30m, 0.25mm ID, 0.25µm (cat.# 13323)Sample: 5,000µg/mL mineral spirits, unweathered, in methylene chloride (cat.# 31225)Inj.: 1µL split (split ratio 20:1), 4mm single gooseneck liner w/ wool (cat.# 22405)Inj. temp.: 250°CCarrier gas: helium, constant flow Linear velocity: 28cm/sec. @ 50°COven temp.: 50°C (hold 2 min.) to 75°C @ 10°C/min. to 300°C @ 20°C/min. (hold 5 min.)Det.: FID @ 300°C

Mineral Spirits

Rxi®-1ms

GC_PC01066





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Arson Accelerants




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Blood Alcohols

Blood Alcohol

5% Carbowax® 20M on CarboBlack B(packed; headspace analysis)

Column: 5% Carbowax® 20M on 80/120 CarboBlack B, 6 ft., 1/8", 2.0mm ID SilcoSmooth® tubing(cat.# 80105)

Inj.: 500µL, headspaceConc.: 0.05gm/dLOven temp.: 90°CInj./det. temp.: 200°CCarrier gas: heliumFlow rate: 18mL/min.

1. acetaldehyde2. methanol3. acetone4. ethanol5. isopropanol6. tert-butanol

GC_PH00478

Blood Alcohol

Rtx®-BAC1 & Rtx®-BAC2 (0.32 mm ID Columns)(headspace analysis)

Dual-column analysis using a two-hole ferrule. Sample: 1.0mL headspace sample of a blood alcohol mix

on a PerkinElmer HS 40 headspace autosamplerOven temp.: 40°CInj. temp.: 200°CCarrier gas: heliumSample equilibration: 70°C, 15 min.Vial pressure: 30psiVial pressurization time: 0.15 min.

Vial sampling time: 0.01 min.Transfer line: 0.32mm ID Hydroguard® fused silica tubingTransfer line temp.: 200°CInjection port sleeve: 2mm IDSplit flow: 20mL/min.

CCoonncc..ww//vv

1. methanol 0.1%2. acetaldehyde 0.2%3. ethanol 0.2%4. isopropanol 0.1%5. acetone 0.01%6. n-propanol 0.1%

Rtx®-BAC1, 30m, 0.32mm ID, 1.8μm (cat.# 18003) Rtx®-BAC2, 30m, 0.32mm ID, 1.2μm (cat.# 18002)

min. 1.0 1.2 1.4 1.6 1.8 2.0 2.2 2.4 2.6 2.8 3.0

6

5

4

3

2

1

6

5

4

3

2

1

GC_PH00241

min. 1.0 1.2 1.4 1.6 1.8 2.0 2.2 2.4 2.6 2.8 3.0


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Glycols, GHB/GBL

Glycols





Inj.: 0.5µL split injectionConc.: 1%Solvent: methanolOven temp.: 100°C to 240°C @ 5°C/min. (hold 5 min.)Inj. temp.: 240°CInj. mode: 100:1 splitInlet liner: 4mm single gooseneck (cat.# 20798)Septa purge: 5.0cc/min.Carrier gas: helium, constant pressurePressure: 12psiLinear velocity: 37cm/sec.Column flow rate: 2.1mL/min.Det.: FID @ 240°CMake-up gas flow: 40cc/min.

GC_EV00474

γ-butyrolactone and γ-butyrolactone-d6

Rxi®-5ms

GC_PH00869

Column: Rxi®-5ms, 30m, 0.25mm ID, 0.25µm (cat.# 13423)Sample: 50µg/mL γ-butyrolactone (GBL) and 25µg/mL

γ-butyrolactone-d6 (GBL-d6) in methanolInj.: 1µL split (1:10), 4mm Siltek® treated single

gooseneck inlet liner (cat.# 20798-214.1)Inj. temp.: 250°CCarrier gas: helium, constant flowFlow rate: 1mL/min.Oven temp.: 40°C (3 min.) to 300°C @ 25°C/min. (hold 5 min.)Det: MSTransfer line

temp.: 280°CScan range: 35-200amuIonization: EIMode: scan

1. GBL-d6 (m/z 92)2. GBL (m/z 86)

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Rxi® Technology!


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GHB/GBL

γ-butyrolactone & 1,4-butanediol


Columns: Rtx®-BAC1, 30m, 0.32mm ID, 1.8µm (cat.# 18003) Rtx®-BAC2, 30m, 0.32mm ID, 1.2µm (cat.# 18002)

Sample: 100µg/mL each in methanol Inj.: 1.0µL split (split ratio 1:10), 4mm single gooseneck

inlet liner with wool (cat.# 22405)Inj. temp.: 240°CCarrier gas: helium, constant flow Flow rate: 3.0mL/min.Oven temp.: 50°C to 240°C @ 10°C/min. (hold 2 min.)Det.: FID @ 240°C

1. 2,3-butanediol2. 1,2-butanediol3. 1,3-butanediol4. 1,4-butanediol5. γ-butyrolactone

GC_PH00808 GC_PH00809


γ-hydroxybutyrate (GHB) and γ-butyrolactone (GBL)

Rtx®-BAC1 and Rtx®-BAC2 (dual column analysis)

GC_PH00870 GC_PH00871

Columns: Rtx®-BAC1, 30m, 0.32mm ID, 1.8µm (cat.# 18003) and Rtx®-BAC2, 30m, 0.32mm ID, 1.2µm (cat.# 18002), connected via universal “Y” Press-Tight® connector (cat.# 20405)

Sample: GHB, GBL, α-methylene-γ-butyrolactone (AMGBL), 10µg/mL each in waterInj.: 1.0mL headspace, split (split ratio 1:10), 1mm split inlet liner (cat.# 20972)Inj. temp.: 200°CCarrier gas: helium, constant pressureLinear velocity: 44cm/sec. @ 50°COven temp.: 50°C (3 min.) to 150°C @ 20°C/min. (hold 7 min.)Det: FID @ 240°CHeadspace autosampler: Teledyne/Tekmar HT3Sample/platen temp.: 100°CSample equilibration: 15 min.Mixing time: 5 min.Vial pressure: 10psigVial pressurization

time: 2 min.Loop fill time: 2 min.Transfer line temp.: 120°C

1. γ-hydroxybutyrate (GHB)/γ-butyrolactone (GBL)2. α-methylene-γ-butyrolactone (AMGBL)

Rtx®-BAC1 Rtx®-BAC2 Sharp peaks and baseline

resolution in less than 5 minutes—

12 samples per hour!


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Abused Inhalants

Abused Inhalants



Oven temp.: 40°C (hold 4 min.) to 120°C @ 10°C/min.Carrier gas: heliumLinear velocity: 50cm/sec.Det.: FIDSample: 250µL headspaceTransfer line temp.: 125°CSample loop temp.: 125°CVial temp.: 70°C

min. 1 2 3 4 5 6 7 8 9 10 11

1

Rtx®-BAC1

2

3

4

5

6

7

8

9

10/11

12

13

14

15

1. methanol2. ethanol3. diethyl ether4. isopropanol5. methylene chloride6. acetone7. methyl tert-butyl ether8. hexane9. chloroform

10. ethyl acetate11. methyl ethyl ketone12. benzene13. trichloroethylene14. toluene15. methyl isobutyl ketone

Acknowledgement: Analyses performed using a Tekmar 7000 Headspace Autosampler on loan courtesy of Tekmar-Dohrmann.

GC_PH00446

1

2

3

4

5

6

7

8

9,11

10

12

13

14

15

Rtx®-BAC2

min. 1 2 3 4 5 6 7 8 9 10 11


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Alkyl Nitrates, Anesthetics

1. tert-butyl nitrite2. iso-butyl nitrite3. sec-butyl nitrite4. n-butyl nitrite5. iso-amyl nitrite

5

43

2

1

min. 2 64

1

5

43

2

Rtx®-BAC1

Rtx®-BAC2

8 10Columns: Rtx®-BAC1, 30m, 0.53mm ID, 3.0µm (cat.# 18001)

Rtx®-BAC2, 30m, 0.53mm ID, 2.0µm (cat.# 18000)Sample: 1.0mL headspace sampleOven temp.: 40°C (hold 5 min.) to 240°C @ 5°C/min.Inj./det. temp.: 240°CCarrier gas: heliumLinear velocity: 65cm/sec.

1. tert-butyl alcohol2. iso-butyl alcohol3. sec-butyl alcohol4. n-butyl alcohol5. iso-amyl alcohol

min. 2 64 8 10

54

3

2

1

54

3

2

1

Alkyl Nitrites


GC_PH00790

abused inhalants

metabolites in blood

1. isoflurane2. enflurane3. halothane4. methoxyflurane

Sample: 1.0mL headspace sample Oven temp.: 40°C (hold 5 min.) to 240°C @ 5°C/min.Inj./det. temp.: 240°CCarrier gas: heliumLinear velocity: 65cm/sec.

Anesthetics

Rtx®-BAC1 & Rtx®-BAC2(headspace analysis)

GC_PH00501 GC_PH00502



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Solvents, Cocaine

Sample: 1.0mL headspace sample Oven temp.: 40°C (hold 5 min.) to 240°C @ 5°C/min.Inj./det. temp.: 240°CCarrier gas: heliumLinear velocity: 65cm/sec.Det.: FID

1. ethyl chloride2. diethyl ether3. methylene chloride4. acetonitrile5. methyl tert-butyl ether6. chloroform7. methyl ethyl ketone8. 1,1,1-trichloroethane9. benzene

10. trichloroethylene11. toluene12. 1,1,2-trichloroethane13. tetrachloroethene14. p-xylene15. m-xylene16. o-xylene17. tetrachloroethane

Solvents

Rtx®-BAC1 & Rtx®-BAC2(headspace analysis)


GC_PH00509 GC_PH00510

Cocaine & Cocaine Adulterants

Rtx®-440

GC_PH00770

Column: Rtx®-440, 30m, 0.25mm ID, 0.50µm (cat.# 12938)Sample: 100µg/mL each compound in methanolInj.: 1.0µL split (split ratio 1:10), laminar cup splitter inlet liner (cat.# 20801)Inj. temp.: 250°CCarrier gas: helium, constant flowFlow rate: 1mL/min.Oven temp.: 150°C to 275°C @ 25°C/min., to 300°C @ 15°C/min. (hold 5.0 min.)Det.: MSTransfer line


1. benzocaine2. phenacetin3. prilocaine4. lidocaine5. caffeine6. procaine7. cocaine8. tetracaine Chromatogram

Search ToolSearch by compound name, synonym,

CAS # or keyword



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Cocaine, Opiates

Cocaine & Metabolites (TMS Derivatives)

Rtx®-5

min. 2 4 6 8 10 12 14 16

GC_PH00254

5

34

Column: Rtx®-5, 30m, 0.25mm ID, 0.25µm (cat.# 10223)Sample: 1.0µL split injection of cocaine and cocaine metabolitesOven temp.: 150°C to 320°C @ 10°C/min.Inj./det. temp.: 250°C/300°CCarrier gas: heliumLinear velocity: 30cm/sec. set @ 50°CFID sensitivity: 2.56 x 10-10 AFSSplit ratio: 30:1

1. ecgonine methyl ester (TMSI)2. ecgonine (TMSI)3. cocaine4. coca ethylene5. benzoylecgonine (TMSI)2

1

Opiates (TMS Derivatives)

Rtx®-5

1 2 3

4

5

6

7,8

9 10

11

min. 4 5 6 7 8 9 10 11 12

GC_PH00233

1. meperidine2. alphaprodine3. methadone4. levorphanol (TMS)5. codeine (TMS)6. hydrocodone7. morphine (TMS)8. hydromorphone (TMS)9. oxycodone (TMS)

10. oxymorphone (TMS)11. nalorphine (TMS)

Column: Rtx®-5, 30m, 0.25mm ID, 0.25µm (cat.# 10223)Sample: 2.0µL split injection of opiatesConc: 2,000ng/µLOven temp.: 200°C to 325°C @ 7°C/min.Inj./det. temp.: 250°C/300°CDet. type: MSIonization: EICarrier gas: heliumMode: full scanLinear velocity: 30cm/sec. set @ 200°CSplit ratio: 50:1

Cocaine and Metabolites (TMS Derivatives)

Rxi®-5Sil MS (100 ng/mL)

CCoolluummnn Rxi®-5Sil MS, 30 m, 0.25 mm ID, 0.25 µm (cat.# 13623)SSaammpplleeDiluent: Butyl chlorideConc.: 100 ng/mLIInnjjeeccttiioonnInj. Vol.: 1 µL splitless (hold 1 min.)Liner: Single Gooseneck w/Wool (cat.# 22286-200.1)Inj. Temp.: 250 °CPurge Flow: 20 mL/min.OOvveennOven Temp: 100 °C to 200 °C at 30 °C/min. to 300 °C at 15 °C/min.CCaarrrriieerr GGaass He, constant linear velocityLinear Velocity: 40 cm/sec., 12.5 psi, 86.2kPa @ 100 °CDDeetteeccttoorr MSMode: SIMTransfer LineTemp.: 310 °CSource Temp.: 250 °CSolvent DelayTime: 4 min.Tune Type: PFTBAIonization Mode: EIIInnssttrruummeenntt Shimadzu 2010 GC & QP2010+ MSNNootteess Samples were prepared as follows:

Standards brought to dryness under nitrogen, then 50 µL BSTFA + 1%TMCS (cat.# 35606) added. 50 µL pyridine was then added, and samples were incubated at 70°C for 30 min. After incubation, samples were diluted with butyl chloride.* Used as derivitazation check

GC_CF1149

NEW!

PPeeaakkss mm//zz 11 mm//zz 22 mm//zz 331. Ecgonine methyl ester 82 96 2562. Ecgonine 82 96 3563. Cocaine 82 182 3034. Cocaethylene 82 196 3175. Benzoylecgonine 82 96 3466. Cannabinol* 409 — —


Sympathomimetic Amines (Basic Drugs) (Underivatized)

Rtx®-5 Amine

1

2

34

5

6

7 8

9

10

11,12

13

14

15

16

17

18

19

21

22

1. phenylethylamine2. amphetamine3. phentermine4. methamphetamine5. fenfluramine6. mephentermine7. cathinone8. phenylpropanolamine9. methcathinone

10. nicotine11. ephedrine12. pseudoephedrine13. phenmetrazine14. phendimetrazine15. methylenedioxyamphetamine16. diethylpropion17. methylenedioxymethamphetamine18. methylenedioxyethylamphetamine19. 4-methyl-2,5-dimethoxyamphetamine20. phenylephrine21. caffeine22. benzphetamine

Column: Rtx®-5 Amine, 30m, 0.25mm ID, 0.50µm (cat.# 12338)Instrument: Varian 3400 GC coupled with Varian Saturn 2000 MS detectorInj.: 1µL, split, split vent flow rate 45mL/min.Inj. temp.: 250°CCarrier gas: heliumDet.: mass spectroscopy data collected using a scan range of 40 amu through 600 amu.Oven temp.: 100°C to 310°C @ 10°C/min.

Ionization performed in the EI Auto mode.

min. 5 7.5 10 12.5 15 17.5 20GC_PH00438

Sympathomimetic Amines (Basic Drugs) (HFBA Derivatized)

Rtx®-200

min. 5 7.5 10 12.5 15 17.5

1014

3

1,2

16

4

8

11

9

7

5

12

13

22

15,20

19 17

18

21

Column: Rtx®-200, 30m, 0.25mm ID, 0.50µm (cat.# 15038)Instrument: Varian 3400 GC coupled with Varian Saturn 2000 MS detectorInj.: 1µL, split, split vent flow rate 45mL/min.Inj. temp.: 250°CCarrier gas: heliumDet.: mass spectroscopy data collected using a scan range of 40 amu through 600 amu.Oven temp.: 100°C to 310°C @ 10°C/min.

Ionization performed in the EI Auto mode.

GC_PH00439

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GC CHROMATOGRAMS | FORENSIC/PHARMACEUTICAL

Sympathomimetic Amines

675-700_GCappPharm.qxp 11/22/2010 9:30 PM Page 676

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Opiates, Cannabinoids

Derivatized Cannabinoids (5 μg/mL)

Rxi®-5Sil MS

CCoolluummnn Rxi®-5Sil MS, 30 m, 0.25 mm ID, 0.25 µm (cat.# 13623)SSaammpplleeDiluent: Ethyl acetateConc.: 5 µg/mL TMS derivativesIInnjjeeccttiioonnInj. Vol.: 1 µL splitless (hold 1 min.)Liner: 3.5mm Gooseneck Splitless w/Wool (cat.# 22286-200.1)Inj. Temp.: 250 °CPurge Flow: 21.4 mL/min.OOvveennOven Temp: 150 °C to 330 °C at 15 °C/min. (hold 3 min.)Carrier Gas He, constant linear velocityLinear Velocity: 40 cm/sec., 13.8 psi, 95.1kPa @ 150 °CDDeetteeccttoorr MSMode: ScanTransfer LineTemp.: 280 °CAnalyzer Type: QuadrupoleSource Temp.: 200 °CElectron Energy: 70 eVSolvent DelayTime: 4 min.Tune Type: PFTBAIonization Mode: EIScan Range: 200-500 amuScan Rate: 5 scans/sec.IInnssttrruummeenntt Shimadzu 2010 GC & QP2010+ MS

GC_CF1145

Excellent peak shape

with short run time.

NEW!

PPeeaakkss1. Cannabidiol2. delta 9 THC3. Cannabinol4. THC-COOH; THCA

GC_CF1150

Extracted Opiates from Blood

Rxi®-5Sil MSPPeeaakkss

1. Hydrocodone2. Codeine3. Oxycodone4. Hydromorphone5. 6-Monoacetylmorphine6. Morphine* Matrix

CCoolluummnn Rxi®-5Sil MS, 30 m, 0.25 mm ID, 0.25 µm (cat.# 13623)SSaammpplleeDiluent: Ethyl acetateConc.: 100 ng/mL propionic anhydride derivativesIInnjjeeccttiioonnInj. Vol.: 1 µL splitless (hold 1 min.)Liner: Gooseneck Splitless (4mm) w/Wool (cat.# 22405)Inj. Temp.: 250 °CPurge Flow: 100 mL/min.OOvveennOven Temp: 65 °C (hold 1 min.) to 315 °C at 15 °C/min.CCaarrrriieerr GGaass He, constant flowFlow Rate: 1 mL/min.Linear Velocity: 35 cm/sec. @ 65 °CDDeetteeccttoorr MSMode: SIMTransfer LineTemp.: 250 °CAnalyzer Type: QuadrupoleSolvent DelayTime: 7 min.Tune Type: PFTBAIonization Mode: EINNootteess Opiates were spiked into a blood sample and extracted

by SPE, then derivatized with propionic anhydride.AAcckknnoowwlleeddggeemmeenntt Data courtesy of Miami Dade County

Medical Examiner Department

NEW!




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Column: Rtx®-35 Amine, 30m, 0.25mm ID, 0.50µm (cat.# 11338)

Sample: 1.0µL split injection of underivatized sympathomimetic amines

Conc. 1000ng/µLInj. temp: 250°CCarrier gas: heliumLinear velocity: 30cm/sec.Oven temp.: 150°C to 240°C @ 7°C/min.Det.: MSDScan range: 40–450amuIonization: EIMode: scan

Sympathomimetic Amines (Basic Drugs) (Underivatized)

Rtx®-35 Amine

GC_PH00574

1. amphetamine2. methamphetamine3. N-ethylamphetamine4. p-methoxyamphetamine (PMA)5. p-methoxymethamphetamine (PMMA)6. methylenedioxyamphetamine (MDA)7. methylenedioxymethamphetamine (MDMA)8. methylenedioxyethylamphetamine (MDEA)9. HMMA

10. MBDB

Derivatized Amphetamines (500 ng/mL)

Rxi®-5Sil MS

PPeeaakkss1. Amphetamine2. Methamphetamine3. MDA4. MDMA5. MDEA

C-contaminant

CCoolluummnn Rxi®-5Sil MS, 30 m, 0.25 mm ID, 0.25 µm (cat.# 13623)SSaammpplleeDiluent: Butyl chlorideConc.: 500 ng/mL HFAA derivativesIInnjjeeccttiioonnInj. Vol.: 1 µL splitless (hold 1 min.)Liner: 3.5mm Gooseneck Splitless w/Wool

(cat.# 22286-200.1)Inj. Temp.: 250 °CPurge Flow: 28 mL/min.OOvveennOven Temp: 75 °C to 300 °C at 15 °C/min.Carrier Gas He, constant linear velocityLinear Velocity: 45 cm/sec., 13.5 psi, 93.1kPa @ 75 °CDDeetteeccttoorr MSMode: ScanTransfer LineTemp.: 250 °CAnalyzer Type: QuadrupoleSource Temp.: 200 °CElectron Energy: 70 eVSolvent DelayTime: 4 min.Tune Type: PFTBAIonization Mode: EIScan Range: 40-300 amuScan Rate: 5 scans/sec.IInnssttrruummeenntt Shimadzu 2010 GC & QP2010+ MS

GC_CF1144

NEW!


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Sympathomimetic Amines (Basic Drugs) (TFAA Derivatives)

Rtx®-5

109

8

7

6

5

4

1

2,3

min. 4 6 8 10 12 14 16 18GC_PH00251

1. amphetamine - TFAA2. phentermine - TFAA3. phenylpropanolamine - TFAA4. ephedrine - TFAA5. methamphetamine - TFAA6. fenfluramine - TFAA7. pseudoephedrine - TFAA8. methylenedioxyamphetamine - TFAA9. methylenedioxymethamphetamine - TFAA

10. methylphenidate - TFAA

Column: Rtx®-5, 30m, 0.25mm ID, 0.25µm (cat.# 10223)Sample: 1.0µL splitless injection of derivatized sympathomimetic aminesConc.: approximately 2.5ng/µLOven temp.: 40°C (hold 1 min.) to 150°C @ 30°C/min.,

to 300°C @ 5°C/min.Inj. temp.: 225°CInterface temp.: 275°CDet.: MSDIonization: EICarrier gas: heliumLinear velocity: 20cm/sec. set @ 100°CSplitless hold time: 1 min.

Sympathomimetic Amines (Basic Drugs) (HFBA Derivatives)

Rtx®-5

1

2

3

4

5

6

7

8

9

10

min. 4 6 8 10 12 14 16 18GC_PH00252

1. amphetamine - HFBA2. phentermine - HFBA3. phenylpropanolamine - HFBA4. ephedrine - HFBA5. methamphetamine - HFBA6. fenfluramine - HFBA7. pseudoephedrine - HFBA8. methylenedioxyamphetamine - HFBA9. methylenedioxymethamphetamine - HFBA

10. methylphenidate - HFBA

Column: Rtx®-5, 30m, 0.25mm ID, 0.25µm (cat.# 10223)Sample: 1.0µL splitless injection of sympathomimetic aminesConc.: approximately 2.5ng/µL.Oven temp.: 40°C (hold 1 min.) to 150°C @ 30°C/min.,

to 300°C @ 5°C/min.Inj. temp.: 225°CInterface temp.: 275°CDet.: MSDIonization: EICarrier gas: heliumLinear velocity: 20cm/sec. set @ 100°CSplitless hold time: 1 min.


678 www.restek.com 800-356-1688 or 814-353-1300


Barbiturates

6 75

Column: Rtx®-35, 30m, 0.53mm ID, 1.0µm (cat.# 10455)Sample: 1.0µL splitless injection of acidic/neutral drugsConc.: 50µg/mLOven temp.: 100°C to 280°C @ 10°C/min. (hold 5 min.)Inj./det. temp.: 250°CCarrier gas: heliumLinear velocity: 40cm/sec. set @ 100°CFID sensitivity: 5.12 x 10-10 AFSSplitless hold time: 0.5 min.

Barbiturates (Acidic/Neutral Drugs) (Underivatized)

Rtx®-35

1

2

3

4

8

9

11

10 12

13

16

15

14

min. 0 5 10 15 20GC_PH00262

1. ethosuximide2. barbital3. methyprylon4. aprobarbital5. butalbital6. amobarbital7. pentobarbital8. secobarbital9. meprobamate

10. carisoprodal11. glutethimide12. phenobarbital13. methaqualone14. primidone15. carbamazepine16. diphenylhydantoin

Column: Rtx®-1701, 15m, 0.53mm ID, 0.50µm (cat.# 12037)Sample: 1.0µL splitless injection of acidic/neutral drugsConc.: 50µg/mL concentrationOven temp.: 100°C to 280°C @ 7°C/min.Inj./det. temp.: 250°C/275°CCarrier gas: heliumLinear velocity: 40cm/sec. set @ 100°CFID sensitivity: 5.12 x 10-10 AFSSplitless hold time: 0.5 min.

6 7

Barbiturates (Acidic/Neutral Drugs) (Underivatized)

Rtx®-1701

1 3

2

45

8

11

9

15

1012

13

14

16

min. 0 5 10 15 20GC_PH00263


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Barbiturates, Acidic/Neutral Drugs

Barbiturates (Acidic/Neutral Drugs) (Underivatized )

Rtx®-35

Column: Rtx®-35, 30m, 0.32mm ID, 0.50µm (cat.# 10439)Sample: 1.0µL split injection of barbituratesOven temp.: 210°C (hold 2 min.) to 300°C @ 7°C/min. (hold 2 min.)Inj./det. temp.: 300°CCarrier gas: heliumLinear velocity: 35cm/sec. set @ 210°CFID sensitivity: 5.12 x 10-10 AFSSplit vent: 30:1

1. barbital2. aprobarbital3. butalbital4. amobarbital5. talbutal6. pentobarbital7. methohexital8. secobarbital9. thiopental

10. hexobarbital11. mephobarbital12. phenobarbital

GC_PH00267

12

11

10

9

8

7

6

4

5

1 2

3

min. 2 4 6 8 10

Separation optimized

using Pro ezGC

software!See page 580 for details.

Acidic/Neutral Drugs

Rxi®-5ms

Column: Rxi®-5ms, 30m, 0.25mm ID, 0.25µm (cat.# 13423)Sample: 1,000µg/mL each in methanolInj.: 1.0µL split (50:1), 20ng each compound on column;

Siltek® treated 4mm gooseneck splitless inlet liner (cat.# 20799-214.5)

Inj. temp.: 250°CCarrier gas: heliumLinear velocity: 30cm/sec., constant pressureOven temp.: 100°C to 220°C @ 15°C/min., to 330°C @

10°C/min. (hold 5 min.)Det.: Agilent 5973 MSDTransfer line

temp.: 300°CScan range: 35-550Tune: PFTBAIonization: EI

1. methprylon2. butalbital3. amobarbital4. meprobamate5. glutethimide6. phenobarbital7. methaqualone8. primidone

GC_PH00815




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Basic Drugs

7

Column: Rtx®-200, 30m, 0.25mm ID, 0.25µm (cat.# 15023)Sample: 1.0µL split injection of a basic drug sample (1mg/mL)Conc.: 1,000ng/µLOven temp.: 100°C to 325°C @ 4°C/min. (hold 10 min.)Inj./det. temp.: 250°C/320°CCarrier gas: heliumLinear velocity: 30cm/sec. set @ 100°CFID sensitivity: 1.28 x 10-10 AFSSplit ratio: 50:1

1

2

4

6

8

10

11

3,5

14

19

17

18

22

23

21

20,25

2430

28,29

27

37

34

33 3638

35

31,32

26

16

15

13

12

9

min. 10 20 30 40 50 60

GC_PH00237

Basic Drugs (Underivatized)

Rtx®-200 1. nicotine2. benzocaine3. cotinine4. meperidine5. caffeine6. benzphetamine7. ketamine8. diphenhydramine9. lidocaine

10. phenyltoloxamine11. tripelennamine12. phenothiazine13. dextromethorphan14. methadone15. amitriptyline16. trimipramine17. tetracaine18. pyrilamine19. medazepam20. bupivacaine21. scopolamine22. codeine23. morphine24. diazepam25. chlorpromazine26. temazepam27. flunitrazepam28. bromazepam29. prazepam30. acetopromazine31. flurazepam32. papaverine33. clonazepam34. haloperidol35. alprazolam36. triazolam37. thioridazine38. trazodone

Basic Drugs (Underivatized)

Rxi®-5ms

Column: Rxi®-5ms, 30m, 0.25mm ID, 0.25µm (cat.# 13423)Sample: 1,000µg/mL each in methanolInj.: 1.0µL split (50:1), 20ng each compound on column; Siltek® treated

4mm gooseneck splitless inlet liner (cat.# 20799-214.5)Inj. temp.: 250°CCarrier gas: heliumLinear velocity: 30cm/sec., constant pressureOven temp.: 100°C to 220°C @ 15°C/min., to 330°C @ 10°C/min. (hold 5 min.)Det.: Agilent 5973 MSDTransfer line

temp.: 300°CScan range: 35-550Tune: PFTBAIonization: EI

1. amphetamine2. methamphetamine3. nicotine4. cotinine5. caffeine6. benzphetamine7. ketamine8. phencyclidine9. methadone

10. cocaine11. codeine12. scopolamine13. alprazolam

GC_PH00814




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Basic Drugs

1. nicotine2. benzocaine3. cotinine4. meperidine5. caffeine6. benzphetamine7. ketamine8. diphenhydramine9. lidocaine

10. phenyltoloxamine11. tripelennamine12. phenothiazine13. dextromethorphan14. methadone15. amitriptyline16. trimipramine17. tetracaine18. pyrilamine19. medazepam20. bupivacaine21. scopolamine22. codeine23. morphine24. diazepam25. chlorpromazine26. temazepam27. flunitrazepam28. bromazepam29. prazepam30. acetopromazine31. flurazepam32. papaverine33. clonazepam34. haloperidol35. alprazolam36. triazolam37. thioridazine38. trazodone

min. 10 20 30 40 50 60

1

2

3

4

5

6

7

8

9

10

11

12

13

14

15

2120

22

24

25

26

28

27

29

30

31

32

23

33

35

36

37

34

1617

18

19

GC_PH00235

Column: Rtx®-5, 30m, 0.25mm ID, 0.25µm (cat.# 10223)Sample: 1.0µL split injection of a basic drug sampleConc.: 1,000ng/µLOven temp.: 100°C to 325°C @ 4°C/min. (hold 10 min.)Inj./det. temp.: 250°C/320°CCarrier gas: heliumLinear velocity: 30cm/sec. set @ 100°CFID sensitivity: 1.28 x 10-10 AFSSplit ratio: 50:1

38

Basic Drugs (Underivatized )

Rtx®-5

Basic Drugs (Underivatized )

Rtx®-35

min. 10 20 30 40 50 60

1

2

3

4

6

8

9

107

5

11

3836

3735

33

3432

30

27

29

2326

24

25

22

21

19

18,20

1514

12 17

16

13

GC_PH00236

Column: Rtx®-35, 30m, 0.25mm ID, 0.25µm (cat.# 10423)Sample: 1.0µL split injection of a basic drug sampleConc.: 1,000ng/µLOven temp.: 100°C to 325°C @ 4°C/min.

(hold 10 min.)Inj./det. temp.: 250°C/320°CCarrier gas: heliumLinear velocity: 30cm/sec. set @ 100°CFID sensitivity: 1.28 x 10-10 AFSSplit ratio: 50:1

3128


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Benzodiazepines, Phenothiazines

Phenothiazines (Basic Drugs) (Underivatized)

Rtx®-5

1

9

87

5,64

3

2

Column: Rtx®-5, 15m, 0.32mm ID, 0.50µm (cat.# 10236)Sample: 1.0µL split injection of phenothiazinesConc.: 2,000ng/µLOven temp.: 200°C to 325°C @ 5°C/min.Inj./det. temp.: 250°C/315°CCarrier gas: heliumLinear velocity: 25cm/sec. set @ 200°CFID sensitivity: 2.56 x 10-10 AFSSplit ratio: 30:1

min. 5 10 15 20 25

10

GC_PH00269

1. phenothiazine2. promethazine3. trimeprazine4. promazine5. chlorprothixene6. chlorpromazine7. trifluoperazine8. acetopromazine9. prochlorperazine

10. thioridazine

Separation optimized

using Pro ezGC

software!

min. 2 4 6 8 10

1

2

3

4

5,6

7

89

10

11

12

13

Column: Rtx®-200, 15m, 0.32mm ID, 0.25µm (cat.# 15021)Sample: 1.0µL split injection of benzodiazepinesConc.: 15ng/componentOven temp.: 225°C to 325°C @ 8°C/min.Inj./det. temp.: 250°C/320°CCarrier gas: heliumLinear velocity: 35cm/sec. set @ 225°CFID sensitivity: 5.12 x 10-10 AFSSplit ratio: 60:1

GC_PH00268

Benzodiazepines (Basic Drugs) (Underivatized)

Rtx®-2001. medazepam2. lorazepam3. diazepam4. desmethyl diazepam5. bromazepam6. prazepam7. temazepam8. flurazepam9. clobazam

10. flunitrazepam11. clonazepam12. alprazolam13. triazolam

Benzodiazepines (15 μg/mL)

Rxi®-5Sil MS

PPeeaakkss1. Oxazepam2. Lorazepam3. Diazepam4. Flunitrazepam5. Prazepam6. Clonazepam7. Alprazolam

CCoolluummnn Rxi®-5Sil MS, 30 m, 0.25 mm ID, 0.25 µm (cat.# 13623)SSaammpplleeDiluent: Butyl chlorideConc.: 15 µg/mLIInnjjeeccttiioonnInj. Vol.: 1 µL splitless (hold 1 min.)Liner: 3.5mm Gooseneck Splitless w/Wool (cat.# 22286-200.1)Inj. Temp.: 280 °CPurge Flow: 32.2 mL/min. (20:1 split)OOvveennOven Temp: 200 °C to 330 °C at 15 °C/min. (hold 3 min.)CCaarrrriieerr GGaass He, constant linear velocityLinear Velocity: 50 cm/sec., 23.7 psi, 163.4kPa @ 200 °CDDeetteeccttoorr MSMode: ScanTransfer LineTemp.: 280 °CAnalyzer Type: QuadrupoleSource Temp.: 200 °CElectron Energy: 70 eVSolvent DelayTime: 4 min.Tune Type: PFTBAIonization Mode: EIScan Range: 50-350 amuScan Rate: 5 scans/sec.IInnssttrruummeenntt Shimadzu 2010 GC & QP2010+ MSGC_CF1148

Good peak shape

with a fast elution

time of <8 min.

NEW!


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Cold Medications

1. phenylpropanolamine2. phenylephrine3. guaifenesin4. pheniramine5. phenyltoloxamine6. chlorpheniramine7. brompheniramine8. dextromethorphan9. pyrilamine

10. codeine11. hydrocodone

Column: Rtx®-5 Amine, 30m, 0.53mm ID, 1.0µm (cat.# 12355)Oven temp.: 175°C to 280°C @ 10°/min. (hold 5.5 min.)Inj./det. temp.: 250°C/280°CCarrier gas: heliumLinear velocity: 40cm/sec.Sample size: 1µLSplit vent flow: 88mL/min.Split ratio: 20:1

1

2

3

4

5

6

7

8

9

10

11

min. 2 4 6 8 10 12 14 16

Cold Medications (Basic Drugs) (Underivatized)

Rtx®-5 Amine

GC_PH00469

Column: Rtx®-35 Amine, 30m, 0.25mm ID, 0.50µm (cat.# 11338)Sample: 1.0µL split injection of underivatized cold medicinesConc.: 1,000ng/µLInj. temp: 250°CCarrier gas: heliumLinear velocity: 30cm/sec.Oven temp.: 250°C to 300°C @ 7°C/min. (hold 7 min.)Det.: MSDScan range: 40–450amuIonization: EIMode: scan

Cold Medications (Basic Drugs) (Underivatized)

Rtx®-35 Amine

1. guaifenesin2. pheniramine3. phenyltoloxamine4. chlorpheniramine5. brompheniramine6. dextromethorphan7. pyrilamine8. triprolidine9. codeine

10. hydrocodone

GC_PH00575


684 www.restek.com 800-356-1688 or 814-353-1300

GC CHROMATOGRAMS | PHARMACEUTICAL

Pesticides in Dietary Supplements

dSPE vs. cSPE Sample Cleanup of Dandelion Root Powder (Dietary Supplement)

Rxi®-5Sil MS

GC_FF1171

CCoolluummnn Rxi®-5Sil MS, 30 m, 0.25 mm ID, 0.25 µm (cat.# 13623)SSaammppllee Dandelion Root powder spiked with 46 pesticides

QuEChERS Internal Standard Mix for GC/MS Analysis (cat.# 33267)anthracene for quality control (cat.# 33264)

Conc.: 80 pg/µLIInnjjeeccttiioonnInj. Vol.: 1 µL splitless (hold 1.5 min.)Liner: 5mm Splitless with wool (cat.# 22975-200.1)Inj. Temp.: 250 °COOvveennOven Temp: 90 °C (hold 1.5 min.) to 340 °C at 8 °C/min.CCaarrrriieerr GGaass He, constant flowFlow Rate: 1.5 mL/min.DDeetteeccttoorr MSMode:Analyzer Type: TOFSource Temp.: 225 °CElectron Energy: 70 eVIonization Mode: EIAcquisition Range: 45-550 amuAcquisition Rate: 5 spectra/sec.IInnssttrruummeenntt LECO Pegasus 4D GCxGC-TOFMSNNootteess Sample Preparation:

Wetting: 1 g of Dandelion Root powder combined with 9 mL of water, shaken well, fortified with pesticides and QuEChERS Internal Standard Mix for GC/MS Analysis (cat.# 33267), soak for 2 hours.

Extraction: 10 mL acetonitrile added then addition of Q-sep™ Q110 (cat.# 26235), centrifuge with Q-sep™ 3000 Centrifuge (cat.# 26230).

dSPE: cleanup procedure according to EN 15662 method, add control standard anthracene (cat.# 33264) to 1 mL extract, add this to Q-sep™ Q110 dSPE tube (cat.# 26235), shake, centrifuge.

cSPE: add control standard anthracene (cat.# 33264) to 1 mL extract, add magnesium sulfate to cartridge, use 6mL Combo SPE Cartridge containing 500mg CarboPrep® 90/500mg PSA (cat.# 26194), concentrate via evaporation.

NEW!

free literatureDeveloping New Methods for Pesticides in Dietary Supplements

Advantages of the QuEChERS Approach

QuEChERS is a simple, effective approach to sample prep that can be applied to the analysisof pesticides in dietary supplements. Here we demonstrate a QuEChERS, cSPE, GC-TOFMSprocedure that results in good recoveries for a wide range of pesticides in dandelion root.

Download your copy from www.restek.com

Applications Notelit. cat.# PHAN1242


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Pesticides in Dietary Supplements

Dietary Supplement (Finished Product) QuEChERS Extract Cleaned with Cartridge SPE

(GCxGC-TOFMS Contour Plot)

GC_FF1191

CCoolluummnn Rxi®-5Sil MS 30 m, 0.25 mm ID, 0.25 µm (cat.# 13623)Rtx®-200 1.5 m, 0.18 mm ID, 0.20 µm (cat.# 45001)

SSaammpplleeDiluent: TolueneIInnjjeeccttiioonnInj. Vol.: 1 µL splitless (hold 1 min.)Liner: Gooseneck Splitless (4mm) w/Wool (cat.# 22405)Inj. Temp.: 250 °CPurge Flow: 40 mL/min.OOvveennOven Temp: Rxi®-5Sil MS: 80 °C (hold 1 min.) to 310 °C at 4 °C/min. (hold 1.5 min.)

Rtx®-200: 90 °C (hold 1 min.) to 320 °C at 4 °C/min. (hold 1.5 min.)CCaarrrriieerr GGaass He, constant flowFlow Rate: 1.8 mL/min.MMoodduullaattiioonnModulatorTemp. Offset: 25 °CSecond DimensionSeparation Time: 4 sec.Hot Pulse Time: 1.2 sec.Cool Timebetween Stages: 0.8 sec.DDeetteeccttoorr TOFMSTransferLine Temp.: 290 °CAnalyzer Type: TOFSource Temp.: 225 °CElectron Energy: 70 eVMass Defect: -20 mu/100 uSolvent DelayTime: 4 min.Ionization Mode: EIAcquisition Range: 45 to 550 amuSpectralAcquisition Rate: 100 spectra/secIInnssttrruummeenntt LECO Pegasus 4D GCxGC-TOFMSNNootteess See application note PHAN1251 for extraction and cleanup details. A 1.5 m length of the Rtx®-200 column was trimmed from a

10 m column. Columns were connected with a Universal Press-Tight® Connector (cat.# 20429).

GCxGC with orthogonal Rxi®-5Sil MS and Rtx®-200 columns is a powerful

way to handle complex samples like dietary supplement extracts.

NEW!

www.restek.com/dietary

Restek is your complete source for analyzing pesticides in dietary supplements.


686 www.restek.com 800-356-1688 or 814-353-1300


Chiral Analyses

Amphetamine and Methamphetamine (TFAA Derivatives)

Rt®-βDEXcst

min. 10 12 14 16 18 20 22 24


Oven temp.: 120°C (hold 1 min.) to 175°C @ 1.5°C/min.

Carrier gas: heliumLinear velocity: 25cm/sec. set @ 120°C Det.: MSD @ 220°C

GC_PH00246

1. (+)methamphetamine - TFAA2. (-)methamphetamine - TFAA3. (+)amphetamine - TFAA4. (-)amphetamine - TFAA

1

2

3 4

Fenfluramine (TFAA Derivative)

Rt®-βDEXcst

min. 15 20 25 30 35 40


Inj.: on-column, 25ng/enantiomerOven temp.: 90°C (hold 1 min.) to 200°C

@ 2°C/min. (hold 3 min.)Carrier gas: hydrogenLinear velocity: 80cm/sec. set @ 60°CDet.: FID @ 220°C

1. (+)-fenfluramine - TFAA2. (-)-fenfluramine - TFAA3. (+)-norfenfluramine - TFAA4. (-)-norfenfluramine - TFAA

1

2

3

4

GC_PH00244

Barbiturates (Underivatized)

Rt®-βDEXcst

min. 10 20 30 40 50


Inj.: on-column, 25ng/enantiomerOven temp.: 60°C (hold 1 min.) to

220°C @ 3°C/min.Carrier gas: hydrogenLinear velocity: 80cm/sec. set @ 60°CDet.: FID @ 220°C

1. (+/-)-hexobarbital2. (+/-)-mephobarbital

12

GC_PH00245


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Chiral Analyses, Steroids

Column: Rt®-βDEXsm, 30m, 0.32mm ID, 0.25µm (cat.# 13104)

Inj.: on-column, 125ng each enantiomer Oven temp.: 175°C to 200°C @ 2°C/min. Inj./det. temp.: 200°C/230°CCarrier gas: heliumLinear velocity: 60cm/sec.Det.: GC/FID Split ratio: 13:1 using cup splitter inlet liner (cat.# 20709)

min. 7 8

(+/-

)ibup

rofe

n

Ibuprofen (Underivatized)

Rt®-βDEXsm

GC_PH00242


Inj.: on-column, approximately 15ng each enantiomerOven temp.: 200°C to 230°C @ 1°C/min.Inj./det. temp.: 200°C/230°C Carrier gas: hydrogenLinear velocity: 80cm/sec.Detector type: GC/FIDSplit ratio: 13:1 using cup splitter inlet liner (cat.# 20709)

min. 20 25

(+/-

)thal

idom

ide

Thalidomide (Underivatized)

Rt®-βDEXcst

GC_PH00243

6

Column: Rtx®-5, 30m, 0.25mm ID, 0.10µm (cat.# 10208)Sample: 0.5µL split injection of anabolic steroidsConc.: 1,000ng/µLOven temp.: 180°C to 340°C @ 10°C/min. (hold 3 min.)Inj./det. temp.: 280°C/340°CCarrier gas: heliumLinear velocity: 35cm/sec. set @ 180°CFID sensitivity: 1.28 x 10-10 AFSSplit ratio: 50:1

1. 5-androstene-3β,17β-diol2. 17α-methyl-5-androstene-3β,17β-diol3. 5α-androstan-17β-ol-3-one4. 19-nortestosterone5. 17α-methylandrostan-17β-ol-3-one6. mesterolone7. testosterone8. 17α-methyltestosterone9. 1-dehydrotestosterone

10. 1-dehydro-17α-methyltestosterone11. bolasterone12. oxymethalone13. 19-nortestosterone-17-propionate14. testosterone propionate15. fluoxymesterone16. 4-chlorotestosterone-17-acetate17. testosterone-17β-cypionate18. 1-dehydrotestosterone benzoate19. 1-dehydrotestosterone undecylenate

Steroids, Anabolic (Underivatized)

Rtx®-5

1

1918

17

2

3

5

7

8

9

10,11

12

1314

15

164

min. 2 4 6 8 10 12 14 16 18GC_PH00255


688 www.restek.com 800-356-1688 or 814-353-1300


Steroids

Steroids: Sex Hormones

Rxi®-1ms

GC_PH00872

Column: Rxi®-1ms, 30m, 0.25mm ID, 0.25µm (cat.# 13323)Sample: 100µg/mL each hormone in methanol or ethanol; compounds derivatized

using 2% methoxylamine HCl (CH3ONH2) in pyridine, then N-trimethylsilylimidazole (TMSI), then analyzed

Inj.: 1.0µL splitless (hold 0.5 min.), 3.5mm single gooseneck inlet liner (cat.# 20961)

Inj. temp.: 250°CCarrier gas: helium, constant flowFlow rate: 1mL/min.Oven temp.: 100°C to 320°C @ 10°C/min. (hold 10 min.)Det: MS: Shimadzu 17A with QP5000Transfer line


1. androsterone2. dehydroepiandrosterone (DHEA)3. 17-α-estradiol4. estrone5. 17-β-estradiol6. testosterone7. derivatization by-product

Low bleed at 300+°C!

Excellent

resolution of

closely eluting

hormones.





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Potential Genotoxic Impurities (PGIs)

Mesylate, Besylate, and Tosylate Genotoxic Impurities

Rxi®-624Sil MS (extracted ion chromatograms)

GC_PH1165

PPeeaakkss RRTT ((mmiinn..)) IIoonnss MMoonniittoorreedd((mm//zz))

1. Methyl methanesulfonate (MMS) 4.253 79, 80, 952. Isopropyl methanesulfonate (iPMS) 5.043 59, 79, 1233. Diethyl sulfate (DES) 6.010 111, 125, 1394. di-isopropyl sulfate (DPS) 6.357 45, 87, 1675. dibutyl sulfate (DBS) 9.260 29, 41, 566. Methyl benzenesulfonate (MBS) 9.463 77, 141, 1727. Ethyl benzenesulfonate (EBS) 9.883 77, 141, 1868. Methyl toluenesulfonate (MTS) 10.337 91, 155, 1869. Ethyl toluenesulfonate (ETS) 10.713 91, 155, 200

10. n-propyl toluenesulfonate (nPTS) 10.827 91, 155, 17211. n-butyl benzenesulfonate (nBBS) 11.07 77, 141, 15912. isopropyl p-toluenesulfonate (iPTS) 11.240 91, 155, 17213. p-toluenesulfonic acid n-butyl ester (nBTS) 11.823 91, 155, 173

* Ortho isomers of ETS.

CCoolluummnn Rxi®-624Sil MS, 20 m, 0.18 mm ID, 1.00 µm (cat.# 13865)SSaammpplleeDiluent: 90:10 acetonitrile:waterConc.: 500 ng/mLIInnjjeeccttiioonnInj. Vol.: 1 µL splitless (hold 0.5 min.)Liner: 3.5mm Single Gooseneck Liner with wool placed 3cm from top (middle) (cat.# 22286)Inj. Temp.: 220 °CPurge Flow: 3 mL/min.OOvveennOven Temp: 80 °C (hold 2 min.) to 300 °C at 20 °C/min. (hold 5 min.)CCaarrrriieerr GGaass He, constant flowLinear Velocity: 45 cm/sec.DDeetteeccttoorr MSMode: SIMTransfer LineTemp.: 200 °CAnalyzer Type: QuadrupoleSource Temp.: 280 °CSolvent DelayTime: 4 min.IonizationMode: EIIInnssttrruummeenntt Shimadzu 2010 GC & QP2010+ MSAAcckknnoowwlleeddggeemmeenntt In collaboration with Merck and Company

Extracted ions for

MMS and iPMS show

compatibility with

polar injection solvents

using a splitless

injection technique for

higher sensitivity.

Low bleed at 300°C allows for “bake-out”oven programs.

NEW!


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Alkyl Halide Genotoxic Impurities

Rxi®-624Sil MS (High Concentration Injection)

PPeeaakkss RRTT ((mmiinn..)) CCoonncc..((µµgg//mmLL))

1. 2-Chloropropane 2.10 12. Bromoethane 2.36 13. 1-Chloropropane 2.72 14. 2-Bromopropane 3.393 15. Butyl chloride 4.627 16. 1-Bromobutane 5.973 1

CCoolluummnn Rxi®-624Sil MS, 20 m, 0.18 mm ID, 1.00 µm (cat.# 13865)SSaammpplleeDiluent: DMSOConc.: 1 µg/mLIInnjjeeccttiioonnInj. Vol.: 1 µL splitless (hold 0.5 min.)Liner: 3.5mm Single Gooseneck Liner with wool placed 3cm

from top (middle) (cat.# 22286)Inj. Temp.: 220 °CPurge Flow: 3 mL/min.OOvveennOven Temp: 40 °C (hold 3 min.) to 200 °C at 20 °C/min.CCaarrrriieerr GGaass He, constant flowLinear Velocity: 40 cm/sec.DDeetteeccttoorr MSMode: ScanTransfer Line Temp.: 200 °CAnalyzer Type: QuadrupoleSource Temp.: 280 °CSolvent Delay Time: 0.5 min.Ionization Mode: EIScan Range: 30-300 amuScan Rate: 5 scans/sec.IInnssttrruummeenntt Shimadzu 2010 GC & QP2010+ MSNotes: Ions monitored 42, 43, 57, 108 m/z

Good retention for hard-to-retain

polar analytes makes method

development easier!

GC_PH1166

NEW!

1. 1-chloropropane2. bromoethane3. 2-chloropropane4. 1-bromopropane5. 2-bromopropane6. 1-bromobutane7. dimethyl sulfate8. methyl methanesulfonate9. ethyl methanesulfonate

10. isopropyl methanesulfonate11. diethyl sulfate12. di-isopropyl sulfate13. di-n-propyl sulfate14. dibutyl sulfate15. methylbenzene sulfonate16. ethylbenzene sulfonate17. methyl toluenesulfonate18. ethyl toluenesulfonate19. n-butyl benzenesulfonate20. n-propyl toluenesulfonate21. isopropyl toluenesulfonate22. n-butyl toluenesulfonate

*ortho isomer of ethyl toluenesulfonate

Column: Rtx®-200, 30m, 0.25mm ID, 1.0µm (cat.# 15053)Sample: 100µg/mL each compound in 90:10 acetonitrile:waterInj.: 1µL, split (10:1), 4mm single gooseneck inlet liner w/ wool (cat.# 22405)Inj. temp.: 220°CCarrier gas: helium, constant flow Flow rate: 1.0mL/min. Oven temp.: 40°C (hold 8.3 min.) to 70°C @ 70°C/min. to 115°C @ 40°C/min. to

250°C @ 30°C/min. to 300°C @ 15°C/min. (hold 3 min.)Det: MSTransfer line temp.: 280°CScan range: 20-250m/zIonization: EIMode: scan

GC_PH01076


Rtx®-200


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Basic Drugs, Anesthetics

1. amitriptyline2. trimipramine3. imipramine4. nortriptyline5. doxepin6. desipramine7. maprotyline8. clomipramine

1

2

3

4

5

6

78

min. 1 2 3 4 5 6

Antidepressants (Basic Drugs) (Underivatized)

Rtx®-1701

Column: Rtx®-1701, 15m, 0.25mm ID, 0.25µm (cat.# 12020)Sample: 1.0µL split injection of antidepressantsConc.: 25ng/componentOven temp.: 225°CInj./det. temp.: 250°C/260°CCarrier gas: heliumLinear velocity: 30cm/sec. set @ 225°CFID sensitivity: 2.56 x 10-10 AFSSplit ratio: 40:1

GC_PH00264

Underivatized Antihistamines (Basic Drugs)

Rtx®-5 Amine

1. phenylpropanolamine2. ephedrine3. pseudoephedrine4. pheniramine5. diphenhydramine6. doxylamine7. phenyltoloxamine8. methapyrilene9. chlorpheniramine

10. brompheniramine11. triprolidine

Column: Rtx®-5 Amine, 30m, 0.32mm ID, 1.0µm (cat.# 12354)

Sample: 1.0µL split injection of antihistaminesConc.: 1,000ng/µLOven temp.: 130°C (hold 5 min.) to 305°C

@ 10°C/min. (hold 5 min.)Inj./det. temp.: 305°CCarrier gas: hydrogenLinear velocity: 43cm/sec. set @ 130°CFID sensitivity: 6.4 x 10-11 AFSSplit ratio: 50:1

GC_PH00247min. 5 10 15 20 25

1

2

11

10

9

8

7

6

5

4

3

Local Anesthetics

Rxi®-5ms

GC_PH00860

Column: Rxi®-5ms, 30m, 0.53mm ID, 1.00µm (cat.# 13455)Sample: 50µg/mL each component in methanolInj.: 1.0µL split (10:1), 4mm split inlet liner with wool (cat.# 20781)Inj. temp.: 250°CCarrier gas: helium, constant flowFlow rate: 5.0mL/min. Oven temp.: 200°C (hold 4 min.) to 320°C @ 30°C/min. (hold 3 min.)Det.: FID @ 300°C

1. benzocaine2. prilocaine3. lidocaine4. procaine5. tetracaine6. bupivacaine7. dibucaine

Good peak shape for

underivatized basic drugs.




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Antiepileptics

Antiepileptics (Underivatized)

Rtx®-20


Sample: 1.0µL split injection of antiepileptic drugsConc.: 1,000ng/µLOven temp.: 150°C to 280°C @

7°C/min. (hold 5 min.)Inj./det. temp.: 250°C/270°CDet.: FIDCarrier gas: heliumLinear velocity: 30cm/sec. set @ 150°CFID sensitivity: 1.28 x 10-10 AFSSplit ratio: 30:1

1

min. 5 10 15 20

2

3 4

5

6

7 8 9

10

11

12

GC_PH00265

Antiepileptics (Underivatized)

Rtx®-1701

1. valproic acid2. ethosuximide3. methsuximide4. phensuximide5. desmethyl methsuximide6. mephenytoin7. ethotoin8. PEMA9. phenobarbital

10. primidone11. carbamazepine12. diphenylhydantoin


Sample: 1.0µL split injection of antiepileptic drugsConc.: 1,000ng/µLOven temp.: 150°C to 280°C @

7°C/min. (hold 5 min.)Inj./det. temp.: 250°C/270°CDet.: FIDCarrier gas: heliumLinear velocity: 30cm/sec. set @ 150°CFID sensitivity: 1.28 x 10-10 AFSSplit ratio: 30:1

GC_PH00266

1

min. 5 10 15 20

23

4

5

6

7 8

910

11

12


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Organic Volatile Impurities: Retention Time Index

CCoommppoouunndd MMSS iioonn cchhaarr..iioonn 4455((55))77//222200((55))formaldehyde 29 30,31 1.16methanol 31 29,30,33 1.36pentane 43 41,42,72,57,29 1.74ethanol 31 45,46,27 1.76diethylether 59 74,45 1.872-chloropropane 43 73,63,80,27 1.95acetone 43 58,27,39 2.06methylal 45 75,29,31 2.071,1-dichloroethene 61 96,61,63 2.082-propanol 45 43,27,59 2.15ethyl formate 45 31,29,27,74 2.2methyl acetate 43 74,59,29 2.33acetonitrile 41 40,39,38 2.332-methylpentane 43 42,41,71,86 2.48methylene chloride 84 49,86,51,88 2.5methyl tert-buyl ether 73 57,41,43,45 2.7trans-1,2-dichloroethene 61 96,98,63 2.76hexane 57 41,86,43 3.05isopropyl ether 45 43,87,69 3.221-propanol 31 42,59,27 3.22methyl cyclopentane 56 41,69,84 3.76nitromethane 61 46,30 3.832-butanone (MEK) 72 43,57 (use 43) 3.9cis-1,2-dichloroethene 96 96,61,98 3.96ethyl acetate 43 61,70 42-butanol 45 59,31 4.21tetrahydrofuran 42 72,71,41 (use 72) 4.34chloroform 83 83,85,47,87,118 4.511,1,1-trichloroethane 97 97,99,61 4.762,2-dimethoxypropane 73 89,43,42,31 4.81cyclohexane 56 84,41,27 4.88carbon tetrachloride 117 117,119 5.04isobutyl alcohol 42 43,31,41,33 5.312-methoxyethanol 45 47,76 5.311,2-dimethoxyethane 45 60,58,90 5.41benzene 78 78 5.41

CCoommppoouunndd MMSS iioonn cchhaarr..iioonn 4455((55))77//222200((55))1,2-dichloroethane 62 62,98 5.55isopropyl acetate 43 61,87 5.59isooctane 57 56,41 5.63methyl isopropyl ketone 43 41,86 6n-heptane (C7) 43 57,71,100 6.061-butanol 56 41,43,55 6.67trichloroethene 95 95,97,134,132 6.73methyl cyclohexane 83 55,98 7.171,4-dioxane 88 58,43,57 7.43propyl acetate 43 61,73 7.612-ethoxyethanol 59 31,45,72 8.12pyridine 79 52,50,51 9.04hexanone (MIBK) 43 58,56,85,100 9.17isoamyl alcohol 55 42,41,43,70 9.33toluene 91 92,65,51 9.37ethylene glycol 31 33 9.69isobutyl acetate 43 56,73 9.911-pentanol 42 55,70,41 10.43formamide 45 29,44 10.491,1-diethoxypropane 59 47,87,103 10.792-hexanone (MBK) 43 58,57,100 10.88butyl acetate 43 56 11.31dimethyl formamide (DMF) 73 44,58 11.68chlorobenzene 112 112,77,114 12.35ethylbenzene 91 91,106 12.64p-xylene 106 106,91 12.93m-xylene 106 106,91 12.93isoamyl acetate 43 55,70 13.28o-xylene 106 106,91 13.74dimethyl sulfoxide 78 63,45 14.06N,N-dimethylacetamide 87 44,43,72 14.45isopropylbenzene (cumene) 105 120,77 14.55anisole 108 78,65,51 14.721-methyl-2-pyrrolidinone 99 98,44,42 19.541,2,3,4-tetrahydronaphthalene 104 132,117,91,65 21.39sulfolane 41 56,55,120 24.77

Rxi®-624Sil MS20 m x 0.18 mm x 1.0 µm dfDead Time 0.81 minutes Constant FlowInitial 45°C (hold 5 min.) 7C/min. to 220°C (hold 5 min.)

Reduce method development time—use a retention time index for column selection.

for more infoSee ppaaggeess 669944--669955 for Rxi®-624Sil MS chromatograms.



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Organic Volatile Impurities/Residual Solvents

Class 1 Residual Solvents for Water-Soluble Articles on Rxi®-624Sil MS

GC_PH1144

CCoonncc..PPeeaakkss RRTT ((mmiinn..)) ((µµgg//mmLL))

1. 1,1-Dichloroethene 3.586 0.072. 1,1,1-Trichloroethane 8.536 0.083. Carbon tetrachloride 9.042 0.034. Benzene 9.787 0.025. 1,2-Dichloroethane 10.112 0.04

* DMSO Interference

CCoolluummnn Rxi®-624Sil MS, 30 m, 0.32 mm ID, 1.80 µm (cat.# 13870)SSaammppllee Residual Solvents - Class 1 (cat.# 36279)Diluent: waterIInnjjeeccttiioonn headspace-loop split (split ratio 5:1)Liner: 1mm Split (cat.# 20972)HHeeaaddssppaaccee--LLooooppInj. Port Temp.: 140 °CInstrument: Tekmar HT3Inj. Time: 1 min.Transfer Line Temp.: 110 °CValve Oven Temp.: 110 °CSample Temp.: 80 °CSample Equil. Time: 60 min.Vial Pressure: 10 psi

Pressurize Time: 0.5 min.PressureEquilibration Time: 0.05 min.

Loop Pressure: 5 psiLoop Fill Time: 0.1 min.OOvveennOven Temp: 40 °C (hold 20 min.) to 240 °C at 10 °C/min. (hold 20 min.)CCaarrrriieerr GGaass He, constant flowLinear Velocity: 35 cm/sec.Dead Time: 1.45 min. @ 40 °CDDeetteeccttoorr FID @ 250 °CData Rate: 5 HzIInnssttrruummeenntt Agilent/HP6890 GCAAcckknnoowwlleeddggeemmeenntt Teledyne Tekmar

GC_PH1146

Class 2 - Mix A Residual Solvents for Water-Soluble Articles on Rxi®-624Sil MS

CCoonncc..PPeeaakkss RRTT ((mmiinn..)) ((µµgg//mmLL))

1. Methanol 2.281 25.002. Acetonitrile 4.009 3.423. Dichloromethane 4.313 5.004. trans-1,2-Dichloroethene 4.798 7.835. cis-1,2-Dichloroethene 7.028 7.836. Tetrahydrofuran 7.706 5.757. Cyclohexane 8.708 32.338. Methylcyclohexane 14.099 9.839. 1,4-Dioxane 15.054 3.17

10. Toluene 22.018 7.4211. Chlorobenzene 26.570 3.0012. Ethylbenzene 26.837 3.0713. m-Xylene 27.147 10.8514. p-Xylene 27.147 2.5315. o-Xylene 27.927 1.63

CCoolluummnn Rxi®-624Sil MS, 30 m, 0.32 mm ID, 1.80 µm (cat.# 13870)SSaammppllee Residual Solvents Class 2 - Mix A (cat.# 36271)Diluent: waterIInnjjeeccttiioonn headspace-loop split (split ratio 5:1)Liner: 1mm Split (cat.# 20972)HHeeaaddssppaaccee--LLooooppInj. Port Temp.: 140 °CInstrument: Tekmar HT3Inj. Time: 1 min.Transfer Line Temp.: 110 °CValve Oven Temp.: 110 °CSample Temp.: 80 °CSample Equil. Time: 60 min.Vial Pressure: 10 psi

Pressurize Time: 0.5 min.Pressure

Equilibration Time: 0.05 min.Loop Pressure: 5 psiLoop Fill Time: 0.1 min.OOvveennOven Temp: 40 °C (hold 20 min.) to 240 °C at 10 °C/min. (hold 20 min.)CCaarrrriieerr GGaass He, constant flowLinear Velocity: 35 cm/sec.Dead Time: 1.45 min. @ 40 °CDDeetteeccttoorr FID @ 250 °CData Rate: 5 HzIInnssttrruummeenntt Agilent/HP6890 GCAAcckknnoowwlleeddggeemmeenntt Teledyne Tekmar

NEW!

NEW!


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CCoolluummnn:: Rxi®-624Sil MS, 30 m, 0.32mm ID, 1.80 µm (cat.# 13870)

Sample: Residual Solvents Class 2 - Mix B (cat.# 36280) Diluent: water Injection: headspace-loop split (split ratio 5:1) Liner: 1 mm Split (cat.# 20972)

HHeeaaddssppaaccee--LLoooopp Inj. Port Temp.: 140 °C Instrument: Tekmar HT3 Inj. Time: 1 min. Transfer Line Temp.: 110 °C Valve Oven Temp.: 110 °C Sample Temp.: 80 °C Sample Equil. Time: 60 min. Vial Pressure: 10 psi Pressurize Time: 0.5 min. Pressure Equilibration Time: 0.05 min. Loop Pressure: 5 psi Loop Fill Time: 0.1 min.

OOvveenn Oven Temp: 40 °C (hold 20 min.) to 240 °C at 10 °C/min. (hold 20 min.) Carrier Gas: He, constant flow Linear Velocity: 35 cm/sec. Dead Time: 1.45 min. @ 40 °C Detector: FID @ 250 °C Data Rate: 5 Hz

IInnssttrruummeenntt:: Agilent/HP6890 GC Acknowledgement: Teledyne Tekmar

PPeeaakkss RRTT ((mmiinn..)) CCoonncc.. ((µµgg//mmLL)) 1. Hexane 5.355 2.42 2. Nitromethane 6.793 0.42 3. Chloroform 8.092 0.50 4. 1,2-Dimethoxyethane 9.980 0.83 5. Trichloroethene 12.941 0.67 6. Pyridine 21.303 1.67 7. 2-Hexanone 24.862 0.42 8. Tetralin 33.781 0.83

GC_PH1148

Class 2—Mix B Residual Solvents for Water-Soluble Articles on Rxi®-624Sil MS

NEW!

free literatureResidual Solvent Analysis

Implementing USP <467>

Download your copy fromwww.restek.com

Applications Notelit. cat.# PHFL1018A


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Organic Volatile Impurities: Retention Time Index

GG1166 GG1166 GG4433 GG2277 GG11 NNAACarrier gas: helium IICCHH SSttaabbiillwwaaxx®® RRttxx®®--WWAAXX RRttxx®®--11330011 RRxxii®®--55mmss RRttxx®®--11 RRttxx®®--220000CCoommppoouunndd CCllaassss RReetteennttiioonn TTiimmee RReetteennttiioonn TTiimmee RReetteennttiioonn TTiimmee RReetteennttiioonn TTiimmee RReetteennttiioonn TTiimmee RReetteennttiioonn TTiimmee1,1,1-trichloroethane 1 3.96 3.49 5.43 5.40 10.82 8.351,1,2-trichloroethene 2 15.72 14.28 10.99 9.77 16.75 14.941,1-dichloroethene 1 2.23 2.04 2.79 4.41 5.73 4.161,2-dichloroethane 1 8.80 7.68 6.15 5.46 10.38 9.74cis-1,2-dichloroethene 2 6.50 5.65 4.79 2.88 8.71 7.11trans-1,2-dichloroethene 2 3.63 3.20 3.55 3.54 7.17 5.161,2-dimethoxyethane 2 4.80 4.18 6.03 5.54 10.98 10.631,4-dioxane 2 8.55 7.49 7.86 7.26 13.54 14.341-butanol 3 11.13 10.08 7.18 5.76 11.49 10.131-pentanol 3 14.95 13.75 11.19 9.44 16.99 14.951-propanol 3 7.69 6.80 4.20 3.37 6.81 6.132-butanol 3 7.25 6.44 5.08 4.16 8.51 7.692-ethoxyethanol 2 13.99 12.70 8.69 7.36 13.91 13.992-methoxyethanol 2 12.42 11.11 6.02 5.14 9.83 10.742-methyl-1-propanol 3 9.32 8.40 6.00 4.79 * *2-propanol 3 4.81 4.25 3.00 2.55 4.91 4.693-methyl-1-butanol 3 13.42 12.25 9.86 8.26 15.28 13.55acetic acid 3 22.47 20.34 6.52 4.61 8.84 8.96acetone 3 3.02 2.64 2.89 2.50 4.64 7.68acetonitrile 2 6.91 5.83 3.28 2.47 4.32 8.89anisole 3 18.65 17.09 17.12 16.28 25.00 22.84benzene 1 5.23 4.54 5.98 3.83 11.63 9.17butyl acetate 3 8.86 7.88 12.12 11.38 19.43 19.63carbon tetrachloride 1 3.96 3.49 5.61 5.90 11.89 7.42chlorobenzene 2 13.91 12.54 13.55 13.14 21.56 18.48chloroform 2 7.31 6.41 5.23 4.64 9.18 6.66cumene 3 12.36 11.17 16.66 16.69 25.88 20.90cyclohexane 2 2.16 2.01 5.37 5.89 * *dichloromethane 2 5.01 4.33 3.31 3.06 5.87 4.88dimethylsulfoxide 3 26.47 24.43 16.62 13.01 18.81 30.95ethanol 3 4.98 4.37 2.52 2.19 4.03 3.80ethyl acetate 3 4.08 3.56 4.87 4.44 9.04 10.35ethyl benzene 2 10.72 9.58 13.86 13.81 22.54 18.18ethyl ether 3 1.72 1.63 2.58 2.67 5.34 3.87ethyl formate 3 3.16 2.78 3.00 2.78 5.46 6.48ethylene glycol 2 28.06 26.23 10.77 6.63 12.59 13.86formamide 2 32.99 30.93 11.85 7.30 12.72 19.93formic acid 3 24.64 22.09 5.19 2.60 5.59 5.06heptane 3 1.98 1.86 6.34 6.98 14.18 7.84hexane 2 1.65 1.58 3.77 4.11 9.06 4.86isobutyl acetate 3 6.99 6.18 10.39 9.69 17.35 18.02isopropyl acetate 3 4.26 3.74 6.19 5.71 11.47 12.38methanol 2 4.23 3.64 1.96 1.80 3.14 2.93methyl acetate 3 3.19 2.80 3.17 2.93 5.80 7.10methylbutyl ketone 2 9.10 8.05 11.81 10.50 17.94 20.81methylcyclohexane 2 2.50 2.30 7.31 7.95 15.49 9.21methylethyl ketone 3 4.33 3.76 4.90 4.09 7.99 11.55methylisobutyl ketone 3 6.84 5.97 9.64 8.49 15.35 18.41m-xylene 2 11.21 10.04 14.29 14.17 23.01 18.78N,N-dimethylacetamide 2 20.75 19.01 12.95 13.96 21.42 30.00N,N-dimethylformamide 2 18.04 16.26 13.09 10.23 16.52 26.19nitromethane 2 11.82 10.31 4.84 3.53 6.30 12.01N-methylpyrrolidone 2 29.84 27.86 25.09 21.85 29.99 38.08o-xylene 2 12.79 11.51 15.46 15.26 24.23 20.33pentane 3 1.49 1.45 2.39 2.62 5.36 3.29propyl acetate 3 5.98 5.29 8.03 7.44 * *p-xylene 2 10.98 9.82 14.29 14.17 22.99 18.69pyridine 2 12.64 11.24 9.60 8.57 15.40 16.45sulfolane 2 47.62 43.31 34.02 28.90 36.76 48.67tert-butylmethyl ether 3 1.94 1.82 3.50 3.59 7.52 5.73tetrahydrofuran 3 3.63 3.19 5.12 4.90 9.81 9.48tetralin 2 25.12 23.48 27.49 27.44 37.27 31.72toluene 2 7.86 6.91 9.80 9.66 17.36 14.001,1-diethoxypropane — 5.42 4.84 11.39 11.38 19.82 15.082,2-dimethoxypropane — 3.11 2.79 5.48 5.55 11.37 8.672-chloropropane — 1.96 1.82 2.67 2.66 5.20 4.612-methylpentane — 1.58 1.52 3.22 3.56 7.72 4.32acetaldehyde — 2.05 1.85 1.86 1.84 3.14 3.90chloroethane — 1.83 1.71 2.14 2.10 3.97 3.55chloromethane — 1.63 1.55 1.70 1.70 3.01 2.73ethylene oxide — 2.05 1.86 1.89 2.02 3.59 3.92formaldehyde — 2.25 1.57 1.68 1.58 2.66 2.59isoamyl acetate — 10.51 9.43 14.84 14.18 22.80 22.62isooctane — 1.85 1.75 5.84 6.59 13.66 8.07isopropyl ether — 1.86 1.76 4.03 4.23 9.03 5.83methyl cyclopentane — 1.91 1.79 4.50 4.93 10.41 5.81methyl isopropyl ketone — 4.93 4.29 6.58 5.69 11.04 14.47methylal — 2.26 2.06 2.84 2.82 5.65 5.09trichloroethene — 6.50 5.70 7.07 7.05 13.58 9.75water — 8.24 7.18 1.74 1.68 2.75 2.57* Not determined

RReetteennttiioonn ttiimmee ddaattaa ccoolllleecctteedd uussiinngg tthhee ffoolllloowwiinngg ccoonnddiittiioonnss:: G16 Stabilwax®: 30m, 0.25mm ID, 0.5µm df, Phase ratio: 125, Oven program: 40ºC, hold 1 min., to 190ºC @ 4ºC/min., hold 15 min., Carrier flow: 1.2mL/min., Dead time: 1.38 min. @ 45ºCG16 Rtx®-WAX: 30m, 0.25mm ID, 0.5µm df, Phase ratio: 125, Oven program: 40ºC, hold 1 min., to 190ºC @ 4ºC/min., hold 15 min., Carrier flow: 1.2mL/min., Dead time: 1.40 min. @ 45ºCG43 Rtx®-1301: 30m, 0.25mm ID, 1.0µm df, Phase ratio: 63, Oven program: 40ºC, hold 1 min., to 190ºC @ 4ºC/min., hold 15 min., Carrier flow: 1.2mL/min., Dead time: 1.40 min. @ 45ºCG27 Rxi®-5ms: 30m, 0.25mm ID, 1.0µm df, Phase ratio: 63, Oven program: 40ºC, hold 1 min., to 190ºC @ 4ºC/min., hold 15 min., Carrier flow: 1.1mL/min., Dead time: 1.49 min. @ 45ºCG1 Rtx®-1: 60m, 0.53mm ID, 3.00µm df, Phase ratio: 43, Oven program: 30ºC, hold 4 min., to 220ºC @ 4ºC/min., Carrier flow: 6.3mL/min., Dead time: 2.54 min. @ 35ºCRtx®-200: 60m, 0.53mm ID, 3.00µm df, Phase ratio: 43, Oven program: 30ºC, hold 4 min., to 220ºC @ 4ºC/min., Carrier flow: 7.8mL/min., Dead time: 2.22 min. @ 35ºC

Reduce method development time—use a retention time index for column selection.


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GC_PH00951

Residual Solvents Class 1

Stabilwax® (G16)


Sample: USP Stock Mixture USP<467> Residual Solvents Class 1 Mix (cat.# 36279) in 20mL headspace vial (cat.# 24685), water diluent

Inj.: headspace injection (split ratio 1:5), 2mm splitless liner IP deactivated (cat.# 20712)

Inj. temp.: 140°CCarrier gas: helium, constant flowFlow rate: 2.15mL/min., 35.2cm/sec.Oven temp.: 50°C for 20 min. to 165°C @ 6°C/min.

(hold for 20 min.) Det.: FID @ 250°C

Headspace ConditionsInstrument: Overbrook Scientific HT200HSyringe temp.: 100°CSample temp.: 80°CSample equil. time.: 45 min.Injection vol.: 1.0mLInjection speed: setting 8Injection dwell: 5 sec.

1. 1,1-dichloroethene2. 1,1,1-trichloroethane3. carbon tetrachloride4. benzene5. 1,2-dichloroethane

GC_PH00952

Residual Solvents Class 2 Mix A

Stabilwax® (G16)


Sample: USP Stock Standard Residual Solvents Class 2 Mix A (cat.# 36271) in 20mL headspacevial (cat.# 24685), water diluent





1. cyclohexane2. methylcyclohexane3. trans-1,2-dichloroethene4. tetrahydrofuran5. methanol6. dichloromethane7. cis-1,2-dichloroethene8. acetonitrile9. toluene

10. 1,4-dioxane11. ethyl benzene12. p-xylene13. m-xylene 14. o-xylene15. chlorobenzene


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GC_PH00953

1. hexane2. 1,2-dimethoxyethane3. trichloroethylene4. chloroform5. 2-hexanone6. nitromethane7. pyridine8. tetralin

Residual Solvents Class 2 Mix B

Stabilwax® (G16)


Sample: USP Stock Standard Residual Solvents Class 2 Mix B (cat.# 36272) in 20mL headspace vial (cat.# 24685), water diluent





Keep up with advances in melamine analysis at www.restek.com/melamine

Melamine Analysis Kit............cat. # 33254 (see page 535)

Detect melamine and related compounds by GC/MS with a completeanalysis kit. Consistent with FDA procedure and new guidance for at-riskpharmaceutical components.

At Risk for MelamineMeet new FDA guidance for melamine contamination

in at-risk pharmaceutical components.

Kit includes (also sold individually):• Rxi®-5Sil MS with 5 meter Integra Guard® Column

• Standards

• Derivatization Reagent

• Accessory Tubes and Syringe Filters

• Easy-to-Follow Instructions with procedural check list to simplify laboratory documentation!


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Organic Volatile Impurities

Rtx®-200 & Rtx®-WAX (GCxGC)

GC_PH00888

Columns: Rtx®-200, 60m, 0.25mm ID, 1.0µm (cat.# 15056)Rtx®-Wax, 2m, 0.18mm ID, 0.3µm (custom)

Sample: 0.2µL mix of 69 neat organic volatile impuritiesInstrument: Agilent 6890 with LECO liquid nitrogen cryojet modulatorInj.: split/splitless, split ratio 600:1; gas saver: 20mL/min. after 1 min.;

4mm ID split inlet liner w/wool (cat.# 20781); injection with band formation (fast injection)Inj. temp.: 250°CCarrier gas: helium, constant flowFlow rate: 1.5mL/min.Oven temp.: Rtx®-200: 35°C (9 min.) to 220°C @ 3°C/min. (hold 1 min.);

Rtx®-Wax: 65°C (9 min.) to 250°C @ 3°C/min. (hold 1 min.)Modulation: modulator offset: 30°C; 2nd dimension separation: 4 sec.; hot pulse: 0.3 sec.;

cool between stages: 1.7 sec.Det: FID @ 250°C; hydrogen: 40mL/min.; air: 450mL/min.; make-up gas: 45mL/min.; sampling rate: 200Hz

did you know?GCxGC Separations

Separation of the complete list of International Conference on Harmonization Class 1, Class 2, and Class 3 organic volatiles requires at least two, and often three, separate analyses on differingcapillary GC columns. While many laboratories do not monitor for the complete list, separation ofOVIs still is a challenge, often characterized by long run times and incomplete separations.

Using comprehensive GCxGC, it is possible to resolve all of these target compounds, in a singleanalysis, with less than a 1-hour run time. In this approach, two columns of differing selectivity areused to separate the compounds in a 2-dimensional plot, as shown above. Various detectors alsocan be employed, including time-of-flight mass spectrometry, to yield reliable information for theentire target compound list in a single analysis.

For more about GCxGC, visit our website and search for GCxGC.


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Column: Rtx®-1301, 30m, 0.53mm ID x 3.0µm (cat.# 16085) Sample: headspace injection of 28 Class 1 and 2 residual solvents for pharmaceutical processing,

prepared at the regulatory limit concentration, using samples shaken and heated at 80°C for 15 min., 1mL headspace injection

Oven temp.: 40°C (hold 20 min.) to 240°C @ 10°C/min. (hold 20 min.)Inj./det. temp.: 200°C/250°CFID sensitivity: 1.1 x 10-11 AFSCarrier gas: hydrogen @ 35cm/sec.Split ratio: 2:1

1. methanol2. 1,1-dichloroethene 3. acetonitrile4. methylene chloride (dichloromethane)5. hexane (C6)6. cis-1,2-dichloroethene7. nitromethane8. chloroform9. cyclohexane

10. 1,1,1-trichloroethane11. carbon tetrachloride12. benzene13. 1,2-dimethoxyethane14. 1,2-dichloroethane15. trichloroethylene (1,1,2-trichlorethene)16. methylcyclohexane17. 1,4-dioxane18. pyridine19. toluene 20. 2-hexanone21. chlorobenzene22. DMF23. ethylbenzene24. m-xylene25. p-xylene26. o-xylene27. N,N-dimethylacetamide28. 1,2,3,4-tetrahydronaphthalene

2 4 6 8 10 12 14 16 18 20 22 24 26 28 30 32 34

1 23

4

5

6

78

9,10

11 12 13,1415

16

17 18

19

20 21

22,23

24,25

26

27

28

GC_PH00553

Residual Solvents

European Pharmacopoeia Class 1 and Class 2

Rtx®-1301(headspace)

Inj.: static headspace injection (see static headspace conditions)Inj. temp.: 180°CCarrier gas: helium, split 2:1Linear velocity: 5mL/min., constant flowOven temp.: 40°C for 20 min. to 240°C at 25°C/min. (hold for 10 min.)Det.: FID @ 250°C

hydrogen flow: 40mL/min.air flow: 450mL/min.make-up flow: 45mL/min.

Static Headspace (Loop) Conditions:Instrument: Teledyne Tekmar HT3Valve oven temp.: 150°CTransfer line temp.: 150°CStandby flow rate: 10mL/min.Platen/sample temp.: 80°CPlaten temp equil. time: 2.00 min.Sample equil. time: 15.00 min.Mixer time: 2.00 min.Mixing level: 5Mixer stabilize time: 0.50 min.Pressurize: 15psiPressurize time: 2.00 min.Pressurize equil. time: 0.50 min.Loop fill pressure: 5psiLoop fill time: 2.00 min.Loop fill equil. time: 0.50 min.Inject time: 1.00 min.

Column: Rtx®-G43, 30m, 0.53mm ID, 3.0µm (cat.# 16085-126)Sample: USP <467> Calibration Mixture #5 (cat.# 36007) in DMSO stock

standard. To each 22mL headspace vial 5ml water, ~ 1.0g of sodium sulfate and 100µL of stock standard were added. The preparation yielded the following concentrations,

Retention Time (min.) Sample Concentration (µg/mL) 1. dichloromethane 5.110 12.02. chloroform 9.285 1.23. benzene 11.173 0.044. trichloroethylene 14.647 1.65. 1,4-dioxane 17.436 7.6

GC_PH00810

Organic Volatile Impurities

USP <467>

Rtx®-G43(static headspace)


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GC CHROMATOGRAMS | SOLVENTS & CHEMICALS

Solvents

Column: Rt®-Q-BOND, 30m, 0.53mm ID, 20µm (cat.# 19742)Sample: solvent mixtureInj.: 1.0µL, split (split vent flow 100mL/min.),

4mm single gooseneck liner (cat.# 20798)Inj. temp.: 200°CCarrier gas: hydrogen, constant pressure, 4.2psiLinear velocity: 40cm/sec. @ 120°COven temp.: 120°C to 240°C @ 5°C/min. (hold 5.0 min.)Det.: FID @ 240°C

Solvent Mixture

Rt®-Q-BOND(PLOT)

1. methanol2. ethanol3. acetonitrile4. acetone5. dichloromethane6. 1,1-dichloroethene7. nitromethane8. trans-1,2-dichloroethylene9. cis-1,2-dichloroethylene

10. tetrahydrofuran11. chloroform12. ethyl acetate13. 1,2-dichloroethane14. 1,1,1-trichloroethane

15. benzene16. 1,2-dimethoxyethane17. trichloroethylene18. 1,4-dioxane19. pyridine20. dimethylformamide21. methylcyclohexane22. toluene23. 2-hexanone24. chlorobenzene25. ethylbenzene26. m-xylene27. p-xylene28. o-xylene

GC_PC01082

NEW!

Solvent Mixture

Rt®-S-BOND(PLOT)

Column: Rt®-S-BOND, 30m, 0.53mm ID, 20µm (cat.# 19746)Sample: solvent mixtureInj.: 1.0µL, split (split vent flow 100mL/min.),



10. tetrahydrofuran11. chloroform12. ethyl acetate13. 1,2-dichloroethane14. 1,1,1-trichloroethane

15. benzene16. 1,2-dimethoxyethane17. trichloroethylene18. 1,4-dioxane19. pyridine20. dimethylformamide21. methylcyclohexane22. toluene23. 2-hexanone24. chlorobenzene25. ethylbenzene26. m-xylene27. p-xylene28. o-xylene

GC_PC01080

NEW!

701-707_GCappChem.qxp 11/22/2010 9:33 PM Page 701

Solvents

HayeSep® Q(micropacked)

5

7

8

6

4

3

2

1

min. 4 8

1. methanol2. ethanol3. acetonitrile4. acetone5. methylene chloride6. n-pentane7. chloroform8. n-hexane

Column: HayeSep® Q, 2m, 1mm ID (cat.# 19017)Sample: 1µL direct injection of a neat solvent mixtureOven temp.: 80°C to 180°C @

16°C/min. (hold 5 min.)Inj./det. temp.: 200°CCarrier gas: heliumFlow: 20mL/min. set @ 40°CFID sensitivity: 512 x 10-11 AFS

GC_CH00328

Solvent Mixture

Rt®-QS-BOND(PLOT)

Column: Rt®-QS-BOND, 30m, 0.53mm ID, 20µm (cat.# 19738)Sample: solvent mixtureInj.: 1.0µL, split (split vent flow 100mL/min.),



10. tetrahydrofuran11. chloroform12. ethyl acetate13. 1,2-dichloroethane14. 1,1,1-trichloroethane15. benzene

16. 1,2-dimethoxyethane17. trichloroethylene18. 1,4-dioxane19. pyridine20. dimethylformamide21. methylcyclohexane22. toluene23. 2-hexanone24. chlorobenzene25. ethylbenzene26. m-xylene27. p-xylene28. o-xylene

GC_PC01081

NEW!

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Solvents





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Aldehydes, Ketones, Amines

Column: Rt®-QS-BOND, 30m, 0.53mm ID (cat.# 19738)Sample: 1,000µg/mL VOA Calibration Mix #1 (ketones)

(cat.# 30006) in methanol:water, 90:10 (v/v)Inj.: 1µL split (split ratio 50:1), 4mm Siltek® single

gooseneck liner (cat.# 20798-214.1)Inj. temp.: 240°CCarrier gas: helium, constant flow Flow rate: 5.7mL/min. @ 40°COven temp.: 60°C to 225°C @ 15°C/min. (hold 10 min.)Det.: FID @ 240°C

GC_PC01015

1. acetone2. 2-butanone3. 2-hexanone4. 4-methyl-2-pentanone

Ketones

Rt®-QS-BOND(PLOT)

GC_CH01137

Peak List1. air2. carbon dioxide3. formaldehyde4. water5. methanol

Column: Rt®-U-BOND, 30m, 0.53mm ID, 20.0µm (cat.# 19750)Sample: formaldehyde (manual headspace)Inj.: 10µL split (split ratio 1:10), 40mL/min. split vent flow rate

2mm split Precision® liner w/wool (cat.# 20823)Inj. temp.: 200°CCarrier gas: helium, constant pressure (7.7psi, 53.1kPa)Linear velocity: 39cm/sec. @ 100°COven temp.: 100°C (hold 1 min.) to 150°C @ 25°C/min. (hold 3 min.)Det.: TCD @ 200°CInstrument: Agilent 5890

Formaldehyde

Rt®-U-BOND(PLOT)

NEW!

Ethanolamines

Rtx®-5 Amine

1

2

3

4

min. 5 10

1. monoethanolamine2. diethanolamine3. triethylene glycol

monomethylether (IS)4. triethanolamine

Column: Rtx®-5 Amine, 15m, 0.25mm ID, 0.50µm (cat.# 12335)Sample: 1.0µL split injection of ethanolamine mix in methanolOn-column conc.: 34ngOven temp.: 50°C (hold 2 min.) to 180°C @

10°C/min. (hold 2 min.)Inj./det. temp.: 280°C/300°CCarrier gas: hydrogenLinear velocity: 43cm/sec. set @ 50°CFID sensitivity: 6.4 x 10-11 AFSSplit ratio: 58:1

GC_CH00296


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Amines

Ethyleneamines

Rtx®-5 Amine

1 23

4

5

6

7

min. 5 10 15 20 25GC_CH00298

Column: Rtx®-5 Amine, 30m, 0.25mm ID, 0.50µm (cat.# 12338)Sample: 3.0µL split injection of ethyleneamine industrial sample On-column conc.: ~5-80ngOven temp.: 40°C (hold 4 min.) to 315°C

@ 10°C/min. (hold 5 min.)Inj./det. temp.: 315°CCarrier gas: hydrogenLinear velocity: 43cm/sec. set @ 40°CFID sensitivity: 6.4 x 10-11 AFSSplit ratio: 20:1

1. isopropanol2. monoethanolamine3. ethylenediamine4. piperazine5. diethylenetriamine6. aminoethylethanolamine7. aminoethylpiperazine

remaining impurities consist of ethyleneamine and piperazinederivatives

Amines (low MW)

Stabilwax®-DB

Column: Stabilwax®-DB, 30m, 0.53mm ID, 1.0µm (cat.# 10855)Sample: 1.0µL direct injection of amines in waterOven temp.: 45°C Inj./det. temp.: 250°CCarrier gas: hydrogenLinear velocity: 40cm/sec. (flow rate: 5cc/min.)FID sensitivity: 1 x 10-11 AFSRecommended

inlet liner: Uniliner®

1. trimethylamine2. dimethylamine3. ethylamine4. methylamine5. isopropylamine6. n-propylamine7. tert-butylamine8. diethylamine9. sec-butylamine

1

2

3

4

5

6

7

89

GC_CH00304 min. 1 2 3

1. methylamine2. dimethylamine 3. trimethylamine4. ethylamine5. isopropylamine6. tert-butylamine7. n-propylamine8. diethylamine9. sec-butylamine

Amines, Primary

Rtx®-35 Amine

1

2/3

4

5

6

78

9

GC_CH00578

Column: Rtx®-35 Amine, 30m, 0.53mm ID, 1.0µm (cat.# 11355)Sample: primary amines, 50ppm on-column conc. in waterInj.: 1.0µL, split (10:1), 4mm base-deactivated single

gooseneck inlet liner (cat.# 20798-210.1)Injector: 250°CCarrier gas: helium, constant pressureLinear velocity: 35.7cm/sec.Oven temp.: 35°C (hold 5.0 min.)Det.: FID @ 300°C


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Amines, Amines & Phenols

1. cyclohexane2. hexamethyleneimine3. 1,4-diaminobutane4. pentamethylenediamine5. 1,2-diaminocyclohexane6. 1,5-diamino-2-methylpentane7. aminomethylcyclopentylamine8. hexamethylenediamine9. 6-aminocapronitrile

10. n-valeramide11. adiponitrile12. bis-hexamethylenetriamine

Hexamethylenediamine (HMD)

Stabilwax®-DB

Column: Stabilwax®-DB, 30m, 0.32mm ID, 0.25µm (cat.# 10824)Sample: 0.4µL direct injection of a neat hexamethylenediamine (HMD)

sampleOn-column conc.: 10 to 1,000ng/componentOven temp.: 95°C (hold 6 min.) to 235°C @

7°C/min. (hold 4 min.)Inj./det. temp.: 250°CCarrier gas: hydrogenLinear velocity: 40cm/sec. FID sensitivity: 2 x 10-11 AFS

GC_CH00302

min. 4 8 12 16 20 24 28 32

1

2

3

4 5

6

7

8

9

10

11

12

Column: Stabilwax®-DB, 30m, 0.53mm ID, 0.5µm (cat.# 10840)Sample: 0.2µL direct injection of a neat hexamethylenediamine

sample onto a Uniliner® inlet linerOven temp.: 95°C (hold 6 min.) to 235°C @

7°C/min. (hold 2 min.)Inj./det. temp.: 255°CCarrier gas: hydrogenLinear velocity: 40cm/sec. (flow rate: 5cc/min.)FID sensitivity: 64 x 10-11 AFS

min. 4 8 12 16 20 24 28

1

23

45

6

7

8

9

10

11

12

GC_CH00303

Amines & Phenols

Rtx®-5 Amine

1. diethylamine2. pyridine3. morpholine4. phenol5. aniline6. 2-chlorophenol7. diethylenetriamine8. octylamine9. 1-methyl-2-pyrrolidinone

10. 2-nitrophenol11. 2,6-dimethylaniline12. nicotine13. 2-nitroaniline

Column: Rtx®-5 Amine, 30m, 0.32mm ID, 1.0µm (cat.# 12354)Sample: 1.0µL split injection of amines and phenols in waterOn-column conc.: 22ngOven temp.: 120°C to 220°C @ 10°C/min.Inj./det. temp.: 305°CCarrier gas: hydrogenLinear velocity: 38cm/sec. set @ 120°CFID sensitivity: 6.4 x 10-11 AFSSplit ratio: 25:1

GC_CH00301min. 2 4 6 8 10

1 2

3

4

5

6

7

8

9

10

11

12

13


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Nitrosamines, Amines/Alcohols/Chlorides, Chlorofluorocarbons

Chlorofluorocarbons

5% Krytox on 60/80 CarboBlack B(packed)

1

2

3

4

5 6

min. 4 8 12 16

1. Freon® 222. Freon® 123. Freon® 214. Freon® 1145. Freon® 114A isomer6. Freon® 11

Column: 5% Krytox on 60/80 CarboBlack B, 3.05m, 1/8" OD, 2.1mm ID SilcoSmooth® stainless steel tubing (cat.# 80127-800)

Inj.: 1µL injected, concentration 20% each componentOven temp.: 50°CInj./det. temp.: 200°C/250°CCarrier gas: nitrogen @ 30mL/min.Det.: FID

GC_CH00323

for more infosee pages 649 & 707 for more chlorofluorocarbon chromatograms.

Amines/Alcohols/Chlorides

Stabilwax®

1

2

3

4

5

6 7

8

9 10

11

12

13 14

1617

15

min. 4 8 12 16 20GC_CH00307

1. n-octyl,N,N-dimethylamine2. n-octyl chloride3. n-decyl-N,N-dimethylamine4. n-decyl chloride5. n-octyl alcohol6. n-dodecyl-N,N-dimethylamine7. n-dodecyl chloride8. n-decyl alcohol9. n-tetradecyl-N,N-dimethylamine

10. n-tetradecyl chloride11. n-dodecyl alcohol12. n-hexadecyl-N,N-dimethylamine13. n-hexadecyl chloride14. n-tetradecyl alcohol15. n-octadecyl-N,N-dimethylamine16. n-hexadecyl alcohol17. n-octadecyl alcohol

Column: Stabilwax®, 30m, 0.53mm ID, 0.25µm (cat.# 10625)Inj.: 0.5µL split injectionOven temp.: 100°C to 250°C @

8°C/min. (hold 5 min.)Inj./det. temp.: 250°C Carrier gas: hydrogenLinear velocity: 40cm/sec. (flow rate: 5.2cc/min.)FID sensitivity: 128 x 10-11 AFSSplit ratio: 40:1

Nitrosamines

Stabilwax®-DB

Column: Stabilwax®-DB, 60m, 0.53mm ID, 1.0µm (cat.# 10858)Sample: direct injection of nitrosaminesConc.: 1.0µg/mLOven temp.: 100°C (hold 1 min.) to 170°C @ 5°C/min. Inj./det. temp.: 200°C Carrier gas: heliumLinear velocity: 100cm/sec. (flow rate: 15cc/min.)Det.: TSD

1. solvent2. N-nitrosodimethylamine3. N-nitrosodiethylamine4. N-nitrosodiisopropylamine5. N-nitrosodipropylamine6. N-nitrosodibutylamine7. N-nitrosopiperidine8. N-nitrosopyrrolidine9. N-nitrosomorpholine

987

6

5

43

2

1

min. 2 4 6 8 10 12 14GC_CH00306


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Chlorofluorocarbons, Cresylic Acids

Freon® 12 & Ethylene Oxide

Rtx®-1

21. Freon® 122. ethylene oxide

Column: Rtx®-1, 30m, 0.53mm ID, 5.0µm (cat.# 10179)Sample: 50µL split injection of Freon® 12 and ETOOven temp.: 25°CInj./det. temp.: 290°CCarrier gas: hydrogenLinear velocity: 40cm/sec. FID sensitivity: 4 x 10-11 AFSSplit vent: 40:1

GC_CH00324

min. 2

1 2

Freon® 12 & Ethylene Oxide

Rtx®-200

1

min. 4

1. Freon® 122. ethylene oxide

Column: Rtx®-200, 30m, 0.53mm ID, 3.0µm (cat.# 15085)Sample: 50µL direct injection of Freon® 12 and ETOOven temp.: 25°CInj./det. temp.: 290°CCarrier gas: hydrogenLinear velocity: 40cm/sec. (flow rate: 5.2cc/min.)

GC_CH00325

Cresylic Acids

Stabilwax®-DA

Column: Stabilwax®-DA, 30m, 0.25mm ID, 0.50µm (cat.# 11038)Sample: Wet needle split injection of cresylic acidsOven temp.: 180°C (hold 2 min.) to 260°C @ 2°C/min.Inj./det. temp.: 250°CCarrier gas: hydrogenLinear velocity: 40cm/sec. (flow rate: 3.2cc/min.)FID sensitivity: 64 x 10-11 AFSSplit ratio: 40:1

1. 2,6-dimethylphenol2. o-cresol3. phenol4. 2,4,6-trimethylphenol5. 2,3,6-trimethylphenol6. o-ethylphenol7. 2,5-dimethylphenol8. p-cresol9. 2,4-dimethylphenol

10. m-cresol11. C3 phenol12. 2,3-xylenol13. C3 phenol14. C3 phenol15. C3 phenol16. p-ethylphenol17. 3,5-xylenol18. m-ethylphenol19. 3,4-xylenol

min. 1 2 3 4 5 6 7 8 9 10 11 12GC_CH00277

1

2

3,4

5

6

7,89

10

1211

14

16,17 18

19

13

15


HPLC CHROMATOGRAMS

HPLC Chromatograms by Column Phase Index . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .709

Environmental . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .710-718Aldehydes, Explosives, Herbicides, Ketones, Pesticides, Polycyclic Aromatic Hydrocarbons

Foods & Flavors . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .719-735Dietary Supplements, Drug Residues, Flavor Compounds, Food Contaminants, Preservatives, Sugars, Vitamins

Pharmaceutical . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .736-743Admixed Drugs, Analgesics, Antiarrhythmics, Antiasthmatics, Antibiotics, Anti-Diabetic, Corticosteroids, Famotidine, Lactulose Concentrate, Potential Genotoxic Impurities, Steroids, Xanthines

Biochemical/Clinical . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .744-746Amino Acids, Catecholamines, Nucleic Acid Bases, Nucleosides, Nucleotides, Oxytocin, Peptides, Proteins, Purines/Pyrimidines

Clinical/Forensic . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .747-751Alcohol Metabolites, Amphetamines, Benzodiazepines, Cocaine, Diuretics, Opiates, Pain Management Drugs, THC

708-735_HPLCapps.qxp 11/22/2010 9:36 PM Page 708

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HPLC CHROMATOGRAMS

HPLC Chromatograms by Column Phase

Allure® AK

carbonyls . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .181, 710Allure® Basix

herbicides . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .714Allure® Biphenyl

antibiotics . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .740corticosteroids . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .741steroids . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .742Allure® C18

herbicides . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .712pesticides . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .716Allure® Organic Acids

fruit juice acids . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .531Allure® PFP Propyl

antibiotics . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .723benzodiazepines . . . . . . . . . . . . . . . . . . . . . . . . . . . . .751catecholamines . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .745cocaine, ecgonine methyl ester . . . . . . . . . . . . . . . . .750nucleic acid bases . . . . . . . . . . . . . . . . . . . . . . . . . . . .744opiates . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .748Pinnacle DB® Aqueous C18

food contaminants . . . . . . . . . . . . . . . . . . . . . . .720, 722pesticides . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .720, 722Pinnacle® DB Biphenyl

drug residues . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .725steroids . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .742Pinnacle® DB C18

vanilla bean extracts . . . . . . . . . . . . . . . . . . . . . . . . . .727xanthines . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .743Pinnacle® DB PAH

PAHs . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .718Pinnacle® II Amino

lactulose concentrate . . . . . . . . . . . . . . . . . . . . . . . . .743sugars . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .727Pinnacle® II C18

allicin . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .730capsaicinoids . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .728morphine sulfate . . . . . . . . . . . . . . . . . . . . . . . . . . . .738phenolic antioxidants . . . . . . . . . . . . . . . . . . . .727, 730Pinnacle® II Cyano

piperine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .728Pinnacle® II PAH

PAHs . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .717Pinnacle® II Silica

hydrocodone bitartrate . . . . . . . . . . . . . . . . . . . . . . .738tocopherols . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .730Ultra Aqueous C18

amino acids (aromatics) . . . . . . . . . . . . . . . . . . . . . .745analgesics . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .737carboxylic acids . . . . . . . . . . . . . . . . . . . . . . . . . . . . .726food contaminants . . . . . . . . . . . . . . . . . . . . . . .721, 722herbicides . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .714pesticides . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .721phenethyl glucosinolate . . . . . . . . . . . . . . . . . . . . . . .730sudan dyes . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722vitamins . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .731Ultra C18

acetaminophen, narcotic analgesics . . . . . . . . . . . . .738aldehydes, ketones . . . . . . . . . . . . . . . . . . . . . . . . . . .710beclomethasone . . . . . . . . . . . . . . . . . . . . . . . . . . . . .739corticosteroids . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .741drug residues . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .724herbicides . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .712hydrocodone bitartrate, acetaminophen . . . . . . . . .743nitrofuran metabolites . . . . . . . . . . . . . . . . . . . . . . . .724vitamins (fat soluble) . . . . . . . . . . . . . . . . . . . . . . . . .732

Ultra C8

explosives . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .711oxycodone . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .738vanillin & ethyl vanillin . . . . . . . . . . . . . . . . . . . . . . .728vitamins . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .733Ultra Carbamate

food contaminants (carbamates) . . . . . . . . . . . . . . .719Ultra Cyano

antiarrhythmics . . . . . . . . . . . . . . . . . . . . . . . . . . . . .739Ultra IBD

antiarrhythmics . . . . . . . . . . . . . . . . . . . . . . . . . . . . .739antibiotics . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .740, 741diflubenzuron (pesticide) . . . . . . . . . . . . . . . . . . . . .716glyburide . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .741nucleosides, nucleotides, & nucleic acid bases . . . .744vitamins . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .732Ultra PFP

purines, pyrimidines . . . . . . . . . . . . . . . . . . . . . . . . .745Ultra Phenyl

guaifenesin, codeine . . . . . . . . . . . . . . . . . . . . . . . . . .743Ultra Quat

paraquat, diquat . . . . . . . . . . . . . . . . . . . . . . . . .189, 715Ultra II® Aqueous C18

dietary supplements . . . . . . . . . . . . . . . . . . . . . . . . . .729herbicides . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .713melatonin . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .729organic acids . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .729vitamins . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .734Ultra II® Aromax

explosives . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .485, 711famotidine and USP impurities . . . . . . . . . . . . . . . .736potential genotoxic impurities . . . . . . . . . . . . . . . . .737vitamins . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .735Ultra II® Biphenyl

alcohol metabolites . . . . . . . . . . . . . . . . . . . . . . . . . .749amphetamines . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .750antibiotics . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .725diuretics . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .749drug residues . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .725drugs of abuse . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .748NSAIDs . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .723pain managment drugs in urine . . . . . . . . . . . . . . . .747sulfa drugs . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .725THC & metabolites . . . . . . . . . . . . . . . . . . . . . . . . . .748Ultra II® C18

vitamins . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .733Ultra II® Carbamate

food contaminants . . . . . . . . . . . . . . . . . . . . . . . . . . .719pesticides (carbamates) . . . . . . . . . . . . . . . . . . . . . . .719Viva C18

oxytocin . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .746peptides . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .745proteins . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .746

HPLC Chromatograms by Column Phase (Alphabetical Order)

GC & HPLC Chromatograms

Compound Indexstarting on page 752





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HPLC CHROMATOGRAMS | ENVIRONMENTAL

Aldehydes, Ketones

Carbonyls by CARB Method 1004 on Allure® AK

LC_EV0393

RReett.. TTiimmeePPeeaakk ((mmiinn..))DNPH derivatives of:1. formaldehyde 4.742. acetaldehyde 5.783. acrolein 6.864. acetone 7.095. propionaldehyde 7.316. crotonaldehyde 8.197. methacrolein 8.558. butyraldehyde 8.799. methylethylketone 9.06

10. benzaldehyde 10.0311. valeraldehyde 10.3912. m-tolualdehyde 11.0813. hexaldehyde 11.36

SSaammppllee::Inj.: 10µLConc.: 3µg/mL each analyte, as

aldehyde/ketoneSample diluent: acetonitrile

CCoolluummnn:: AAlllluurree®® AAKKCat.#: 9159525-700Dimensions: 200mm x 4.6mmParticle size: 5µmPore size: 60Å

CCoonnddiittiioonnss::Mobile phase: A) water : B) acetonitrile

TTiimmee ((mmiinn..)) %%BB0 608 70

10 100Flow: 1.5mL/min.Temp.: 30°CDet.: UV @ 360nm

Aldehydes and Ketones (DNPH derivatives) on Ultra C18

(40°C)

0 2 4 6 8 10 12 14 min.

LC_0036

1

2

4

5

7

8

3

6

9

10 11

12 13

PPeeaakk LLiisstt::DNPH derivatives of:

1. formaldehyde2. acetaldehyde3. acetone4. acrolein5. propionaldehyde6. crotonaldehyde7. MEK8. methacrolein9. butyraldehyde

10. benzaldehyde11. valeraldehyde12. m-tolualdehyde13. hexanaldehyde

SSaammppllee::Inj.: 10µLConc.: 3.0µg/mL each derivative

CCoolluummnn:: UUllttrraa CC1188Cat.#: 9174565Dimensions: 150mm x 4.6mmParticle size: 5µmPore size: 100Å

CCoonnddiittiioonnss::Mobile phase:

Solvent A: waterSolvent B: acetonitrileSolvent C: tetrahydrofuran50-30% A/30-65% B/20-5% C, 0-15 min.

Flow rate: 1.5mL/min.Det.: UV @ 365nmTemp.: 40°C


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Explosives

Explosives

EPA Method 8330B

Ultra II® Aromax

1. HMX2. RDX3. nitroglycerin4. nitrobenzene5. 4-amino-2,6-dinitrotoluene6. 3,5-dinitroaniline7. 2-nitrotoluene8. 2-amino-4,6-dinitrotoluene9. 3-nitrotoluene

10. PETN11. 4-nitrotoluene12. 1,3-dinitrobenzene13. 2,6-dinitrotoluene14. tetryl15. 2,4-dinitrotoluene16. 1,3,5-trinitrobenzene17. 2,4,6-trinitrotoluene

SSaammppllee:: Nitroaromatics and Nitramine Explosives by HPLC,EPA 8330B (cat.# 33204)

Inj.: 10µLConc.: 10µg/mL each componentSample diluent: methanol

CCoolluummnn:: Ultra II® AromaxCat.#: 9607575Dimensions: 250mm x 4.6mmParticle size: 5µmPore size: 100Å

CCoonnddiittiioonnss::Instrument: Shimadzu Prominence UFLCXRMobile phase: water:methanol, 35:65 (v/v)Flow: 1.2mL/min.Temp.: 30°CDet.: UV @ 254nm and 210nm

LC_EV0484

Sample: Nitroaromatics and Nitramine Explosives by HPLC,EPA 8330B (cat.# 33204)

Inj.: 10µLConc.: 50µg/mL each componentSample diluent: methanol

Column: Ultra C8cat.# 9103575

Dimensions: 250mm x 4.6mmParticle size: 5µmPore size: 100Å

Conditions:Instrument: Shimadzu ProminenceMobile phase: water:methanol, 52:48 (v/v)Flow: 1.2mL/min.Temp.: 30°CDet.: UV @ 254nm and 210nm

LC_EV0485

Explosives

EPA Method 8330B

Ultra C8

1. HMX2. RDX3. nitroglycerin4. nitrobenzene5. 4-amino-2,6-dinitrotoluene6. 3,5-dinitroaniline7. 2-nitrotoluene8. 2-amino-4,6-dinitrotoluene9. 3-nitrotoluene

10. PETN11. 4-nitrotoluene12. 1,3-dinitrobenzene13. 2,6-dinitrotoluene14. tetryl15. 2,4-dinitrotoluene16. 1,3,5-trinitrobenzene17. 2,4,6-trinitrotoluene

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Herbicides

LC_0319

Herbicides (Phenylurea) on Ultra C18

PPeeaakk LLiisstt:: CCoonncc.. ((µµgg//mmLL oorr ppppmm))1. tebuthiuron 22. thidiazuron 23. monuron 54. fluometuron 25. diuron 26. propanil 27. siduron 28. linuron 29. carbazole 5

10. diflubenzuron 2

SSaammppllee::Inj.: 20µLConc.: see peak listSample diluent: acetonitrile


CCoonnddiittiioonnss::Mobile phase: A: 25mM phosphate buffer, pH 2.5

B: acetonitrileTTiimmee ((mmiinn..)) %%BB

0 408 40

14 5518 5519 40

Flow: 1.5mL/min.Temp.: ambientDet.: UV @ 245nm

LC_0309

SSaammppllee::Inj.: 5µL custom mixConc.: approx. 20µg/mL eachDiluent: acetonitrile

CCoolluummnn:: AAlllluurree®® CC1188Cat.#: 9164565Dimensions: 150mm x 4.6mmParticle size: 5µmPore size: 60Å

CCoonnddiittiioonnss::Mobile phase: A: water


0 2010 4015 4026 8034 80

34.1 20Flow: 1.2mL/min.Temp.: ambientDet.: UV @ 220nm

PPeeaakk LLiisstt:: RReett.. TTiimmee ((mmiinn..))1. cyanazine 12.042. methabenzthiazuron 13.883. chlortoluron 14.594. secbumeton 15.745. isoproturon 16.186. diuron 16.787. linuron 22.488. flusilazole 24.299. ethofumesate 24.53

10. neburon 25.7411. pendimethalin 31.46

Herbicides on Allure® C18


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Herbicides

Phenoxyacid Herbicides on Ultra II® Aqueous C18 (LC/MS/MS)

PPeeaakkss RRTT ((mmiinn..)) MMRRMM 11 MMRRMM 221. Dicamba 1.14 219.0 → 175.0 221.0 → 177.02. Bentazon 1.32 239.0 → 132.0 239.0 → 175.03. 2,4-D 3.10 218.9 → 161.0 220.9 → 163.04. 3,5-DCBA 3.10 189.0 → 144.8 189.0 → 59.05. 4-Nitrophenol 3.10 138.1 → 108.1 138.1 → 46.06. MCPA 3.16 199.0 → 141.0 201.0 → 143.07. Dichlorprop 4.02 233.0 → 161.0 235.0 → 163.08. 2,4,5-T 4.46 252.9 → 194.9 254.9 → 196.99. Dinoseb 5.03 239.0 → 133.9 239.0 → 193.8

10. 2,4-DB 5.18 247.0 → 161.0 249.0 → 163.011. 2,4,5-TP 5.20 266.9 → 195.0 266.9 → 159.012. Acifluorfen 5.67 359.9 → 316.1 359.9 → 195.013. Pentachlorophenol 6.20 264.8 → 35.0 264.8 → 37.0

CCoolluummnn Ultra II® Aqueous C18 (cat.# 9608312)Dimensions: 100 mm x 2.1 mm IDParticle Size: 3 µmPore Size: 100 ÅTemp.: 35 °C

SSaammppllee phenoxyacid herbicidesDiluent: acetonitrileConc.: 100 ppbInj. Vol.: 10 µL

MMoobbiillee PPhhaasseeA: 10mM ammonium acetate in waterB: 10mM ammonium acetate in methanol

TTiimmee ((mmiinn..)) %%AA %%BB0 80 208 10 9012 0 100

14.8 0 10015 80 20

Flow: 0.5 mL/min.DDeetteeccttoorr Applied Biosystems/MDS Sciex LC/MS/MS

Model #: 4000 QTRAP™ LC/MS/MS SystemIon Source: ElectrosprayIon Mode: ESI-Ion Spray Voltage: -4.2 kVESI Voltage: -4.2 VGas 1: 50 psi (344.7 kPa)Gas 2: 60 psi (413.7 kPa)Source Temp.: 600 °CMode: MRM

IInnssttrruummeenntt Applied Biosystems/MDS Sciex LC/MS/MS SystemAAcckknnoowwlleeddggeemmeenntt Work performed at Applied Biosystems

LC_EV0511

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Herbicides

Phenoxyacid Herbicides on Ultra Aqueous C18

LC_EV0355

LC_EV0356

SSaammppllee::Sample: Chlorinated Acids by HPLC, Mix A (cat.# 32431),

or Chlorinated Acids by HPLC, Mix B (cat.# 32430)1,000µg/mL each component in acetonitrile

Inj.: 10µLConc.: 10ppm each analyteSample diluent: acetonitrile

CCoolluummnn:: UUllttrraa AAqquueeoouuss CC1188Cat.#: 9178565Dimensions: 150mm x 4.6mmParticle size: 5µmPore size: 100Å

CCoonnddiittiioonnss::Mobile phase: A) 0.05% H3PO4 B) acetonitrile

TTiimmee ((mmiinn..)) %%BB0 20.0

28 80.033 90.034 20.0


MMiixx AA aanndd MMiixx BB1. picloram2. chloramben3. 4-nitrophenol4. dicamba5. bentazon

2,4-dichlorophenyl aceticacid (SS) (not included)

7. 2,4-D8. MCPA9. 3,5-dichlorobenzoic acid

10. MCPP11. dichlorprop12. 2,4,5-T13. 2,4-DB14. 2,4,5-TP (Silvex)15. acifluorfen

1,4-dichlorobenzene(IS) (not included)

17. dinoseb18. pentachlorophenol

MMiixx AA aanndd MMiixx BB1. picloram2. chloramben3. 4-nitrophenol4. dicamba5. bentazon

2,4-dichlorophenyl aceticacid (SS) (not included)

7. 2,4-D8. MCPA9. 3,5-dichlorobenzoic acid

10. MCPP11. dichlorprop12. 2,4,5-T13. 2,4-DB14. 2,4,5-TP (Silvex)15. acifluorfen

1,4-dichlorobenzene(IS) (not included)

17. dinoseb18. pentachlorophenol

SSaammppllee::Sample: Chlorinated Acids by HPLC, Mix A (cat.# 32431),

or Chlorinated Acids by HPLC, Mix B (cat.# 32430)1,000µg/mL each component in acetonitrile

Inj.: 10µLConc.: 10ppm each analyteSample diluent: acetonitrile

CCoolluummnn:: AAlllluurree®® BBaassiixxCat.#: 9161565Dimensions: 150mm x 4.6mmParticle size: 5µmPore size: 60Å

CCoonnddiittiioonnss::Mobile phase: A) 0.05% H3PO4 B) acetonitrile

TTiimmee ((mmiinn..)) %%BB0 20.0

28 80.033 90.034 20.0


Phenoxyacid Herbicides on Allure® Basix

LC_EV0357

LC_EV0358


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Herbicides

PPeeaakk LLiisstt:: PPeeaakk ttiimmee (min.)1. diquat 7.52. paraquat 8.8

SSaammppllee::Inj.: 20µLConc.: 20ppm each component (above);

20µg/mL, 40µg/mL, and 100µg/mLeach component at 308nm (left) and at 257nm (right)

Sample diluent: water

CCoolluummnn:: UUllttrraa QQuuaattCat.#: 9181565Dimensions: 150mm x 4.6mmParticle size: 5µm

CCoonnddiittiioonnss::Mobile phase: Ultra Quat Reagent Solution (cat.# 32441):

acetonitrile, 95:5 (v/v)Flow: 1.0 mL/min.Temp.: 27°C Det.: UV @ 257nm (paraquat)

UV @ 308nm (diquat)

Paraquat and Diquat on Ultra Quat

min.

12

LC_0321

min.

diquat308nm paraquat

257nm

100µg/mL

40µg/mL

20µg/mL

100µg/mL

40µg/mL

20µg/mL

Paraquat and Diquat on Ultra Quat

SSaammppllee::Inj.: 10µLConc.: 5µg/mL each componentSample diluent: DI waterSample temp.: ambient

CCoolluummnn:: UUllttrraa QQuuaattCat.#: 5181352Dimensions: 50mm x 2.1mmParticle size: 3µmPore size: 100Å

CCoonnddiittiioonnss::Mobile phase: 10mM heptafluorobutyric acid:acetonitrile, 95:5 (v/v)Flow: 0.3mL/min.Temp.: ambientDet.: Applied Biosystems/MDS SCIEX API 3200™

MS/MS systemInterface: electrosprayIon Mode: positiveTemp.: 600°CIon Spray

voltage: 5,500VCollision exit

potential: 3VCurtain Gas: 15psi (103kPa)Gas supply 1: 70psi (483kPa)Gas supply 2: 60psi (414kPa)Quantitation: (MRM)Q1/Q3: unit resolutionDwell time: 200 ms

PPrreeccuurrssoorr IIoonn FFrraaggmmeenntt IIoonn DDPP CCoolllliissiioonn EEnneerrggyy((aammuu)) ((aammuu)) ((VV)) ((eeVV))

diquat, 183+ 157+ 30 30paraquat, 93 (2+) 171+ 20 20

PPeeaakk LLiisstt1. diquat2. paraquat

*Data courtesy of Houssain El Aribi, Ph.D., LC/MS Product and Application Specialist, MDS SCIEX,71 Four Valley Drive, Concord, Ontario, Canada, L4K 4V8

LC_EV0383

paraquat dichloride [CAS# 1910-42-5]

diquat dibromide[CAS # 85-00-7]

Fast, sensitive

LC/MS/MS analysis!


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Pesticides

Pesticides on Allure® C18

PPeeaakk LLiisstt::1. desisopropyl atrazine2. desethyl atrazine3. simazine4. terbuthylazine desethyl5. cyanazine6. methabenzthiazuron7. chlortoluron8. atrazine9. secbumeton

10. isoproturon11. diuron12. terbumeton13. terbuthylazine14. linuron15. flusilazole16. ethofumesate17. neburon

SSaammppllee::Inj.: 5µLConc.: approx. 10ppm each pesticideSolvent: acetonitrile

CCoolluummnn:: AAlllluurree®® CC1188Cat.#: 9164565Dimensions: 150mm x 4.6mmParticle size: 5µmPore size: 60Å

CCoonnddiittiioonnss::Mobile phase A: 20mM K2HPO4, pH 7.0


0 2010 4015 4030 70

30.1 20Flow: 1.2mL/min.Temp.: ambient Det.: UV @ 220nm

LC_0310

Diflubenzuron (Pesticide) on Ultra IBD

0 2 4 6 8 10 12 14 min.

PPeeaakk LLiisstt::1. diflubenzuron2. N,N'-bis-(chlorobenzyl)urea

SSaammppllee::Inj.: 10µLConc.: 1mg/mLSolvent: water:acetonitrile

(1:1, v/v)

CCoolluummnn:: UUllttrraa IIBBDDCat.#: 9175365Dimensions: 150mm x 4.6mmParticle size: 3µmPore size: 100Å

CCoonnddiittiioonnss::Mobile phase: water:acetonitrile

(45:55, v/v)Solvent A: 65% 0.1M ammonium

acetate pH 6.0Flow rate: 1.0mL/min.Temp.: ambientDet.: UV @ 260nm

1

2

LC_0081



Fax: 814-353-1309—24-hours a day


Outside the U.S.Contact your Restek representative:Refer to our list on pages 4-5 or visit ourwebsite at www.restek.com

Jamie Hubler, Customer Service


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PPeeaakk LLiisstt:: RReetteennttiioonn TTiimmee1. naphthalene 6.192. acenaphthylene 7.163. 1-methylnaphthalene 7.784. 2-methylnaphthalene 8.175. acenaphthene 8.466. fluorene 8.827. phenanthrene 9.648. anthracene 10.399. fluoranthene 11.22

10. pyrene 11.7511. benzo(a)anthracene 13.5512. chrysene 13.9113. benzo(j)fluoranthene 14.9214. benzo(b)fluoranthene 15.2715. benzo(k)fluoranthene 15.8216. benzo(a)pyrene 16.3517. dibenzo(a,h)anthracene 17.1018. benzo(ghi)perylene 17.6719. indeno(1,2,3-cd)pyrene 17.99

Polycyclic Aromatic Hydrocarbons on Pinnacle® II PAH

EPA 8310 – 18 component standard + benzo(j)fluoranthene

SSaammppllee::Inj.: 10µLConc.: 20µg/mL each componentSample diluent: acetonitrile

CCoolluummnn:: PPiinnnnaaccllee®® IIII PPAAHHCat.#: 9219463Dimensions: 150mm x 3.2mmParticle size: 4µmPore size: 110Å

CCoonnddiittiioonnss::Instrument: Shimadzu Prominence HPLCMobile phase: A: purified water


0 407 6016 10018.9 10019 40

Flow: 1.2mL/min.Temp.: 30°CDet.: UV @ 254nm

LC_EV0449

NEW!


Pinnacle® II PAH

1. naphthalene2. acenaphthylene3. acenaphthene4. fluorene5. phenanthrene6. anthracene7. fluoranthene8. pyrene9. benzo(a)anthracene

10. chrysene11. benzo(b)fluoranthene12. benzo(k)fluoranthene13. benzo(a)pyrene14. benzo(ghi)perylene15. dibenzo(a,h)anthracene16. indeno(1,2,3-cd)pyrene

* contaminant

SSaammppllee:: Inj.: 10µLConc.: 10µg/mL each componentSample diluent: methanol

CCoolluummnn:: PPiinnnnaaccllee®® IIII PPAAHH Cat.#: 9219463Dimensions: 150mm x 3.2mmParticle size: 4µmPore size: 110Å

CCoonnddiittiioonnss::Instrument: Shimadzu ProminenceMobile phase: A: water

B: methanolTTiimmee ((mmiinn..)) %%BB

0.0 7510.0 9022.0 100


LC_EV0480

0 2 4 6 8 10 12 14 16 18 20 22 24

1

2

*3

4

5

6

78

9

10

12

1113

1415

16

Baseline resolution of PAHs

in methanol!


718 www.restek.com 800-356-1688 or 814-353-1300



EU 256/2005 Polycyclic Aromatic Hydrocarbons

on Pinnacle® DB PAHPPeeaakk LLiisstt::

1. cyclopenta(c,d)pyrene2. benzo(a)anthracene3. chrysene4. 5-methylchrysene5. benzo(j)fluoranthene6. benzo(b)fluoranthene7. benzo(k)fluoranthene8. benzo(a)pyrene9. dibenzo(a,l)pyrene

10. dibenzo(a,h)anthracene11. benzo(ghi)perylene12. indeno(1,2,3-cd)pyrene13. dibenzo(a,e)pyrene14. dibenzo(a,i)pyrene15. dibenzo(a,h)pyrene


CCoolluummnn:: PPiinnnnaaccllee®® DDBB PPAAHHCat.#: 9470252Dimensions: 50mm x 2.1mmParticle size: 1.9µmPore size: 140Å



0 501 902 955 1007 100


LC_EV0470

min.

EPA Method 610 Polycyclic Aromatic Hydrocarbons

on Pinnacle® DB PAHPPeeaakk LLiisstt::

1. naphthalene2. acenaphthylene3. 1-methylnaphthalene4. 2-methylnaphthalene5. acenaphthene6. fluorene7. phenanthrene8. anthracene9. fluoranthene

10. pyrene11. benzo(a)anthracene12. chrysene13. benzo(b)fluoranthene14. benzo(k)fluoranthene15. benzo(a)pyrene16. dibenzo(a,h)anthracene17. benzo(ghi)perylene18. indeno(1,2,3-cd)pyrene


CCoolluummnn:: PPiinnnnaaccllee®® DDBB PPAAHHCat.#: 9470252Dimensions: 50mm x 2.1mmParticle size: 1.9µmPore size: 140Å



0 501 603 1005 100


LC_EV0469


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HPLC CHROMATOGRAMS | FOODS & FLAVORS

Food Contaminants

Carbamate Pesticides on Ultra II® Carbamate (LC/MS/MS)

Time (min.)0.0 1.0 2.0 3.0 4.0 5.0 6.0 7.0 8.0 9.0 10.0

PPeeaakkss RRTT ((mmiinn..)) TTrraannssiittiioonn 11 TTrraannssiittiioonn 221. Aldicarb sulfone 1.9 223.1 → 86.1 223.1 → 148.02. Aldicarb sulfoxide 2.2 207.1 → 132.1 207.1 → 89.13. Oxamyl 2.4 237.1 → 72.1 237.1 → 90.14. Methomyl 2.6 163.1 → 88.1 163.1 → 106.05. 3-Hydroxycarbofuran 3.5 238.1 → 163.1 238.1 → 181.26. Aldicarb 4.5 208.1 → 116.0 208.1 → 88.97. Propoxur 5.1 210.1 → 111.0 210.1 → 168.18. Carbofuran 5.3 222.1 → 165.2 222.1 → 123.09. Carbaryl 5.8 202.1 → 145.1 202.1 → 127.1

10. Methiocarb 7.0 226.1 → 169.2 226.1 → 121.0

1

2

3

4

5 6

7

8

9

10

LC_EV0510

CCoolluummnn Ultra II® Carbamate (cat.# 9611312)Dimensions: 100 mm x 2.1 mm IDParticle Size: 3 µmPore Size: 100 ÅTemp.: 35 °C

SSaammppllee 531.1 Carbamate Pesticide Calibration Mixture (cat.# 32273)

Diluent: acetonitrileConc.: 100 ppb each pesticideInj. Vol.: 5 µL

MMoobbiillee PPhhaasseeA: 10 mM NH4OAc in waterB: 10 mM NH4OAc in methanol

TTiimmee ((mmiinn..)) %%BB0 101 108 9010 9011 10

Flow: 0.5 mL/min.

IInnssttrruummeenntt Applied Biosystems/MDS Sciex LC/MS/MS SystemDDeetteeccttoorr Applied Biosystems/MDS Sciex LC/MS/MSModel #: 4000 QTRAP™ LC/MS/MS systemIon Source: TurboIonSpray®

Ion Mode: ESI+Ion Spray Voltage: 5 kVGas 1: 40 psi (275.8 kPa)Gas 2: 60 psi (413.7 kPa)Source Temp.: 500 °C

NEW!

Carbamates in Orange Oil on Ultra Carbamate (LC-TOFMS)

PPeeaakk LLiisstt::1. aldicarb sulfone2. aldicarb sulfoxide3. oxamyl4. methomyl5. 3-hydroxycarbofuran6. aldicarb7. propoxur8. carbofuran9. carbaryl

10. methiocarb11. BDMC (IS)

SSaammppllee:: 531.1 Carbamate Pesticide Calibration Mix (cat.# 32273) and Internal Standard 4-bromo-3,5-dimethylphenyl-N-methylcarbamate (cat.# 32274) 50:50 spiked into unprocessed orange oil at 10ppm

Inj.: 3µLConc.: 10ppmSample diluent: methanolMatrix: orange oil

CCoolluummnn:: UUllttrraa CCaarrbbaammaatteeCat. #: 9177352Dimensions: 50mm x 2.1mmParticle size: 3µmPore size: 100Å

CCoonnddiittiioonnss::Mobile phase: A: 2mM ammonium acetate:methanol, 90:10

B: 2mM ammonium acetate:methanol, 10:90TTiimmee ((mmiinn..)) %%BB

0 2020 10025 100

Flow: 200µL/min.Temp.: ambientDet.: LECO Unique® LC-TOFMSInterface: ESIIon mode: PositiveTemp.: 130°C Nebulizer pressure: 100kPaDesolvation gas (N2): 4,000cc/min.Interface temperature: 120°CNozzle: (+) 62VCapillary: (+) 2.75kV

LC_FF0472


720 www.restek.com 800-356-1688 or 814-353-1300


Food Contaminants

LC_EV0479A

PPeeaakk LLiisstt::CCoommppoouunndd PPoollaarriittyy MMooll.. WWtt.. RRTT ((mmiinn..)) TTrraannssiittiioonn 11methamidophos positive 141.13 0.45 142.0 → 94.0acephate positive 183.17 0.62 184.0 → 142.8bentazone negative 240.28 0.77 239.0 → 131.8omethoate positive 213.14 1.07 214.0 → 124.9bromoxynil negative 276.91 1.32 275.9 → 80.8butoxycarboxin positive 222.27 1.64 223.1 → 86.1aldicarb sulfoxide positive 206.26 2.03 207.1 → 132.1methomyl positive 162.21 2.08 163.1 → 88.1Ioxynil negative 370.92 2.46 369.8 → 126.7thiamethoxam positive 291.7 2.7 292.0 → 211.0monocrotophos positive 223.17 2.73 224.1 → 127.0dimethoate positive 229.26 2.9 230.1 → 199.0fenuron positive 164.21 3.1 165.1 → 72.1dioxacarb positive 223.23 3.12 224.0 → 123.0dicrotophos positive 237.19 3.28 238.0 → 112.0vamidothion positive 287.34 3.45 288.0 → 146.0carbendazim positive 191.19 3.73 192.0 → 160.0aldicarb positive 190.27 3.73 208.1 → 116.0formetanate positive 221.26 3.74 222.1 → 165.2 acetamiprid positive 222.67 3.95 223.1 → 126.1carbetamide positive 236.27 3.99 237.0 → 192.0oxamyl positive 219.26 3.99 237.1 → 72.2 aminocarb positive 208.26 4.11, 4.44 209.2 → 137.1propoxur positive 209.24 4.15 210.1 → 111.0oxadixyl positive 278.31 4.21 279.0 → 219.0bendiocarb positive 223.23 4.24 224.1 → 109.1thiacloprid positive 252.71 4.25 253.2 → 126.1thiophanate methyl positive 342.4 4.3 343.0 → 151.0methabenzhiazuron positive 221.28 4.31 222.0 → 165.1tricyclazole positive 189.23 4.35 190.0 → 163.0pyracarbolid positive 217.27 4.38 218.2 → 125.0propamocarb positive 188.27 4.41 189.2 → 102.2 carboxin positive 235.3 4.51 236.0 → 143.0ethiofencarb positive 225.31 4.52 226.1 → 106.9carbaryl positive 201.22 4.58 202.1 → 145.1thiabendazole positive 201.25 4.6 202.0 → 175.0carbanilide positive 212.25 4.6 213.1 → 94.0clethodim positive 359.91 4.61 360.0 → 164.0tebuthiuron positive 228.32 4.68 229.2 → 172.4

CCoommppoouunndd PPoollaarriittyy MMooll.. WWtt.. RRTT ((mmiinn..)) TTrraannssiittiioonn 11fluometuron positive 232.21 4.75 233.1 → 72.0metobromuron positive 259.1 4.82 259.0 → 170.2flutriafol positive 301.3 4.84 302.0 → 123.0chlortoluron positive 212.68 4.92 213.1 → 72.2simetryn positive 213.31 4.96 214.0 → 124.0pirimicarb positive 238.29 4.97 239.2 → 72.1forchlorfenuron positive 247.68 5.04 248.0 → 129.1siduron positive 232.32 5.09 233.3 → 137.2ethofumesate positive 286.35 5.11 304.0 → 121.0cycluron positive 198.31 5.13 199.1 → 89.1diuron positive 233.1 5.13 233.1 → 72.0diethofencarb positive 267.33 5.15 268.0 → 226.0furalaxyl positive 301.34 5.18 302.2 → 95.0methiocarb positive 225.31 5.24 226.1 → 169.2secbumeton positive 225.29 5.24 226.2 → 169.9terbumeton positive 225.29 5.25 226.2 → 169.9prometon positive 225.29 5.26 226.2 → 142.3paclobutrazol positive 293.8 5.26 294.0 → 70.0promecarb positive 207.27 5.27 208.2 → 109.2dimoxystrobin positive 326.39 5.27 327.1 → 205.0ametryn positive 227.33 5.29 228.2 → 186.2methoprotryne positive 271.39 5.32 272.2 → 240.2triadimefon positive 293.75 5.32 294.0 → 197.0mexacarbate positive 222.28 5.34 223.2 → 166.2fludioxinil negative 248.19 5.34 247.0 → 179.9boscalid negative 343.21 5.36 343.0 → 307azoxystrobin positive 403.3 5.36 404.1 → 372.1methoxyfenozide positive 368.47 5.38 369.0 → 149.0cyproconazole positive 291.78 5.39 292.2 → 70.2prothioconazole negative 344.26 5.41 341.9 → 305.8flufenacet positive 363.34 5.46 364.0 → 152.0butafenacil positive 474.82 5.47 492.2 → 331.1myclobutanil positive 288.78 5.51 289.0 → 70.0dimethomorph positive 387.86 5.52, 5.54 388.0 → 301.0bromuconazole 47 positive 377.06 5.54 378.0 → 159.0prometryn positive 241.36 5.55 242.2 → 158.1fipronil negative 437.15 5.56 434.9 → 329.8triticonazole positive 317.81 5.58 318.0 → 70.0tetraconazole positive 372.12 5.6 372.0 → 159.0uniconazole positive 291.78 5.62 292.2 → 70.2fluoxastrobin positive 458.83 5.62 459.2 → 427.2cyazofamid positive 324.78 5.63 325.0 → 108.0terbutryn positive 241.36 5.65 242.2 → 186.0tebufenozide positive 352.47 5.65 353.1 → 133.1chloroxuron positive 290.75 5.67 291.0 → 72.0picoxystrobin positive 367.25 5.67 368.0 → 145.0carfentrazone-ethyl positive 412.17 5.69 412.0 → 346.0diclobutrazol positive 328.21 5.71 328.0 → 70.0fenoxycarb positive 301.34 5.72 302.0 → 88.1diflubenzuron positive 310.67 5.72 311.2 → 158.1neburon positive 275.18 5.74 275.0 → 88.0flusiazole positive 315.4 5.76 316.0 → 247.0epoxiconazole positive 329.76 5.76 330.0 → 121.0fenbuconazole positive 336.82 5.76 337.0 → 125.0bupirimate positive 316.41 5.77 317.0 → 166.0zoxamide positive 336.54 5.77 336.2 → 187.1rotenone positive 394.42 5.79 395.0 → 213.0benalaxyl positive 325.41 5.83 326.0 → 148.0tebuconazole positive 307.82 5.84 308.0 → 70.0penconazole positive 284.19 5.93 284.0 → 159.0cyprodinil positive 225.29 5.96 226.0 → 93.0propiconazole positive 342.22 5.96 342.0 → 159.0alanycarb positive 399.52 5.98 400.1 → 238.2triflumuron positive 358.68 5.99 359.1 → 156.1thiobencarb positive 257.78 6 258.1 → 125.0pyraclostrobin positive 387.83 6 388.0 → 194.0benzoximate positive 363.8 6.01 364.0 → 199.0pinoxaden positive 400.52 6.01 401.3 → 317.2clofentezine positive 303.15 6.11 303.0 → 138.0trifloxystrobin positive 408.38 6.12 409.2 → 186.0prochloraz positive 376.67 6.21 376.0 → 308.0difenoconazole positive 406.28 6.29 406.0 → 251.0benfuracarb positive 410.53 6.29 411.2 → 195.1triflumizole positive 345.75 6.38 346.1 → 278.1buprofezin positive 305.44 6.4 306.0 → 201.0piperonyl butoxide positive 338.45 6.42 356.2 → 177.2pyriproxyfen positive 321.28 6.52 322.0 → 96.0propargite positive 350.48 6.68 368.0 → 231.0etoxazole positive 359.42 6.87 360.1 → 141.0amitraz positive 293.41 6.89 294.2 → 163.3noviflumuron negative 529.1 7.08 527.1 → 343.8pyridaben positive 364.94 7.18 365.0 → 147.0fenpyroximate positive 421.5 7.2 422.0 → 366.0fenpropimorph positive 303.49 7.38 304.0 → 147.0spiroxamine positive 297.48 7.63, 7.81 298.0 → 144.0spinosyn A positive 731.97 8.37 732.6 → 142.2

Pesticides on Pinnacle® DB Aqueous C18 (LC/MS/MS, ESI+)

SSaammppllee:: multicomponent pesticide standard

Inj.: 5µLConc.: 33.3ppb each pesticide Sample diluent: acetonitrile

CCoolluummnn:: Pinnacle® DB Aqueous C18 Cat.#: 9418252Dimensions: 50mm x 2.1mmParticle size: 1.9µmPore size: 140Å

CCoonnddiittiioonnss::Mobile phase: A: 10mM NH4OAc in water

B: 10mM NH4OAc in methanol

TTiimmee ((mmiinn..)) %%BB0.0 101.0 108.0 90

10.0 9011.0 10

Flow: 600µL/min.Temp.: 35°C Instrument: Shimadzu Prominence® UFLCXRDet.: Applied Biosystems 4000 QTRAP®

LC/MS/MS systemIon Source: TurboIonSpray®, ESI+IonSpray Voltage, ESI voltage: 5kV (ESI+)Gas 1: 40psiGas 2: 60psiSource Temp.: 500°C; max pressure ~7,200psi

NEW!


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Food Contaminants

Sample: multicomponent pesticide standard Inj.: 10µLConc.: 1ppb each pesticide Sample diluent: acetonitrile

Column: Ultra Aqueous C18 Cat. #: 9178312Dimensions: 100mm x 2.1mmParticle size: 3µmPore size: 100Å

Conditions:Instrument: Shimadzu Prominence® UFLCXRMobile phase: A: 10 mM NH4OAc in water

B: 10 mM NH4OAc in methanol

TTiimmee ((mmiinn..)) %%BB0.0 208.0 90

12.0 10014.8 10014.9 20

Flow: 500µL/minTemp.: 35°C

Det.: Applied Biosystems 4000 QTRAP® LC/MS/MS systemIon Source: TurboIonSpray®

A & C: ESI+B: ESI-

IonSpray Voltage: 5kV (ESI+), -4.2kV (ESI-)Gas 1: 50psiGas 2: 60psiSource Temp.: 600°C

Pesticides on

Ultra Aqueous C18 (LC/MS/MS)

1.0 2.0 3.0 4.0 5.0 6.0 7.0 8.0 9.0 10.0 11.0 12.0 13.0 14.0 15.0

Time (min.)

0.0

1.0 2.0 3.0 4.0 5.0 6.0 7.0 8.0 9.0 10.0 11.0 12.0 13.0 14.0 15.0

Time, min

0.0

1.0 2.0 3.0 4.0 5.0 6.0 7.0 8.0 9.0 10.0 11.0 12.0 13.0 14.0

Time (min.)

0.0

A: Pesticides in positive ion mode

B: Pesticides in negative ion mode

C: Improved retention of difficultpesticides in positive ion mode

LC_FF0490A

LC_FF0490

LC_FF0490B

met

ham

idop

hos

acep

hate

omet

hoat

e

prop

amoc

arb

NEW!

Visit www.restek.com/cat005 toview our "Comprehensive PesticideResidue Analysis by LC/MS/MS Using anUltra Aqueous C18 Column" article(contains compound identificationsand MS details).

formoreinfo


722 www.restek.com 800-356-1688 or 814-353-1300


Food Contaminants

SSaammppllee::Inj.: 20µL, mixture of Sudan I, Sudan II, Sudan III, Sudan IVConc.: 20µg/mL each componentSample diluent: methanol


CCoonnddiittiioonnss::Mobile phase: methanol:water, 97:3Flow: 1mL/min.Temp.: ambientDet.: UV @ 476/493/512/357nm (left) or UV @ 488/520nm (right)

Sudan Dyes on Ultra Aqueous C18

1. Sudan I2. Sudan II3. Sudan III4. Sudan IV

LC_FF0326 LC_FF0327

Fixed Dual Wavelength

Detector

wa

ve

len

gth

ch

an

ge

Photodiode Array

Detector

Monitor Sudan I, II, III, and IV

in a single, isocratic analysis!

Pesticides on Pinnacle® DB Aqueous C18 (LC/MS/MS, ESI-)

LC_FF0479B

SSaammppllee:: multicomponent pesticide standard

Inj.: 5µLConc.: 33.3ppb each pesticide Sample diluent: acetonitrile

CCoolluummnn:: Pinnacle® DB Aqueous C18 Cat.#: 9418252Dimensions: 50mm x 2.1mmParticle size: 1.9µmPore size: 140Å

CCoonnddiittiioonnss::Mobile phase: A: 10 mM NH4OAc in water

B: 10 mM NH4OAc in methanol

TTiimmee ((mmiinn..)) %%BB0.0 101.0 108.0 9010.0 9011.0 10

Flow: 600µL/minTemp.: 35°C Instrument: Shimadzu Prominence® UFLCXRDet.: Applied Biosystems 4000 QTRAP® LC/MS/MS system

Ion Source: TurboIonSpray®, ESI-IonSpray Voltage, ESI voltage: -4.2kV (ESI-)Gas 1: 40psiGas 2: 60psiSource Temp.: 500°C; max pressure ~7,200psi

PPeeaakk LLiisstt::CCoommppoouunndd PPoollaarriittyy MMooll.. WWtt.. RRTT ((mmiinn..)) TTrraannssiittiioonn 11bentazone negative 240.28 0.77 239.0 → 131.8bromoxynil negative 276.91 1.32 275.9 → 80.8Ioxynil negative 370.92 2.46 369.8 → 126.7fludioxinil negative 248.19 5.34 247.0 → 179.9boscalid negative 343.21 5.36 343.0 → 307prothioconazole negative 344.26 5.41 341.9 → 305.8fipronil negative 437.15 5.56 434.9 → 329.8noviflumuron negative 529.1 7.08 527.1 → 343.8

NEW!


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Drug Residues

Nonsteroidal Anti-inflammatory Drugs (NSAIDs)

Ultra II® Biphenyl

LC_PH0487


CCoolluummnn:: Ultra II® Biphenyl Cat.#: 9609853Dimensions: 50mm x 3.0mmParticle size: 2.2µmPore size: 100Å

CCoonnddiittiioonnss::Instrument: Shimadzu Prominence UFLCXRMobile phase: 20mM potassium phosphate,

pH 2.5 with H3PO4:methanol (30:70)


Peak List Ret. Time (min.)1. ketoprofen 0.8942. piroxicam 1.0683. sulindac 1.1974. diclofenac 1.465

NEW!

High organic

(60% acetonitrile) means

better LC/MS sensitivity!

SSaammppllee::Inj.: 5µLConc.: ~50µg/mL each componentSample diluent: mobile phase

CCoolluummnn:: AAlllluurree®® PPFFPP PPrrooppyyllCat.#: 9169565Dimensions: 150mm x 4.6mmParticle size: 5µmPore size: 60Å

CCoonnddiittiioonnss::Mobile phase: 10mM potassium phosphate

monobasic (pH 2.5): acetonitrile, 40:60 (v/v)


PPeeaakk LLiisstt::1. norfloxacin2. levofloxacin3. ciprofloxacin4. lomefloxacin5. enrofloxacin6. sparfloxacin

LC_PH0420

Antibiotic Fluoroquinolones on Allure® PFP Propyl

For more information on Biphenyl columns, visitwww.restek/biphenyl


724 www.restek.com 800-356-1688 or 814-353-1300


Drug Residues

PPeeaakk LLiisstt:: CCoonncc.. ((ppppbb)) TTiimmee ((mmiinn))1. d5-AMOZ 0.3 3.72. AMOZ 0.3 3.83. AHD 0.3 5.464. d4-AOZ 0.3 5.495. AOZ 0.3 5.516. SC 0.3 5.6


CCoonnddiittiioonnss::Mobile phase: A: 0.05% formic acid in methanol

B: 0.05% formic acid – 5 mM NH4 formate in waterTTiimmee ((mmiinn)) %%BB

0 902.5 905 10

10 1012 9015 90

Flow: 200µL/min.Temp.: 30°CDet.: MS/MS triple quadrupoles (Thermo Scientific Discovery)

AAnnaallyyzzeerr PPaarraammeetteerrss::Ion source: ESI (electrospray ionization)Only segment: 15 min. Polarity: positiveData type: centroidScan mode: SRM productScan width (m/z): 0.7Scan time (s): 0.25Peak width: Q1: within 0.7

Q2: 0.7Collision gaspressure (mTorr): 1.5 (argon)Divert valve: active, with 3 positions

Positions-1° 2 min., 2° 8 min., 3° 5 min.

AAnnaallyyttee PPrreecc.. IIoonn PPrroodd.. IIoonn CCoolllliissiioonn EE TTuubbee LLeennssAOZ 236 134 12 V 120AMOZ 335 291 10 V 100SC 209 166 12 V 80AHD 249 134 12 V 110

AMOZ = 3-amino-5-morpholinomethyl-2-oxazolidinoneAHD = 1-aminohydantoin hydrochlorideAOZ = 3-amino-2-oxazolidinoneSC = semicarbazide

Nitrofuran Metabolites on Ultra C18 (LC/MS/MS)

LC_0323

d5-AMOZ

AMOZ

AHD

d4-AOZ

AOZ

SC

for more infoVisit www.restek.com/cat004 to view our "Analysis of Nitrofuransin Honey Using LC/MS/MS and an Ultra C18 Column" article.


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Drug Residues


CCoolluummnn:: Ultra II® Biphenyl Cat.#: 9609853Dimensions: 50mm x 3.0mmParticle size: 2.2µmPore size: 100Å

CCoonnddiittiioonnss::Instrument: Shimadzu Prominence UFLCXRMobile phase: 0.1% formic acid

in water:methanol (75:25)Time (min.) %B

0 253.5 65


PPeeaakk LLiisstt RReett.. TTiimmee ((mmiinn..))1. sulfadiazine 1.4962 sulfathiazole 1.6633. sulfamerazine 1.9974. sulfamethoxazole 2.3815. sulfamethazine 2.5236. sulfachlorpyridizine 2.6517. sulfamethoxine 3.228

Sulfa Drugs

Ultra II® Biphenyl

LC_PH0489

NEW!

SSaammppllee:: milk spiked at 200ppb with sulfonamides, extracted with Q-sep™ Q110 QuEChERSextraction tube (cat.# 26213), and cleaned up with Q-sep™ Q211 QuEChERS dSPEclean-up tube (cat.# 26216), then concentrated.

Inj.: 10µLConc.: 4µg/mLSample diluent: 0.2% formic acid

CCoolluummnn:: Pinnacle® DB BiphenylCat. #: 9409312Dimensions: 100mm x 2.1mmParticle size: 3µmPore size: 140Å

CCoonnddiittiioonnss::Instrument: Agilent 1100 with LECO Unique® LC-TOFMSMobile phase: A: 0.2% formic acid

B: methanol:acetonitrile (80:20), with 0.2% formic acidTime (min.) %B

0 1520 10030 100

Flow: 1mL/min. with preinjection split delivering 0.2mL/min. to columnTemp.: ambientDet.: LECO Unique® LC-TOFMSInterface: ESIIon mode: positiveTemp.: 120°C Capillary: 3.8kVCone: 50VDesolvation gas: 4L/min.Collected: 200-1,000 m/z

Compound [M+H]+

1. sulfadiazine 2512. sulfathiazole 2563. sulfamerazine 2654. sulfamethazine 2795. sulfamethoxypyridazine 2816. sulfamethoxazole 2547. sulfachloropyridazine 2858. sulfadimethoxine 3119. sulfaquinoxaline 301

Sulfonamides in Milk on Pinnacle® DB Biphenyl (LC-TOFMS)

LC_FF0502

NEW!


726 www.restek.com 800-356-1688 or 814-353-1300


Preservatives

Carboxylic Acids on Ultra Aqueous C18

PPeeaakk LLiisstt:: CCoonncc.. ((µµgg//mmLL))::1. malonic acid 5002. lactic acid 5003. acetic acid 1,0004. citric acid 1,0005. succinic acid 2,0006. fumaric acid 10

SSaammppllee::Inj.: 10µLSolvent: water

CCoolluummnn:: UUllttrraa AAqquueeoouuss CC1188Cat.#: 9178565 Dimensions: 150mm x 4.6mmParticle size: 5µmPore size: 100Å

CCoonnddiittiioonnss::Mobile phase: 50mM potassium

phosphate, pH 2.5: acetonitrile (99:1)


LC_0140

1

2

3

4

5

6

0 1 2 3 4 min.

LC_0297

Carboxylic Acids (Pyruvic and Lactic) on

Ultra Aqueous C18

CCoonncc..PPeeaakk LLiisstt:: ((mmgg//mmLL))

1. pyruvic acid 52. lactic acid 50

SSaammppllee::Inj.: 5µLSolvent: 50mM potassium

phosphate, pH 2.5

CCoolluummnn:: UUllttrraa AAqquueeoouuss CC1188Cat.#: 9178565 Dimensions: 150mm x 4.6mmParticle size: 5µmPore size: 100Å


phosphate, pH 2.5Flow: 1.0mL/min.Temp.: 26°CDet.: UV @ 210nm

restekinnovation!Excellent peak symmetry in100% aqueous mobile phase!

Innovative

food solutions

at your fingertips!Visit Restek’s new website at

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Preservatives, Sugars

LC_0198

1

2

3

4

0 2 4 6 8 10 12 14 16 18 min.

Phenolic Antioxidants on Pinnacle® II C18

PPeeaakk LLiisstt:: CCoonncc.. ((ppppmm))1. propyl gallate 1682. TBHQ 1823. 2-BHA + 3-BHA 1974. BHT 193

SSaammppllee::Inj.: 10µLSolvent: methanol

CCoolluummnn:: PPiinnnnaaccllee®® IIII CC1188Cat.#: 9214565 Dimensions: 150mm x 4.6mmParticle size: 5µmPore size: 110Å

CCoonnddiittiioonnss::Mobile phase: A: 1% acetic acid

B: methanolTTiimmee BB((mmiinn..)) ((%%))

0 504 50

10 9025 9026 50

Flow: 1.0mL/min.Temp.: 30°C Det.: UV @ 280nm

PPeeaakk LLiisstt:: CCoonncc.. ((mmgg//mmLL))1. fructose 2.02. glucose 2.13. sucrose 4.04. maltose 4.55. lactose 4.4

LC_0223

Sugars on Pinnacle® II Amino (3μm)

CCoolluummnn:: PPiinnnnaaccllee®® IIII AAmmiinnooCat.#: 9217365Dimensions: 150mm x 4.6mm Particle size: 3µmPore size: 110Å

CCoonnddiittiioonnss::Mobile phase: water:acetonitrile (25:75, v/v)Flow: 1.5mL/min.Temp.: 35°C Det.: refractive index @ 35°C

SSaammppllee::Inj.: 5µLSolvent: mobile phase

LC_0252

Vanilla Bean Extract on Pinnacle® DB C18

(Fast LC)

PPeeaakk LLiisstt RReett.. TTiimmee ((mmiinn..))1. vanillin 2.00

CCoolluummnn:: PPiinnnnaaccllee®® DDBB CC1188Cat.#: 9414555Dimensions: 50mm x 4.6mmParticle size: 5µmPore size: 140Å

CCoonnddiittiioonnss::Mobile phase: 0.2% v/v phosphoric acid in

water:methanol (80:20 v/v)Flow: 2mL/min.Temp.: 27°C Det.: UV @ 254nm

SSaammppllee::Inj.: 5µLConc.: 20% v/v

commercial extract in water




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Flavor Compounds

SSaammppllee:: Inj.: 10mLConc.: 5% solution of

vanilla extractSolvent: 40% ethanol


CCoonnddiittiioonnss::Mobile phases: A: 1.2% acetic acid in water

B: methanolTTiimmee ((mmiinn..)) %% BB

0.0 20.05.0 20.0

15.0 40.020.0 40.025.0 20.0


PPeeaakk LLiisstt::1. vanillin

Vanillin on Ultra C8

LC_0149

1

0 2 4 6 8 10 12 14 16 18 min.

Vanillin and Ethyl Vanillin on Ultra C8


CCoonnddiittiioonnss::Mobile phases: A: 1.2% acetic acid

B: methanolTTiimmee ((mmiinn..)) %%BB

0.0 20.05.0 20.0

15.0 40.020.0 40.025.0 20.0


0 2 4 6 8 10 12 14 16 18 min.

2

1

PPeeaakk LLiisstt:: CCoonncc.. ((mmgg//mmLL))1. vanillin 0.122. ethyl vanillin 0.04

SSaammppllee::Inj.: 10µLSolvent: 40% ethanol

LC_0148

0 1 2 3 4 5 6 7 min.

1

LC_0181

Black Pepper: Piperine on Pinnacle® II Cyano

PPeeaakk LLiisstt::1. piperine

SSaammppllee::Inj.: 5µLConc.: 100µg/mLSolvent: methanol

CCoolluummnn:: PPiinnnnaaccllee®® IIII CCyyaannooCat.#: 9216565Dimensions: 150mm x 4.6mmParticle size: 5µmPore size: 110Å

CCoonnddiittiioonnss::Mobile phase: water:acetonitrile (50:50 v/v)Flow: 1.0mL/min.Temp.: ambient Det.: UV/Vis @ 345nm

Capsaicinoids: Heat Level Assay for

Habañero Nuggets on Pinnacle® II C18

CCoolluummnn:: PPiinnnnaaccllee®® IIII CC1188Cat.#: 9214565Dimensions: 150mm x 4.6mmParticle size: 5µmPore size: 110Å

CCoonnddiittiioonnss::Mobile phase: A: 1% acetic acid in water (v/v)

B: acetonitrileTTiimmee ((mmiinn..)) %% BB

0 502 509 80

12 8013 50


PPeeaakk LLiisstt::1. ethanol2. unknown3. capsaicin4. dihydrocapsaicin

SSaammppllee::Inj.: 10µL habañero nugget extractConc.: 0.8g sample in 200mLSolvent: ethanol

LC_0160


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Dietary Supplements

Organic Acids

Ultra II® Aqueous C18Peak List Ret. Time (min.)

1. tartaric acid 2.0612. quinic acid 2.2103. malic acid 2.5964. citric acid 4.1775. fumaric acid 5.853

SSaammppllee:: Inj.: 5µLConc.: 10µg/mL fumaric acid,

2,000µg/mL each other acidsSample diluent: water

CCoolluummnn:: Ultra II® Aqueous C18Cat.#: 9608565Dimensions: 150mm x 4.6mmParticle size: 5µmPore size: 100Å

CCoonnddiittiioonnss::Instrument: Shimadzu Prominence UFLCXRMobile phase: 100% 20mM potassium phosphate (pH2.5) Flow: 1.0mL/min.Temp.: 30°CDet.: UV @ 226nm

LC_PH0498

NEW!

SSaammppllee:: Inj.: 1µLConc.: 100µg/mL Sample diluent: water:methanol (60:40)


CCoonnddiittiioonnss::Instrument: Shimadzu Prominence UFLCXRMobile phase: water:methanol (60:40)Flow: 2.0mL/min.Temp.: 40°CDet.: UV @ 222nmPressure: 240bar

LC_PH0506

Melatonin

Ultra II® Aqueous C18

Peak List Ret. Time (min.)1. melatonin 3.117

NEW!


730 www.restek.com 800-356-1688 or 814-353-1300


Dietary Supplements

LC_0174

0 2 4 6 8 min.

1

Allicin in Garlic Tablets on Pinnacle® II C18

CCoolluummnn:: PPiinnnnaaccllee®® IIII CC1188Cat.#: 9214565Dimensions: 150mm x 4.6mmParticle size: 5µmPore size: 110Å

CCoonnddiittiioonnss::Mobile phase: water:methanol

(50:50 v/v)Flow: 0.8mL/min.Temp.: 30°C Det.: UV @ 240nm

Phenethyl Glucosinolate on Ultra Aqueous C18

SSaammppllee::Inj.: 10µLConc.: 1,000µg/mLSolvent: water


CCoonnddiittiioonnss::Mobile phase: A: 50mM potassium

phosphate, pH 2.5B: acetonitrileTTiimmee ((mmiinn..)):: %% BB

0.0 010 7511 016 0


PPeeaakk LLiisstt::1. phenethyl glucosinolate

LC_0166

SSaammppllee::Inj.: 20µLConc.: 1.2mg/mL

garlic tablet in waterSolvent: deionized water

PPeeaakk LLiisstt::1. allicin

Phenolics in Echinacea on Pinnacle® II C18

LC_0195

CCoolluummnn:: PPiinnnnaaccllee®® IIII CC1188Cat.#: 9214565 Dimensions: 150mm x 4.6mmParticle size: 5µmPore size: 110Å

CCoonnddiittiioonnss::Mobile phase: A: 0.1% phosphoric acid


0 1013 2214 4014.5 4015 1020 10


PPeeaakk LLiisstt::1. caftaric acid2. chlorogenic acid3. echinacoside4. cichoric acid

SSaammppllee::Inj.: 10µLConc.: 6.7mg/mL Echinacea capsule

contents in sample diluentSolvent: ethanol:water (70:30, v/v)Sample temp.: 25°C

0 2 4 6 8 10 12 14 min.

1

2

4

3

LC_0197

Tocopherols in Soy Oil on Pinnacle® II Silica

PPeeaakk LLiisstt::1. α-tocopherol2. β-tocopherol3. γ-tocopherol4. δ-tocopherol

SSaammppllee::Inj.: 10µLConc.: approx. 1.25% soy oilSolvent: hexane

CCoolluummnn:: PPiinnnnaaccllee®® IIII SSiilliiccaaCat.#: 9210565 Dimensions: 150mm x 4.6mmParticle size: 5µmPore size: 110Å

CCoonnddiittiioonnss::Mobile phase: isopropyl alcohol:hexane

(0.5:99.5)Flow: 0.6mL/min.Temp.: 30°C Det.: UV @ 295nm


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Vitamins & Dietary Supplements

LC_CF0492

SSaammppllee:: Inj.: 20µLConc.: extracted serum sample

CCoolluummnn:: UUllttrraa AAqquueeoouuss CC1188 Cat.#: 9178352Dimensions: 50mm x 2.1mmParticle size: 3µmPore size: 100Å

CCoonnddiittiioonnss::Instrument: Shimadzu Prominence® UFLCXRMobile phase: A: 0.1% formic acid in water

B: 0.1% formic acid in methanolTTiimmee ((mmiinn..)) %%BB0.00 502.5 1003.5 1003.6 505.00 50

Flow: 700µL/min.Temp.: 40°CDet.: Applied Biosystems 3200 QTRAP™ LC/MS/MS systemIon source: TurboIonSpray®, APCI+Mode: MRMDwell time: 100msec.

DDeecclluusstteerriinngg RReett.. TTiimmeeCCoommppoouunndd QQ11 QQ33 ppootteennttiiaall ((VV)) ((mmiinn..))d6-25-OH D3 (IS) 389.3 211.2 68 3.0025-OH D3 383.3 211.2 68 3.0025-OH D2 395.3 229.2 55 3.0425-OH D3 383.3 229.2 68 3.0025-OH D2 395.3 269.2 55 3.0425-OH D2 395.3 119.0 55 3.04

Vitamin D on

Ultra Aqueous C18 (LC/MS/MS) NEW!

for more infoVisit www.restek.com/cat003 to view our "5 Minute Analysisof Vitamin D in Serum by LC/MS/MS" article.


732 www.restek.com 800-356-1688 or 814-353-1300



PPeeaakk LLiisstt:: CCoonncc.. ((mmgg//mmLL))1. solvent front n/a2. menadione (vitamin K3) 0.453. all-trans-retinol (vitamin A) 0.344. vitamin D3 0.45. unknown n/a6. α tocopherol (vitamin E) 2.47. α tocopherol acetate

(vitamin E acetate) 2.48. unknown n/a9. phylloquinone (vitamin K1) 0.84

Vitamins (Fat Soluble) on Ultra C18

CCoolluummnn:: UUllttrraa CC1188Cat.#: 9174575 Dimensions: 250mm x 4.6mmParticle size: 5µmPore size: 100Å

CCoonnddiittiioonnss::Mobile phase: acetonitrile:methanol

(90:10, v/v)TTiimmee ((mmiinn..)) FFllooww ((mmLL//mmiinn..))

1.00 1.005.00 1.005.01 2.00

50.0 2.00Temp.: 30°CDet.: UV @ 280nm

1

2

3

4

5

67

8

9

0 10 20 30 40 min.LC_0144

SSaammppllee:: Solvent: diethyl ether

SSaammppllee::Inj.: 1.0µLSolvent: mobile phase

CCoolluummnn:: UUllttrraa IIBBDDCat.#: 9175565 Dimensions: 150mm x 4.6mmParticle size: 5µmPore size: 100Å


phosphate, pH 2.5Flow: 1.0mL/min.Temp.: ambientDet.: UV @ 254nm

LC_0227

Vitamins Thiamin (Vitamin B1) and Ascorbic Acid

(Vitamin C) on Ultra IBD

PPeeaakk LLiisstt:: CCoonncc.. ((mmgg//mmLL))1. thiamin 2.52. ascorbic acid 2.5

For more information on dietary supplements, visit

www.restek.com/dietary

Restek is your Complete Source for

Analyzing Pesticides in

Dietary Supplements


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min.0.00 0.25 0.50 0.75 1.00 1.25 1.50 1.75 2.00 2.25 2.50

Fat Soluble Vitamins

Ultra II® C18

Peak List Ret. Time (min.)1. vitamin K2 0.9052. vitamin D2 1.2243. vitamin D3 1.3054. vitamin E acetate 1.8285. vitamin K1 2.169

SSaammppllee:: Inj.: 1µLConc.: 100µg/mL each componentSample diluent: acetone

CCoolluummnn:: Ultra II® C18 Cat.#: 9604853Dimensions: 50mm x 3.0mmParticle size: 2.2µmPore size: 100Å

CCoonnddiittiioonnss::Instrument: Shimadzu Prominence UFLCXRMobile phase: acetonitrile:methanol (85:15)Flow: 1.5mL/min.Temp.: ambientDet.: UV @ 230nm

1

23

4

5

LC_PH0492

NEW!

Vitamins B1, B2, B3, and B6

Ultra C8Peak List Ret. Time (min.)

1. vitamin B3 (nicotinamide) 2.7322. vitamin B6 (pyridoxine) 5.6153. vitamin B2 (riboflavin) 8.7194. vitamin B1 (thiamine) 19.004

SSaammppllee:: Inj.: 5µLConc.: 50µg/mL each componentSample diluent: water:methanol (80:20)

CCoolluummnn:: Ultra C8Cat.#: 9103575Dimensions: 250mm x 4.6mmParticle size: 5µmPore size: 100Å

CCoonnddiittiioonnss::Instrument: Shimadzu Prominence UFLCXRMobile phase: 0.008M sodium 1-hexanesulfonate:methanol:glacial acetic acid:

triethylamine (817.5:175:7.5:0.2)Flow: 2.0mL/min.Temp.: 50°CDet.: UV @ 270nm

LC_PH0497

NEW!


734 www.restek.com 800-356-1688 or 814-353-1300



Water Soluble B Vitamins




CCoonnddiittiioonnss::Instrument: Shimadzu Prominence UFLCXRMobile phase: A. 10mM potassium phosphate (pH 2.5)

B. acetonitrile Time (min.) %B0 21.5 25 75

Flow: 1.5mL/min.Temp.: 40°CDet.: UV @ 210nmPressure: 105bar

Peak List Ret. Time (min.)1. vitamin B3 2.4722. vitamin B6 2.7643. vitamin B5 3.8044. vitamin B9 4.1265. vitamin B12 4.2616. vitamin B2 4.3297. vitamin B7 4.472

LC_PH0503

NEW!

Vitamin C


SSaammppllee:: Inj.: 2µLConc.: 100µg/mL Sample diluent: water


CCoonnddiittiioonnss::Instrument: Shimadzu Prominence UFLCXRMobile phase: 100% 10mM potassium phosphate (pH2.5) Flow: 1.5mL/min.Temp.: 40°CDet.: UV @ 242nmPressure: 95bar

Peak List Ret. Time (min.)1. ascorbic acid (vitamin C) 1.759

LC_PH0504

NEW!


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LC_PH0505

Vitamin A Compounds

Ultra II® Aromax

Peak List Ret. Time (min.)1. retinol 0.8322. β-carotene 0.950

SSaammppllee:: Inj.: 2µLConc.: 100µg/mL each componentSample diluent: acetone

CCoolluummnn:: Ultra II® AromaxCat.#: 9607853Dimensions: 50mm x 3.0mmParticle size: 2.2µmPore size: 100Å

CCoonnddiittiioonnss::Instrument: Shimadzu Prominence UFLCXRMobile phase: methanol:acetonitrile (99:1)Flow: 0.8mL/min.Temp.: ambientDet.: UV @ 325nm and 480nmPressure: 105barUVat 325 (in red)

UVat 480 (in black)

NEW!





736 www.restek.com 800-356-1688 or 814-353-1300

HPLC CHROMATOGRAMS | PHARMACEUTICAL

Famotidine

Peak List Ret. Time (min.)1. impurity A 2.0942. famotidine 4.4603. impurity D 4.9374. impurity C 5.3345. impurity B 7.480

SSaammppllee:: Inj.: 5µLConc.: 100µg/mL famotidine, 10µg/mL each impuritySample diluent: methanol


CCoonnddiittiioonnss::Instrument: Shimadzu Prominence UFLCXRMobile phase: 20mM potassium phosphate (pH 2.5):methanol


Flow: 1.2mL/min.Temp.: 40°CPressure: 345barDet.: UV @ 268nm

LC_PH0494

Faster! 3μm

8 min.

SSaammppllee:: Inj.: 10µLConc.: 100µg/mL famotidine, 10µg/mL

each impuritySample diluent: methanol






LC_PH0495

Fast! 5μm

15 min.


LC_PH0493

SSaammppllee:: Inj.: 2µLConc.: 100µg/mL famotidine, 10µg/mL each impuritySample diluent: methanol

CCoolluummnn:: Ultra II® AromaxCat.#: 9607853Dimensions: 50mm x 3.0mmParticle size: 2.2µmPore size: 100Å




Fastest! 2.2μm

4 min.

Famotidine and USP Impurities

Ultra II® Aromax NEW!


LC_PH0482B

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Potential Genotoxic Impurities, Analgesics

Potential Genotoxic Impurities

Ultra II® Aromax

Peak List M/Z*1. ethyl benzenesulfonate 2042. isopropyl toluenesulfonate 2323. n-propyl toluenesulfonate 2324. n-butyl toluenesulfonate 246*All M/Z are [M+NH4]+

SSaammppllee:: Inj.: 100µLConc.: 10ng/mL each PGI in 1mg/mL dorzolamideSample diluent: mobile phase

CCoolluummnn:: Ultra II® Aromax Cat.#: 9607312Dimensions: 100mm x 2.1mmParticle size: 3µmPore size: 100Å

CCoonnddiittiioonnss::Instrument: Agilent 1100Mobile phase: A: 0.2% ammonium acetate in water

B: 0.2% ammonium acetate in methanolFlow: 0.3mL/min.Temp.: ambientDet.: LECO TOF-MS

NEW!

Hydroxybenzoic Acids on Ultra Aqueous C18

LC_PH0400

1. 3,5-dihydroxybenzoic acid2. 2,5-dihydroxybenzoic acid3. 4-hydroxybenzoic acid4. 3-hydroxybenzoic acid5. 2,4-dihydroxybenzoic acid6. benzoic acid7. salicylic acid

SSaammppllee::Inj.: 5µLConc.: 50µg/mL each componentSample diluent: mobile phase

CCoolluummnn:: UUllttrraa AAqquueeoouuss CC1188 Cat.#: 9178565Dimensions: 150mm x 4.6mmParticle size: 5µmPore size: 100Å

CCoonnddiittiioonnss::Mobile phase: A: 20mM potassium phosphate (pH 2.5);

B: acetonitrileTTiimmee((mmiinn..)) %%BB0.00 205.00 50

10.00 50



738 www.restek.com 800-356-1688 or 814-353-1300


Analgesics

PPeeaakk LLiisstt:: CCoonncc.. ((µµgg//mmLL))U. unknown unknown1. morphine sulfate 2042. acetaminophen 923. codeine phosphate 2164. oxycodone HCl 2065. hydrocodone bitartrate 218

LC_0221

Analgesic Acetaminophen and Narcotic Analgesics

on Ultra C18

SSaammppllee::Inj.: 4.0µLSample: raw material mixSolvent: mobile phase


CCoonnddiittiioonnss::Mobile phase: A: 10mm potassium

phosphate, pH 2.8B: acetonitrile:methanol,

(90:10, v/v)(85A:15B, v/v)


CCoolluummnn:: PPiinnnnaaccllee®® IIII CC1188Cat.#: 9214575-700Dimensions: 250mm x 4.6mmParticle size: 5µmPore size: 110Å

CCoonnddiittiioonnss::Mobile phase: A: 0.73g 1-heptane

sulfonic acid and 10mL glacial acetic acid, diluted to 720mL with water, pH = 2.33B: methanol (72A:28B, v/v)

Flow: 1.00mL/min.Temp.: 26.5°C Det.: UV @ 284nm

LC_0209

Narcotic Analgesic Morphine Sulfate Raw Material -

USP 25: Resolution Solution on Pinnacle® II C18

PPeeaakk LLiisstt:: CCoonncc.. ((µµgg//mmLL))1. unknown unknown2. phenol 0.153. morphine sulfate 0.24


0 1 2 3 4 min.

PPeeaakk LLiisstt:: RReett.. TTiimmee ((mmiinn..)) IInnjj.. %% RRSSDD ((nn == 55)) 1. hydrocodone bitartrate 3.1 0.37%

SSaammppllee::Inj.: 20µLConc.: 1µg/mLSample: assay standardSolvent: mobile phase

LC_0211

Narcotic Analgesic Hydrocodone Bitartrate by USP 25

on Pinnacle® II Silica

CCoolluummnn:: PPiinnnnaaccllee®® IIII SSiilliiccaaCat.#: 9210575Dimensions: 250mm x 4.6mmParticle size: 5µmPore size: 110Å

CCoonnddiittiioonnss::Mobile phase: A: 800mL acetonitrile; 4mL water;

1mL diethylamineB: methanol (55A:45B, v/v)


Impurities resolvedfrom primary peak.


CCoonnddiittiioonnss::Mobile phase: A: 5mM hexane sulfonic acid

with 2mL TEA and 3mL ofphosphoric acid per liter. pH adjusted to 2.5B: methanol (90A:10B, v/v)


Narcotic Analgesic Oxycodone HCl Raw Material by

USP 25: Resolution Solution on Ultra C8

LC_0213

PPeeaakk LLiisstt:: CCoonncc.. ((µµgg//mmLL)) RReett.. TTiimmee ((mmiinn..)) RRRRTT TTaaiilliinngg RReess..1. codeine phosphate 13 19.3 0.7 1.1 —2. oxycodone HCl 9 26.8 1.0 0.99 3.3

SSaammppllee::Inj.: 10µLSample: resolution solutionSolvent: mobile phase


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Antiarrhythmics, Antiasthmatics

Antiarrhythmic Calcium Channel Blockers

on Ultra Cyano

1

PPeeaakk LLiisstt::1. diltiazem2. nifedipine impurity3. verapamil4. nifedipine5. nicardipine

LC_0062

0 1 2 3 4 5 6 7 8 9 min.

2

3

4

5

SSaammppllee::Inj.: 5µLConc.: 100mg/mLSolvent: acetonitrile:water (1:1)

CCoolluummnn:: UUllttrraa CCyyaannooCat.#: 9106565Dimensions: 150mm x 4.6mmParticle size: 5µmPore size: 100Å


phosphate monobasic, pH 3.0:acetonitrile (70:30, v/v)

Flow rate: 1.2mL/min.Temp.: 30°C (±1°C)Det.: 235nm

Antiarrhythmic Furosemide on Ultra IBD

PPeeaakk LLiisstt::1. uracil (marker)2. furosemide

SSaammppllee::Inj.: 5µLConc.: 1000µg/mLSolvent: acetonitrile:water

(60:40, v/v)


CCoonnddiittiioonnss::Mobile phase: 20mM ammonium

acetate, pH 4.5:acetonitrile (70:30, v/v)

Flow rate: 2.0mL/min.Temp.: 27°CDet.: UV @ 280nm

LC_0071

Impurities in Furosemide(enlargement of baseline)

PPeeaakk LLiisstt::1. beclomethasone2. deschlorobeclomethasone

SSaammppllee::Inj.: 10µLConc.: 79.5µg/mL (beclomethasone)Solvent: water:acetonitrile (10:90, v/v)


CCoonnddiittiioonnss::Mobile phase: water:acetonitrile (70:30, v/v)Flow: 1.0mL/min.Temp.: 25°CDet.: UV @ 238nm

Antiasthmatic Beclomethasone on Ultra C18

0 5 10 15 20 min.

1

2

LC_0120





740 www.restek.com 800-356-1688 or 814-353-1300


Antibiotics

Antibiotic Cephalexin on Ultra IBD

1

PPeeaakk LLiisstt::1. cephalexin2. cephradine

SSaammppllee::Inj.: 10µLConc.: 500µg/mLSolvent: acetonitrile:water

(10:90, v/v)



formate, pH 2.5:acetonitrile(90:10, v/v)


2

0 2 4 6 8 10 min.

LC_0094

PPeeaakk LLiisstt::1. penicillin V

SSaammppllee::Inj.: 2.5µLConc.: 1.2mg/mLSolvent: acetonitrile:water

(10:90,v/v)



formate, pH 2.5:acetonitrile (95:5, v/v)


Antibiotic Penicillin V on Ultra IBD

1

0 1 2 3 4 5 6 7 8 min.

LC_0096

Antibiotic Cephaloridine on Ultra IBD

(Reversed Phase)

PPeeaakk LLiisstt::1. cephaloridine

SSaammppllee::Inj.: 5µLConc.: 1mg/mLSolvent: acetonitrile:water

(50:50, v/v)


CCoonnddiittiioonnss::Mobile phase: acetonitrile:

20mM ammonium phosphate, pH 4.0 (20:80, v/v)


LC_0102

1

0 1 2 3 4 5 6 7 8 min.

Tetracycline Mix on Allure® Biphenyl

LC_PH0347

RReett.. TTiimmeePPeeaakk LLiisstt ((mmiinn..))

1. oxytetracycline 4.592. degradation peak 5.193. tetracycline 6.324. degradation peak 11.165. chlortetracycline 15.816. doxycycline 19.66

SSaammppllee::Inj.: 30µLConc.: 100µg/mL each componentSample diluent: methanol

CCoolluummnn:: AAlllluurree®® BBiipphheennyyllCat.#: 9166565Dimensions: 150mm x 4.6mmParticle size: 5µmPore size: 60Å

CCoonnddiittiioonnss::Mobile phase: 20mM ammonium phosphate

(pH 2.5):acetonitrile, 80:20Flow: 1mL/min.Temp.: ambientDet.: UV @ 254nm


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Antibiotics, Anti-Diabetic, Corticosteroids

Anti-Diabetic Glyburide (Glybenclamide) on Ultra IBD

1

PPeeaakk LLiisstt::1. unknown2. glyburide

SSaammppllee::Inj.: 1µLConc.: 500µg/mLSolvent: water:methanol:acetonitrile

(1:1:2, v/v)


CCoonnddiittiioonnss::Mobile phase: water with

0.1% (v/v) acetic acid:acetonitrile (95:05, v/v)


2

0 1 2 3 4 5 min.

LC_0069

PPeeaakk LLiisstt::1. uracil (void marker)2. triamcinolone3. hydrocortisone4. dexamethasone5. corticosterone6. deoxycorticosterone

SSaammppllee::Inj.: 5µLConc.: 100µg/mLSolvent: mobile phase

Corticosteroids on Ultra C18

0 1 2 3 4 5 6 min.

LC_0108

3

2

1

4

5

6


CCoonnddiittiioonnss::Mobile phase: water:methanol

(30:70, v/v)Flow: 1.0mL/min.Temp.: 30°CDet.: UV @ 220nm

Corticosteroids on Allure® Biphenyl

LC_PH0330


1. hydrocortisone 4.192. prednisone 4.793. cortisone 5.084. dexamethasone 6.375. corticosterone 9.016. cortisone acetate 15.757. desoxycorticosterone 25.94



CCoonnddiittiioonnss::Mobile phase: water:acetonitrile, 60:40Flow: 1mL/min.Temp.: ambientDet.: UV @ 254nm

Antibiotic Amoxicillin on Ultra IBD

PPeeaakk LLiisstt::1. amoxicillin

SSaammppllee::Inj.: 5µLConc.: 1.5mg/mLSolvent: acetonitrile:water

(10:90, v/v)





1

0 1 2 3 4 5 6 min.

LC_0095


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Steroids

Endogenous Steroids on Allure® Biphenyl

LC_PH0334


1. β-estradiol 3.762. testosterone 5.083. progesterone 14.05


CCoolluummnn:: AAlllluurree®® BBiipphheennyyll Cat.#: 9166565Dimensions: 150mm x 4.6mmParticle size: 5µmPore size: 60Å

CCoonnddiittiioonnss::Mobile phase: water:acetonitrile, 40:60Flow: 1mL/min.Temp.: ambientDet.: UV @ 220nm

Contraceptive Hormones on Allure® Biphenyl

LC_PH0328


1. β-estradiol 3.802. ethynyl estradiol 4.453. norethindrone 6.154. norgestrel 8.41

SSaammppllee::Inj.: 5µLConc.: 100µg/mL each

componentSample diluent: methanol


CCoonnddiittiioonnss::Mobile phase: water:acetonitrile,

40:60Flow: 1mL/min.Temp.: ambientDet.: UV @ 220nm

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PPeeaakk LLiisstt::1. estriol2. 17β-estradiol3. 17α-estradiol4. ethynyl estradiol5. testosterone6. estrone7. norethindrone


CCoolluummnn:: 11..99µµmm PPiinnnnaaccllee®® DDBB BBiipphheennyyllCat.#: 9409252Dimensions: 50mm x 2.1mmParticle size: 1.9µmPore size: 140Å


B: methanol

TTiimmee((mmiinn)) %%BB0 301 303 70

Flow: 0.8 mL/min.Temp.: 30ºCDet.: UV @ 220nm

LC_PH0453

Hormones on 1.9μm Pinnacle® DB Biphenyl


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Lactulose Concentrate, Xanthines, Admixed Drugs

Admixtures: Expectorant/Antitussive Guaifenesin and

Narcotic Analgesic Codeine on Ultra Phenyl

1

PPeeaakk LLiisstt:: CCoonncc.. ((µµgg//mmLL))1. codeine 8252. guaifenesin 375

SSaammppllee::Inj.: 5µLSolvent: methanol:water (50:50)

CCoolluummnn:: UUllttrraa PPhheennyyllCat.#: 9105565Dimensions: 150mm x 4.6mmParticle size: 5µmPore size: 100Å


formate, pH 2.5:acetonitrile(80:20, v/v)


0 1 2 3 4 5 6 min.

LC_0088

2PPeeaakk LLiisstt:: CCoonncc.. RReett.. TTiimmee RRRRTT TTaaiilliinngg RReessoolluuttiioonn IInnjj.. %% RRSSDD

((µµgg//mmLL)) ((mmiinn..)) ((nn == 55))1. acetaminophen 0.76 3.304 1.0 1.1 — 1.12. hydrocodone bitartrate 0.0076 6.664 2.0 1.1 17.0 0.9

SSaammppllee::Inj.: 25µLSample: 500mg acetaminophen with

5mg hydrocodone bitartrate (tablet)Solvent: mobile phase

LC_0212

Admixtures: Hydrocodone Bitartrate/Acetaminophen

by USP 25 on Ultra C18


CCoonnddiittiioonnss::Mobile phase: 6.8g potassium

monobasic with 0.2mL TEA per liter:acetonitrile (85:15, v/v)


(hydrocodone bitartrate) and 295nm (acetaminophen).

PPeeaakk LLiisstt:: CCoonncc.. ((mmgg//mmLL)) RReett.. TTiimmee ((mmiinn..)) RRRRTT RReess.. IInnjj.. %% RRSSDD((nn == 55))

1. fructose 0.4 4.6 0.44 — —2. galactose 6.4 6.1 0.58 — —3. epi-lactose unknown 10.0 0.95 — —4. lactulose 40 10.5 1.00 1.1 0.3%5. lactose 4.8 12.7 1.21 2.9 —

SSaammppllee::Inj.: 20µL resolution standardSolvent: acetonitrile:water (50:50)

LC_0222

Laxative Lactulose Concentrate by USP 25: Resolution

Solution on Pinnacle® II Amino

CCoolluummnn:: PPiinnnnaaccllee®® IIII AAmmiinnooCat.#: 9217365Dimensions: 150mm x 4.6mmParticle size: 3µmPore size: 110Å

CCoonnddiittiioonnss::Mobile phase: 10mM sodium phosphate

monobasic in water, pH 4.8:acetonitrile (22:78, v/v)

Flow: 1.3mL/min.Temp.: 40°C Det.: refractive index @ 40°C

0 1 2 3 4 5 6 7 min.

1

2

3

4

LC_0241

Xanthines on Pinnacle® DB C18


CCoolluummnn:: PPiinnnnaaccllee®® DDBB CC1188Cat.#: 9414565Dimensions: 150mm x 4.6mmParticle size: 5µmPore size: 140Å

CCoonnddiittiioonnss::Mobile phase: 20mM KH2PO4,

pH 3.0:acetonitrile (90:10 v/v)


PPeeaakk LLiisstt:: CCoonncc.. ((µµgg//mmLL))1. theobromine 2252. theophylline 4183. β-hydroxyethyltheophylline 4184. caffeine 400


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HPLC CHROMATOGRAMS | BIOCHEMICAL/CLINICAL

Nucleotides, Nucleosides, Nucleic Acid Bases

0 1 2 3 4 5 6 7 8 9 min.

LC_0137

SSaammppllee::Inj.: 1.0µLConc. 100µg/mL eachSolvent: 20 mM ammonium acetate,

pH 5.0 Note: 1-3 drops of ammonium hydroxide added to keep guanine in solution



acetate, pH 5.0: methanol (85:15, v/v)


Nucleic Acid Bases on Allure® PFP Propyl

1

2

3

4

5

PPeeaakk LLiisstt::1. cytosine 2. uracil3. guanine4. thymine5. adenine

Nucleotides, Nucleosides, and

Nitrogenous Bases on Ultra IBD

PPeeaakk LLiisstt:: CCoonncc.. ((µµgg//mmLL))1. CDP 1462. CMP 1133. ATP 1174. ADP 1455. cytidine 1556. TMP 1577. AMP 1258. guanine 369. guanosine 103

10. adenine 3811. adenosine 115

0 2 4 6 8 10 12 14 16 18 min.

6 7

89

10

11

12

3

4

5

LC_0128



acetate, pH 5.8:methanol (97.5:2.5)


SSaammppllee::Inj.: 20µLSolvent: 20mM ammonium

acetate, pH 5.8

Uracil, Uridine, UTP, UDP, and UMP on Ultra IBD

PPeeaakk LLiisstt:: CCoonncc.. ((µµgg//mmLL))1. UTP 3602. UDP 3603. UMP 2844. uracil 905. uridine 230


acetate, pH 5.8





LC_0133

0 2 4 6 min.

1

2

3

4

5

Thymine, Thymidine, TTP, TDP,

and TMP on Ultra IBD

PPeeaakk LLiisstt:: CCoonncc.. ((µµgg//mmLL))1. TTP 2242. TDP 1523. TMP 3464. thymine 885. thymidine 318


acetate, pH 5.8





LC_01320 2 4 6 8 10 12 14 16 min.

1

2

3

45


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Catecholamines, Purines/Pyrimidines, Amino Acids, Peptides

0 5 10 15 20 25 min.

Purines/Pyrimidines on Ultra PFP

CCoolluummnn:: UUllttrraa PPFFPPCat.#: 9176575Dimensions: 250mm x 4.6mmParticle size: 5µmPore size: 100Å

CCoonnddiittiioonnss::Mobile phase: 0.001% formic acid in water:

methanol (50:50, v/v) Flow: 1.0mL/min.Temp.: ambientDet.: UV @ 260nm

1

2

3

4

5

PPeeaakk LLiisstt::1. cytosine 2. 5-methylcytosine3. uracil4. uric acid5. hypoxanthine6. xanthine7. thymine8. purine9. theobromine

10. ethyluracil11. 6-methylpurine12. 1,7-dimethylxanthine13. theophylline14. propyluracil

SSaammppllee::Inj.: 10µLConc.: 100µg/mL eachSolvent: mobile phase

6

7

8

11

9 10

121413

LC_0136

PPeeaakk LLiisstt:: CCoonncc.. ((mmgg//mmLL))1. tyrosine 0.22. phenylalanine 1.63. tryptophan 0.4

SSaammppllee:: Inj.: 20µLSolvent: mobile phase A

Aromatic Amino Acids on Ultra Aqueous C18


CCoonnddiittiioonnss::Mobile phases: A: 50mM potassium

phosphate, pH 2.5B: acetonitrile

5% - 20% B: 0-5 min.20% - 5% B: 5-6 min.Hold at 5% B: 6-13 min.


0 2 4 6 8 10 min.LC_0146

1

2

3

0.0 2.0 4.0 6.0 8.0 10.0 12.0 14.0 16.0 18.0 20.0

1 2 34 5

6 7

mfr. Hmfr. H

mfr. D

mfr. C

mfr. F

Viva

*

SSaammppllee::Inj.: 20µL peptide test mix

CCoolluummnn:: VViivvaa CC1188Cat.#: 9514562Dimensions: 150mm x 2.1mmParticle size: 5µmPore size: 300Å

CCoonnddiittiioonnss::Mobile phase: A: 0.08% trifluoroacetic acid in water (pH 2.0)

B: 0.08% TFA in acetonitrile, 10% B to 40% B in 20 min.Flow: 0.2mL/min.Det.: UV @ 214nm* High levels of trace metals (~100ppm) in the silica enhance this separation.

1. val-tyr2. val-tyr-val3. meth enkephalin4. val-4-angiotensin III5. angiotensin II, III6. leucine enkephalin7. angiotensin I

Peptide Mix on Viva C18

LC_BC0386

Catecholamines on Allure® PFP Propyl

PPeeaakk LLiisstt RReetteennttiioonn TTiimmee ((mmiinn..))1. norepinephrine 3.502. levodopa 5.433. epinephrine 7.274. tyrosine 7.775. dopamine 11.3

SSaammppllee::Inj.: 10µLConc.: 40µg/mL each componentSample diluent: mobile phaseSample temp.: ambient

CCoolluummnn:: AAlllluurree®® PPFFPP PPrrooppyyll Cat.#: 9169565Dimensions: 150mm x 4.6mmParticle size: 5µmPore size: 60Å


phosphate (pH 3.0, adjusted with formic acid)

Flow: 1mL/min.Temp.: 35°CDet.: UV @ 266nm

LC_BA0349


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Proteins, Oxytocin

Note excellent peak shapes and

resolution on the Viva column!

Protein Mix on Viva C18

SSaammppllee::Inj.: 20µLConc.: 0.08mg/mL each proteinSample diluent: 0.10% TFA in water / 0.10%

TFA in acetonitrile, 80:20, v/vSample temp.: 25°C

CCoolluummnnss:: WWiiddee PPoorree CC1188Dimensions: 150mm x 2.1mmParticle size: 5µmPore size: 300Å

CCoonnddiittiioonnss::Mobile phase: A: 0.10% TFA in water,

B: 0.10% TFA in acetonitrile, 20% B to 70% B in 30 min.

Flow: 0.20mL/min.Temp.: 25ºC (or ambient)Det.: UV @ 214nm

VViivvaa CC1188(cat.# 9514562)

PPeeaakk LLiisstt RReett.. TTiimmee ((mmiinn..))1. ribonuclease A 11.312. cytochrome c 14.653. holo-transferrin 16.324. apomyoglobin 20.34

Manufacturer A

Manufacturer B

Manufacturer C

Manufacturer D

LC_0324

freeliteratureViva Wide Pore HPLC

Columns

ExceptionalPerformance forPeptides, Proteins, orOther Large Molecules

Download your freecopy fromwww.restek.com.

Flyerlit. cat.# 59939

PEGylated Oxytocin on Viva C18 (LC/MS)

SSaammppllee:: ooxxyyttoocciinn PPEEGGyyllaattiioonn rreeaaccttiioonn pprroodduuccttssInj.: 20µLConc.: 300pmoles/µLSample diluent: 0.1% formic acid in water (v:v)

CCoolluummnn:: VViivvaa CC1188Cat.#: 9514561Dimensions: 150mm x 1.0mmParticle size: 5µmPore size: 300Å

LC_PH0467

CCoonnddiittiioonnss::Mobile phase: 0.1% formic acid in water:0.1%formic acid in acetonitrile, 60:40Flow: 0.1mL/min.Temp.: ambientDet.: Micromass Quattro IIInterface: ESIIon mode: positiveTemp.: 200°C Capillary: 2.25kVCone: 40V


Pain Management Drugs in Urine on Ultra II® Biphenyl (LC/MS/MS)

PPeeaakkss RRTT ((mmiinn..)) MMRRMM11 MMRRMM221. Acetaminophen 1.18 152/110 152/652. Morphine 1.79 286/157 286/1813. Codeine 3.21 300/165 300/2154. Oxycodone 3.46 316/298 316/2415. Hydrocodone 3.60 300/199 300/1716. Fentanyl 6.61 337/132 337/2167. Buprenorphine 6.66 468/187 468/848. Lorazepam 6.79 321/275 321/2299. Diazepam 8.06 285/154 285/193

10. Methadone 8.21 310/77 310/223

CCoolluummnn Ultra II® Biphenyl (cat.# 9609352)Dimensions: 50 mm x 2.1 mm IDParticle Size: 3 µmPore Size: 100 ÅTemp.: 40 °CSSaammpplleeConc.: 5 ng/mL in 1:10 urine:mobile phaseInj. Vol.: 5 µLMMoobbiillee PPhhaassee

A: 0.1% formic acid in waterB: 0.1% formic acid in methanol

TTiimmee ((mmiinn..)) FFllooww ((mmLL//mmiinn..)) %%AA %%BB0 0.5 90 10

10 0.5 0 10010.1 0.5 90 1012 0.5 90 10

DDeetteeccttoorr Applied Biosystems/MDS Sciex LC/MS/MSModel #: API-5000™Ion Source: TurboIonSpray®

Ion Mode: ESI+Curtain Gas: 25 psi (172.4 kPa)Gas 1: 60 psi (413.7 kPa)Gas 2: 40 psi (275.8 kPa)Source Temp.: 550 °CSource Voltage: 2000 VMode: MRMDwell Time: 50 msIInnssttrruummeenntt Applied Biosystems/MDS Sciex

LC/MS/MS SystemAAcckknnoowwlleeddggeemmeenntt Special thanks to Applied Biosystems

for providing instrument time.

LC_CF0516

Recommended for opiates.

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HPLC CHROMATOGRAMS | CLINICAL/FORENSIC

Pain Management Drugs



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Opiates, THC

Opiates on Allure® PFP Propyl (LC/MS/MS)

SSaammppllee:: ooppiiaatteess Inj.: 10µLConc.: 25ug/mL Solvent: methanol


1. morphine2. oxymorphone3. hydromorphone4. codeine5. 6-monoacetylmorphine6. oxycodone7. hydrocodone

CCoonnddiittiioonnss::Instrument: Shimadzu Prominence HPLCMobile phase: A: 0.1% formic acid in water

B: 0.1% formic acid in 80:20, methanol:acetonitrile

TTiimmee:: %%BB0.0 103.00 506.00 506.10 108.10 Stop pumps

Flow: 0.40mL/min.Temp.: 30°C

Det.: Applied Biosystems/MDS Sciex API 3200™ MS/MS systemIon source: Electrospray, positive IonSpray voltage: 5,500 Gas 1: 65psi (448kPa)Gas 2: 45psi (310kPa)Source temp.: 600°C

MMaassss SSppeeccttrroommeetteerr EExxppeerriimmeennttss::DDeecclluusstteerriinngg CCoolllliissiioonn

CCoommppoouunndd QQ11 QQ33 PPootteennttiiaall ((VV)) EEnneerrggyy ((VV))morphine 286 152 46 79morphine 286 165 46 51hydromorphone 286 185 46 41hydromorphone 286 157 46 55oxymorphone 302 227 36 37oxymorphone 302 198 36 55codeine 300 152 46 85codeine 300 115 46 89hydrocodone 300 199 46 39hydrocodone 300 128 46 69oxycodone 316 240 31 39oxycodone 316 256 31 336-monoacetylmorphine 328 211 51 556-monoacetylmorphine 328 193 51 35LC_PH0454

CCoolluummnn Ultra II® Biphenyl (cat.# 9609853)Dimensions: 50 mm x 3.0 mm IDParticle Size: 2.2 µmPore Size: 100 ÅTemp.: 35 °C

SSaammpplleeDiluent: AcetonitrileConc.: 50 ng/mLInj. Vol.: 20 µLMobile Phase


TTiimmee ((mmiinn..)) %%BB0 50

0.50 503.50 1004.50 1004.60 506.00 50

Flow: 0.7 mL/min.

DDeetteeccttoorr Applied Biosystems/MDS Sciex LC/MS/MSModel #: 3200 Q-TrapIon Source: TurboIonSpray®

Ion Mode: ESI+Ion Spray Voltage: 5 kVCurtain Gas: 25 psi (172.4 kPa)Gas 1: 50 psi (344.7 kPa)Gas 2: 60 psi (413.7 kPa)Source Temp.: 550 °CMode: MRMDwell Time: 50 msIInnssttrruummeenntt Applied Biosystems/MDS Sciex LC/MS/MS System

PPeeaakkss MMRRMM11 ((QQ11//QQ33)) MMRRMM22 ((QQ11//QQ33))1. Cannabidiol 315/123 315/1932. THC-COOH-gluc 345/299 345/1933. THC-COOH 345/299 345/1934. Cannabinol 311/223 311/1785. Δ9-THC 315/193 315/123

THC and Metabolites on Ultra II® Biphenyl (LC/MS/MS)

LC_CF0512

NEW!


Alcohol Metabolites on

Ultra II® Biphenyl (LC/MS)

Peak List m/z k' Intensity1. matrix 125 — —2. ethyl glucuronide 221 2.75 220,4083. ethyl sulfate 125 4.02 236,693

Sample: Inj.: 5µLConc.: 5µg/mL each componentSample diluent: urine diluted 1:10 with mobile phase

Column: Ultra II® BiphenylCat.#: 9609552Dimensions: 50mm x 2.1mmParticle size: 5µmPore size: 100Å

Conditions:Instrument: Shimadzu Prominence UFLCXRMobile phase: A: 5mM dihexylammonium acetate in water

B: 5mM dihexylammonium acetate in methanolTime (min.) %B

0.0 402.5 402.6 1005.4 1005.5 407.5 40

Flow: 0.3mL/min.Temp.: 40°CDet.: Shimadzu LCMS-2010EVIon source: ESI-Mode: SIMSource temp.: 200°CSource voltage: -4,000V

LC_CF0500

NEW!

Diuretics in Urine on Ultra II® Biphenyl

(LC/MS/MS, Positive Run)

CCoolluummnn Ultra II® Biphenyl (cat.# 9609352)Dimensions: 50 mm x 2.1 mm IDParticle Size: 3 µmPore Size: 100 ÅTemp.: 40°C

SSaammpplleeConc.: 500 ng/mL diuretics in urine, diluted 10x inmobile phaseInj. Vol.: 5 µL

MMoobbiillee PPhhaassee A: 0.1% formic acid in waterB: 0.1% formic acid in methanol

TTiimmee ((mmiinn..)) FFllooww ((mmLL//mmiinn..)) %%AA %%BB0 0.5 90 10

6.00 0.5 0 1006.1 0.5 90 108.00 0.5 90 10

DDeetteeccttoorr Applied Biosystems/MDS Sciex LC/MS/MSModel #: API 5000Ion Source: TurboIonSpray®

Curtain Gas: 25 psi (172.4 kPa)Gas 1: 60 psi (413.7 kPa)Gas 2: 40 psi (275.8 kPa)Source Temp.: 550°CMode: MRMDwell Time: 50 ms

Ion Mode: ESI+Ion Spray Voltage: 5.5 kV

LC_CF0509

MMRRMM11 MMRRMM22 MMRRMM33((QQ11//QQ33)) ((QQ11//QQ33)) ((QQ11//QQ33))

1. Amiloride 230/171 230/116 230/602. Triamterene 254/237 254/104 254/1413. Indapamine 366/132 366/91 366/1174. Ethacrynic acid 303/179 303/194 303/2575. Bumetanide 365/240 365/156 365/284

Good retention for

hydrophilic compounds!

Diuretics on Ultra II® Biphenyl

(LC/MS/MS, Negative Run)

Ion Mode: ESI-Ion Spray Voltage: -4.5 kV

MMRRMM11 MMRRMM22 MMRRMM33((QQ11//QQ33)) ((QQ11//QQ33)) ((QQ11//QQ33))

1. Acetazolamide 221/83 221/80 221/582. Chlorothiazide 294/214 294/179 294/2153. Hydrochlorothiazide 296/78 296/269 296/2054. Bendroflumethiazide 420/289 420/328 420/1975. Furosemide 329/285 329/205 329/78

LC_CF0510

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Alcohol Metabolites, Diuretics


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Amphetamines, Cocaine

Amphetamines on Ultra II® Biphenyl (LC/MS)

CCoolluummnn Ultra II® Biphenyl (cat.# 9609552)Dimensions: 50 mm x 2.1 mm IDParticle Size: 5 µmPore Size: 100 ÅTemp.: 30 °CSSaammpplleeDiluent: mobile phaseConc.: 2 µg/mLInj. Vol.: 5 µLMMoobbiillee PPhhaassee


TTiimmee ((mmiinn..)) FFllooww ((mmLL//mmiinn..)) %%AA %%BB0 0.3 80 2010 0.3 5 95

10.1 0.3 80 2012.0 0.3 80 20

DDeetteeccttoorr Shimadzu 2010EVAcquisition Type: ScanScan Speed: 2000 amu/sec.Heat Block: 200 °CInterface: ESI+Interface Temp.: 250 °CScan Range: 100 - 250 amuEvent Time: 0.1 sec.IInnssttrruummeenntt Shimadzu UFLCXRNNootteess Data were collected in scan mode. An extracted ion chromatogram is shown.

LC_CF0518

Peaks RT (min.) m/z1. Amphetamine 2.812 135.952. Methamphetamine 3.432 149.953. MDA 3.537 179.954. MDMA 4.092 193.955. MDEA 4.679 207.95

NEW!

Cocaine and Ecgonine Methyl Ester on

Allure® PFP Propyl (LC/MS/MS)

PPeeaakk LLiisstt::1. EME (ecgonine methyl ester) 2. COC (cocaine)

SSaammppllee::Inj.: 10µLConc.: 1µg/mLSolvent: waterTemp.: 4°C


Data Courtesy of Shane Needham, Pfizer Inc. LC_0126

XIC of +MRM (3 pairs) for304.0 / 182.0 amu 2.35e3 cps

2

0 0.5 1.0 1.5 2.0 2.5 3.0 3.5 4.0 4.5 min.

XIC of +MRM (3 pairs) for200.0 / 182.0 amu 1.30e3 cps

1

0 0.5 1.0 1.5 2.0 2.5 3.0 3.5 4.0 4.5 min.



Flow: 0.6mL/min.Column temp.: ambientDet.: Applied Biosystems/MDS SCIEX

API 3200™ MS/MS systemInterface: turbo ion spray, ESIInterface temp.: 150°CIon mode: positive ESI probe voltage: 5,000VOrifice: + 71VRing: + 265VCollision gas: nitrogenCollision gas pressure: 2.2 mTorrCollision gas energy: 28 eV (COC)

26 eV (EME)Electron multiplier: 2,100 voltsAuxilary gas flow: 7,000cc/min.Nebulizer gas setting: 15lb/in.2

Curtain gas setting: 12lb/in.2

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Benzodiazepines

Benzodiazepines on Allure® PFP Propyl (LC/MS/MS)

SSaammppllee:: bbeennzzooddiiaazzeeppiinneessInj.: 20µLConc.: NA Solvent: NA


CCoonnddiittiioonnss::Instrument: Shimadzu Prominence HPLCMobile phase: A: 0.1% formic acid and 1mM

ammonium formate in waterB: 0.1% formic acid and 1mM ammonium formate in acetonitrile

TTiimmee FFllooww %%BB((mmiinn..)) ((µµLL//mmiinn..))

0.0 500 1010.00 1000 9015.00 1000 9015.50 500 1017.50 500 10

Flow: see gradient tableTemp.: 40°CDet.: Applied Biosystems/MDS Sciex

API 3200™ MS/MS systemIon Source: Electrospray, positive IonSpray

Voltage: NA Gas 1: NAGas 2: NASource

Temp.: 500°C

Data courtesy of: Applied Biosystems MDS Sciex

LC_PH0463

Analyze 27

benzodiazepines

in less than

10 minutes!

CCoommppoouunndd NNaammee RReetteennttiioonn TTiimmee PPrreeccuurrssoorr IIoonn MMRRMM 11 MMRRMM 22 DDPP CCEE CCEE LLOOQQ((mmiinn..)) ((aammuu)) ((aammuu)) ((aammuu)) ((MMRRMM 11)) ((MMRRMM 22)) ((nngg//mmLL))

7-aminonitrazepam 3.2 252.1 121.1 94.0 51 35 53 1.07-aminoclonazepam 3.3 286.1 121.0 222.2 46 41 35 0.57-aminoflunitrazepam 3.8 284.1 135.1 226.0 51 39 49 0.5Bromazepam 3.8 316.0/318.0 182.1 182.1 51 45 45 5.0α-hydroxyalprazolam 4.1 325.1 297.2 204.9 51 31 59 2.0α-hydroxytriazolam 4.1 359.0 239.2 176.0 61 63 37 5.0Oxazepam 4.2 287.0 241.1 268.9 41 27 19 10.0Lorazepam 4.3 321.0/323.1 275.0 277.0 41 31 27 5.0Estazolam 4.4 295.0 205.0 267.1 51 53 31 2.0Zaleplon 4.4 306.2 236.3 264.2 56 35 27 0.52-hydroxyethylflurazepam 4.5 333.1 211.2 109.0 56 51 41 1.0Desmethylflunitrazepam 4.5 300.1 254.2 198.2 56 35 51 2.0Nitrazepam 4.6 282.0 236.1 180.2 71 35 51 2.0Clonazepam 4.7 316.0 270.2 214.0 56 41 51 2.0Desalkylflurazepam 4.7 289.1 140.1 226.1 71 41 39 2.0Temazepam 4.7 301.1/303.1 255.1 257.2 35 30 30 5.0Triazolam 4.7 343.0 238.9 314.9 61 53 37 1.0Alprazolam 4.8 309.1 205.1 281.1 56 53 35 1.0Lormetazepam 4.8 335.0/337.1 289.0 291.1 41 29 29 2.0Clobazam 4.9 301.1 259.1 224.3 46 29 47 1.0Flunitrazepam 5.0 314.0 268.1 239.1 56 35 49 1.0Nordiazepam 5.0 271.1 140.2 164.9 46 37 35 2.0Zolpiclone 5.4 389.1 244.8 217.0 16 25 41 1.0D5-Diazepam 5.4 290.1 198.2 - 55 41 -Diazepam 5.5 285.0 193.2 154.1 55 41 37 1.0Chlordiazepoxide 6.0 300.1 227.1 283.2 36 31 21 5.0Prazepam 6.1 325.1 271.1 140.0 81 31 53 2.0Zolpidem 7.4 308.1 235.1 236.1 56 39 35 0.2Midazolam 7.9 326.1 291.3 222.0 56 33 63 0.5Flurazepam 8.5 388.2 315.1 317.1 36 27 27 0.1Medazepam 9.0 271.0 91.1 207.3 46 41 39 2.0D3-Doxepine 9.1 283.0 107.1 - 41 35 -

MRM Transitions, retention times,and LOQ values.

Bar color indicates shared precursor ions.Note compounds with shared precursor ionsare baseline resolved on the Allure® PFPPropyl column, as shown by retention timecomparison. Data courtesy of Applied Biosystems MDS Sciex.


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INDEX

Compound Index for GC Chromatograms

acenaphthene . . . . . . . . . . . . . . . . . . . .43, 45, 73, 87, 97, 98, 555 - 559, 561 - 567, 636 - 638

acenaphthene-d10 . . . . . . . . . . . . . . . . . . . .43, 87, 497, 554, 559 - 565, 567, 568, 635

acenaphthylene . . . . . . . . . . . . . . . .39, 43, 45, 73, 87, 97, 98, 555 - 559, 561 - 568, 636 - 638

acephate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .576, 577acetaldehyde . . . . . . . . . . . . . . . . . . . .82, 607, 628, 630, 667acetic acid . . . . . . . . . . . . . . . . . . . . . . . . . .67, 615, 629 - 631acetochlor . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .497, 560acetone . . . . . . . . . . . .82, 85, 100, 103, 111, 409, 547 - 551,

607 - 609, 628, 630, 667, 670, 701 - 703acetonitrile . . . . . . . . . . . . . . . . . .83, 85, 103, 547, 548, 607,

672, 694, 697, 700 - 702acetophenone . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .566, 633acetopromazine . . . . . . . . . . . . . . . . . . . . . . . . . . . . .680 - 682acetovanillone . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .629n-acetyl galactose amine . . . . . . . . . . . . . . . . . . . . . . . . . .640n-acetyl glucose amine . . . . . . . . . . . . . . . . . . . . . . . . . . . .6402-acetylaminofluorene . . . . . . . . . . . . . . . . . . . . . . . . . . . .566acetylene . . . . . . . . . . . . . . .76, 129, 606, 647, 650, 652 - 654acifluorfen methyl ester . . . . . . . . . . . . . . . . . . . . . . . . . . .579acrylamide . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .639acrylonitrile . . . . . . . . . . . . . . . . . . . .100, 103, 547 - 551, 607active amyl alcohol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .630adiponitrile . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .66, 705air . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .654, 703alachlor . . . . . . . . . . . . . . . . . . . . . . .497, 568, 571, 572, 590aldrin . . . . . . . . . . . . . . . . . . . . . . .53, 89, 569 - 572, 635, 639alkanes . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .634alkylthiophenes . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .664allyl alcohol . . . . . . . . . . . . . . . . . . . . . . . . . . . . .100, 549, 550allyl chloride . . . . . . . . . . . . . . . . . . . . . . .100, 103, 547 - 5514-allyl-2,6-dimethoxyphenol . . . . . . . . . . . . . . . . . . . . . . . .629alprazolam . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .680 - 682ametryne . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .568, 578, 581AMGBL (α-methylene-γ-butyrolactone) . . . . . . . . . . . . . . .6694-aminobiphenyl . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5666-aminocapronitrile . . . . . . . . . . . . . . . . . . . . . . . . . . .66, 7052-amino-4,6-dinitrotoluene . . . . . . . . . . . . . . . . . . . .593, 5944-amino-2,6-dinitrotoluene . . . . . . . . . . . . . . . . . . . .593, 594aminoethylethanolamine . . . . . . . . . . . . . . . . . . . . . . . . . .704aminoethylpiperazine . . . . . . . . . . . . . . . . . . . . . . . . . . . . .704aminomethylcyclopentylamine . . . . . . . . . . . . . . . . . . .66, 7052-amino-4-nitrotoluene . . . . . . . . . . . . . . . . . . . . . . . . . . .5932-amino-6-nitrotoluene . . . . . . . . . . . . . . . . . . . . . . . . . . .593amitriptyline . . . . . . . . . . . . . . . . . . . . . . . . . . . .680, 681, 691ammelide . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .638ammeline . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .638amobarbital . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .678, 679amphetamine . . . . . . . . . . . . . . . . . . . . . . .65, 675 - 677, 680(+)amphetamine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .686(-)amphetamine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .686n-amyl acetate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .103, 547iso-amyl alcohol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .671n-amyl alcohol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .630amyl cinnamal . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .61amyl cinnamic aldehyde . . . . . . . . . . . . . . . . . . . . . . . . . . .626tert-amyl methyl ether . . . . . . . . . . . . . . .100, 103, 547 - 550iso-amyl nitrite . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .671amylcinnamyl alcohol 1 . . . . . . . . . . . . . . . . . . . . . . . . . . . .61amylcinnamyl alcohol 2 . . . . . . . . . . . . . . . . . . . . . . . . . . . .615α-androstan-17β-ol-3-one . . . . . . . . . . . . . . . . . . . . . . . .6875-androstene-3β,17β-diol . . . . . . . . . . . . . . . . . . . . . . . . .687androsterone . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .688anethole . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .626aniline . . . . . . . . . . . . . . . . . . . . . . . . . .43, 87, 561 - 567, 705anisaldehyde . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .626anise alcohol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .61anthracene . . . . . . . . . . . . . . . . . . . . . .43, 45, 73, 87, 97, 98,

555 - 559, 561 - 568, 636 - 638aprobarbital . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .678, 679arabinitol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .640arachidic acid . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .59, 646Aramite isomer . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .566argon . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .109, 648Aroclor 1242 . . . . . . . . . . . . . . . . . . . . . . . . . . . . .93, 586, 587Aroclor 1254 . . . . . . . . . . . . . . . . . . . . . . . . . . . . .93, 586, 587Aroclor 1260 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .587Aroclor 1262 . . . . . . . . . . . . . . . . . . . . . . . . . . . . .93, 586, 587

aspon . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .91, 573 - 575atraton . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .568, 578, 581atrazine . . . . . . .497, 566, 568, 571, 572, 578, 581, 582, 590azinphos-ethyl . . . . . . . . . . . . . . . . . . . . . . . . . . .91, 573 - 575azinphos-methyl . . . . . . . . . . . . . . . . . . . . . . . . .91, 573 - 577azobenzene . . . . . . . . . . . . . . . . . . . .560 - 562, 564, 566, 567B100 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .81, 644, 645Balan . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .581barbital . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .678, 679BDE compounds . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .92, 588behenic acid . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .59, 646bentazon methyl ester . . . . . . . . . . . . . . . . . . . . . . . . . . . .579benzaldehyde . . . . . . . . . . . . . . . . . . . . . . .566, 626, 633, 634benzene . . . . . . . . . . . . .75, 84, 85, 100, 101, 103, 128, 409,

467, 547 - 551, 595, 597, 606 - 610, 633, 651, 654 - 657, 670, 672, 694, 697, 700 - 702

benzeneacetaldehyde . . . . . . . . . . . . . . . . . . . . . . . . . . . . .633benzidine . . . . . . . . . . . . . . . . . . . . . . . . . . . .43, 87, 561 - 567benzo(a)anthracene . . . . . .43, 45, 73, 87, 97, 98, 555 - 559,

561 - 568, 636 - 638benzo(b)fluoranthene . . . . .43, 45, 73, 87, 97, 98, 555 - 559,

561 - 565, 567, 568, 636 - 638benzo(j)fluoranthene . . . .45, 73, 98, 557, 558, 566, 637, 638benzo(k)fluoranthene . . . . .43, 45, 73, 87, 97, 98, 555 - 559,

561 - 568, 636 - 638benzo(ghi)perylene . . . . . . .43, 45, 73, 87, 97, 98, 555 - 559,

561 - 568, 636 - 638benzo(a)pyrene . . . . . . . . . .43, 45, 73, 87, 97, 98, 555 - 559,

561 - 568, 636 - 638benzo(e)pyrene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .638benzocaine . . . . . . . . . . . . . . . . . . . . . . . . .672, 680, 681, 691benzoguanamine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .638benzoic acid . . . . . . . . . . . . .43, 87, 561 - 565, 567, 629, 641benzoic acid, methyl ester . . . . . . . . . . . . . . . . . . . . . . . . .633benzothiophene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .664benzoylecgonine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .673benzphetamine . . . . . . . . . . . . . . . . . . . . . . . . . .676, 680, 681benzyl alcohol . . . . . . . . . . . . . . . . . . . . .43, 61, 87, 561 - 567benzyl benzoate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .61benzyl butyl phthalate . . . . . . . . . . . . . . . . . . . .554, 566 - 568benzyl chloride . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .409, 609benzyl cinnamate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .61benzyl salicylate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .61, 641benzylethyl phthalate . . . . . . . . . . . . . . . . . . . . . . . . . . . . .592α-bergamotene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .627trans-α-bergamotene . . . . . . . . . . . . . . . . . . . . . . . .625, 628BHA . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .611, 628α-BHC . . . . . . . . . . . . . . . . . .53, 89, 569, 570, 572, 635, 639β-BHC . . . . . . . . . . . . . . . . . . .53, 89, 569, 570, 572, 635, 639δ-BHC . . . . . . . . . . . . . . . . . . .53, 89, 569, 570, 572, 635, 639γ-BHC . . . . . . . . . . . . . . . . . . . . . .53, 89, 569 - 572, 590, 639BHT . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .611biodiesel . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .644, 645biphenyl . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .566, 638β-bisabolene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .625, 628bis(2-chloroethoxy)methane . . . . . . . . . . . . .43, 87, 561 - 567bis(2-chloroethyl)ether . . . . . . . . . . . . . . . . .43, 87, 561 - 567bis(2-chloroisopropyl)ether . . . . . . . . . . . . .43, 87, 561 - 567bis(2-ethylhexyl)adipate . . . . . . . . . . . .43, 87, 554, 561 - 568bis(2-ethylhexyl)phthalate . . . . . . . . . .43, 87, 554, 561 - 568bis-hexamethylenetriamine . . . . . . . . . . . . . . . . . . . . .66, 705bisphenol A . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .592Bladex . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .568bolasterone . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .687bolstar . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .91, 573 - 575borneol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .627(+/-)borneol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .612β-bourbonene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .626brassicasterol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .623bromacil . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .568, 581, 590bromazepam . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .680 - 682bromobenzene . . . . . . . . . . . . . . . . .100, 101, 103, 547 - 5511-bromobutane . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .690bromochloroacetic acid . . . . . . . . . . . . . . . . . . . . . . . . . . .603bromochloroacetonitrile . . . . . . . . . . . . . . . . . . . . . . .589, 5904-bromo-1-chlorobenzene . . . . . . . . . . . . . . . . . . . . . . . . .101bromochloromethane . . . . . . . . . . . . . . . . . . . .100, 101, 103,

467, 547 - 551, 607, 6081,2-bromo-3-chloropropane . . . . . . . . . . . . . . . . . . . . . . . .1012-bromo-1-chloropropane . . . . . . . . . . . . . . . . . . . . .467, 548

bromodichloroacetic acid . . . . . . . . . . . . . . . . . . . . . . . . . .603bromodichloromethane . . . . . . .100, 101, 103, 409, 411, 467,

547 - 551, 589, 590, 607 - 609bromoethane . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .690bromoethene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6084-bromofluorobenzene . . . . . . . . . . . .103, 467, 547, 551, 5894-bromo-1-fluorobenzene . . . . . . . . . . . . . . . . .100, 548 - 5504-bromofluoromethane . . . . . . . . . . . . . . . . . . . . . . . . . . .607bromoform . . . . . . . . . . . . . . . .100, 101, 103, 409, 411, 467,

547 - 551, 589, 590, 607 - 609bromomethane . . . . . . . . . . . . .100, 101, 103, 234, 409, 467,

547 - 551, 606 - 6091-bromo-2-nitrobenzene . . . . . . . . . . . . . . . . . . . . . . . . . .5774-bromophenyl phenyl ether . . . . . . . . . . . . .43, 87, 561 - 5671-bromopropane . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6902-bromopropane . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .690brompheniramine . . . . . . . . . . . . . . . . . . . . . . . . . . . .683, 691bupivacaine . . . . . . . . . . . . . . . . . . . . . . . . . . . .680, 681, 691butachlor . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5681,3-butadiene . . . . . .76, 129, 409, 607 - 610, 650, 652 - 654butalbital . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .678, 679butane . . . . . . . . . . . . . . . . . . . . . . . . . . . .129, 131, 607, 664n-butane . . . . . . . . . . . . . . . . . . .76, 129, 606, 649 - 654, 6621,2-butanediol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6691,3-butanediol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6691,4-butanediol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6692,3-butanediol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .669butanetriol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .81, 644, 6451-butanol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .605, 6332-butanol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .128, 656n-butanol . . . . . . . . . . . . . . . . . . . . . . . . .58, 80, 85, 607, 642sec-butanol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .630tert-butanol . . . . . . . . . . . . . . . . . . . . . .75, 80, 642, 657, 6672-butanone . . . . . . . . . . . . . . . .100, 103, 547 - 551, 605, 7031-butene . . . . . . . . . . . . . . .76, 129, 606, 649, 650, 652 - 654cis-2-butene . . . . . . . . . . . . . . . .76, 129, 606, 650, 652 - 654trans-2-butene . . . . . . . . . .76, 129, 606, 649, 650, 652 - 654butyl chloride . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .690butyl acetate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .103, 547n-butyl acetate . . . . . . . . . . . . . . . . . . . . . . . . . .100, 549, 550iso-butyl alcohol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .671n-butyl alcohol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .671sec-butyl alcohol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .671tert-butyl alcohol . . . . . . . . . . . . . . .100, 103, 547 - 550, 671sec-butylamine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .704tert-butylamine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .704butylate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .568butylbenzene . . . . . . . . . . . . . . . . . . . . . . . . . . .607, 661, 662n-butylbenzene . . . . . . . . . . . . .100, 101, 103, 547 - 551, 662sec-butylbenzene . . . . . . . . . . .100, 101, 103, 547 - 551, 607tert-butylbenzene . . . . . . . . . . .100, 101, 103, 547 - 551, 607n-butyl benzenesulfonate . . . . . . . . . . . . . . . . . . . . . .689, 690butyl benzyl phthalate . . . . . . . . . . . . . . . . . .43, 87, 561 - 565butyl Cellosolve . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .643butylcyclohexane . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6101,3-butylene glycol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6021,4-butylene glycol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .602butyl ether . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .633n-butyl ether . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .634iso-butyl nitrite . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .671n-butyl nitrite . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .671sec-butyl nitrite . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .671tert-butyl nitrite . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .671tert-butyl phenol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .592n-butyl toluenesulfonate . . . . . . . . . . . . . . . . . . . . . . . . . .690butyric acid . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .629n-butyric acid . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .615γ-butyrolactone (GBL) . . . . . . . . . . . . . . . . . . . . . . . .668, 669C1 (methane) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .652C2 (ethane) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .652C3 phenol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .707C3 (propane) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .652C4:0 (methyl butyrate) . . . . . . . . . . . . . . . . . . . . . . . . . . . .617C6 (hexane) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .660C6:0 (methyl hexanoate) . . . . . . . . . . . . . . . . . . . . . . . . . .617C7 (heptane) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .658, 660C8 (octane) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .658, 660C8:0 (methyl octanoate) . . . . . . . . . . . . . . . . . . . . . . . . . . .617C9 (nonane) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .658, 660C10 (decane) . . . . . . . . . . . . . . . . . . . . . . . . . . .600, 658, 660

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INDEX


C10-C100 hydrocarbons . . . . . . . . . . . . . . . . . . . . . . . . . . . .79C10-C24 hydrocarbons . . . . . . . . . . . . . . . . . . . . . . . . . . . .663C10-C44 hydrocarbons . . . . . . . . . . . . . . . . . . . . . . . . . . . .659C10:0 (methyl decanoate) . . . . . . . . . . . . . . . . . . . . . . . . .617C11 (undecane) . . . . . . . . . . . . . . . . . . . . . . . . . .75, 658, 660C11:0 (methyl undecanoate) . . . . . . . . . . . . . . . . . . . . . . .617C12 (dodecane) . . . . . . . . . . . . . . . . . . . . . .75, 600, 658, 660C12:0 (methyl laurate) . . . . . . . . . . . . . . . . . . . . . . . . . . . .617C13 (tridecane) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .75, 658C13:0 (methyl tridecanoate) . . . . . . . . . . . . . . . . . . . . . . .617C14 (tetradecane) . . . . . . . . . . . . . . . . . . . . . . .600, 658, 660C14:0 (methyl myristate) . . . . . . . . . . . . . . . . . . . . . . . . . .617C14:1 (methyl myristoleate) . . . . . . . . . . . . . . . . . . . . . . . .617C15 (pentadecane) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .658C15:0 (methyl pentadecanoate) . . . . . . . . . . . . . . . . . . . . .617C15:1 (methyl pentadecenoate) . . . . . . . . . . . . . . . . . . . . .617C16 (hexadecane) . . . . . . . . . . . . . . . . . . . . . . . .600, 658, 660C16:0 (methyl palmitate) . . . . . . . . . . . . . . . . . . . . . . . . . .617C16:1 (methyl palmitoleate) . . . . . . . . . . . . . . . . . . . . . . . .617C17 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .664C17 (heptadecane) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .658C17:0 (methyl heptadecanoate) . . . . . . . . . . . . . . . . . . . . .617C17:1 (methyl heptadecenoate) . . . . . . . . . . . . . . . . . . . . .617C18 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .664C18 (octadecane) . . . . . . . . . . . . . . . . . . . . . . . .600, 658, 660C18:0 (methyl stearate) . . . . . . . . . . . . . . . . . . . .69, 617, 619C18:1 (methyl elaidate) . . . . . . . . . . . . . . . . . . . .69, 617, 619C18:1 (methyl oleate) . . . . . . . . . . . . . . . . . . . . . .69, 617, 619C18:1 (methyl petroselaidate) . . . . . . . . . . . . . . . . . . .69, 619C18:1 (methyl petroselinate) . . . . . . . . . . . . . . . . . . . .69, 619C18:1 (methyl transvaccenate) . . . . . . . . . . . . . . . . . .69, 619C18:1 (methyl vaccenate) . . . . . . . . . . . . . . . . . . . . . . .69, 619C18:2 (methyl linoleaidate) . . . . . . . . . . . . . . . . . . . . . . . .617C18:2 (methyl linoleate) . . . . . . . . . . . . . . . . . . . .69, 617, 619C18:3 (methyl linolenate) . . . . . . . . . . . . . . . . . . . . . . . . . .617C18:3 (methyl γ-linolenate) . . . . . . . . . . . . . . . . . . . . . . . .617C19 (nonadecane) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .658C20 (eicosane) . . . . . . . . . . . . . . . . . . . . . . . . . .600, 658, 660C20:0 (methyl arachidate) . . . . . . . . . . . . . . . . . . . . . . . . .617C20:1 (methyl eicosenoate) . . . . . . . . . . . . . . . . . . . . . . . .617C20:2 (methyl eicosadienoate) . . . . . . . . . . . . . . . . . . . . .617C20:3 (methyl eicosatrienoate) . . . . . . . . . . . . . . . . . . . . .617C20:4 (methyl arachidonate) . . . . . . . . . . . . . . . . . . . . . . .617C20:5 (methyl eicosapentaenoate) . . . . . . . . . . . . . . . . . .617C21:0 (methyl heneicosanoate) . . . . . . . . . . . . . . . . . . . . .617C22 (docosane) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .600, 658C22:0 (methyl behenate) . . . . . . . . . . . . . . . . . . . . . . . . . .617C22:1 (methyl erucate) . . . . . . . . . . . . . . . . . . . . . . . . . . . .617C22:2 (methyl docosadienoate) . . . . . . . . . . . . . . . . . . . . .617C22:6 (methyl docosahexaenoate) . . . . . . . . . . . . . . . . . . .617C23 (tricosane) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .658C23:0 (methyl tricosanoate) . . . . . . . . . . . . . . . . . . . . . . . .617C24 (tetracosane) . . . . . . . . . . . . . . . . . . . . . . .600, 658, 660C24:0 (methyl lignocerate) . . . . . . . . . . . . . . . . . . . . . . . . .617C24:1 (methyl nervonate) . . . . . . . . . . . . . . . . . . . . . . . . . .617C25 (pentacosane) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .658C26 (hexacosane) . . . . . . . . . . . . . . . . . . . . . . . . . . . .600, 658C28 (octacosane) . . . . . . . . . . . . . . . . . . . . . . . .600, 658, 660C30 (triacontane) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .658C32 (dotriacontane) . . . . . . . . . . . . . . . . . . . . . . . . . .658, 660C34 (tetratriacontane) . . . . . . . . . . . . . . . . . . . . . . . . . . . .658C36 (hexatriacontane) . . . . . . . . . . . . . . . . . . . . . . . .658, 660C38 (octatriacontane) . . . . . . . . . . . . . . . . . . . . . . . . . . . . .658C40 (tetracontane) . . . . . . . . . . . . . . . . . . . . . . . . . . .658, 660C42 (dotetracontane) . . . . . . . . . . . . . . . . . . . . . . . . . . . . .658C44 (tetratetracontane) . . . . . . . . . . . . . . . . . . . . . . . . . . .660C5-C106 hydrocarbons . . . . . . . . . . . . . . . . . . . . . . . .658, 659C5-C44 hydrocarbons . . . . . . . . . . . . . . . . . . . . . . . . . .77, 660C7 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .651C8-C100 hydrocarbons . . . . . . . . . . . . . . . . . . . . . . . . . . . . .78C8-C40 hydrocarbons . . . . . . . . . . . . . . . . . . . . . . . . . . . . .598δ-cadenene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .627caffeine . . . . . . . . . . . . . . . . . . . . . . . . . . . .672, 676, 680, 681campesterol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .623camphene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .625, 626, 628(+/-)camphene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .612camphor . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .61, 626(+/-)camphor . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .612cannabidiol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .674cannabinol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .673, 674

caproic acid . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .615caprolactam . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .566carbamazepine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .678, 692carbazole . . . . . . . . . . . . . . . . . . . . . . . . . . . .43, 87, 561 - 567carbon dioxide . . . . . . . . . . . . . . . . . .130, 548, 647, 654, 703carbon disulfide . . . . . . . .100, 103, 409, 547 - 551, 608, 609carbon monoxide . . . . . . . . . . . . . . . . . . . .109, 130, 647, 648carbon tetrachloride . . . . . . .84, 85, 100, 101, 103, 409, 467,

547 - 551, 589, 590, 606, 608, 609, 694, 697, 700carbonyl sulfide . . . . . . . . . . . . . . . . . . . . . . . . . . . . .632, 664carbophenothion . . . . . . . . . . . . . . . . . . . . . . . . .91, 573 - 575carboxin . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5683-carene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .625carisoprodal . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .678carveol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .626D carveol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .628L carveol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .628cis-carveol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .626trans-carveol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .626carvone . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .625, 626, 628(+)carvone . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .613(-)carvone . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .613cis-carvyl acetate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .626α-caryophyllene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .626β-caryophyllene . . . . . . . . . . . . . . . . . . . . . . . . . . . .625 - 628cathinone . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .676chloral hydrate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .589chloramben methyl ester . . . . . . . . . . . . . . . . . . . . . . . . . .579α-chlordane . . . . . . . . . . . . . . . . . . . . .53, 89, 569 - 572, 639cis-chlordane . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .635trans-chlordane . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .635γ-chlordane . . . . . . . . . . . . . . . . . . . . . .53, 89, 569 - 572, 639chlorfenvinphos . . . . . . . . . . . . . . . . . . . . . . . . .91, 573 - 575chloroacetonitrile . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5514-chloroaniline . . . . . . . . . . . . . . . . . . . . . . .43, 87, 561 - 567chlorobenzene . . . . . . . . . . . . . . .83, 100, 101, 103, 409, 467,

547 - 551, 606 - 609, 694, 697, 700 - 702chlorobenzene-d5 . . . . . . . . . . .100, 103, 547 - 550, 607, 608chlorobenzilate . . . . . . . . . . . . . . . . . . . . . . . . . . .53, 568, 5722-chlorobiphenyl . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5831-chlorobutane . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .551chlorodibromoacetic acid . . . . . . . . . . . . . . . . . . . . . . . . . .603chlorodibromomethane . . . . . . . . . . . . . . . . . . . . . . . . . . .411chlorodifluoromethane . . . . . . . . . . . . . . . . . . . . . . . . .74, 607chloroethane . . . . . . . . . . . . . . .100, 101, 103, 234, 409, 467,

547 - 551, 606 - 6092-chloroethanol . . . . . . . . . . . . . . . . .100, 103, 547, 549, 5502-chloroethyl vinyl ether . . . . . . . . . . . . . . . . . .101, 467, 548chloroform . . . . . . . . . .83, 85, 100, 101, 103, 409, 411, 467,

547 - 551, 589, 590, 606 - 609, 670, 672, 695, 698, 700 - 702

chloromethane . . . . . . . . . . . . .100, 101, 103, 234, 409, 467, 547 - 551, 606 - 609

4-chloro-3-methylphenol . . . . . . . . . . . .43, 87, 553, 560 - 5671-chloronaphthalene . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5662-chloronaphthalene . . . . . . . . . . . . . . . . . . .43, 87, 561 - 567chloroneb . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .568, 5724-chloro-3-nitro-trifluoride . . . . . . . . . . . . . . . . . . . . . . . . .5771-chlorooctane . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .596chloropentafluoroethane . . . . . . . . . . . . . . . . . . . . . . . . . . .742-chlorophenol . . . . . . . . . . . . . . .43, 87, 553, 560 - 567, 7052-chlorophenol-d4 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5604-chlorophenol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .394-chlorophenyl phenyl ether . . . . . . . . . . . . .43, 87, 561 - 567chloropicrin . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .589, 590chloroprene . . . . . . . . . . . . . . . . . . . . . . . . . . . .103, 547, 5481-chloropropane . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6902-chloropropane . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6903-chloropropene . . . . . . . . . . . . . . . . . . . . . . . . . . . . .606, 6084-chlorotestosterone-17-acetate . . . . . . . . . . . . . . . . . . . .687chlorothalonil . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .568, 5722-chlorotoluene . . . . . . . . . . . . .100, 101, 103, 547 - 551, 6084-chlorotoluene . . . . . . . . . . . . . . . . .100, 101, 103, 547 - 551chlorpheniramine . . . . . . . . . . . . . . . . . . . . . . . . . . . .683, 691chlorpromazine . . . . . . . . . . . . . . . . . . . . . . . . . . . . .680 - 682chlorpropham . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .568chlorprothixene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .682chlorpyrifos . . . . . . . . . . . . . . . . .91, 497, 568, 573 - 577, 635chlorpyrifos methyl . . . . . . . . . . . . . . . . . . .91, 573 - 575, 6355-α-cholestane . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .625

cholesterol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .623, 625chrysene . . . . . . . . . . . . . . . . . . . . . . . .43, 45, 73, 87, 97, 98,

555 - 559, 561 - 568, 636 - 638chrysene-d12 . . . .43, 87, 497, 554, 559 - 565, 567, 568, 6351,8-cineole . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .626, 628cinnamaldehyde . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .634trans-cinnamaldehyde . . . . . . . . . . . . . . . . . . . . . . . . . . . . .61cinnamic alcohol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .626cinnamic aldehyde . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .641cinnamyl acetate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .641cinnamyl alcohol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .61, 641citral 1 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .61citral 2 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .61citronellal . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .625 - 628citronellol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .61β-citronellol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .626, 627(+)-(R)-β-citronellol . . . . . . . . . . . . . . . . . . . . . . . . .612, 613(-)-(S)-β-citronellol . . . . . . . . . . . . . . . . . . . . . . . . . . .612, 613citronellyl acetate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .625citronellyl formate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .612clobazam . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .682clomipramine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .691clonazepam . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .680 - 682coca ethylene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .673cocaine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .672, 673, 680codeine . . . . . . . . . . . . . . . . . . . . . . . .673, 674, 680, 681, 683cotinine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .680, 681coumaphos . . . . . . . . . . . . . . . . . . . . . . . . . . . . .91, 573 - 575coumarin . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .61, 626m-cresol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .707o-cresol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .707p-cresol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .629, 707crotoxyphos . . . . . . . . . . . . . . . . . . . . . . . . . . . . .91, 573 - 575cumene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .655cyanazine . . . . . . . . . . . . . . . . . .497, 560, 568, 572, 582, 590cyanuric acid . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .638cycloate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .568cyclohexane . . . . . . . . . . . . . . . . . .66, 75, 83, 409, 608 - 610,

657, 694, 697, 700, 705cyclohexyl phthalate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .592cyclopentane . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .606cyclopropane . . . . . . . . . . . . . . . . . . . . . . . . . . .129, 650, 652p-cymene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .625, 626, 6282,4-D . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5802,4-D methyl ester . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .579dacthal . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .568dalapon . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .580, 603dalapon methyl ester . . . . . . . . . . . . . . . . . . . . . . . . .579, 604dandelion root powder . . . . . . . . . . . . . . . . . . . . . . . . . . . .6842,4-DB . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5802,4-DB methyl ester . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .579DBOB . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5804,4'-DBOB . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .579DCAA . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .580DCAA methyl ester . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .579DCB . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .53DCPA . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .572, 5792,4'-DDD . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .534,4'-DDD . . . . . . . . . . . . . . . . .53, 89, 569, 570, 572, 635, 6392,4'-DDE . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .534,4'-DDE . . . . . . . . . . . . . . . . .53, 89, 569, 570, 572, 635, 6392,4'-DDT . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .53, 6354,4'-DDT . . . . . . . . . . . . . . . . .53, 89, 569, 570, 572, 635, 639decachlorobiphenyl . . . . . . . . . . . . . . .89, 569, 570, 583 - 585decafluorobiphenyl . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .636(+/-)δ-decalactones . . . . . . . . . . . . . . . . . . . . . . . . . . . . .613(+/-)γ-decalactones . . . . . . . . . . . . . . . . . . . . . . . . . . . . .613decanal . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .628, 633, 634decane . . . . . . . . . . . . . . . . . . . . . . . . . . . .124, 596, 610, 661n-decane . . . . . . . . . . . . . . . . . . . . . . .597, 654, 655, 661, 662decanoic acid . . . . . . . . . . . . . . . . . . . . . . . . . . . .67, 629, 631decanol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6253-decanol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .67, 631n-decyl alcohol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7061-decylamine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .39n-decyl chloride . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .706n-decyl-N,N-dimethylamine . . . . . . . . . . . . . . . . . . . . . . . .7061-dehydro-17α-methyltestosterone . . . . . . . . . . . . . . . . .687dehydroepiandrosterone (DHEA) . . . . . . . . . . . . . . . . . . . .6881-dehydrotestosterone . . . . . . . . . . . . . . . . . . . . . . . . . . . .687

For GC Chromatograms cont'd Chromatogram Search Tool: www.restek.com/chromatograms


754 www.restek.com

INDEX


1-dehydrotestosterone benzoate . . . . . . . . . . . . . . . . . . . .6871-dehydrotestosterone undecylenate . . . . . . . . . . . . . . . .687demeton-O . . . . . . . . . . . . . . . . . . . . . . . . . . . . .91, 573 - 575demeton-S . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .91, 573 - 575demeton-S-methyl . . . . . . . . . . . . . . . . . . . . . . . . . . .576, 577deoxyglucitol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .640deoxyribitol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .640desethyl-atrazine . . . . . . . . . . . . . . . . . . . . . . . . . . . .497, 582desethyl-terbuthylazine . . . . . . . . . . . . . . . . . . . . . . . . . . .582desipramine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .691desisopropylatrazine . . . . . . . . . . . . . . . . . . . . . . . . .497, 582desmethyl diazepam . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .682desmethyl methsuximide . . . . . . . . . . . . . . . . . . . . . . . . . .692dextromethorphan . . . . . . . . . . . . . . . . . . . . . . .680, 681, 683diallate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .566cis-diallate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .53trans-diallate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .531,4-diaminobutane . . . . . . . . . . . . . . . . . . . . . . . . . . . .66, 7051,2-diaminocyclohexane . . . . . . . . . . . . . . . . . . . . . . . .66, 7051,5-diamino-2-methylpentane . . . . . . . . . . . . . . . . . . .66, 7052,6-diamino-4-nitrotoluene . . . . . . . . . . . . . . . . . . . . . . . . .5932,3-diaminotoluene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5932,4-diaminotoluene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5932,6-diaminotoluene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .593diazepam . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .680 - 682diazinon . . . . . . . . . . . . . . . . . . . .91, 560, 568, 573 - 575, 635dibenzo(a,h)acridine . . . . . . . . . . . . . . . .45, 73, 98, 557, 637dibenzo(a,j)acridine . . . . . . . . . . . . .45, 73, 98, 557, 566, 637dibenzo(a,h)anthracene . . . . . . . . . . . .43, 45, 73, 87, 97, 98,

555 - 559, 561 - 568, 636 - 6387H-dibenzo(c,g)carbazole . . . . . . . . . . . .45, 73, 98, 557, 637dibenzofuran . . . . . . . . . . . . . . . . . . . . . . . . .43, 87, 561 - 567dibenzo(a,e)pyrene . . . . . . . . . . . . . . . . .45, 73, 98, 557, 637dibenzo(a,h)pyrene . . . . . . . . . . . . . . . . .45, 73, 98, 557, 637dibenzo(a,i)pyrene . . . . . . . . . . . . . . . . . .45, 73, 98, 557, 637dibromoacetic acid . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .603dibromoacetonitrile . . . . . . . . . . . . . . . . . . . . . . . . . .589, 5904,4'-dibromobiphenyl . . . . . . . . . . . . . . . . . . . . . . . . . . . . .572dibromochloromethane . . . . . . . . . . .100, 101, 103, 409, 467,

547 - 551, 589, 590, 607 - 609dibromochloropropane . . . . . . . . . . . . . . . . . . . . . . . . . . . .6071,2-dibromo-3-chloropropane . . . . . . . . . . . . . .100, 103, 411,

547 - 551, 589, 5901,2-dibromoethane . . . . . . . . . . . . . .100, 101, 103, 409, 411,

547 - 551, 589, 590, 606 - 609dibromofluoromethane . . . . . . . . . . . . . . .100, 103, 547 - 550dibromomethane . . . . . . . . . . . . . . . .100, 101, 103, 547 - 5512,3-dibromopropionic acid . . . . . . . . . . . . . . . . . . . . . . . . .6032,5-dibromotoluene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .595dibucaine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .691dibutyl phthalate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .592di-n-butyl phthalate . . . . . . . . . . . . . . . .43, 87, 554, 561 - 568dibutyl sulfate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .689, 690dibutyltin . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .592, 593dicamba . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .580dicamba methyl ester . . . . . . . . . . . . . . . . . . . . . . . . . . . . .579dichloroacetic acid . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .603dichloroacetonitrile . . . . . . . . . . . . . . . . . . . . . . . . . .589, 5901,2-dichlorobenzene . . . . . . . . . . .43, 87, 100, 101, 103, 409,

547 - 551, 561 - 567, 606 - 6091,2-dichlorobenzene-d4 . . . . . . . . . . . . . . . . . . . . . . . . . . .5511,3-dichlorobenzene . . . . . . . . . . .43, 87, 100, 101, 103, 409,

547 - 551, 561 - 567, 606 - 6091,4-dichlorobenzene . . . . . . . . . . .43, 87, 100, 101, 103, 409,

547 - 551, 554, 561 - 567, 606 - 6091,4-dichlorobenzene-d4 . . . . . . . . . . . .43, 87, 100, 103, 497,

547 - 550, 559, 561 - 565, 5673,3'-dichlorobenzidine . . . . . . . . . . . . . . . . . .43, 87, 561 - 566dichlorobenzilate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5663,5-dichlorobenzoic acid methyl ester . . . . . . . . . . . . . . . .5792,3-dichlorobiphenyl . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5831,4-dichlorobutane . . . . . . . . . . . . . . . . . . . . . . .101, 467, 548cis-1,4-dichloro-2-butene . . . . . . . . . . . . . . . . . .103, 547, 548trans-1,4-dichloro-2-butene . . . . . . . . . . . .103, 547, 548, 551dichlorodifluoromethane . . . . . . .74, 100, 101, 103, 234, 409,

547 - 551, 606, 607, 6091,1-dichloroethane . . . . . . . . . . . . . .100, 101, 103, 409, 467,

547 - 551, 606 - 6091,2-dichloroethane . . . . . . . .84, 85, 100, 101, 103, 409, 467,

547 - 551, 606 - 609, 694, 697, 700 - 702

1,2-dichloroethane-d4 . . . . . . . . . . . . . . . . . . . .103, 547, 5481,1-dichloroethene . . . . . . . .84, 85, 100, 101, 103, 409, 467,

547 - 551, 606 - 609, 694, 697, 700 - 702cis-1,2-dichloroethene . . . . . . . . . . . .83, 100, 101, 103, 409,

547 - 551, 606 - 609, 694, 697, 700trans-1,2-dichloroethene . . . . . .83, 100, 101, 103, 409, 467,

547 - 551, 607 - 609, 694, 697cis-1,2-dichloroethylene . . . . . . . . . . . . . . . . . . . . . . .701, 702trans-1,2-dichloroethylene . . . . . . . . . . . . . . . . . . . . .701, 702dichlorofenthion . . . . . . . . . . . . . . . . . . . . . . . . .91, 573 - 575dichlorofluoromethane . . . . . . . . . . . . . . . . . . . . . . . . . . . .608dichloromethane (also see

methylene chloride) . . . . . . . . .83, 607,694, 697, 700 - 7022,4-dichlorophenol . . . . . . . . . . . . . . . .43, 87, 553, 560 - 5672,6-dichlorophenol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5661,2-dichloropropane . . . . . . . . . . . . .100, 101, 103, 409, 467,

547 - 551, 606 - 6091,3-dichloropropane . . . . . . . . . . . . .100, 101, 103, 547 - 5512,2-dichloropropane . . . . . . . . . . . . .100, 101, 103, 547 - 5511,1-dichloropropanone . . . . . . . . . . . . . . . . . . . . . . . .551, 5901,1-dichloro-2-propanone . . . . . . . . . . . . . . . . . . . . . . . . . .5891,1-dichloropropene . . . . . . . . . . . . .100, 101, 103, 547 - 551cis-1,3-dichloropropene . . . . . . . . . .100, 101, 103, 409, 467,

547 - 551, 606, 608, 609trans-1,3-dichloropropene . . . . . . . .100, 101, 103, 409, 467,

547 - 551, 606, 608, 609dichlorotetrafluoroethane . . . . . . . . . . . . . . . . .409, 607 - 6091,2-dichlorotetrafluoroethane . . . . . . . . . . . . . . . . . . . . . .6061,2-dichlorotetrafluoroethene . . . . . . . . . . . . . . . . . . . . . .234dichlorprop . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .580dichlorprop methyl ester . . . . . . . . . . . . . . . . . . . . . . . . . .579dichlorvos . . . . . . . . . . . . . . . . . . . . . .91, 568, 573 - 577, 635dicrotophos . . . . . . . . . . . . . . . . . . . . . . . . . . . . .91, 573 - 575dieldrin . . . . . . . . . . . . . . . . . . . . .53, 89, 569 - 572, 635, 639diesel . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .598, 600diesel fuel #2 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .663, 666diethanolamine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .64, 703diethylamine . . . . . . . . . . . . . . . . . . . . . . . . . .46, 63, 704, 705m-diethylbenzene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .655o-diethylbenzene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .655p-diethylbenzene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .655diethylene glycol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .602di(ethyleneglycol) butyl ether . . . . . . . . . . . . . . . . . . . . . . .629diethylenetriamine . . . . . . . . . . . . . . . . . . . . . . . . . . .704, 705diethyl ether (ethyl ether) . .85, 103, 547, 548, 551, 670, 672diethyl 2-hydroxyglutarate . . . . . . . . . . . . . . . . . . . . . . . . .629diethyl malate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .629diethyl nonanedioate . . . . . . . . . . . . . . . . . . . . . . . . . . . . .629diethyl octanedioate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .629diethyl phthalate . . . . . . . . . .43, 87, 554, 561 - 568, 592, 629diethylpropion . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .676diethyl succinate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .629diethyl sulfate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .689, 6901,4-difluorobenzene . . . . . . . . . . . . .100, 548 - 550, 607, 608diglycerides . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .623diheptyl phthalate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .592dihexyl phthalate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .592dihydrocarvone . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .626trans-dihydrocarvyl acetate . . . . . . . . . . . . . . . . . . . . . . . .626diisobutyl phthalate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .629diisopropyl ether . . . . . . . . . . . . . . . . . . . .100, 103, 547 - 550di-isopropyl sulfate . . . . . . . . . . . . . . . . . . . . . . . . . . .689, 690dimethenamid . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .497dimethoate . . . . . . . . . . . . . . . . . . . . . . . . . . . . .91, 573 - 577dimethoxybenzene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6291,2-dimethoxyethane . . . . . . . . . . . . .83, 695, 698, 700 - 702N,N-dimethylacetamide . . . . . . . . . . . . . . . . . . . . . . . . . . .700dimethylamine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .63, 704dimethylaminoazobenzene . . . . . . . . . . . . . . . . . . . . . . . . .5662,6-dimethylaniline . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7053,3-dimethylbenzidine . . . . . . . . . . . . . . . . . .43, 87, 561 - 5667,12-dimethylbenzo(a)anthracene . . . . . . . . . . . . . . . . . . .566dimethylbenzothiophenes . . . . . . . . . . . . . . . . . . . . . . . . . .6642,3-dimethylbutane . . . . . . . . . . . . . . . . . . . . . . . . . . . .75, 6571,2-dimethylcyclopentane . . . . . . . . . . . . . . . . . . . . . . . . . .6571-tert-2-dimethylcyclopentane . . . . . . . . . . . . . . . . . . . . . . .75dimethyl disulfide . . . . . . . . . . . . . . . . . . . . . . . . . . . .605, 632dimethylethylamine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .63dimethylformamide . . . . . . . . . . . . . . . . . . . . . . . . . .700 - 7023,5-dimethyl-2,4(5H) furandione . . . . . . . . . . . . . . . . . . . .629

2,3-dimethylheptane . . . . . . . . . . . . . . . . . . . . . . .75, 610, 6572,6-dimethylnaphthalene . . . . . . . . . . . . . . . . . . . . . . . . . .6381,2-dimethyl-3-nitrobenzene . . . . . . . . . . . . . . . . . . . . . . .5601,3-dimethyl-2-nitrobenzene . . . . . . . . . . . . . . . . . . . . . . .5602,3-dimethylpentane . . . . . . . . . . . . . . . . . . . . . . . . . .606, 6102,4-dimethylpentane . . . . . . . . . . . . . . . . . . . . . . . . . .661, 6622,4-dimethylphenol . . . . . . . . . . . .43, 87, 553, 560 - 567, 7072,4-dimethylphenol-3,5,6-d3 . . . . . . . . . . . . . . . . . . . . . . . .5602,5-dimethylphenol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7072,6-dimethylphenol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .707α,α,α-dimethylphenylamine . . . . . . . . . . . . . . . . . . . . . . .566dimethyl phthalate . . . . . . . . . . . .43, 87, 554, 561 - 568, 592dimethyl sulfate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .690dimethyl sulfide . . . . . . . . . . . . . . . . . . . . . . . . . . . . .632, 664dimethyl sulfoxide . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6293,5-dinitroaniline . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5941,2-dinitrobenzene . . . . . . . . . . . . . . . . . . . .43, 87, 561 - 5671,3-dinitrobenzene . . . . . . . . . . . .43, 87, 561 - 567, 593, 5941,4-dinitrobenzene . . . . . . . . . . . . . . . .43, 87, 561 - 567, 5932,2'-dinitrobiphenyl . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5934,6-dinitro-2-methylphenol . . . . . . . . . . . . . .43, 87, 561 - 5671,3-dinitronaphthalene . . . . . . . . . . . . . . . . . . . . . . . . . . . .5932,4-dinitrophenol . . . . . . . . . . . . . . . . .43, 87, 553, 560 - 5672,3-dinitrotoluene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5932,4-dinitrotoluene . . . . . . . . . . . . .43, 87, 561 - 568, 593, 5942,6-dinitrotoluene . . . . . . . . . . . . .43, 87, 561 - 568, 593, 5943,4-dinitrotoluene . . . . . . . . . . . . . . . . . . . . . . . . . . . .593, 594dinoseb . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .580dinoseb methyl ester . . . . . . . . . . . . . . . . . . . . . . . . . . . . .579dioctyl phthalate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .592di-n-octyl phthalate . . . . . . . . . . . . . . . .43, 87, 554, 561 - 5681,4-dioxane . . . . . . .43, 83, 85, 87, 103, 409, 547, 561 - 566,

607 - 609, 694, 697, 700 - 702dioxathion . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .91, 573 - 575dioxins . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .95dipentyl phthalate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .592diphenamid . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .568diphenhydramine . . . . . . . . . . . . . . . . . . . . . . . .680, 681, 691diphenylamine . . . . . . . . . . . . . . . . . .561, 562, 564, 566, 567diphenyl ether . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .566diphenylhydantoin . . . . . . . . . . . . . . . . . . . . . . . . . . . .678, 6921,2-diphenylhydrazine . . . . . . . . . . . . . . . . . .43, 87, 560 - 565di-n-propyl sulfate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .690disulfoton . . . . . . . . . . . . . . . . . . . . . .91, 560, 568, 573 - 575disulfoton sulfone . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .568DMSO . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .83(+/-)δ-dodecalactones . . . . . . . . . . . . . . . . . . . . . . . . . . .613(+/-)γ-dodecalactones . . . . . . . . . . . . . . . . . . . . . . . . . . .613dodecanal . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .625dodecane . . . . . . . . . . . . . .124, 596, 597, 607, 610, 633, 661n-dodecane . . . . . . . . . . . . . . . . . . . . . .80, 597, 655, 661, 662dodecanoic acid . . . . . . . . . . . . . . . . . . . . . . . . . .67, 629, 631dodecanol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .629n-dodecyl alcohol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .706n-dodecyl chloride . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .706n-dodecyl-N,N-dimethylamine . . . . . . . . . . . . . . . . . . . . . .706dotricontane . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .124, 661doxepin . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .691doxylamine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .691ecgonine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .673ecgonine methyl ester . . . . . . . . . . . . . . . . . . . . . . . . . . . .673eicosane . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .124, 661γ-elemene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .627, 628endosulfan I . . . . . . . . . . . . . .53, 89, 569, 570, 572, 635, 639endosulfan II . . . . . . . . . . . . .53, 89, 569, 570, 572, 635, 639endosulfan sulfate . . . . . . . . .53, 89, 569, 570, 572, 635, 639endrin . . . . . . . . . . . . . . . . . .53, 89, 569 - 572, 590, 635, 639endrin aldehyde . . . . . . . . . . .53, 89, 569, 570, 572, 590, 639endrin ketone . . . . . . . . . . . . . . . . .53, 89, 569, 570, 590, 639enflurane . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .671ephedrine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .676, 677, 691EPN . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .91, 573 - 575Eptam . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .581EPTC . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .497, 568erucic acid . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .59, 64617α-estradiol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .68817β-estradiol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .688estragole . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .61estrone . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .688ethalfluralin . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .497



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INDEX


ethane . . . . . . . . . . . . .76, 129, 131, 606, 647, 649 - 654, 664ethanol . . . . . . . .58, 75, 80, 82, 85, 100, 111, 549, 550, 628,

630, 642, 657, 661, 662, 667, 670, 701, 702ethion . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .91, 573 - 577ethoprop . . . . . . . . . . . . . . . . . . . . . . . . . . .91, 568, 573 - 575ethosuximide . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .678, 692ethotoin . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .692ethyl acetate . . . . . . . .85, 100, 103, 409, 547, 549, 550, 609,

628, 630, 634, 670, 701, 702ethylamine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .704N-ethylamphetamine . . . . . . . . . . . . . . . . . . . . . . . . . .65, 675ethylbenzene . . . . . . . . . . . . .75, 83, 100, 101, 103, 409, 467,

547 - 551, 595, 597, 606, 608 - 610, 633, 634, 654, 655, 657, 694, 697, 700 - 702

ethylbenzene sulfonate . . . . . . . . . . . . . . . . . . . . . . .689, 690ethyl-tert-butyl ether . . . . . . . . . . . . . . . .100, 103, 547 - 550ethyl butyrate . . . . . . . . . . . . . . . . . . . . . . . . . . .626, 628, 641ethyl chloride . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .672ethyl decanoate . . . . . . . . . . . . . . . . . . . . . . . . . .67, 629, 631ethyl dodecanoate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .629ethylene . . . . . . . . . . .76, 129, 606, 647, 649, 650, 652 - 654ethylenediamine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .704ethylene glycol . . . . . . . . . . . . . . . . . . . . . . . . . .601, 602, 668ethylene oxide . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .85, 707ethyl formate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .630ethyl hexadecanoate . . . . . . . . . . . . . . . . . . . . . . . . . . . . .629ethyl 9-hexadecanoate . . . . . . . . . . . . . . . . . . . . . . . . . . . .6292-ethyl-1-hexanol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6052-ethylhexyl phthalate . . . . . . . . . . . . . . . . . . . . . . . . . . . .592ethyl homovanillate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .629ethyl (R)-(+)-3-hydroxybutyrate . . . . . . . . . . . . . . . . . . . .614ethyl (S)-(+)-3-hydroxybutyrate . . . . . . . . . . . . . . . . . . . .614ethyl γ-lactone 2-hydroxyglutarate . . . . . . . . . . . . . . . . . .629ethyl laurate . . . . . . . . . . . . . . . . . . . . . . . . . . . . .67, 626, 631ethyl linoleate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .629ethyl mercaptan . . . . . . . . . . . . . . . . . . . . . . . . . . . . .632, 664ethyl methacrylate . . . . . . . . . .100, 103, 547 - 551, 566, 607ethyl methanesulfonate . . . . . . . . . . . . . . . . . . . . . . .566, 6901-ethyl-2-methylbenzene . . . . . . . . . . . . . . . . . . . . . . . . . .655(R)-ethyl 2-methylbutyrate . . . . . . . . . . . . . . . . . . . . . . . . .614(S)-ethyl 2-methylbutyrate . . . . . . . . . . . . . . . . . . . . . . . . .614ethyl myristate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .67, 631ethyl octanoate . . . . . . . . . . . . . . . . . . . . . . . . . . .67, 629, 631ethyl palmitate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .67, 6313-ethylpentane . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .75, 657m-ethylphenol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .707o-ethylphenol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .707p-ethylphenol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .707ethyl propionate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .628ethyl stearate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .629ethyl tetradecanoate . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6292-ethylthiophene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6644-ethyltoluene . . . . . . . . . . . . . . . . . . . . . . . . . . .409, 608, 609p-ethyltoluene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .606ethyl toluenesulfonate . . . . . . . . . . . . . . . . . . . . . . . .689, 690ethyl undecanoate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .629ethyl vanillate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .629ethyl vanillin . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .626etridiazole . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .568, 572etrimphos . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .635eucalyptol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .61, 612, 641eugenol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .61, 626, 627FAMEs

cis/trans Isomers . . . . . . . . . . . . . . . . . . . . . . . . . . . .619Marine Oil Standard . . . . . . . . . . . . . . . . . . .70, 620, 621NLEA Mix . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .57, 618PUFA, Animal Source . . . . . . . . . . . . . . . . . . . . . . . . .621Saw Palmetto . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .621Vegetable Oils . . . . . . . . . . . . . . . . . . . . . . . . . . .621, 622

famphur . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .91, 573 - 575trans-β-farnesene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .626farnesol 1 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .61farnesol 2 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .61fatty acid ester . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .629fatty acids (free) . . . . . . . . . . . . . . . . . . . . . . . . . . . . .615, 616fenamiphos . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .568fenarimol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .568fenfluramine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .676, 677(+)-fenfluramine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .686(-)-fenfluramine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .686

fenitrothion . . . . . . . . . . . . . . . . . . . . . . . . .91, 573 - 575, 635fensulfothion . . . . . . . . . . . . . . . . . . . . . . . . . . . .91, 573 - 575fenthion . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .91, 573 - 575flunitrazepam . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .680 - 682fluoranthene . . . . . . . . . . . .43, 45, 73, 87, 97, 98, 555 - 559,

561 - 568, 636 - 638fluorene . . . . . . . . . . . . . . . .43, 45, 73, 87, 97, 98, 555 - 559,

561 - 568, 636 - 638fluorobenzene . . . . . . . . . . . . . . . . . .101, 103, 467, 547, 5512-fluorobiphenyl . . . . . . . . . . . . . . .43, 87, 97, 497, 554, 556,

559, 561 - 567, 5961-fluoronaphthalene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .612-fluorophenol . . . . . . . . . . . . . . .43, 87, 497, 559, 561 - 567fluoxymesterone . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .687flurazepam . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .680 - 682fluridone . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .568fonofos . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .497, 560fonophos . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .91, 573 - 575formaldehyde . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .703formic acid . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .629Freon 11 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .409, 609, 706Freon 12 . . . . . . . . . . . . . . . . . . . . . . .409, 609, 649, 706, 707Freon 21 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .706Freon 22 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .706Freon 113 . . . . . . . . . . . . . . . . . . . . . . . . . .101, 409, 548, 609Freon 114 . . . . . . . . . . . . . . . . . . . . . .234, 409, 609, 649, 706Freon 114A isomer . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .706Freon 133a . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .649Freon 134a/22 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .649Freon TF . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .608fucitol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6402(5H)-furanone . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .629furans . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .95furfural . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .628, 629, 633furfuryl alcohol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .629gadoleic acid . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .59, 646galactitol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .640GBL (γ-butyrolactone) . . . . . . . . . . . . . . . . . . . . . . . .668, 669GBL-d6 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .668geosmin . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .605geranial . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .625, 628geraniol . . . . . . . . . . . . . . . . . . . . . . . .61, 612, 625 - 627, 641geranyl acetate . . . . . . . . . . . . . . . . . . . . . . . . . . . . .625 - 628germacrene-Δ . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .626, 627GHB (γ-hydroxybutyrate) . . . . . . . . . . . . . . . . . . . . . . . . . .669glucitol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .640glucoheptitol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .640glutethimide . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .678, 679glyceraldehyde . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .640glycerol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .602GOAL . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .581guaiacol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .629guaifenesin . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .683haloperidol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .680, 681halothane . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .671helium . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .648heneicosane . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .596n-heneicosane . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .597heptachlor . . . . . . . . . . . . . . .53, 89, 569 - 572, 590, 635, 639heptachlor epoxide . . . . . . . .53, 89, 568 - 572, 590, 635, 6392,2',3,3',4,4',5-heptachlorobiphenyl . . . . . . . . . . . . . . . . . .5832,2',3,4,4',5,5'-heptachlorobiphenyl . . . . . . . . . . . . . . . . . .5832,2',3,4,4',5',6-heptachlorobiphenyl . . . . . . . . . . . . . . . . . .5832,2',3,4',5,5',6-heptachlorobiphenyl . . . . . . . . . . . . . . . . . .583n-heptadecane . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .662(+/-)δ-heptalactones . . . . . . . . . . . . . . . . . . . . . . . . . . . .613(+/-)γ-heptalactones . . . . . . . . . . . . . . . . . . . . . . . . . . . .613heptane . . . . . . . . . . . . . . . .85, 124, 409, 607, 609, 610, 661n-heptane . . . . . . . . . . . . . . . . . . . . . .606, 608, 654, 661, 662heptanes . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .651heptanoic acid . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .615, 629heptanol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6252-heptanone . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .605, 6074-heptanone . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .633, 634n-heptyl phenol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .592hexachlorobenzene . . . . . . . . . . . . . . . .43, 53, 87, 561 - 568,

571, 572, 590, 6352,2',3,4,4',5'-hexachlorobiphenyl . . . . . . . . . . . . . . . . . . . .5832,2',3,4,5,5'-hexachlorobiphenyl . . . . . . . . . . . . . . . . . . . . .5832,2',3,5,5',6-hexachlorobiphenyl . . . . . . . . . . . . . . . . . . . . .583

2,2',4,4',5,5'-hexachlorobiphenyl . . . . . . . . . . . . . . . . . . . .583hexachlorobutadiene . . . . . . . . . .43, 87, 100, 101, 548 - 551,

561 - 567, 606 - 608hexachloro-1,3-butadiene . . . . . . . . . . . . .103, 409, 547, 609hexachlorocyclopentadiene . . . . . . . . . .43, 53, 87, 561 - 568,

571, 572, 590hexachloroethane . . . . . . . . . . . . . . . . .43, 87, 551, 561 - 567hexachloropropene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .566hexadecane . . . . . . . . . . . . . . . . . . . . . . . . . . . .124, 596, 661n-hexadecane . . . . . . . . . . . . . . . . . . . . . . . . . . .597, 661, 662hexadecanoic acid . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .629hexadecanol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .629hexadecyl hexadecanoate . . . . . . . . . . . . . . . . . . . . . . . . .611n-hexadecyl alcohol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .706n-hexadecyl chloride . . . . . . . . . . . . . . . . . . . . . . . . . . . . .706n-hexadecyl-N,N-dimethylamine . . . . . . . . . . . . . . . . . . . .706(+/-)δ-hexalactones . . . . . . . . . . . . . . . . . . . . . . . . . . . . .613hexamethylenediamine . . . . . . . . . . . . . . . . . . . . . . . .66, 705hexamethyleneimine . . . . . . . . . . . . . . . . . . . . . . . . . .66, 705hexamethylphosphoramide . . . . . . . . . . . . . . . . .91, 573 - 575hexanal . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .633n-hexanal . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .628hexane . . . . . . . . . . . . .83, 124, 131, 409, 596, 609, 610, 628,

652, 655, 661, 664, 670, 695, 698, 700n-hexane . . . . . . . .76, 85, 597, 606, 608, 654, 661, 662, 7021,6-hexanediol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .39hexanes . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .651, 653hexanoic acid . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6292-hexanone . . . . . . . . . . . . . . . .83, 100, 103, 547 - 551, 605,

607, 695, 698, 700 - 7033-hexanone . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .605hexatriacontane . . . . . . . . . . . . . . . . . . . . . . . . .124, 596, 661n-hexatriacontane . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .597hexazinone . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .568, 581trans-2-hexenal . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .628hexene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .652trans-2-hexenol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .626hexobarbital . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .679(+/-)-hexobarbital . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .686hexyl cinnamal 1 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .61hexyl cinnamal 2 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .61n-hexyl phenol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .592HMMA . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .65, 675α-humulene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .625hydrocodone . . . . . . . . . . . . . . . . . . . . . . . . . . . .673, 674, 683hydrogen . . . . . . . . . . . . . . . . . . . . . . . . . .109, 130, 647, 648hydrogen sulfide . . . . . . . . . . . . . . . . . . . . . . . . . . . . .632, 664hydromorphone . . . . . . . . . . . . . . . . . . . . . . . . . . . . .673, 6741-hydroxy-2,3-butadione . . . . . . . . . . . . . . . . . . . . . . . . . .629γ-hydroxybutyrate (GHB) . . . . . . . . . . . . . . . . . . . . . . . . . .6694-hydroxycinnamic acid . . . . . . . . . . . . . . . . . . . . . . . . . . .629hydroxycitronellal . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .641hydroxycitronellol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .61hydroxymethylfurfural . . . . . . . . . . . . . . . . . . . . . . . . . . . .6291-hydroxy-2-propanone acetate . . . . . . . . . . . . . . . . . . . . .629(+/-)ibuprofen . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .687imipramine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .691indeno(1,2,3-cd)pyrene . . . . . . . . . . . . .43, 45, 73, 87, 97, 98,

555 - 559, 561 - 568, 636 - 638inositol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .640iodomethane . . . . . . . . . . . . . . . . . . . . . . . .103, 547, 548, 551α-ionone . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .626, 628β-ionone . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .626, 628(+)-(2R)-β-irone . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .613(-)-(2R)-β-irone . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .613(+)-(2R,6S)-cis-α-irone . . . . . . . . . . . . . . . . . . . . . . . . . . .613(-)-(2S,6R)-cis-α-irone . . . . . . . . . . . . . . . . . . . . . . . . . . . .613(+)-(2R,6S)-cis-γ-irone . . . . . . . . . . . . . . . . . . . . . . . . . . .613(-)-(2S,6R)-cis-γ-irone . . . . . . . . . . . . . . . . . . . . . . . . . . . . .613(+)-(2S,6S)-trans-α-irone . . . . . . . . . . . . . . . . . . . . . . . . .613(-)-(2R,6R)-trans-α-irone . . . . . . . . . . . . . . . . . . . . . . . . . .613(+)-(2R,6R)-trans-γ-irone . . . . . . . . . . . . . . . . . . . . . . . . .613(-)-(2S,6S)-trans-γ-irone . . . . . . . . . . . . . . . . . . . . . . . . . . .613isoamyl alcohol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .630isoamyl decanoate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .629isoamyl octanoate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .629isoborneol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .605(+/-)isoborneol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .612isobutane . . . . . . . . . . . . . .76, 129, 131, 606, 649 - 654, 664isobutanol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .58, 630, 642



756 www.restek.com

INDEX


isobutene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .129isobutyl alcohol . . . . . . . . . . . . . . . . . . . . .100, 103, 547 - 550isobutyl decanoate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .629isobutylene . . . . . . . . . . . . . . . . .76, 129, 649, 650, 652 - 654isobutyl phthalate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .592isobutyric acid . . . . . . . . . . . . . . . . . . . . . . .67, 615, 629, 631isocaproic acid . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .615isodrin . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .53, 566isoeugenol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .61isoflurane . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .671isoheptane . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .606isohexane . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .606isomenthone . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .612α-isomethyl ionone 1 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .61α-isomethyl ionone 2 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .61isopentane . .76, 129, 131, 606, 610, 650 - 654, 661, 662, 664isophorone . . . . . . . . . . . . . . . . . . . . . . . . . .43, 87, 561 - 568isopropanol . . . . . . . . . . . . . . . . . . .58, 82, 85, 607, 630, 633,

642, 643, 667, 670, 7042-isopropyl-3-methoxypyrazine . . . . . . . . . . . . . . . . . . . . .605isopropyl acetate . . . . . . . . . . . . . . . .100, 103, 547, 549, 550isopropyl alcohol . . . . . . . . . . . . . . . . .80, 409, 608, 609, 628isopropylamine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .46, 704isopropyl benzene . . .100, 101, 103, 547 - 551, 607, 610, 654isopropyl methanesulfonate . . . . . . . . . . . . . . . . . . . .689, 6904-isopropyltoluene . . . . . . . . . . . . . . . . . . . . . . . . . . .103, 547p-isopropyltoluene . . . . . . . . . . . . . .100, 101, 548 - 551, 610isopropyl toluenesulfonate . . . . . . . . . . . . . . . . . . . . .689, 690isosafrole . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .566isovaleric acid . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .615, 629cis-jasmone . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .626jet fuel . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .599kepone . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .53, 566kerosene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .663, 665ketamine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .680, 6812-keto-3-deoxyoctanate . . . . . . . . . . . . . . . . . . . . . . . . . . .640cis-lactone . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .67, 631trans-lactone . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .67, 631leptophos . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .91, 573 - 575levorphanol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .673lidocaine . . . . . . . . . . . . . . . . . . . . . . . . . . .672, 680, 681, 691lignoceric acid . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .59, 646lilial . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .61limonene . . . . . . . . . . . . . . . . . . . . . . . .61, 625, 627, 641, 643(-/+)limonene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .612δ-limonene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .628l-limonene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .626trans-limonene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .628cis-limonene monoxide . . . . . . . . . . . . . . . . . . . . . . . . . . . .628trans-limonene monoxide . . . . . . . . . . . . . . . . . . . . . . . . . .628linalool . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .61, 625 - 628(-/+)linalool . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .612(-)-(R)-linalool . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .612(+)-(S)-linalool . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .612linalyl acetate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .626linoleic acid . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .59, 646linolenic acid . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .59, 646lorazepam . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .682lyral 1 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .61lyral 2 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .61malathion . . . . . . . . . . . . . . . . . . . . . . . . . .91, 573 - 577, 635mannitol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .640maprotyline . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .691MBDB . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .65, 675MCPA . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .580MCPA methyl ester . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .579MCPP . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .580MCPP methyl ester . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .579MDA . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .675MDEA . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .675MDMA . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .675medazepam . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .680 - 682melamine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .638menthofuran . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .626l-menthol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .626menthone . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .612l-menthone . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .626meperidine . . . . . . . . . . . . . . . . . . . . . . . . . . . . .673, 680, 681mephentermine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .676mephenytoin . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .692

mephobarbital . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .679(+/-)-mephobarbital . . . . . . . . . . . . . . . . . . . . . . . . . . . . .686meprobamate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .678, 679merphos . . . . . . . . . . . . . . . . . . . . . . . . . . .91, 568, 573 - 575merphos oxide . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .568merphos oxone . . . . . . . . . . . . . . . . . . . . . . . . . .91, 573 - 575mesitylene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .655mesterolone . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .687metachlor . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .572methacrifos . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .635methacrylonitrile . . . . . . . . . . . . . . . .103, 547, 548, 551, 607methadone . . . . . . . . . . . . . . . . . . . . . . . . . . . . .673, 680, 681methamidophos . . . . . . . . . . . . . . . . . . . . . . . . . . . . .576, 577methamphetamine . . . . . . . . . . . . . . . . . . .65, 675 - 677, 680(+)methamphetamine . . . . . . . . . . . . . . . . . . . . . . . . . . . .686(-)methamphetamine . . . . . . . . . . . . . . . . . . . . . . . . . . . . .686methane . . . . . . . . . . . . . . .76, 109, 129 - 131, 647 - 654, 664methanol . . . . . . . . . . . . . . . .58, 63, 80, 82, 83, 85, 595, 628,

630, 642, 667, 670, 694, 697, 700 - 703methapyrilene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .566, 691methaqualone . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .678, 679methcathinone . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .676methidathion . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .576, 577methohexital . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .679p-methoxyamphetamine (PMA) . . . . . . . . . . . . . . . . . .65, 675methoxychlor . . . . . . . . . . . . . . . .53, 89, 569 - 572, 590, 639methoxyflurane . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .671p-methoxymethamphetamine (PMMA) . . . . . . . . . . . .65, 675methsuximide . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .692methyl acetate . . . . . . . . . . . . . . . . . . . . . . . . . .103, 547, 548methyl acetylene . . . . . . . . . . . . . . . . . . . . . . . . . . . .650, 652methyl acrylate . . . . . . . . . . . . . . . . . . . . .100, 103, 547 - 551methylamine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .70417α-methylandrostan-17β-ol-3-one . . . . . . . . . . . . . . . . .68717α-methyl-5-androstene-3β,17β-diol . . . . . . . . . . . . . . .687methylbenzene sulfonate . . . . . . . . . . . . . . . . . . . . . .689, 690methylbenzothiophenes . . . . . . . . . . . . . . . . . . . . . . . . . . .664methyl bromochloroacetate . . . . . . . . . . . . . . . . . . . . . . . .604methyl bromodichloroacetate . . . . . . . . . . . . . . . . . . . . . .6042-methylbutane . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6622-methyl-1-butanol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6052-methyl-2-butanol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6053-methyl-2-butanol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6052-methyl-1-butene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6062-methyl-2-butene . . . . . . . . . . . . . . . . . . . . . . . .76, 653, 6542-methylbutene-2 . . . . . . . . . . . . . . . . . . . . . . . . .75, 129, 6573-methyl-1-butene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .129methyl tert-butyl ether . . . . . . . . .75, 80, 100, 101, 103, 409,

547 - 551, 595, 608 - 610, 657, 670, 672methyl-d3-tert-butyl ether . . . . . . . . . . . . . . . . . . . . . . . . .548methyl butyl ketone . . . . . . . . . . . . . . . . . . . . . .409, 608, 609(R)-2-methylbutyrate . . . . . . . . . . . . . . . . . . . . . . . . . . . . .614(S)-2-methylbutyrate . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6142-methylbutyric acid . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .629methyl Cellosolve . . . . . . . . . . . . . . . . . . . . . . . . . . . . .58, 642methyl chlorodibromoacetate . . . . . . . . . . . . . . . . . . . . . .6043-methylcholanthrene . . . . . . . . . . .45, 73, 98, 557, 566, 637methylcyclohexane . . . . . . . . . . .83, 606, 694, 697, 700 - 702methyl cyclopentane . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6061-methylcyclopentene . . . . . . . . . . . . . . . . . . . . . . . . .75, 657methylcyclopentenolone . . . . . . . . . . . . . . . . . . . . . . . . . . .629methyl decanoate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .629methyl dibromoacetate . . . . . . . . . . . . . . . . . . . . . . . . . . .604methyl 2,3-dibromopropionate . . . . . . . . . . . . . . . . . . . . . .604methyl dichloroacetate . . . . . . . . . . . . . . . . . . . . . . . . . . . .604methyldiethylamine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .634-methyl-2,5-dimethoxyamphetamine . . . . . . . . . . . . . . . .6762-methyl-4,6-dinitrophenol . . . . . . . . . . . . . . . . . . . . .553, 560methyl dodecanoate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .629α-methylene-γ-butyrolactone (AMGBL) . . . . . . . . . . . . . . .669methylene chloride (dichloromethane) . . . .85, 100, 101, 103,

409, 467, 547 - 551, 606, 608, 609, 628, 633, 670, 672, 700, 702

methylenedioxyamphetamine . . . . . . . . . . . . . . .65, 675 - 677methylenedioxyethylamphetamine . . . . . . . . . . . .65, 675, 676methylenedioxymethamphetamine . . . . . . . . . . .65, 675 - 677methylethylamine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .631-methylethylbenzene . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6331,2-methylethylbenzene . . . . . . . . . . . . . . . . . . . . . . . .75, 6571-methyl-3-ethylbenzene . . . . . . . . . . . . . . . . . . . . . . . . . .610

methyl ethyl ketone . . . . . .85, 409, 607 - 609, 656, 670, 672methyl eugenol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .612-methyl-furan . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6053-methyl-furan . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6055-methyl furfural . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6294-methylguaiacol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .629methyl heptadecanoate . . . . . . . . . . . . . . . . . . . . . . . .59, 6466-methyl-5-hepten-2-one . . . . . . . . . . . . . . . . . . . . . . . . . .625methyl hexadecanoate . . . . . . . . . . . . . . . . . . . . . . . . . . . .6293-methylhexane . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .606methyl (R)-(+)-3-hydroxybutyrate . . . . . . . . . . . . . . . . . . .614methyl (S)-(+)-3-hydroxybutyrate . . . . . . . . . . . . . . . . . . .614methyl isobutyl ketone . . . . . . . . . . . . . . . .409, 608, 609, 670methyl mercaptan . . . . . . . . . . . . . . . . . . . . . . . . . . .632, 664methyl methacrylate . . . . . . . . . . . . . . . . .100, 103, 547 - 551methyl methanesulfonate . . . . . . . . . . . . . . . . .566, 689, 690methyl monobromoacetate . . . . . . . . . . . . . . . . . . . . . . . .604methyl monochloroacetate . . . . . . . . . . . . . . . . . . . . . . . . .604methyl myristate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .67, 6311-methylnaphthalene . . . . . . . . . . .43, 45, 73, 75, 87, 97, 98,

556 - 558, 561 - 567, 636 - 638, 6572-methylnaphthalene . . . . . . . . . . . . . .43, 45, 73, 87, 97, 98,

556 - 558, 561 - 567, 636 - 6382-methyl-5-nitroaniline . . . . . . . . . . . . . . . . . . . . . . . . . . . .5665-methylnonane . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .75, 657methyl nonanoate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .39methyl-2-nonynoate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .61methyl 8-octadecenoate . . . . . . . . . . . . . . . . . . . . . . . . . . .629methyl-2-octynoate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .61methyl paraoxon . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5682-methylpentane . . . . . . . . . . . . . . . . . . . . . . . .595, 661, 6623-methylpentane . . . . . . . . . . . . . . . . . . . . . . . . . . . . .597, 6064-methyl-2-pentanone . . . . . . .100, 103, 547 - 551, 607, 7031-methylphenanthrene . . . . . . . . . . . . . . . . . . . . . . . . . . . .638methylphenidate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6772-methylphenol . . . . . . . . . . . . . . . . . . . . . . .43, 87, 560 - 5673-methylphenol . . . . . . . . . . . . . . . . . . . . . . .43, 87, 561 - 5674-methylphenol . . . . . . . . . . . . . . . . . . . . . . .43, 87, 561 - 5672-methyl propane . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6622-methyl-1-propanol . . . . . . . . . . . . . . . . . . . . . . . . . .605, 6331-methyl-2-pyrrolidinone . . . . . . . . . . . . . . . . . . . . . . . . . .705methyl stearate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .629α-methylstyrene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .60717α-methyltestosterone . . . . . . . . . . . . . . . . . . . . . . . . . .687methyl tetradecanoate . . . . . . . . . . . . . . . . . . . . . . . . . . . .6292-methylthiophene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6643-methylthiophene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6644-methyltoluene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .606methyl toluenesulfonate . . . . . . . . . . . . . . . . . . . . . . .689, 690methyl tribromoacetate . . . . . . . . . . . . . . . . . . . . . . . . . . .604methyl trichloroacetate . . . . . . . . . . . . . . . . . . . . . . . . . . .604methyprylon . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .678, 679metolachlor . . . . . . . . . . . . . . . . . . . . . . . . . . . .497, 568, 590metribuzin . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .497, 568, 572mevinphos . . . . . . . . . . . . . . . . . . . . . . . . . .91, 568, 573 - 575MGK-264 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .568Mineral Spirits . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .666Mirex . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .53molinate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5686-monoacetylmorphine . . . . . . . . . . . . . . . . . . . . . . . . . . . .674monobromoacetic acid . . . . . . . . . . . . . . . . . . . . . . . . . . . .603monobutyltin . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .592, 593monochloroacetic acid . . . . . . . . . . . . . . . . . . . . . . . . . . . .603monocrotophos . . . . . . . . . . . . . . . . . . . . . . . . . .91, 573 - 575monoethanolamine . . . . . . . . . . . . . . . . . . . . . . . .64, 703, 704morphine . . . . . . . . . . . . . . . . . . . . . . . . . .673, 674, 680, 681morpholine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .705motor oil . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .598, 663myrcene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .625, 626, 628β-myrcene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .626myristic acid . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .59, 646naled . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .91, 573 - 575nalorphine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6731-naphthalenamine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .566naphthalene . . . . . . . . . . . . . .43, 45, 73, 75, 87, 97, 98, 100,

101, 103, 547 - 551, 555 - 559, 561 - 568, 595, 597, 607, 636 - 638, 657

naphthalene-d8 . . .43, 87, 497, 554, 559, 561 - 565, 567, 6351,4-naphthoquinone . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5662-naphthylamine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .566



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napropamide . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .568neo-Pentane . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .651neral . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .625, 628nerol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .625 - 627nerolidol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .629nervonic acid . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .59, 646neryl acetate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .625 - 628nicotine . . . . . . . . . . . . . . . . . . . . . . . . . . . .676, 680, 681, 7052-nitroaniline . . . . . . . . . . . . . . . . . . . . .43, 87, 561 - 567, 7053-nitroaniline . . . . . . . . . . . . . . . . . . . . . . . . .43, 87, 561 - 5674-nitroaniline . . . . . . . . . . . . . . . . . . . . . . . . .43, 87, 561 - 5674-nitroanisole . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .579nitrobenzene . . . .43, 87, 100, 103, 547 - 551, 560 - 567, 594nitrobenzene-d5 . . . . . . . . . .43, 87, 497, 554, 559, 561 - 5673-nitrobiphenyl . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .593nitrogen . . . . . . . . . . . . . . . . . . . . . . . . . . .109, 130, 647, 648nitroglycerine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .594nitromethane . . . . . . . . . . . . . . . . . . .83, 695, 698, 700 - 7022-nitrophenol . . . . . . . . . . . . . . . .43, 87, 553, 560 - 567, 7054-nitrophenol . . . . . . . . . . . . . . . . . . . .43, 87, 553, 560 - 5672-nitropropane . . . . . . . . . . . . . . . . . . . . . .103, 547, 548, 5514-nitroquinoline-1-oxide . . . . . . . . . . . . . . . . . . . . . . . . . . .566N-nitroso-n-butylamine . . . . . . . . . . . . . . . . . . . . . . . . . . . .566N-nitrosodibutylamine . . . . . . . . . . . . . . . . . . . . . . . . . . . .706N-nitrosodiethylamine . . . . . . . . . . . . . . . . . . . . . . . .566, 706N-nitrosodiisopropylamine . . . . . . . . . . . . . . . . . . . . . . . . .706N-nitrosodimethylamine . . . . . . . . . . . .43, 87, 561 - 567, 706N-nitrosodiphenylamine . . . . . . . . . . . . . . . .43, 87, 561 - 565N-nitrosodipropylamine . . . . . . . . . . . . . . . . . . . . . . . . . . .706N-nitrosomethylethylamine . . . . . . . . . . . . . . . . . . . . . . . .5664-nitrosomorpholine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .566N-nitrosomorpholine . . . . . . . . . . . . . . . . . . . . . . . . . . . . .706N-nitrosopiperidine . . . . . . . . . . . . . . . . . . . . . . . . . .566, 706N-nitroso-di-n-propylamine . . . . . . . . . . . . .43, 87, 561 - 567N-nitrosopyrrolidine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .706nitrosopyrrolydine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5662-nitrotoluene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .593, 5943-nitrotoluene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .593, 5944-nitrotoluene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .593, 5942-nitro-m-xylene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .568cis-nonachlor . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .571trans-nonachlor . . . . . . . . . . . . . . . . . . . . . . . . . . . . .568, 5712,2',3,3',4,4',5,5',6-nonachlorobiphenyl . . . . . . . . . . . . . . . .583(+/-)δ-nonalactones . . . . . . . . . . . . . . . . . . . . . . . . . . . . .613(+/-)γ-nonalactones . . . . . . . . . . . . . . . . . . . . . . . . . . . . .613nonanal . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .625, 628, 634nonane . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .124, 610, 661n-nonane . . . . . . . . . . . . . . . . . . . . . . . . . .595, 606, 654, 655nonanoic acid . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .629nonyl acetate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .625n-nonyl phenol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .592nootketone . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .626, 628(+)-norfenfluramine . . . . . . . . . . . . . . . . . . . . . . . . . . . . .686(-)-norfenfluramine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .686norflurazon . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .56819-nortestosterone . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .68719-nortestosterone-17-propionate . . . . . . . . . . . . . . . . . .687nortriptyline . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .691cis-ocimene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .626octacosane . . . . . . . . . . . . . . . . . . . . . . . . . . . . .124, 596, 661n-octacosane . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .597octadecane . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .124, 661n-octadecyl alcohol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .706n-octadecyl-N,N-dimethylamine . . . . . . . . . . . . . . . . . . . . .706(+/-)δ-octalactones . . . . . . . . . . . . . . . . . . . . . . . . . . . . .613(+/-)γ-octalactones . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .613octanal . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .625, 628octane . . . . . . . . . . . . . . . . . . . . .124, 596, 607, 610, 661, 662n-octane . . . . . . . . . . . . . . . . . . . . . . .597, 654, 655, 661, 662octanoic acid . . . . . . . . . . . . . . . . . . . . . . . . . . . .67, 629, 631octanol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .625, 626, 6281-octanol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6053-octanol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .605, 6263-octanone . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6051-octen-3-ol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .605(+/-)1-octen-3-ol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .613octyl acetate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6253-octyl acetate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .626n-octyl alcohol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .706octylamine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .705

n-octyl chloride . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .706n-octyl-N,N-dimethylamine . . . . . . . . . . . . . . . . . . . . . . . . .706n-octyl phenol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .592tert-octyl phenol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .592oleic acid . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .59, 646omethoate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .576, 577Ordram . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .581oxadiazon . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .581oxazepam . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .682oxychlordane . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .635oxycodone . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .673, 674oxygen . . . . . . . . . . . . . . . . . . . . . . . . . . . .109, 130, 647, 648oxymethalone . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .687oxymorphone . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .673Paarlan . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .581palmitic acid . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .59, 646palmitoleic acid . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .59, 646papaverine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .680, 681parathion-ethyl . . . . . . . . . . . . . . . . . . . . . . . . . .91, 573 - 575parathion-methyl . . . . . . . . . . . . . . . . . . . . . . . . .91, 573 - 575pebulate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .568PEMA . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .692pendimethalin . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .497pentachloroanisole . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .579pentachlorobenzene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5662,2',3,4,5'-pentachlorobiphenyl . . . . . . . . . . . . . . . . . . . . . .5832,2',4,5,5'-pentachlorobiphenyl . . . . . . . . . . . . . . . . . . . . . .5832,3,3',4',6-pentachlorobiphenyl . . . . . . . . . . . . . . . . . . . . . .583pentachloroethane . . . . . . . . . . . . . .100, 103, 547 - 551, 566pentachloronitrobenzene . . . . . . . . . . . . . . . . . . . . . .566, 572pentachlorophenol . . . . . . . . . . . . . . . .43, 87, 553, 560 - 568pentadecane . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .39n-pentadecane . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .661, 662pentafluorobenzene . . . . . . . . . . . . . . . . .100, 467, 548 - 550(+/-)δ-pentalactones . . . . . . . . . . . . . . . . . . . . . . . . . . . .613pentamethylenediamine . . . . . . . . . . . . . . . . . . . . . . . .66, 705pentane . . . . . . . . . . . . . . . . . . . . . . .124, 129, 131, 661, 664n-pentane . . . . . .76, 129, 595, 606, 650 - 654, 661, 662, 7022-pentanol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .605pentatriacontane . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .596n-pentatriacontane . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5971-pentene . . . . . . . . . . . . . . . . . . . . . . . . . . .76, 129, 653, 654cis-2-pentene . . . . . . . . . . . . . . . . . . . .76, 129, 606, 653, 654trans-2-pentene . . . . . . . . . . . . . . . . . . . . . .76, 129, 606, 653pentobarbital . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .678, 679n-pentyl phenol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5922-pentyl-furan . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .605cis-permethrin . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .568, 572trans-permethrin . . . . . . . . . . . . . . . . . . . . . . . . . . . .568, 572perylene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .638perylene-d12 . . . . . . . . . . . . . . . . . .43, 87, 97, 497, 554, 556,

559, 561 - 565, 567, 568, 635PETN . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .594α-phellandrene . . . . . . . . . . . . . . . . . . . . . . . . .625, 626, 628phenacetin . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .566, 672phenanthrene . . . . . . . . . . . . . . . . . . . .43, 45, 73, 87, 97, 98,

555 - 559, 561 - 568, 636 - 638phenanthrene-d10 . . . . . . . . . . . . . . . . . . . . .43, 87, 497, 554,

559 - 565, 567, 568, 635, 636phencyclidine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .680phendimetrazine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .676pheniramine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .683, 691phenmetrazine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .676phenobarbital . . . . . . . . . . . . . . . . . . . . . . . . . . .678, 679, 692phenol . . . . . . . . . . . . . .43, 87, 553, 560 - 567, 629, 705, 707phenol-d6 . . . . . . . . . . . . . . .43, 87, 497, 559, 561 - 565, 567phenothiazine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .680 - 682phensuximide . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .692phentermine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .676, 677phenyl acetaldehyde . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .611,4-phenylenediamine . . . . . . . . . . . . . . . . . . . . . . . . . . . .566phenylephrine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .676, 6832-phenylethanol . . . . . . . . . . . . . . . . . . . . . . . . . .67, 629, 6312-phenylethyl acetate . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6292-phenylethyl decanoate . . . . . . . . . . . . . . . . . . . . . . . . . .629phenylethylamine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .676phenylpropanolamine . . . . . . . . . . . . . . . . .676, 677, 683, 691phenyltoloxamine . . . . . . . . . . . . . . . . . . . .680, 681, 683, 691phorate . . . . . . . . . . . . . . . . . . . . . . . . . . . .91, 497, 573 - 575phosmet . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .91, 573 - 575

phosphamidon . . . . . . . . . . . . . . . . . . . . . . .91, 573 - 575, 635phosphamidon isomer . . . . . . . . . . . . . . . . . . . .91, 573 - 575phthalide . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .629phytane . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .664picloram methyl ester . . . . . . . . . . . . . . . . . . . . . . . . . . . .5792-picoline . . . . . . . . . . . . . . . . . . . . . . . . . .100, 549, 550, 566α-pinene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .625, 626, 628(-/+)α-pinene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .612β-pinene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .625, 626, 628(+/-)β-pinene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .612piperazine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .704pirimiphos methyl . . . . . . . . . . . . . . . . . . . . . . . .576, 577, 635prazepam . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .680 - 682prilocaine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .672, 691primidone . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .678, 679, 692pristane . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .664procaine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .672, 691prochlorperazine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .682α-prodine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .673profenfos . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .576, 577promazine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .682promethazine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .682prometon . . . . . . . . . . . . . . . . . . . . . .497, 560, 568, 578, 581prometryne . . . . . . . . . . . . . . . . . . . . . . . . . . . . .568, 578, 581pronamide . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .568propachlor . . . . . . . . . . . . . . . . . . . . . . . . .497, 568, 572, 581propadiene . . . . . . . . . . . . . . . . . . . . .76, 129, 650, 652 - 654propane . . . . . . . . . . . . . . . .76, 129, 131, 606, 649 - 654, 664n-propane . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6621-propanol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .607n-propanol . . . . . . . . . . . . . . . . . . . .58, 82, 85, 630, 642, 667propargyl alcohol . . . . . . . . . . . . . . . . . . . . . . . .100, 549, 550propazine . . . . . . . . . . . . . . . . . . . . . . . . . .497, 568, 578, 5814-propenyl-2,6-dimethoxyphenol . . . . . . . . . . . . . . . . . . . .629propionic acid . . . . . . . . . . . . . . . . . . . . . . . .67, 615, 629, 631propionitrile . . . . . . . . . . . . . . . . . . . . . . . .103, 547, 548, 551propiovanillone . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .629propyl acetate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .103, 547n-propyl acetate . . . . . . . . . . . . . . . . . . . . . . . . .100, 549, 550n-propylamine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .704propylbenzene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .633n-propylbenzene . . . . . . . . . . . . . . .100, 101, 103, 547 - 551,

606, 607, 655, 661, 662propylene . . . . . . . . . . . . . . . . . . .76, 129, 131, 409, 606, 609,

649, 650, 652 - 654, 664propylene glycol . . . . . . . . . . . . . . . . . . . . . . . . .601, 602, 6681,2-propylene glycol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6021,3-propylene glycol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .602n-propyl toluenesulfonate . . . . . . . . . . . . . . . . . . . . .689, 690propyzamide . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .566, 568Prowl . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .581pseudoephedrine . . . . . . . . . . . . . . . . . . . . . . . .676, 677, 691pyrazophos . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .576, 577pyrene . . . . . . . . . . . . . . . . .43, 45, 73, 87, 97, 98, 555 - 559,

561 - 568, 636 - 638pyrene-d10 . . . . . . . . . . . . . . . . . . . . . .43, 87, 561 - 565, 568pyridine . . . . . . . . . . . . . . . . . . . .38, 43, 83, 85, 87, 100, 549,

550, 561 - 567, 695, 698, 700 - 702, 705pyrilamine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .680, 681, 683quinalphos . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .577RDX . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .594rhamnitol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .640ribitol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .640Ro-Neet . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .581ronnel . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .91, 573 - 575(+)-(2R,4S)-cis-rose oxide . . . . . . . . . . . . . . . . . . . . . . . . .612(-)-(2S,4R)-cis-rose oxide . . . . . . . . . . . . . . . . . . . . . . . . . .612(+)-(2S,4S)-trans-rose oxide . . . . . . . . . . . . . . . . . . . . . . .612(-)-(2R,4R)-trans-rose oxide . . . . . . . . . . . . . . . . . . . . . . . .612sabinene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .625, 626, 628trans-sabinenehydrate . . . . . . . . . . . . . . . . . . . . . . . . . . . .626safrole . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .61, 566scopolamine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .680, 681secbumeton . . . . . . . . . . . . . . . . . . . . . . . . . . . .578, 581, 582secobarbital . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .678, 679Sencor . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .581siloxane . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .629simazine . . . . . . . . . . .497, 568, 571, 572, 578, 581, 582, 590simetryne . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .568, 578, 581sinapic acid . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .629



758 www.restek.com

INDEX


β-sitosterol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .623Sonar . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .568squalene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .623stearic acid . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .59, 646stigmasterol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .623stirofos . . . . . . . . . . . . . . . . . . . . . . . . . . . .91, 568, 573 - 575styrene . .100, 101, 103, 409, 547 - 551, 606 - 609, 633, 634sulfotepp . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .91, 573 - 575Sutan . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .581syringealdehyde . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6292,4,5-T . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5802,4,5-T methyl ester . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .579talbutal . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .679TBP . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5771,2,3,4-TCDD . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5911,2,3,7-TCDD . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5911,2,3,8-TCDD . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5911,2,6,7-TCDD . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5911,2,7,8-TCDD . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5911,4,7,8-TCDD . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5912,3,7,8-TCDD . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .96, 591TCDF . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .962,4,5,6-TCMX . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .53tebuthiuron . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .568temazepam . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .680 - 682TEPP . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .91, 573 - 575terbacil . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .568, 581terbufos . . . . . . . . . . . . . . . . . . .91, 497, 560, 568, 573 - 575terbumeton . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .582terbuthylazine . . . . . . . . . . . . . . . . . . . . . . . . . . .578, 581, 582terbutryne . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .568, 578, 581p-terphenyl-d14 . . . . . . . . . . . . . . . . . . . .43, 87, 97, 497, 554,

556, 559, 561 - 567(-/+)terpinen-4-ol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .612α-terpinene . . . . . . . . . . . . . . . . . . . . . . . . . . . .625, 626, 628γ-terpinene . . . . . . . . . . . . . . . . . . . . . . . . . . . . .625, 626, 628terpinene-4-ol . . . . . . . . . . . . . . . . . . . . . . . . . . .625, 626, 628α-terpineol . . . . . . . . . . . . . . . . . . . . . . . . . . . .605, 625 - 628(+/-)α-terpineol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .612terpinolene . . . . . . . . . . . . . . . . . . . . . . . . . . . . .625, 626, 628terrazole . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .568testosterone . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .687, 688testosterone-17β-cypionate . . . . . . . . . . . . . . . . . . . . . . .687testosterone propionate . . . . . . . . . . . . . . . . . . . . . . . . . .687tetrabutyltin . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .592, 593tetracaine . . . . . . . . . . . . . . . . . . . . . . . . . .672, 680, 681, 6911,2,4,5-tetrachlorobenzene . . . . . . . . . . . . . . . . . . . . . . . .5662,2',3,5'-tetrachlorobiphenyl . . . . . . . . . . . . . . . . . . . . . . . .5832,2',5,5'-tetrachlorobiphenyl . . . . . . . . . . . . . . . . . . . . . . . .5832,3',4,4'-tetrachlorobiphenyl . . . . . . . . . . . . . . . . . . . . . . . .583tetrachloroethane . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6721,1,1,2-tetrachloroethane . . . . . . . . . . . . . . . . .100, 101, 103,

411, 547 - 551, 6071,1,2,2-tetrachloroethane . . . . . . . . . . . . . .74, 100, 101, 103,

409, 467, 547 - 551, 606, 608, 609tetrachloroethene . . . . . . . . . . . . . . . . . . .100, 101, 103, 467,

547 - 551, 606 - 608, 672tetrachloroethylene . . . . . . . . . . . . . . . . . .409, 589, 590, 6092,3,4,5-tetrachlorophenol . . . . . . . . . . . . . . . . . . . . . . . . . .5602,3,5,6-tetrachlorophenol . . . . . . . . . . . . . . .43, 87, 561 - 5672,3,4,6-tetrachlorophenol . . . . . . . . . . . . . . .43, 87, 561 - 5672,4,5,6-tetrachloro-m-xylene . . . . . . . . . . . .89, 569, 570, 583tetracontane . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .124, 661tetracosane . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .124, 661tetradecane . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .124, 661n-tetradecane . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .661, 662tetradecanoic acid . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .629tetradecanol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .629n-tetradecyl alcohol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .706n-tetradecyl chloride . . . . . . . . . . . . . . . . . . . . . . . . . . . . .706n-tetradecyl-N,N-dimethylamine . . . . . . . . . . . . . . . . . . . .706tetrahydrofuran . . . . . . . . . .83, 85, 100, 103, 409, 547 - 551,

607 - 609, 633, 634, 694, 697, 701, 7021,2,3,4-tetrahydronaphthalene . . . . . . . . . . . . . . . . . . . . .700tetralin . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .83, 695, 6981,2,3,5-tetramethylbenzene . . . . . . . . . . . . . . . . . . . . .75, 657tetrapropyltin . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .592, 593tetratetracontane . . . . . . . . . . . . . . . . . . . . . . . . . . . .124, 661Tetryl . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .594(+/-)thalidomide . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .687Δ9-THC . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .674

THC-COOH . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .674thionazin . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .91, 573 - 575thiopental . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .679thiophene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .664thioridazine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .680 - 682α-thujene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .625, 628thymol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .641Tillam . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .581α-tocopherol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .611β-tocopherol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .611δ-tocopherol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .611γ-tocopherol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .611DL-α-tocotrienol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .611DL-β-tocotrienol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .611DL-δ-tocotrienol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .611DL-γ-tocotrienol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .611tokuthion (prothiofos) . . . . . . . . . . . . . . . . . . . . .91, 573 - 577Tolban . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .581tolclofos-methyl . . . . . . . . . . . . . . . . . . . . . . . . . . . . .576, 577toluene . . . . . . . . . .75, 83, 85, 100, 101, 103, 128, 409, 467,

547 - 551, 595, 597, 606 - 610, 633, 634, 654 - 657, 661, 662, 670, 672, 694, 697, 700 - 702

toluene-d8 . . . . . . . . . . . . . . . . . . . . .100, 103, 547 - 550, 610p-toluenesulfonic acid n-butyl ester (nBTS) . . . . . . . . . . .689o-toluidine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5662,4,5-TP (Silvex) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5802,4,5-TP (Silvex) methyl ester . . . . . . . . . . . . . . . . . . . . . .579TPP . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .577trazodone . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .680, 681Treflan . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .581triacosan . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .629triadimefon . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .568triallate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .497triazolam . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .680 - 682tribromoacetic acid . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6032,4,6-tribromophenol . . . . . . . . . . . . . .43, 87, 497, 559 - 567tributyl phosphate . . . . . . . . . . . . . . . . . . . . . . . .91, 573 - 576tributyltin . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .592, 593tricaprin . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .81, 645trichlorfon . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .91, 573 - 575trichloroacetic acid . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .603trichloroacetonitrile . . . . . . . . . . . . . . . . . . . . . . . . . .589, 5901,2,3-trichlorobenzene . . . . . . . . . . .100, 101, 103, 547 - 5511,2,4-trichlorobenzene . . . . . . . . . . . . .43, 87, 100, 101, 103,

409, 547 - 551, 561 - 567, 606 - 6092,2',5-trichlorobiphenyl . . . . . . . . . . . . . . . . . . . . . . . . . . . .5832,4',5-trichlorobiphenyl . . . . . . . . . . . . . . . . . . . . . . . . . . . .5831,1,1-trichloroethane . . . . . .84, 85, 100, 101, 103, 409, 467,

547 - 551, 589, 590, 606 - 609, 672, 694, 697, 700 - 7021,1,2-trichloroethane . . . . . . . . . . . .100, 101, 103, 409, 467,

547 - 551, 589, 590, 606 - 609, 672trichloroethene . . . . . . . . . . . . . . . . . . . . .100, 101, 103, 467,

547 - 551, 606 - 608, 695trichloroethylene . . . . . . . . . . . . . . . . . .83, 85, 409, 589, 590,

609, 670, 672, 698, 700 - 702trichlorofluoromethane . . . . . . . . . . .100, 101, 103, 234, 409,

467, 547 - 551, 606 - 609trichloronate . . . . . . . . . . . . . . . . . . . . . . . . . . . .91, 573 - 5752,4,5-trichlorophenol . . . . . . . . . . . . . . . . . .43, 87, 561 - 5672,4,6-trichlorophenol . . . . . . . . . . . . . .43, 87, 553, 560 - 5671,2,3-trichloropropane . . . . . . .100, 101, 103, 411, 547 - 551,

589, 590, 603, 6041,1,1-trichloropropanone . . . . . . . . . . . . . . . . . . . . . . . . . .5901,1,1-trichloro-2-propanone . . . . . . . . . . . . . . . . . . . . . . . .5891,1,2-Trichlorotrifluoroethane . . . . . . . . . . . . . . . . . .103, 5471,1,2-trichloro-1,2,2-trifluoroethane . . . . . . . . .409, 606, 609tri-o-cresyl phosphate . . . . . . . . . . . . . . . . . . . . .91, 573 - 575tricyclazole . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .568tridecane . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .39n-tridecane . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .80, 661, 662triethanolamine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .64, 703triethylamine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .46, 63triethylene glycol monomethylether . . . . . . . . . . . . . .64, 703trifluoperazine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .682trifluralin . . . . . . . . . . . . . . . . . . . . . .497, 568, 572, 582, 590triglycerides . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .623triglycerides, butter . . . . . . . . . . . . . . . . . . . . . . . . . . .72, 624trimeprazine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .682trimethylamine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .63, 7041,2,3-trimethylbenzene . . . . . . . . . . . . . . . . . . . . . . . . . . . .610

1,2,4-trimethylbenzene . . . . . .100, 101, 103, 409, 547 - 551, 595, 597, 606 - 609

1,3,5-trimethylbenzene . . . . . . . . . . . . . . .100, 101, 103, 409, 547 - 551, 606 - 610

2,3,5-trimethylnaphthalene . . . . . . . . . . . . . . . . . . . . . . . .6382,2,3-trimethylpentane . . . . . . . . . . . . . . . . . . . . .75, 606, 6572,2,4-trimethylpentane . . . . . . . . . . . . . . . .595, 597, 606, 6082,3,3-trimethylpentane . . . . . . . . . . . . . . . . . . . . . . . . .75, 6572,3,6-trimethylphenol . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7072,4,6-trimethylphenol . . . . . . . . . . . . . . . . . . . . . . . . . . . . .707trimipramine . . . . . . . . . . . . . . . . . . . . . . . . . . . .680, 681, 6911,3,5-trinitrobenzene . . . . . . . . . . . . . . . . . . . . . . . . .566, 594trinitrotoluene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5942,3,4-trinitrotoluene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5932,4,5-trinitrotoluene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5932,4,6-trinitrotoluene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .593tripelennamine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .680, 681tripentyltin . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .592triphenyl phosphate . . . . . . . . . . . . . .91, 560, 568, 573 - 576triphenylene . . . . . . . . . . . . . . . . . . .45, 73, 98, 557, 558, 637triprolidine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .683, 691undecane . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .124, 610, 661n-undecane . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .80, 6551-undecanol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .39unleaded gasoline . . . . . . . . . . . . . . . . . . . . . . .599, 663, 665valencene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .626, 628n-valeramide . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .66, 705valeric acid . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .629n-valeric acid . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .615valproic acid . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .692vanillin . . . . . . . . . . . . . . . . . . . . . . . . .67, 626, 629, 631, 641vanillin methyl ketone . . . . . . . . . . . . . . . . . . . . . . . . . . . .629Vernam . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .581vernolate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .568vinyl acetate . . . . . . . . . . . .100, 103, 409, 547, 549, 550, 609vinyl chloride . . . . . . . . . . . . . . .100, 101, 103, 234, 409, 467,

547 - 551, 606 - 6094-vinylguaiacol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .629viridiflorol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .626volatile organic impurities . . . . . . . . . . . . . . . . . . . . . . . . .699water . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .111, 703whiskey lactone . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .629m-xylene . . . . . . . . . . . . . .83, 100, 101, 103, 409, 547 - 551,

595, 597, 606 - 610, 654,655, 672, 694, 697, 700 - 702

o-xylene . . . . . . . . . . . . . . .83, 100, 101, 103, 409, 547 - 551, 595, 597, 606 - 610, 654,

655, 672, 694, 697, 700 - 702p-xylene . . . . . . . . . . . . . . . . . . . . .75, 83, 100, 101, 103, 409,

547 - 551, 595, 606 - 610, 654, 655, 657, 661, 662, 672, 694, 697, 700 - 702

2,3-xylenol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7073,4-xylenol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7073,5-xylenol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .707xylitol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .640






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INDEX

Compound Index for HPLC Chromatograms

acenaphthene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .717, 718acenaphthylene . . . . . . . . . . . . . . . . . . . . . . . . . . . . .717, 718acephate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722acetaldehyde . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .181, 710acetaminophen . . . . . . . . . . . . . . . . . . . . . . . . .738, 743, 747acetamiprid . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722acetazolamide . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .749acetic acid . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .726acetone . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .181, 710acifluorfen . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .713, 714acrolein . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .181, 710adenine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .744adenosine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .744ADP . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .744AHD (1-aminohydantoin hydrochloride) . . . . . . . . . . . . . .724alanycarb . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722aldicarb . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .719, 722aldicarb sulfone . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .719aldicarb sulfoxide . . . . . . . . . . . . . . . . . . . . . . . . . . .719, 722allicin . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .730alprazolam . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .751ametryne . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722amiloride . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7497-amino clonazepam . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7517-amino flunitrazepam . . . . . . . . . . . . . . . . . . . . . . . . . . .7517-amino nitrazepam . . . . . . . . . . . . . . . . . . . . . . . . . . . . .751aminocarb . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7222-amino-4,6-dinitrotoluene . . . . . . . . . . . . . . . . . . . .485, 7114-amino-2,6-dinitrotoluene . . . . . . . . . . . . . . . . . . . .485, 711amitraz . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722amoxicillin . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .741AMOZ

(3-amino-5-morpholinomethyl-2-oxazolidinone) . . . . . .724d5-AMOZ

(3-amino-5-morpholinomethyl-2-oxazolidinone) . . . . . .724AMP . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .744amphetamine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .750angiotensin I . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .745angiotensin II, III . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .745anthracene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .717, 718AOZ (3-amino-2-oxazolidinone) . . . . . . . . . . . . . . . . . . . .724d4-AOZ (3-amino-2-oxazolidinone) . . . . . . . . . . . . . . . . . .724apomyoglobin . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .746ascorbic acid . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .732, 734ATP . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .744atrazine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .716azoxystrobin . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722BDMC . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .719beclomethasone . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .739benalaxyl . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722bendiocarb . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722bendroflumethiazide . . . . . . . . . . . . . . . . . . . . . . . . . . . . .749benfuracarb . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722bentazon . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .713, 714, 722benzaldehyde . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .181, 710benzo(a)anthracene . . . . . . . . . . . . . . . . . . . . . . . . .717, 718benzo(b)fluoranthene . . . . . . . . . . . . . . . . . . . . . . . .717, 718benzo(j)fluoranthene . . . . . . . . . . . . . . . . . . . . . . . .717, 718benzo(k)fluoranthene . . . . . . . . . . . . . . . . . . . . . . . .717, 718benzo(ghi)perylene . . . . . . . . . . . . . . . . . . . . . . . . . .717, 718benzo(a)pyrene . . . . . . . . . . . . . . . . . . . . . . . . . . . . .717, 718benzoic acid . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .737benzoximate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722BHA . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7272-BHA . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7273-BHA . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .727BHT . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .727boscalid . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722bromazepam . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .751bromoxynil . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722bromuconazole . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722bumetanide . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .749bupirimate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722buprenorphine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .747buprofezin . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722butafenacil . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722butoxycarboxin . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722n-butyl toluenesulfonate . . . . . . . . . . . . . . . . . . . . . . . . . .737butyraldehyde . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .181, 710caffeine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .743caftaric acid . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .730cannabidiol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .748cannabinol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .748capsaicin . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .728carbanilide . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722carbaryl . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .719, 722carbazole . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .712

carbendazim . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722carbetamide . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722carbofuran . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .719carboxin . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722carfentrazone-ethyl . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722β-carotene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .735CDP . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .744cephalexin . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .740cephaloridine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .740cephradine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .740chloramben . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .714chlordiazepoxide . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .751chlorogenic acid . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .730chlorothiazide . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .749chloroxuron . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722chlortetracycline . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .740chlortoluron . . . . . . . . . . . . . . . . . . . . . . . . . . .712, 716, 722chrysene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .717, 718cichoric acid . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .730ciprofloxacin . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .723citric acid . . . . . . . . . . . . . . . . . . . . . . . . . . . . .531, 726, 729clethodim . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722clobazam . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .751clofentezine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722clonazepam . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .751CMP . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .744COC . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .750cocaine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .750codeine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .743, 747, 748codeine phosphate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .738corticosterone . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .741cortisone . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .741cortisone acetate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .741crotonaldehyde . . . . . . . . . . . . . . . . . . . . . . . . . . . . .181, 710cyanazine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .712, 716cyazofamid . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722cyclopenta(c,d)pyrene . . . . . . . . . . . . . . . . . . . . . . . . . . .718cycluron . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722cyproconazole . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722cyprodinil . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722cytidine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .744cytochrome c . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .746cytosine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .744, 7452,4-D . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .713, 7142,4-DB . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .713, 7143,5-DCBA . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .713desalkylflurazepam . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .751deschlorobeclomethasone . . . . . . . . . . . . . . . . . . . . . . . .739desisopropylatrazine . . . . . . . . . . . . . . . . . . . . . . . . . . . . .716desmethyl flunitrazepam . . . . . . . . . . . . . . . . . . . . . . . . .751desoxycorticosterone . . . . . . . . . . . . . . . . . . . . . . . . . . . .741dexamethasone . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .741diazepam . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .747, 751d5-diazepam . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .751dibenzo(a,h)anthracene . . . . . . . . . . . . . . . . . . . . . .717, 718dibenzo(a,e)pyrene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .718dibenzo(a,h)pyrene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .718dibenzo(a,i)pyrene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .718dibenzo(a,l)pyrene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .718dicamba . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .713, 7141,4-dichlorobenzene . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7143,5-dichlorobenzoic acid . . . . . . . . . . . . . . . . . . . . . . . . . .7142,4-dichlorophenylacetic acid . . . . . . . . . . . . . . . . . . . . . .714dichlorprop . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .713, 714diclobutrazol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722diclofenac . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .723dicrotophos . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722diethofencarb . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722difenoconazole . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722diflubenzuron . . . . . . . . . . . . . . . . . . . . . . . . . .712, 716, 722dihydrocapsaicin . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7282,4-dihydroxybenzoic acid . . . . . . . . . . . . . . . . . . . . . . . .7372,5-dihydroxybenzoic acid . . . . . . . . . . . . . . . . . . . . . . . .7373,5-dihydroxybenzoic acid . . . . . . . . . . . . . . . . . . . . . . . .737diltiazem . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .739dimethoate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722dimethomorph . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7221,7-dimethylxanthine . . . . . . . . . . . . . . . . . . . . . . . . . . . .745dimoxystrobin . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7223,5-dinitroaniline . . . . . . . . . . . . . . . . . . . . . . . . . . . .485, 7111,3-dinitrobenzene . . . . . . . . . . . . . . . . . . . . . . . . . .485, 7112,4-dinitrotoluene . . . . . . . . . . . . . . . . . . . . . . . . . . .485, 7112,6-dinitrotoluene . . . . . . . . . . . . . . . . . . . . . . . . . . .485, 711dinoseb . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .713, 714dioxacarb . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722diquat . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .189, 715diuron . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .712, 716, 722

dopamine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .745d3-doxepine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .751doxycycline . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .740ecgonine methyl ester . . . . . . . . . . . . . . . . . . . . . . . . . . .750echinacoside . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .730EME . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .750enrofloxacin . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .723epi-lactose . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .743epinephrine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .745epoxiconazole . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722estazolam . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .75117α-estradiol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .74217β-estradiol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .742β-estradiol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .742estriol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .742estrone . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .742ethacrynic acid . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .749ethiofencarb . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722ethofumesate . . . . . . . . . . . . . . . . . . . . . . . . . .712, 716, 722ethyl glucuronide . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .749ethyl sulfate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .749ethylbenzene sulfonate . . . . . . . . . . . . . . . . . . . . . . . . . . .737ethyluracil . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .745ethyl vanillin . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .728ethynyl estradiol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .742etoxazole . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722famotidine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .736fenbuconazole . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722fenoxycarb . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722fenpropimorph . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722fenpyroximate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722fentanyl . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .747fenuron . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722fipronil . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722fludioxinil . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722flufenacet . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722flunitrazepam . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .751fluometuron . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .712, 722fluoranthene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .717, 718fluorene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .717, 718fluoxastrobin . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722flurazepam . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .751flusiazole . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722flusilazole . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .712, 716flutriafol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722forchlorfenuron . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722formaldehyde . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .181, 710formetanate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722fructose . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .727, 743fumaric acid . . . . . . . . . . . . . . . . . . . . . . . . . . .531, 726, 729furalaxyl . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722furosemide . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .739, 749galactose . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .743glucose . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .727glyburide . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .741guaifenesin . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .743guanine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .744guanosine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .744hexanaldehyde . . . . . . . . . . . . . . . . . . . . . . . . . . . . .181, 710HMX . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .485, 711holo-transferrin . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .746hydrochlorothiazide . . . . . . . . . . . . . . . . . . . . . . . . . . . . .749hydrocodone . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .747, 748hydrocodone bitartrate . . . . . . . . . . . . . . . . . . . . . .738, 743hydrocortisone . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .741hydromorphone . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .748α-hydroxyalprazolam . . . . . . . . . . . . . . . . . . . . . . . . . . . .7513-hydroxybenzoic acid . . . . . . . . . . . . . . . . . . . . . . . . . . .7374-hydroxybenzoic acid . . . . . . . . . . . . . . . . . . . . . . . . . . .7373-hydroxycarbofuran . . . . . . . . . . . . . . . . . . . . . . . . . . . .7192-hydroxyethylflurazepam . . . . . . . . . . . . . . . . . . . . . . . . .751β-hydroxyethyltheophylline . . . . . . . . . . . . . . . . . . . . . . . .743α-hydroxytriazolam . . . . . . . . . . . . . . . . . . . . . . . . . . . . .751hypoxanthine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .745indapamine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .749indeno(1,2,3-cd)pyrene . . . . . . . . . . . . . . . . . . . . . . .717, 718Ioxynil . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722isopropyl toluenesulfonate . . . . . . . . . . . . . . . . . . . . . . . .737isoproturon . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .712, 716ketoprofen . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .723lactic acid . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .726lactose . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .727, 743lactulose . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .743leucine enkephalin . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .745levodopa . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .745levofloxacin . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .723linuron . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .712, 716

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Compound Index for HPLC Chromatograms

lomefloxacin . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .723lorazepam . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .747, 751lormetazepam . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .751malic acid . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .531, 729malonic acid . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .726maltose . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .727MCPA . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .713, 714MCPP . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .714MDA . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .750MDEA . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .750MDMA . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .750medazepam . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .751MEK . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .710melatonin . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .729menadione . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .732methabenzthiazuron . . . . . . . . . . . . . . . . . . . . .712, 716, 722methacrolein . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .181, 710methadone . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .747methamidophos . . . . . . . . . . . . . . . . . . . . . . . . . . . .720, 722methamphetamine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .750meth enkephalin . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .745methiocarb . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .719, 722methomyl . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .719, 722methoprotryne . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722methoxyfenozide . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7225-methylchrysene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7185-methylcytosine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .745methyl ethyl ketone . . . . . . . . . . . . . . . . . . . . . . . . .181, 7101-methylnaphthalene . . . . . . . . . . . . . . . . . . . . . . . .717, 7182-methylnaphthalene . . . . . . . . . . . . . . . . . . . . . . . .717, 7186-methylpurine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .745metobromuron . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722mexacarbate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722midazolam . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7516-monoacetylmorphine . . . . . . . . . . . . . . . . . . . . . . . . . . .748monocrotophos . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722monuron . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .712morphine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .747, 748morphine sulfate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .738myclobutanil . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722N,N'-bis-(chlorobenzyl)urea . . . . . . . . . . . . . . . . . . . . . . .716naphthalene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .717, 718neburon . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .712, 716, 722nicardipine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .739nicotinamide . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .733nifedipine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .739nitrazepam . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .751nitrobenzene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .485, 711nitroglycerine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .485, 7114-nitrophenol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .713, 7142-nitrotoluene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .485, 7113-nitrotoluene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .485, 7114-nitrotoluene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .485, 711nordiazepam . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .751nordihydrocapsaicin . . . . . . . . . . . . . . . . . . . . . . . . . . . . .728norepinephrine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .745norethindrone . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .742norfloxacin . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .723norgestrel . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .742noviflumuron . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722omethoate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722oxadixyl . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722oxamyl . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .719, 722oxazepam . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .751oxycodone . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .747, 748oxycodone HCl . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .738oxymorphone . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .748oxytetracycline . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .740oxytocin . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .746paclobutrazol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722paraquat . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .189, 715penconazole . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722pendimethalin . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .712penicillin V . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .740pentachlorophenol . . . . . . . . . . . . . . . . . . . . . . . . . .713, 714PETN . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .485, 711phenanthrene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .717, 718phenethyl glucosinolate . . . . . . . . . . . . . . . . . . . . . . . . . .730phenol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .738phenylalanine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .745phylloquinone . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .732picloram . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .714picoxystrobin . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722pinoxaden . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722piperine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .728piperonyl butoxide . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722pirimicarb . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722

piroxicam . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .723prazepam . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .751prednisone . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .741prochloraz . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722progesterone . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .742promecarb . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722prometon . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722prometryne . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722propamocarb . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722propanil . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .712propargite . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722propiconazole . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722propionaldehyde . . . . . . . . . . . . . . . . . . . . . . . . . . . .181, 710propoxur . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .719, 722propyl gallate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .727n-propyl toluenesulfonate . . . . . . . . . . . . . . . . . . . . . . . . .737propyluracil . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .745prothioconazole . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722purine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .745pyracarbolid . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722pyraclostrobin . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722pyrene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .717, 718pyridaben . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722pyridoxine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .733pyriproxyfen . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722pyruvic acid . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .726quinic acid . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .531, 729RDX . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .485, 711retinol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .735all-trans-retinol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .732riboflavin . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .733ribonuclease A . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .746rotenone . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722salicylic acid . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .737SC (semicarbazide) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .724secbumeton . . . . . . . . . . . . . . . . . . . . . . . . . . .712, 716, 722siduron . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .712, 722Silvex . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .714simazine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .716simetryne . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722sparfloxacin . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .723spinosyn A . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722spiroxamine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722succinic acid . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .726sucrose . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .727Sudan I . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722Sudan II . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722Sudan III . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722Sudan IV . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722sulfachlorpyridazine . . . . . . . . . . . . . . . . . . . . . . . . . . . . .725sulfadiazine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .725sulfadimethoxine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .725sulfamerazine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .725sulfamethazine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .725sulfamethoxazole . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .725sulfamethoxine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .725sulfamethoxypyridazine . . . . . . . . . . . . . . . . . . . . . . . . . .725sulfaquinoxaline . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .725sulfathiazole . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .725sulindac . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7232,4,5-T . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .713, 714tartaric acid . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .531, 729TBHQ . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .727TDP . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .744tebuconazole . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722tebufenozide . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722tebuthiuron . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .712, 722temazepam . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .751terbumeton . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .716, 722terbuthylazine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .716terbuthylazine desethyl . . . . . . . . . . . . . . . . . . . . . . . . . . .716terbutryne . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722testosterone . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .742tetraconazole . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722tetracycline . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .740Tetryl . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .485, 711Δ9-THC . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .748THC-COOH . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .748THC-COOH-gluc . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .748theobromine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .743, 745theophylline . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .743, 745thiabendazole . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722thiacloprid . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722thiamethoxam . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722thiamin . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .732thiamine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .733thidiazuron . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .712

thiobencarb . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722thiophanate methyl . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722thymidine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .744thymine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .744, 745TMP . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .744α-tocopherol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .730, 732α-tocopherol acetate . . . . . . . . . . . . . . . . . . . . . . . . . . . .732β-tocopherol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .730δ-tocopherol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .730γ-tocopherol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .730m-tolualdehyde . . . . . . . . . . . . . . . . . . . . . . . . . . . . .181, 7102,4,5-TP (Silvex) . . . . . . . . . . . . . . . . . . . . . . . . . . . .713, 714triadimefon . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722triamcinolone . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .741triamterene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .749triazolam . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .751tricyclazole . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722trifloxystrobin . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722triflumizole . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722triflumuron . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7221,3,5-trinitrobenzene . . . . . . . . . . . . . . . . . . . . . . . .485, 7112,4,6-trinitrotoluene . . . . . . . . . . . . . . . . . . . . . . . . .485, 711triticonazole . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722tryptophan . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .745TTP . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .744tyrosine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .745UDP . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .744UMP . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .744uniconazole . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722uracil . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .741, 744, 745uric acid . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .745uridine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .744UTP . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .744val-4-angiotensin III . . . . . . . . . . . . . . . . . . . . . . . . . . . . .745val-tyr . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .745val-tyr-val . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .745valeraldehyde . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .181, 710vamidothion . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722vanillin . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .727, 728verapamil . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .739vitamin B1 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .733vitamin B12 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .734vitamin B2 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .733, 734vitamin B3 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .733, 734vitamin B5 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .734vitamin B6 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .733, 734vitamin B7 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .734vitamin B9 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .734vitamin C . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .734vitamin D2 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .731, 733vitamin D3 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .731 - 733vitamin E acetate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .733vitamin K1 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .733vitamin K2 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .733xanthine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .745zaleplon . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .751zolpiclone . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .751zolpidem . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .751zoxamide . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .722

For HPLC Chromatograms cont'd Chromatogram Search Tool: www.restek.com/chromatograms





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INDEX

Catalog #10000 . . . . . . . . . . . . . . .3410000-600 . . . . . . . . . . .3410001 . . . . . . . . . . . . . . .3410001-600 . . . . . . . . . . .3410002 . . . . . . . . . . . . . . .3410002-600 . . . . . . . . . . .3410003 . . . . . . . . . . . . . . .3310003-600 . . . . . . . . . . .3310005 . . . . . . . . . . . . . . .3310005-600 . . . . . . . . . . .3310012 . . . . . . . . . . . . . . .3310013 . . . . . . . . . . . . . . .3310014 . . . . . . . . . . . . . . .3310015 . . . . . . . . . . . . . . .3310022 . . . . . . . . . . . . . . .3310023 . . . . . . . . . . . . . . .3310024 . . . . . . . . . . . . . . .3310025 . . . . . . . . . . . . . . .3310026 . . . . . . . . . .33,88,9010027 . . . . . . . . . .33,88,9010029 . . . . . . . . . . . .33,4010029-600 . . . . . . . . .33,4010032 . . . . . . . . . . . . . . .3310033 . . . . . . . . . . . . . . .3310034 . . . . . . . . . . . . . . .3310035 . . . . . . . . . . . . . . .3310036 . . . . . . . . . . . . . . .3310037 . . . . . . . . . . . . . . .3310039 . . . . . . . . . . . .33,4010039-600 . . . . . . . . .33,4010040 . . . . . . . . . . . . . . .3310040-600 . . . . . . . . . . .3310041 . . . . . . . . . . . . . . .3310042 . . . . . . . . . . . . . . .3310043 . . . . . . . . . . . . . . .3310043-600 . . . . . . . . . . .3310044 . . . . . . . . . . . . . . .3310044-600 . . . . . . . . . . .3310045 . . . . . . . . . . . .33,8810045-600 . . . . . . . . . . .3310046 . . . . . . . . . . . . . . .3310047 . . . . . . . . . . . . . . .3310048 . . . . . . . . . . . . . . .3310048-600 . . . . . . . . . . .3310049 . . . . . . . . . . . . . . .3310049-600 . . . . . . . . . . .3310054 . . . . . . . . . . . .33,4010054-600 . . . . . . . . .33,4010059 . . . . . . . . . . . .33,4010059-600 . . . . . . . . .33,4010064 . . . . . . . . . . . .33,4010064-600 . . . . . . . . .33,4010065 . . . . . . . . . . . . . . .3310066 . . . . . . . . . . . . . . .3310067 . . . . . . . . . . . . . . .3310068 . . . . . . . . . . . . . . .3310069 . . . . . . . . . . . . . . .3310070 . . . . . . . . . . . . . . .3310073 . . . . . . . . . . . .33,4010073-600 . . . . . . . . .33,4010075 . . . . . . . . . . . . . . .3410076 . . . . . . . . . . . . . . .3410077 . . . . . . . . . . . . . . .3410078 . . . . . . . . . . . . . . .3410079 . . . . . . . . . . . . . . .3410079-600 . . . . . . . . . . .3410080 . . . . . . . . . . . . . . .3410080-600 . . . . . . . . . . .3410081 . . . . . . . . . . . . . . .3410081-600 . . . . . . . . . . .3410082 . . . . . . . . . . . . . . .3410083 . . . . . . . . . . . . . . .3410084 . . . . . . . . . . . . . . .3410085 . . . . . . . . . . . . . . .3410086 . . . . . . . . . . . . . . .3410087 . . . . . . . . . . . . . . .3410088 . . . . . . . . . . . . . . .3410089 . . . . . . . . . . . . . . .3410090 . . . . . . . . . . . . . . .3410097 . . . . . . . . . . . . . . .3310098 . . . . . . . . . . . . . . .3310099 . . . . . . . . . . . . . . .33

10100 . . . . . . . . . . . . . . .3310101 . . . . . . . . . . . . . . .3310102 . . . . . . . . . . . . . . .3310105 . . . . . . . . . . . . . . .4910106 . . . . . . . . . . . . . . .4910107 . . . . . . . . . . . . . . .4910108 . . . . . . . . . . . . . . .4910109 . . . . . . . . . . . . . . .4910110 . . . . . . . . . . . . . . .4910111 . . . . . . . . . . . . . . .4910112 . . . . . . . . . . . . . . .4910120 . . . . . . . . . . . . . . .4910121 . . . . . . . . . . . . . . .4910122 . . . . . . . . . . . . . . .4910123 . . . . . . . . . . . . . . .4910123-124 . . . . . . . . .35,4910124 . . . . . . . . . . . . . . .4910125 . . . . . . . . . . . . . . .4910126 . . . . . . . . . . . . . . .4910127 . . . . . . . . . . . . . . .4910128 . . . . . . . . . . . . . . .4910129 . . . . . . . . . . . . . . .4910130 . . . . . . . . . . . . . . .4910135 . . . . . . . . . . . . . . .4910136 . . . . . . . . . . . . . . .4910137 . . . . . . . . . . . . . . .4910138 . . . . . . . . . . . . . . .4910139 . . . . . . . . . . . . . . .4910140 . . . . . . . . . . . . . . .4910141 . . . . . . . . . . . . . . .4910142 . . . . . . . . . . . . . . .4910143 . . . . . . . . . . . . . . .4910144 . . . . . . . . . . . . . . .4910147 . . . . . . . . . . . . . . .7510148 . . . . . . . . . . . . . . .7510149 . . . . . . . . . . . . . . .7510150 . . . . . . . . . . . . . . .4910151 . . . . . . . . . . . . . . .4910152 . . . . . . . . . . . . . . .4910153 . . . . . . . . . . . . . . .4910154 . . . . . . . . . . . . . . .4910155 . . . . . . . . . . . . . . .4910155-126 . . . . . . . . .35,4910156 . . . . . . . . . . . . . . .4910157 . . . . . . . . . . . . . . .4910158 . . . . . . . . . . . . . . .4910159 . . . . . . . . . . . . . . .4910160 . . . . . . . . . . . . . . .4910165 . . . . . . . . . . . . . . .7510166 . . . . . . . . . . . . . . .4910167 . . . . . . . . . . . . . . .4910169 . . . . . . . . . . . . . . .4910170 . . . . . . . . . . . . . . .4910172 . . . . . . . . . . . . . . .4910173 . . . . . . . . . . . . . . .4910175 . . . . . . . . . . . . . . .4910176 . . . . . . . . . . . . . . .4910177 . . . . . . . . . . . . . . .4910178 . . . . . . . . . . . . . . .4910179 . . . . . . . . . . . . . . .4910179-126 . . . . . . . . .35,4910180 . . . . . . . . . . . . . . .4910181 . . . . . . . . . . . . . . .4910182 . . . . . . . . . . . . . . .4910183 . . . . . . . . . . . . . . .4910184 . . . . . . . . . . . . . . .4910185 . . . . . . . . . . . . . . .4910187 . . . . . . . . . . . . . . .4910188 . . . . . . . . . . . . . . .4910189 . . . . . . . . . . . . . . .4910190 . . . . . . . . . . . . . . .4910191 . . . . . . . . . . . . . . .4910192 . . . . . . . . . . . . . . .4910193 . . . . . . . . . . . . . . .4910194 . . . . . . . . . . . . . . .4910198 . . . . . . . . . . . . . . .4910199 . . . . . . . . . . . . . . .7710205 . . . . . . . . . . . . . . .5010206 . . . . . . . . . . . . . . .5010207 . . . . . . . . . . . . . . .5010208 . . . . . . . . . . . . . . .5010209 . . . . . . . . . . . . . . .50

10210 . . . . . . . . . . . . . . .5010211 . . . . . . . . . . . . . . .5010212 . . . . . . . . . . . . . . .5010213 . . . . . . . . . . . . . . .5010214 . . . . . . . . . . . . . . .5010215 . . . . . . . . . . . . . . .5010220 . . . . . . . . . . . . . . .5010221 . . . . . . . . . . . . . . .5010222 . . . . . . . . . . . . . . .5010223 . . . . . . . . . . . . . . .5010223-124 . . . . . . . . . . .3510223-127 . . . . . . . . . . .3510223-600 . . . . . . . . . . .5010224 . . . . . . . . . . . . . . .5010224-125 . . . . . . . . . . .3510225 . . . . . . . . . . . . . . .5010226 . . . . . . . . . . . . . . .5010227 . . . . . . . . . . . . . . .5010227-125 . . . . . . . . . . .3510228 . . . . . . . . . . . . . . .5010229 . . . . . . . . . . . . . . .5010230 . . . . . . . . . . . . . . .5010235 . . . . . . . . . . . . . . .5010236 . . . . . . . . . . . . . . .5010237 . . . . . . . . . . . . . . .5010238 . . . . . . . . . . . . . . .5010238-600 . . . . . . . . . . .5010239 . . . . . . . . . . . . . . .5010240 . . . . . . . . . . . . . . .5010241 . . . . . . . . . . . . . . .5010242 . . . . . . . . . . . . . . .5010243 . . . . . . . . . . . . . . .5010244 . . . . . . . . . . . . . . .5010245 . . . . . . . . . . . . . . .5010250 . . . . . . . . . . . . . . .5010251 . . . . . . . . . . . . . . .5010252 . . . . . . . . . . . . . . .5010253 . . . . . . . . . . . . . . .5010253-124 . . . . . . . . . . .3510254 . . . . . . . . . . . . . . .5010254-125 . . . . . . . . . . .3510254-600 . . . . . . . . . . .5010255 . . . . . . . . . . . . . . .5010256 . . . . . . . . . . . . . . .5010257 . . . . . . . . . . . . . . .5010258 . . . . . . . . . . . . . . .5010259 . . . . . . . . . . . . . . .5010260 . . . . . . . . . . . . . . .5010266 . . . . . . . . . . . . . . .5010267 . . . . . . . . . . . . . . .5010269 . . . . . . . . . . . . . . .5010270 . . . . . . . . . . . . . . .5010270-600 . . . . . . . . . . .5010272 . . . . . . . . . . . . . . .5010273 . . . . . . . . . . . . . . .5010275 . . . . . . . . . . . . . . .5010277 . . . . . . . . . . . . . . .5010279 . . . . . . . . . . . . . . .5010279-126 . . . . . . . . .35,8610281 . . . . . . . . . . . . . . .5010282 . . . . . . . . . . . . . . .5010283 . . . . . . . . . . . . . . .5010284 . . . . . . . . . . . . . . .5010285 . . . . . . . . . . . . . . .5010287 . . . . . . . . . . . . . . .5010288 . . . . . . . . . . . . . . .5010290 . . . . . . . . . . . . . . .5010291 . . . . . . . . . . . . . . .8110292 . . . . . . . . . . . . . . .8110293 . . . . . . . . . . . . . . .8110294 . . . . . . . . . . . . . . .8110295 . . . . . . . . . . . . . . .9210296 . . . . . . . . . . . . . . .9210320 . . . . . . . . . . . . . . .5110321 . . . . . . . . . . . . . . .5110322 . . . . . . . . . . . . . . .5110323 . . . . . . . . . . . . . . .5110324 . . . . . . . . . . . . . . .5110325 . . . . . . . . . . . . . . .5110335 . . . . . . . . . . . . . . .5110336 . . . . . . . . . . . . . . .5110338 . . . . . . . . . . . . . . .51

10339 . . . . . . . . . . . . . . .5110350 . . . . . . . . . . . . . . .5110351 . . . . . . . . . . . . . . .5110352 . . . . . . . . . . . . . . .5110353 . . . . . . . . . . . . . . .5110354 . . . . . . . . . . . . . . .5110355 . . . . . . . . . . . . . . .5110420 . . . . . . . . . . . . . . .5110421 . . . . . . . . . . . . . . .5110422 . . . . . . . . . . . . . . .5110423 . . . . . . . . . . . . . . .5110424 . . . . . . . . . . . . . . .5110425 . . . . . . . . . . . . . . .5110435 . . . . . . . . . . . . . . .5110436 . . . . . . . . . . . . . . .5110437 . . . . . . . . . . . . . . .5110438 . . . . . . . . . . . . . . .5110439 . . . . . . . . . . . . . . .5110440 . . . . . . . . . . . . . . .5110450 . . . . . . . . . . . . . . .5110451 . . . . . . . . . . . . . . .5110452 . . . . . . . . . . . . . . .5110453 . . . . . . . . . . . . . . .5110454 . . . . . . . . . . . . . . .5110455 . . . . . . . . . . . . . . .5110467 . . . . . . . . . . . . . . .5110470 . . . . . . . . . . . . . . .5110482 . . . . . . . . . . . . . . .5110485 . . . . . . . . . . . . . . .5110520 . . . . . . . . . . . . . . .5210521 . . . . . . . . . . . . . . .5210522 . . . . . . . . . . . . . . .5210523 . . . . . . . . . . . . . . .5210524 . . . . . . . . . . . . . . .5210535 . . . . . . . . . . . . . . .5210536 . . . . . . . . . . . . . . .5210537 . . . . . . . . . . . . . . .5210538 . . . . . . . . . . . . . . .5210539 . . . . . . . . . . . . . . .5210540 . . . . . . . . . . . . . . .5210550 . . . . . . . . . . . . . . .5210551 . . . . . . . . . . . . . . .5210552 . . . . . . . . . . . . . . .5210553 . . . . . . . . . . . . . . .5210554 . . . . . . . . . . . . . . .5210555 . . . . . . . . . . . . . . .5210567 . . . . . . . . . . . . . . .5210569 . . . . . . . . . . . . . . .5210570 . . . . . . . . . . . . . . .5210605 . . . . . . . . . . . . . . .5910608 . . . . . . . . . . . . . . .5910611 . . . . . . . . . . . . . . .5910620 . . . . . . . . . . . . . . .5910621 . . . . . . . . . . . . . . .5910622 . . . . . . . . . . . . . . .5910623 . . . . . . . . . . . . . . .5910623-124 . . . . . . . . . . .3510624 . . . . . . . . . . . .59,8410625 . . . . . . . . . . . .59,8410626 . . . . . . . . . . . . . . .5910627 . . . . . . . . . . . . . . .5910628 . . . . . . . . . . . . . . .5910635 . . . . . . . . . . . . . . .5910636 . . . . . . . . . . . . . . .5910637 . . . . . . . . . . . . . . .5910638 . . . . . . . . . . . . . . .5910639 . . . . . . . . . . . . . . .5910640 . . . . . . . . . . . . . . .5910641 . . . . . . . . . . . . . . .5910642 . . . . . . . . . . . . . . .5910643 . . . . . . . . . . . . . . .5910651 . . . . . . . . . . . . . . .5910652 . . . . . . . . . . . . . . .5910654 . . . . . . . . . . . . . . .5910654-125 . . . . . . . . . . .3510655 . . . . . . . . . . . . . . .5910655-126 . . . . . . . . . . .3510657 . . . . . . . . . . . . . . .5910658 . . . . . . . . . . . . . . .5910666 . . . . . . . . . . . . . . .5910667 . . . . . . . . . . . . . . .5910669 . . . . . . . . . . . . . . .59

10670 . . . . . . . . . . . . . . .5910672 . . . . . . . . . . . . . . .5910708 . . . . . . . . . . . . . . .5710710 . . . . . . . . . . . . . . .5710711 . . . . . . . . . . . . . . .5710713 . . . . . . . . . . . . . . .5710714 . . . . . . . . . . . . . . .5710723 . . . . . . . . . . . . . . .5710724 . . . . . . . . . . . . . . .5710725 . . . . . . . . . . . . . . .5710726 . . . . . . . . . . . . . . .5710727 . . . . . . . . . . . . . . .5710728 . . . . . . . . . . . . . . .5710729 . . . . . . . . . . . . . . .5710730 . . . . . . . . . . . . . . .5710758 . . . . . . . . . . . . . . .9610759 . . . . . . . . . . . . . . .9610820 . . . . . . . . . . . . . . .6610821 . . . . . . . . . . . . . . .6610823 . . . . . . . . . . . . . . .6610824 . . . . . . . . . . . . . . .6610838 . . . . . . . . . . . . . . .6610839 . . . . . . . . . . . . . . .6610840 . . . . . . . . . . . . . . .6610851 . . . . . . . . . . . . . . .6610852 . . . . . . . . . . . . . . .6610854 . . . . . . . . . . . . . . .6610855 . . . . . . . . . . . . . . .6610857 . . . . . . . . . . . . . . .6610858 . . . . . . . . . . . . . . .6610869 . . . . . . . . . . . . . . .6610900 . . . . . . . . . . . . . .10210901 . . . . . . . . . . . . . .10210902 . . . . . . . . . . . . . .10210903 . . . . . . . . . . . . . .10210904 . . . . . . . . . . . . . .10210905 . . . . . . . . . . . . . .10210906 . . . . . . . . . . . . . .10210908 . . . . . . . . . . . . . .10210909 . . . . . . . . . . . . . .10210910 . . . . . . . . . . . . . .10210915 . . . . . . . . . . . . . .10210916 . . . . . . . . . . . . . .10210919 . . . . . . . . . . . . . .10210920 . . . . . . . . . . . . . .10210921 . . . . . . . . . . . . . .10210968 . . . . . . . . . . . . . . .5510968-124 . . . . . . . . . . .3510969 . . . . . . . . . . . . . . .5510970 . . . . . . . . . . . . . . .5510970-125 . . . . . . . . . . .3510971 . . . . . . . . . . . . . . .5510971-126 . . . . . . . . . . .3510972 . . . . . . . . . . . . . . .5510973 . . . . . . . . . . . . . . .5510974 . . . . . . . . . . . . . . .5510975 . . . . . . . . . . . . . . .5510982 . . . . . . . . . . . . . . .5510986 . . . . . . . . . . . . . .10210998 . . . . . . . . . . . . . . .8010999 . . . . . . . . . . . . . . .8011005 . . . . . . . . . . . . . . .6711006 . . . . . . . . . . . . . . .6711007 . . . . . . . . . . . . . . .6711008 . . . . . . . . . . . . . . .6711009 . . . . . . . . . . . . . . .6711010 . . . . . . . . . . . . . . .6711011 . . . . . . . . . . . . . . .6711012 . . . . . . . . . . . . . . .6711013 . . . . . . . . . . . . . . .6711020 . . . . . . . . . . . . . . .6711021 . . . . . . . . . . . . . . .6711022 . . . . . . . . . . . . . . .6711023 . . . . . . . . . . . . . . .6711024 . . . . . . . . . . . . . . .6711025 . . . . . . . . . . . . . . .6711026 . . . . . . . . . . . . . . .6711027 . . . . . . . . . . . . . . .6711028 . . . . . . . . . . . . . . .6711035 . . . . . . . . . . . . . . .6711036 . . . . . . . . . . . . . . .6711037 . . . . . . . . . . . . . . .67

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13423 . . . . . . . . . . . . . . .4113424 . . . . . . . . . . . . . . .4113425 . . . . . . . . . . . . . . .4113426 . . . . . . . . . . . . . . .4113427 . . . . . . . . . . . . . . .4113435 . . . . . . . . . . . . . . .4113436 . . . . . . . . . . . . . . .4113437 . . . . . . . . . . . . . . .4113438 . . . . . . . . . . . . . . .4113439 . . . . . . . . . . . . . . .4113440 . . . . . . . . . . . . . . .4113441 . . . . . . . . . . . . . . .4113442 . . . . . . . . . . . . . . .4113450 . . . . . . . . . . . . . . .4113451 . . . . . . . . . . . . . . .4113452 . . . . . . . . . . . . . . .4113453 . . . . . . . . . . . . . . .4113454 . . . . . . . . . . . . . . .4113455 . . . . . . . . . . . . . . .4113456 . . . . . . . . . . . . . . .4113457 . . . . . . . . . . . . . . .4113467 . . . . . . . . . . . . . . .4113470 . . . . . . . . . . . . . . .4113481 . . . . . . . . . . . . . . .4113497 . . . . . . . . . . . . . . .4113498 . . . . . . . . . . . . . . .4113499 . . . . . . . . . . . . . . .4113501 . . . . . . . . . . . .44,6013502 . . . . . . . . . . . . . . .4413520 . . . . . . . . . . . . . . .4413521 . . . . . . . . . . . . . . .4413522 . . . . . . . . . . . . . . .4413523 . . . . . . . . . . . . . . .4413524 . . . . . . . . . . . . . . .4413525 . . . . . . . . . . . . . . .4413535 . . . . . . . . . . . . . . .4413536 . . . . . . . . . . . . . . .4413537 . . . . . . . . . . . . . . .4413538 . . . . . . . . . . . . . . .4413539 . . . . . . . . . . . . . . .4413540 . . . . . . . . . . . . . . .4413550 . . . . . . . . . . . . . . .4413551 . . . . . . . . . . . . . . .4413552 . . . . . . . . . . . . . . .4413553 . . . . . . . . . . . . . . .4413554 . . . . . . . . . . . . . . .4413555 . . . . . . . . . . . . . . .4413567 . . . . . . . . . . . . . . .4413569 . . . . . . . . . . . . . . .4413570 . . . . . . . . . . . . . . .4413605 . . . . . . . . . .42,87,9713608 . . . . . . . . . .42,87,9713620 . . . . . . . . . .42,87,9713620-127 . . . . . . . . .35,4213621 . . . . . . . . . . . .42,8713623 . . . . . . .42,87,95,9713623-124 . . . . . . . . .35,4213623-127 . . . . . . . . .35,4213624 . . . . . . . . . . . .42,8713626 . . . . . . . . . .42,87,9713635 . . . . . . . . . .42,87,9713635-124 . . . . . . . . .35,4213638 . . . . . . . . . .42,87,9713638-124 . . . . . . . . .35,4213638-127 . . . . . . . . .35,4213639 . . . . . . . . . . . .42,8713639-125 . . . . . . . . .35,4213650 . . . . . . . . . . . .42,8713653 . . . . . . . . . . . .42,8713654 . . . . . . . . . . . .42,8713654-125 . . . . . . . . .35,4213670 . . . . . . . . . . . .42,8713697 . . . . . . . . . . . .42,8713705 . . . . . . . . . . . .44,9413708 . . . . . . . . . . . .44,9413709 . . . . . . . . . . . .44,9413720 . . . . . . . . . . . .44,9413721 . . . . . . . . . . . .44,9413723 . . . . . . . . . . . .44,9413724 . . . . . . . . . . . .44,9413726 . . . . . . . . . . . .44,9413727 . . . . . . . . . . . .44,94

13738 . . . . . . . . . . . .44,9413739 . . . . . . . . . . . .44,9413740 . . . . . . . . . . . .44,9413750 . . . . . . . . . . . .44,9413753 . . . . . . . . . . . .44,9413754 . . . . . . . . . . . .44,9413767 . . . . . . . . . . . .44,9413770 . . . . . . . . . . . .44,9413820 . . . . . . . . . . . . . . .4413821 . . . . . . . . . . . . . . .4413823 . . . . . . . . . . . . . . .4413824 . . . . . . . . . . . . . . .4413835 . . . . . . . . . . . . . . .4413836 . . . . . . . . . . . . . . .4413837 . . . . . . . . . . . . . . .4413838 . . . . . . . . . . . . . . .4413839 . . . . . . . . . . . . . . .4413840 . . . . . . . . . . . . . . .4413850 . . . . . . . . . . . . . . .4413851 . . . . . . . . . . . . . . .4413852 . . . . . . . . . . . . . . .4413853 . . . . . . . . . . . . . . .4413854 . . . . . . . . . . . . . . .4413855 . . . . . . . . . . . . . .44 813865 . . . . . . . . .46,83,10313868 . . . . . . . . .46,83,10313870 . . . . . . . . .46,83,10313871 . . . . . . . . .46,83,10313872 . . . . . . . . .46,83,10313905 . . . . . . . . . . . . . . .4713906 . . . . . . . . . . . . . . .4713908 . . . . . . . . . . . . . . .4713909 . . . . . . . . . . . . . . .4713910 . . . . . . . . . . . . . . .4713923 . . . . . . . . . . . . . . .4713924 . . . . . . . . . . . . . . .4713950 . . . . . . . . . . . . . . .4713951 . . . . . . . . . . . . . . .4713952 . . . . . . . . . . . . . . .4713953 . . . . . . . . . . . . . . .4713954 . . . . . . . . . . . . . . .4713955 . . . . . . . . . . . . . . .4713956 . . . . . . . . . . . . . . .4714005 . . . . . . . . . . . . . . .5614006 . . . . . . . . . . . . . . .5614007 . . . . . . . . . . . . . . .5614008 . . . . . . . . . . . . . . .5614009 . . . . . . . . . . . . . . .5614010 . . . . . . . . . . . . . . .5614020 . . . . . . . . . . . . . . .5614021 . . . . . . . . . . . . . . .5614022 . . . . . . . . . . . . . . .5614023 . . . . . . . . . . . . . . .5614024 . . . . . . . . . . . . . . .5614025 . . . . . . . . . . . . . . .5614026 . . . . . . . . . . . . . . .5614027 . . . . . . . . . . . . . . .5614035 . . . . . . . . . . . . . . .5614036 . . . . . . . . . . . . . . .5614037 . . . . . . . . . . . . . . .5614038 . . . . . . . . . . . . . . .5614039 . . . . . . . . . . . . . . .5614040 . . . . . . . . . . . . . . .5614041 . . . . . . . . . . . . . . .5614042 . . . . . . . . . . . . . . .5614043 . . . . . . . . . . . . . . .5614051 . . . . . . . . . . . . . . .5614052 . . . . . . . . . . . . . . .5614054 . . . . . . . . . . . . . . .5614055 . . . . . . . . . . . . . . .5614057 . . . . . . . . . . . . . . .5614058 . . . . . . . . . . . . . . .5614102 . . . . . . . . . .45,73,9814111 . . . . . . . . . .45,73,9814120 . . . . . . . . . .45,73,9814121 . . . . . . . . . .45,73,9814123 . . . . . . . . . .45,73,9814124 . . . . . . . . . .45,73,9814126 . . . . . . . . . .45,73,9815020 . . . . . . . . . . . . . . .5415021 . . . . . . . . . . . . . . .5415022 . . . . . . . . . . . . . . .54

15023 . . . . . . . . . . . . . . .5415024 . . . . . . . . . . . . . . .5415025 . . . . . . . . . . . . . . .5415026 . . . . . . . . . . . . . . .5415027 . . . . . . . . . . . . . . .5415028 . . . . . . . . . . . . . . .5415029 . . . . . . . . . . . . . . .5415030 . . . . . . . . . . . . . . .5415035 . . . . . . . . . . . . . . .5415036 . . . . . . . . . . . . . . .5415037 . . . . . . . . . . . . . . .5415038 . . . . . . . . . . . . . . .5415039 . . . . . . . . . . . . . . .5415040 . . . . . . . . . . . . . . .5415041 . . . . . . . . . . . . . . .5415042 . . . . . . . . . . . . . . .5415043 . . . . . . . . . . . . . . .5415044 . . . . . . . . . . . . . . .5415045 . . . . . . . . . . . . . . .5415050 . . . . . . . . . . . . . . .5415051 . . . . . . . . . . . . . . .5415052 . . . . . . . . . . . . . . .5415053 . . . . . . . . . . . . . . .5415054 . . . . . . . . . . . . . . .5415055 . . . . . . . . . . . . . . .5415056 . . . . . . . . . . . . . . .5415057 . . . . . . . . . . . . . . .5415058 . . . . . . . . . . . . . . .5415059 . . . . . . . . . . . . . . .5415060 . . . . . . . . . . . . . . .5415066 . . . . . . . . . . . . . . .5415067 . . . . . . . . . . . . . . .5415069 . . . . . . . . . . . . . . .5415070 . . . . . . . . . . . . . . .5415072 . . . . . . . . . . . . . . .5415073 . . . . . . . . . . . . . . .5415075 . . . . . . . . . . . . . . .5415082 . . . . . . . . . . . . . . .5415085 . . . . . . . . . . . . . . .5415088 . . . . . . . . . . . . . . .5415091 . . . . . . . . . . . . . . .5415101 . . . . . . . . . . . . . . .6115102 . . . . . . . . . . . . . . .6115103 . . . . . . . . . . . . . . .6115104 . . . . . . . . . . . . . . .6115105 . . . . . . . . . . . . . . .6115608 . . . . . . . . . . . . . . .5415609 . . . . . . . . . . . . . . .5415623 . . . . . . . . . . . . . . .5415624 . . . . . . . . . . . . . . .5415638 . . . . . . . . . . . . . . .5415639 . . . . . . . . . . . . . . .5415653 . . . . . . . . . . . . . . .5415654 . . . . . . . . . . . . . . .5416016 . . . . . . . . . . . . . . .5516020 . . . . . . . . . . . . . . .5516021 . . . . . . . . . . . . . . .5516022 . . . . . . . . . . . . . . .5516023 . . . . . . . . . . . . . . .5516024 . . . . . . . . . . . . . . .5516025 . . . . . . . . . . . . . . .5516026 . . . . . . . . . . . . . . .5516027 . . . . . . . . . . . . . . .5516028 . . . . . . . . . . . . . . .5516035 . . . . . . . . . . . . . . .5516036 . . . . . . . . . . . . . . .5516037 . . . . . . . . . . . . . . .5516038 . . . . . . . . . . . . . . .5516039 . . . . . . . . . . . . . . .5516040 . . . . . . . . . . . . . . .5516041 . . . . . . . . . . . . . . .5516042 . . . . . . . . . . . . . . .5516043 . . . . . . . . . . . . . . .5516050 . . . . . . . . . . . . . . .5516051 . . . . . . . . . . . . . . .5516052 . . . . . . . . . . . . . . .5516053 . . . . . . . . . . . . . . .5516054 . . . . . . . . . . . . . . .5516055 . . . . . . . . . . . . . . .5516056 . . . . . . . . . . . . . . .5516057 . . . . . . . . . . . . . . .5516058 . . . . . . . . . . . . . . .55

16066 . . . . . . . . . . . . . . .5516067 . . . . . . . . . . . . . . .5516069 . . . . . . . . . . . . . . .5516070 . . . . . . . . . . . . . . .5516072 . . . . . . . . . . . . . . .5516073 . . . . . . . . . . . . . . .5516076 . . . . . . . . . . . . . . .5516082 . . . . . . . . . . . . . . .5516085 . . . . . . . . . . . . . . .5516085-126 . . . . . . . . .35,8616088 . . . . . . . . . . . . . . .5516091 . . . . . . . . . . . . . . .5516092 . . . . . . . . . . . . . . .5516093 . . . . . . . . . . . . . . .5517005 . . . . . . . . . . . . . . .7217006 . . . . . . . . . . . . . . .7217007 . . . . . . . . . . . . . . .7217008 . . . . . . . . . . . . . . .7217009 . . . . . . . . . . . . . . .7217010 . . . . . . . . . . . . . . .7217023 . . . . . . . . . . . . . . .5217024 . . . . . . . . . . . . . . .5217025 . . . . . . . . . . . . . . .5217038 . . . . . . . . . . . . . . .5217039 . . . . . . . . . . . . . . .5217040 . . . . . . . . . . . . . . .5217053 . . . . . . . . . . . . . . .5217054 . . . . . . . . . . . . . . .5217055 . . . . . . . . . . . . . . .5218000 . . . . . . . . . . . . . . .8218001 . . . . . . . . . . . . . . .8218002 . . . . . . . . . . . . . . .8218003 . . . . . . . . . . . . . . .8218010 . . . . . . . . . . . . . . .7118023 . . . . . . . . . . . . . . .7118024 . . . . . . . . . . . . . . .7118038 . . . . . . . . . . . . . . .7118039 . . . . . . . . . . . . . . .7118053 . . . . . . . . . . . . . . .7118054 . . . . . . . . . . . . . . .7118074 . . . . . . . . . . . . . . .9918075 . . . . . . . . . . . . . . .9918076 . . . . . . . . . . . . . . .6318077 . . . . . . . . . . . . . . .6318078 . . . . . . . . . . . . . . .6318079 . . . . . . . . . . . . . . .9919000 . . . . . . . . . . . . . .13219001 . . . . . . . . . . . . . .13219002 . . . . . . . . . . . . . .13219003 . . . . . . . . . . . . . .13219004 . . . . . . . . . . . . . .13219005 . . . . . . . . . . . . . .13219006 . . . . . . . . . . . . . .13219007 . . . . . . . . . . . . . .13219008 . . . . . . . . . . . . . .13219009 . . . . . . . . . . . . . .13219010 . . . . . . . . . . . . . .13219011 . . . . . . . . . . . . . .13219012 . . . . . . . . . . . . . .13219013 . . . . . . . . . . . . . .13219014 . . . . . . . . . . . . . .13219015 . . . . . . . . . . . . . .13219016 . . . . . . . . . . . . . .13219017 . . . . . . . . . . . . . .13219018 . . . . . . . . . . . . . .13219019 . . . . . . . . . . . . . .13219020 . . . . . . . . . . . . . .13219021 . . . . . . . . . . . . . .13219022 . . . . . . . . . . . . . .13219023 . . . . . . . . . . . . . .13219040 . . . . . . . . . . . . . .13219041 . . . . . . . . . . . . . .13219042 . . . . . . . . . . . . . .13219043 . . . . . . . . . . . . . .13219044 . . . . . . . . . . . . . .13219308 . . . . . . . . . . . . . .10119309 . . . . . . . . . . . . . .10119315 . . . . . . . . . . . . . .10119316 . . . . . . . . . . . . . .10119319 . . . . . . . . . . . . . .10119320 . . . . . . . . . . . . . .10119374 . . . . . . . . . . . . . .101

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INDEX

Catalog #


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INDEX

Catalog #19385 . . . . . . . . . . . . . .10119388 . . . . . . . . . . . . . .10119389 . . . . . . . . . . . . . .10119720 . . . . . . . . . . . . . .10919721 . . . . . . . . . . . . . .10919722 . . . . . . . . . . . . . .10919723 . . . . . . . . . . . . . .10919736 . . . . . . . . . . . . . . .6019737 . . . . . . . . . . . . . .11019738 . . . . . . . . . . . . . .11019739 . . . . . . . . . . . . . .11019740 . . . . . . . . . . . . . .11019741 . . . . . . . . . . . . . .11019742 . . . . . . . . . . . . . .11019743 . . . . . . . . . . . . . .11019744 . . . . . . . . . . . . . .11019745 . . . . . . . . . . . . . .11019746 . . . . . . . . . . . . . .11019747 . . . . . . . . . . . . . .11019748 . . . . . . . . . . . . . .11019749 . . . . . . . . . . . . . .11019750 . . . . . . . . . . . . . .11019751 . . . . . . . . . . . . . .11019752 . . . . . . . . . . . . . .11019753 . . . . . . . . . . . . . .11119754 . . . . . . . . . . . . . .11119755 . . . . . . . . . . .76,10819756 . . . . . . . . . . .76,10819757 . . . . . . . . . . .76,10819758 . . . . . . . . . . .76,10819759 . . . . . . . . . . .76,10819760 . . . . . . . . . . .76,10819761 . . . . . . . . . . .76,10819762 . . . . . . . . . . .76,10819763 . . . . . . . . . . .74,10819764 . . . . . . . . . . . . . .11019765 . . . . . . . . . . . . . .11019767 . . . . . . . . . . . . . .11019768 . . . . . . . . . . . . . .11019769 . . . . . . . . . . . . . .11019770 . . . . . . . . . . . . . .11019771 . . . . . . . . . . . . . .11019772 . . . . . . . . . . . . . .11019773 . . . . . . . . . . . . . .10919775 . . . . . . . . . . . .76,10819776 . . . . . . . . . . . .76,10819804 . . . . . . . . . . . . . .13119805 . . . . . . . . . . . . . .13119806 . . . . . . . . . . . . . .13119807 . . . . . . . . . . . . . .13119808 . . . . . . . . . . . . . .13019809 . . . . . . . . . . . . . .13019810 . . . . . . . . . . . . . .13019908 . . . . . . . . . . . . . .10019909 . . . . . . . . . . . . . .10019915 . . . . . . . . . . . . . .10019916 . . . . . . . . . . . . . .10019919 . . . . . . . . . . . . . .10019920 . . . . . . . . . . . . . .10019974 . . . . . . . . . . . . . .10019985 . . . . . . . . . . . . . .10019988 . . . . . . . . . . . . . .10020101 . . . . . . . . . . . . . .28120106 . . . . . . . . . . . . . .28220108 . . . . . . . . . . . . . .28120109 . . . . . . . . . . . . . .28120110 . . . . . . . . . .234,258,

264,280,33620112 . . . . . . . . . . . . . .28120113 . . . . . . . . . . . . . .28220114 . . . . . . . . . .215,27920116 . . . . . . . . . . . . . .27720117 . . . . . . .220,244,28220120 . . . . . . . . . . . . . .24120121 . . . . . . . . . . . . . .27120122 . . . . . . . . . . . . . .28220124 . . . . . . . . . . . . . .28220133 . . . . . . . . . . . . . .38220134 . . . . . . . . . . . . . .32520135 . . . . . . . . . . . . . .27520136 . . . . . . . . . . . . . .27520137 . . . . . . . . . . . . . .292

20140 . . . . . . . . . . . . . .29220141 . . . . . . . . . . . . . .29220142 . . . . . . . . . . . . . .29320143 . . . . . . . . . . . . . .29320144 . . . . . . . . . . . . . .29320145 . . . . . . . . . . . . . .29320146 . . . . . . . . . . . . . .29120147 . . . . . . . . . .293,33520148 . . . . . . .293,335,33620149 . . . . . . . . . .293,33520150 . . . . . . . . . .293,33520151 . . . . . . . . . . . . . .29320152 . . . . . . . . . . . . . .29320153 . . . . . . . . . . . . . .29320154 . . . . . . . . . . . . . .29320155 . . . . . . . . . . . . . .29320156 . . . . . . . . . . . . . .29320157 . . . . . . . . . . . . . .29320158 . . . . . . . . . . . . . .29320159 . . . . . . . . . . . . . .29320162 . . . . . . . . . . . . . .38520163 . . . . . . . . . . . . . .38520164 . . . . . . . . . . . . . .37120165 . . . . . . . . . . . . . .37120166 . . . . . . . . . . . . . .37120167 . . . . . . . . . . . . . .37020168 . . . . . . . . . . . . . .37020169 . . . . . . . . . . . . . .37020170 . . . . . . . . . . . . . .37020171 . . . . . . . . . . . . . .37020172 . . . . . . . . . . . . . .37020174 . . . . . . . . . . . . . .37820175 . . . . . . . . . . . . . .37820177 . . . . . . . . . . . . . .30520178 . . . . . . . . . . . . . .38120179 . . . . . . . . . . . . . .38120181 . . .215,231,244,27920182 . . . . . . . . . . . . . .27720185 . . . . . . . . . . . . . .32420188 . . . . . . . . . .325,33320189 . . . . . . . . . .325,33320190 . . . . . . . . . .325,33320191 . . . . . . . . . .325,33320192 . . . . . . . . . . . . . .32420193 . . . . . . . . . . . . . .32420197 . . . . . . . . . . . . . .27520198 . . . . . . . . . . . . . .27520199 . . . . . . . . . . . . . .27520200 . . . . . . . . . .284,29020201 . . . . . . .269,284,29020202 . . . . . . .269,284,29020203 . . . . . . . . . . . . . .28520204 . . . . . . . . . . . . . .28520205 . . . . . . . . . . . . . .28520206 . . . . . . . . . . . . . .28520207 . . . . . . . . . . . . . .28520208 . . . . . . . . . . . . . .28520209 . . . . . . . . . . . . . .28520210 . . . . . . . . . .269,28520211 . . . . . . . . . . . . . .28420212 . . . . . . . . . . . . . .28420213 . . . . . . . . . . . . . .28420215 . . . . . . . . . . . . . .28520217 . . . . . . . . . . . . . .28520218 . . . . . . . . . . . . . .28520219 . . . . . . . . . . . . . .28520220 . . . . . . . . . . . . . .28520221 . . . . . . . . . . . . . .28520222 . . . . . . . . . . . . . .28520223 . . . . . . . . . . . . . .28520224 . . . . . . .269,284,29020225 . . . . . . . . . . . . . .28520226 . . . . . . . . . . . . . .28520227 . . . . . . . . . .284,29020228 . . . . . . .269,284,29020229 . . . . . . . . . . . . . .28420230 . . . . . . . . . . . . . .28420231 . . . . . . . . . . . . . .28420232 . . . . . . . . . . . . . .28420233 . . . . . . . . . . . . . .28420234 . . . . . . . . . . . . . .26620238 . . . . . . . . . . . . . .284

20239 . . . . . . . . . . . . . .28420240 . . . . . . . . . . . . . .28520243 . . . . . . . . . . . . . .25120244 . . . . . . . . . . . . . .25120246 . . . . . . .233,269,28520248 . . . . . . . . . . . . . .28420249 . . . . . . . . . . . . . .28420250 . . . . . . . . . . . . . .28420251 . . . . . . . . . . . . . .28420252 . . . . . . . . . . . . . .28420253 . . . . . . . . . . . . . .28420254 . . . . . . . . . . . . . .28520255 . . . . . . . . . . . . . .28520257 . . . . . . . . . . . . . .28520258 . . . . . . . . . . . . . .28520262 . . . . . . . . . . . . . .24720263 . . . . . . . . . . . . . .28420264 . . . . . . . . . . . . . .28420265 . . . . . . . . . . . . . .22620266 . . . . . . . . . . . . . .22620267 . . . . . . . . . . . . . .22620268 . . . . . . . . . . . . . .22620270 . . . . . . . . . .227,29120271 . . . . . . . . . .227,29120272 . . . . . . . . . .227,29120273 . . . . . . . . . .227,29120274 . . . . . . . . . .227,29120275 . . . . . . . . . . . . . .28420276 . . . . . . . . . .270,29020277 . . . . . . . . . .270,29020278 . . . . . . . . . .270,29020279 . . . . . . . . . .270,29020280 . . . . . . .256,286,28920281 . . . . . . .256,286,28920282 . . . . . . .256,286,28920283 . . . . . . .256,286,28920284 . . . . . . .256,286,28920285 . . . . . . .256,286,28920286 . . . . . . . . . . . . . .29320287 . . . . . . . . . .293,33620294 . . . . . . . . . . . . . .21420295 . . . . . . . . . . . . . .21420296 . . . . . . . . . .219,26220297 . . . . . . . . . .219,26220298 . . . . . . . . . .219,26220299 . . . . . . . . . .219,26220301 . . . . . . . . . . . . . .26620305 . . . . . . . . . . . . . .26620307 . . . . . . . . . . . . . .26620308 . . . . . . . . . . . . . .26620309 . . . . . . . . . . . . . .26620310 . . . . . . . . . . . . . .26620311 . . . . . . . . . . . . . .26620314 . . . . . . . . . . . . . .26620315 . . . . . . . . . . . . . .26620316 . . . . . . . . . . . . . .26620319 . . . . . . . . . . . . . .26620320 . . . . . . . . . . . . . .26620339 . . . . . . . . . .215,27920342 . . . . . . . . . . . . . .26520343 . . . . . . . . . . . . . .26520344 . . . . . . . . . . . . . .26520345 . . . . . . . . . . . . . .25920346 . . . . . . . . . . . . . .25920347 . . . . . . . . . . . . . .25920348 . . . . . . . . . . . . . .25920366 . . . . . . . . . . . . . .24720375 . . . . . . . . . . . . . .25120377 . . . . . . . . . . . . . .21920387 . . . . . . . . . .248,28020388 . . . . . . . . . . . . . .29120389 . . . . . . . . . . . . . .29220390 . . . . . . . . . . . . . .22320391 . . . . . . . . . . . . . .22320392 . . . . . . .223,233,26920393 . . . . . . .223,233,26920394 . . . . . . . . . . . . . .29220395 . . . . . . . . . . . . . .29220396 . . . . . . . . . . . . . .29220397 . . . . . . . . . . . . . .29220398 . . . . . . . . . . . . . .29220399 . . . . . . . . . . . . . .292

20400 . . . . . . . . . .288,28920401 . . . . . . . . . .288,28920402 . . . . . . . . . .288,28920403 . . . . .88,90,270,28820403-261 . . . . . . .270,28820404 . . . . . . . . . .270,28820404-261 . . . . . . .270,28820405 . . . . . . .270,288,29020405-261 . . .270,288,29020406 . . . . . . .270,288,29020406-261 . . .270,288,29020409 . . . . . . . . . . . . . .22820411 . . . . . . . . . .233,26920412 . . . . . . . . . .233,26920420 . . . . . . . . . . . . . .29120421 . . . . . . . . . . . . . .29120422 . . . . . . . . . . . . . .29120423 . . . . . . . . . . . . . .29120427 . . . . . . . . . .227,29120428 . . . . . . . . . .227,29120429 . . . . . . . . . .288,28920430 . . . . . . . . . .288,28920435 . . . . . . . . . .233,26920436 . . . . . . . . . .233,26920445 . . . . . . . . . .270,28820446 . . . . . . . . . . . . . .28820446-261 . . . . . . . . . .28820447 . . . . . . . . . . . . . .28820447-261 . . . . . . . . . .28820448 . . . . . . . . . . . . . .28820448-261 . . . . . . . . . .28820449 . . . . . . . . . .288,28920469 . . . . . . . . . .270,28820474 . . . . . . . . . . . . . .22320475 . . . . . . . . . . . . . .22320476 . . . . . . . . . . . . . .22320477 . . . . . . . . . . . . . .22320480 . . . . . . . . . .288,28920482 . . . . . . . . . . . . . .28820483 . . . . . . . . . . . . . .28820484 . . . . . . . . . . . . . .28820485 . . . . . . .270,288,29020486 . . . . . . .270,288,29020487 . . . . . . . . . .270,28820504 . . . . . . . . . . . . . .26520508 . . . . . . . . . . . . . .21820509 . . . . . . . . . . . . . .21820522 . . . . . . .114,277,32420523 . . . . . . .114,277,32420535 . . . . . . . . . . . . . .29220536 . . . . . . . . . . . . . .29220537 . . . . . . . . . . . . . .29220543 . . . . . . . . . . . . . .25620544 . . . . . . . . . . . . . .25620568 . . . . . . . . . . . . . .33520584 . . . . . . . . . . . . . .43720585 . . . . . . . . . . . . . .43720586 . . . . . . . . . . . . . .43720587 . . . . . . . . . . . . . .43720588 . . . . . . . . . . . . . .43720589 . . . . . . . . . . . . . .43720600 . . . . . . . . . . . . . .29720601 . . . . . . . . . . . . . .29720610 . . . . . . . . . . . . . .31220611 . . . . . . . . . . . . . .31220612 . . . . . . . . . . . . . .27520613 . . . . . . . . . . . . . .27520618 . . . . . . . . . . . . . .28120623 . . . . . . . . . . . . . .29720624 . . . . . . . . . . . . . .29720625 . . . . . . . . . . . . . .29720626 . . . . . . . . . . . . . .29820631 . . . . . . .220,224,22520634 . . . . . . . . . . . . . .22920635 . . . . . . . . . . . . . .31220636 . . . . . . . . . . . . . .29820637 . . . . . . . . . . . . . .29820638 . . . . . . . . . . . . . .29720643 . . . . . . . . . . . . . .23520645 . . . . . . . . . .233,26920646 . . . . . . . . . . . . . .31020647 . . . . . . . . . . . . . .310

20648 . . . . . . . . . . . . . .31020650 . . . . . . . . . . . . . .24220652 . . . . . . . . . . . . . .24220654 . . . . . . . . . . . . . .24220655 . . . . . . . . . . . . . .24220657 . . . . . . . . . . . . . .24220658 . . . . . . . . . . . . . .24220660 . . . . . . . . . . . . . .24220662 . . . . . . . . . . . . . .31120663 . . . . . . . . . . . . . .31120664 . . . . . . . . . . . . . .31120665 . . . . . . . . . . . . . .31120666 . . . . . . . . . . . . . .31120667 . . . . . . . . . . . . . .31120668350 . . . . . . . . . . .31220668580 . . . . . . . . . . .31220668590 . . . . . . . . . . .31220670 . . . . . . . . . . . . . .24020671 . . . . . . . . . . . . . .24020672 . . . . . . . . . . . . . .24020673 . . . . . . . . . . . . . .24020674 . . . . . . . . . . . . . .27120675 . . . . . . . . . . . . . .27120676 . . . . . . . . . . . . . .27120677 . . . . . . . . . . . . . .30720677-551 . . . . . . . . . .30720680 . . . . . . . . . . . . . .30820680-551 . . . . . . . . . .30820681 . . . . . . . . . . . . . .30820682 . . . . . . . . . . . . . .30820683 . . . . . . . . . . . . . .30820684 . . . . . . . . . . . . . .30820684-550 . . . . . . . . . .30820685 . . . . . . . . . . . . . .29720686 . . . . . . . . . . . . . .29720697 . . . . . . . . . . . . . .30620698 . . . . . . . . . . . . . .29820699 . . . . . . . . . . . . . .29820706 . . . . . . . . . . . . . .21720707 . . . . . . . . . . . . . .21720708 . . . . . . . . . . . . . .21720709 . . . . . . . . . . . . . .21720710 . . . . . . . . . . . . . .21720711 . . . . . . . . . . . . . .26120712 . . . . . . . . . . . . . .21620713 . . . . . . . . . . . . . .21620714 . . . . . . . . . . . . . .21620715 . . . . . . . . . . . . . .25920716 . . . . . . . . . . . . . .25920717 . . . . . . . . . . . . . .25920718 . . . . . . . . . . . . . .25920719 . . . . . . . . . . . . . .25920720 . . . . . . . . . . . . . .25920721 . . . . . . . . . . . . . .25920722 . . . . . . . . . . . . . .25920723 . . . . . . . . . . . . . .25920724 . . . . . . . . . . . . . .25920725 . . . . . . . . . . . . . .25920726 . . . . . . . . . . . . . .21820727 . . . . . . . . . . . . . .25920728 . . . . . . . . . . . . . .25920729 . . . . . . . . . . . . . .21820730 . . . . . . . . . . . . . .24520731 . . . . . . . . . . . . . .24520732 . . . . . . . . . . . . . .24520733 . . . . . . . . . . . . . .24620734 . . . . . . . . . . . . . .24620735 . . . . . . . . . . . . . .24620736 . . . . . . . . . . . . . .24520737 . . . . . . . . . . . . . .24520738 . . . . . . . . . . . . . .24520739 . . . . . . . . . . . . . .24520740 . . . . . . . . . . . . . .24520741 . . . . . . . . . . . . . .24520742 . . . . . . . . . . . . . .24620743 . . . . . . . . . . . . . .24620744 . . . . . . . . . . . . . .24620745 . . . . . . . . . . . . . .24520746 . . . . . . . . . . . . . .24520756 . . . . . . . . . . . . . .21820759 . . . . . . . . . . . . . .26020762 . . . . . . . . . . . . . .260

20765 . . . . . . . . . . . . . .26020768 . . . . . . . . . . . . . .26020771 . . . . . . . . . . . . . .21820772 . . . . . . .133,216,23220773 . . . . . . . . . . . . . .21620774 . . . . . . . . . . . . . .21620775 . . . . . . . . . . . . . .26020776 . . . . . . . . . . . . . .26020777 . . . . . . . . . . . . . .26020778 . . . . . . . . . . . . . .26020779 . . . . . . . . . . . . . .26020780 . . . . . . . . . . . . . .26020781 . . . . . . . . . . . . . .21720782 . . . . . . . . . . . . . .21720783 . . . . . . . . . . . . . .21720784 . . . . . . . . . . . . . .21620785 . . . . . . . . . . . . . .21620786 . . . . . . . . . . . . . .21620787 . . . . . . . . . . . . . .26520788 . . . . . . . . . . . . . .26520792 . . . . . . . . . . . . . .25920793 . . . . . . . . . . . . . .25920794 . . . . . . . . . . . . . .25920795 . . . . . . . . . . . . . .21620796 . . . . . . . . . . . . . .21620797 . . . . . . . . . . . . . .21620798 . . . . . . . . . . . . . .21620799 . . . . . . . . . . . . . .21620800 . . . . . . . . . . . . . .21620801 . . . . . . . . . . . . . .21720802 . . . . . . . . . . . . . .21720803 . . . . . . . . . . . . . .25920804 . . . . . . . . . . . . . .25920809 . . . . . . . . . . . . . .25320810 . . . . . . . . . . . . . .25320811 . . . . . . . . . . . . . .25320812 . . . . . . . . . . . . . .25320813 . . . . . . . . . . . . . .25320814 . . . . . . . . . . . . . .25320815 . . . . . . . . . . . . . .25320816 . . . . . . . . . . . . . .25320817 . . . . . . . . . . . . . .25320818 . . . . . . . . . . . . . .25320819 . . . . . . . . . . . . . .24620822 . . . . . . . . . . . . . .24620823 . . . . . . . . . . . . . .21720824 . . . . . . . . . . . . . .21720827 . . . . . . . . . . . . . .24520828 . . . . . . . . . . . . . .24520829 . . . . . . . . . . . . . .24520830 . . . . . . . . . . . . . .24520832 . . . . . . . . . . . . . .24520833 . . . . . . . . . . . . . .24520834 . . . . . . . . . . . . . .24520835 . . . . . . . . . . . . . .24520836 . . . . . . . . . . . . . .24520837 . . . . . . . . . . . . . .24620838 . . . . . . . . . . . . . .24620839 . . . . . . . . . . . . . .24620840 . . . . . . . . . . . . . .24620841 . . . . . . . . . . . . . .25320842 . . . . . . . . . . . . . .25320845 . . . . . . . . . . . . . .25920846 . . . . . . . . . . . . . .25920847 . . . . . . . . . . . . . .25920848 . . . . . . . . . . . . . .25920849 . . . . . . . . . . . . . .25920850 . . . . . . . . . . . . . .26020851 . . . . . . . . . . . . . .26020852 . . . . . . . . . . . . . .26020853 . . . . . . . . . . . . . .24520854 . . . . . . . . . . . . . .24520855 . . . . . . . . . . . . . .24620856 . . . . . . . . . . . . . .24620857 . . . . . . . . . . . . . .24620858 . . . . . . . . . . . . . .24620859 . . . . . . . . . . . . . .26120860 . . . . . . . . . . . . . .24920861 . . . . . . . . . . . . . .24920862 . . . . . . . . . . . . . .24920863 . . . . . . . . . . . . . .24920864 . . . . . . . . . . . . . .249


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INDEX

Catalog #20865 . . . . . . . . . . . . . .24920868 . . . . . . . . . . . . . .24920869 . . . . . . . . . . . . . .24920870 . . . . . . . . . . . . . .24920871 . . . . . . . . . . . . . .24920876 . . . . . . . . . . . . . .24920877 . . . . . . . . . . . . . .24920881 . . . . . . . . . . . . . .26320882 . . . . . . . . . . . . . .26320883 . . . . . . .221,224,22520884 . . . . . . . . . . . . . .24120885 . . . . . . . . . . . . . .25320886 . . . . . . . . . . . . . .25320893 . . . . . . . . . . . . . .24920894 . . . . . . . . . . . . . .24920895 . . . . . . . . . . . . . .21620896 . . . . . . . . . . . . . .21620897 . . . . . . . . . . . . . .25920898 . . . . . . . . . . . . . .25920899 . . . . . . . . . . . . . .24520900 . . . . . . . . . . . . . .24520901 . . . . . . . . . . . . . .26120902 . . . . . . . . . . . . . .26620903 . . . . . . . . . . . . . .26620904 . . . . . . . . . . . . . .25920905 . . . . . . . . . . . . . .25920906 . . . . . . . . . . . . . .25920907 . . . . . . . . . . . . . .21620908 . . . . . . . . . . . . . .21620909 . . . . . . . . . . . . . .26120910 . . . . . . . . . . . . . .24520911 . . . . . . . . . . . . . .24520912 . . . . . . . . . . . . . .21620913 . . . . . . . . . . . . . .21620914 . . . . . . . . . . . . . .21620915 . . . . . . . . . . . . . .21620916 . . . . . . . . . . . . . .25320917 . . . . . . . . . . . . . .25320929 . . . . . . . . . . . . . .24220936 . . . . . . . . . . . . . .25320937 . . . . . . . . . . . . . .25320937-231.5 . . . . . . . . .25320938 . . . . . . . . . . . . . .25320939 . . . . . . . . . . . . . .25320940 . . . . . . . . . . . . . .25320941 . . . . . . . . . . . . . .25320942 . . . . . . . . . . . . . .25320943 . . . . . . . . . . . . . .25320944 . . . . . . . . . . . . . .25320945 . . . . . . . . . . . . . .25320946 . . . . . . . . . . . . . .25320947 . . . . . . . . . . . . . .25320948 . . . . . . . . . . . . . .25320949 . . . . . . . . . . . . . .25320950 . . . . . . . . . . . . . .25320951 . . . . . . . . . . . . . .25320952 . . . . . . . . . . . . . .25320953 . . . . . . . . . . . . . .25320954 . . . . . . . . . . . . . .21820955 . . . . . . . . . . . . . .25020956 . . . . . . . . . . . . . .25020957 . . . . . . . . . . . . . .25020964 . . . . . . . . . . . . . .23220965 . . . . . . . . . . . . . .23220966 . . . . . . . . . . . . . .23220967 . . . . . . . . . . . . . .23220970 . . . . . . . . . . . . . .25920971 . . . . . . . . . . . . . .25920972 . . . . . . . . . . . . . .21720973 . . . . . . . . . . . . . .21720974 . . . . . . . . . . . . . .21820975 . . . . . . . . . . . . . .21820976 . . . . . . . . . . . . . .24920977 . . . . . . . . . . . . . .24920978 . . . . . . . . . . . . . .24920979 . . . . . . . . . . . . . .21720980 . . . . . . . . . . . . . .21620981 . . . . . . . . . . . . . .21620982 . . . . . . . . . . . . . .21620983 . . . . . . . . . . . . . .21620984 . . . . . . . . . . . . . .21620985 . . . . . . . . . . . . . .216

20986 . . . . . . . . . . . . . .21620987 . . . . . . . . . . . . . .21620988 . . . . . . . . . . . . . .21620989 . . . . . . . . . . . . . .21820990 . . . . . . . . . . . . . .21720991 . . . . . . . . . . . . . .21720992 . . . . . . . . . . . . . .26120993 . . . . . . . . . . . . . .26120994 . . . . . . . . . . . . . .21720995 . . . . . . . . . . . . . .21720996 . . . . . . . . . . . . . .21720997 . . . . . . . . . . . . . .21620998 . . . . . . . . . . . . . .21820999 . . . . . . . . . . . . . .21421000 . . . . . . . . . .239,27521001 . . . . . . . . . . . . . .23921002 . . . . . . . . . . . . . .26121003 . . . . . . . . . . . . . .25021004 . . . . . . . . . . . . . .25421005 . . . . . . . . . . . . . .25421006 . . . . . . . . . . . . . .25421007 . . . . . . . . . . . . . .28421008 . . . . . . . . . . . . . .28421009 . . . . . . . . . . . . . .22321010 . . . . . . . . . . . . . .22321011 . . . . . . . . . . . . . .22321012 . . . . . . . . . . . . . .22321015 . . .234,258,264,29321016 . . .234,258,264,29321018 . . . . . . .234,258,26421020 . . . . . . . . . . . . . .24921021 . . . . . . . . . . . . . .24921022 . . . . . . . . . . . . . .21721023 . . . . . . . . . . . . . .21721024 . . . . . . . . . . . . . .26121025 . . . . . . . . . . . . . .26121026 . . . . . . . . . . . . . .24521027 . . . . . . . . . . . . . .24521028 . . . . . . . . . . . . . .25321029 . . . . . . . . . . . . . .25321030 . . . . . . . . . . . . . .25921031 . . . . . . . . . . . . . .25921032 . . . . . . . . . . . . . .21721033 . . . . . . . . . . . . . .21721034 . . . . . . . . . .221,27821035 . . . . . . . . . . . . . .27121036 . . . . . . . . . . . . . .28421037 . . . . . . . . . . . . . .28421038 . . . . . . . . . . . . . .28421040 . . . . . . . . . . . . . .22121041 . . . . . . . . . . . . . .22121043 . . . . . . .234,258,26421044 . . . . . . . . . . . . . .27821045 . . . . . . . . . . . . . .26021046 . . . . . . . . . . . . . .26021050 . . . . . . . . . . . . . .36521051 . . . . . . . . . . . . . .36521052 . . . . . . . . . . . . . .21821053 . . . . . . . . . . . . . .21821054 . . . . . . . . . . . . . .21821055 . . . . . . . . . . . . . .21821058 . . . . . . . . . . . . . .28421059 . . . . . . . . . . . . . .28421060 . . . . . . . . . . . . . .28421061 . . . . . . . . . . . . . .28421065 . . . . . . . . . . . . . .13321066 . . . . . . . . . . . . . .13321067 . . . . . . . . . . . . . .13321073 . . . . . . . . . . . . . .24421074 . . . . . . . . . . . . . .24421075 . . . . . . . . . . . . . .24421077 . . . . . . . . . . . . . .26021079 . . . . . . . . . . . . . .26021080 . . . . . . . . . . . . . .25421081 . . . . . . . . . . . . . .25421082 . . . . . . . . . . . . . .25421083 . . . . . . . . . . . . . .25421105 . . . . . . . . . . . . . .28921106 . . . . . . . . . . . . . .28921107 . . . . . . . . . . . . . .28921108 . . . . . . . . . . . . . .28921109 . . . . . . . . . . . . . .271

21110 . . . . . . . . . . . . . .21721111 . . . . . . . . . . . . . .21721112 . . . . . . . . . . . . . .25921113 . . . . . . . . . . . . . .25921114 . . . . . . . . . . . . . .25421115 . . . . . . . . . . . . . .25421116 . . . . . . . . . . . . . .25421117 . . . . . . . . . . . . . .25421118 . . . . . . . . . . . . . .43421121 . . . . . . . . . .251,28621122 . . . . . . . . . . . . . .28621123 . . . . . . . . . . . . . .28621124 . . . . . . . . . . . . . .28621125 . . . . . . . . . . . . . .28621126 . . . . . . . . . . . . . .28621127 . . . . . . . . . . . . . .28621128 . . . . . . . . . . . . . .28621131 . . . . . . . . . . . . . .23921132 . . . . . . . . . . . . . .23921135 . . . . . . . . . . . . . .23921136 . . . . . . . . . . . . . .23921137 . . . . . . . . . . . . . .23921138 . . . . . . . . . . . . . .23921139 . . . . . . . . . . . . . .23921140 . . . . . . . . . . . . . .35821141 . . . . . . . . . . . . . .35821142 . . . . . . . . . . . . . .35821143 . . . . . . . . . . . . . .35821147 . . . . . . . . . . . . . .35921148 . . . . . . . . . . . . . .36021149 . . . . . . . . . . . . . .35921150 . . . . . . . . . . . . . .27121151 . . . . . . . . . . . . . .27121152 . . . . . . . . . . . . . .35621153 . . . . . . . . . . . . . .35621154 . . . . . . . . . . . . . .35821155 . . . . . . . . . . . . . .35821156 . . . . . . . . . . . . . .21721157 . . . . . . . . . . . . . .21721159 . . . . . . . . . .252,28021160 . . . . . . . . . . . . . .36321161 . . . . . . . . . . . . . .36321162 . . . . . . . . . . . . . .36321163 . . . . . . . . . . . . . .36321164 . . . . . . . . . . . . . .36321165 . . . . . . . . . . . . . .36321166 . . . . . . . . . . . . . .36321167 . . . . . . . . . . . . . .36321172 . . . . . . . . . . . . . .24321174 . . . . . . . . . . . . . .35621175 . . . . . . . . . . . . . .35621176 . . . . . . . . . . . . . .35921177 . . . . . . . . . . . . . .35921178 . . . . . . . . . . . . . .35921179 . . . . . . . . . . . . . .35921192 . . . . . . . . . . . . . .35921193 . . . . . . . . . . . . . .35921194 . . . . . . . . . . . . . .35921195 . . . . . . . . . . . . . .35921196 . . . . . . . . . . . . . .35621197 . . . . . . . . . . . . . .35621198 . . . . . . . . . . . . . .35621199 . . . . . . . . . . . . . .35621202 . . . . . . . . . . . . . .37421205 . . . . . . . . . . . . . .38521206 . . . . . . . . . . . . . .38521207 . . . . . . . . . . . . . .38521208 . . . . . . . . . . . . . .38521209 . . . . . . . . . . . . . .38521210 . . . . . . . . . . . . . .37021211 . . . . . . . . . . . . . .37021212 . . . . . . . . . . . . . .37021213 . . . . . . . . . . . . . .37021214 . . . . . . . . . . . . . .37021215 . . . . . . . . . . . . . .37021218 . . . . . . . . . . . . . .37221220 . . . . . . . . . . . . . .37121221 . . . . . . . . . . . . . .37021223 . . . . . . . . . . . . . .37021224 . . . . . . . . . . . . . .37121228 . . . . . . . . . . . . . .37121229 . . . . . . . . . . . . . .371

21230 . . . . . . . . . . . . . .37021237 . . . . . . . . . . . . . .24321238 . . . . . . . . . . . . . .22221239 . . . . . . . . . . . . . .22221240 . . . . . . . . . .222,22821241 . . . . . . . . . .222,22821242 . . . . . . .222,224,22521243 . . . . . . .222,224,22521244 . . . . . . . . . . . . . .22221245 . . . . . . . . . . . . . .22221246 . . . . . . .222,233,26921247 . . . . . . .222,233,26921248 . . . . . . . . . . . . . .22221249 . . . . . . . . . . . . . .22221250 . . . . . . . . . . . . . .34821251 . . . . . . . . . . . . . .34821252 . . . . . . . . . . . . . .34821253 . . . . . . . . . . . . . .34821254 . . . . . . . . . . . . . .34821255 . . . . . . . . . . . . . .34621256 . . . . . . . . . . . . . .34621257 . . . . . . . . . . . . . .34621258 . . . . . . . . . . . . . .34621259 . . . . . . . . . . . . . .34621260 . . . . . . . . . .347,38421261 . . . . . . . . . .347,38421262 . . . . . . . . . .347,38421263 . . . . . . . . . .347,38421264 . . . . . . . . . .347,38421265 . . . . . . . . . . . . . .34821270 . . . . . . . . . . . . . .34621271 . . . . . . . . . . . . . .34621272 . . . . . . . . . . . . . .24521273 . . . . . . . . . . . . . .24521274 . . . . . . . . . . . . . .24521275 . . . . . . . . . .385,43721276 . . . . . . . . . .385,43721277 . . . . . . . . . .385,43721278 . . . . . . . . . .385,43721279 . . . . . . . . . .385,43721283 . . . . . . . . . . . . . .38521284 . . . . . . . . . . . . . .37221285 . . . . . . . . . . . . . .25021286 . . . . . . . . . . . . . .25021287 . . . . . . . . . . . . . .25021288 . . . . . . . . . . . . . .25021289 . . . . . . . . . . . . . .25021290 . . . . . . . . . . . . . .25021291 . . . . . . . . . . . . . .25021292 . . . . . . . . . . . . . .25021293 . . . . . . . . . . . . . .24621294 . . . . . . . . . . . . . .24621295 . . . . . . . . . . . . . .24621296 . . . . . . . . . . . . . .24621297 . . . . . . . . . . . . . .24621298 . . . . . . . . . . . . . .24621299 . . . . . . . . . . . . . .25521301 . . . . . . . . . . . . . .24121302 . . . . . . . . . . . . . .24121303 . . . . . . . . . . . . . .23221305 . . . . . . . . . . . . . .22321306 . . . . . . . . . . . . . .22321307 . . . . . . . . . . . . . .22321308 . . . . . . . . . . . . . .22321309 . . . . . . . . . . . . . .22021311 . . . . . . . . . . . . . .22121312 . . . . . . . . . . . . . .22121313 . . . . . . . . . . . . . .23521314 . . . . . . . . . . . . . .23521315 . . . . . . . . . . . . . .22321316 . . . . . . . . . . . . . .22321317 . . . . . . . . . . . . . .22321318 . . . . . . . . . . . . . .22321319 . . . . . . . . . . . . . .22321320 . . . . . . . . . . . . . .22321321 . . . . . . . . . . . . . .31221322 . . . . . . . . . . . . . .31221323 . . . . . . . . . . . . . .23421325 . . . . . . . . . . . . . .32321327 . . . . . . . . . . . . . .31221333 . . . . . . . . . . . . . .31221334 . . . . . . . . . . . . . .311

21336 . . . . . . . . . . . . . .31121337 . . . . . . . . . . . . . .31121338 . . . . . . . . . . . . . .31121339 . . . . . . . . . . . . . .31121340 . . . . . . . . . . . . . .31121344 . . . . . . . . . . . . . .31121347 . . . . . . . . . . . . . .31221348 . . . . . . . . . . . . . .31221349 . . . . . . . . . . . . . .31221353 . . . . . . . . . . . . . .22021356 . . . . . . . . . . . . . .33721360-12 . . . . . . . . . . .30921360-2 . . . . . . . . . . . .30921360-7 . . . . . . . . . . . .30921361-11 . . . . . . . . . . .30921361-5 . . . . . . . . . . . .30921361-6 . . . . . . . . . . . .30921384 . . . . . . . . . . . . . .29221385 . . . . . . . . . . . . . .29221386 . . . . . . . . . . . . . .29221387 . . . . . . . . . .270,29221388 . . . . . . . . . .270,29221389 . . . . . . . . . .270,29221392 . . . . . . . . . . . . . .25521393 . . . . . . . . . . . . . .22021394 . . . . . . . . . . . . . .43521394-PI . . . . . . . . . . .43521399 . . . . . . . . . .221,27821400 . . . . . . . . . . . . . .43621401 . . . . . . . . . . . . . .43621402 . . . . . . . . . . . . . .43621409 . . . . . . . . . .223,22721468 . . . . . . . . . . . . . .26021469 . . . . . . . . . . . . . .26021470 . . . . . . . . . . . . . .26021471 . . . . . . . . . . . . . .26021472 . . . . . . . . . . . . . .28521473 . . . . . . . . . . . . . .28521474 . . . . . . . . . . . . . .28521475 . . . . . . . . . . . . . .24721476 . . . . . . . . . . . . . .24721487 . . . . . . . . . . .24,58021500 . . . . . . . . . . . . . .31921501 . . . . . . . . . . . . . .31921502 . . . . . . . . . . . . . .31921503 . . . . . . . . . . . . . .31921504 . . . . . . . . . . . . . .31921505 . . . . . . . . . . . . . .31921506 . . . . . . . . . . . . . .31921507 . . . . . . . . . . . . . .31921508 . . . . . . . . . . . . . .31921509 . . . . . . . . . . . . . .31921510 . . . . . . . . . . . . . .31921511 . . . . . . . . . . . . . .31921512 . . . . . . . . . . . . . .31921513 . . . . . . . . . . . . . .31921514 . . . . . . . . . . . . . .31921515 . . . . . . . . . . . . . .31921516 . . . . . . . . . . . . . .31921517 . . . . . . . . . . . . . .31921540 . . . . . . . . . . . . . .31721541 . . . . . . . . . . . . . .31721542 . . . . . . . . . . . . . .31721543 . . . . . . . . . . . . . .31721544 . . . . . . . . . . . . . .31721545 . . . . . . . . . . . . . .31721546 . . . . . . . . . . . . . .31721547 . . . . . . . . . . . . . .31721548 . . . . . . . . . . . . . .31721549 . . . . . . . . . .317,41721550 . . . . . . . . . . . . . .31721551 . . . . . . . . . . . . . .31721552 . . . . . . . . . . . . . .31721553 . . . . . . . . . . . . . .31721554 . . . . . . . . . . . . . .31721555 . . . . . . . . . . . . . .31721556 . . . . . . . . . . . . . .31721557 . . . . . . . . . . . . . .31721558 . . . . . . . . . . . . . .31721559 . . . . . . . . . . . . . .31721572 . . . . . . . . . . . . . .43321572-R100 . . . . . . . . .433

21581 . . . . . . . . . . . . . .27121582 . . . . . . . . . . . . . .27121583 . . . . . . . . . . . . . .27121584 . . . . . . . . . . . . . .27121586 . . . . . . . . . . . . . .31721587 . . . . . . . . . . . . . .31721588 . . . . . . . . . . . . . .31721589 . . . . . . . . . . . . . .31721590 . . . . . . . . . . . . . .31921592 . . . . . . . . . . . . . .31921593580 . . . . . . . . . . .31221601 . . . . . . . . . . . . . .28221610 . . . . . . . . . .229,30321620 . . . . . . . . . . . . . .24021621 . . . . . . . . . . . . . .24021642 . . . . . . . . . . . . . .21421646 . . . . . . . . . . . . . .30821647 . . . . . . . . . . . . . .30821648 . . . . . . . . . . . . . .30721649 . . . . . . . . . . . . . .30621650 . . . . . . . . . . . . . .13321651 . . . . . . . . . . . . . .13321652 . . . . . . . . . . . . . .30721653 . . . . . . . . . . . . . .30621653-551 . . . . . . . . . .30621653-552 . . . . . . . . . .30621654 . . . . . . . . . . . . . .30621655 . . . . . . . . . . . . . .30621657 . . . . . . . . . . . . . .30321660 . . . . . . . . . . . . . .30321661 . . . . . . . . . . . . . .30321666 . . . . . . . . . . . . . .31021667 . . . . . . . . . . . . . .31021668 . . . . . . . . . . . . . .31021669 . . . . . . . . . . . . . .31021671 . . . . . . . . . . . . . .30521682 . . . . . . . . . . . . . .24021683 . . . . . . . . . . . . . .24021685 . . . . . . . . . . . . . .23221686 . . . . . . . . . . . . . .24021687 . . . . . . . . . . . . . .24021688 . . . . . . . . . . . . . .24021689 . . . . . . . . . . . . . .24021690 . . . . . . . . . . . . . .26321691 . . . . . . . . . . . . . .23221694 . . . . . . . . . . . . . .24021695 . . . . . . . . . . . . . .24021696 . . . . . . . . . . . . . .24021697 . . . . . . . . . . . . . .24021699 . . . . . . . . . . . . . .23921700 . . . . . . . . . . . . . .21821701 . . . . . . . . . . . . . .21821702 . . . . . . . . . . . . . .21821703 . . . . . . . . . . . . . .21821704 . . . . . . . . . . . . . .21721705 . . . . . . . . . . . . . .25021706 . . . . . . . . . . . . . .25021707 . . . . . . . . . . . . . .25021708 . . . . . . . . . . . . . .26121709 . . . . . . . . . . . . . .26121710 . . . . . . . . . . . . . .22321711 . . . . . . . . . . . . . .26121712 . . . . . . . . . . . . . .26121713 . . . . . . . . . . . . . .25021714 . . . . . . . . . . . . . .26121715 . . . . . . . . . . . . . .26121716 . . . . . . . . . . . . . .26121717 . . . . . . . . . . . . . .24521718 . . . . . . . . . . . . . .24521719 . . . . . . . . . . . . . .25021720 . . . . . . . . . . . . . .35921721 . . . . . . . . . . . . . .35921722 . . . . . . . . . . . . . .35921723 . . . . . . . . . . . . . .36021724 . . . . . . . . . . . . . .35621725 . . . . . . . . . . . . . .35621728 . . . . . . . . . . . . . .35721729 . . . . . . . . . . . . . .35721730 . . . . . . . . . . . . . .35721731 . . . . . . . . . . . . . .35721732 . . . . . . . . . . . . . .35721733 . . . . . . . . . . . . . .357


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INDEX

Catalog #21734 . . . . . . . . . . . . . .35721741 . . . . . . . . . . . . . .36221742 . . . . . . . . . . . . . .36221743 . . . . . . . . . . . . . .36221744 . . . . . . . . . . . . . .36221745 . . . . . . . . . . . . . .36221746 . . . . . . . . . . . . . .36221749 . . . . . . . . . . . . . .36221750 . . . . . . . . . . . . . .36221751 . . . . . . . . . . . . . .36221752 . . . . . . . . . . . . . .36221753 . . . . . . . . . . . . . .36121754 . . . . . . . . . . . . . .36121755 . . . . . . . . . . . . . .36121756 . . . . . . . . . . . . . .36121761 . . . . . . . . . . . . . .36321762 . . . . . . . . . . . . . .36321763 . . . . . . . . . . . . . .36321764 . . . . . . . . . . . . . .36321765 . . . . . . . . . . . . . .36321766 . . . . . . . . . . . . . .36321767 . . . . . . . . . . . . . .36321768 . . . . . . . . . . . . . .36321769 . . . . . . . . . . . . . .36221770 . . . . . . . . . . . . . .36221771 . . . . . . . . . . . . . .36221772 . . . . . . . . . . . . . .36221773 . . . . . . . . . . . . . .36221774 . . . . . . . . . . . . . .36221775 . . . . . . . . . . . . . .36021776 . . . . . . .356,361,36221777 . . . . . . .356,361,36221779 . . . . . . . . . .356,36121780 . . . . . . . . . .356,36121782 . . . . . . . . . . . . . .35621787 . . . . . . . . . . . . . .36221788 . . . . . . . . . . . . . .36221795 . . . . . . . . . . . . . .35921796 . . . . . . . . . . . . . .36421797 . . . . . . . . . . . . . .36421798 . . . . . . . . . . . . . .36421799 . . . . . . . . . . . . . .36421800 . . . . . . . . . . . . . .31621801 . . . . . . . . . . . . . .31621802 . . . . . . . . . . . . . .31621803 . . . . . . . . . . . . . .31621804 . . . . . . . . . . . . . .31621805 . . . . . . . . . . . . . .31621806 . . . . . . . . . . . . . .31621807 . . . . . . . . . . . . . .31621808 . . . . . . . . . . . . . .31621809 . . . . . . . . . . . . . .31621810 . . . . . . . . . . . . . .31621811 . . . . . . . . . . . . . .31621815 . . . . . . . . . . . . . .31621816 . . . . . . . . . . . . . .31621817 . . . . . . . . . . . . . .31621818 . . . . . . . . . . . . . .31621819 . . . . . . . . . . . . . .31621820 . . . . . . . . . . . . . .31621823 . . . . . . . . . . . . . .31621824 . . . . . . . . . . . . . .31621825 . . . . . . . . . . . . . .31621826 . . . . . . . . . . . . . .31621827 . . . . . . . . . . . . . .31621828 . . . . . . . . . . . . . .31621829 . . . . . . . . . . . . . .31621830 . . . . . . . . . . . . . .31621831 . . . . . . . . . . . . . .31621832 . . . . . . . . . . . . . .31621833 . . . . . . . . . .300,31621834 . . . . . . . . . . . . . .31621835 . . . . . . . . . . . . . .31621836 . . . . . . . . . . . . . .31621837 . . . . . . . . . . . . . .31621841 . . . . . . . . . . . . . .31621842 . . . . . . . . . . . . . .31621843 . . . . . . . . . . . . . .31621844 . . . . . . . . . . . . . .31621845 . . . . . . . . . . . . . .31621846 . . . . . . . . . . . . . .31621847 . . . . . . . . . . . . . .316

21848 . . . . . . . . . . . . . .31621878 . . . . . . . . . . . . . .22121879 . . . . . . . . . . . . . .22121883 . . . . . . .219,241,27821884 . . . . . . . . . . . . . .22121891 . . . . . . . . . . . . . .26021892 . . . . . . . . . . . . . .26021893 . . . . . . . . . .263,28021894 . . . . . . . . . .235,27821895 . . . . . . . . . . . . . .25121896 . . . . . . . . . . . . . .26021896-200.1 . . . . . . . . .26021897 . . . . . . . . . . . . . .26021897-200.5 . . . . . . . . .26021898 . . . . . . . . . . . . . .25521899 . . . . . . . . . . . . . .25521900 . . . . . . . . . . . . . .31621901 . . . . . . . . . . . . . .31621902 . . . . . . . . . .316,41721903 . . . . . . . . . . . . . .31621904 . . . . . . . . . . . . . .31621905 . . . . . . . . . . . . . .31621906 . . . . . . . . . . . . . .31621907 . . . . . . . . . . . . . .31621908 . . . . . . . . . . . . . .31621909 . . . . . . . . . . . . . .31621910 . . . . . . . . . . . . . .31621911 . . . . . . . . . .316,41721915 . . . . . . . . . . . . . .31621916 . . . . . . . . . . . . . .31621917 . . . . . . . . . . . . . .31621918 . . . . . . . . . . . . . .31621919 . . . . . . . . . . . . . .31621920 . . . . . . . . . . . . . .31621923 . . . . . . . . . . . . . .31621924 . . . . . . . . . . . . . .31621925 . . . . . . . . . . . . . .31621926 . . . . . . . . . . . . . .31621927 . . . . . . . . . . . . . .31621928 . . . . . . . . . . . . . .31621929 . . . . . . . . . . . . . .31621930 . . . . . . . . . . . . . .31621931 . . . . . . . . . . . . . .31621932 . . . . . . . . . . . . . .31621933 . . . . . . . . . .300,31621934 . . . . . . . . . . . . . .31621935 . . . . . . . . . . . . . .31621936 . . . . . . . . . .316,41721937 . . . . . . . . . . . . . .31621941 . . . . . . . . . . . . . .31621942 . . . . . . . . . . . . . .31621943 . . . . . . . . . . . . . .31621944 . . . . . . . . . . . . . .31621945 . . . . . . . . . . . . . .31621946 . . . . . . . . . . . . . .31621947 . . . . . . . . . . . . . .31621948 . . . . . . . . . . . . . .31621957 . . . . . . . . . . . . . .31621958 . . . . . . . . . . . . . .31621959 . . . . . . . . . . . . . .31621960 . . . . . . . . . . . . . .31621961 . . . . . . . . . . . . . .31621962 . . . . . . . . . . . . . .31621982 . . . . . . . . . . . . . .29921983 . . . . . . . . . . . . . .29921984 . . . . . . . . . . . . . .30021991 . . . . . . . . . .296,29821992 . . . . . . . . . . . . . .29821997 . . . . . . . . . .296,29721999 . . . . . . . . . . . . . .29622004 . . . . . . . . . . . . . .30822005 . . . . . . . . . . . . . .30822006 . . . . . . . . . . . . . .30822007 . . . . . . . . . . . . . .30822008 . . . . . . . . . . . . . .30822010 . . . . . . . . . .296,29722011 . . . . . . . . . . . . . .29722012 . . . . . . . . . . . . . .29822013 . . . . . . . . . . . . . .29822014 . . . . . . . . . . . . . .29722015 . . . . . . . . . . . . . .29722016 . . . . . . . . . . . . . .298

22017 . . . . . . . . . . . . . .29822019 . . . . . . . . . . . . . .29922020 . . . . . . . . . . . . . .29922021 . . . . . . . . . . . . . .29922022 . . . . . . . . . . . . . .29922023 . . . . . . . . . . . . . .30022025 . . . . . . . . . . . . . .30022026 . . . . . . . . . . . . . .30022027 . . . . . . . . . . . . . .30022028 . . . . . . . . . . . . . .29922029 . . . . . . . . . . . . . .29922030 . . . . . . . . . . . . . .29922031 . . . . . . . . . . . . . .29922032 . . . . . . . . . . . . . .43322038 . . . . . . . . . . . . . .42322039 . . . . . . . . . . . . . .42322040 . . . . . . . . . . . . . .42322041 . . . . . . . . . . . . . .42322042 . . . . . . . . . . . . . .42322043 . . . . . . . . . . . . . .42322044 . . . . . . . . . . . . . .42322045 . . . . . . . . . . . . . .42322046 . . . . . . . . . . . . . .42322047 . . . . . . . . . . . . . .42322049 . . . . . . . . . . . . . .42322050 . . . . . . . . . . . . . .42322051 . . . . . . . . . . . . . .42322052 . . . . . . . . . . . . . .42322053 . . . . . . . . . . . . . .42322054 . . . . . . . . . . . . . .42322055 . . . . . . . . . . . . . .42322056 . . . . . . . . . . . . . .42322057 . . . . . . . . . . . . . .42322058 . . . . . . . . . . . . . .42322061 . . . . . . . . . .300,35022062 . . . . . . . . . .300,35022064 . . . . . . . . . .229,30322065 . . . . . . .220,230,28022066 . . . . . . . . . . . . . .28222067 . . . . . . . . . . . . . .24422068 . . . . . . . . . .228,23822069 . . . . . . . . . .228,23822071 . . . . . . . . . . . . . .23922072 . . . . . . . . . . . . . .24922073 . . . . . . . . . . . . . .24922074 . . . . . . . . . . . . . .25422075 . . . . . . . . . . . . . .25422076 . . . . . . . . . . . . . .23022077 . . . . . . . . . . . . . .24122078 . . . . . . .224,225,22822079 . . . . . . . . . . . . . .25122080 . . . . . . . . . . . . . .22922081 . . . . . . . . . . . . . .29722082 . . . . . . . . . . . . . .25822083 . . . . . . . . . . . . . .22322084 . . . . . . . . . . . . . .22322085 . . . . . . . . . . . . . .22322086 . . . . . . . . . . . . . .22322089 . . . . . . . . . . . . . .25522090 . . . . . . . . . . . . . .41022091 . . . . . . . . . . . . . .41022092 . . . . . . . . . . . . . .41022093 . . . . . . . . . . . . . .41022094 . . . . . . . . . . . . . .41122095 . . . . . . . . . . . . . .41122096 . . . . . . . . . . . . . .41122097 . . . . . . . . . . . . . .41122098 . . . . . . . . . . . . . .41522099 . . . . . . . . . . . . . .41522100 . . . . . . . . . . . . . .41422101 . . . . . . . . . . . . . .41422102 . . . . . . . . . . . . . .41522103 . . . . . . . . . . . . . .41522104 . . . . . . . . . . . . . .42322105 . . . . . . . . . . . . . .41122106 . . . . . . . . . . . . . .41122107 . . . . . . . . . . . . . .41122108 . . . . . . . . . . . . . .41122111 . . . . . . . . . . . . . .43522111-PI . . . . . . . . . . .43522112 . . . . . . . . . . . . . .43522112-PI . . . . . . . . . . .435

22113 . . . . . . . . . . . . . .43522113-PI . . . . . . . . . . .43522114 . . . . . . . . . . . . . .42622115 . . . . . . . . . . . . . .42622116 . . . . . . . . . . . . . .42622117 . . . . . . . . . . . . . .42622118 . . . . . . . . . . . . . .42322119 . . . . . . . . . . . . . .42322120 . . . . . . . . . . . . . .42322121 . . . . . . . . . . . . . .41322122 . . . . . . . . . . . . . .42022123 . . . . . . . . . . . . . .42022124 . . . . . . . . . . . . . .42022128 . . . . . . . . . .231,27722129 . . . . . . . . . . . . . .30722130 . . . . . . . . . . . . . .30722131 . . . . . . . . . . . . . .30722132 . . . . . . . . . . . . . .30722133 . . . . . . . . . . . . . .30722134 . . . . . . . . . . . . . .30722135 . . . . . . . . . . . . . .30722171 . . . . . . . . . . . . . .24922172 . . . . . . . . . . . . . .24922173 . . . . . . . . . . . . . .24922174 . . . . . . . . . . . . . .24922175 . . . . . . . . . . . . . .22422176 . . . . . . . . . . . . . .22422177 . . . . . . . . . . . . . .22422178 . . . . . . . . . . . . . .22422179 . . . . . . . . . .239,27522180 . . . . . . . . . .239,27522181 . . . . . . . . . .221,27522182 . . . . . . . . . .252,27622183 . . . . . . . . . .257,27622184 . . . . . . . . . .263,27622185 . . . . . . . . . .248,27622186 . . . . . . . . . .231,27622187 . . . . . . . . . . . . . .28222188 . . . . . . . . . . . . . .32222189 . . . . . . . . . . . . . .32222190 . . . . . . . . . . . . . .32222191 . . . . . . . . . . . . . .32222192 . . . . . . . . . . . . . .32222193 . . . . . . . . . . . . . .32222194 . . . . . . . . . . . . . .32222195 . . . . . . . . . . . . . .32222196 . . . . . . . . . . . . . .32222197 . . . . . . . . . . . . . .32222198 . . . . . . . . . . . . . .32222199 . . . . . . . . . . . . . .32222200 . . . . . . . . . . . . . .32222201 . . . . . . . . . . . . . .32222204 . . . . . . . . . . . . . .32222205 . . . . . . . . . . . . . .32222209 . . . . . . . . . . . . . .32222210 . . . . . . . . . . . . . .28522211 . . . . . . . . . . . . . .28522212 . . . . . . . . . . . . . .28522213 . . . . . . . . . . . . . .28422214 . . . . . . . . . . . . . .28422215 . . . . . . . . . . . . . .28422216 . . . . . . . . . . . . . .28422217 . . . . . . . . . . . . . .28422218 . . . . . . . . . . . . . .28422219 . . . . . . . . . . . . . .28522220 . . . . . . . . . . . . . .28922221 . . . . . . .256,286,28922222 . . . . . . .256,286,28922223 . . . . . . . . . .227,29122224 . . . . . . . . . .227,29122225 . . . . . . . . . .227,29122268 . . . . . . . . . . . . . .21822269 . . . . . . . . . . . . . .21822269-214.5 . . . . . . . . .21822270 . . . . . . . . . . . . . .21822271 . . . . . . . . . . . . . .21822272 . . . . . . . . . . . . . .21822273 . . . . . . . . . . . . . .21822274 . . . . . . . . . . . . . .24922275 . . . . . . . . . . . . . .24922276 . . . . . . . . . . . . . .24922277 . . . . . . . . . . . . . .249

22278 . . . . . . . . . . . . . .25022279 . . . . . . . . . . . . . .25022280 . . . . . . . . . . . . . .26122281 . . . . . . . . . . . . . .26122282 . . . . . . . . . . . . . .26622283 . . . . . . . . . . . . . .24922284 . . . . . . . . . . . . . .24922285 . . . . . . . . . . . . . .24922286 . . . . . . . . . . . . . .24922287 . . . . . . . . . . . . . .24922288 . . . . . . . . . . . . . .25322289 . . . . . . . . . . . . . .25322290 . . . . . . . . . . . . . .34922292 . . . . . . . . . . . . . .34922293 . . . . . . . . . . . . . .34922294 . . . . . . . . . . . . . .34922296 . . . . . . . . . . . . . .34922297 . . . . . . . . . . . . . .34922298 . . . . . . . . . . . . . .34922299 . . . . . . . . . . . . . .34922318 . . . . . . . . . . . . . .24722319 . . . . . . . . . . . . . .24722320 . . . . . . . . . . . . . .24722328 . . . . . . . . . . . . . .24022329 . . . . . . . . . . . . . .23822330 . . . . . . . . . .257,27822331 . . . . . . . . . . . . . .25122332 . . . . . . . . . . . . . .24322333 . . . . . . . . . .252,27822334 . . . . . . . . . .252,28022335 . . . . . . . . . .263,27822336 . . . . . . . . . . . . . .21922337 . . . . . . . . . . . . . .24322338 . . . . . . . . . . . . . .36622339 . . . . . . . . . . . . . .36622340 . . . . . . . . . . . . . .36622341 . . . . . . . . . . . . . .36622342 . . . . . . . . . . . . . .36622343 . . . . . . . . . . . . . .24322344 . . . . . . . . . . . . . .30022345 . . . . . . . . . . . . . .30022346 . . . . . . . . . . . . . .30022347 . . . . . . . . . . . . . .22122348 . . . . . . . . . . . . . .22122349 . . . . . . . . . . . . . .22722350 . . . . . . . . . . . . . .22722351 . . . . . . . . . . . . . .22722352 . . . . . . . . . . . . . .22722353 . . . . . . . . . . . . . .24422354 . . . . . . . . . . . . . .24422355 . . . . . . . . . . . . . .24422400 . . . . . . . . . . . . . .21622401 . . . . . . . . . . . . . .21622402 . . . . . . . . . . . . . .21622403 . . . . . . . . . . . . . .21622404 . . . . . . . . . . . . . .21622405 . . . . . . . . . . . . . .21622406 . . . . . . . . . . . . . .21622407 . . . . . . . . . . . . . .21622408 . . . . . . . . . . . . . .21622409 . . . . . . . . . . . . . .21622410 . . . . . . . . . . . . . .21622411 . . . . . . . . . . . . . .25422412 . . . . . . . . . . . . . .25422413 . . . . . . . . . . . . . .25422414 . . . . . . . . . . . . . .25422415 . . . . . . . . . . . . . .24422416 . . . . . . . . . . . . . .24422417 . . . . . . . . . . . . . .24422418 . . . . . . . . . . . . . .24422419 . . . . . . . . . . . . . .24422420 . . . . . . . . . . . . . .24422421 . . . . . . . . . . . . . .26022422 . . . . . . . . . . . . . .26022423 . . . . . . . . . . . . . .26422426 . . . . . . . . . .133,23222427 . . . . . . . . . .133,23222429 . . . . . . . . . .133,23222430 . . . . . . . . . .133,23222433 . . . . . . . . . . . . . .36522434 . . . . . . . . . . . . . .36522435 . . . . . . . . . . . . . .365

22436 . . . . . . . . . . . . . .36522437 . . . . . . . . . . . . . .36522438 . . . . . . . . . . . . . .36522439 . . . . . . . . . . . . . .36522440 . . . . . . . . . . . . . .36522452 . . . . . . . . . . . . . .31022454 . . . . . . . . . . . . . .25822455 . . . . . . . . . .258,28022456 . . . . . . . . . . . . . .30122457 . . . . . . . . . . . . . .30122458 . . . . . . . . . . . . . .30122459 . . . . . . . . . . . . . .30122460 . . . . . . . . . . . . . .30122461 . . . . . . . . . . . . . .30122462 . . . . . . . . . . . . . .30122463 . . . . . . . . . . . . . .30122464 . . . . . . . . . . . . . .30222465 . . . . . . . . . . . . . .30222466 . . . . . . . . . . . . . .30222467 . . . . . . . . . . . . . .30222468 . . . . . . . . . . . . . .30222469 . . . . . . . . . . . . . .30222470 . . . . . . . . . . . . . .30222471 . . . . . . . . . . . . . .30222472 . . . . . . . . . . . . . .30222473 . . . . . . . . . . . . . .30222474 . . . . . . . . . . . . . .30222475 . . . . . . . . . . . . . .30222476 . . . . . . . . . . . . . .30222477 . . . . . . . . . . . . . .30222478 . . . . . . . . . . . . . .30222479 . . . . . . . . . . . . . .30222480 . . . . . . . . . . . . . .30222481 . . . . . . . . . . . . . .30222482 . . . . . . . . . . . . . .32722483 . . . . . . . . . . . . . .32722484 . . . . . . . . . . . . . .34322485 . . . . . . . . . . . . . .32522486 . . . . . . . . . . . . . .32522487 . . . . . . . . . . . . . .32522488 . . . . . . . . . . . . . .32122489 . . . . . . . . . . . . . .32122490 . . . . . . . . . . . . . .32122491 . . . . . . . . . . . . . .32122492 . . . . . . . . . . . . . .32122493 . . . . . . . . . . . . . .32122494 . . . . . . . . . . . . . .32122495 . . . . . . . . . . . . . .32122496 . . . . . . . . . . . . . .32122497 . . . . . . . . . . . . . .32122500 . . . . . . . . . . . . . .32022501 . . . . . . . . . . . . . .32022502 . . . . . . . . . . . . . .32022503 . . . . . . . . . . . . . .32022504 . . . . . . . . . . . . . .32022505 . . . . . . . . . . . . . .32022506 . . . . . . . . . . . . . .32022507 . . . . . . . . . . . . . .32022508 . . . . . . . . . . . . . .32022509 . . . . . . . . . . . . . .32022520 . . . . . . . . . . . . . .31722521 . . . . . . . . . . . . . .31722522 . . . . . . . . . . . . . .31722523 . . . . . . . . . . . . . .31722524 . . . . . . . . . . . . . .31722525 . . . . . . . . . . . . . .31722526 . . . . . . . . . . . . . .31722527 . . . . . . . . . . . . . .31722528 . . . . . . . . . . . . . .31722530 . . . . . . . . . . . . . .31722531 . . . . . . . . . . . . . .31722532 . . . . . . . . . . . . . .31722533 . . . . . . . . . . . . . .31722534 . . . . . . . . . . . . . .31722535 . . . . . . . . . . . . . .31722536 . . . . . . . . . . . . . .32022537 . . . . . . . . . . . . . .32022538 . . . . . . . . . . . . . .32022539 . . . . . . . . . . . . . .32022540 . . . . . . . . . . . . . .31522541 . . . . . . . . . . . . . .31522542 . . . . . . . . . . . . . .315


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Catalog #22543 . . . . . . . . . . . . . .31522544 . . . . . . . . . . . . . .31522545 . . . . . . . . . . . . . .31522546 . . . . . . . . . . . . . .31522547 . . . . . . . . . . . . . .31522548 . . . . . . . . . . . . . .31522549 . . . . . . . . . . . . . .31522550 . . . . . . . . . . . . . .31522551 . . . . . . . . . . . . . .31522552 . . . . . . . . . . . . . .31522553 . . . . . . . . . . . . . .31522554 . . . . . . . . . . . . . .31522555 . . . . . . . . . . . . . .31522556 . . . . . . . . . . . . . .31522557 . . . . . . . . . . . . . .31522558 . . . . . . . . . . . . . .31522559 . . . . . . . . . . . . . .31522560 . . . . . . . . . . . . . .13722561 . . . . . . . . . . . . . .31522562 . . . . . . . . . . . . . .31522563 . . . . . . . . . . . . . .31522564 . . . . . . . . . . . . . .31522565 . . . . . . . . . . . . . .31522566 . . . . . . . . . . . . . .31522567 . . . . . . . . . . . . . .31522568 . . . . . . . . . . . . . .31522569 . . . . . . . . . . . . . .31522570 . . . . . . . . . . . . . .31522571 . . . . . . . . . . . . . .31522573 . . . . . . . . . . . . . .31522574 . . . . . . . . . . . . . .31522575 . . . . . . . . . . . . . .31522576 . . . . . . . . . . . . . .31522577 . . . . . . . . . . . . . .31522578 . . . . . . . . . . . . . .31522579 . . . . . . . . . . . . . .31522580 . . . . . . . . . . . . . .31522581 . . . . . . . . . . . . . .31522582 . . . . . . . . . . . . . .31522583 . . . . . . . . . . . . . .31522584 . . . . . . . . . . . . . .31522585 . . . . . . . . . . . . . .31522586 . . . . . . . . . . . . . .31522587 . . . . . . . . . . . . . .31522588 . . . . . . . . . . . . . .31522589 . . . . . . . . . . . . . .31522590 . . . . . . . . . . . . . .31522591 . . . . . . . . . . . . . .31522592 . . . . . . . . . . . . . .31522593 . . . . . . . . . . . . . .31522594 . . . . . . . . . . . . . .31522595 . . . . . . . . . . . . . .31522596 . . . . . . . . . . . . . .31522597 . . . . . . . . . . . . . .31522598 . . . . . . . . . . . . . .25422599 . . . . . . . . . . . . . .25422600 . . . . . . . . . . . . . .30322601 . . . . . . . . . . . . . .30322602 . . . . . . . . . . . . . .30322603 . . . . . . . . . . . . . .30322604 . . . . . . . . . . . . . .30322605 . . . . . . . . . . . . . .30322606 . . . . . . . . . . . . . .30322607 . . . . . . . . . . . . . .30322608 . . . . . . . . . . . . . .24722609 . . . . . . . . . . . . . .24722610 . . . . . . . . . . . . . .31522611 . . . . . . . . . . . . . .31522612 . . . . . . . . . . . . . .31522613 . . . . . . . . . . . . . .31522614 . . . . . . . . . . . . . .31522615 . . . . . . . . . . . . . .31522616 . . . . . . . . . . . . . .31522617 . . . . . . . . . . . . . .31522618 . . . . . . . . . . . . . .31522620 . . . . . . . . . . . . . .31522621 . . . . . . . . . . . . . .32422622 . . . . . . . . . . . . . .32522623 . . . . . . . . . . . . . .32522624 . . . . . . . . . . . . . .32522627 . . . . . . . . . . . . . .32522656 . . . . . . . . . .203,274

22656-R . . . . . . . . .203,27422657 . . . . . . . . . .203,204,

273,274,29622658 . . . . . . .204,273,29622659 . . . . . . . . . . . . . .23522660 . . . . . . . . . . . . . .23622661 . . . . . . . . . . . . . .23622662 . . . . . . . . . . . . . .23722663 . . . . . . . . . . . . . .23722664 . . . . . . . . . . . . . .22622665 . . . . . . . . . . . . . .22622666 . . . . . . . . . . . . . .22622667 . . . . . . . . . . . . . .22622668 . . . . . . . . . . . . . .22622669 . . . . . . . . . . . . . .22622670 . . . . . . . . . . . . . .22622671 . . . . . . . . . . . . . .22622672 . . . . . . . . . . . . . .22622673 . . . . . . . . . . . . . .22622674 . . . . . . . . . . . . . .22622683 . . . . . . . . . . . . . .26222684 . . . . . . . . . .219,22722685 . . . . . . . . . . . . . .23722686 . . . . . . . . . . . . . .22622687 . . . . . . . . . . . . . .23722688 . . . . . . . . . . . . . .25122689 . . . . . . . . . . . . . .22022690 . . . . . . . . . . . . . .43422691 . . . . . . . . . . . . . .43422692 . . . . . . . . . . . . . .24322694 . . . . . . . . . . . . . .24222695 . . . . . . . . . . . . . .24322697 . . . . . . . . . . . . . .36422698 . . . . . . . . . . . . . .36422701 . . . . . . . . . . . . . .36422702 . . . . . . . . . . . . . .36422703 . . . . . . . . . . . . . .36422704 . . . . . . . . . . . . . .36422705 . . . . . . . . . . . . . .36422706 . . . . . . . . . . . . . .36422707 . . . . . . . . . . . . . .36422709 . . . . . . . . . . . . . .36422710 . . . . . . . . . . . . . .36422711 . . . . . . . . . . . . . .36422712 . . . . . . . . . . . . . .36422713 . . . . . . . . . . . . . .36422714 . . . . . . . . . . . . . .36422715 . . . . . . . . . . . . . .36422716 . . . . . . . . . . . . . .36422717 . . . . . . . . . . . . . .36422718 . . . . . . . . . . . . . .36422719 . . . . . . . . . . . . . .36422720 . . . . . . . . . . . . . .36422721 . . . . . . . . . . . . . .22522722 . . . . . . . . . . . . . .22522723 . . . . . . . . . . . . . .22522724 . . . . . . . . . .224,22522725 . . . . . . . . . .224,22522726 . . . . . . . . . .224,22522727 . . . . . . . . . .224,22522728 . . . . . . . . . .224,22522729 . . . . . . . . . .224,22522730 . . . . . . . . . . . . . .22522731 . . . . . . . . . .224,22522732 . . . . . . . . . .224,22522733 . . . . . . . . . . . . . .22522734 . . . . . . . . . . . . . .22522735 . . . . . . . . . . . . . .22522736 . . . . . . . . . . . . . .22522737 . . . . . . . . . . . . . .34922741 . . . . . . . . . . . . . .34922742 . . . . . . . . . . . . . .34922743 . . . . . . . . . . . . . .34922744 . . . . . . . . . . . . . .34922745 . . . . . . . . . . . . . .34922746 . . . . . . . . . . . . . .34922747 . . . . . . . . . . . . . .34922748 . . . . . . . . . . . . . .34922749 . . . . . . . . . . . . . .37722750 . . . . . . . . . . . . . .37722751 . . . . . . . . . . . . . .37722753 . . . . . . . . . . . . . .377

22754 . . . . . . . . . . . . . .37722755 . . . . . . . . . . . . . .37722756 . . . . . . . . . . . . . .37722757 . . . . . . . . . . . . . .37722758 . . . . . . . . . . . . . .37722759 . . . . . . . . . . . . . .37722760 . . . . . . . . . . . . . .37722761 . . . . . . . . . . . . . .37722762 . . . . . . . . . . . . . .37722763 . . . . . . . . . . . . . .37722764 . . . . . . . . . . . . . .37722765 . . . . . . . . . . . . . .37722766 . . . . . . . . . . . . . .36922767 . . . . . . . . . . . . . .36922768 . . . . . . . . . . . . . .36922769 . . . . . . . . . . . . . .36922770 . . . . . . . . . . . . . .36922771 . . . . . . . . . . . . . .36922772 . . . . . . . . . . . . . .36922773 . . . . . . . . . . . . . .36922774 . . . . . . . . . . . . . .36922775 . . . . . . . . . . . . . .36922776 . . . . . . . . . . . . . .36922777 . . . . . . . . . . . . . .36922778 . . . . . . . . . . . . . .36922779 . . . . . . . . . .247,26222780 . . . . . . . . . .247,26222781 . . . . . . . . . .247,26222782 . . . . . . . . . .247,26222783 . . . . . . . . . . . . . .38522784 . . . . . . . . . . . . . .38522788 . . . . . . . . . . . . . .35722789 . . . . . . . . . . . . . .35722790 . . . . . . . . . . . . . .35722791 . . . . . . . . . . . . . .35722792 . . . . . . . . . . . . . .35722793 . . . . . . . . . . . . . .35722800 . . . . . . . . . .229,30322809 . . . . . . . . . . . . . .21922810 . . . . . . . . . . . . . .21922811 . . . . . . . . . . . . . .21922812 . . . . . . . . . . . . . .21922813 . . . . . . . . . . . . . .21922814 . . . . . . . . . . . . . .21922815 . . . . . . . . . . . . . .21922820 . . . . . . . . . .229,30322831 . . . . . . . . . . . . . .36322832 . . . . . . . . . . . . . .36322833 . . . . . . . . . . . . . .36322834 . . . . . . . . . . . . . .36322835 . . . . . . . . . . . . . .36322836 . . . . . . . . . . . . . .36322839 . . . . . . .204,273,29622839-R . . . . .204,273,29622840 . . . . . . . . . . . . . .43722841 . . . . . . . . . . . . . .43722842 . . . . . . . . . . . . . .43722843 . . . . . . . . . . . . . .43722844 . . . . . . . . . . . . . .43722845 . . . . . . . . . . . . . .43722846 . . . . . . . . . . . . . .43722847 . . . . . . . . . . . . . .43722848 . . . . . . . . . . . . . .43722849 . . . . . . . . . . . . . .43722850 . . . . . . . . . . . . . .43722855 . . . . . . . . . . . . . .24322856 . . . . . . . . . .358,36722857 . . . . . . . . . .358,36722858 . . . . . . . . . . . . . .27822863 . . . . . . . . . . . . . .31722864 . . . . . . . . . . . . . .31722865 . . . . . . . . . . . . . .31722866 . . . . . . . . . . . . . .31722867 . . . . . . . . . . . . . .31722868 . . . . . . . . . . . . . .31722869 . . . . . . . . . . . . . .31722870 . . . . . . . . . . . . . .31722871 . . . . . . . . . . . . . .31722872 . . . . . . . . . . . . . .31722873 . . . . . . . . . . . . . .31722875 . . . . . . . . . . . . . .31722876 . . . . . . . . . . . . . .317

22878 . . . . . . . . . . . . . .31722879 . . . . . . . . . . . . . .31722880 . . . . . . . . . . . . . .31722881 . . . . . . . . . . . . . .31722882 . . . . . . . . . . . . . .31722883 . . . . . . . . . . . . . .31722884 . . . . . . . . . . . . . .31722885 . . . . . . . . . . . . . .31722886 . . . . . . . . . . . . . .31722887 . . . . . . . . . . . . . .31722889 . . . . . . . . . . . . . .31722890 . . . . . . . . . . . . . .31722891 . . . . . . . . . . . . . .31722892 . . . . . . . . . . . . . .31722893 . . . . . . . . . . . . . .31722894 . . . . . . . . . . . . . .31722896 . . . . . . . . . . . . . .32022897 . . . . . . . . . . . . . .32022898 . . . . . . . . . . . . . .32122899 . . . . . . . . . . . . . .32122900 . . . . . . . . . . . . . .32122901 . . . . . . . . . . . . . .32122902 . . . . . . . . . . . . . .32122903 . . . . . . . . . . . . . .32122904 . . . . . . . . . . . . . .31522905 . . . . . . . . . . . . . .31522906 . . . . . . . . . . . . . .31522907 . . . . . . . . . . . . . .31522909 . . . . . . . . . . . . . .31522910 . . . . . . . . . . . . . .31522911 . . . . . . . . . . . . . .31522912 . . . . . . . . . . . . . .31522914 . . . . . . . . . . . . . .32022915 . . . . . . . . . . . . . .32022916 . . . . . . . . . . . . . .41822917 . . . . . . . . . . . . . .41822918 . . . . . . . . . . . . . .41822919 . . . . . . . . . . . . . .41822920 . . . . . . . . . . . . . .41822921 . . . . . . . . . . . . . .43522921-PI . . . . . . . . . . .43522922 . . . . . . . . . . . . . .43522922-PI . . . . . . . . . . .43522923 . . . . . . . . . . . . . .43522923-PI . . . . . . . . . . .43522924 . . . . . . . . . . . . . .43522924-PI . . . . . . . . . . .43522925 . . . . . . . . . . . . . .43522925-PI . . . . . . . . . . .43522926 . . . . . . . . . . . . . .43522926-PI . . . . . . . . . . .43522927 . . . . . . . . . . . . . .43522927-PI . . . . . . . . . . .43522928 . . . . . . . . . . . . . .43522928-PI . . . . . . . . . . .43522929 . . . . . . . . . . . . . .43522929-PI . . . . . . . . . . .43522930 . . . . . . . . . . . . . .41722931 . . . . . . . . . . . . . .41722932 . . . . . . . . . . . . . .41722933 . . . . . . . . . . . . . .41722934 . . . . . . . . . . . . . .41722935 . . . . . . . . . . . . . .41722936 . . . . . . . . . . . . . .41722937 . . . . . . . . . . . . . .41722938 . . . . . . . . . . . . . .41722939 . . . . . . . . . . . . . .41722940 . . . . . . . . . . . . . .41722941 . . . . . . . . . . . . . .41722942 . . . . . . . . . . . . . .41722943 . . . . . . . . . . . . . .41722944 . . . . . . . . . . . . . .41722945 . . . . . . . . . . . . . .41722946 . . . . . . . . . . . . . .41722947 . . . . . . . . . . . . . .41722948 . . . . . . . . . . . . . .41722949 . . . . . . . . . . . . . .41722973 . . . . . . . . . . . . . .21622974 . . . . . . . . . . . . . .21622975 . . . . . . . . . . . . . .21622976 . . . . . . . . . . . . . .21622979 . . . . . . . . . . . . . .218

22980 . . . . . . . . . . . . . .21822983 . . . . . . . . . . . . . .21722984 . . . . . . . . . . . . . .21722985 . . . . . . . . . . . . . .21722986 . . . . . . . . . . . . . .24522987 . . . . . . . . . . . . . .24522988 . . . . . . . . . . . . . .24522989 . . . . . . . . . . . . . .24522990 . . . . . . . . . . . . . .24622991 . . . . . . . . . . . . . .24622992 . . . . . . . . . . . . . .24622993 . . . . . . . . . . . . . .24622994 . . . . . . . . . . . . . .23022995 . . . . . . . . . . . . . .23022996 . . . . . . . . . . . . . .23022997 . . . . . . . . . .257,28022998 . . . . . . . . . .281,32322999 . . . . . . .257,281,32323001 . . . . . . . . . . . . . .32323002 . . . . . . . . . . . . . .32323004 . . . . . . . . . . . . . .32323009 . . . . . . . . . . . . . .32523010 . . . . . . . . . . . . . .23923011 . . . . . . . . . . . . . .32423012 . . . . . . . . . . . . . .32423015 . . . . . . . . . . . . . .27723016 . . . . . . . . . . . . . .28023017 . . . . . . . . . . . . . .28023018 . . . . . . .220,230,28023019 . . . . . . . . . .263,28023020 . . . . . . . . . . . . . .27123026 . . . . . . . . . . . . . .27723027 . . . . . . . . . . . . . .27723029 . . . . . . . . . . . . . .32423030 . . . . . . . . . . . . . .32423031 . . . . . . . . . .229,30323032 . . . . . . . . . .229,30323033 . . . . . . . . . . . . . .32323034 . . . . . . .241,281,32323035 . . . . . . . . . .228,23823036 . . . . . . . . . . . . . .23823037 . . . . . . . . . . . . . .23823038 . . . . . . . . . . . . . .24823039 . . . . . . . . . . . . . .22923040 . . . . . . . . . . . . . .22923041 . . . . . . . . . . . . . .23823042 . . . . . . . . . . . . . .22923043 . . . . . . . . . . . . . .23823044 . . . . . . . . . . . . . .23823045 . . . . . . . . . . . . . .23823052 . . . . . . . . . . . . . .23823053 . . . . . . . . . . . . . .23823057 . . . . . . . . . . . . . .25523058 . . . . . . . . . . . . . .25523061 . . . . . . . . . . . . . .24823062 . . . . . . . . . . . . . .24823063 . . . . . . . . . . . . . .24823064 . . . . . . . . . . . . . .23823065 . . . . . . . . . . . . . .30423066 . . . . . . . . . . . . . .30423067 . . . . . . . . . . . . . .30423068 . . . . . . . . . . . . . .30423069 . . . . . . . . . . . . . .30423070 . . . . . . . . . . . . . .30423071 . . . . . . . . . . . . . .30423072 . . . . . . . . . . . . . .23623073 . . . . . . . . . . . . . .23623074 . . . . . . . . . . . . . .23623075 . . . . . . . . . . . . . .23623076 . . . . . . . . . . . . . .23623078 . . . . . . . . . . . . . .24023079 . . . . . . . . . . . . . .24023080 . . . . . . . . . . . . . .25623081 . . . . . . . . . .236,25823082 . . . . . . . . . . . . . .36323083 . . . . . . . . . . . . . .36323084 . . . . . . . . . . . . . .36323085 . . . . . . . . . . . . . .36323086 . . . . . . . . . . . . . .36323087 . . . . . . . . . . . . . .36323088 . . . . . . . . . . . . . .36323089 . . . . . . . . . . . . . .363

23090 . . . . . . . . . . . . . .36323091 . . . . . . . . . . . . . .36323092 . . . . . . . . . . . . . .36323093 . . . . . . . . . . . . . .36323094 . . . . . . . . . . . . . .36323095 . . . . . . . . . . . . . .36323100 . . . . . . . . . . . . . .31423101 . . . . . . . . . . . . . .31423102 . . . . . . . . . . . . . .31423103 . . . . . . . . . . . . . .31423104 . . . . . . . . . . . . . .31423105 . . . . . . . . . . . . . .31423106 . . . . . . . . . . . . . .31423107 . . . . . . . . . . . . . .31423108 . . . . . . . . . . . . . .31423109 . . . . . . . . . . . . . .31423110 . . . . . . . . . . . . . .31423111 . . . . . . . . . . . . . .31423112 . . . . . . . . . . . . . .31423113 . . . . . . . . . . . . . .31423114 . . . . . . . . . . . . . .31423115 . . . . . . . . . . . . . .31423116 . . . . . . . . . . . . . .31423117 . . . . . . . . . . . . . .31423118 . . . . . . . . . . . . . .31423119 . . . . . . . . . . . . . .31423120 . . . . . . . . . . . . . .31423121 . . . . . . . . . . . . . .31423122 . . . . . . . . . . . . . .31423123 . . . . . . . . . . . . . .31423124 . . . . . . . . . . . . . .31423125 . . . . . . . . . . . . . .31423126 . . . . . . . . . . . . . .31423127 . . . . . . . . . . . . . .31423128 . . . . . . . . . . . . . .31423129 . . . . . . . . . .310,31423130 . . . . . . . . . . . . . .31423131 . . . . . . . . . . . . . .31423132 . . . . . . . . . . . . . .31423133 . . . . . . . . . . . . . .31423134 . . . . . . . . . .310,31423135 . . . . . . . . . . . . . .31423136 . . . . . . . . . .310,31423137 . . . . . . . . . . . . . .31423138 . . . . . . . . . . . . . .31423139 . . . . . . . . . . . . . .31423140 . . . . . . . . . . . . . .31423141 . . . . . . . . . . . . . .31323142 . . . . . . . . . . . . . .32223143 . . . . . . . . . . . . . .32223144 . . . . . . . . . . . . . .32223145 . . . . . . . . . . . . . .32223146 . . . . . . . . . . . . . .32223147 . . . . . . . . . . . . . .32223148 . . . . . . . . . . . . . .32223149 . . . . . . . . . . . . . .32223150 . . . . . . . . . . . . . .31423151 . . . . . . . . . . . . . .31423152 . . . . . . . . . . . . . .31423153 . . . . . . . . . . . . . .31423154 . . . . . . . . . . . . . .31423155 . . . . . . . . . . . . . .31423156 . . . . . . . . . . . . . .31423157 . . . . . . . . . . . . . .31423158 . . . . . . . . . . . . . .31423159 . . . . . . . . . . . . . .31423160 . . . . . . . . . . . . . .31423161 . . . . . . . . . . . . . .31423162 . . . . . . . . . . . . . .31423163 . . . . . . . . . . . . . .31423164 . . . . . . . . . . . . . .31423165 . . . . . . . . . . . . . .31423166 . . . . . . . . . . . . . .31423167 . . . . . . . . . . . . . .31423168 . . . . . . . . . . . . . .31423169 . . . . . . . . . . . . . .31423170 . . . . . . . . . . . . . .31423171 . . . . . . . . . . . . . .31423172 . . . . . . . . . . . . . .31423173 . . . . . . . . . . . . . .31423174 . . . . . . . . . . . . . .31423175 . . . . . . . . . . . . . .314


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INDEX

Catalog #23176 . . . . . . . . . . . . . .31423177 . . . . . . . . . . . . . .31423178 . . . . . . . . . . . . . .31423179 . . . . . . . . . .310,31423180 . . . . . . . . . . . . . .31423181 . . . . . . . . . . . . . .31423182 . . . . . . . . . . . . . .31423183 . . . . . . . . . . . . . .31423184 . . . . . . . . . .310,31423185 . . . . . . . . . . . . . .31423186 . . . . . . . . . .310,31423187 . . . . . . . . . . . . . .31423188 . . . . . . . . . . . . . .31423189 . . . . . . . . . . . . . .31423190 . . . . . . . . . . . . . .31423191 . . . . . . . . . . . . . .31423192 . . . . . . . . . . . . . .31423193 . . . . . . . . . . . . . .31423194 . . . . . . . . . . . . . .31423195 . . . . . . . . . . . . . .31423196 . . . . . . . . . . . . . .31423197 . . . . . . . . . . . . . .31323198 . . . . . . . . . . . . . .32223199 . . . . . . . . . . . . . .32223200 . . . . . . . . . . . . . .32223201 . . . . . . . . . . . . . .32223202 . . . . . . . . . . . . . .32223203 . . . . . . . . . . . . . .32223204 . . . . . . . . . . . . . .32223205 . . . . . . . . . . . . . .32223206 . . . . . . . . . . . . . .32223207 . . . . . . . . . . . . . .32223208 . . . . . . . . . . . . . .32223209 . . . . . . . . . . . . . .32223210 . . . . . . . . . . . . . .32223211 . . . . . . . . . . . . . .32223212 . . . . . . . . . . . . . .32223213 . . . . . . . . . . . . . .32223214 . . . . . . . . . . . . . .32223215 . . . . . . . . . . . . . .32223216 . . . . . . . . . . . . . .32223300.1 . . . . . . . . . . . .21023300.25 . . . . . . . . . . .21023300.5 . . . . . . . . . . . .21023301.1 . . . . . . . . . . . .21023301.25 . . . . . . . . . . .21023301.5 . . . . . . . . . . . .21023302.1 . . . . . . . . . . . .21023302.25 . . . . . . . . . . .21023302.5 . . . . . . . . . . . .21023303.1 . . . . . . . . . . . .21023303.25 . . . . . . . . . . .21023303.5 . . . . . . . . . . . .21023304.1 . . . . . . . . . . . .21023304.25 . . . . . . . . . . .21023304.5 . . . . . . . . . . . .21023305.1 . . . . . . . . . . . .21023305.25 . . . . . . . . . . .21023305.5 . . . . . . . . . . . .21023306.1 . . . . . . . . . . . .21023306.5 . . . . . . . . . . . .21023307.1 . . . . . . . . . . . .21023307.5 . . . . . . . . . . . .21023308.1 . . . . . . . . . . . .21023308.25 . . . . . . . . . . .21023308.5 . . . . . . . . . . . .21023309.1 . . . . . . . . . . . .21023309.5 . . . . . . . . . . . .21023310.1 . . . . . . . . . . . .21023310.25 . . . . . . . . . . .21023310.5 . . . . . . . . . . . .21023311.1 . . . . . . . . . . . .21023311.25 . . . . . . . . . . .21023311.5 . . . . . . . . . . . .21023312.1 . . . . . . . . . . . .21023312.25 . . . . . . . . . . .21023312.5 . . . . . . . . . . . .21023313.1 . . . . . . . . . . . .21023313.25 . . . . . . . . . . .21023313.5 . . . . . . . . . . . .21023314.1 . . . . . . . . . . . .21023314.25 . . . . . . . . . . .210

23314.5 . . . . . . . . . . . .21023315.1 . . . . . . . . . . . .21023315.25 . . . . . . . . . . .21023315.5 . . . . . . . . . . . .21023316.1 . . . . . . . . . . . .21023316.25 . . . . . . . . . . .21023316.5 . . . . . . . . . . . .21023317.1 . . . . . . . . . . . .21023317.5 . . . . . . . . . . . .21023318.1 . . . . . . . . . . . .21123318.25 . . . . . . . . . . .21123318.5 . . . . . . . . . . . .21123319.1 . . . . . . . . . . . .21123319.25 . . . . . . . . . . .21123319.5 . . . . . . . . . . . .21123320.1 . . . . . . . . . . . .21123320.5 . . . . . . . . . . . .21123321.1 . . . . . . . . . . . .21123321.5 . . . . . . . . . . . .21123322.1 . . . . . . . . . . . .21123322.5 . . . . . . . . . . . .21123323.1 . . . . . . . . . . . .21123323.25 . . . . . . . . . . .21123323.5 . . . . . . . . . . . .21123324.1 . . . . . . . . . . . .21123324.25 . . . . . . . . . . .21123324.5 . . . . . . . . . . . .21123325.1 . . . . . . . . . . . .21123325.25 . . . . . . . . . . .21123325.5 . . . . . . . . . . . .21123326.1 . . . . . . . . . . . .21123326.25 . . . . . . . . . . .21123326.5 . . . . . . . . . . . .21123327.1 . . . . . . . . . . . .21123327.5 . . . . . . . . . . . .21123328.1 . . . . . . . . . . . .21123328.5 . . . . . . . . . . . .21123329.1 . . . . . . . . . . . .21123329.25 . . . . . . . . . . .21123329.5 . . . . . . . . . . . .21123330.1 . . . . . . . . . . . .21123330.5 . . . . . . . . . . . .21123331.1 . . . . . . . . . . . .21123331.5 . . . . . . . . . . . .21123332.1 . . . . . . . . . . . .21123332.5 . . . . . . . . . . . .21123338 . . . . . . . . . . . . . .40723339 . . . . . . . . . . . . . .40423340 . . . . . . . . . . . . . .40423341 . . . . . . . . . . . . . .40423342 . . . . . . . . . . . . . .40423343 . . . . . . . . . . . . . .40423344 . . . . . . . . . . . . . .40423345 . . . . . . . . . . . . . .40523346 . . . . . . . . . . . . . .40523347 . . . . . . . . . . . . . .40523348 . . . . . . . . . . . . . .40523349 . . . . . . . . . . . . . .40523350 . . . . . . . . . . . . . .40523351 . . . . . . . . . . . . . .40523352 . . . . . . . . . . . . . .40523353 . . . . . . . . . . . . . .40523354 . . . . . . . . . . . . . .40523355 . . . . . . . . . . . . . .40523356 . . . . . . . . . . . . . .40523357 . . . . . . . . . . . . . .40523358 . . . . . . . . . . . . . .40523359 . . . . . . . . . . . . . .40523360 . . . . . . . . . . . . . .40523362 . . . . . . . . . . . . . .40523363 . . . . . . . . . . . . . .40523364 . . . . . . . . . . . . . .40523365 . . . . . . . . . . . . . .40523366 . . . . . . . . . . . . . .40523367 . . . . . . . . . . . . . .40523368 . . . . . . . . . . . . . .40523369 . . . . . . . . . . . . . .40523370 . . . . . . . . . . . . . .40623372 . . . . . . . . . . . . . .40623373 . . . . . . . . . . . . . .40623374 . . . . . . . . . . . . . .40623375 . . . . . . . . . . . . . .406

23376 . . . . . . . . . . . . . .40623377 . . . . . . . . . . . . . .40623378 . . . . . . . . . . . . . .40623379 . . . . . . . . . . . . . .40623380 . . . . . . . . . . . . . .40623381 . . . . . . . . . . . . . .40623382 . . . . . . . . . . . . . .40623383 . . . . . . . . . . . . . .40623384 . . . . . . . . . . . . . .40623385 . . . . . . . . . . . . . .40623386 . . . . . . . . . . . . . .40623387 . . . . . . . . . . . . . .40623388 . . . . . . . . . . . . . .40723389 . . . . . . . . . . . . . .40723390 . . . . . . . . . . . . . .40723391 . . . . . . . . . . . . . .40723392 . . . . . . . . . . . . . .40723393 . . . . . . . . . . . . . .40723394 . . . . . . . . . . . . . .40723395 . . . . . . . . . . . . . .40723396 . . . . . . . . . . . . . .36623397 . . . . . . . . . . . . . .36623398 . . . . . . . . . . . . . .36623399 . . . . . . . . . . . . . .36623400 . . . . . . . . . . . . . .31223401 . . . . . . . . . . . . . .31223402 . . . . . . . . . . . . . .31223403 . . . . . . . . . . . . . .21923404 . . . . . . . . . . . . . .21923405 . . . . . . . . . .224,22523406 . . . . . . . . . . . . . .22223407 . . . . . . . . . . . . . .22223408 . . . . . . . . . . . . . .22223409 . . . . . . . . . . . . . .22223410 . . . . . . . . . . . . . .22223411 . . . . . . . . . . . . . .22223412 . . . . . . . . . . . . . .22223413 . . . . . . . . . . . . . .22223414 . . . . . . . . . . . . . .22223415 . . . . . . . . . . . . . .22323416 . . . . . . . . . . . . . .22323417 . . . . . . . . . . . . . .22323418 . . . . . . . . . . . . . .22223419 . . . . . . . . . . . . . .22223420 . . . . . . . . . . . . . .22223996 . . . . . . . . . . . . . .40223997 . . . . . . . . . . . . . .38923998 . . . . . . . . . . . . . .40223999 . . . . . . . . . . . . . .40324002 . . . . . . . . . . . . . .39524003 . . . . . . . . . . . . . .39524004 . . . . . . . . . . . . . .39724008 . . . . . . . . . . . . . .39524011 . . . . . . . . . . . . . .39624014 . . . . . . . . . . . . . .39524016 . . . . . . . . . . . . . .39524017 . . . . . . . . . . . . . .39724020 . . . . . . . . . . . . . .39724021 . . . . . . . . . . . . . .39724025 . . . . . . . . . . . . . .39724027 . . . . . . . . . . . . . .39724028 . . . . . . . . . . . . . .39724029 . . . . . . . . . . . . . .39724030 . . . . . . . . . . . . . .39724031 . . . . . . . . . . . . . .39224032 . . . . . . . . . . . . . .39224034 . . . . . . . . . . . . . .39224035 . . . . . . . . . . . . . .39224036 . . . . . . . . . . . . . .39224038 . . . . . . . . . . . . . .39224048 . . . . . . . . . . . . . .39724049 . . . . . . . . . . . . . .39424050 . . . . . . . . . . . . . .39224051 . . . . . . . . . . . . . .39224052 . . . . . . . . . . . . . .39224053 . . . . . . . . . . . . . .42624054 . . . . . . . . . . . . . .42424055 . . . . . . . . . . . . . .42424056 . . . . . . . . . . . . . .42424057 . . . . . . . . . . . . . .42424058 . . . . . . . . . . . . . .42424059 . . . . . . . . . . . . . .424

24060 . . . . . . . . . . . . . .42424061 . . . . . . . . . . . . . .42424062 . . . . . . . . . . . . . .42424063 . . . . . . . . . . . . . .42424064 . . . . . . . . . . . . . .42424065 . . . . . . . . . . . . . .42424066 . . . . . . . . . . . . . .42424067 . . . . . . . . . . . . . .42424068 . . . . . . . . . . . . . .42424069 . . . . . . . . . . . . . .42424070 . . . . . . . . . . . . . .42424071 . . . . . . . . . . . . . .42424072 . . . . . . . . . . . . . .42424073 . . . . . . . . . . . . . .42424074 . . . . . . . . . . . . . .42424075 . . . . . . . . . . . . . .42424076 . . . . . . . . . . . . . .42424077 . . . . . . . . . . . . . .42424078 . . . . . . . . . . . . . .42424079 . . . . . . . . . . . . . .42424080 . . . . . . . . . . . . . .42424081 . . . . . . . . . . . . . .42424082 . . . . . . . . . . . . . .42424083 . . . . . . . . . . . . . .42424084 . . . . . . . . . . . . . .42424085 . . . . . . . . . . . . . .42424086 . . . . . . . . . . . . . .42424087 . . . . . . . . . . . . . .42424088 . . . . . . . . . . . . . .42424089 . . . . . . . . . . . . . .42424090 . . . . . . . . . . . . . .42424091 . . . . . . . . . . . . . .42424100 . . . . . . . . . . . . . .41224104 . . . . . . . . . . . . . .41224108 . . . . . . . . . . . . . .41224120 . . . . . . . . . .412,41724121 . . . . . . . . . . . . . .42124123 . . . . . . . . . . . . . .41924129 . . . . . . . . . . . . . .43024130 . . . . . . . . . . . . . .43524130-PI . . . . . . . . . . .43524131 . . . . . . . . . . . . . .43524131-PI . . . . . . . . . . .43524132 . . . . . . . . . . . . . .43524132-PI . . . . . . . . . . .43524133 . . . . . . . . . . . . . .43524133-PI . . . . . . . . . . .43524134 . . . . . . . . . . . . . .43524134-PI . . . . . . . . . . .43524140 . . . . . . . . . . . . . .41024140-650 . . . . . . . . . .41024141 . . . . . . . . . . . . . .41024141-650 . . . . . . . . . .41024142 . . . . . . . . . . . . . .41024142-650 . . . . . . . . . .41024143 . . . . . . . . . . . . . .41024143-650 . . . . . . . . . .41024144 . . . . . . . . . . . . . .41224145 . . . . . . . . . . . . . .41224146 . . . . . . . . . . . . . .41224147 . . . . . . . . . . . . . .41224148 . . . . . . . . . . . . . .41224151 . . . . . . . . . . . . . .41924160 . . . . . . . . . . . . . .41424161 . . . . . . . . . . . . . .41424162 . . . . . . . . . . . . . .41424163 . . . . . . . . . . . . . .41424164 . . . . . . . . . . . . . .41424165 . . . . . . . . . . . . . .41424166 . . . . . . . . . . . . . .41424167 . . . . . . . . . . . . . .41424168 . . . . . . . . . . . . . .41424169 . . . . . . . . . . . . . .41424170 . . . . . . . . . .415,41724171 . . . . . . . . . .415,41724172 . . . . . . . . . . . . . .41124173 . . . . . . . . . . . . . .41124174 . . . . . . . . . . . . . .41124175 . . . . . . . . . . . . . .41124176 . . . . . . . . . . . . . .41124177 . . . . . . . . . . . . . .41124178 . . . . . . . . . . . . . .411

24179 . . . . . . . . . . . . . .41124180 . . . . . . . . . . . . . .41024180-650 . . . . . . . . . .41024181 . . . . . . . . . . . . . .41024181-650 . . . . . . . . . .41024182 . . . . . . . . . . . . . .41024182-650 . . . . . . . . . .41024183 . . . . . . . . . . . . . .41024183-650 . . . . . . . . . .41024185 . . . . . . . . . . . . . .42124186 . . . . . . . . . . . . . .42124187 . . . . . . . . . . . . . .42124188 . . . . . . . . . . . . . .42124189 . . . . . . . . . . . . . .42124190 . . . . . . . . . . . . . .42124191 . . . . . . . . . . . . . .42124192 . . . . . . . . . . . . . .42124193 . . . . . . . . . . . . . .42124194 . . . . . . . . . . . . . .42124195 . . . . . . . . . . . . . .42124196 . . . . . . . . . . . . . .42124197 . . . . . . . . . . . . . .42124198 . . . . . . . . . . . . . .42124199 . . . . . . . . . . . . . .42124205 . . . . . . . . . . . . . .42124206 . . . . . . . . . . . . . .42124207 . . . . . . . . . . . . . .42124208 . . . . . . . . . . . . . .42124215 . . . . . . . . . . . . . .41924216 . . . . . . . . . . . . . .41424217 . . . . . . . . . . . . . .41424218 . . . . . . . . . . . . . .41524219 . . . . . . . . . . . . . .41524226 . . . . . . . . . . . . . .41924229 . . . . . . . . . . . . . .41524230 . . . . . . . . . . . . . .42624232 . . . . . . . . . . . . . .41524233 . . . . . . . . . . . . . .41524234 . . . . . . . . . . . . . .41524235 . . . . . . . . . . . . . .41524236 . . . . . . . . . . . . . .41524237 . . . . . . . . . . . . . .41524238 . . . . . . . . . . . . . .41524239 . . . . . . . . . . . . . .41524245 . . . . . . . . . . . . . .41524246 . . . . . . . . . . . . . .41524247 . . . . . . . . . . . . . .41524248 . . . . . . . . . . . . . .41524249 . . . . . . . . . . . . . .41524255 . . . . . . . . . . . . . .41524256 . . . . . . . . . . . . . .41524257 . . . . . . . . . . . . . .41524258 . . . . . . . . . . . . . .41524259 . . . . . . . . . . . . . .41524260 . . . . . . . . . . . . . .41524261 . . . . . . . . . . . . . .41524262 . . . . . . . . . . . . . .41524263 . . . . . . . . . . . . . .41524264 . . . . . . . . . . . . . .41524265 . . . . . . . . . . . . . .41524266 . . . . . . . . . . . . . .41524267 . . . . . . . . . . . . . .41824268 . . . . . . . . . . . . . .41324269 . . . . . . . . . . . . . .41224270 . . . . . . . . . . . . . .41224282 . . . . . . . . . .418,41924285 . . . . . . . . . . . . . .41324295 . . . . . . . . . . . . . .42624323 . . . . . . . . . . . . . .22824324 . . . . . . . . . .214,24424351 . . . . . . . . . . . . . .35624352 . . . . . . . . . . . . . .35624353 . . . . . . . . . . . . . .35624354 . . . . . . . . . . . . . .35624355 . . . . . . . . . . . . . .35624356 . . . . . . . . . . . . . .35624357 . . . . . . . . . . . . . .35624358 . . . . . . . . . . . . . .35624359 . . . . . . . . . . . . . .35624360 . . . . . . . . . . . . . .35624361 . . . . . . . . . . . . . .35624362 . . . . . . . . . . . . . .356

24363 . . . . . . . . . . . . . .35624364 . . . . . . . . . . . . . .35624365 . . . . . . . . . . . . . .35624366 . . . . . . . . . . . . . .35624367 . . . . . . . . . . . . . .35624368 . . . . . . . . . . . . . .35624369 . . . . . . . . . . . . . .35624370 . . . . . . . . . . . . . .35624383 . . . . . . . . . . . . . .35624384 . . . . . . . . . . . . . .35624385 . . . . . . . . . . . . . .35624386 . . . . . . . . . . . . . .35624433 . . . . . . . . . . . . . .35724434 . . . . . . . . . . . . . .35724443 . . . . . . . . . . . . . .35724444 . . . . . . . . . . . . . .35724445 . . . . . . . . . . . . . .35724446 . . . . . . . . . . . . . .35724453 . . . . . . . . . . . . . .35724454 . . . . . . . . . . . . . .35724455 . . . . . . . . . . . . . .35724456 . . . . . . . . . . . . . .35724473 . . . . . . . . . . . . . .35824474 . . . . . . . . . . . . . .35824485 . . . . . . . . . . . . . .35824486 . . . . . . . . . . . . . .35824487 . . . . . . . . . . . . . .35824488 . . . . . . . . . . . . . .35824493 . . . . . . . . . . . . . .35824494 . . . . . . . . . . . . . .35824495 . . . . . . . . . . . . . .35824496 . . . . . . . . . . . . . .35824497 . . . . . . . . . . . . . .35824498 . . . . . . . . . . . . . .35824501 . . . . . . . . . . . . . .35824502 . . . . . . . . . . . . . .35824503 . . . . . . . . . . . . . .35824504 . . . . . . . . . . . . . .35824505 . . . . . . . . . . . . . .35824506 . . . . . . . . . . . . . .35824508 . . . . . . . . . . . . . .36024510 . . . . . . . . . . . . . .36024511 . . . . . . . . . . . . . .36024512 . . . . . . . . . . . . . .36024513 . . . . . . . . . . . . . .35624516 . . . . . . . . . .356,36124517 . . . . . . . . . .356,36124518 . . . . . . . . . . . . . .35624518A . . . . . . . . . . . . .35624519 . . . . . . . . . . . . . .35624520 . . . . . . . . . . . . . .35624529 . . . . . . . . . . . . . .34924530 . . . . . . . . . .375,37824531 . . . . . . . . . . . . . .37824532 . . . . . . . . . . . . . .37824533 . . . . . . . . . . . . . .37824534 . . . . . . . . . . . . . .37824535 . . . . . . . . . . . . . .37824536 . . . . . . . . . . . . . .37824537 . . . . . . . . . . . . . .37824538 . . . . . . . . . . . . . .37824539 . . . . . . . . . . . . . .37824540 . . . . . . . . . . . . . .37824541 . . . . . . . . . . . . . .37924542 . . . . . . . . . . . . . .37924543 . . . . . . . . . . . . . .37924544 . . . . . . . . . . . . . .37924545 . . . . . . . . . . . . . .38024546 . . . . . . . . . . . . . .38024547 . . . . . . . . . . . . . .38024548 . . . . . . . . . . . . . .38024549 . . . . . . . . . . . . . .38024551 . . . . . . . . . . . . . .38024555 . . . . . . . . . . . . . .38024556 . . . . . . . . . . . . . .38024557 . . . . . . . . . . . . . .38124558 . . . . . . . . . . . . . .38124559 . . . . . . . . . . . . . .38124560 . . . . . . . . . . . . . .38124561 . . . . . . . . . . . . . .38124562 . . . . . . . . . . . . . .38124563 . . . . . . . . . . . . . .381


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INDEX

Catalog #24564 . . . . . . . . . . . . . .38124567 . . . . . . . . . . . . . .38124568 . . . . . . . . . . . . . .38124571 . . . . . . . . . . . . . .38124572 . . . . . . . . . . . . . .38124575 . . . . . . . . . . . . . .38124576 . . . . . . . . . . . . . .38124578 . . . . . . . . . . . . . .38124581 . . . . . . . . . . . . . .38124582 . . . . . . . . . . . . . .38124584 . . . . . . . . . . . . . .38124591 . . . . . . . . . . . . . .38124592 . . . . . . . . . . . . . .37024593 . . . . . . . . . . . . . .37024594 . . . . . . . . . . . . . .37024595 . . . . . . . . . . . . . .37024596 . . . . . . . . . . . . . .37024597 . . . . . . . . . . . . . .37024598 . . . . . . . . . . . . . .37024599 . . . . . . . . . . . . . .37024600 . . . . . . . . . . . . . .37024605 . . . . . . . . . . . . . .38224606 . . . . . . . . . . . . . .38224607 . . . . . . . . . . . . . .38224608 . . . . . . . . . . . . . .38224609 . . . . . . . . . . . . . .38224615 . . . . . . . . . . . . . .38324616 . . . . . . . . . . . . . .38324617 . . . . . . . . . .375,37824619 . . . . . . . . . . . . . .35924620 . . . . . . . . . . . . . .35924621 . . . . . . . . . . . . . .35924622 . . . . . . . . . . . . . .35924623 . . . . . . . . . . . . . .36024624 . . . . . . . . . . . . . .36024625 . . . . . . . . . . . . . .36024626 . . . . . . . . . . . . . .36024627 . . . . . . . . . . . . . .36024628 . . . . . . . . . . . . . .36024629 . . . . . . . . . . . . . .36024630 . . . . . . . . . . . . . .35924631 . . . . . . . . . . . . . .35924632 . . . . . . . . . . . . . .35924633 . . . . . . . . . . . . . .35924634 . . . . . . . . . . . . . .35924635 . . . . . . . . . . . . . .35924636 . . . . . . . . . . . . . .35924637 . . . . . . . . . . . . . .35924638 . . . . . . . . . . . . . .35924639 . . . . . . . . . . . . . .35924640 . . . . . . . . . . . . . .35924641 . . . . . . . . . . . . . .35924642 . . . . . . . . . . . . . .36124643 . . . . . . . . . . . . . .36124644 . . . . . . . . . . . . . .36124645 . . . . . . . . . . . . . .36124646 . . . . . . . . . . . . . .35624647 . . . . . . . . . . . . . .35624648 . . . . . . . . . . . . . .35624649 . . . . . . . . . . . . . .35624651 . . . . . . . . . . . . . .35624652 . . . . . . . . . . . . . .35624653 . . . . . . . . . . . . . .35624654 . . . . . . . . . . . . . .36224655 . . . . . . . . . . . . . .36224656 . . . . . . . . . . . . . .36224657 . . . . . . . . . . . . . .36224658 . . . . . .215,231,248,

279,361,36724659 . . . . . . . . . . . . . .36124662 . . . . . . . . . . . . . .36224663 . . . . . . . . . . . . . .36224664 . . . . . . . . . . . . . .36224665 . . . . . . . . . . . . . .36224668 . . . . . . . . . . . . . .35824669 . . . . . . . . . . . . . .35824670 . . . . . . . . . . . . . .35824671 . . . . . . . . . . . . . .35624672 . . . . . . . . . . . . . .35624673 . . . . . . . . . . . . . .35624674 . . . . . . . . . . . . . .35624675 . . . . . . . . . . . . . .361

24676 . . . . . . . . . . . . . .36124677 . . . . . . . . . . . . . .36024678 . . . . . . . . . . . . . .36224679 . . . . . . . . . . . . . .36224680 . . . . . . . . . . . . . .36224681 . . . . . . . . . . . . . .36224683 . . . . . . . . . . . . . .36324684 . . . . . . . . . . . . . .36324685 . . . . . . . . . . . . . .36324686 . . . . . . . . . . . . . .36324691 . . . . . . . . . . . . . .36024692 . . . . . . . . . .356,36124693 . . . . . . . . . .356,36124694 . . . . . . .364,400,40124699 . . . . . . . . . . . . . .23524700 . . . . . . . . . . . . . .37824701 . . . . . . . . . . . . . .37824702 . . . . . . . . . . . . . .37824703 . . . . . . . . . . . . . .37824704 . . . . . . . . . . . . . .37824705 . . . . . . . . . . . . . .37824706 . . . . . . . . . . . . . .37824707 . . . . . . . . . . . . . .37824708 . . . . . . . . . . . . . .37824709 . . . . . . . . . . . . . .37824710 . . . . . . . . . . . . . .37824711 . . . . . . . . . . . . . .37824712 . . . . . . . . . . . . . .37824713 . . . . . . . . . . . . . .37824715 . . . . . . . . . . . . . .37824716 . . . . . . . . . . . . . .37824717 . . . . . . . . . . . . . .38124718 . . . . . . . . . . . . . .37924719 . . . . . . . . . . . . . .37924720 . . . . . . . . . . . . . .37924721 . . . . . . . . . . . . . .37924722 . . . . . . . . . . . . . .37924723 . . . . . . . . . . . . . .37924724 . . . . . . . . . . . . . .38124725 . . . . . . . . . . . . . .38124726 . . . . . . . . . . . . . .38124727 . . . . . . . . . . . . . .38124728 . . . . . . . . . . . . . .38124729 . . . . . . . . . . . . . .38124730 . . . . . . . . . . . . . .38124734 . . . . . . . . . . . . . .38124735 . . . . . . . . . . . . . .38124737 . . . . . . . . . . . . . .38124738 . . . . . . . . . . . . . .38124739 . . . . . . . . . . . . . .38124741 . . . . . . . . . . . . . .38124742 . . . . . . . . . . . . . .38124743 . . . . . . . . . . . . . .38124746 . . . . . . . . . . . . . .37524747 . . . . . . . . . . . . . .37524748 . . . . . . . . . . . . . .37524749 . . . . . . . . . . . . . .37524750 . . . . . . . . . . . . . .38124752 . . . . . . . . . . . . . .38124755 . . . . . . . . . . . . . .38124757 . . . . . . . . . . . . . .38124759 . . . . . . . . . .348,38124760 . . . . . . . . . . . . . .38124761 . . . . . . . . . . . . . .38124762 . . . . . . . . . . . . . .38124763 . . . . . . . . . .382,38324764 . . . . . . . . . .382,38324765 . . . . . . . . . .382,38324766 . . . . . . . . . . . . . .37924767 . . . . . . . . . . . . . .37924768 . . . . . . . . . . . . . .37924769 . . . . . . . . . . . . . .37924770 . . . . . . . . . . . . . .38024771 . . . . . . . . . . . . . .38024772 . . . . . . . . . . . . . .38024773 . . . . . . . . . . . . . .38024774 . . . . . . . . . . . . . .38024775 . . . . . . . . . . . . . .38024776 . . . . . . . . . . . . . .38024777 . . . . . . . . . . . . . .38024778 . . . . . . . . . . . . . .38024779 . . . . . . . . . . . . . .380

24780 . . . . . . . . . . . . . .37024781 . . . . . . . . . . . . . .37024782 . . . . . . . . . . . . . .37024783 . . . . . . . . . . . . . .37024784 . . . . . . . . . . . . . .37024785 . . . . . . . . . . . . . .37024786 . . . . . . . . . . . . . .37024787 . . . . . . . . . . . . . .37024789 . . . . . . . . . . . . . .37124790 . . . . . . . . . . . . . .37024791 . . . . . . . . . . . . . .37024793 . . . . . . . . . . . . . .37024794 . . . . . . . . . . . . . .37024795 . . . . . . . . . . . . . .37024797 . . . . . . . . . . . . . .37124798 . . . . . . . . . . . . . .37124799 . . . . . . . . . . . . . .37124800 . . . . . . . . . . . . . .37124801 . . . . . . . . . . . . . .37124802 . . . . . . . . . . . . . .38224803 . . . . . . . . . . . . . .38224804 . . . . . . . . . . . . . .38224805 . . . . . . . . . . . . . .38224806 . . . . . . . . . . . . . .38224807 . . . . . . . . . . . . . .38224808 . . . . . . . . . .347,38424809 . . . . . . . . . .347,38424810 . . . . . . . . . . . . . .37324811 . . . . . . . . . . . . . .37324812 . . . . . . . . . . . . . .37324813 . . . . . . . . . . . . . .37324814 . . . . . . . . . . . . . .37324815 . . . . . . . . . . . . . .37324816 . . . . . . . . . . . . . .37324817 . . . . . . . . . . . . . .37324818 . . . . . . . . . . . . . .37324819 . . . . . . . . . . . . . .23724820 . . . . . . . . . . . . . .37124821 . . . . . . . . . . . . . .37124823 . . . . . . . . . . . . . .37124824 . . . . . . . . . . . . . .37124825 . . . . . . . . . . . . . .37124826 . . . . . . . . . . . . . .37124827 . . . . . . . . . .251,28624828 . . . . . . . . . .251,28624829 . . . . . . . . . .251,28624830 . . . . . . . . . . . . . .38024831 . . . . . . . . . . . . . .38024832 . . . . . . . . . . . . . .38024833 . . . . . . . . . . . . . .38024834 . . . . . . . . . . . . . .38024835 . . . . . . . . . . . . . .38024836 . . . . . . . . . . . . . .38024837 . . . . . . . . . . . . . .38024838 . . . . . . . . . . . . . .38024839 . . . . . . . . . . . . . .38024840 . . . . . . . . . . . . . .37524841 . . . . . . . . . . . . . .37524842 . . . . . . . . . . . . . .37524843 . . . . . . . . . . . . . .37524844 . . . . . . . . . . . . . .37524845 . . . . . . . . . . . . . .37524846 . . . . . . . . . . . . . .37524847 . . . . . . . . . . . . . .37524848 . . . . . . .233,269,28524849 . . . . . . .233,269,28524850 . . . . . . . . . . . . . .37424851 . . . . . . . . . . . . . .37424852 . . . . . . . . . . . . . .37424853 . . . . . . . . . . . . . .37424854 . . . . . . . . . . . . . .37424855 . . . . . . . . . . . . . .37424857 . . . . . . . . . . . . . .37424858 . . . . . . . . . . . . . .37424860 . . . . . . . . . . . . . .34824861 . . . . . . . . . . . . . .34824862 . . . . . . . . . . . . . .34824863 . . . . . . . . . . . . . .34824864 . . . . . . . . . . . . . .34824865 . . . . . . . . . . . . . .34824866 . . . . . . . . . .347,38424867 . . . . . . . . . .347,384

24868 . . . . . . . . . .347,38424869 . . . . . . . . . .347,38424870 . . . . . . . . . .347,38424871 . . . . . . . . . .347,38424873 . . . . . . . . . . . . . .34624874 . . . . . . . . . . . . . .34624875 . . . . . . . . . . . . . .34624876 . . . . . . . . . . . . . .34624877 . . . . . . . . . . . . . .34624880 . . . . . . . . . . . . . .38324881 . . . . . . . . . . . . . .38324882 . . . . . . . . . . . . . .38324883 . . . . . . . . . . . . . .38324884 . . . . . . . . . . . . . .38324885 . . . . . . . . . . . . . .38324886 . . . . . . . . . . . . . .38324887 . . . . . . . . . . . . . .38324888 . . . . . . . . . . . . . .38324889 . . . . . . . . . . . . . .38324890 . . . . . . . . . . . . . .38324891 . . . . . . . . . . . . . .38324892 . . . . . . . . . . . . . .38324894 . . . . . . . . . . . . . .37124895 . . . . . . . . . . . . . .37024896 . . . . . . . . . . . . . .25624898 . . . . . . . . . . . . . .38324899 . . . . . . . . . . . . . .25124900 . . . . . . . . . . . . . .36524901 . . . . . . . . . . . . . .36524902 . . . . . . . . . . . . . .36524903 . . . . . . . . . . . . . .36524904 . . . . . . . . . . . . . .36524905 . . . . . . . . . . . . . .36524906 . . . . . . . . . . . . . .36524907 . . . . . . . . . . . . . .36524912 . . . . . . . . . . . . . .28424913 . . . . . . . . . . . . . .30524914 . . . . . . . . . . . . . .30524915 . . . . . . . . . . . . . .30524916 . . . . . . . . . . . . . .25624917 . . . . . . . . . . . . . .25624918 . . . . . . . . . .220,28324919 . . . . . . . . . . . . . .38224920 . . . . . . . . . . . . . .37724921 . . . . . . . . . . . . . .37724922 . . . . . . . . . .374,37724923 . . . . . . . . . . . . . .37724924 . . . . . . . . . . . . . .37624925 . . . . . . . . . . . . . .37724926 . . . . . . . . . . . . . .37724927 . . . . . . . . . . . . . .37624928 . . . . . . . . . . . . . .37724929 . . . . . . . . . . . . . .37724930 . . . . . . . . . . . . . .37724931 . . . . . . . . . . . . . .37724932 . . . . . . . . . . . . . .37724933 . . . . . . . . . . . . . .37724934 . . . . . . . . . . . . . .37624935 . . . . . . . . . . . . . .37624937 . . . . . . . . . .257,28324938 . . . . . . . . . .375,37824939 . . . . . . . . . . . . . .38224940 . . . . . . . . . . . . . .38224941 . . . . . . . . . .347,38424942 . . . . . . . . . . . . . .38224943 . . . . . . . . . . . . . .38224944 . . . . . . . . . . . . . .38224945 . . . . . . . . . .347,38424952 . . . . . . . . . . . . . .37324953 . . . . . . . . . . . . . .37324956 . . . . . . . . . . . . . .37424962 . . . . . . . . . . . . . .37624967 . . . . . . . . . . . . . .37824969 . . . . . . . . . . . . . .25624970 . . . . . . . . . . . . . .25624971 . . . . . . . . . . . . . .25524972 . . . . . . . . . . . . . .25524973 . . . . . . . . . . . . . .25624974 . . . . . . . . . . . . . .26124975 . . . . . . . . . . . . . .26124976 . . . . . . . . . . . . . .21724977 . . . . . . . . . . . . . .217

24978 . . . . . . . . . . . . . .24624979 . . . . . . . . . . . . . .24624980 . . . . . . . . . . . . . .32924981 . . . . . . . . . . . . . .32924982 . . . . . . . . . . . . . .32924983 . . . . . . . . . . . . . .32924984 . . . . . . . . . . . . . .32924985 . . . . . . . . . . . . . .32924986 . . . . . . . . . . . . . .32924989 . . . . . . . . . . . . . .33724990 . . . . . . . . . . . . . .32724993 . . . . . . . . . . . . . .19524994 . . . . . . . . . . . . . .19524995 . . . . . . . . . . . . . .19524996 . . . . . . . . . . . . . .19524997 . . . . . . . . . . . . . .19524998 . . . . . . . . . . . . . .41624999 . . . . . . . . . . . . . .41625008 . . . . . . . . . . . . . .34225009 . . . . . . . . . . . . . .34225010 . . . . . . . . . . . . . .34225012 . . . . . . . . . . . . . .34025013 . . . . . . . . . . . . . .34025014 . . . . . . . . . . . . . .34025015 . . . . . . . . . .334,33625016 . . . . . . . . . . . . . .33425017 . . . . . . . . . . . . . .34525018 . . . . . . . . . . . . . .34525020 . . . . . . . . . . . . . .34525021 . . . . . . . . . . . . . .19725022 . . . . . . . . . .196,19725023 . . . . . . . . . .196,19725024 . . . . . . . . . . . . . .19625026 . . . . . . . . . . . . . .19625028 . . . . . . . . . . . . . .13525030 . . . . . . . . . . . . . .13525032 . . . . . . . . . . . . . .13725033 . . . . . . . . . . . . . .13725034 . . . . . . . . . . . . . .13725035 . . . . . . . . . . . . . .13725036 . . . . . . . . . . . . . .13725037 . . . . . . . . . . . . . .13725038 . . . . . . . . . . . . . .13725039 . . . . . . . . . . . . . .13725040 . . . . . . . . . . . . . .19725042 . . . . . . . . . . . . . .13525043 . . . . . . . . . . . . . .33525044 . . . . . . . . . . . . . .13525045 . . . . . . . . . . . . . .13725046 . . . . . . . . . . . . . .13725047 . . . . . . . . . . . . . .13725048 . . . . . . . . . . . . . .13725049 . . . . . . . . . . . . . .13725050 . . . . . . . . . . . . . .13725051 . . . . . . . . . . . . . .13725052 . . . . . . . . . . . . . .13725053 . . . . . . . . . . . . . .13725054 . . . . . . . . . . . . . .13725055 . . . . . . . . . . . . . .13725056 . . . . . . . . . . . . . .13725057 . . . . . . . . . .196,19725058 . . . . . . . . . . . . . .32725059 . . . . . . . . . . . . . .32725060 . . . . . . . . . . . . . .19725061 . . . . . . . . . . . . . .19725062 . . . . . . . . . . . . . .19625065 . . . . . . . . . .332,33625066 . . . . . . . . . .332,33625067 . . . . . . . . . .332,33625068 . . . . . . . . . . . . . .33225069 . . . . . . . . . .333,33625070 . . . . . . . . . .333,33625071 . . . . . . . . . . . . . .35125072 . . . . . . . . . . . . . .35125073 . . . . . . . . . . . . . .35125074 . . . . . . . . . . . . . .35125075 . . . . . . . . . . . . . .35125076 . . . . . . . . . . . . . .35125077 . . . . . . . . . . . . . .35125078 . . . . . . . . . . . . . .35125080 . . . . . . . . . . . . . .13525081 . . . . . . . . . . . . . .135

25082 . . . . . . . . . . . . . .19725083 . . . . . . . . . . . . . .19725084 . . . . . . . . . . . . . .19725085 . . . . . . . . . . . . . .19725086 . . . . . . . . . . . . . .19725087 . . . . . . . . . . . . . .19725088 . . . . . . . . . . . . . .19725095 . . . . . . . . . .334,33625096 . . . . . . . . . .334,33625097 . . . . . . . . . . . . . .33625100 . . . . . . . . . . . . . .35125101 . . . . . . . . . . . . . .35125102 . . . . . . . . . . . . . .35125103 . . . . . . . . . . . . . .35125104 . . . . . . . . . . . . . .35125105 . . . . . . . . . . . . . .35125106 . . . . . . . . . . . . . .35125107 . . . . . . . . . . . . . .35125108 . . . . . . . . . . . . . .35125109 . . . . . . . . . . . . . .35125110 . . . . . . . . . . . . . .35125111 . . . . . . . . . . . . . .35125112 . . . . . . . . . . . . . .35125113 . . . . . . . . . . . . . .35125114 . . . . . . . . . . . . . .35125115 . . . . . . . . . . . . . .35125116 . . . . . . . . . . . . . .35125117 . . . . . . . . . . . . . .35125118 . . . . . . . . . . . . . .35125119 . . . . . . . . . . . . . .35125120 . . . . . . . . . . . . . .35125121 . . . . . . . . . . . . . .35125122 . . . . . . . . . . . . . .35125123 . . . . . . . . . . . . . .35125124 . . . . . . . . . . . . . .35125125 . . . . . . . . . . . . . .35125126 . . . . . . . . . . . . . .35125127 . . . . . . . . . . . . . .35125128 . . . . . . . . . . . . . .35125129 . . . . . . . . . . . . . .35125130 . . . . . . . . . . . . . .35125131 . . . . . . . . . . . . . .35125132 . . . . . . . . . . . . . .35125133 . . . . . . . . . . . . . .35125134 . . . . . . . . . . . . . .35125135 . . . . . . . . . . . . . .35125138 . . . . . . . . . . . . . .34425139 . . . . . . . . . .327,33725140 . . . . . . . . . .327,33725143 . . . . . . . . . . . . . .33125144 . . . . . . . . . . . . . .33125145 . . . . . . . . . . . . . .33125146 . . . . . . . . . . . . . .33125147 . . . . . . . . . . . . . .35025148 . . . . . . . . . . . . . .35025149 . . . . . . . . . . . . . .35025150 . . . . . . . . . . . . . .35025151 . . . . . . . . . . . . . .35025152 . . . . . . . . . . . . . .35025153 . . . . . . . . . . . . . .35025154 . . . . . . . . . . . . . .35025155 . . . . . . . . . . . . . .35025156 . . . . . . . . . . . . . .35025157 . . . . . . . . . . . . . .35025158 . . . . . . . . . . . . . .35025159 . . . . . . . . . . . . . .35025160 . . . . . . . . . . . . . .33225162 . . . . . . . . . . . . . .33225170 . . . . . . . . . . . . . .33225171 . . . . . . . . . . . . . .33225172 . . . . . . . . . . . . . .33225173 . . . . . . . . . . . . . .33225174 . . . . . . . . . . . . . .33225175 . . . . . . . . . . . . . .33225176 . . . . . . . . . . . . . .33225181 . . . . . . . . . . . . . .33525182 . . . . . . . . . . . . . .33525183 . . . . . . . . . . . . . .33525184 . . . . . . . . . . . . . .33525185 . . . . . . . . . . . . . .33525186 . . . . . . . . . . . . . .33525187 . . . . . . . . . . . . . .335


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INDEX

Catalog #25188 . . . . . . . . . . . . . .33525189 . . . . . . . . . . . . . .34125190 . . . . . . . . . . . . . .33525191 . . . . . . . . . . . . . .33525192 . . . . . . . . . . . . . .33525193 . . . . . . . . . . . . . .33525194 . . . . . . . . . . . . . .34125208 . . . . . . . . . . . . . .33525209 . . . . . . . . . . . . . .33525210 . . . . . . . . . . . . . .33525211 . . . . . . . . . . . . . .33525212 . . . . . . . . . . . . . .33525213 . . . . . . . . . . . . . .33525214 . . . . . . . . . . . . . .33525215 . . . . . . . . . . . . . .33525216 . . . . . . . . . . . . . .33525217 . . . . . . . . . . . . . .33525218 . . . . . . . . . . . . . .33525219 . . . . . . . . . . . . . .33525220 . . . . . . . . . . . . . .33525221 . . . . . . . . . . . . . .33525222 . . . . . . . . . . . . . .33525223 . . . . . . . . . . . . . .33525224 . . . . . . . . . . . . . .33525225 . . . . . . . . . . . . . .33525226 . . . . . . . . . . . . . .33525227 . . . . . . . . . . . . . .33525228 . . . . . . . . . . . . . .33525229 . . . . . . . . . . . . . .33525230 . . . . . . . . . . . . . .33525231 . . . . . . . . . . . . . .33525232 . . . . . . . . . . . . . .33525233 . . . . . . . . . . . . . .33525234 . . . . . . . . . . . . . .33525235 . . . . . . . . . . . . . .33525236 . . . . . . . . . . . . . .33525237 . . . . . . . . . . . . . .33525238 . . . . . . . . . . . . . .34025239 . . . . . . . . . . . . . .34025240 . . . . . . . . . .332,33625241 . . . . . . . . . .332,33625242 . . . . . . . . . .332,33625243 . . . . . . . . . .332,33625244 . . . . . . . . . .332,33625245 . . . . . . . . . .332,33625246 . . . . . . . . . .332,33625247 . . . . . . . . . .332,33625248 . . . . . . . . . .332,33625249 . . . . . . . . . .332,33625250 . . . . . . . . . .332,33625251 . . . . . . . . . .332,33625252 . . . . . . . . . .332,33625253 . . . . . . . . . .332,33625254 . . . . . . . . . .332,33625255 . . . . . . . . . .332,33625256 . . . . . . . . . . . . . .40025257 . . . . . . . . . . . . . .40025258 . . . . . . . . . . . . . .32725259 . . . . . . . . . . . . . .32725260 . . . . . . . . . . . . . .32725261 . . . . . . . . . . . . . .32725262 . . . . . . . . . . . . . .32725263 . . . . . . . . . . . . . .32725264 . . . . . . . . . . . . . .32725265 . . . . . . . . . . . . . .32725266 . . . . . . . . . . . . . .32725267 . . . . . . . . . . . . . .32725268 . . . . . . . . . . . . . .32725269 . . . . . . . . . . . . . .32725270 . . . . . . . . . . . . . .32725271 . . . . . . . . . . . . . .32725272 . . . . . . . . . . . . . .32725273 . . . . . . . . . . . . . .32725275 . . . . . . . . . . . . . .32725276 . . . . . . . . . . . . . .32725277 . . . . . . . . . . . . . .32725278 . . . . . . . . . . . . . .32725279 . . . . . . . . . . . . . .33025280 . . . . . . . . . . . . . .33025281 . . . . . . . . . . . . . .33025282 . . . . . . . . . . . . . .32925284 . . . . . . . . . . . . . .329

25285 . . . . . . . . . . . . . .32925287 . . . . . . . . . . . . . .32925288 . . . . . . . . . . . . . .32925289 . . . . . . . . . . . . . .32925290 . . . . . . . . . . . . . .32925291 . . . . . . . . . . . . . .32925292 . . . . . . . . . . . . . .32925293 . . . . . . . . . . . . . .32925294 . . . . . . . . . . . . . .32925295 . . . . . . . . . . . . . .32925300 . . . . . . . . . . . . . .33825301 . . . . . . . . . . . . . .33825302 . . . . . . . . . . . . . .33825303 . . . . . . . . . . . . . .33825304 . . . . . . . . . . . . . .33825305 . . . . . . . . . . . . . .33825306 . . . . . . .333,336,33825307 . . . . . . .333,336,33825308 . . . . . . . . . .333,33625309 . . . . . . . . . .333,33625310 . . . . . . . . . .333,33625311 . . . . . . .336,338,34225312 . . . . . . .336,338,34225313 . . . . . . . . . . . . . .34225314 . . . . . . . . . . . . . .34225315 . . . . . . . . . . . . . .34225319 . . . . . . . . . . . . . .33825320 . . . . . . . . . . . . . .33225321 . . . . . . . . . .336,33725322 . . . . . . . . . . . . . .33625323 . . . . . . . . . .335,33625324 . . . . . . . . . . . . . .33425325 . . . . . . . . . . . . . .33725326 . . . . . . . . . . . . . .34425327 . . . . . . . . . . . . . .34425328 . . . . . . . . . . . . . .34425329 . . . . . . . . . . . . . .34425330 . . . . . . . . . . . . . .34425331 . . . . . . . . . . . . . .34425332 . . . . . . . . . . . . . .34425333 . . . . . . . . . . . . . .34425334 . . . . . . . . . . . . . .34425335 . . . . . . . . . . . . . .34425336 . . . . . . . . . . . . . .34425337 . . . . . . . . . . . . . .34425338 . . . . . . . . . . . . . .34425339 . . . . . . . . . . . . . .34425340 . . . . . . . . . . . . . .34025341 . . . . . . . . . . . . . .34425342 . . . . . . . . . . . . . .34425343 . . . . . . . . . . . . . .34425344 . . . . . . . . . . . . . .32725345 . . . . . . . . . . . . . .32725347 . . . . . . . . . . . . . .32725348 . . . . . . . . . . . . . .32725349 . . . . . . . . . . . . . .32725360 . . . . . . . . . . . . . .33125361 . . . . . . . . . . . . . .33125362 . . . . . . . . . . . . . .33125363 . . . . . . . . . . . . . .33125364 . . . . . . . . . . . . . .33125365 . . . . . . . . . . . . . .33125366 . . . . . . . . . . . . . .33125367 . . . . . . . . . . . . . .33125368 . . . . . . . . . . . . . .33125369 . . . . . . . . . . . . . .33125370 . . . . . . . . . . . . . .33125371 . . . . . . . . . . . . . .33125372 . . . . . . . . . . . . . .33125373 . . . . . . . . . . . . . .33125374 . . . . . . . . . . . . . .33125375 . . . . . . . . . . . . . .33125378 . . . . . . . . . . . . . .33125379 . . . . . . . . . . . . . .33125380 . . . . . . . . . . . . . .33125381 . . . . . . . . . . . . . .33125382 . . . . . . . . . . . . . .33125384 . . . . . . . . . . . . . .33125385 . . . . . . . . . . . . . .33125386 . . . . . . . . . . . . . .33125387 . . . . . . . . . . . . . .33125388 . . . . . . . . . . . . . .331

25389 . . . . . . . . . . . . . .33125392 . . . . . . . . . . . . . .33125393 . . . . . . . . . . . . . .40125394 . . . . . . . . . . . . . .40125395 . . . . . . . . . . . . . .33825399 . . . . . . . . . . . . . .32725400 . . . . . . . . . . . . . .13525401 . . . . . . . . . . . . . .13525403 . . . . . . . . . . . . . .33025404 . . . . . . . . . . . . . .33025405 . . . . . . . . . . . . . .33025406 . . . . . . . . . . . . . .33025407 . . . . . . . . . . . . . .33025408 . . . . . . . . . . . . . .33025409 . . . . . . . . . . . . . .33025410 . . . . . . . . . . . . . .33025412 . . . . . . . . . . . . . .33125417 . . . . . . . . . . . . . .33125420 . . . . . . . . . . . . . .33125423 . . . . . . . . . . . . . .33025424 . . . . . . . . . . . . . .33025427 . . . . . . . . . . . . . .33025428 . . . . . . . . . . . . . .33125429 . . . . . . . . . . . . . .33125431 . . . . . . . . . . . . . .32825432 . . . . . . . . . . . . . .32825433 . . . . . . . . . . . . . .32825434 . . . . . . . . . . . . . .32825435 . . . . . . . . . . . . . .32825436 . . . . . . . . . . . . . .32825437 . . . . . . . . . . . . . .32825438 . . . . . . . . . . . . . .32825439 . . . . . . . . . . . . . .32825440 . . . . . . . . . . . . . .32825441 . . . . . . . . . . . . . .32825442 . . . . . . . . . . . . . .32825444 . . . . . . . . . . . . . .32825445 . . . . . . . . . . . . . .32825446 . . . . . . . . . . . . . .32825447 . . . . . . . . . . . . . .32825448 . . . . . . . . . . . . . .32825450 . . . . . . . . . . . . . .32825451 . . . . . . . . . . . . . .32825452 . . . . . . . . . . . . . .32825453 . . . . . . . . . . . . . .32825454 . . . . . . . . . . . . . .32825455 . . . . . . . . . . . . . .32825456 . . . . . . . . . . . . . .32825457 . . . . . . . . . . . . . .32825458 . . . . . . . . . . . . . .32825459 . . . . . . . . . . . . . .32825460 . . . . . . . . . . . . . .32825461 . . . . . . . . . . . . . .32825462 . . . . . . . . . . . . . .32825463 . . . . . . . . . . . . . .32825464 . . . . . . . . . . . . . .32825465 . . . . . . . . . . . . . .32825466 . . . . . . . . . . . . . .32725467 . . . . . . . . . .327,33725468 . . . . . . . . . . . . . .32925469 . . . . . . . . . . . . . .32925470 . . . . . . . . . . . . . .32925471 . . . . . . . . . . . . . .32925472 . . . . . . . . . . . . . .32925473 . . . . . . . . . . . . . .32925474 . . . . . . . . . . . . . .33025475 . . . . . . . . . . . . . .33025476 . . . . . . . . . . . . . .33025477 . . . . . . . . . . . . . .33025478 . . . . . . . . . . . . . .33025479 . . . . . . . . . . . . . .33025480 . . . . . . . . . . . . . .33025481 . . . . . . . . . . . . . .33025482 . . . . . . . . . . . . . .33025483 . . . . . . . . . . . . . .33025484 . . . . . . . . . . . . . .33025485 . . . . . . . . . . . . . .33025486 . . . . . . . . . . . . . .33025487 . . . . . . . . . . . . . .33025488 . . . . . . . . . . . . . .33025489 . . . . . . . . . . . . . .33025490 . . . . . . . . . . . . . .330

25492 . . . . . . . . . . . . . .33125493 . . . . . . . . . . . . . .33125494 . . . . . . . . . . . . . .33125495 . . . . . . . . . . . . . .33125496 . . . . . . . . . . . . . .33125497 . . . . . . . . . . . . . .33125498 . . . . . . . . . . . . . .33125499 . . . . . . . . . . . . . .39425500 . . . . . . . . . . . . . .13425501 . . . . . . . . . . . . . .13425502 . . . . . . . . . . . . . .13425503 . . . . . . . . . . . . . .13425504 . . . . . . . . . . . . . .13425506 . . . . . . . . . . . . . .13425507 . . . . . . . . . . . . . .13425508 . . . . . . . . . . . . . .13425509 . . . . . . . . . . . . . .13425510 . . . . . . . . . . . . . .13425511 . . . . . . . . . . . . . .13425550 . . . . . . . . . . . . . .13725551 . . . . . . . . . . . . . .13725552 . . . . . . . . . . . . . .13725553 . . . . . . . . . . . . . .13725561 . . . . . . . . . . . . . .13725562 . . . . . . . . . . . . . .13725563 . . . . . . . . . . . . . .13725564 . . . . . . . . . . . . . .13725565 . . . . . . . . . . . . . .13725566 . . . . . . . . . . . . . .13725567 . . . . . . . . . . . . . .13725568 . . . . . . . . . . . . . .13725569 . . . . . . . . . . . . . .13725570 . . . . . . . . . . . . . .13725571 . . . . . . . . . . . . . .13725572 . . . . . . . . . . . . . .13725573 . . . . . . . . . . . . . .13725574 . . . . . . . . . . . . . .13725575 . . . . . . . . . . . . . .13725576 . . . . . . . . . . . . . .13725577 . . . . . . . . . . . . . .13725578 . . . . . . . . . . . . . .13725579 . . . . . . . . . . . . . .13725580 . . . . . . . . . . . . . .13725581 . . . . . . . . . . . . . .13725582 . . . . . . . . . . . . . .13725583 . . . . . . . . . . . . . .13725584 . . . . . . . . . . . . . .13725585 . . . . . . . . . . . . . .13725586 . . . . . . . . . . . . . .13725587 . . . . . . . . . . . . . .13725588 . . . . . . . . . . . . . .13725589 . . . . . . . . . . . . . .13725590 . . . . . . . . . . . . . .13725591 . . . . . . . . . . . . . .13725592 . . . . . . . . . . . . . .13725593 . . . . . . . . . . . . . .13725594 . . . . . . . . . . . . . .13725595 . . . . . . . . . . . . . .13725596 . . . . . . . . . . . . . .13725597 . . . . . . . . . . . . . .13725598 . . . . . . . . . . . . . .13725599 . . . . . . . . . . . . . .13725608 . . . . . . . . . . . . . .13725609 . . . . . . . . . . . . . .13725610 . . . . . . . . . . . . . .13725611 . . . . . . . . . . . . . .13725612 . . . . . . . . . . . . . .13725613 . . . . . . . . . . . . . .13725614 . . . . . . . . . . . . . .13725615 . . . . . . . . . . . . . .13725616 . . . . . . . . . . . . . .13725620 . . . . . . . . . . . . . .13725621 . . . . . . . . . . . . . .13725622 . . . . . . . . . . . . . .13725623 . . . . . . . . . . . . . .13725624 . . . . . . . . . . . . . .13725625 . . . . . . . . . . . . . .13725626 . . . . . . . . . . . . . .13725627 . . . . . . . . . . . . . .13725628 . . . . . . . . . . . . . .13725629 . . . . . . . . . . . . . .13625630 . . . . . . . . . . . . . .136

25631 . . . . . . . . . . . . . .13625632 . . . . . . . . . . . . . .13625634 . . . . . . . . . . . . . .13625635 . . . . . . . . . . . . . .13625636 . . . . . . . . . . . . . .13625638 . . . . . . . . . . . . . .13625639 . . . . . . . . . . . . . .13625640 . . . . . . . . . . . . . .13625641 . . . . . . . . . . . . . .13425642 . . . . . . . . . . . . . .13425657 . . . . . . . . . . . . . .13625661 . . . . . . . . . . . . . .13625665 . . . . . . . . . . . . . .13625668 . . . . . . . . . . . . . .13625988 . . . . . . . . . . . . . .39725989 . . . . . . . . . . . . . .39225990 . . . . . . . . . .196,19725991 . . . . . . . . . .395,39625992 . . . . . . . . . . . . . .39626000 . . . . . . . . . . . . . .39426001 . . . . . . . . . . . . . .39426002 . . . . . . . . . . . . . .39426003 . . . . . . . . . . . . . .39426004 . . . . . . . . . . . . . .39426005 . . . . . . . . . . . . . .39426006 . . . . . . . . . . . . . .39426007 . . . . . . . . . . . . . .39426008 . . . . . . . . . . . . . .39426009 . . . . . . . . . . . . . .39426010 . . . . . . . . . . . . . .39426011 . . . . . . . . . . . . . .39426012 . . . . . . . . . . . . . .39426013 . . . . . . . . . . . . . .39426014 . . . . . . . . . . . . . .39426015 . . . . . . . . . . . . . .39426016 . . . . . . . . . . . . . .39426017 . . . . . . . . . . . . . .39426018 . . . . . . . . . . . . . .39426019 . . . . . . . . . . . . . .39426020 . . . . . . . . . . . . . .39426021 . . . . . . . . . . . . . .39426022 . . . . . . . . . . . . . .39726023 . . . . . . . . . . . . . .39726024 . . . . . . . . . . . . . .39726029 . . . . . . . . . . . . . .39426030 . . . . . . . . . . . . . .39226031 . . . . . . . . . . . . . .39226032 . . . . . . . . . . . . . .39426033 . . . . . . . . . . . . . .39826034 . . . . . . . . . . . . . .39226035 . . . . . . . . . . . . . .39226036 . . . . . . . . . . . . . .39226037 . . . . . . . . . . . . . .39226038 . . . . . . . . . . . . . .39226039 . . . . . . . . . . . . . .39226040 . . . . . . . . . . . . . .39226043 . . . . . . . . . . . . . .39226044 . . . . . . . . . . . . . .39426045 . . . . . . . . . . . . . .39426046 . . . . . . . . . . . . . .39426047 . . . . . . . . . . . . . .39426050 . . . . . . . . . . . . . .39226051 . . . . . . . . . . . . . .39226052 . . . . . . . . . . . . . .39226053 . . . . . . . . . . . . . .39226054 . . . . . . . . . . . . . .39226055 . . . . . . . . . . . . . .39226056 . . . . . . . . . . . . . .39226057 . . . . . . . . . . . . . .39226058 . . . . . . . . . . . . . .39226059 . . . . . . . . . . . . . .39226060 . . . . . . . . . . . . . .39226061 . . . . . . . . . . . . . .39226062 . . . . . . . . . . . . . .39226063 . . . . . . . . . . . . . .39426065 . . . . . . . . . . . . . .39426077 . . . . . . . . . . . . . .39526078 . . . . . . . . . . . . . .39526079 . . . . . . . . . . . . . .39526080 . . . . . . . . . . . . . .39526081 . . . . . . . . . . . . . .39526082 . . . . . . . . . . . . . .395

26083 . . . . . . . . . .395,39626084 . . . . . . . . . .395,39626085 . . . . . . . . . . . . . .39226086 . . . . . . . . . . . . . .39226087 . . . . . . . . . . . . . .39326088 . . . . . . . . . . . . . .39326091 . . . . . . . . . . . . . .39326092 . . . . . . . . . . . . . .39326093 . . . . . . . . . . . . . .39426096 . . . . . . . . . . . . . .40026097 . . . . . . . . . . . . . .40026098 . . . . . . . . . . . . . .40026099 . . . . . . . . . . . . . .40026100 . . . . . . . . . . . . . .40026101 . . . . . . . . . . . . . .40026110 . . . . . . . . . . . . . .40026111 . . . . . . . . . . . . . .40026112 . . . . . . . . . . . . . .40026113 . . . . . . . . . . . . . .40026114 . . . . . . . . . . . . . .40026115 . . . . . . . . . . . . . .40026116 . . . . . . . . . . . . . .40026117 . . . . . . . . . . . . . .40026118 . . . . . . . . . . . . . .40026119 . . . . . . . . . . . . . .40026120 . . . . . . . . . . . . . .40026121 . . . . . . . . . .364,40026122 . . . . . . . . . .364,40026123 . . . . . . . . . . . . . .38926124 . . . . . . . . . . . . . .38926125 . . . . . . . . . . . . . .38926126 . . . . . . . . . . . . . .38926127 . . . . . . . . . . . . . .39326128 . . . . . . . . . . . . . .39326129 . . . . . . . . . . . . . .39326130 . . . . . . . . . .395,39626131 . . . . . . . . . .395,39626132 . . . . . . . . . . . . . .40126133 . . . . . . . . . . . . . .40126134 . . . . . . . . . . . . . .40126135 . . . . . . . . . . . . . .39826136 . . . . . . . . . . . . . .39826137 . . . . . . . . . . . . . .39826138 . . . . . . . . . . . . . .27126139 . . . . . . . . . . . . . .27126140 . . . . . . . . . . . . . .27126141 . . . . . . . . . . . . . .27126142 . . . . . . . . . . . . . .39926143 . . . . . . . . . . . . . .39926144 . . . . . . . . . . . . . .39926145 . . . . . . . . . . . . . .39926146 . . . . . . . . . . . . . .39926147 . . . . . . . . . . . . . .39926148 . . . . . . . . . . . . . .39926149 . . . . . . . . . . . . . .39926150 . . . . . . . . . . . . . .39926151 . . . . . . . . . . . . . .39926152 . . . . . . . . . . . . . .39926153 . . . . . . . . . . . . . .39926155 . . . . . . . . . . . . . .39926156 . . . . . . . . . . . . . .39926157 . . . . . . . . . . . . . .39926158 . . . . . . . . . . . . . .39926159 . . . . . . . . . . . . . .40226160 . . . . . . . . . . . . . .40226161 . . . . . . . . . . . . . .40226162 . . . . . . . . . . . . . .40226166 . . . . . . . . . . . . . .40026167 . . . . . . . . . . . . . .40126168 . . . . . . . . . . . . . .40126169 . . . . . . . . . . . . . .40126170 . . . . . . . . . . . . . .40126171 . . . . . . . . . . . . . .40126172 . . . . . . . . . . . . . .40126173 . . . . . . . . . . . . . .40126174 . . . . . . . . . . . . . .40126175 . . . . . . . . . . . . . .40126176 . . . . . . . . . . . . . .40126177 . . . . . . . . . . . . . .40126178 . . . . . . . . . . . . . .40126179 . . . . . . . . . . . . . .40126180 . . . . . . . . . . . . . .400


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INDEX

Catalog #26181 . . . . . . . . . . . . . .40326182 . . . . . . . . . . . . . .40326183 . . . . . . . . . . . . . .40326184 . . . . . . . . . . . . . .40026185 . . . . . . . . . . . . . .40326187 . . . . . . . . . .400,40126188 . . . . . . . . . .400,40126189 . . . . . . . . . . . . . .40126190 . . . . . . . . . . . . . .40026191 . . . . . . . . . . . . . .40126193 . . . . . . . . . . . . . .39326194 . . . . . . . . . . . . . .39326195 . . . . . . . . . . . . . .39326204 . . . . . . . . . . . . . .39826205 . . . . . . . . . . . . . .39226206 . . . . . . . . . . . . . .39326207 . . . . . . . . . . . . . .39226208 . . . . . . . . . . . . . .39426209 . . . . . . . . . . . . . .41526210 . . . . . . . . . . . . . .41526211 . . . . . . . . . . . . . .41526212 . . . . . . . . . . . . . .41526215 . . . . . . . . . . . . . .38926216 . . . . . . . . . . . . . .38926217 . . . . . . . . . . . . . .38926218 . . . . . . . . . . . . . .38926219 . . . . . . . . . . . . . .38926220 . . . . . . . . . . . . . .38926221 . . . . . . . . . . . . . .38926222 . . . . . . . . . . . . . .38926223 . . . . . . . . . . . . . .38926224 . . . . . . . . . . . . . .38926225 . . . . . . . . . . . . . .38926226 . . . . . . . . . . . . . .38926228 . . . . . . . . . . . . . .39226229 . . . . . . . . . . . . . .40026230 . . . . . . . . . . . . . .39026231 . . . . . . . . . . . . . .39026232 . . . . . . . . . . . . . .39026233 . . . . . . . . . . . . . .39026234 . . . . . . . . . . . . . .39026235 . . . . . . . . . . . . . .38926236 . . . . . . . . . . . . . .38926237 . . . . . . . . . . . . . .38926238 . . . . . . . . . . . . . .38926239 . . . . . . . . . . . . . .38926246 . . . . . . . . . . . . . .40226247 . . . . . . . . . . . . . .40226248 . . . . . . . . . . . . . .40226249 . . . . . . . . . . . . . .39026250 . . . . . . . . . . . . . .39626251 . . . . . . . . . . . . . .40226252 . . . . . . . . . . . . . .42026253 . . . . . . . . . . . . . .42026254 . . . . . . . . . . . . . .42026255 . . . . . . . . . . . . . .42026256 . . . . . . . . . . . . . .42026257 . . . . . . . . . . . . . .42026258 . . . . . . . . . . . . . .42026259 . . . . . . . . . . . . . .42026260 . . . . . . . . . . . . . .40126261 . . . . . . . . . .215,231,

248,279,36726262 . . . . . . . . . .215,231,

248,279,36726263 . . . . . . . . . . . . . .41626264 . . . . . . . . . . . . . .41626265 . . . . . . . . . . . . . .41626266 . . . . . . . . . . . . . .41626267 . . . . . . . . . . . . . .41626268 . . . . . . . . . . . . . .41626269 . . . . . . . . . . . . . .41626270 . . . . . . . . . . . . . .41626271 . . . . . . . . . . . . . .41626272 . . . . . . . . . . . . . .41626273 . . . . . . . . . . . . . .41626274 . . . . . . . . . . . . . .41626275 . . . . . . . . . . . . . .41626276 . . . . . . . . . . . . . .41626277 . . . . . . . . . . . . . .41626278 . . . . . . . . . . . . . .41626279 . . . . . . . . . . . . . .416

26280 . . . . . . . . . . . . . .41626281 . . . . . . . . . . . . . .41626282 . . . . . . . . . . . . . .41626283 . . . . . . . . . . . . . .41626284 . . . . . . . . . . . . . .41626285 . . . . . . . . . . . . . .41626286 . . . . . . . . . . . . . .41626287 . . . . . . . . . . . . . .41626288 . . . . . . . . . . . . . .41626289 . . . . . . . . . . . . . .41626290 . . . . . . . . . . . . . .41626291 . . . . . . . . . . . . . .41626292 . . . . . . . . . . . . . .41626293 . . . . . . . . . . . . . .41626294 . . . . . . . . . . . . . .41626295 . . . . . . . . . . . . . .41626296 . . . . . . . . . . . . . .41626297 . . . . . . . . . . . . . .43626298 . . . . . . . . . . . . . .43626299 . . . . . . . . . . . . . .43626300 . . . . . . . . . . . . . .43626301 . . . . . . . . . . . . . .43626302 . . . . . . . . . . . . . .43626303 . . . . . . . . . . . . . .43626304 . . . . . . . . . . . . . .43626305 . . . . . . . . . . . . . .43626306 . . . . . . . . . . . . . .43626307 . . . . . . . . . . . . . .43626308 . . . . . . . . . . . . . .43626309 . . . . . . . . . . . . . .43626310 . . . . . . . . . . . . . .43626311 . . . . . . . . . . . . . .43626312 . . . . . . . . . . . . . .43626313 . . . . . . . . . . . . . .43626314 . . . . . . . . . . . . . .43626315 . . . . . . . . . . . . . .43626316 . . . . . . . . . . . . . .43626317 . . . . . . . . . . . . . .43626318 . . . . . . . . . . . . . .43626319 . . . . . . . . . . . . . .43626320 . . . . . . . . . . . . . .43626322 . . . . . . . . . . . . . .43626323 . . . . . . . . . . . . . .43626324 . . . . . . . . . . . . . .43626326 . . . . . . . . . . . . . .43626327 . . . . . . . . . . . . . .43626393 . . . . . . . . . . . . . .32726394 . . . . . . . . . . . . . .33626395 . . . . . . . . . . . . . .33926396 . . . . . . . . . .339,34326397 . . . . . . . . . .339,34326398 . . . . . . . . . .339,34326399 . . . . . . . . . .339,34326400 . . . . . . . . . . . . . .34526401 . . . . . . . . . . . . . .34526402 . . . . . . . . . . . . . .34526403 . . . . . . . . . . . . . .34526404 . . . . . . . . . . . . . .34526405 . . . . . . . . . . . . . .34526406 . . . . . . . . . . . . . .34526407 . . . . . . . . . . . . . .34526408 . . . . . . . . . . . . . .35126409 . . . . . . . . . . . . . .34426410 . . . . . . . . . . . . . .34426411 . . . . . . . . . . . . . .34426412 . . . . . . . . . . . . . .34426413 . . . . . . . . . . . . . .34426414 . . . . . . . . . . . . . .34426415 . . . . . . . . . . . . . .34426416 . . . . . . . . . . . . . .34426417 . . . . . . . . . . . . . .34526418 . . . . . . . . . . . . . .34526419 . . . . . . . . . . . . . .34526420 . . . . . . . . . . . . . .34526421 . . . . . . . . . . . . . .34526422 . . . . . . . . . . . . . .34526423 . . . . . . . . . . . . . .32726424 . . . . . . . . . . . . . .32726425 . . . . . . . . . . . . . .32826426 . . . . . . . . . . . . . .32926427 . . . . . . . . . . . . . .32926428 . . . . . . . . . . . . . .331

26429 . . . . . . . . . . . . . .33126430 . . . . . . . . . . . . . .33126510 . . . . . . . . . . . . . .33526511 . . . . . . . . . . . . . .33526512 . . . . . . . . . . . . . .33526513 . . . . . . . . . . . . . .33526514 . . . . . . . . . . . . . .33526515 . . . . . . . . . . . . . .33526516 . . . . . . . . . . . . . .34326517 . . . . . . . . . . . . . .34326518 . . . . . . . . . . . . . .34326519 . . . . . . . . . . . . . .33126520 . . . . . . . . . . . . . .32726521 . . . . . . . . . . . . . .32926525 . . . . . . . . . . . . . .32726526 . . . . . . . . . . . . . .32726527 . . . . . . . . . . . . . .32726528 . . . . . . . . . . . . . .32726529 . . . . . . . . . . . . . .32726530 . . . . . . . . . . . . . .32726531 . . . . . . . . . . . . . .32726532 . . . . . . . . . . . . . .32726533 . . . . . . . . . . . . . .32726534 . . . . . . . . . . . . . .32726535 . . . . . . . . . . . . . .32726536 . . . . . . . . . . . . . .32726537 . . . . . . . . . . . . . .32726538 . . . . . . . . . . . . . .33926539 . . . . . . . . . . . . . .33926540 . . . . . . . . . . . . . .33926541 . . . . . . . . . . . . . .33926542 . . . . . . . . . . . . . .33926543 . . . . . . . . . . . . . .33826544 . . . . . . . . . . . . . .33826545 . . . . . . . . . . . . . .33826546 . . . . . . . . . . . . . .35126547 . . . . . . . . . . . . . .33126548 . . . . . . . . . . . . . .33626549 . . . . . . . . . . . . . .34026550 . . . . . . . . . . . . . .33826551 . . . . . . . . . . . . . .33827100 . . . . . . . . . .205,21927101 . . . . . . . . . .205,21927102 . . . . . . . . . . . . . .20527103 . . . . . . . . . . . . . .20527104 . . . . . . .205,255,26227105 . . . . . . .205,255,26227106 . . .205,219,255,26227107 . . .205,219,255,26227108 . . . . . . .205,219,26227109 . . . . . . .205,219,26227110 . . .205,219,247,26227111 . . .205,219,247,26227112 . . . . . . . . . . . . . .20527113 . . . . . . . . . . . . . .20527114 . . . . . . . . . . . . . .20527115 . . . . . . . . . . . . . .20527116 . . . . . . . . . .205,25527117 . . . . . . . . . .205,25527118 . . . . . . . . . .205,25127119 . . . . . . . . . .205,25127120 . . . . . . . . . .205,21927121 . . . . . . . . . .205,21927122 . . . . . . . . . .205,21927123 . . . . . . . . . . . . . .20527124 . . . . . . . . . . . . . .20527125 . . . . . . . . . . . . . .20527126 . . . . . . . . . . . . . .20527127 . . . . . . . . . . . . . .20527128 . . . . . . . . . . . . . .20527129 . . . . . . . . . . . . . .20527130 . . . . . . . . . . . . . .20527131 . . . . . . . . . . . . . .20527132 . . . . . . . . . .205,26227133 . . . . . . . . . .205,26227134 . . . . . . . . . .205,26227135 . . . . . . .205,219,26227136 . . . . . . .205,219,26227137 . . . . . . .205,219,26227138 . . . . . . .205,219,26227139 . . . . . . .205,219,26227140 . . . . . . .205,219,262

27141 . . .205,219,247,26227142 . . .205,219,247,26227143 . . .205,219,247,26227144 . . . . . . . . . . . . . .20527145 . . . . . . . . . . . . . .20527146 . . . . . . . . . . . . . .20527147 . . . . . . . . . . . . . .20527148 . . . . . . . . . . . . . .20527149 . . . . . . . . . . . . . .20527150 . . . . . . . . . . . . . .20527151 . . . . . . . . . . . . . .20527152 . . . . . . . . . . . . . .20527153 . . . . . . . . . .205,25127154 . . . . . . . . . .205,25127155 . . . . . . . . . .205,25127156 . . . . . . . . . .205,26227157 . . . . . . . . . .205,26227158 . . . . . . .205,219,26227159 . . . . . . .205,219,26227160 . . . . . . .205,219,26227161 . . . . . . .205,219,26227162 . . .205,219,247,26227163 . . .205,219,247,26227164 . . . . . . . . . . . . . .20527165 . . . . . . . . . . . . . .20527166 . . . . . . . . . . . . . .20527167 . . . . . . . . . . . . . .20527168 . . . . . . . . . . . . . .20527169 . . . . . . . . . . . . . .20527170 . . . . . . . . . .205,25127171 . . . . . . . . . .205,25127184 . . . . . . . . . . . . . .22827185 . . . . . . . . . .233,26927190 . . . . . . . . . . . . . .24127191 . . . . . . . . . . . . . .24127192 . . . . . . . . . . . . . .24127193 . . . . . . . . . . . . . .24127194 . . . . . . . . . . . . . .23727195 . . . . . . . . . . . . . .23727196 . . . . . . . . . . . . . .23727197 . . . . . . . . . . . . . .33827198 . . . . . . . . . . . . . .33830001 . . . . . . . . . . . . . .48630002 . . . . . . . . . . . . . .48630003 . . . . . . .443,469,48630004 . . . . . . . . . . . . . .48630005 . . . . . . . . . . . . . .48630006 . . . . . . .476,478,48730007 . . . . . . . . . . . . . .48730008 . . . . . . . . . . . . . .48730009 . . . . . . . . . . . . . .48730010 . . . . . . . . . . . . . .48730011 . . . . . . . . . . . . . .48630020 . . . . . . . . . . . . . .46630021 . . . . . . . . . . . . . .46630022 . . . . . . . . . . . . . .46630023 . . . . . . . . . .466,47130024 . . . . . . . . . . . . . .47030025 . . . . . . . . . .443,46730026 . . .443,467,471,50530027 . . . . . . . . . .445,46730028 . . . . . . . . . .445,46730029 . . . . . . . . . .445,46730030 . . . . . . .446,467,47130031 . . . . . . . . . .447,46730032 . . . . . . .445,467,47130035 . . . . . . . . . . . . . .46430036 . . . . . . . . . . . . . .45130037 . . . . . . . . . . . . . .45130038 . . . . . . . . . . . . . .45130040 . . . . . . .444,452,46730041 . . . . . . . . . .452,47230042 . . . . . .452,457,471,

476,477,48730043 . . . . . . . . . . . . . .45230044 . . . . . . . . . . . . . .45330045 . . . . . . . . . . . . . .45330046 . . . . . . . . . . . . . .45330047 . . . . . . . . . . . . . .45330048 . . . . . . . . . .448,467,

471,505,51130049 . . . . . . . . . .445,467

30051 . . . . . . .471,476,50330055 . . . . . . . . . . . . . .46730056 . . . . . . . . . . . . . .47130057 . . . . . . . . . . . . . .47130062 . . . . . . . . . . . . . .47130065 . . . . . . . . . . . . . .50330066 . . . . . . .444,504,50530067 . . . . . . .443,477,50430068 . . . . . . .448,504,51130069 . . . . . . . . . . . . . .50330073 . . . . . . . . . . . . . .47730074 . . . . . . . . . . . . . .47730075 . . . . . . . . . . . . . .47730076 . . . . . . . . . . . . . .47830080 . . . . . . . . . . . . . .47030081 . . . . . . .448,501,50530082 . . . . . . .443,477,50430083 . . . . . . .448,504,51130084 . . . . . . .444,504,51130086 . . . . . . . . . . . . . .47230089 . . . . . . . . . . . . . .44830090 . . . . . . . . . . . . . .48830091 . . . . . . . . . . . . . .48630092 . . . . . . . . . . . . . .48630093 . . . . . . . . . .448,48630094 . . . . . . . . . .443,50230095 . . . . . . . . . .503,51230096 . . . . . . .448,502,52330097 . . . . . . . . . .448,52330098 . . . . . . . . . .448,52330099 . . . . . . . . . .448,52330100 . . . . . . . . . . . . . .52330201 . . . . . . . . . . . . . .45630202 . . . . . . . . . . . . . .45730203 . . . . . . . . . . . . . .45730204 . . . . . . . . . . . . . .45730205 . . . . . . .448,501,50530206 . . . . . . .448,501,50530207 . . . . . . . . . .443,50230208 . . . . . . . . . .443,50230209 . . . . . . . . . . . . . .45130210 . . . . . . . . . . . . . .45130211 . . . . . . . . . . . . . .45130212 . . . . . . . . . .464,47630213 . . . . . . .471,476,50330214 . . . . . . . . . . . . . .47630215 . . . . . . . . . . . . . .47630216 . . . . . . .448,478,48730217 . . . . . . . . . . . . . .47630218 . . . . . . . . . . . . . .47630219 . . . . . . . . . . . . . .45130220 . . . . . . . . . . . . . .45130221 . . . . . . . . . . . . . .45130222 . . . . . . . . . . . . . .47130223 . . . . . . . . . .444,46730224 . . . . . . . . . .448,46730225 . . . . . . . . . .443,46730226 . . . . . . . . . .443,46730227 . . . . . . . . . .445,46730228 . . . . . . . . . .443,46730230 . . . . . . . . . .443,46730231 . . . . . . . . . .503,50730235 . . . . . . . . . . . . . .45130236 . . . . . . . . . . . . . .50730237 . . . . . . . . . . . . . .50430238 . . . . . . . . . .444,47830239 . . . . . . . . . . . . . .45330240 . . . . . . . . . . . . . .47730241 . . . . . . . . . . . . . .47730242 . . . . . . . . . . . . . .47830243 . . . . . . . . . . . . . .46630244 . . . . . . . . . . . . . .46730245 . . . . . . . . . . . . . .44330246 . . . . . . . . . .443,46430248 . . . . . . . . . . . . . .44330249 . . . . . . . . . . . . . .44330250 . . . . . . . . . . . . . .44330251 . . . . . . . . . . . . . .44330252 . . . . . . . . . . . . . .44330253 . . . . . . . . . . . . . .44330254 . . . . . . . . . . . . . .44330258 . . . . . . . . . . . . . .444

30259 . . . . . . . . . . . . . .44430261 . . . . . . . . . . . . . .44430263 . . . . . . . . . . . . . .44430264 . . . . . . . . . . . . . .44430265 . . . . . . . . . .444,47730266 . . . . . . . . . . . . . .44430267 . . . . . . . . . . . . . .44430270 . . . . . . . . . . . . . .44430271 . . . . . . . . . . . . . .44430272 . . . . . . . . . . . . . .44430274 . . . . . . . . . . . . . .44530275 . . . . . . . . . . . . . .44530276 . . . . . . . . . . . . . .44530277 . . . . . . . . . . . . . .44530278 . . . . . . . . . . . . . .44530279 . . . . . . . . . . . . . .44530280 . . . . . . . . . . . . . .44530281 . . . . . . . . . . . . . .44530283 . . . . . . . . . . . . . .44530284 . . . . . . . . . . . . . .44530285 . . . . . . . . . . . . . .44530286 . . . . . . . . . . . . . .44530287 . . . . . . . . . . . . . .44530288 . . . . . . .445,478,50730289 . . . . . . . . . . . . . .44530290 . . . . . . . . . . . . . .44530292 . . . . . . . . . . . . . .44630293 . . . . . . . . . . . . . .44630294 . . . . . . . . . . . . . .44630297 . . . . . . . . . . . . . .44630299 . . . . . . . . . . . . . .44730300 . . . . . . . . . . . . . .45730304 . . . . . . . . . . . . . .45730310 . . . . . . . . . . . . . .48930400 . . . . . . . . . . . . . .44730401 . . . . . . . . . . . . . .44730402 . . . . . . . . . .446,47830403 . . . . . . . . . . . . . .44730404 . . . . . . . . . . . . . .44730407 . . . . . . . . . . . . . .44730409 . . . . . . . . . . . . . .44730410 . . . . . . . . . . . . . .44830411 . . . . . . . . . . . . . .44830412 . . . . . . . . . . . . . .44830413 . . . . . . . . . . . . . .44830414 . . . . . . . . . . . . . .44830415 . . . . . . . . . . . . . .44830416 . . . . . . . . . . . . . .44830418 . . . . . . . . . . . . . .44830419 . . . . . . . . . . . . . .44830420 . . . . . . . . . . . . . .44830421 . . . . . . . . . . . . . .44830422 . . . . . . . . . . . . . .44830423 . . . . . . . . . . . . . .44830424 . . . . . . . . . . . . . .44830425 . . . . . . . . . . . . . .44830426 . . . . . . . . . . . . . .44830427 . . . . . . . . . . . . . .47730429 . . . . . . . . . . . . . .44830430 . . . . . . . . . . . . . .44430431 . . . . . . . . . . . . . .45230432 . . . . . . . . . . . . . .45230433 . . . . . . . . . . . . . .51130434 . . . . . . . . . . . . . .50830435 . . . . . . . . . .444,50830436 . . . . . . . . . .448,52330437 . . . . . . . . . . . . . .52330438 . . . . . . . . . . . . . .48730439 . . . . . .452,457,471,

476,477,48730442 . . . . . . . . . . . . . .48730444 . . . . . . . . . . . . . .45330445 . . . . . . . . . . . . . .45330446 . . . . . . . . . . . . . .45330447 . . . . . . . . . . . . . .45730450 . . . . . . . . . . . . . .51230451 . . . . . . . . . . . . . .51230452 . . . . . . . . . . . . . .50830453 . . . . . . . . . .444,50830454 . . . . . . . . . . . . . .50830456 . . . . . . . . . . . . . .48730457 . . . . . . . . . . . . . .486


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INDEX

Catalog #30460 . . . . . . . . . . . . . .48730461 . . . . . . . . . . . . . .50530462 . . . . . . . . . . . . . .44830463 . . . . . . . . . .452,47230464 . . . . . . . . . .452,47230465 . . . . . . . . . .478,50730466 . . . . . . .445,478,50730467 . . . . . . .446,478,50730468 . . . . . . . . . . . . . .50930469 . . . . . . . . . . . . . .44330470 . . . . . . . . . .443,47830471 . . . . . . .476,507,51030472 . . . . . . . . . .446,50230473 . . . . . . . . . . . . . .44730474 . . . . . . . . . . . . . .44330475 . . . . . . . . . . . . . .47730476 . . . . . . . . . .445,47830477 . . . . . . . . . . . . . .47830479 . . . . . . . . . . . . . .47730482 . . . . . .447,456,469,

477,479,486,48930483 . . . . . . . . . . . . . .50130484 . . . . . . . . . .456,46630485 . . . . . . . . . . . . . .50430486 . . . . . . .504,509,51130487 . . . . . . .448,503,52330488 . . . . . . .471,476,50330489 . . . . . . . . . . . . . .47830492 . . . . . . . . . . . . . .48830494 . . . . . . . . . . . . . .44330495 . . . . . . . . . . . . . .44330496 . . . . . . . . . . . . . .50730497 . . . . . . . . . . . . . .46630498 . . . . . . . . . . . . . .44530540 . . . . . . . . . . . . . .51030541 . . . . . . . . . . . . . .51030542 . . . . . . . . . . . . . .51030543 . . . . . . . . . . . . . .51030544 . . . . . . . . . . . . . .51030545 . . . . . . . . . . . . . .51030600 . . . . . . . . . . . . . .46430601 . . . . . . . . . . . . . .45730602 . . . . . . . . . . . . . .45730603 . . . . . . . . . .452,45630604 . . . . . . . . . . . . . .50830605 . . . . . . . . . . . . . .50830607 . . . . . . . . . . . . . .45630608 . . . . . . . . . .463,49930609 . . . . . . . . . .444,46230611 . . . . . . . . . . . . . .49830612 . . . . . . . . . .448,49830613 . . . . . . . . . .446,49930614 . . . . . . . . . .445,47730615 . . . . . . . . . . . . . .46230616 . . . . . . . . . . . . . .46230617 . . . . . . . . . .443,47830618 . . . . . . . . . .443,47830619 . . . . . . . . . . . . . .45730621 . . . . . . . . . . . . . .44330622 . . . . . . . . . . . . . .44330624 . . . . . . . . . . . . . .48630625 . . . . . . . . . . . . . .48630626 . . . . . . . . . . . . . .47830627 . . . . . . . . . .445,47830628 . . . . . . . . . .445,47830629 . . . . . . . . . .443,47830630 . . . . . . . . . . . . . .48630631 . . . . . . . . . .443,47830632 . . . . . . . . . . . . . .48730633 . . . . . . . . . . . . . .47730634 . . . . . . . . . . . . . .44430645 . . . . . . .443,464,47830646 . . . . . . .443,464,47830671 . . . . . . . . . .448,51530672 . . . . . . . . . . . . . .51530673 . . . . . . . . . . . . . .51530674 . . . . . . . . . . . . . .51530709 . . . . . . . . . . . . . .51730712 . . . . . . . . . . . . . .51730713 . . . . . . . . . . . . . .51730714 . . . . . . . . . . . . . .51730715 . . . . . . . . . . . . . .517

30716 . . . . . . . . . . . . . .51730717 . . . . . . . . . . . . . .51730718 . . . . . . . . . . . . . .51730719 . . . . . . . . . . . . . .51730720 . . . . . . . . . . . . . .51730721 . . . . . . . . . . . . . .51730722 . . . . . . . . . . . . . .51730723 . . . . . . . . . . . . . .51730724 . . . . . . . . . . . . . .51731001 . . .444,469,479,48931002 . . . . . . . . . . . . . .48931003 . . . . . . . . . . . . . .48831004 . . . . . . . . . .479,48931004.15 . . . . . . . .479,48931004.25 . . . . . . . .479,48931005 . . . . . . . . . . . . . .48931006 . . . . . . .468,479,48831006.15 . . . .468,479,48831006.25 . . . .468,479,48831007 . . . . . . . . . . . . . .49131008 . . . . . . . . . . . . . .49131009 . . . . . . . . . . . . . .49131010 . . . . . . . . . . . . . .49131011 . . . . . . .465,474,49131012 . . . . . . . . . . . . . .49131013 . . . . . . . . . . . . . .49131014 . . . . . . . . . . . . . .47931014.15 . . . . . . . . . . .47931014.25 . . . . . . . . . . .47931024 . . . . . . . . . .479,48931024.15 . . . . . . . .479,48931024.25 . . . . . . . .479,48931025 . . . . . . . . . .479,48831025.15 . . . . . . . .479,48831025.25 . . . . . . . .479,48831026 . . . . . . . . . .445,49131027 . . . . . . . . . . . . . .47031028 . . . . . . . . . . . . . .47031029 . . . . . . . . . . . . . .46431030 . . . . . . .464,480,49131031 . . . . . . . . . . . . . .46431032 . . . . . . . . . . . . . .46531033 . . . . . . . . . . . . . .46531034 . . . . . . . . . . . . . .46531035 . . . . . . . . . . . . . .46531036 . . . . . . . . . . . . . .46831037 . . . . . . . . . .443,46831039 . . . . . . . . . .444,46831040 . . .444,455,468,47531041 . . . . . . . . . .444,46831043 . . . . . . .447,468,50931044 . . . . . . .447,460,46831045 . . . . . . . . . .447,46831046 . . . . . . . . . .447,46831047 . . . . . . . . . .446,46831048 . . . . . . . . . .447,46831049 . . . . . . . . . .447,46831061 . . . . . . . . . . . . . .47931061.15 . . . . . . . . . . .47931061.25 . . . . . . . . . . .47931062 . . . . . . . . . .479,48931062.15 . . . . . . . .479,48931062.25 . . . . . . . .479,48931063 . . . . . . . . . .479,48831063.15 . . . . . . . .479,48831063.25 . . . . . . . .479,48831064 . . . . . . . . . . . . . .51231065 . . .443,504,506,50931066 . . .448,504,506,50731071 . . . . . . . . . . . . . .47931071.15 . . . . . . . . . . .47931071.25 . . . . . . . . . . .47931072 . . . . . . . . . . . . . .48931073 . . . . . . . . . . . . . .48831074 . . . . . . . . . .479,48931074.15 . . . . . . . .479,48931074.25 . . . . . . . .479,48931075 . . . . . . . . . . . . . .48931082 . . . . . . . . . . . . . .48931083 . . . . . . . . . . . . . .48831084 . . . . . . . . . .479,48931084.15 . . . . . . . .479,489

31084.25 . . . . . . . .479,48931085 . . . . . . . . . . . . . .48931086 . . . . . . . . . .479,48931086.15 . . . . . . . .479,48931086.25 . . . . . . . .479,48931087 . . . . . . . . . .479,48831087.15 . . . . . . . .479,48831087.25 . . . . . . . .479,48831088 . . . . . . . . . . . . . .47231089 . . . . . . . . . . . . . .47231090 . . . . . . . . . . . . . .47231091 . . . . . . . . . .446,46831092 . . . . . . . . . .446,46831093 . . . . . . .445,501,50631094 . . . . . . .446,501,50631095 . . . . . . .448,504,51031096 . . . . . . .446,504,51031097 . . . . . . . . . .448,504,

506,507,51031098 . . .444,504,509,51131200 . . . . . . . . . . . . . .50131206 . . . . . . .468,479,48831206.15 . . . .468,479,48831206.25 . . . .468,479,48831208 . . . . . . . . . . . . . .49231209 . . . . . . . . . . . . . .49231210 . . . . . . . . . . . . . .49231211 . . . . . . .444,489,49231212 . . . . . . . . . . . . . .48931214 . . . . . . .506,509,51131215 . . . . . . . . . .446,50231216 . . . . . . . . . .446,50231217 . . . . . . . . . .446,50231218 . . . . . . .446,502,50631219 . . . . . . . . . .446,50231220 . . . . . . . . . .446,50231222 . . . . . . . . . . . . . .51531223 . . . . . . . . . . . . . .51531224 . . . . . . . . . .513,52331225 . . . . . . .447,503,52331226 . . . . . . . . . .447,52331227 . . . . . . . . . .447,52331228 . . . . . . . . . .447,52331229 . . . . . . .446,502,52331230 . . . . . . . . . .446,52331231 . . . . . . . . . .446,52331232 . . . . . . . . . .446,52331233 . . . . . . .445,502,52331234 . . . . . . . . . .445,52331235 . . . . . . . . . .445,52331236 . . . . . . . . . .445,52331237 . . . . . . . . . . . . . .52331238 . . . . . . . . . . . . . .52331239 . . . . . . . . . . . . . .52331240 . . . . . . . . . . . . . .50331241 . . . . . . . . . . . . . .48931242 . . . . . . . . . .446,50231243 . . . . . . . . . .446,50231244 . . . . . . . . . .446,50231246 . . . . . . . . . .446,50231248 . . . . . . .446,502,50631249 . . . . . . .446,502,50631250 . . . . . . . . . .446,50231252 . . . . . . . . . .446,50231253 . . . . . . . . . . . . . .50231254 . . . . . . . . . .446,50231256 . . . . . . .446,501,50631257 . . . . . . .446,501,50631258 . . . . . . .445,501,50631259 . . . . . . .445,501,50631260 . . . . . . .447,503,52331261 . . . . . . .447,503,52331262 . . . . . . . . . .446,50231264 . . . . . . . . . . . . . .46531266 . . . . . . . . . . . . . .50731267 . . . . . . . . . . . . . .44331268 . . . . . . . . . . . . . .44331269 . . . . . . . . . . . . . .44331270 . . . . . . . . . . . . . .44331271 . . . . . . . . . . . . . .44331272 . . . . . . . . . . . . . .44331273 . . . . . . . . . . . . . .443

31274 . . . . . . . . . . . . . .44331275 . . . . . . . . . . . . . .44431276 . . . . . . . . . . . . . .44431277 . . . . . . . . . . . . . .44631278 . . . . . . . . . . . . . .44631279 . . . . . . . . . . . . . .44631280 . . . . . . . . . . . . . .44731281 . . . . . . . . . . . . . .44731282 . . . . . . . . . . . . . .44731283 . . . . . . . . . . . . . .44731284 . . . . . . . . . . . . . .44431285 . . . . . . . . . . . . . .44731291 . . . . . . . . . . . . . .44531292 . . . . . . . . . . . . . .44631296 . . . . . . . . . . . . . .44731297 . . . . . . . . . . . . . .44731298 . . . . . . . . . . . . . .44731299 . . . . . . . . . . . . . .44831400 . . . . . . . . . . . . . .44831401 . . . . . . . . . .448,46831402 . . . . . . . . . . . . . .44831403 . . . . . . . . . . . . . .44731409 . . . . . . . . . . . . . .44531415 . . . . . . . . . .443,48131420 . . . . . . . . . . . . . .44331426 . . . . . . . . . . . . . .44531427 . . . . . . . . . . . . . .44731428 . . . . . . . . . . . . . .44731429 . . . . . . . . . . . . . .44731430 . . . . . . . . . . . . . .44431435 . . . . . . . . . . . . . .44631436 . . . . . . . . . . . . . .44631439 . . . . . . . . . . . . . .44831441 . . . . . . . . . . . . . .44331442 . . . . . . . . . . . . . .44531443 . . . . . . . . . . . . . .44531444 . . . . . . . . . . . . . .44531449 . . . . . . . . . . . . . .44331450 . . . . . . . . . . . . . .48431451 . . . . . . . . . . . . . .48431452 . . .445,473,484,52431453 . . .445,473,484,52431454 . . . . . . . . . . . . . .48531455 . . . . . . . . . . . . . .46531456 . . . . . . . . . .447,50731457 . . . . . . . . . . . . . .47031458 . . . . . . . . . . . . . .50831459 . . . . . . . . . . . . . .50831460 . . . . . . . . . . . . . .50831462 . . . . . . . . . . . . . .49131463 . . . . . . . . . . . . . .49131464 . . . . . . .447,501,50631465 . . . . . . . . . .448,50131469 . . . . . . . . . . . . . .51231470 . . . . . . . . . . . . . .44331472 . . . . . . . . . . . . . .49631473 . . . . . . . . . . . . . .49631474 . . . . . . . . . .448,49631475 . . . . . . . . . .448,49631476 . . . . . . . . . .448,49631477 . . . . . . . . . .448,49631478 . . . . . . . . . .448,49631479 . . . . . . . . . . . . . .50931480 . . . . . . . . . . . . . .50931481 . . . . . . . . . . . . . .50931482 . . . . . . . . . . . . . .51131483 . . . . . . . . . . . . . .51131484 . . . . . . . . . . . . . .51131485 . . . . . . . . . . . . . .51031486 . . . . . . . . . . . . . .51031487 . . . . . . . . . .447,51031488 . . . . . . . . . . . . . .51231489 . . . . . . . . . . . . . .51231490 . . . . . . . . . . . . . .51231491 . . . . . . . . . . . . . .51231492 . . . . . . . . . . . . . .48931493 . . . . . . . . . . . . . .48931494 . . . . . . . . . . . . . .49031496 . . . . . . . . . . . . . .44331497 . . . . . . . . . . . . . .44531498 . . .447,474,485,52431499 . . .447,474,485,524

31600 . . .447,474,485,52431601 . . .445,474,485,52431602 . . .447,474,485,52431607 . . . . . . . . . . . . . .47331608 . . . . . . . . . . . . . .47331609 . . . . . . . . . . . . . .47331610 . . . . . . . . . . . . . .47331612 . . .447,474,485,52431613 . . . . . . . . . .513,52331614 . . . . . . . . . . . . . .50731615 . . . . . . . . . .469,47931616 . . . . . . . . . . . . . .48031617 . . . . . . . . . . . . . .48031618 . . . . . . . . . . . . . .48131619 . . . . . . . . . . . . . .48131620 . . . . . . . . . . . . . .48131621 . . . . . . . . . . . . . .48231622 . . . . . . . . . . . . . .48231623 . . . . . . . . . . . . . .48231624 . . . . . . . . . .443,48231625 . . . . . . . . . . . . . .48131626 . . . . . . . . . . . . . .48231627 . . . . . . . . . . . . . .48231628 . . . . . . . . . .529,53631629 . . . . . . .448,529,53631630 . . . . . . . . . . . . . .50031631 . . . . . . . . . . . . . .50031636 . . . . . . . . . .448,50031637 . . . . . . . . . . . . . .50131638 . . . . . . . . . . . . . .50631639 . . . . . . . . . . . . . .51131641 . . . . . . . . . . . . . .50031644 . . . . . . . . . . . . . .46231645 . . . . . . . . . . . . . .46231646 . . . . . . . . . . . . . .46331647 . . . . . . . . . . . . . .46331648 . . . . . . . . . .448,46331649 . . . . . . .445,463,47531650 . . . . . . . . . .445,46331651 . . . . . . . . . .445,46331652 . . . . . . .445,463,47531653 . . . . . . . . . .443,46331654 . . . . . . . . . . . . . .44631655 . . . . . . . . . .444,46331656 . . . . . . . . . .446,46331657 . . .447,474,485,52431658 . . .447,474,485,52431659 . . .447,474,485,52431660 . . .447,474,485,52431661 . . .445,474,485,52431662 . . .445,474,485,52431663 . . .445,474,485,52431664 . . .445,474,485,52431665 . . .446,474,485,52431666 . . .448,474,485,52431667 . . .448,474,485,52431668 . . .448,474,485,52431669 . . .448,474,485,52431670 . . .443,474,485,52431671 . . .443,474,485,52431672 . . . . . . . . . . . . . .44731673 . . . . . . . . . . . . . .50431674 . . . . . . . . . . . . . .51531675 . . . . . . . . . . . . . .51531676 . . . . . . . . . . . . . .50031677 . . . . . . . . . . . . . .50031678 . . . . . . . . . . . . . .50031679 . . . . . . . . . . . . . .50031680 . . . . . . . . . . . . . .50031681 . . . . . . . . . .448,50031682 . . . . . . . . . . . . . .50031684 . . . . . . . . . . . . . .49831685 . . . . . . . . . .447,49831687 . . . . . . . . . . . . . .48031687.15 . . . . . . . . . . .48031687.25 . . . . . . . . . . .48031688 . . . . . . . . . .480,49131689 . . . . . . . . . . . . . .48031691 . . . . . . . . . . . . . .45931692 . . . . . . . . . . . . . .45931693 . . . . . . . . . . . . . .45931694 . . . . . . . . . . . . . .460

31695 . . . . . . . . . . . . . .46031696 . . . . . . . . . . . . . .46031697 . . . . . . . . . . . . . .46031698 . . . . . . . . . .501,51131699 . . . . . . . . . .199,53931800 . . . . . . . . . . . . . .44431801 . . . . . . . . . . . . . .44431802 . . . . . . . . . . . . . .44431803 . . . . . . . . . . . . . .44431804 . . . . . . . . . . . . . .44431805 . . . . . . . . . .199,53931806 . . . . . . . . . . . . . .48131807 . . . . . . . . . . . . . .53131808 . . . . . . . . . . . . . .48331809 . . . . . . . . . .199,53931810 . . . . . . . . . . . . . .49231811 . . . . . . . . . .446,49231813 . . . . . . . . . . . . . .49231814 . . . . . . . . . . . . . .51131815 . . . . . . . . . . . . . .48131816 . . . . . . . . . .448,50631817 . . . . . . . . . . . . . .50631818 . . . . . . . . . . . . . .50631819 . . . . . . . . . .501,50531821 . . .447,474,485,52431822 . . .443,452,456,46831823 . . . . . . . . . .446,52431825 . . . . . . . . . .458,45931826 . . . . . . . . . .458,45931827 . . . . . . . . . . . . . .45931828 . . . . . . .448,459,46831829 . . . . . . . . . . . . . .46831830 . . . . . . . . . . . . . .50731831 . . . . . . . . . . . . . .50731832 . . . . . . . . . . . . . .50731833 . . . . . . . . . . . . . .44431834 . . .464,480,490,49131835 . . . . . . .445,491,49231836 . . . . . . . . . . . . . .44431837 . . . . . . . . . .446,48331838 . . . . . . . . . .444,50231839 . . . . . . . . . .446,50231840 . . . . . . . . . .445,53931841 . . . . . . . . . . . . . .48331842 . . . . . . . . . .444,48331843 . . . . . . . . . . . . . .48331844 . . . . . . . . . . . . . .45331845 . . . . . . . . . . . . . .45331846 . . . . . . . . . . . . . .47231847 . . . . . . . . . .443,47231848 . . . . . . . . . . . . . .47231850 . . . . . . . . . . . . . .48031852 . . . . . . . . . .480,49131853 . . . . . . . . . . . . . .44531854 . . . . . . . . . .443,46231855 . . . . . . .444,462,46831856 . . . . . . .444,455,47531857 . . . . . . . . . . . . . .47431858 . . . . . . . . . .444,50031859 . . . . . . . . . .448,50031860 . . . . . . . . . .448,50031864 . . . . . . . . . . . . . .49831865 . . . . . . . . . . . . . .49831866 . . . . . . . . . . . . . .49831867 . . . . . . . . . . . . . .49831868 . . . . . . . . . . . . . .49831870 . . . . . . .447,488,49831871 . . . . . . . . . . . . . .49931872 . . . . . . . . . . . . . .49931873 . . . . . . . . . . . . . .49931877 . . . . . . . . . .447,50731879 . . . . . . . . . .443,48131880 . . .445,502,504,51631881 . . . . . . . . . .443,46331882 . . . . . . . . . .443,46331885 . . . . . . . . . .479,48831885.15 . . . . . . . .479,48831885.25 . . . . . . . .479,48831886 . . . . . . . . . .479,48831886.15 . . . . . . . .479,48831886.25 . . . . . . . .479,48831887 . . . . . . . . . .479,488


772 www.restek.com

INDEX

Catalog #31887.15 . . . . . . . .479,48831887.25 . . . . . . . .479,48831888 . . . . . . . . . .479,48831888.15 . . . . . . . .479,48831888.25 . . . . . . . .479,48831889 . . . . . . . . . .479,48831889.15 . . . . . . . .479,48831889.25 . . . . . . . .479,48831890 . . .443,474,485,52431891 . . . . . . . . . . . . . .52831892 . . . . . . . . . . . . . .52831893 . . . . . . . . . . . . . .52831894 . . . . . . . . . . . . . .52831896 . . . . . . . . . . . . . .46231897 . . . . . . . . . . . . . .46231898 . . . . . . . . . . . . . .45631899 . . . . . . . . . . . . . .45831900 . . . . . . . . . . . . . .49031902 . . . . . . . . . . . . . .49031903 . . . . . . . . . . . . . .49031904 . . . . . . . . . . . . . .49031905 . . . . . . . . . . . . . .49032000 . . . . . . . . . .473,49332001 . . . . . . . . . . . . . .49332002 . . . . . . . . . . . . . .49332003 . . . . . . . . . . . . . .49532004 . . . . . . . . . . . . . .49532005 . . . . . . . . . .448,453,

454,469,49532006 . . .443,469,482,49532007 . . .443,469,482,49532008 . . .443,469,482,49532009 . . .443,469,482,49532010 . . .443,469,482,49532011 . . .443,469,482,49532012 . . .443,469,482,49532013 . . . . . . . . . . . . . .47032014 . . . . . . . . . . . . . .47032015 . . . . . .448,453,454,

469,470,49532016 . . .444,469,470,49532017 . . . . . . . . . .448,49332018 . . . . . . . . . . . . . .49432019 . . . . . . . . . . . . . .49232021 . . . . . . .444,469,49532022 . . . . . . . . . . . . . .46532023 . . . . . . . . . . . . . .49232024 . . . . . . . . . . . . . .45332025 . . . . . . . . . .444,49332027 . . . . . . . . . .448,49332028 . . . . . . . . . .448,49332029 . . . . . . .444,454,49332030 . . . . . . .444,454,49332031 . . . . . . . . . . . . . .49432032 . . . . . . . . . . . . . .49432033 . . . . . . . . . . . . . .49432034 . . . . . . . . . . . . . .49432039 . . . . . . .469,482,49532040 . . . . . . . . . . . . . .49432041 . . . . . . . . . . . . . .49232042 . . . . . . . . . . . . . .49232045 . . . . . . . . . . . . . .45432049 . . .445,455,466,47532050 . . .445,455,466,47532053 . . . . . . .444,455,47532054 . . . . . . .455,466,47532055 . . . . . . .455,466,47532056 . . . . . .444,455,463,

466,475,48432057 . . . . . . . . . .444,455,

463,466,47532058 . . . . . . . . . .466,47532059 . . . . . . . . . .466,47532060 . . . . . . . . . . . . . .46532061 . . . . . . . . . .455,47532062 . . . . . . . . . .455,47532063 . . . . . . . . . . . . . .45532064 . . .443,469,482,49532065 . . .443,469,482,49532066 . . .443,469,482,49532067 . . .443,469,482,49532068 . . .443,469,482,495

32069 . . .443,469,482,49532070 . . .443,469,482,49532071 . . . . . . . . . .448,453,

454,469,49532072 . . . . . . .444,469,49532073 . . . . . . . . . . . . . .49332074 . . . . . . . . . . . . . .49332075 . . . . . . . . . .443,469,

482,495,51632076 . . . . . . . . . .443,469,

482,495,51632077 . . . . . . . . . .443,469,

482,495,51632078 . . . . . . . . . .443,469,

482,495,51632079 . . . . . . . . . .443,469,

482,495,51632080 . . . . . . . . . .443,469,

482,495,51632081 . . . . . . . . . .443,469,

482,495,51632082 . . . . . . . . . .443,469,

482,495,51632083 . . . . . . . . . .443,469,

482,495,51632084 . . . . . . . . . .443,469,

482,495,51632085 . . . . . . . . . .443,469,

482,495,51632086 . . . . . . . . . .443,469,

482,495,51632087 . . . . . . . . . .443,469,

482,495,51632088 . . . . . . . . . .443,469,

482,495,51632089 . . . . . . . . . . . . . .49632090 . . . . . . . . . . . . . .49632091 . . . . . . . . . .447,45432092 . . . . . . . . . .444,45432093 . . . . . . . . . . . . . .45432094 . . . . . . . . . . . . . .45432095 . . . . . . . . . . . . . .45432096 . . . . . . . . . . . . . .45432097 . . . . . . . . . . . . . .45532098 . . . . . . . . . . . . . .44432099 . . . . . . . . . . . . . .44432200 . . . . . . . . . . . . . .44432201 . . . . . . . . . . . . . .44432202 . . . . . . . . . . . . . .44432203 . . . . . . . . . . . . . .44432204 . . . . . . . . . . . . . .44332205 . . . . . . . . . . . . . .44332206 . . . . . . . . . . . . . .44332207 . . . . . . . . . . . . . .44432208 . . . . . . . . . . . . . .44332209 . . . . . . . . . . . . . .44332211 . . . . . . . . . . . . . .44432212 . . . . . . . . . . . . . .44432215 . . . . . . . . . . . . . .44432216 . . . . . . . . . . . . . .44432217 . . . . . . . . . . . . . .44332218 . . . . . . . . . . . . . .44532219 . . . . . . . . . . . . . .44532220 . . . . . . . . . . . . . .44532221 . . . . . . . . . . . . . .44532222 . . . . . . . . . . . . . .44532223 . . . . . . . . . . . . . .44532224 . . . . . . . . . . . . . .44532226 . . . . . . . . . . . . . .44332227 . . . . . . . . . . . . . .44432228 . . . . . . . . . . . . . .44632230 . . . . . . . . . . . . . .44632231 . . . . . . . . . . . . . .44632232 . . . . . . . . . . . . . .44632233 . . . . . . . . . . . . . .44632235 . . . . . . . . . . . . . .44732236 . . . . . . . . . . . . . .44832238 . . . . . . . . . . . . . .44832239 . . . . . . . . . . . . . .44432240 . . . . . . . . . . . . . .44432241 . . . . . . . . . . . . . .44432243 . . . . . . . . . . . . . .448

32244 . . . . . . . . . . . . . .44832245 . . . . . . . . . . . . . .44832246 . . . . . . . . . . . . . .44832247 . . . . . . . . . . . . . .44432248 . . . . . . . . . . . . . .44432249 . . . . . . . . . . . . . .44532250 . . . . . . . . . . . . . .44532251 . . . . . . . . . . . . . .44532252 . . . . . . . . . . . . . .44532253 . . . . . .444,455,463,

466,475,48432254 . . . . . . . . . .444,455,

463,466,47532255 . . . . . . . . . . . . . .44332256 . . . . . . . . . . . . . .44332257 . . . . . . . . . . . . . .44332261 . . . . . . . . . . . . . .44432264 . . . . . . . . . .445,47532265 . . . . . . . . . .447,47532266 . . . . . . . . . . . . . .44732268 . . . . . . . . . . . . . .44732269 . . . . . . . . . .446,47532271 . . . . . . . . . .446,47532273 . . . . . . . . . . . . . .46132274 . . . . . . . . . .443,46132275 . . . . . . . . . . . . . .46132277 . . . . . . . . . . . . . .47432278 . . . . . . . . . . . . . .47432279 . . . . . . . . . .443,47432280 . . . . . . . . . .448,47432281 . . . . . . . . . .448,47432282 . . . . . . . . . .444,47432283 . . . . . . . . . .448,49632284 . . . . . . . . . .448,49632285 . . . . . . . . . .447,49632286 . . . . . . . . . .446,49632287 . . . . . . . . . .446,49632288 . . . . . . . . . .446,49632289 . . .444,454,493,49632290 . . . . . . . . . .496,49932291 . . . . . . . .88,472,49432292 . . . . . . . .88,473,49432293 . . . . . . . . . .447,49632294 . . . . . . . . . .496,49932297 . . . . . . . . . . . . . .49432298 . . . . . . . . . . . . . .49432299 . . . . . . .469,482,49532400 . . . . . . . . . . . . . .49632401 . . . . . . . . . . . . . .49632404 . . . . . . . . . . . . . .49532406 . . . . . . . . . . . . . .49732407 . . . . . . . . . . . . . .49732408 . . . . . . . . . . . . . .49732409 . . .443,469,482,49532410 . . .443,469,482,49532412 . . . . . . . . . . . . . .53632413 . . . . . . . . . . . . . .53632414 . . . . . . . . . . . . . .53632415 . . .458,473,481,49432416 . . . . . . . . . . . . . .47332417 . . . . . . .454,465,49332418 . . . . . . . . . . . . . .49932419 . . . . . . . . . . . . . .48132420 . . . . . . . . . . . . . .45832423 . . . . . . . . . .454,45832424 . . . . . . . . . .448,51632425 . . . . . . . . . .448,51632426 . . . . . . . . . .446,46132427 . . . . . . . . . .446,46132428 . . . . . . . . . .443,46132429 . . . . . . . . . .463,48432430 . . . . . . . . . .463,48432431 . . . . . . . . . .463,48432432 . . . . . .444,455,463,

466,475,48432433 . . . . . . . . . . . . . .46132434 . . . . . . . . . . . . . .46132435 . . . . . . . . . . . . . .46132436 . . . . . . . . . . . . . .44732437 . . . . . . . . . .189,46132438 . . . . . . . . . . . . . .46232439 . . .445,455,466,475

32441 . . . . . . .189,199,46132443 . . . . . . . . . . . . . .45532444 . . . . . . . . . . . . . .45532445 . . . . . . . . . .444,49932446 . . . . . . . . . .444,49932447 . . . . . . . . . .448,49932448 . . . . . . . . . .447,49932449 . . . . . . . . . .447,49932450 . . . . . . . . . . . . . .44532453 . . . . . . . . . .473,49332454 . . . . . . . . . . . . . .49332456 . . . . . . .469,482,49532457 . . . . . . . . . .473,49333000 . . . . . . . . . .448,51333001 . . . . . . . . . .448,51333002 . . . . . . . . . .446,51333003 . . . . . . . . . .446,51333004 . . . . . . . . . .446,51333007 . . . . . . . . . . . . . .45933008 . . . . . . . . . . . . . .45933009 . . . . . . . . . . . . . .45933010 . . . . . . . . . . . . . .45933011 . . . . . . . . . . . . . .45933012 . . . . . . . . . .454,45833013 . . . . . . . . . .454,45833017 . . . . . . . . . . . . . .44333020 . . . . . . . . . .446,51633021 . . . . . . . . . .447,51633022 . . . . . . . . . .445,51633023 . . . . . . . . . .448,51633024 . . . . . . . . . .443,51633025 . . . . . . . . . .448,51633026 . . . . . . . . . .447,51633027 . . . . . .447,456,469,

477,479,486,48933028 . . . . . . . . . .479,48933028.15 . . . . . . . .479,48933028.25 . . . . . . . .479,48933029 . . . . . . . . . .479,48833029.15 . . . . . . . .479,48833029.25 . . . . . . . .479,48833030 . . . . . . . . . .479,48933030.15 . . . . . . . .479,48933030.25 . . . . . . . .479,48933031 . . . . . . . . . . . . . .47933031.15 . . . . . . . . . . .47933031.25 . . . . . . . . . . .47933032 . . . . . . . . . .443,51633033 . . . . . . . . . .448,51633034 . . . . . . . . . . . . . .51633035 . . . . . . . . . . . . . .51933036 . . . . . . . . . . . . . .51933037 . . . . . . . . . . . . . .52033038 . . . . . . . . . . . . . .52033039 . . . . . . . . . . . . . .52033040 . . . . . . . . . . . . . .52033041 . . . . . . . . . . . . . .52033042 . . . . . . . . . . . . . .52033043 . . . . . . . . . . . . . .51933044 . . . . . . . . . . . . . .51933045 . . . . . . . . . . . . . .51933046 . . . . . . . . . . . . . .51933047 . . . . . . . . . . . . . .51933048 . . . . . . . . . . . . . .51933049 . . . . . . . . . . . . . .51833050 . . . . . . . . . . . . . .51833051 . . . . . . . . . . . . . .51833052 . . . . . . . . . . . . . .51833053 . . . . . . . . . . . . . .51833054 . . . . . . . . . . . . . .51833055 . . . . . . . . . . . . . .51833056 . . . . . . . . . . . . . .51833057 . . . . . . . . . . . . . .52033058 . . . . . . . . . . . . . .52033059 . . . . . . . . . . . . . .52033060 . . . . . . . . . . . . . .51933061 . . . . . . . . . . . . . .51933062 . . . . . . . . . . . . . .51933063 . . . . . . . . . . . . . .52133064 . . . . . . . . . . . . . .52133065 . . . . . . . . . . . . . .52133066 . . . . . . . . . . . . . .521

33067 . . . . . . . . . . . . . .52133068 . . . . . . . . . . . . . .52133069 . . . . . . . . . . . . . .52133070 . . . . . . . . . . . . . .52133071 . . . . . . . . . . . . . .52133072 . . . . . . . . . . . . . .52133073 . . . . . . . . . . . . . .48033073.15 . . . . . . . . . . .48033073.25 . . . . . . . . . . .48033074 . . . . . . .443,483,51333075 . . . . . . .443,483,51333077 . . . . . . .443,483,51333079 . . . . . . .443,483,51333080 . . . . . . .444,483,51333082 . . . . . . .446,483,51333083 . . . . . . .446,483,51333084 . . . . . . .446,483,51333086 . . . . . . .447,483,51333088 . . . . . . . . . .483,51333091 . . . . . . .446,483,51333092 . . . . . . . . . .443,46133093 . . . . . . . . . .483,51333094 . . . . . . . . . .443,46133095 . . . . . . .446,483,51333096 . . . . . . . . . .443,46133098 . . . . . . . . . . . . . .45933099 . . . . . . . . . .443,46133200 . . . . . . . . . .447,46133201 . . . . . . . . . .447,46133202 . . . . . . . . . .443,46133203 . . . . . . . . . .445,46133204 . . . . . . . . . . . . . .48433205 . . . . . . . . . .445,48433207 . . . . . . . . . .443,45833208 . . . . . . . . . .443,45833209 . . . . . . . . . .447,45833211 . . . . . . . . . . . . . .45833227 . . . . . . . . . . . . . .47233228 . . . . . . . . . .446,47233229 . . . . . . . . . . . . . .47233247 . . . . . . . . . .446,53533248 . . . . . . . . . .444,53533249 . . . . . . . . . .443,53533250 . . . . . . . . . .443,53533251 . . . . . . . . . .443,53533252 . . . . . . . . . .443,53533253 . . . . . . . . . . . . . .53533254 . . . . . . . . . . . . . .53533255 . . . . . . . . . .447,53433256 . . . . . . . . . .447,53433257 . . . . . . . . . .447,53433258 . . . . . . . . . .448,53433259 . . . . . . . . . .448,53433260 . . . . . . . . . .448,53433261 . . . . . . . . . .447,53433262 . . . . . . . . . .447,53433263 . . . . . . . . . .447,53433264 . . . . . . . . . .443,53433265 . . . . . . . . . . . . . .53433266 . . . . . . . . . . . . . .53433267 . . . . . . . . . . . . . .53433268 . . . . . . . . . . . . . .53433900 . . . . . . . . . . . . . .46033901 . . . . . .445,460,473,

474,485,52433902 . . . . . . . . . .447,46033903 . . . . . . . . . .448,46033905 . . . . . . . . . . . . . .48433906 . . . . . . . . . . . . . .53933908 . . . . . . . . . . . . . .53933909 . . . . . . . . . . . . . .53933910 . . . . . . . . . .447,45633911 . . . . . . . . . .447,45633912 . . . . . . . . . . . . . .44833913 . . . . . . . . . . . . . .48834000 . . . . . . . . . .444,52534002 . . . . . . . . . .446,52534003 . . . . . . . . . .446,52534004 . . . . . . . . . .446,52534005 . . . . . . . . . .446,52534006 . . . . . . . . . .447,52534007 . . . . . . . . . .447,525

34008 . . . . . . . . . .444,52534009 . . . . . . . . . .448,52534010 . . . . . . . . . .444,52534011 . . . . . . . . . .444,52534015 . . . . . . . . . .444,52534016 . . . . . . . . . .443,52534017 . . . . . . . . . .445,52534018 . . . . . . . . . .445,52534020 . . . . . . . . . .443,52534021 . . . . . . . . . .446,52534022 . . . . . . . . . .443,52534024 . . . . . . . . . .447,52534025 . . . . . . . . . .447,52534026 . . . . . . . . . .447,52534027 . . . . . . . . . .447,52534028 . . . . . . . . . .443,52534029 . . . . . . . . . .443,52534030 . . . . . . . . . .443,52534031 . . . . . . . . . .443,52534032 . . . . . . . . . .443,52534033 . . . . . . . . . .446,52534034 . . . . . . . . . .446,52534035 . . . . . . . . . .446,52534036 . . . . . . . . . .447,52534037 . . . . . . . . . .447,52534038 . . . . . . . . . .448,52534039 . . . . . . . . . .448,52534041 . . . . . . . . . .448,52534042 . . . . . . . . . .443,52534043 . . . . . . . . . .443,52534044 . . . . . . . . . .444,52534045 . . . . . . . . . .444,52534046 . . . . . . . . . .444,52534047 . . . . . . . . . .444,52534049 . . . . . . . . . .446,52534050 . . . . . . . . . .446,52534051 . . . . . . . . . .446,52534053 . . . . . . . . . .447,52534054 . . . . . . . . . .447,52534055 . . . . . . . . . .447,52534056 . . . . . . . . . .448,52534057 . . . . . . . . . .448,52534058 . . . . . . . . . .446,52534059 . . . . . . . . . .446,52534060 . . . . . . . . . .447,52534062 . . . . . . . . . .447,52534063 . . . . . . . . . .446,52534064 . . . . . . . . . .446,52534065 . . . . . . . . . .447,52534066 . . . . . . . . . .444,52534067 . . . . . . . . . .448,52534068 . . . . . . . . . .448,52534069 . . . . . . . . . .445,52534070 . . . . . . . . . .446,52534071 . . . . . . . . . .446,52534072 . . . . . . . . . .446,52534073 . . . . . . . . . .447,52534077 . . . . . . . . . .443,52534078 . . . . . . . . . .443,52534079 . . . . . . . . . .447,52534080 . . . . . . . . . .448,52534081 . . . . . . . . . .444,52534082 . . . . . . . . . .445,52534083 . . . . . . . . . .445,52534084 . . . . . . . . . .444,52534085 . . . . . . . . . .447,52534086 . . . . . . . . . .444,52534400 . . . . . . . . . . . . . .42734400-PI . . . . . . . . . . .42734402 . . . . . . . . . . . . . .42834402-PI . . . . . . . . . . .42834404 . . . . . . . . . . . . . .42834404-PI . . . . . . . . . . .42834406 . . . . . . . . . . . . . .42834406-PI . . . . . . . . . . .42834408 . . . . . . . . . . . . . .42834408-PI . . . . . . . . . . .42834412 . . . . . . . . . . . . . .42834412-PI . . . . . . . . . . .42834414 . . .429,471,476,50334414-PI .429,471,476,50334418 . . . . . . . . . .429,499


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INDEX

Catalog #34418-PI . . . . . . . .429,49934420 . . . . . . . . . . . . . .43034420-PI . . . . . . . . . . .43034421 . . . . . . . . . . . . . .42734421-PI . . . . . . . . . . .42734422 . . . . . . . . . . . . . .42834422-PI . . . . . . . . . . .42834423 . . . . . . . . . . . . . .42834423-PI . . . . . . . . . . .42834424 . . . . . . . . . . . . . .42834424-PI . . . . . . . . . . .42834425 . . . . . . . . . . . . . .42834425-PI . . . . . . . . . . .42834427 . . . . . . . . . . . . . .42834427-PI . . . . . . . . . . .42834428 . . .429,471,476,50334428-PI .429,471,476,50334429 . . . . . . . . . . . . . .43034429-PI . . . . . . . . . . .43034430 . . . . . . . . . . . . . .42734430-PI . . . . . . . . . . .42734431 . . . . . . . . . . . . . .42734431-PI . . . . . . . . . . .42734432 . . . . . . . . . . . . . .42734432-PI . . . . . . . . . . .42734433 . . . . . . . . . . . . . .42734433-PI . . . . . . . . . . .42734434 . . . . . . . . . . . . . .42834434-PI . . . . . . . . . . .42834435 . . . . . . . . . . . . . .42834435-PI . . . . . . . . . . .42834436 . . . . . . . . . . . . . .42834436-PI . . . . . . . . . . .42834437 . . . . . . . . . . . . . .42834437-PI . . . . . . . . . . .42834438 . . . . . . . . . . . . . .43134439 . . . . . . . . . . . . . .43134440 . . . . . . . . . . . . . .43134441 . . . . . . . . . . . . . .43134442 . . . . . . . . . . . . . .43134443 . . . . . . . . . . . . . .43134445 . . . . . . . . . . . . . .43034445-PI . . . . . . . . . . .43034448 . . . . . . . . . . . . . .43234449 . . . . . . . . . . . . . .43234449-PI . . . . . . . . . . .43234451 . . . . . . . . . . . . . .43234452 . . . . . . . . . . . . . .43234452-PI . . . . . . . . . . .43234453 . . . . . . . . . . . . . .43234453-PI . . . . . . . . . . .43234454 . . . . . . . . . . . . . .43234454-PI . . . . . . . . . . .43234455 . . . . . . . . . . . . . .43234457 . . . . . . . . . . . . . .43234457-PI . . . . . . . . . . .43234458 . . . . . . . . . . . . . .43234458-PI . . . . . . . . . . .43234459 . . . . . . . . . . . . . .43234459-PI . . . . . . . . . . .43234460 . . . . . . . . . . . . . .43234461 . . . . . . . . . . . . . .43234461-PI . . . . . . . . . . .43234462 . . . . . . . . . . . . . .43234462-PI . . . . . . . . . . .43234463 . . . . . . . . . . . . . .43234464 . . . . . . . . . . . . . .43234464-PI . . . . . . . . . . .43234465 . . . . . . . . . . . . . .43234466 . . . . . . . . . . . . . .43234466-PI . . . . . . . . . . .43234467 . . . . . . . . . . . . . .43234468 . . . . . . . . . . . . . .43234468-PI . . . . . . . . . . .43234469 . . . . . . . . . . . . . .43234469-PI . . . . . . . . . . .43234471 . . . . . . . . . . . . . .43234472 . . . . . . . . . . . . . .43234472-PI . . . . . . . . . . .43234473 . . . . . . . . . . . . . .43234474 . . . . . . . . . . . . . .43234474-PI . . . . . . . . . . .432

34476 . . . . . . . . . . . . . .43234477 . . . . . . . . . . . . . .43234477-PI . . . . . . . . . . .43234478 . . . . . . . . . . . . . .43234478-PI . . . . . . . . . . .43234479 . . . . . . . . . . . . . .43234479-PI . . . . . . . . . . .43234480 . . . . . . . . . . . . . .43234480-PI . . . . . . . . . . .43234482 . . . . . . . . . . . . . .43234483 . . . . . . . . . . . . . .43234483-PI . . . . . . . . . . .43234484 . . . . . . . . . . . . . .43234485 . . . . . . . . . . . . . .43234485-PI . . . . . . . . . . .43234487 . . . . . . . . . . . . . .43234488 . . . . . . . . . . . . . .43234488-PI . . . . . . . . . . .43234489 . . . . . . . . . . . . . .43234489-PI . . . . . . . . . . .43234491 . . . . . . . . . . . . . .43234492 . . . . . . . . . . . . . .43234492-PI . . . . . . . . . . .43234493 . . . . . . . . . . . . . .43234493-PI . . . . . . . . . . .43234494 . . . . . . . . . . . . . .43234495 . . . . . . . . . . . . . .43234495-PI . . . . . . . . . . .43234496 . . . . . . . . . . . . . .43234497 . . . . . . . . . . . . . .43234497-PI . . . . . . . . . . .43234498 . . . . . . . . . . . . . .43234499 . . . . . . . . . . . . . .43234499-PI . . . . . . . . . . .43234500 . . . . . . . . . . . . . .43234500-PI . . . . . . . . . . .43234501 . . . . . . . . . . . . . .43234501-PI . . . . . . . . . . .43234502 . . . . . . . . . . . . . .43234502-PI . . . . . . . . . . .43234504 . . . . . . . . . . . . . .43234505 . . . . . . . . . . . . . .43234505-PI . . . . . . . . . . .43234507 . . . . . . . . . . . . . .43234508 . . . . . . . . . . . . . .43234508-PI . . . . . . . . . . .43234511 . . . . . . . . . . . . . .43234511-PI . . . . . . . . . . .43234512 . . . . . . . . . . . . . .43234512-PI . . . . . . . . . . .43234514 . . . . . . . . . . . . . .43234514-PI . . . . . . . . . . .43234515 . . . . . . . . . . . . . .43234516 . . . . . . . . . . . . . .43234516-PI . . . . . . . . . . .43234518 . . . . . . . . . . . . . .43234519 . . . . . . . . . . . . . .43234519-PI . . . . . . . . . . .43234521 . . . . . . . . . . . . . .43234522 . . . . . . . . . . . . . .43234522-PI . . . . . . . . . . .43234524 . . . . . . . . . . . . . .43234525 . . . . . . . . . . . . . .43234525-PI . . . . . . . . . . .43234527 . . . . . . . . . . . . . .43234528 . . . . . . . . . . . . . .43234528-PI . . . . . . . . . . .43234529 . . . . . . . . . . . . . .43234530 . . . . . . . . . . . . . .43234530-PI . . . . . . . . . . .43234531 . . . . . . . . . . . . . .43234532 . . . . . . . . . . . . . .43234532-PI . . . . . . . . . . .43234534 . . . . . . . . . . . . . .43234534-PI . . . . . . . . . . .43234537 . . . . . . . . . . . . . .43234537-PI . . . . . . . . . . .43234539 . . . . . . . . . . . . . .43234539-PI . . . . . . . . . . .43234540 . . . . . . . . . .429,50834540-PI . . . . . . . .429,50834541 . . . . . . . . . . . . . .429

34541-PI . . . . . . . . . . .42934542 . . . . . . . . . . . . . .42934542-PI . . . . . . . . . . .42934560 . . . . . . . . . . . . . .42934561 . . . . . . . . . . . . . .42934561-PI . . . . . . . . . . .42935000 . . . . . . . . . . . . . .53835002 . . . . . . . . . . . . . .53835003 . . . . . . . . . . . . . .53835004 . . . . . . . . . .199,53935005 . . . . . . . . . .199,53935010 . . . . . . . . . . . . . .53335011 . . . . . . . . . . . . . .53335012 . . . . . . . . . . . . . .53335013 . . . . . . . . . . . . . .53335014 . . . . . . . . . . . . . .53335015 . . . . . . . . . . . . . .53335016 . . . . . . . . . . . . . .53335017 . . . . . . . . . . . . . .53335018 . . . . . . . . . . . . . .53335021 . . . . . . . . . . . . . .53335022 . . . . . . . . . . . . . .53335023 . . . . . . . . . . . . . .53335024 . . . . . . . . . . . . . .53335025 . . . . . . . . . . . . . .53335026 . . . . . . . . . . . . . .53335027 . . . . . . . . . . . . . .53335034 . . . . . . . . . . . . . .53335035 . . . . . . . . . . . . . .53335036 . . . . . . . . . . . . . .53335037 . . . . . . . . . .446,53235038 . . . . . . . . . .446,53235039 . . . . . . . . . .446,53235040 . . . . . . . . . .447,53235041 . . . . . . . . . .446,53235042 . . . . . . . . . .447,53235043 . . . . . . . . . .447,53235044 . . . . . . . . . .447,53235045 . . . . . . . . . .447,53235046 . . . . . . . . . .447,53235047 . . . . . . . . . .447,53235048 . . . . . . . . . .447,53235049 . . . . . . . . . .447,53235050 . . . . . . . . . .446,53235051 . . . . . . . . . .447,53235052 . . . . . . . . . .447,53235053 . . . . . . . . . .447,53235054 . . . . . . . . . .447,53235055 . . . . . . . . . .447,53235056 . . . . . . . . . .446,53235057 . . . . . . . . . .446,53235058 . . . . . . . . . .446,53235059 . . . . . . . . . .446,53235060 . . . . . . . . . .446,53235061 . . . . . . . . . .446,53235062 . . . . . . . . . .446,53235063 . . . . . . . . . .446,53235064 . . . . . . . . . .447,53235065 . . . . . . . . . .447,53235066 . . . . . . . . . . . . . .53135077 . . . . . . . . . . . . . .53235078 . . . . . . . . . . . . . .53235079 . . . . . . . . . . . . . .53135080 . . . . . . . . . . . . . .53135081 . . . . . . . . . . . . . .53135100 . . . . . . . . . .529,53335101 . . . . . . . . . .529,53335202 . . . . . . . . . . . . . .53835222 . . . . . . . . . . . . . .44535226 . . . . . . . . . . . . . .53835262 . . . . . . . . . . . . . .44335272 . . . . . . . . . . . . . .53135600 . . . . . . . . . . . . . .53735601 . . . . . . . . . . . . . .53735602 . . . . . . . . . . . . . .53735603 . . . . . . . . . . . . . .53735604 . . . . . . . . . . . . . .53735605 . . . . . . . . . . . . . .53735606 . . . . . . . . . . . . . .53735607 . . . . . . . . . . . . . .53735608 . . . . . . . . . . . . . .53735610 . . . . . . . . . . . . . .537

35611 . . . . . . . . . . . . . .53735612 . . . . . . . . . . . . . .53735614 . . . . . . . . . . . . . .53735615 . . . . . . . . . . . . . .53735616 . . . . . . . . . . . . . .53735617 . . . . . . . . . . . . . .53735618 . . . . . . . . . . . . . .53735619 . . . . . . . . . . . . . .53735620 . . . . . . . . . . . . . .53735621 . . . . . . . . . . . . . .53735622 . . . . . . . . . . . . . .53735623 . . . . . . . . . . . . . .53735624 . . . . . . . . . . . . . .53735625 . . . . . . . . . . . . . .53736002 . . . . . . . . . . . . . .52836004 . . . . . . . . . . . . . .52836005 . . . . . . . . . .445,52836006 . . . . . . . . . . . . . .52836007 . . . . . . . . . . . . . .52836008 . . . . . . . . . . . . . .52836009 . . . . . . . . . . . . . .52836224 . . . . . . . . . .447,51636225 . . . .79,120,447,51636226 . . . . . . . . . .447,51636227 . . . .79,120,447,51636228 . . . . . . . . . . . . . .52836232 . . . . . . . . . . . . . .52436233 . . . . . . . . . . . . . .52436234 . . . . . . . . . . . . . .52436235 . . . . . . . . . . . . . .52436236 . . . . . . . . . . . . . .52436237 . . . . . . . . . . . . . .52436238 . . . . . . . . . . . . . .52436239 . . . . . . . . . . . . . .52436242 . . . . . . . . . . . . . .52436243 . . . . . . . . . . . . . .52436244 . . . . . . . . . . . . . .52436245 . . . . . . . . . . . . . .52436246 . . . . . . . . . . . . . .52436247 . . . . . . . . . . . . . .52436248 . . . . . . . . . . . . . .52436249 . . . . . . . . . . . . . .52436251 . . . . . . . . . . . . . .52436252 . . . . . . . . . . . . . .52436253 . . . . . . . . . . . . . .52436254 . . . . . . . . . . . . . .52436255 . . . . . . . . . . . . . .52436256 . . . . . . . . . . . . . .52436257 . . . . . . . . . . . . . .52436258 . . . . . . . . . . . . . .52436259 . . . . . . . . . . . . . .52436260 . . . . . . . . . . . . . .52436261 . . . . . . . . . . . . . .52836262 . . . . . . . . . . . . . .52436263 . . . . . . . . . . . . . .52436264 . . . . . . . . . . . . . .52436265 . . . . . . . . . . . . . .52436266 . . . . . . . . . . . . . .52436267 . . . . . . . . . . . . . .52436268 . . . . . . . . . . . . . .52436269 . . . . . . . . . . . . . .52436270 . . . . . . . . . . . . . .52936271 . . . . . . . . . . . . . .52736273 . . . . . . . . . . . . . .52736274 . . . . . . . . . . . . . .52936275 . . . . . . . . . . . . . .52936276 . . . . . . . . . . . . . .52436277 . . . . . . . . . . . . . .52436278 . . . . . . . . . . . . . .52436279 . . . . . . . . . . . . . .52736280 . . . . . . . . . . . . . .52736281 . . . . . . . . . .443,52736282 . . . . . . . . . .443,52736283 . . . . . . . . . .444,52736284 . . . . . . . . . .444,52736285 . . . . . . . . . .444,52736286 . . . . . . . . . .444,52736287 . . . . . . . . . .445,52736288 . . . . . . . . . .445,52736289 . . . . . . . . . .445,52736290 . . . . . . . . . .445,52736291 . . . . . . . . . .445,527

36292 . . . . . . . . . .445,52736293 . . . . . . . . . .445,52736294 . . . . . . . . . .445,52736295 . . . . . . . . . .445,52736296 . . . . . . . . . .445,52736297 . . . . . . . . . .445,52736298 . . . . . . . . . .446,52736299 . . . . . . . . . .446,52736332 . . . . . . . . . . . . . .52436333 . . . . . . . . . . . . . .52436334 . . . . . . . . . . . . . .52436335 . . . . . . . . . . . . . .52436336 . . . . . . . . . . . . . .52436337 . . . . . . . . . . . . . .52436338 . . . . . . . . . . . . . .52436339 . . . . . . . . . . . . . .52436340 . . . . . . . . . . . . . .52536341 . . . . . . . . . . . . . .52536400 . . . . . . . . . .446,52736401 . . . . . . .446,507,52736402 . . . . . . . . . .446,52736403 . . . . . . . . . .446,52736404 . . . . . . . . . .447,52736405 . . . . . . . . . .447,52736406 . . . . . . . . . .447,52736407 . . . . . . . . . .447,52736408 . . . . . . . . . .448,52736409 . . . . . . . . . .448,52736410 . . . . . . . . . .448,52736411 . . . . . . . . . .448,52736412 . . . . . . . . . .448,52736413 . . . . . . . . . .448,52736414 . . . . . . . . . .448,52736415 . . . . . . . . . .448,52736416 . . . . . . . . . .448,52736417 . . . . . . . . . . . . . .52436418 . . . . . . . . . . . . . .52436419 . . . . . . . . . . . . . .52436420 . . . . . . . . . . . . . .52440101 . . . . . . . . . . . . . . .4940102 . . . . . . . . . . . . . . .4940103 . . . . . . . . . . . . . . .4940110 . . . . . . . . . . . . . . .4940111 . . . . . . . . . . . . . . .4940112 . . . . . . . . . . . . . . .4940201 . . . . . . . . . . . . . . .5040202 . . . . . . . . . . . . . . .5040203 . . . . . . . . . . . . . . .5040210 . . . . . . . . . . . . . . .5040211 . . . . . . . . . . . . . . .5040212 . . . . . . . . . . . . . . .5040401 . . . . . . . . . . . . . . .5140402 . . . . . . . . . . . . . . .5140410 . . . . . . . . . . . . . . .5140411 . . . . . . . . . . . . . . .5140501 . . . . . . . . . . . . . . .5240502 . . . . . . . . . . . . . . .5240510 . . . . . . . . . . . . . . .5240511 . . . . . . . . . . . . . . .5240602 . . . . . . . . . . . . . . .5940701 . . . . . . . . . . . . . . .5740702 . . . . . . . . . . . . . . .5740703 . . . . . . . . . . . . . . .5740914 . . . . . . . . . . . . . .10240915 . . . . . . . . . . . . . .10240924 . . . . . . . . . . . . . . .5540925 . . . . . . . . . . . . . . .5541101 . . . . . . . . . . . . . . .4941102 . . . . . . . . . . . . . . .4941103 . . . . . . . . . . . . . . .4941104 . . . . . . . . . . . . . . .4941201 . . . . . . . . . . . . . . .5041202 . . . . . . . . . . . . . . .5041203 . . . . . . . . . . . . . . .5041204 . . . . . . . . . . . . . . .5041302 . . . . . . . . . . . . . . .9341303 . . . . . . . . . . . . . . .9341304 . . . . . . . . . . . . . . .9341601 . . . . . . . . . . . . . . .5841602 . . . . . . . . . . . . . . .5841603 . . . . . . . . . . . . . . .5841604 . . . . . . . . . . . . . . .58

42001 . . . . . . . . . . . . . . .5642002 . . . . . . . . . . . . . . .5642010 . . . . . . . . . . . . . . .5642011 . . . . . . . . . . . . . . .5642101 . . . . . . . . . . . . . . .8842102 . . . . . . . . . . . . . . .8842201 . . . . . . . . . . . . . . .5642202 . . . . . . . . . . . . . . .5642301 . . . . . . . . . . . . . . .8842302 . . . . . . . . . . . . . . .8842601 . . . . . . . . . . . .59,6042902 . . . . . . . . . . . . . . .5342903 . . . . . . . . . . . . . . .5343101 . . . . . . . . . . . .60,8843301 . . . . . . . . . . . .60,8843302 . . . . . . . . . . . .60,8843601 . . . . . . .42,60,87,9743602 . . . . . . . . . .42,87,9743604 . . . . . . . . . .42,87,9743605 . . . . . . . . . . . . .42,8743607 . . . . . . . . . . . . . . .9543701 . . . . . . . . . . . .44,9443702 . . . . . . . . . . . .44,9443800 . . . . . . . . . . . . . . .6043801 . . . . . . . . . . . . . . .6043802 . . . . . . . . . . . . . . .6043815 . . . . . . . . . . . . . . .6043816 . . . . . . . . . . . . . . .6043817 . . . . . . . . . . . . . . .6043820 . . . . . . . . . . . . . . .6043821 . . . . . . . . . . . . . . .6043830 . . . . . . . . . . . . . . .6043831 . . . . . . . . . . . . . . .6043835 . . . . . . . . . . . . . . .6043836 . . . . . . . . . . . . . . .6045001 . . . . . . . . . . . . . . .5445002 . . . . . . . . . . . . . . .5445003 . . . . . . . . . . . . . . .5445010 . . . . . . . . . . . . . . .5445011 . . . . . . . . . . . . . . .5445012 . . . . . . . . . . . . . . .5449314 . . . . . . . . . . . . . .10149315 . . . . . . . . . . . . . .10149914 . . . . . . . . . . . . . .10049915 . . . . . . . . . . . . . .10070044 . . . . . . . . . . . . . .11470044-600 . . . . . . . . . .11470045 . . . . . . . . . . . . . .11470045-600 . . . . . . . . . .11470046 . . . . . . . . . . . . . .11470047 . . . . . . . . . . . . . .11470080 . . . . . . . . . . . . . .11470081 . . . . . . . . . . . . . .11470083 . . . . . . . . . . . . . .11470084 . . . . . . . . . . . . . .11470086 . . . . . . . . . . . . . .11470087 . . . . . . . . . . . . . .11470089 . . . . . . . . . . . . . .11470090 . . . . . . . . . . . . . .11470101 . . . . . . . .79,115,12070102 . . . . . . . . . . . . . .11570104 . . . . . . . . . . .79,12070105 . . . . . . . . . . . . . .11570106 . . . . . . . . . . . . . .11570107 . . . . . . . . . . . . . .11570109 . . . . . . . . . . . . . .11570112 . . . . . . . . . . .78,12070114 . . . . . . . . . . . . . .11570115 . . . . . . . . . . .78,12070116 . . . . . . . . . . . . . .11570117 . . . . . . . . . . . . . .11570118 . . . . . . . . . . .78,12070119 . . . . . . . . . . .78,12070120 . . . . . . . . . . . . . .11570121 . . . . . . . . . . . . . .11570122 . . . . . . . . . . . . . .11570123 . . . . . . . . . . . . . .11570124 . . . . . . . . . . . . . .11570125 . . . . . . . . . . . . . .11570126 . . . . . . . . . . . . . .11570127 . . . . . . . . . . . . . .11570128 . . . . . . . . . . . . . .115


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INDEX

Catalog #70129 . . . . . . . . . . . . . .11570130 . . . . . . . . . . .78,12070131 . . . . . . . . . . .78,12070132 . . . . . . . . .77,78,12070133 . . . . . . . . . . .78,12070134 . . . . . . . . . . . .78,12070135 . . . . . . . . . . . . . .11570136 . . . . . . . . . . . . . .11570137 . . . . . . . . . . . . . .11570138 . . . . . . . . . . . . . .11570139 . . . . . . . . . . . . . .11570140 . . . . . . . . . . . . . .11570141 . . . . . . . . . . . . . .11570142 . . . . . . . . . . . . . .11570143 . . . . . . . . . . . . . .11570144 . . . . . . . . . . . . . .11570150 . . . . . . . . . . . . . .11570151 . . . . . . . . . . . . . .11570152 . . . . . . . . . . . . . .11570153 . . . . . . . . . . . . . .11570154 . . . . . . . . . . . . . .11570155 . . . . . . . . . . . . . .11570156 . . . . . . . . . . . . . .11570157 . . . . . . . . . . . . . .11570158 . . . . . . . . . . . . . .11570159 . . . . . . . . . . . . . .11570167 . . . . . . . . . . . . . .11570170 . . . . . . . . . . . . . .11570173 . . . . . . . . . . . . . .11570177 . . . . . . . . . . . . . .11570179 . . . . . . . . . . . . . .11570181 . . . . . . . . . . . . . .11570182 . . . . . . . . . . . . . .11570183 . . . . . . . . . . . . . .11570184 . . . . . . . . . . . . . .11570185 . . . . . . . . . . . . . .11570187 . . . . . . . . . . . . . .11570188 . . . . . . . . . . . . . .11570189 . . . . . . . . . . . . . .11570191 . . . . . . . . . . . . . .11570192 . . . . . . . . . . . . . .11570193 . . . . . . . . . . . . . .11570199 . . . . . . . . . . .77,11970205 . . . . . . . . . . . . . .11670208 . . . . . . . . . . . . . .11670211 . . . . . . . . . . . . . .11670220 . . . . . . . . . . . . . .11670221 . . . . . . . . . . . . . .11670222 . . . . . . . . . . . . . .11670223 . . . . . . . . . . . . . .11670224 . . . . . . . . . . . . . .11670225 . . . . . . . . . . . . . .11670226 . . . . . . . . . . . . . .11670227 . . . . . . . . . . . . . .11670228 . . . . . . . . . . . . . .11670235 . . . . . . . . . . . . . .11670236 . . . . . . . . . . . . . .11670237 . . . . . . . . . . . . . .11670238 . . . . . . . . . . . . . .11670239 . . . . . . . . . . . . . .11670240 . . . . . . . . . . . . . .11670241 . . . . . . . . . . . . . .11670242 . . . . . . . . . . . . . .11670243 . . . . . . . . . . . . . .11670250 . . . . . . . . . . . . . .11670251 . . . . . . . . . . . . . .11670252 . . . . . . . . . . . . . .11670253 . . . . . . . . . . . . . .11670254 . . . . . . . . . . . . . .11670255 . . . . . . . . . . . . . .11670256 . . . . . . . . . . . . . .11670257 . . . . . . . . . . . . . .11670258 . . . . . . . . . . . . . .11670267 . . . . . . . . . . . . . .11670270 . . . . . . . . . . . . . .11670273 . . . . . . . . . . . . . .11670277 . . . . . . . . . . . . . .11670279 . . . . . . . . . . . . . .11670281 . . . . . . . . . . . . . .11670282 . . . . . . . . . . . . . .11670283 . . . . . . . . . . . . . .11670284 . . . . . . . . . . . . . .116

70285 . . . . . . . . . . . . . .11670287 . . . . . . . . . . . . . .11670288 . . . . . . . . . . . . . .11670289 . . . . . . . . . . .81,11970290 . . . . . . . . . . .81,11970291 . . . . . . . . . . .81,11970292 . . . . . . . . . . .81,11970293 . . . . . . . . . . .81,11970294 . . . . . . . . . . .81,11970320 . . . . . . . . . . . . . .11670321 . . . . . . . . . . . . . .11670322 . . . . . . . . . . . . . .11670323 . . . . . . . . . . . . . .11670324 . . . . . . . . . . . . . .11670325 . . . . . . . . . . . . . .11670326 . . . . . . . . . . . . . .11670327 . . . . . . . . . . . . . .11670328 . . . . . . . . . . . . . .11670350 . . . . . . . . . . . . . .11670351 . . . . . . . . . . . . . .11670352 . . . . . . . . . . . . . .11670353 . . . . . . . . . . . . . .11670354 . . . . . . . . . . . . . .11670355 . . . . . . . . . . . . . .11670356 . . . . . . . . . . . . . .11670357 . . . . . . . . . . . . . .11670358 . . . . . . . . . . . . . .11670381 . . . . . . . . . . . . . .11670382 . . . . . . . . . . . . . .11670384 . . . . . . . . . . . . . .11670385 . . . . . . . . . . . . . .11670387 . . . . . . . . . . . . . .11670388 . . . . . . . . . . . . . .11670435 . . . . . . . . . . . . . .11770438 . . . . . . . . . . . . . .11770450 . . . . . . . . . . . . . .11770452 . . . . . . . . . . . . . .11770453 . . . . . . . . . . . . . .11770455 . . . . . . . . . . . . . .11770458 . . . . . . . . . . . . . .11770467 . . . . . . . . . . . . . .11770470 . . . . . . . . . . . . . .11770473 . . . . . . . . . . . . . .11770482 . . . . . . . . . . . . . .11770485 . . . . . . . . . . . . . .11770488 . . . . . . . . . . . . . .11770552 . . . . . . . . . . . . . .11770555 . . . . . . . . . . . . . .11770558 . . . . . . . . . . . . . .11770567 . . . . . . . . . . . . . .11770569 . . . . . . . . . . . . . .11770570 . . . . . . . . . . . . . .11770573 . . . . . . . . . . . . . .11770605 . . . . . . . . . . . . . .11870608 . . . . . . . . . . . . . .11870611 . . . . . . . . . . . . . .11870620 . . . . . . . . . . . . . .11870621 . . . . . . . . . . . . . .11870622 . . . . . . . . . . . . . .11870623 . . . . . . . . . . . . . .11870624 . . . . . . . . . . . . . .11870625 . . . . . . . . . . . . . .11870626 . . . . . . . . . . . . . .11870627 . . . . . . . . . . . . . .11870628 . . . . . . . . . . . . . .11870635 . . . . . . . . . . . . . .11870636 . . . . . . . . . . . . . .11870637 . . . . . . . . . . . . . .11870638 . . . . . . . . . . . . . .11870639 . . . . . . . . . . . . . .11870640 . . . . . . . . . . . . . .11870641 . . . . . . . . . . . . . .11870642 . . . . . . . . . . . . . .11870643 . . . . . . . . . . . . . .11870651 . . . . . . . . . . . . . .11870652 . . . . . . . . . . . . . .11870654 . . . . . . . . . . . . . .11870655 . . . . . . . . . . . . . .11870657 . . . . . . . . . . . . . .11870658 . . . . . . . . . . . . . .11870666 . . . . . . . . . . . . . .11870667 . . . . . . . . . . . . . .118

70669 . . . . . . . . . . . . . .11870670 . . . . . . . . . . . . . .11870672 . . . . . . . . . . . . . .11870900 . . . . . . . . . . . . . .12170903 . . . . . . . . . . . . . .12170908 . . . . . . . . . . . . . .12170909 . . . . . . . . . . . . . .12170910 . . . . . . . . . . . . . .12170915 . . . . . . . . . . . . . .12170916 . . . . . . . . . . . . . .12170919 . . . . . . . . . . . . . .12170920 . . . . . . . . . . . . . .12170921 . . . . . . . . . . . . . .12170922 . . . . . . . . . . . . . .12170923 . . . . . . . . . . . . . .12170924 . . . . . . . . . . . . . .12170925 . . . . . . . . . . . . . .12170926 . . . . . . . . . . . . . .12170927 . . . . . . . . . . . . . .12170928 . . . . . . . . . . . . . .12170929 . . . . . . . . . . . . . .12170968 . . . . . . . . . . . . . .12170969 . . . . . . . . . . . . . .12170971 . . . . . . . . . . . . . .12170973 . . . . . . . . . . . . . .12171811 . . . . . . . . . . . . . .11571812 . . . . . . . . . . . . . .11571813 . . . . . . . . . . . . . .11571814 . . . . . . . . . . . . . .11571815 . . . . . . . . . . . . . .11571816 . . . . . . . . . . . . . .11571821 . . . . . . . . . . . . . .11671822 . . . . . . . . . . . . . .11671823 . . . . . . . . . . . . . .11671824 . . . . . . . . . . . . . .11671825 . . . . . . . . . . . . . .11671826 . . . . . . . . . . . . . .11671891 . . . . . . . . . . . . . .12171892 . . . . . . . . . . . . . .12171893 . . . . . . . . . . . . . .12171894 . . . . . . . . . . . . . .12172020 . . . . . . . . . . . . . .11872021 . . . . . . . . . . . . . .11872022 . . . . . . . . . . . . . .11872023 . . . . . . . . . . . . . .11872024 . . . . . . . . . . . . . .11872025 . . . . . . . . . . . . . .11872026 . . . . . . . . . . . . . .11872027 . . . . . . . . . . . . . .11872028 . . . . . . . . . . . . . .11872037 . . . . . . . . . . . . . .11872040 . . . . . . . . . . . . . .11872043 . . . . . . . . . . . . . .11872050 . . . . . . . . . . . . . .11872051 . . . . . . . . . . . . . .11872052 . . . . . . . . . . . . . .11872053 . . . . . . . . . . . . . .11872054 . . . . . . . . . . . . . .11872055 . . . . . . . . . . . . . .11872056 . . . . . . . . . . . . . .11872057 . . . . . . . . . . . . . .11872058 . . . . . . . . . . . . . .11872066 . . . . . . . . . . . . . .11872067 . . . . . . . . . . . . . .11872069 . . . . . . . . . . . . . .11872070 . . . . . . . . . . . . . .11872072 . . . . . . . . . . . . . .11872073 . . . . . . . . . . . . . .11872082 . . . . . . . . . . . . . .11872085 . . . . . . . . . . . . . .11872088 . . . . . . . . . . . . . .11875035 . . . . . . . . . . . . . .11875038 . . . . . . . . . . . . . .11875050 . . . . . . . . . . . . . .11875052 . . . . . . . . . . . . . .11875053 . . . . . . . . . . . . . .11875055 . . . . . . . . . . . . . .11875058 . . . . . . . . . . . . . .11875067 . . . . . . . . . . . . . .11875070 . . . . . . . . . . . . . .11875073 . . . . . . . . . . . . . .11875082 . . . . . . . . . . . . . .118

75085 . . . . . . . . . . . . . .11875088 . . . . . . . . . . . . . .11876020 . . . . . . . . . . . . . .11776021 . . . . . . . . . . . . . .11776022 . . . . . . . . . . . . . .11776023 . . . . . . . . . . . . . .11776024 . . . . . . . . . . . . . .11776025 . . . . . . . . . . . . . .11776026 . . . . . . . . . . . . . .11776027 . . . . . . . . . . . . . .11776028 . . . . . . . . . . . . . .11776050 . . . . . . . . . . . . . .11776051 . . . . . . . . . . . . . .11776052 . . . . . . . . . . . . . .11776053 . . . . . . . . . . . . . .11776054 . . . . . . . . . . . . . .11776055 . . . . . . . . . . . . . .11776056 . . . . . . . . . . . . . .11776057 . . . . . . . . . . . . . .11776058 . . . . . . . . . . . . . .11776066 . . . . . . . . . . . . . .11776067 . . . . . . . . . . . . . .11776069 . . . . . . . . . . . . . .11776070 . . . . . . . . . . . . . .11776072 . . . . . . . . . . . . . .11776073 . . . . . . . . . . . . . .11776082 . . . . . . . . . . . . . .11776085 . . . . . . . . . . . . . .11776088 . . . . . . . . . . . . . .11777005 . . . . . . . . . . . . . .11977007 . . . . . . . . . . . . . .11977008 . . . . . . . . . . . . . .11977010 . . . . . . . . . . . . . .11977020 . . . . . . . . . . . . . .11777023 . . . . . . . . . . . . . .11777035 . . . . . . . . . . . . . .11777038 . . . . . . . . . . . . . .11777050 . . . . . . . . . . . . . .11777053 . . . . . . . . . . . . . .11779712 . . . . . . . . . . . . . .11079712-273 . . . . . . . . . .11079714 . . . . . . . . . . . . . .10879714-273 . . . . . . . . . .10879716 . . . . . . . . . . . . . .11079716-273 . . . . . . . . . .11079717 . . . . . . . . . . . . . .10979718 . . . . . . . . . . . . . .11079723 . . . . . . . . . . . . . .10979723-273 . . . . . . . . . .10980000- . . . . . . . . . . . . .12680105- . . . . . . . . . . . . .12780106- . . . . . . . . . . . . .12780107- . . . . . . . . . . . . .12780111- . . . . . . . . . . . . .12780116- . . . . . . . . . . . . .12780121- . . . . . . . . . . . . .12780122- . . . . . . . . . . . . .12780125- . . . . . . . . . . . . .12680126- . . . . . . . . . . . . .12680127- . . . . . . . . . . . . .12780128- . . . . . . . . . . . . .12680129- . . . . . . . . . . . . .12680205- . . . . . . . . . . . . .12780206- . . . . . . . . . . . . .12780207- . . . . . . . . . . . . .12780211- . . . . . . . . . . . . .12780216- . . . . . . . . . . . . .12780305- . . . . . . . . . . . . .12780311- . . . . . . . . . . . . .12780400- . . . . . . . . . . . . .12680401- . . . . . . . . . . . . .12680405- . . . . . . . . . . . . .12680409- . . . . . . . . . . . . .12680415- . . . . . . . . . . . . .12680416- . . . . . . . . . . . . .12680417- . . . . . . . . . . . . .12680420- . . . . . . . . . . . . .12680425- . . . . . . . . . . . . .12680426- . . . . . . . . . . . . .12680427- . . . . . . . . . . . . .12680428- . . . . . . . . . . . . .12780429- . . . . . . . . . . . . .127

80430- . . . . . . . . . . . . .12780433- . . . . . . . . . . . . .12680434- . . . . . . . . . . . . .12680435- . . . . . . . . . . . . .12680439- . . . . . . . . . . . . .12780440- . . . . . . . . . . . . .12780441- . . . . . . . . . . . . .12680442- . . . . . . . . . . . . .12680443- . . . . . . . . . . . . .12680444- . . . . . . . . . . . . .12680445- . . . . . . . . . . . . .12680446- . . . . . . . . . . . . .12680447- . . . . . . . . . . . . .12680448- . . . . . . . . . . . . .12680449- . . . . . . . . . . . . .12680450- . . . . . . . . . . . . .12680451- . . . . . . . . . . . . .12780452- . . . . . . . . . . . . .12780453- . . . . . . . . . . . . .12780454- . . . . . . . . . . . . .12780455- . . . . . . . . . . . . .12780456- . . . . . . . . . . . . .12780457- . . . . . . . . . . . . .12780458- . . . . . . . . . . . . .12780459- . . . . . . . . . . . . .12780460- . . . . . . . . . . . . .12780461- . . . . . . . . . . . . .12680462- . . . . . . . . . . . . .12680463- . . . . . . . . . . . . .12680464- . . . . . . . . . . . . .12680465- . . . . . . . . . . . . .12680466- . . . . . . . . . . . . .12680467- . . . . . . . . . . . . .12680468- . . . . . . . . . . . . .12680469- . . . . . . . . . . . . .12680470- . . . . . . . . . . . . .12680471- . . . . . . . . . . . . .12680472- . . . . . . . . . . . . .12680473- . . . . . . . . . . . . .12780474- . . . . . . . . . . . . .12780475- . . . . . . . . . . . . .12780476- . . . . . . . . . . . . .12780477- . . . . . . . . . . . . .12680478- . . . . . . . . . . . . .12680479- . . . . . . . . . . . . .12680480- . . . . . . . . . . . . .12780482- . . . . . . . . . . . . .13180483- . . . . . . . . . . . . .13180484- . . . . . . . . . . . . .13180485- . . . . . . . . . . . . .13180486- . . . . . . . . . . . . .13083606- . . . . . . . . . . . . .12888012- . . . . . . . . . . . . .12788013- . . . . . . . . . . . . .12788014- . . . . . . . . . . . . .12788015- . . . . . . . . . . . . .1279100311 . . . . . . . . . . . .1889100312 . . . . . . . . . . . .1889100313 . . . . . . . . . . . .1889100315 . . . . . . . . . . . .1889100331 . . . . . . . . . . . .1889100332 . . . . . . . . . . . .1889100333 . . . . . . . . . . . .1889100335 . . . . . . . . . . . .1889100351 . . . . . . . . . . . .1889100352 . . . . . . . . . . . .1889100353 . . . . . . . . . . . .1889100355 . . . . . . . . . . . .18891005 . . . . . . . . . . . . . .194910050210 . . . . . .188,198910050212 . . . . . .188,198910050220 . . . . . .188,198910050222 . . . . . .188,1989100510 . . . . . . . . . . . .1889100511 . . . . . . . . . . . .1889100512 . . . . . . . . . . . .1889100513 . . . . . . . . . . . .1889100515 . . . . . . . . . . . .1889100517 . . . . . . . . . . . .1889100518 . . . . . . . . . . . .1889100519 . . . . . . . . . . . .1889100521 . . . . . . . . . . . .188

9100522 . . . . . . . . . . . .1889100523 . . . . . . . . . . . .1889100525 . . . . . . . . . . . .1889100531 . . . . . . . . . . . .1889100532 . . . . . . . . . . . .1889100533 . . . . . . . . . . . .1889100535 . . . . . . . . . . . .1889100550 . . . . . . . . . . . .1889100551 . . . . . . . . . . . .1889100552 . . . . . . . . . . . .1889100553 . . . . . . . . . . . .1889100555 . . . . . . . . . . . .1889100557 . . . . . . . . . . . .1889100558 . . . . . . . . . . . .1889100559 . . . . . . . . . . . .1889100560 . . . . . . . . . . . .1889100561 . . . . . . . . . . . .1889100562 . . . . . . . . . . . .1889100563 . . . . . . . . . . . .1889100565 . . . . . . . . . . . .1889100567 . . . . . . . . . . . .1889100568 . . . . . . . . . . . .1889100569 . . . . . . . . . . . .1889100570 . . . . . . . . . . . .1889100572 . . . . . . . . . . . .1889100573 . . . . . . . . . . . .1889100575 . . . . . . . . . . . .1889100577 . . . . . . . . . . . .1889100578 . . . . . . . . . . . .1889100579 . . . . . . . . . . . .1889101311 . . . . . . . . . . . .1859101312 . . . . . . . . . . . .1859101313 . . . . . . . . . . . .1859101315 . . . . . . . . . . . .1859101331 . . . . . . . . . . . .1859101332 . . . . . . . . . . . .1859101333 . . . . . . . . . . . .1859101335 . . . . . . . . . . . .1859101351 . . . . . . . . . . . .1859101352 . . . . . . . . . . . .1859101353 . . . . . . . . . . . .1859101355 . . . . . . . . . . . .18591015 . . . . . . . . . . . . . .194910150210 . . . . . .185,198910150212 . . . . . .185,198910150220 . . . . . .185,198910150222 . . . . . .185,1989101511 . . . . . . . . . . . .1859101512 . . . . . . . . . . . .1859101513 . . . . . . . . . . . .1859101515 . . . . . . . . . . . .1859101521 . . . . . . . . . . . .1859101522 . . . . . . . . . . . .1859101523 . . . . . . . . . . . .1859101525 . . . . . . . . . . . .1859101531 . . . . . . . . . . . .1859101532 . . . . . . . . . . . .1859101533 . . . . . . . . . . . .1859101535 . . . . . . . . . . . .1859101551 . . . . . . . . . . . .1859101552 . . . . . . . . . . . .1859101553 . . . . . . . . . . . .1859101555 . . . . . . . . . . . .1859101561 . . . . . . . . . . . .1859101562 . . . . . . . . . . . .1859101563 . . . . . . . . . . . .1859101565 . . . . . . . . . . . .1859101571 . . . . . . . . . . . .1859101572 . . . . . . . . . . . .1859101573 . . . . . . . . . . . .1859101575 . . . . . . . . . . . .1859102311 . . . . . . . . . . . .1849102312 . . . . . . . . . . . .1849102313 . . . . . . . . . . . .1849102315 . . . . . . . . . . . .1849102331 . . . . . . . . . . . .1849102332 . . . . . . . . . . . .1849102333 . . . . . . . . . . . .1849102335 . . . . . . . . . . . .1849102351 . . . . . . . . . . . .1849102352 . . . . . . . . . . . .1849102353 . . . . . . . . . . . .184


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INDEX

Catalog #9102355 . . . . . . . . . . . .18491025 . . . . . . . . . . . . . .194910250210 . . . . . .184,198910250212 . . . . . .184,198910250220 . . . . . .184,198910250222 . . . . . .184,1989102511 . . . . . . . . . . . .1849102512 . . . . . . . . . . . .1849102513 . . . . . . . . . . . .1849102515 . . . . . . . . . . . .1849102521 . . . . . . . . . . . .1849102522 . . . . . . . . . . . .1849102523 . . . . . . . . . . . .1849102525 . . . . . . . . . . . .1849102531 . . . . . . . . . . . .1849102532 . . . . . . . . . . . .1849102533 . . . . . . . . . . . .1849102535 . . . . . . . . . . . .1849102551 . . . . . . . . . . . .1849102552 . . . . . . . . . . . .1849102553 . . . . . . . . . . . .1849102555 . . . . . . . . . . . .1849102561 . . . . . . . . . . . .1849102562 . . . . . . . . . . . .1849102563 . . . . . . . . . . . .1849102565 . . . . . . . . . . . .1849102571 . . . . . . . . . . . .1849102572 . . . . . . . . . . . .1849102573 . . . . . . . . . . . .1849102575 . . . . . . . . . . . .1849103311 . . . . . . . . . . . .1839103312 . . . . . . . . . . . .1839103313 . . . . . . . . . . . .1839103315 . . . . . . . . . . . .1839103331 . . . . . . . . . . . .1839103332 . . . . . . . . . . . .1839103333 . . . . . . . . . . . .1839103335 . . . . . . . . . . . .1839103351 . . . . . . . . . . . .1839103352 . . . . . . . . . . . .1839103353 . . . . . . . . . . . .1839103355 . . . . . . . . . . . .18391035 . . . . . . . . . . . . . .194910350210 . . . . . .183,198910350212 . . . . . .183,198910350220 . . . . . .183,198910350222 . . . . . .183,1989103510 . . . . . . . . . . . .1839103511 . . . . . . . . . . . .1839103512 . . . . . . . . . . . .1839103513 . . . . . . . . . . . .1839103515 . . . . . . . . . . . .1839103517 . . . . . . . . . . . .1839103518 . . . . . . . . . . . .1839103519 . . . . . . . . . . . .1839103521 . . . . . . . . . . . .1839103522 . . . . . . . . . . . .1839103523 . . . . . . . . . . . .1839103525 . . . . . . . . . . . .1839103531 . . . . . . . . . . . .1839103532 . . . . . . . . . . . .1839103533 . . . . . . . . . . . .1839103535 . . . . . . . . . . . .1839103550 . . . . . . . . . . . .1839103551 . . . . . . . . . . . .1839103552 . . . . . . . . . . . .1839103553 . . . . . . . . . . . .1839103555 . . . . . . . . . . . .1839103557 . . . . . . . . . . . .1839103558 . . . . . . . . . . . .1839103559 . . . . . . . . . . . .1839103560 . . . . . . . . . . . .1839103561 . . . . . . . . . . . .1839103562 . . . . . . . . . . . .1839103563 . . . . . . . . . . . .1839103565 . . . . . . . . . . . .1839103567 . . . . . . . . . . . .1839103568 . . . . . . . . . . . .1839103569 . . . . . . . . . . . .1839103570 . . . . . . . . . . . .1839103571 . . . . . . . . . . . .1839103572 . . . . . . . . . . . .183

9103573 . . . . . . . . . . . .1839103575 . . . . . . . . . . . .1839103577 . . . . . . . . . . . .1839103578 . . . . . . . . . . . .1839103579 . . . . . . . . . . . .1839105311 . . . . . . . . . . . .1869105312 . . . . . . . . . . . .1869105313 . . . . . . . . . . . .1869105315 . . . . . . . . . . . .1869105331 . . . . . . . . . . . .1869105332 . . . . . . . . . . . .1869105333 . . . . . . . . . . . .1869105335 . . . . . . . . . . . .1869105351 . . . . . . . . . . . .1869105352 . . . . . . . . . . . .1869105353 . . . . . . . . . . . .1869105355 . . . . . . . . . . . .18691055 . . . . . . . . . . . . . .194910550210 . . . . . .186,198910550212 . . . . . .186,198910550220 . . . . . .186,198910550222 . . . . . .186,1989105510 . . . . . . . . . . . .1869105511 . . . . . . . . . . . .1869105512 . . . . . . . . . . . .1869105513 . . . . . . . . . . . .1869105515 . . . . . . . . . . . .1869105517 . . . . . . . . . . . .1869105518 . . . . . . . . . . . .1869105519 . . . . . . . . . . . .1869105521 . . . . . . . . . . . .1869105522 . . . . . . . . . . . .1869105523 . . . . . . . . . . . .1869105525 . . . . . . . . . . . .1869105531 . . . . . . . . . . . .1869105532 . . . . . . . . . . . .1869105533 . . . . . . . . . . . .1869105535 . . . . . . . . . . . .1869105550 . . . . . . . . . . . .1869105551 . . . . . . . . . . . .1869105552 . . . . . . . . . . . .1869105553 . . . . . . . . . . . .1869105555 . . . . . . . . . . . .1869105557 . . . . . . . . . . . .1869105558 . . . . . . . . . . . .1869105559 . . . . . . . . . . . .1869105560 . . . . . . . . . . . .1869105561 . . . . . . . . . . . .1869105562 . . . . . . . . . . . .1869105563 . . . . . . . . . . . .1869105565 . . . . . . . . . . . .1869105567 . . . . . . . . . . . .1869105568 . . . . . . . . . . . .1869105569 . . . . . . . . . . . .1869105570 . . . . . . . . . . . .1869105571 . . . . . . . . . . . .1869105572 . . . . . . . . . . . .1869105573 . . . . . . . . . . . .1869105575 . . . . . . . . . . . .1869105577 . . . . . . . . . . . .1869105578 . . . . . . . . . . . .1869105579 . . . . . . . . . . . .1869106311 . . . . . . . . . . . .1859106312 . . . . . . . . . . . .1859106313 . . . . . . . . . . . .1859106315 . . . . . . . . . . . .1859106331 . . . . . . . . . . . .1859106332 . . . . . . . . . . . .1859106333 . . . . . . . . . . . .1859106335 . . . . . . . . . . . .1859106351 . . . . . . . . . . . .1859106352 . . . . . . . . . . . .1859106353 . . . . . . . . . . . .1859106355 . . . . . . . . . . . .18591065 . . . . . . . . . . . . . .194910650210 . . . . . .185,198910650212 . . . . . .185,198910650220 . . . . . .185,198910650222 . . . . . .185,1989106510 . . . . . . . . . . . .1859106511 . . . . . . . . . . . .1859106512 . . . . . . . . . . . .185

9106513 . . . . . . . . . . . .1859106515 . . . . . . . . . . . .1859106517 . . . . . . . . . . . .1859106518 . . . . . . . . . . . .1859106519 . . . . . . . . . . . .1859106521 . . . . . . . . . . . .1859106522 . . . . . . . . . . . .1859106523 . . . . . . . . . . . .1859106525 . . . . . . . . . . . .1859106531 . . . . . . . . . . . .1859106532 . . . . . . . . . . . .1859106533 . . . . . . . . . . . .1859106535 . . . . . . . . . . . .1859106550 . . . . . . . . . . . .1859106551 . . . . . . . . . . . .1859106552 . . . . . . . . . . . .1859106553 . . . . . . . . . . . .1859106555 . . . . . . . . . . . .1859106557 . . . . . . . . . . . .1859106558 . . . . . . . . . . . .1859106559 . . . . . . . . . . . .1859106560 . . . . . . . . . . . .1859106561 . . . . . . . . . . . .1859106562 . . . . . . . . . . . .1859106563 . . . . . . . . . . . .1859106565 . . . . . . . . . . . .1859106567 . . . . . . . . . . . .1859106568 . . . . . . . . . . . .1859106569 . . . . . . . . . . . .1859106570 . . . . . . . . . . . .1859106571 . . . . . . . . . . . .1859106572 . . . . . . . . . . . .1859106573 . . . . . . . . . . . .1859106575 . . . . . . . . . . . .1859106577 . . . . . . . . . . . .1859106578 . . . . . . . . . . . .1859106579 . . . . . . . . . . . .1859107311 . . . . . . . . . . . .1869107312 . . . . . . . . . . . .1869107313 . . . . . . . . . . . .1869107315 . . . . . . . . . . . .1869107331 . . . . . . . . . . . .1869107332 . . . . . . . . . . . .1869107333 . . . . . . . . . . . .1869107335 . . . . . . . . . . . .1869107351 . . . . . . . . . . . .1869107352 . . . . . . . . . . . .1869107353 . . . . . . . . . . . .1869107355 . . . . . . . . . . . .18691075 . . . . . . . . . . . . . .194910750210 . . . . . .186,198910750212 . . . . . .186,198910750220 . . . . . .186,198910750222 . . . . . .186,1989107511 . . . . . . . . . . . .1869107512 . . . . . . . . . . . .1869107513 . . . . . . . . . . . .1869107515 . . . . . . . . . . . .1869107521 . . . . . . . . . . . .1869107522 . . . . . . . . . . . .1869107523 . . . . . . . . . . . .1869107525 . . . . . . . . . . . .1869107531 . . . . . . . . . . . .1869107532 . . . . . . . . . . . .1869107533 . . . . . . . . . . . .1869107535 . . . . . . . . . . . .1869107551 . . . . . . . . . . . .1869107552 . . . . . . . . . . . .1869107553 . . . . . . . . . . . .1869107555 . . . . . . . . . . . .1869107561 . . . . . . . . . . . .1869107562 . . . . . . . . . . . .1869107563 . . . . . . . . . . . .1869107565 . . . . . . . . . . . .1869107571 . . . . . . . . . . . .1869107572 . . . . . . . . . . . .1869107573 . . . . . . . . . . . .1869107575 . . . . . . . . . . . .186915950210 . . . . . .181,1989159523-700 . . . . . . . .1819159525-700 . . . . . . . .181916050210 . . . . . .181,198

916050212 . . . . . .181,198916050220 . . . . . .181,198916050222 . . . . . .181,1989160510 . . . . . . . . . . . .1819160511 . . . . . . . . . . . .1819160512 . . . . . . . . . . . .1819160513 . . . . . . . . . . . .1819160515 . . . . . . . . . . . .1819160517 . . . . . . . . . . . .1819160518 . . . . . . . . . . . .1819160519 . . . . . . . . . . . .1819160521 . . . . . . . . . . . .1819160522 . . . . . . . . . . . .1819160523 . . . . . . . . . . . .1819160525 . . . . . . . . . . . .1819160531 . . . . . . . . . . . .1819160532 . . . . . . . . . . . .1819160533 . . . . . . . . . . . .1819160535 . . . . . . . . . . . .1819160550 . . . . . . . . . . . .1819160551 . . . . . . . . . . . .1819160552 . . . . . . . . . . . .1819160553 . . . . . . . . . . . .1819160555 . . . . . . . . . . . .1819160557 . . . . . . . . . . . .1819160558 . . . . . . . . . . . .1819160559 . . . . . . . . . . . .1819160560 . . . . . . . . . . . .1819160561 . . . . . . . . . . . .1819160562 . . . . . . . . . . . .1819160563 . . . . . . . . . . . .1819160565 . . . . . . . . . . . .1819160567 . . . . . . . . . . . .1819160568 . . . . . . . . . . . .1819160569 . . . . . . . . . . . .1819160570 . . . . . . . . . . . .1819160571 . . . . . . . . . . . .1819160572 . . . . . . . . . . . .1819160573 . . . . . . . . . . . .1819160575 . . . . . . . . . . . .1819160577 . . . . . . . . . . . .1819160578 . . . . . . . . . . . .1819160579 . . . . . . . . . . . .181916150210 . . . . . .178,198916150212 . . . . . .178,198916150220 . . . . . .178,198916150222 . . . . . .178,1989161510 . . . . . . . . . . . .1789161511 . . . . . . . . . . . .1789161512 . . . . . . . . . . . .1789161513 . . . . . . . . . . . .1789161515 . . . . . . . . . . . .1789161517 . . . . . . . . . . . .1789161518 . . . . . . . . . . . .1789161519 . . . . . . . . . . . .1789161521 . . . . . . . . . . . .1789161522 . . . . . . . . . . . .1789161523 . . . . . . . . . . . .1789161525 . . . . . . . . . . . .1789161531 . . . . . . . . . . . .1789161532 . . . . . . . . . . . .1789161533 . . . . . . . . . . . .1789161535 . . . . . . . . . . . .1789161550 . . . . . . . . . . . .1789161551 . . . . . . . . . . . .1789161552 . . . . . . . . . . . .1789161553 . . . . . . . . . . . .1789161555 . . . . . . . . . . . .1789161557 . . . . . . . . . . . .1789161558 . . . . . . . . . . . .1789161559 . . . . . . . . . . . .1789161560 . . . . . . . . . . . .1789161561 . . . . . . . . . . . .1789161562 . . . . . . . . . . . .1789161563 . . . . . . . . . . . .1789161565 . . . . . . . . . . . .1789161567 . . . . . . . . . . . .1789161568 . . . . . . . . . . . .1789161569 . . . . . . . . . . . .1789161570 . . . . . . . . . . . .1789161571 . . . . . . . . . . . .1789161572 . . . . . . . . . . . .178

9161573 . . . . . . . . . . . .1789161575 . . . . . . . . . . . .1789161577 . . . . . . . . . . . .1789161578 . . . . . . . . . . . .1789161579 . . . . . . . . . . . .178916450210 . . . . . .178,198916450212 . . . . . .178,198916450220 . . . . . .178,198916450222 . . . . . .178,1989164510 . . . . . . . . . . . .1789164511 . . . . . . . . . . . .1789164512 . . . . . . . . . . . .1789164513 . . . . . . . . . . . .1789164515 . . . . . . . . . . . .1789164517 . . . . . . . . . . . .1789164518 . . . . . . . . . . . .1789164519 . . . . . . . . . . . .1789164521 . . . . . . . . . . . .1789164522 . . . . . . . . . . . .1789164523 . . . . . . . . . . . .1789164525 . . . . . . . . . . . .1789164531 . . . . . . . . . . . .1789164532 . . . . . . . . . . . .1789164533 . . . . . . . . . . . .1789164535 . . . . . . . . . . . .1789164550 . . . . . . . . . . . .1789164551 . . . . . . . . . . . .1789164552 . . . . . . . . . . . .1789164553 . . . . . . . . . . . .1789164555 . . . . . . . . . . . .1789164557 . . . . . . . . . . . .1789164558 . . . . . . . . . . . .1789164559 . . . . . . . . . . . .1789164560 . . . . . . . . . . . .1789164561 . . . . . . . . . . . .1789164562 . . . . . . . . . . . .1789164563 . . . . . . . . . . . .1789164565 . . . . . . . . . . . .1789164567 . . . . . . . . . . . .1789164568 . . . . . . . . . . . .1789164569 . . . . . . . . . . . .1789164570 . . . . . . . . . . . .1789164571 . . . . . . . . . . . .1789164572 . . . . . . . . . . . .1789164573 . . . . . . . . . . . .1789164575 . . . . . . . . . . . .1789164577 . . . . . . . . . . . .1789164578 . . . . . . . . . . . .1789164579 . . . . . . . . . . . .178916550210 . . . . . .180,198916550212 . . . . . .180,198916550220 . . . . . .180,198916550222 . . . . . .180,1989165563 . . . . . . . . . . . .1809165565 . . . . . . . . . . . .1809165575 . . . . . . . . . . . .1809165585 . . . . . . . . . . . .180916650210 . . . . . .180,198916650212 . . . . . .180,198916650220 . . . . . .180,198916650222 . . . . . .180,1989166510 . . . . . . . . . . . .1809166511 . . . . . . . . . . . .1809166512 . . . . . . . . . . . .1809166513 . . . . . . . . . . . .1809166515 . . . . . . . . . . . .1809166517 . . . . . . . . . . . .1809166518 . . . . . . . . . . . .1809166519 . . . . . . . . . . . .1809166521 . . . . . . . . . . . .1809166522 . . . . . . . . . . . .1809166523 . . . . . . . . . . . .1809166525 . . . . . . . . . . . .1809166531 . . . . . . . . . . . .1809166532 . . . . . . . . . . . .1809166533 . . . . . . . . . . . .1809166535 . . . . . . . . . . . .1809166550 . . . . . . . . . . . .1809166551 . . . . . . . . . . . .1809166552 . . . . . . . . . . . .1809166553 . . . . . . . . . . . .1809166555 . . . . . . . . . . . .180

9166557 . . . . . . . . . . . .1809166558 . . . . . . . . . . . .1809166559 . . . . . . . . . . . .1809166560 . . . . . . . . . . . .1809166561 . . . . . . . . . . . .1809166562 . . . . . . . . . . . .1809166563 . . . . . . . . . . . .1809166565 . . . . . . . . . . . .1809166567 . . . . . . . . . . . .1809166568 . . . . . . . . . . . .1809166569 . . . . . . . . . . . .1809166570 . . . . . . . . . . . .1809166571 . . . . . . . . . . . .1809166572 . . . . . . . . . . . .1809166573 . . . . . . . . . . . .1809166575 . . . . . . . . . . . .1809166577 . . . . . . . . . . . .1809166578 . . . . . . . . . . . .1809166579 . . . . . . . . . . . .180916850210 . . . . . .179,198916850212 . . . . . .179,198916850220 . . . . . .179,198916850222 . . . . . .179,1989168511 . . . . . . . . . . . .1799168512 . . . . . . . . . . . .1799168513 . . . . . . . . . . . .1799168515 . . . . . . . . . . . .1799168521 . . . . . . . . . . . .1799168522 . . . . . . . . . . . .1799168523 . . . . . . . . . . . .1799168525 . . . . . . . . . . . .1799168531 . . . . . . . . . . . .1799168532 . . . . . . . . . . . .1799168533 . . . . . . . . . . . .1799168535 . . . . . . . . . . . .1799168551 . . . . . . . . . . . .1799168552 . . . . . . . . . . . .1799168553 . . . . . . . . . . . .1799168555 . . . . . . . . . . . .1799168561 . . . . . . . . . . . .1799168562 . . . . . . . . . . . .1799168563 . . . . . . . . . . . .1799168565 . . . . . . . . . . . .1799168571 . . . . . . . . . . . .1799168572 . . . . . . . . . . . .1799168573 . . . . . . . . . . . .1799168575 . . . . . . . . . . . .179916950210 . . . . . .179,198916950212 . . . . . .179,198916950220 . . . . . .179,198916950222 . . . . . .179,1989169510 . . . . . . . . . . . .1799169511 . . . . . . . . . . . .1799169512 . . . . . . . . . . . .1799169513 . . . . . . . . . . . .1799169515 . . . . . . . . . . . .1799169517 . . . . . . . . . . . .1799169518 . . . . . . . . . . . .1799169519 . . . . . . . . . . . .1799169521 . . . . . . . . . . . .1799169522 . . . . . . . . . . . .1799169523 . . . . . . . . . . . .1799169525 . . . . . . . . . . . .1799169531 . . . . . . . . . . . .1799169532 . . . . . . . . . . . .1799169533 . . . . . . . . . . . .1799169535 . . . . . . . . . . . .1799169550 . . . . . . . . . . . .1799169551 . . . . . . . . . . . .1799169552 . . . . . . . . . . . .1799169553 . . . . . . . . . . . .1799169555 . . . . . . . . . . . .1799169557 . . . . . . . . . . . .1799169558 . . . . . . . . . . . .1799169559 . . . . . . . . . . . .1799169560 . . . . . . . . . . . .1799169561 . . . . . . . . . . . .1799169562 . . . . . . . . . . . .1799169563 . . . . . . . . . . . .1799169565 . . . . . . . . . . . .1799169567 . . . . . . . . . . . .1799169568 . . . . . . . . . . . .179


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INDEX

Catalog #9169569 . . . . . . . . . . . .1799169570 . . . . . . . . . . . .1799169571 . . . . . . . . . . . .1799169572 . . . . . . . . . . . .1799169573 . . . . . . . . . . . .1799169575 . . . . . . . . . . . .1799169577 . . . . . . . . . . . .1799169578 . . . . . . . . . . . .1799169579 . . . . . . . . . . . .1799174311 . . . . . . . . . . . .1829174312 . . . . . . . . . . . .1829174313 . . . . . . . . . . . .1829174315 . . . . . . . . . . . .1829174331 . . . . . . . . . . . .1829174332 . . . . . . . . . . . .1829174333 . . . . . . . . . . . .1829174335 . . . . . . . . . . . .1829174351 . . . . . . . . . . . .1829174352 . . . . . . . . . . . .1829174353 . . . . . . . . . . . .1829174355 . . . . . . . . . . . .182917436B . . . . . . . . . . . .18291745 . . . . . . . . . . . . . .194917450210 . . . . . .182,198917450212 . . . . . .182,198917450220 . . . . . .182,198917450222 . . . . . .182,1989174510 . . . . . . . . . . . .1829174511 . . . . . . . . . . . .1829174512 . . . . . . . . . . . .1829174513 . . . . . . . . . . . .1829174514 . . . . . . . . . . . .1829174515 . . . . . . . . . . . .1829174517 . . . . . . . . . . . .1829174518 . . . . . . . . . . . .1829174519 . . . . . . . . . . . .1829174521 . . . . . . . . . . . .1829174522 . . . . . . . . . . . .1829174523 . . . . . . . . . . . .1829174525 . . . . . . . . . . . .1829174531 . . . . . . . . . . . .1829174532 . . . . . . . . . . . .1829174533 . . . . . . . . . . . .1829174535 . . . . . . . . . . . .1829174550 . . . . . . . . . . . .1829174551 . . . . . . . . . . . .1829174552 . . . . . . . . . . . .1829174553 . . . . . . . . . . . .1829174555 . . . . . . . . . . . .1829174557 . . . . . . . . . . . .1829174558 . . . . . . . . . . . .1829174559 . . . . . . . . . . . .1829174560 . . . . . . . . . . . .1829174561 . . . . . . . . . . . .1829174562 . . . . . . . . . . . .1829174563 . . . . . . . . . . . .1829174564 . . . . . . . . . . . .1829174565 . . . . . . . . . . . .1829174567 . . . . . . . . . . . .1829174568 . . . . . . . . . . . .1829174569 . . . . . . . . . . . .1829174570 . . . . . . . . . . . .1829174571 . . . . . . . . . . . .1829174572 . . . . . . . . . . . .1829174573 . . . . . . . . . . . .1829174575 . . . . . . . . . . . .1829174577 . . . . . . . . . . . .1829174578 . . . . . . . . . . . .1829174579 . . . . . . . . . . . .1829175311 . . . . . . . . . . . .1849175312 . . . . . . . . . . . .1849175313 . . . . . . . . . . . .1849175315 . . . . . . . . . . . .1849175331 . . . . . . . . . . . .1849175332 . . . . . . . . . . . .1849175333 . . . . . . . . . . . .1849175335 . . . . . . . . . . . .1849175351 . . . . . . . . . . . .1849175352 . . . . . . . . . . . .1849175353 . . . . . . . . . . . .1849175355 . . . . . . . . . . . .184917550210 . . . . . .184,198

917550212 . . . . . .184,198917550220 . . . . . .184,198917550222 . . . . . .184,1989175510 . . . . . . . . . . . .1849175511 . . . . . . . . . . . .1849175512 . . . . . . . . . . . .1849175513 . . . . . . . . . . . .1849175515 . . . . . . . . . . . .1849175517 . . . . . . . . . . . .1849175518 . . . . . . . . . . . .1849175519 . . . . . . . . . . . .1849175521 . . . . . . . . . . . .1849175522 . . . . . . . . . . . .1849175523 . . . . . . . . . . . .1849175525 . . . . . . . . . . . .1849175531 . . . . . . . . . . . .1849175532 . . . . . . . . . . . .1849175533 . . . . . . . . . . . .1849175535 . . . . . . . . . . . .1849175550 . . . . . . . . . . . .1849175551 . . . . . . . . . . . .1849175552 . . . . . . . . . . . .1849175553 . . . . . . . . . . . .1849175555 . . . . . . . . . . . .1849175557 . . . . . . . . . . . .1849175558 . . . . . . . . . . . .1849175559 . . . . . . . . . . . .1849175560 . . . . . . . . . . . .1849175561 . . . . . . . . . . . .1849175562 . . . . . . . . . . . .1849175563 . . . . . . . . . . . .1849175565 . . . . . . . . . . . .1849175567 . . . . . . . . . . . .1849175568 . . . . . . . . . . . .1849175569 . . . . . . . . . . . .1849175570 . . . . . . . . . . . .1849175571 . . . . . . . . . . . .1849175572 . . . . . . . . . . . .1849175573 . . . . . . . . . . . .1849175575 . . . . . . . . . . . .1849175577 . . . . . . . . . . . .1849175578 . . . . . . . . . . . .1849175579 . . . . . . . . . . . .1849176311 . . . . . . . . . . . .1879176312 . . . . . . . . . . . .1879176313 . . . . . . . . . . . .1879176315 . . . . . . . . . . . .1879176331 . . . . . . . . . . . .1879176332 . . . . . . . . . . . .1879176333 . . . . . . . . . . . .1879176335 . . . . . . . . . . . .1879176351 . . . . . . . . . . . .1879176352 . . . . . . . . . . . .1879176353 . . . . . . . . . . . .1879176355 . . . . . . . . . . . .187917650210 . . . . . .187,198917650212 . . . . . .187,198917650220 . . . . . .187,198917650222 . . . . . .187,1989176510 . . . . . . . . . . . .1879176511 . . . . . . . . . . . .1879176512 . . . . . . . . . . . .1879176513 . . . . . . . . . . . .1879176515 . . . . . . . . . . . .1879176517 . . . . . . . . . . . .1879176518 . . . . . . . . . . . .1879176519 . . . . . . . . . . . .1879176521 . . . . . . . . . . . .1879176522 . . . . . . . . . . . .1879176523 . . . . . . . . . . . .1879176525 . . . . . . . . . . . .1879176531 . . . . . . . . . . . .1879176532 . . . . . . . . . . . .1879176533 . . . . . . . . . . . .1879176535 . . . . . . . . . . . .1879176550 . . . . . . . . . . . .1879176551 . . . . . . . . . . . .1879176552 . . . . . . . . . . . .1879176553 . . . . . . . . . . . .1879176555 . . . . . . . . . . . .1879176557 . . . . . . . . . . . .1879176558 . . . . . . . . . . . .187

9176559 . . . . . . . . . . . .1879176560 . . . . . . . . . . . .1879176561 . . . . . . . . . . . .1879176562 . . . . . . . . . . . .1879176563 . . . . . . . . . . . .1879176565 . . . . . . . . . . . .1879176567 . . . . . . . . . . . .1879176568 . . . . . . . . . . . .1879176569 . . . . . . . . . . . .1879176570 . . . . . . . . . . . .1879176571 . . . . . . . . . . . .1879176572 . . . . . . . . . . . .1879176573 . . . . . . . . . . . .1879176575 . . . . . . . . . . . .1879176577 . . . . . . . . . . . .1879176578 . . . . . . . . . . . .1879176579 . . . . . . . . . . . .1879177311 . . . . . . . . . . . .1889177312 . . . . . . . . . . . .1889177313 . . . . . . . . . . . .1889177315 . . . . . . . . . . . .1889177351 . . . . . . . . . . . .1889177352 . . . . . . . . . . . .1889177353 . . . . . . . . . . . .1889177354 . . . . . . . . . . . .1889177355 . . . . . . . . . . . .188917750210 . . . . . .188,198917750212 . . . . . .188,198917750220 . . . . . .188,198917750222 . . . . . .188,1989177575 . . . . . . . . . . . .1889178311 . . . . . . . . . . . .1839178312 . . . . . . . . . . . .1839178313 . . . . . . . . . . . .1839178315 . . . . . . . . . . . .1839178331 . . . . . . . . . . . .1839178332 . . . . . . . . . . . .1839178333 . . . . . . . . . . . .1839178335 . . . . . . . . . . . .1839178351 . . . . . . . . . . . .1839178352 . . . . . . . . . . . .1839178353 . . . . . . . . . . . .1839178355 . . . . . . . . . . . .183917850210 . . . . . .183,198917850212 . . . . . .183,198917850220 . . . . . .183,198917850222 . . . . . .183,1989178510 . . . . . . . . . . . .1839178511 . . . . . . . . . . . .1839178512 . . . . . . . . . . . .1839178513 . . . . . . . . . . . .1839178515 . . . . . . . . . . . .1839178517 . . . . . . . . . . . .1839178518 . . . . . . . . . . . .1839178519 . . . . . . . . . . . .1839178521 . . . . . . . . . . . .1839178522 . . . . . . . . . . . .1839178523 . . . . . . . . . . . .1839178525 . . . . . . . . . . . .1839178531 . . . . . . . . . . . .1839178532 . . . . . . . . . . . .1839178533 . . . . . . . . . . . .1839178535 . . . . . . . . . . . .1839178550 . . . . . . . . . . . .1839178551 . . . . . . . . . . . .1839178552 . . . . . . . . . . . .1839178553 . . . . . . . . . . . .1839178555 . . . . . . . . . . . .1839178557 . . . . . . . . . . . .1839178558 . . . . . . . . . . . .1839178559 . . . . . . . . . . . .1839178560 . . . . . . . . . . . .1839178561 . . . . . . . . . . . .1839178562 . . . . . . . . . . . .1839178563 . . . . . . . . . . . .1839178565 . . . . . . . . . . . .1839178567 . . . . . . . . . . . .1839178568 . . . . . . . . . . . .1839178569 . . . . . . . . . . . .1839178570 . . . . . . . . . . . .1839178571 . . . . . . . . . . . .1839178572 . . . . . . . . . . . .183

9178573 . . . . . . . . . . . .1839178575 . . . . . . . . . . . .1839178577 . . . . . . . . . . . .1839178578 . . . . . . . . . . . .1839178579 . . . . . . . . . . . .183918150210 . . . . . .189,198918150212 . . . . . .189,198918150220 . . . . . .189,198918150222 . . . . . .189,1989181565 . . . . . . . . . . . .189920950210 . . . . . .176,198920950220 . . . . . .176,1989209565 . . . . . . . . . . . .1769209575 . . . . . . . . . . . .17692103 . . . . . . . . . . . . . .1949210311 . . . . . . . . . . . .1779210312 . . . . . . . . . . . .1779210313 . . . . . . . . . . . .1779210315 . . . . . . . . . . . .1779210331 . . . . . . . . . . . .1779210332 . . . . . . . . . . . .1779210333 . . . . . . . . . . . .1779210335 . . . . . . . . . . . .1779210351 . . . . . . . . . . . .1779210352 . . . . . . . . . . . .1779210353 . . . . . . . . . . . .1779210355 . . . . . . . . . . . .1779210361 . . . . . . . . . . . .1779210362 . . . . . . . . . . . .1779210363 . . . . . . . . . . . .1779210365 . . . . . . . . . . . .17792105 . . . . . . . . . . . . . .194921050210 . . . . . .177,198921050212 . . . . . .177,198921050220 . . . . . .177,198921050222 . . . . . .177,1989210510 . . . . . . . . . . . .1779210511 . . . . . . . . . . . .1779210512 . . . . . . . . . . . .1779210513 . . . . . . . . . . . .1779210515 . . . . . . . . . . . .1779210517 . . . . . . . . . . . .1779210518 . . . . . . . . . . . .1779210519 . . . . . . . . . . . .1779210521 . . . . . . . . . . . .1779210522 . . . . . . . . . . . .1779210523 . . . . . . . . . . . .1779210525 . . . . . . . . . . . .1779210531 . . . . . . . . . . . .1779210532 . . . . . . . . . . . .1779210533 . . . . . . . . . . . .1779210535 . . . . . . . . . . . .1779210550 . . . . . . . . . . . .1779210551 . . . . . . . . . . . .1779210552 . . . . . . . . . . . .1779210553 . . . . . . . . . . . .1779210555 . . . . . . . . . . . .1779210557 . . . . . . . . . . . .1779210558 . . . . . . . . . . . .1779210559 . . . . . . . . . . . .1779210560 . . . . . . . . . . . .1779210561 . . . . . . . . . . . .1779210562 . . . . . . . . . . . .1779210563 . . . . . . . . . . . .1779210565 . . . . . . . . . . . .1779210567 . . . . . . . . . . . .1779210568 . . . . . . . . . . . .1779210569 . . . . . . . . . . . .1779210570 . . . . . . . . . . . .1779210571 . . . . . . . . . . . .1779210572 . . . . . . . . . . . .1779210573 . . . . . . . . . . . .1779210575 . . . . . . . . . . . .1779210577 . . . . . . . . . . . .1779210578 . . . . . . . . . . . .1779210579 . . . . . . . . . . . .17792133 . . . . . . . . . . . . . .1949213311 . . . . . . . . . . . .1749213312 . . . . . . . . . . . .1749213313 . . . . . . . . . . . .1749213315 . . . . . . . . . . . .1749213331 . . . . . . . . . . . .174

9213332 . . . . . . . . . . . .1749213333 . . . . . . . . . . . .1749213335 . . . . . . . . . . . .1749213351 . . . . . . . . . . . .1749213352 . . . . . . . . . . . .1749213353 . . . . . . . . . . . .1749213355 . . . . . . . . . . . .1749213361 . . . . . . . . . . . .1749213362 . . . . . . . . . . . .1749213363 . . . . . . . . . . . .1749213365 . . . . . . . . . . . .17492135 . . . . . . . . . . . . . .194921350210 . . . . . .174,198921350212 . . . . . .174,198921350220 . . . . . .174,198921350222 . . . . . .174,1989213510 . . . . . . . . . . . .1749213511 . . . . . . . . . . . .1749213512 . . . . . . . . . . . .1749213513 . . . . . . . . . . . .1749213514 . . . . . . . . . . . .1749213515 . . . . . . . . . . . .1749213517 . . . . . . . . . . . .1749213518 . . . . . . . . . . . .1749213519 . . . . . . . . . . . .1749213521 . . . . . . . . . . . .1749213522 . . . . . . . . . . . .1749213523 . . . . . . . . . . . .1749213525 . . . . . . . . . . . .1749213531 . . . . . . . . . . . .1749213532 . . . . . . . . . . . .1749213533 . . . . . . . . . . . .1749213535 . . . . . . . . . . . .1749213550 . . . . . . . . . . . .1749213551 . . . . . . . . . . . .1749213552 . . . . . . . . . . . .1749213553 . . . . . . . . . . . .1749213555 . . . . . . . . . . . .1749213557 . . . . . . . . . . . .1749213558 . . . . . . . . . . . .1749213559 . . . . . . . . . . . .1749213560 . . . . . . . . . . . .1749213561 . . . . . . . . . . . .1749213562 . . . . . . . . . . . .1749213563 . . . . . . . . . . . .1749213564 . . . . . . . . . . . .1749213565 . . . . . . . . . . . .1749213567 . . . . . . . . . . . .1749213568 . . . . . . . . . . . .1749213569 . . . . . . . . . . . .1749213570 . . . . . . . . . . . .1749213571 . . . . . . . . . . . .1749213572 . . . . . . . . . . . .1749213573 . . . . . . . . . . . .1749213575 . . . . . . . . . . . .1749213577 . . . . . . . . . . . .1749213578 . . . . . . . . . . . .1749213579 . . . . . . . . . . . .17492143 . . . . . . . . . . . . . .1949214311 . . . . . . . . . . . .1739214312 . . . . . . . . . . . .1739214313 . . . . . . . . . . . .1739214315 . . . . . . . . . . . .1739214331 . . . . . . . . . . . .1739214332 . . . . . . . . . . . .1739214333 . . . . . . . . . . . .1739214335 . . . . . . . . . . . .1739214351 . . . . . . . . . . . .1739214352 . . . . . . . . . . . .1739214353 . . . . . . . . . . . .1739214355 . . . . . . . . . . . .1739214361 . . . . . . . . . . . .1739214362 . . . . . . . . . . . .1739214363 . . . . . . . . . . . .1739214365 . . . . . . . . . . . .17392145 . . . . . . . . . . . . . .194921450210 . . . . . .173,198921450212 . . . . . .173,198921450220 . . . . . .173,198921450222 . . . . . .173,1989214510 . . . . . . . . . . . .1739214511 . . . . . . . . . . . .173

9214512 . . . . . . . . . . . .1739214513 . . . . . . . . . . . .1739214514 . . . . . . . . . . . .1739214515 . . . . . . . . . . . .1739214517 . . . . . . . . . . . .1739214518 . . . . . . . . . . . .1739214519 . . . . . . . . . . . .1739214521 . . . . . . . . . . . .1739214522 . . . . . . . . . . . .1739214523 . . . . . . . . . . . .1739214525 . . . . . . . . . . . .1739214531 . . . . . . . . . . . .1739214532 . . . . . . . . . . . .1739214533 . . . . . . . . . . . .1739214535 . . . . . . . . . . . .1739214550 . . . . . . . . . . . .1739214551 . . . . . . . . . . . .1739214552 . . . . . . . . . . . .1739214553 . . . . . . . . . . . .1739214555 . . . . . . . . . . . .1739214557 . . . . . . . . . . . .1739214558 . . . . . . . . . . . .1739214559 . . . . . . . . . . . .1739214560 . . . . . . . . . . . .1739214561 . . . . . . . . . . . .1739214562 . . . . . . . . . . . .1739214563 . . . . . . . . . . . .1739214564 . . . . . . . . . . . .1739214565 . . . . . . . . . . . .1739214567 . . . . . . . . . . . .1739214568 . . . . . . . . . . . .1739214569 . . . . . . . . . . . .1739214570 . . . . . . . . . . . .1739214571 . . . . . . . . . . . .1739214572 . . . . . . . . . . . .1739214573 . . . . . . . . . . . .1739214575 . . . . . . . . . . . .1739214577 . . . . . . . . . . . .1739214578 . . . . . . . . . . . .1739214579 . . . . . . . . . . . .17392153 . . . . . . . . . . . . . .1949215311 . . . . . . . . . . . .1759215312 . . . . . . . . . . . .1759215313 . . . . . . . . . . . .1759215315 . . . . . . . . . . . .1759215331 . . . . . . . . . . . .1759215332 . . . . . . . . . . . .1759215333 . . . . . . . . . . . .1759215335 . . . . . . . . . . . .1759215351 . . . . . . . . . . . .1759215352 . . . . . . . . . . . .1759215353 . . . . . . . . . . . .1759215355 . . . . . . . . . . . .1759215361 . . . . . . . . . . . .1759215362 . . . . . . . . . . . .1759215363 . . . . . . . . . . . .1759215365 . . . . . . . . . . . .17592155 . . . . . . . . . . . . . .194921550210 . . . . . .175,198921550212 . . . . . .175,198921550220 . . . . . .175,198921550222 . . . . . .175,1989215511 . . . . . . . . . . . .1759215512 . . . . . . . . . . . .1759215513 . . . . . . . . . . . .1759215515 . . . . . . . . . . . .1759215521 . . . . . . . . . . . .1759215522 . . . . . . . . . . . .1759215523 . . . . . . . . . . . .1759215525 . . . . . . . . . . . .1759215531 . . . . . . . . . . . .1759215532 . . . . . . . . . . . .1759215533 . . . . . . . . . . . .1759215535 . . . . . . . . . . . .1759215551 . . . . . . . . . . . .1759215552 . . . . . . . . . . . .1759215553 . . . . . . . . . . . .1759215555 . . . . . . . . . . . .1759215561 . . . . . . . . . . . .1759215562 . . . . . . . . . . . .1759215563 . . . . . . . . . . . .1759215565 . . . . . . . . . . . .175


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Catalog #9215571 . . . . . . . . . . . .1759215572 . . . . . . . . . . . .1759215573 . . . . . . . . . . . .1759215575 . . . . . . . . . . . .17592163 . . . . . . . . . . . . . .1949216311 . . . . . . . . . . . .1759216312 . . . . . . . . . . . .1759216313 . . . . . . . . . . . .1759216315 . . . . . . . . . . . .1759216331 . . . . . . . . . . . .1759216332 . . . . . . . . . . . .1759216333 . . . . . . . . . . . .1759216335 . . . . . . . . . . . .1759216351 . . . . . . . . . . . .1759216352 . . . . . . . . . . . .1759216353 . . . . . . . . . . . .1759216355 . . . . . . . . . . . .1759216361 . . . . . . . . . . . .1759216362 . . . . . . . . . . . .1759216363 . . . . . . . . . . . .1759216365 . . . . . . . . . . . .17592165 . . . . . . . . . . . . . .194921650210 . . . . . .175,198921650212 . . . . . .175,198921650220 . . . . . .175,198921650222 . . . . . .175,1989216510 . . . . . . . . . . . .1759216511 . . . . . . . . . . . .1759216512 . . . . . . . . . . . .1759216513 . . . . . . . . . . . .1759216515 . . . . . . . . . . . .1759216517 . . . . . . . . . . . .1759216518 . . . . . . . . . . . .1759216519 . . . . . . . . . . . .1759216521 . . . . . . . . . . . .1759216522 . . . . . . . . . . . .1759216523 . . . . . . . . . . . .1759216525 . . . . . . . . . . . .1759216531 . . . . . . . . . . . .1759216532 . . . . . . . . . . . .1759216533 . . . . . . . . . . . .1759216535 . . . . . . . . . . . .1759216550 . . . . . . . . . . . .1759216551 . . . . . . . . . . . .1759216552 . . . . . . . . . . . .1759216553 . . . . . . . . . . . .1759216555 . . . . . . . . . . . .1759216557 . . . . . . . . . . . .1759216558 . . . . . . . . . . . .1759216559 . . . . . . . . . . . .1759216560 . . . . . . . . . . . .1759216561 . . . . . . . . . . . .1759216562 . . . . . . . . . . . .1759216563 . . . . . . . . . . . .1759216565 . . . . . . . . . . . .1759216567 . . . . . . . . . . . .1759216568 . . . . . . . . . . . .1759216569 . . . . . . . . . . . .1759216570 . . . . . . . . . . . .1759216571 . . . . . . . . . . . .1759216572 . . . . . . . . . . . .1759216573 . . . . . . . . . . . .1759216575 . . . . . . . . . . . .1759216577 . . . . . . . . . . . .1759216578 . . . . . . . . . . . .1759216579 . . . . . . . . . . . .1759217311 . . . . . . . . . . . .1769217312 . . . . . . . . . . . .1769217313 . . . . . . . . . . . .1769217315 . . . . . . . . . . . .1769217331 . . . . . . . . . . . .1769217332 . . . . . . . . . . . .1769217333 . . . . . . . . . . . .1769217335 . . . . . . . . . . . .1769217351 . . . . . . . . . . . .1769217352 . . . . . . . . . . . .1769217353 . . . . . . . . . . . .1769217355 . . . . . . . . . . . .1769217361 . . . . . . . . . . . .1769217362 . . . . . . . . . . . .1769217363 . . . . . . . . . . . .1769217365 . . . . . . . . . . . .176

92175 . . . . . . . . . . . . . .194921750210 . . . . . .176,198921750212 . . . . . .176,198921750220 . . . . . .176,198921750222 . . . . . .176,1989217511 . . . . . . . . . . . .1769217512 . . . . . . . . . . . .1769217513 . . . . . . . . . . . .1769217515 . . . . . . . . . . . .1769217521 . . . . . . . . . . . .1769217522 . . . . . . . . . . . .1769217523 . . . . . . . . . . . .1769217525 . . . . . . . . . . . .1769217531 . . . . . . . . . . . .1769217532 . . . . . . . . . . . .1769217533 . . . . . . . . . . . .1769217535 . . . . . . . . . . . .1769217551 . . . . . . . . . . . .1769217552 . . . . . . . . . . . .1769217553 . . . . . . . . . . . .1769217555 . . . . . . . . . . . .1769217561 . . . . . . . . . . . .1769217562 . . . . . . . . . . . .1769217563 . . . . . . . . . . . .1769217565 . . . . . . . . . . . .1769217571 . . . . . . . . . . . .1769217572 . . . . . . . . . . . .1769217573 . . . . . . . . . . . .1769217575 . . . . . . . . . . . .1769219412 . . . . . . . . . . . .1749219413 . . . . . . . . . . . .1749219415 . . . . . . . . . . . .1749219422 . . . . . . . . . . . .1749219423 . . . . . . . . . . . .1749219425 . . . . . . . . . . . .1749219452 . . . . . . . . . . . .1749219453 . . . . . . . . . . . .1749219455 . . . . . . . . . . . .1749219462 . . . . . . . . . . . .1749219463 . . . . . . . . . . . .1749219465 . . . . . . . . . . . .1749219472 . . . . . . . . . . . .1749219473 . . . . . . . . . . . .1749219475 . . . . . . . . . . . .174921950210 . . . . . .174,198921950212 . . . . . .174,198921950220 . . . . . .174,198921950222 . . . . . .174,1989409212 . . . . . . . . . . . .1709409232 . . . . . . . . . . . .1709409252 . . . . . . . . . . . .1709409311 . . . . . . . . . . . .1709409312 . . . . . . . . . . . .1709409313 . . . . . . . . . . . .1709409315 . . . . . . . . . . . .1709409331 . . . . . . . . . . . .1709409332 . . . . . . . . . . . .1709409333 . . . . . . . . . . . .1709409335 . . . . . . . . . . . .1709409351 . . . . . . . . . . . .1709409352 . . . . . . . . . . . .1709409353 . . . . . . . . . . . .1709409355 . . . . . . . . . . . .1709409361 . . . . . . . . . . . .1709409362 . . . . . . . . . . . .1709409363 . . . . . . . . . . . .1709409365 . . . . . . . . . . . .170940950210 . . . . . .170,198940950212 . . . . . .170,198940950220 . . . . . .170,198940950222 . . . . . .170,1989409510 . . . . . . . . . . . .1709409511 . . . . . . . . . . . .1709409512 . . . . . . . . . . . .1709409513 . . . . . . . . . . . .1709409515 . . . . . . . . . . . .1709409517 . . . . . . . . . . . .1709409518 . . . . . . . . . . . .1709409519 . . . . . . . . . . . .1709409521 . . . . . . . . . . . .1709409522 . . . . . . . . . . . .1709409523 . . . . . . . . . . . .170

9409525 . . . . . . . . . . . .1709409531 . . . . . . . . . . . .1709409532 . . . . . . . . . . . .1709409533 . . . . . . . . . . . .1709409535 . . . . . . . . . . . .1709409550 . . . . . . . . . . . .1709409551 . . . . . . . . . . . .1709409552 . . . . . . . . . . . .1709409553 . . . . . . . . . . . .1709409555 . . . . . . . . . . . .1709409557 . . . . . . . . . . . .1709409558 . . . . . . . . . . . .1709409559 . . . . . . . . . . . .1709409560 . . . . . . . . . . . .1709409561 . . . . . . . . . . . .1709409562 . . . . . . . . . . . .1709409563 . . . . . . . . . . . .1709409565 . . . . . . . . . . . .1709409567 . . . . . . . . . . . .1709409568 . . . . . . . . . . . .1709409569 . . . . . . . . . . . .1709409570 . . . . . . . . . . . .1709409571 . . . . . . . . . . . .1709409572 . . . . . . . . . . . .1709409573 . . . . . . . . . . . .1709409575 . . . . . . . . . . . .1709409577 . . . . . . . . . . . .1709409578 . . . . . . . . . . . .1709409579 . . . . . . . . . . . .1709410212 . . . . . . . . . . . .1729410232 . . . . . . . . . . . .1729410252 . . . . . . . . . . . .1729410311 . . . . . . . . . . . .1729410312 . . . . . . . . . . . .1729410313 . . . . . . . . . . . .1729410315 . . . . . . . . . . . .1729410331 . . . . . . . . . . . .1729410332 . . . . . . . . . . . .1729410333 . . . . . . . . . . . .1729410335 . . . . . . . . . . . .1729410351 . . . . . . . . . . . .1729410352 . . . . . . . . . . . .1729410353 . . . . . . . . . . . .1729410355 . . . . . . . . . . . .1729410361 . . . . . . . . . . . .1729410362 . . . . . . . . . . . .1729410363 . . . . . . . . . . . .1729410365 . . . . . . . . . . . .17294105 . . . . . . . . . . . . . .194941050210 . . . . . .172,198941050212 . . . . . .172,198941050220 . . . . . .172,198941050222 . . . . . .172,1989410510 . . . . . . . . . . . .1729410511 . . . . . . . . . . . .1729410512 . . . . . . . . . . . .1729410513 . . . . . . . . . . . .1729410515 . . . . . . . . . . . .1729410517 . . . . . . . . . . . .1729410518 . . . . . . . . . . . .1729410519 . . . . . . . . . . . .1729410521 . . . . . . . . . . . .1729410522 . . . . . . . . . . . .1729410523 . . . . . . . . . . . .1729410525 . . . . . . . . . . . .1729410531 . . . . . . . . . . . .1729410532 . . . . . . . . . . . .1729410533 . . . . . . . . . . . .1729410535 . . . . . . . . . . . .1729410550 . . . . . . . . . . . .1729410551 . . . . . . . . . . . .1729410552 . . . . . . . . . . . .1729410553 . . . . . . . . . . . .1729410555 . . . . . . . . . . . .1729410557 . . . . . . . . . . . .1729410558 . . . . . . . . . . . .1729410559 . . . . . . . . . . . .1729410560 . . . . . . . . . . . .1729410561 . . . . . . . . . . . .1729410562 . . . . . . . . . . . .1729410563 . . . . . . . . . . . .1729410565 . . . . . . . . . . . .172

9410567 . . . . . . . . . . . .1729410568 . . . . . . . . . . . .1729410569 . . . . . . . . . . . .1729410570 . . . . . . . . . . . .1729410571 . . . . . . . . . . . .1729410572 . . . . . . . . . . . .1729410573 . . . . . . . . . . . .1729410575 . . . . . . . . . . . .1729410577 . . . . . . . . . . . .1729410578 . . . . . . . . . . . .1729410579 . . . . . . . . . . . .1729413212 . . . . . . . . . . . .1679413232 . . . . . . . . . . . .1679413252 . . . . . . . . . . . .1679413311 . . . . . . . . . . . .1679413312 . . . . . . . . . . . .1679413313 . . . . . . . . . . . .1679413315 . . . . . . . . . . . .1679413331 . . . . . . . . . . . .1679413332 . . . . . . . . . . . .1679413333 . . . . . . . . . . . .1679413335 . . . . . . . . . . . .1679413351 . . . . . . . . . . . .1679413352 . . . . . . . . . . . .1679413353 . . . . . . . . . . . .1679413355 . . . . . . . . . . . .16794135 . . . . . . . . . . . . . .194941350210 . . . . . .167,198941350212 . . . . . .167,198941350220 . . . . . .167,198941350222 . . . . . .167,1989413510 . . . . . . . . . . . .1679413511 . . . . . . . . . . . .1679413512 . . . . . . . . . . . .1679413513 . . . . . . . . . . . .1679413515 . . . . . . . . . . . .1679413517 . . . . . . . . . . . .1679413518 . . . . . . . . . . . .1679413519 . . . . . . . . . . . .1679413521 . . . . . . . . . . . .1679413522 . . . . . . . . . . . .1679413523 . . . . . . . . . . . .1679413525 . . . . . . . . . . . .1679413531 . . . . . . . . . . . .1679413532 . . . . . . . . . . . .1679413533 . . . . . . . . . . . .1679413535 . . . . . . . . . . . .1679413550 . . . . . . . . . . . .1679413551 . . . . . . . . . . . .1679413552 . . . . . . . . . . . .1679413553 . . . . . . . . . . . .1679413555 . . . . . . . . . . . .1679413557 . . . . . . . . . . . .1679413558 . . . . . . . . . . . .1679413559 . . . . . . . . . . . .1679413560 . . . . . . . . . . . .1679413561 . . . . . . . . . . . .1679413562 . . . . . . . . . . . .1679413563 . . . . . . . . . . . .1679413565 . . . . . . . . . . . .1679413567 . . . . . . . . . . . .1679413568 . . . . . . . . . . . .1679413569 . . . . . . . . . . . .1679413570 . . . . . . . . . . . .1679413571 . . . . . . . . . . . .1679413572 . . . . . . . . . . . .1679413573 . . . . . . . . . . . .1679413575 . . . . . . . . . . . .1679413577 . . . . . . . . . . . .1679413578 . . . . . . . . . . . .1679413579 . . . . . . . . . . . .1679414212 . . . . . . . . . . . .1669414232 . . . . . . . . . . . .1669414252 . . . . . . . . . . . .1669414311 . . . . . . . . . . . .1669414312 . . . . . . . . . . . .1669414313 . . . . . . . . . . . .1669414315 . . . . . . . . . . . .1669414331 . . . . . . . . . . . .1669414332 . . . . . . . . . . . .1669414333 . . . . . . . . . . . .1669414335 . . . . . . . . . . . .166

9414351 . . . . . . . . . . . .1669414352 . . . . . . . . . . . .1669414353 . . . . . . . . . . . .1669414355 . . . . . . . . . . . .16694145 . . . . . . . . . . . . . .194941450210 . . . . . .166,198941450212 . . . . . .166,198941450220 . . . . . .166,198941450222 . . . . . .166,1989414510 . . . . . . . . . . . .1669414511 . . . . . . . . . . . .1669414512 . . . . . . . . . . . .1669414513 . . . . . . . . . . . .1669414515 . . . . . . . . . . . .1669414517 . . . . . . . . . . . .1669414518 . . . . . . . . . . . .1669414519 . . . . . . . . . . . .1669414521 . . . . . . . . . . . .1669414522 . . . . . . . . . . . .1669414523 . . . . . . . . . . . .1669414525 . . . . . . . . . . . .1669414531 . . . . . . . . . . . .1669414532 . . . . . . . . . . . .1669414533 . . . . . . . . . . . .1669414535 . . . . . . . . . . . .1669414550 . . . . . . . . . . . .1669414551 . . . . . . . . . . . .1669414552 . . . . . . . . . . . .1669414553 . . . . . . . . . . . .1669414555 . . . . . . . . . . . .1669414557 . . . . . . . . . . . .1669414558 . . . . . . . . . . . .1669414559 . . . . . . . . . . . .1669414560 . . . . . . . . . . . .1669414561 . . . . . . . . . . . .1669414562 . . . . . . . . . . . .1669414563 . . . . . . . . . . . .1669414565 . . . . . . . . . . . .1669414567 . . . . . . . . . . . .1669414568 . . . . . . . . . . . .1669414569 . . . . . . . . . . . .1669414570 . . . . . . . . . . . .1669414571 . . . . . . . . . . . .1669414572 . . . . . . . . . . . .1669414573 . . . . . . . . . . . .1669414575 . . . . . . . . . . . .1669414577 . . . . . . . . . . . .1669414578 . . . . . . . . . . . .1669414579 . . . . . . . . . . . .166941550210 . . . . . .168,198941550212 . . . . . .168,198941550220 . . . . . .168,198941550222 . . . . . .168,1989415511 . . . . . . . . . . . .1689415512 . . . . . . . . . . . .1689415513 . . . . . . . . . . . .1689415515 . . . . . . . . . . . .1689415521 . . . . . . . . . . . .1689415522 . . . . . . . . . . . .1689415523 . . . . . . . . . . . .1689415525 . . . . . . . . . . . .1689415531 . . . . . . . . . . . .1689415532 . . . . . . . . . . . .1689415533 . . . . . . . . . . . .1689415535 . . . . . . . . . . . .1689415551 . . . . . . . . . . . .1689415552 . . . . . . . . . . . .1689415553 . . . . . . . . . . . .1689415555 . . . . . . . . . . . .1689415561 . . . . . . . . . . . .1689415562 . . . . . . . . . . . .1689415563 . . . . . . . . . . . .1689415565 . . . . . . . . . . . .1689415571 . . . . . . . . . . . .1689415572 . . . . . . . . . . . .1689415573 . . . . . . . . . . . .1689415575 . . . . . . . . . . . .1689416212 . . . . . . . . . . . .1689416232 . . . . . . . . . . . .1689416252 . . . . . . . . . . . .16894165 . . . . . . . . . . . . . .194941650210 . . . . . .168,198

941650212 . . . . . .168,198941650220 . . . . . .168,198941650222 . . . . . .168,1989416510 . . . . . . . . . . . .1689416511 . . . . . . . . . . . .1689416512 . . . . . . . . . . . .1689416513 . . . . . . . . . . . .1689416515 . . . . . . . . . . . .1689416517 . . . . . . . . . . . .1689416518 . . . . . . . . . . . .1689416519 . . . . . . . . . . . .1689416521 . . . . . . . . . . . .1689416522 . . . . . . . . . . . .1689416523 . . . . . . . . . . . .1689416525 . . . . . . . . . . . .1689416531 . . . . . . . . . . . .1689416532 . . . . . . . . . . . .1689416533 . . . . . . . . . . . .1689416535 . . . . . . . . . . . .1689416550 . . . . . . . . . . . .1689416551 . . . . . . . . . . . .1689416552 . . . . . . . . . . . .1689416553 . . . . . . . . . . . .1689416555 . . . . . . . . . . . .1689416557 . . . . . . . . . . . .1689416558 . . . . . . . . . . . .1689416559 . . . . . . . . . . . .1689416560 . . . . . . . . . . . .1689416561 . . . . . . . . . . . .1689416562 . . . . . . . . . . . .1689416563 . . . . . . . . . . . .1689416565 . . . . . . . . . . . .1689416567 . . . . . . . . . . . .1689416568 . . . . . . . . . . . .1689416569 . . . . . . . . . . . .1689416570 . . . . . . . . . . . .1689416571 . . . . . . . . . . . .1689416572 . . . . . . . . . . . .1689416573 . . . . . . . . . . . .1689416575 . . . . . . . . . . . .1689416577 . . . . . . . . . . . .1689416578 . . . . . . . . . . . .1689416579 . . . . . . . . . . . .1689418212 . . . . . . . . . . . .1719418232 . . . . . . . . . . . .1719418252 . . . . . . . . . . . .1719418311 . . . . . . . . . . . .1719418312 . . . . . . . . . . . .1719418313 . . . . . . . . . . . .1719418315 . . . . . . . . . . . .1719418331 . . . . . . . . . . . .1719418332 . . . . . . . . . . . .1719418333 . . . . . . . . . . . .1719418335 . . . . . . . . . . . .1719418351 . . . . . . . . . . . .1719418352 . . . . . . . . . . . .1719418353 . . . . . . . . . . . .1719418355 . . . . . . . . . . . .1719418361 . . . . . . . . . . . .1719418362 . . . . . . . . . . . .1719418363 . . . . . . . . . . . .1719418365 . . . . . . . . . . . .171941850210 . . . . . .171,198941850212 . . . . . .171,198941850220 . . . . . .171,198941850222 . . . . . .171,1989418510 . . . . . . . . . . . .1719418511 . . . . . . . . . . . .1719418512 . . . . . . . . . . . .1719418513 . . . . . . . . . . . .1719418515 . . . . . . . . . . . .1719418517 . . . . . . . . . . . .1719418518 . . . . . . . . . . . .1719418519 . . . . . . . . . . . .1719418521 . . . . . . . . . . . .1719418522 . . . . . . . . . . . .1719418523 . . . . . . . . . . . .1719418525 . . . . . . . . . . . .1719418531 . . . . . . . . . . . .1719418532 . . . . . . . . . . . .1719418533 . . . . . . . . . . . .1719418535 . . . . . . . . . . . .171


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Catalog #9418550 . . . . . . . . . . . .1719418551 . . . . . . . . . . . .1719418552 . . . . . . . . . . . .1719418553 . . . . . . . . . . . .1719418555 . . . . . . . . . . . .1719418557 . . . . . . . . . . . .1719418558 . . . . . . . . . . . .1719418559 . . . . . . . . . . . .1719418560 . . . . . . . . . . . .1719418561 . . . . . . . . . . . .1719418562 . . . . . . . . . . . .1719418563 . . . . . . . . . . . .1719418565 . . . . . . . . . . . .1719418567 . . . . . . . . . . . .1719418568 . . . . . . . . . . . .1719418569 . . . . . . . . . . . .1719418570 . . . . . . . . . . . .1719418571 . . . . . . . . . . . .1719418572 . . . . . . . . . . . .1719418573 . . . . . . . . . . . .1719418575 . . . . . . . . . . . .1719418577 . . . . . . . . . . . .1719418578 . . . . . . . . . . . .1719418579 . . . . . . . . . . . .1719419212 . . . . . . . . . . . .1699419232 . . . . . . . . . . . .1699419252 . . . . . . . . . . . .1699419311 . . . . . . . . . . . .1699419312 . . . . . . . . . . . .1699419313 . . . . . . . . . . . .1699419315 . . . . . . . . . . . .1699419331 . . . . . . . . . . . .1699419332 . . . . . . . . . . . .1699419333 . . . . . . . . . . . .1699419335 . . . . . . . . . . . .1699419351 . . . . . . . . . . . .1699419352 . . . . . . . . . . . .1699419353 . . . . . . . . . . . .1699419355 . . . . . . . . . . . .1699419361 . . . . . . . . . . . .1699419362 . . . . . . . . . . . .1699419363 . . . . . . . . . . . .1699419365 . . . . . . . . . . . .169941950210 . . . . . .169,198941950212 . . . . . .169,198941950220 . . . . . .169,198941950222 . . . . . .169,1989419510 . . . . . . . . . . . .1699419511 . . . . . . . . . . . .1699419512 . . . . . . . . . . . .1699419513 . . . . . . . . . . . .1699419515 . . . . . . . . . . . .1699419517 . . . . . . . . . . . .1699419518 . . . . . . . . . . . .1699419519 . . . . . . . . . . . .1699419521 . . . . . . . . . . . .1699419522 . . . . . . . . . . . .1699419523 . . . . . . . . . . . .1699419525 . . . . . . . . . . . .1699419531 . . . . . . . . . . . .1699419532 . . . . . . . . . . . .1699419533 . . . . . . . . . . . .1699419535 . . . . . . . . . . . .1699419550 . . . . . . . . . . . .1699419551 . . . . . . . . . . . .1699419552 . . . . . . . . . . . .1699419553 . . . . . . . . . . . .1699419555 . . . . . . . . . . . .1699419557 . . . . . . . . . . . .1699419558 . . . . . . . . . . . .1699419559 . . . . . . . . . . . .1699419560 . . . . . . . . . . . .1699419561 . . . . . . . . . . . .1699419562 . . . . . . . . . . . .1699419563 . . . . . . . . . . . .1699419565 . . . . . . . . . . . .1699419567 . . . . . . . . . . . .1699419568 . . . . . . . . . . . .1699419569 . . . . . . . . . . . .1699419570 . . . . . . . . . . . .1699419571 . . . . . . . . . . . .1699419572 . . . . . . . . . . . .169

9419573 . . . . . . . . . . . .1699419575 . . . . . . . . . . . .1699419577 . . . . . . . . . . . .1699419578 . . . . . . . . . . . .1699419579 . . . . . . . . . . . .1699425212 . . . . . . . . . . . .1719425232 . . . . . . . . . . . .1719425252 . . . . . . . . . . . .1719425510 . . . . . . . . . . . .1719425517 . . . . . . . . . . . .1719425518 . . . . . . . . . . . .1719425519 . . . . . . . . . . . .1719425550 . . . . . . . . . . . .1719425557 . . . . . . . . . . . .1719425558 . . . . . . . . . . . .1719425559 . . . . . . . . . . . .1719425560 . . . . . . . . . . . .1719425567 . . . . . . . . . . . .1719425568 . . . . . . . . . . . .1719425569 . . . . . . . . . . . .1719425570 . . . . . . . . . . . .1719425577 . . . . . . . . . . . .1719425578 . . . . . . . . . . . .1719425579 . . . . . . . . . . . .1719470212 . . . . . . . . . . . .1729470232 . . . . . . . . . . . .1729470252 . . . . . . . . . . . .172951050210 . . . . . .193,198951050212 . . . . . .193,198951050220 . . . . . .193,198951050222 . . . . . .193,1989510511 . . . . . . . . . . . .1939510512 . . . . . . . . . . . .1939510513 . . . . . . . . . . . .1939510515 . . . . . . . . . . . .1939510521 . . . . . . . . . . . .1939510522 . . . . . . . . . . . .1939510523 . . . . . . . . . . . .1939510525 . . . . . . . . . . . .1939510531 . . . . . . . . . . . .1939510532 . . . . . . . . . . . .1939510533 . . . . . . . . . . . .1939510535 . . . . . . . . . . . .1939510551 . . . . . . . . . . . .1939510552 . . . . . . . . . . . .1939510553 . . . . . . . . . . . .1939510555 . . . . . . . . . . . .1939510561 . . . . . . . . . . . .1939510562 . . . . . . . . . . . .1939510563 . . . . . . . . . . . .1939510565 . . . . . . . . . . . .1939510571 . . . . . . . . . . . .1939510572 . . . . . . . . . . . .1939510573 . . . . . . . . . . . .1939510575 . . . . . . . . . . . .193951250210 . . . . . .191,198951250212 . . . . . .191,198951250220 . . . . . .191,198951250222 . . . . . .191,1989512510 . . . . . . . . . . . .1919512511 . . . . . . . . . . . .1919512512 . . . . . . . . . . . .1919512513 . . . . . . . . . . . .1919512515 . . . . . . . . . . . .1919512517 . . . . . . . . . . . .1919512518 . . . . . . . . . . . .1919512519 . . . . . . . . . . . .1919512521 . . . . . . . . . . . .1919512522 . . . . . . . . . . . .1919512523 . . . . . . . . . . . .1919512525 . . . . . . . . . . . .1919512531 . . . . . . . . . . . .1919512532 . . . . . . . . . . . .1919512533 . . . . . . . . . . . .1919512535 . . . . . . . . . . . .1919512550 . . . . . . . . . . . .1919512551 . . . . . . . . . . . .1919512552 . . . . . . . . . . . .1919512553 . . . . . . . . . . . .1919512555 . . . . . . . . . . . .1919512557 . . . . . . . . . . . .1919512558 . . . . . . . . . . . .191

9512559 . . . . . . . . . . . .1919512560 . . . . . . . . . . . .1919512561 . . . . . . . . . . . .1919512562 . . . . . . . . . . . .1919512563 . . . . . . . . . . . .1919512565 . . . . . . . . . . . .1919512567 . . . . . . . . . . . .1919512568 . . . . . . . . . . . .1919512569 . . . . . . . . . . . .1919512570 . . . . . . . . . . . .1919512571 . . . . . . . . . . . .1919512572 . . . . . . . . . . . .1919512573 . . . . . . . . . . . .1919512575 . . . . . . . . . . . .1919512577 . . . . . . . . . . . .1919512578 . . . . . . . . . . . .1919512579 . . . . . . . . . . . .191951350210 . . . . . .191,198951350212 . . . . . .191,198951350220 . . . . . .191,198951350222 . . . . . .191,1989513510 . . . . . . . . . . . .1919513511 . . . . . . . . . . . .1919513512 . . . . . . . . . . . .1919513513 . . . . . . . . . . . .1919513515 . . . . . . . . . . . .1919513517 . . . . . . . . . . . .1919513518 . . . . . . . . . . . .1919513519 . . . . . . . . . . . .1919513521 . . . . . . . . . . . .1919513522 . . . . . . . . . . . .1919513523 . . . . . . . . . . . .1919513525 . . . . . . . . . . . .1919513531 . . . . . . . . . . . .1919513532 . . . . . . . . . . . .1919513533 . . . . . . . . . . . .1919513535 . . . . . . . . . . . .1919513550 . . . . . . . . . . . .1919513551 . . . . . . . . . . . .1919513552 . . . . . . . . . . . .1919513553 . . . . . . . . . . . .1919513555 . . . . . . . . . . . .1919513557 . . . . . . . . . . . .1919513558 . . . . . . . . . . . .1919513559 . . . . . . . . . . . .1919513560 . . . . . . . . . . . .1919513561 . . . . . . . . . . . .1919513562 . . . . . . . . . . . .1919513563 . . . . . . . . . . . .1919513565 . . . . . . . . . . . .1919513567 . . . . . . . . . . . .1919513568 . . . . . . . . . . . .1919513569 . . . . . . . . . . . .1919513570 . . . . . . . . . . . .1919513571 . . . . . . . . . . . .1919513572 . . . . . . . . . . . .1919513573 . . . . . . . . . . . .1919513575 . . . . . . . . . . . .1919513577 . . . . . . . . . . . .1919513578 . . . . . . . . . . . .1919513579 . . . . . . . . . . . .1919514311 . . . . . . . . . . . .1909514312 . . . . . . . . . . . .1909514313 . . . . . . . . . . . .1909514315 . . . . . . . . . . . .1909514331 . . . . . . . . . . . .1909514332 . . . . . . . . . . . .1909514333 . . . . . . . . . . . .1909514335 . . . . . . . . . . . .1909514351 . . . . . . . . . . . .1909514352 . . . . . . . . . . . .1909514353 . . . . . . . . . . . .1909514355 . . . . . . . . . . . .1909514361 . . . . . . . . . . . .1909514362 . . . . . . . . . . . .1909514363 . . . . . . . . . . . .1909514365 . . . . . . . . . . . .190951450210 . . . . . .190,198951450212 . . . . . .190,198951450220 . . . . . .190,198951450222 . . . . . .190,1989514510 . . . . . . . . . . . .190

9514511 . . . . . . . . . . . .1909514512 . . . . . . . . . . . .1909514513 . . . . . . . . . . . .1909514515 . . . . . . . . . . . .1909514517 . . . . . . . . . . . .1909514518 . . . . . . . . . . . .1909514519 . . . . . . . . . . . .1909514521 . . . . . . . . . . . .1909514522 . . . . . . . . . . . .1909514523 . . . . . . . . . . . .1909514525 . . . . . . . . . . . .1909514531 . . . . . . . . . . . .1909514532 . . . . . . . . . . . .1909514533 . . . . . . . . . . . .1909514535 . . . . . . . . . . . .1909514550 . . . . . . . . . . . .1909514551 . . . . . . . . . . . .1909514552 . . . . . . . . . . . .1909514553 . . . . . . . . . . . .1909514555 . . . . . . . . . . . .1909514557 . . . . . . . . . . . .1909514558 . . . . . . . . . . . .1909514559 . . . . . . . . . . . .1909514560 . . . . . . . . . . . .1909514561 . . . . . . . . . . . .1909514562 . . . . . . . . . . . .1909514563 . . . . . . . . . . . .1909514565 . . . . . . . . . . . .1909514567 . . . . . . . . . . . .1909514568 . . . . . . . . . . . .1909514569 . . . . . . . . . . . .1909514570 . . . . . . . . . . . .1909514571 . . . . . . . . . . . .1909514572 . . . . . . . . . . . .1909514573 . . . . . . . . . . . .1909514575 . . . . . . . . . . . .1909514577 . . . . . . . . . . . .1909514578 . . . . . . . . . . . .1909514579 . . . . . . . . . . . .190951650210 . . . . . .192,198951650212 . . . . . .192,198951650220 . . . . . .192,198951650222 . . . . . .192,1989516511 . . . . . . . . . . . .1929516512 . . . . . . . . . . . .1929516513 . . . . . . . . . . . .1929516515 . . . . . . . . . . . .1929516521 . . . . . . . . . . . .1929516522 . . . . . . . . . . . .1929516523 . . . . . . . . . . . .1929516525 . . . . . . . . . . . .1929516531 . . . . . . . . . . . .1929516532 . . . . . . . . . . . .1929516533 . . . . . . . . . . . .1929516535 . . . . . . . . . . . .1929516551 . . . . . . . . . . . .1929516552 . . . . . . . . . . . .1929516553 . . . . . . . . . . . .1929516555 . . . . . . . . . . . .1929516561 . . . . . . . . . . . .1929516562 . . . . . . . . . . . .1929516563 . . . . . . . . . . . .1929516565 . . . . . . . . . . . .1929516571 . . . . . . . . . . . .1929516572 . . . . . . . . . . . .1929516573 . . . . . . . . . . . .1929516575 . . . . . . . . . . . .192951950210 . . . . . .192,198951950212 . . . . . .192,198951950220 . . . . . .192,198951950222 . . . . . .192,1989519511 . . . . . . . . . . . .1929519512 . . . . . . . . . . . .1929519513 . . . . . . . . . . . .1929519515 . . . . . . . . . . . .1929519521 . . . . . . . . . . . .1929519522 . . . . . . . . . . . .1929519523 . . . . . . . . . . . .1929519525 . . . . . . . . . . . .1929519531 . . . . . . . . . . . .1929519532 . . . . . . . . . . . .1929519533 . . . . . . . . . . . .192

9519535 . . . . . . . . . . . .1929519551 . . . . . . . . . . . .1929519552 . . . . . . . . . . . .1929519553 . . . . . . . . . . . .1929519555 . . . . . . . . . . . .1929519561 . . . . . . . . . . . .1929519562 . . . . . . . . . . . .1929519563 . . . . . . . . . . . .1929519565 . . . . . . . . . . . .1929519571 . . . . . . . . . . . .1929519572 . . . . . . . . . . . .1929519573 . . . . . . . . . . . .1929519575 . . . . . . . . . . . .1929600212 . . . . . . . . . . . .1649600232 . . . . . . . . . . . .164960023E . . . . . . . . . . . .1649600252 . . . . . . . . . . . .164960025E . . . . . . . . . . . .16496003 . . . . . . . . . . . . . .1949600311 . . . . . . . . . . . .1649600312 . . . . . . . . . . . .1649600315 . . . . . . . . . . . .164960031E . . . . . . . . . . . .1649600331 . . . . . . . . . . . .1649600332 . . . . . . . . . . . .1649600335 . . . . . . . . . . . .164960033E . . . . . . . . . . . .1649600351 . . . . . . . . . . . .1649600352 . . . . . . . . . . . .1649600355 . . . . . . . . . . . .164960035E . . . . . . . . . . . .1649600361 . . . . . . . . . . . .1649600362 . . . . . . . . . . . .1649600365 . . . . . . . . . . . .164960036E . . . . . . . . . . . .16496005 . . . . . . . . . . . . . .194960050210 . . . . . .164,198960050212 . . . . . .164,198960050220 . . . . . .164,198960050222 . . . . . .164,1989600510 . . . . . . . . . . . .1649600511 . . . . . . . . . . . .1649600512 . . . . . . . . . . . .1649600515 . . . . . . . . . . . .1649600517 . . . . . . . . . . . .1649600518 . . . . . . . . . . . .1649600519 . . . . . . . . . . . .164960051E . . . . . . . . . . . .1649600521 . . . . . . . . . . . .1649600522 . . . . . . . . . . . .1649600525 . . . . . . . . . . . .164960052E . . . . . . . . . . . .1649600531 . . . . . . . . . . . .1649600532 . . . . . . . . . . . .1649600535 . . . . . . . . . . . .164960053E . . . . . . . . . . . .1649600550 . . . . . . . . . . . .1649600551 . . . . . . . . . . . .1649600552 . . . . . . . . . . . .1649600555 . . . . . . . . . . . .1649600557 . . . . . . . . . . . .1649600558 . . . . . . . . . . . .1649600559 . . . . . . . . . . . .164960055E . . . . . . . . . . . .1649600560 . . . . . . . . . . . .1649600561 . . . . . . . . . . . .1649600562 . . . . . . . . . . . .1649600565 . . . . . . . . . . . .1649600567 . . . . . . . . . . . .1649600568 . . . . . . . . . . . .1649600569 . . . . . . . . . . . .164960056E . . . . . . . . . . . .1649600570 . . . . . . . . . . . .1649600571 . . . . . . . . . . . .1649600572 . . . . . . . . . . . .1649600575 . . . . . . . . . . . .1649600577 . . . . . . . . . . . .1649600578 . . . . . . . . . . . .1649600579 . . . . . . . . . . . .164960057E . . . . . . . . . . . .1649600812 . . . . . . . . . . . .164960081E . . . . . . . . . . . .164

9600832 . . . . . . . . . . . .164960083E . . . . . . . . . . . .1649600852 . . . . . . . . . . . .164960085E . . . . . . . . . . . .16496033 . . . . . . . . . . . . . .1949603311 . . . . . . . . . . . .1589603312 . . . . . . . . . . . .1589603315 . . . . . . . . . . . .158960331E . . . . . . . . . . . .1589603331 . . . . . . . . . . . .1589603332 . . . . . . . . . . . .158960333E . . . . . . . . . . . .1589603335 . . . . . . . . . . . .158960335E . . . . . . . . . . . .1589603351 . . . . . . . . . . . .1589603352 . . . . . . . . . . . .1589603355 . . . . . . . . . . . .1589603361 . . . . . . . . . . . .1589603362 . . . . . . . . . . . .1589603365 . . . . . . . . . . . .158960336E . . . . . . . . . . . .15896035 . . . . . . . . . . . . . .194960350210 . . . . . .158,198960350212 . . . . . .158,198960350220 . . . . . .158,198960350222 . . . . . .158,1989603510 . . . . . . . . . . . .1589603511 . . . . . . . . . . . .1589603512 . . . . . . . . . . . .1589603515 . . . . . . . . . . . .1589603517 . . . . . . . . . . . .1589603518 . . . . . . . . . . . .1589603519 . . . . . . . . . . . .158960351E . . . . . . . . . . . .1589603521 . . . . . . . . . . . .1589603522 . . . . . . . . . . . .1589603525 . . . . . . . . . . . .158960352E . . . . . . . . . . . .1589603531 . . . . . . . . . . . .1589603532 . . . . . . . . . . . .1589603535 . . . . . . . . . . . .158960353E . . . . . . . . . . . .1589603550 . . . . . . . . . . . .1589603551 . . . . . . . . . . . .1589603552 . . . . . . . . . . . .1589603555 . . . . . . . . . . . .1589603557 . . . . . . . . . . . .1589603558 . . . . . . . . . . . .1589603559 . . . . . . . . . . . .158960355E . . . . . . . . . . . .1589603560 . . . . . . . . . . . .1589603561 . . . . . . . . . . . .1589603562 . . . . . . . . . . . .1589603565 . . . . . . . . . . . .1589603567 . . . . . . . . . . . .1589603568 . . . . . . . . . . . .1589603569 . . . . . . . . . . . .158960356E . . . . . . . . . . . .1589603570 . . . . . . . . . . . .1589603571 . . . . . . . . . . . .1589603572 . . . . . . . . . . . .1589603575 . . . . . . . . . . . .1589603577 . . . . . . . . . . . .1589603578 . . . . . . . . . . . .1589603579 . . . . . . . . . . . .158960357E . . . . . . . . . . . .1589604212 . . . . . . . . . . . .157960421E . . . . . . . . . . . .1579604232 . . . . . . . . . . . .157960423E . . . . . . . . . . . .1579604252 . . . . . . . . . . . .157960425E . . . . . . . . . . . .15796043 . . . . . . . . . . . . . .1949604311 . . . . . . . . . . . .1579604312 . . . . . . . . . . . .1579604315 . . . . . . . . . . . .157960431E . . . . . . . . . . . .1579604331 . . . . . . . . . . . .1579604332 . . . . . . . . . . . .1579604335 . . . . . . . . . . . .157960433E . . . . . . . . . . . .1579604351 . . . . . . . . . . . .157


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INDEX

Catalog #9604352 . . . . . . . . . . . .1579604355 . . . . . . . . . . . .157960435E . . . . . . . . . . . .1579604361 . . . . . . . . . . . .1579604362 . . . . . . . . . . . .1579604365 . . . . . . . . . . . .157960436E . . . . . . . . . . . .15796045 . . . . . . . . . . . . . .194960450210 . . . . . .157,198960450212 . . . . . .157,198960450220 . . . . . .157,198960450222 . . . . . .157,1989604510 . . . . . . . . . . . .1579604511 . . . . . . . . . . . .1579604512 . . . . . . . . . . . .1579604515 . . . . . . . . . . . .1579604517 . . . . . . . . . . . .1579604518 . . . . . . . . . . . .1579604519 . . . . . . . . . . . .157960451E . . . . . . . . . . . .1579604521 . . . . . . . . . . . .1579604522 . . . . . . . . . . . .1579604525 . . . . . . . . . . . .157960452E . . . . . . . . . . . .1579604531 . . . . . . . . . . . .1579604532 . . . . . . . . . . . .1579604535 . . . . . . . . . . . .157960453E . . . . . . . . . . . .1579604550 . . . . . . . . . . . .1579604551 . . . . . . . . . . . .1579604552 . . . . . . . . . . . .1579604555 . . . . . . . . . . . .1579604557 . . . . . . . . . . . .1579604558 . . . . . . . . . . . .1579604559 . . . . . . . . . . . .157960455E . . . . . . . . . . . .1579604560 . . . . . . . . . . . .1579604561 . . . . . . . . . . . .1579604562 . . . . . . . . . . . .1579604565 . . . . . . . . . . . .1579604567 . . . . . . . . . . . .1579604568 . . . . . . . . . . . .1579604569 . . . . . . . . . . . .157960456E . . . . . . . . . . . .1579604570 . . . . . . . . . . . .1579604571 . . . . . . . . . . . .1579604572 . . . . . . . . . . . .1579604575 . . . . . . . . . . . .1579604577 . . . . . . . . . . . .1579604578 . . . . . . . . . . . .1579604579 . . . . . . . . . . . .157960457E . . . . . . . . . . . .1579604812 . . . . . . . . . . . .157960481E . . . . . . . . . . . .1579604832 . . . . . . . . . . . .157960483E . . . . . . . . . . . .1579604852 . . . . . . . . . . . .157960485E . . . . . . . . . . . .1579605311 . . . . . . . . . . . .1629605312 . . . . . . . . . . . .1629605315 . . . . . . . . . . . .162960531E . . . . . . . . . . . .1629605331 . . . . . . . . . . . .1629605332 . . . . . . . . . . . .1629605335 . . . . . . . . . . . .162960533E . . . . . . . . . . . .1629605351 . . . . . . . . . . . .1629605352 . . . . . . . . . . . .1629605355 . . . . . . . . . . . .162960535E . . . . . . . . . . . .1629605361 . . . . . . . . . . . .1629605362 . . . . . . . . . . . .1629605365 . . . . . . . . . . . .162960536E . . . . . . . . . . . .162960550210 . . . . . .162,198960550212 . . . . . .162,198960550220 . . . . . .162,198960550222 . . . . . .162,1989605510 . . . . . . . . . . . .1629605511 . . . . . . . . . . . .1629605512 . . . . . . . . . . . .1629605515 . . . . . . . . . . . .162

9605517 . . . . . . . . . . . .1629605518 . . . . . . . . . . . .1629605519 . . . . . . . . . . . .162960551E . . . . . . . . . . . .1629605521 . . . . . . . . . . . .1629605522 . . . . . . . . . . . .1629605525 . . . . . . . . . . . .162960552E . . . . . . . . . . . .1629605531 . . . . . . . . . . . .1629605532 . . . . . . . . . . . .1629605535 . . . . . . . . . . . .162960553E . . . . . . . . . . . .1629605550 . . . . . . . . . . . .1629605551 . . . . . . . . . . . .1629605552 . . . . . . . . . . . .1629605555 . . . . . . . . . . . .1629605557 . . . . . . . . . . . .1629605558 . . . . . . . . . . . .1629605559 . . . . . . . . . . . .162960555E . . . . . . . . . . . .1629605560 . . . . . . . . . . . .1629605561 . . . . . . . . . . . .1629605562 . . . . . . . . . . . .1629605565 . . . . . . . . . . . .1629605567 . . . . . . . . . . . .1629605568 . . . . . . . . . . . .1629605569 . . . . . . . . . . . .162960556E . . . . . . . . . . . .1629605570 . . . . . . . . . . . .1629605571 . . . . . . . . . . . .1629605572 . . . . . . . . . . . .1629605575 . . . . . . . . . . . .1629605577 . . . . . . . . . . . .1629605578 . . . . . . . . . . . .1629605579 . . . . . . . . . . . .162960557E . . . . . . . . . . . .1629606212 . . . . . . . . . . . .163960621E . . . . . . . . . . . .1639606232 . . . . . . . . . . . .163960623E . . . . . . . . . . . .1639606252 . . . . . . . . . . . .163960625E . . . . . . . . . . . .1639606311 . . . . . . . . . . . .1639606312 . . . . . . . . . . . .1639606315 . . . . . . . . . . . .163960631E . . . . . . . . . . . .1639606331 . . . . . . . . . . . .1639606332 . . . . . . . . . . . .1639606335 . . . . . . . . . . . .163960633E . . . . . . . . . . . .1639606351 . . . . . . . . . . . .1639606352 . . . . . . . . . . . .1639606355 . . . . . . . . . . . .163960635E . . . . . . . . . . . .1639606361 . . . . . . . . . . . .1639606362 . . . . . . . . . . . .1639606365 . . . . . . . . . . . .163960636E . . . . . . . . . . . .163960650210 . . . . . .163,198960650212 . . . . . .163,198960650220 . . . . . .163,198960650222 . . . . . .163,1989606510 . . . . . . . . . . . .1639606511 . . . . . . . . . . . .1639606512 . . . . . . . . . . . .1639606515 . . . . . . . . . . . .1639606517 . . . . . . . . . . . .1639606518 . . . . . . . . . . . .1639606519 . . . . . . . . . . . .163960651E . . . . . . . . . . . .1639606521 . . . . . . . . . . . .1639606522 . . . . . . . . . . . .1639606525 . . . . . . . . . . . .163960652E . . . . . . . . . . . .1639606531 . . . . . . . . . . . .1639606532 . . . . . . . . . . . .1639606535 . . . . . . . . . . . .163960653E . . . . . . . . . . . .1639606550 . . . . . . . . . . . .1639606551 . . . . . . . . . . . .1639606552 . . . . . . . . . . . .1639606555 . . . . . . . . . . . .163

9606557 . . . . . . . . . . . .1639606558 . . . . . . . . . . . .1639606559 . . . . . . . . . . . .163960655E . . . . . . . . . . . .1639606560 . . . . . . . . . . . .1639606561 . . . . . . . . . . . .1639606562 . . . . . . . . . . . .1639606565 . . . . . . . . . . . .1639606567 . . . . . . . . . . . .1639606568 . . . . . . . . . . . .1639606569 . . . . . . . . . . . .163960656E . . . . . . . . . . . .1639606570 . . . . . . . . . . . .1639606571 . . . . . . . . . . . .1639606572 . . . . . . . . . . . .1639606575 . . . . . . . . . . . .1639606577 . . . . . . . . . . . .1639606578 . . . . . . . . . . . .1639606579 . . . . . . . . . . . .163960657E . . . . . . . . . . . .1639607212 . . . . . . . . . . . .161960721E . . . . . . . . . . . .1619607232 . . . . . . . . . . . .161960723E . . . . . . . . . . . .1619607252 . . . . . . . . . . . .161960725E . . . . . . . . . . . .1619607311 . . . . . . . . . . . .1619607312 . . . . . . . . . . . .1619607315 . . . . . . . . . . . .161960731E . . . . . . . . . . . .1619607331 . . . . . . . . . . . .1619607332 . . . . . . . . . . . .1619607335 . . . . . . . . . . . .161960733E . . . . . . . . . . . .1619607351 . . . . . . . . . . . .1619607352 . . . . . . . . . . . .1619607355 . . . . . . . . . . . .161960735E . . . . . . . . . . . .1619607361 . . . . . . . . . . . .1619607362 . . . . . . . . . . . .1619607365 . . . . . . . . . . . .161960736E . . . . . . . . . . . .161960750210 . . . . . .161,198960750212 . . . . . .161,198960750220 . . . . . .161,198960750222 . . . . . .161,1989607510 . . . . . . . . . . . .1619607511 . . . . . . . . . . . .1619607512 . . . . . . . . . . . .1619607515 . . . . . . . . . . . .1619607517 . . . . . . . . . . . .1619607518 . . . . . . . . . . . .1619607519 . . . . . . . . . . . .161960751E . . . . . . . . . . . .1619607521 . . . . . . . . . . . .1619607522 . . . . . . . . . . . .1619607525 . . . . . . . . . . . .161960752E . . . . . . . . . . . .1619607531 . . . . . . . . . . . .1619607532 . . . . . . . . . . . .1619607535 . . . . . . . . . . . .161960753E . . . . . . . . . . . .1619607550 . . . . . . . . . . . .1619607551 . . . . . . . . . . . .1619607552 . . . . . . . . . . . .1619607555 . . . . . . . . . . . .1619607557 . . . . . . . . . . . .1619607558 . . . . . . . . . . . .1619607559 . . . . . . . . . . . .161960755E . . . . . . . . . . . .1619607560 . . . . . . . . . . . .1619607561 . . . . . . . . . . . .1619607562 . . . . . . . . . . . .1619607565 . . . . . . . . . . . .1619607567 . . . . . . . . . . . .1619607568 . . . . . . . . . . . .1619607569 . . . . . . . . . . . .161960756E . . . . . . . . . . . .1619607570 . . . . . . . . . . . .1619607571 . . . . . . . . . . . .1619607572 . . . . . . . . . . . .1619607575 . . . . . . . . . . . .161

9607577 . . . . . . . . . . . .1619607578 . . . . . . . . . . . .1619607579 . . . . . . . . . . . .161960757E . . . . . . . . . . . .1619608311 . . . . . . . . . . . .1599608312 . . . . . . . . . . . .1599608315 . . . . . . . . . . . .159960831E . . . . . . . . . . . .1599608331 . . . . . . . . . . . .1599608332 . . . . . . . . . . . .1599608335 . . . . . . . . . . . .159960833E . . . . . . . . . . . .1599608351 . . . . . . . . . . . .1599608352 . . . . . . . . . . . .1599608355 . . . . . . . . . . . .159960835E . . . . . . . . . . . .1599608361 . . . . . . . . . . . .1599608362 . . . . . . . . . . . .1599608365 . . . . . . . . . . . .159960850210 . . . . . .159,198960850212 . . . . . .159,198960850220 . . . . . .159,198960850222 . . . . . .159,1989608510 . . . . . . . . . . . .1599608511 . . . . . . . . . . . .1599608512 . . . . . . . . . . . .1599608515 . . . . . . . . . . . .1599608517 . . . . . . . . . . . .1599608518 . . . . . . . . . . . .1599608519 . . . . . . . . . . . .159960851E . . . . . . . . . . . .1599608521 . . . . . . . . . . . .1599608522 . . . . . . . . . . . .1599608525 . . . . . . . . . . . .159960852E . . . . . . . . . . . .1599608531 . . . . . . . . . . . .1599608532 . . . . . . . . . . . .1599608535 . . . . . . . . . . . .159960853E . . . . . . . . . . . .1599608550 . . . . . . . . . . . .1599608551 . . . . . . . . . . . .1599608552 . . . . . . . . . . . .1599608555 . . . . . . . . . . . .1599608557 . . . . . . . . . . . .1599608558 . . . . . . . . . . . .1599608559 . . . . . . . . . . . .159960855E . . . . . . . . . . . .1599608560 . . . . . . . . . . . .1599608561 . . . . . . . . . . . .1599608562 . . . . . . . . . . . .1599608565 . . . . . . . . . . . .1599608567 . . . . . . . . . . . .1599608568 . . . . . . . . . . . .1599608569 . . . . . . . . . . . .159960856E . . . . . . . . . . . .1599608570 . . . . . . . . . . . .1599608571 . . . . . . . . . . . .1599608572 . . . . . . . . . . . .1599608575 . . . . . . . . . . . .1599608577 . . . . . . . . . . . .1599608578 . . . . . . . . . . . .1599608579 . . . . . . . . . . . .159960857E . . . . . . . . . . . .1599609212 . . . . . . . . . . . .160960921E . . . . . . . . . . . .1609609232 . . . . . . . . . . . .160960923E . . . . . . . . . . . .1609609252 . . . . . . . . . . . .160960925E . . . . . . . . . . . .1609609311 . . . . . . . . . . . .1609609312 . . . . . . . . . . . .1609609315 . . . . . . . . . . . .160960931E . . . . . . . . . . . .1609609331 . . . . . . . . . . . .1609609332 . . . . . . . . . . . .1609609335 . . . . . . . . . . . .160960933E . . . . . . . . . . . .1609609351 . . . . . . . . . . . .1609609352 . . . . . . . . . . . .1609609355 . . . . . . . . . . . .160960935E . . . . . . . . . . . .1609609361 . . . . . . . . . . . .160

9609362 . . . . . . . . . . . .1609609365 . . . . . . . . . . . .160960936E . . . . . . . . . . . .160960950210 . . . . . .160,198960950212 . . . . . .160,198960950220 . . . . . .160,198960950222 . . . . . .160,1989609510 . . . . . . . . . . . .1609609511 . . . . . . . . . . . .1609609512 . . . . . . . . . . . .1609609515 . . . . . . . . . . . .1609609517 . . . . . . . . . . . .1609609518 . . . . . . . . . . . .1609609519 . . . . . . . . . . . .160960951E . . . . . . . . . . . .1609609521 . . . . . . . . . . . .1609609522 . . . . . . . . . . . .1609609525 . . . . . . . . . . . .160960952E . . . . . . . . . . . .1609609531 . . . . . . . . . . . .1609609532 . . . . . . . . . . . .1609609535 . . . . . . . . . . . .160960953E . . . . . . . . . . . .1609609550 . . . . . . . . . . . .1609609551 . . . . . . . . . . . .1609609552 . . . . . . . . . . . .1609609555 . . . . . . . . . . . .1609609557 . . . . . . . . . . . .1609609558 . . . . . . . . . . . .1609609559 . . . . . . . . . . . .160960955E . . . . . . . . . . . .1609609560 . . . . . . . . . . . .1609609561 . . . . . . . . . . . .1609609562 . . . . . . . . . . . .1609609565 . . . . . . . . . . . .1609609567 . . . . . . . . . . . .1609609568 . . . . . . . . . . . .1609609569 . . . . . . . . . . . .160960956E . . . . . . . . . . . .1609609570 . . . . . . . . . . . .1609609571 . . . . . . . . . . . .1609609572 . . . . . . . . . . . .1609609575 . . . . . . . . . . . .1609609577 . . . . . . . . . . . .1609609578 . . . . . . . . . . . .1609609579 . . . . . . . . . . . .160960957E . . . . . . . . . . . .1609611311 . . . . . . . . . . . .1659611312 . . . . . . . . . . . .1659611315 . . . . . . . . . . . .165961131E . . . . . . . . . . . .1659611331 . . . . . . . . . . . .1659611332 . . . . . . . . . . . .1659611335 . . . . . . . . . . . .165961133E . . . . . . . . . . . .1659611351 . . . . . . . . . . . .1659611352 . . . . . . . . . . . .1659611355 . . . . . . . . . . . .165961135E . . . . . . . . . . . .1659611361 . . . . . . . . . . . .1659611362 . . . . . . . . . . . .1659611365 . . . . . . . . . . . .165961136E . . . . . . . . . . . .165961150210 . . . . . .165,198961150212 . . . . . .165,198961150220 . . . . . .165,198961150222 . . . . . .165,1989611510 . . . . . . . . . . . .1659611511 . . . . . . . . . . . .1659611512 . . . . . . . . . . . .1659611515 . . . . . . . . . . . .1659611517 . . . . . . . . . . . .1659611518 . . . . . . . . . . . .1659611519 . . . . . . . . . . . .165961151E . . . . . . . . . . . .1659611521 . . . . . . . . . . . .1659611522 . . . . . . . . . . . .1659611525 . . . . . . . . . . . .165961152E . . . . . . . . . . . .1659611531 . . . . . . . . . . . .1659611532 . . . . . . . . . . . .1659611535 . . . . . . . . . . . .165

961153E . . . . . . . . . . . .1659611550 . . . . . . . . . . . .1659611551 . . . . . . . . . . . .1659611552 . . . . . . . . . . . .1659611555 . . . . . . . . . . . .1659611557 . . . . . . . . . . . .1659611558 . . . . . . . . . . . .1659611559 . . . . . . . . . . . .165961155E . . . . . . . . . . . .1659611560 . . . . . . . . . . . .1659611561 . . . . . . . . . . . .1659611562 . . . . . . . . . . . .1659611565 . . . . . . . . . . . .1659611567 . . . . . . . . . . . .1659611568 . . . . . . . . . . . .1659611569 . . . . . . . . . . . .165961156E . . . . . . . . . . . .1659611570 . . . . . . . . . . . .1659611571 . . . . . . . . . . . .1659611572 . . . . . . . . . . . .1659611575 . . . . . . . . . . . .1659611577 . . . . . . . . . . . .1659611578 . . . . . . . . . . . .1659611579 . . . . . . . . . . . .165961157E . . . . . . . . . . . .1659612565 . . . . . . . . . . . .165KT676001-4035 . . . . . .343KT953751-0000 . . . . . .343KT953753-0000 . . . . . .343KT953761-0000 . . . . . .343KT953771-0000 . . . . . .343KT953781-0000 . . . . . .343KT953825-0000 . . . . . .343KT953826-0000 . . . . . .343KT953827-0000 . . . . . .343KT953828-0000 . . . . . .343KT953829-0000 . . . . . .343KT953830-0000 . . . . . .343KT953835-0000 . . . . . .343KT953845-0000 . . . . . .343


780 www.restek.com

INDEX

Alphabetical

AAAcccceessssoorriieess

GC . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .200 - 325HPLC . . . . . . . . . . . . . . . . . . . . . . . . . . . .326 - 351Sample Preparation . . . . . . . . . . . . . . . .387 - 407

AAddaappttoorrss.. SSeeee aallssoo CCoonnnneeccttoorrss..Micropacked Inlet Conversion Kits . . . . .133, 232Packed Column Inlet Adaptor Kit . . . . . . . . . . .133

AAddssoorrbbeenntt,, BBuullkk .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..442266AAggiilleenntt GGCC IInnssttrruummeenntt PPaarrttss .. .. .. .. .. .. .. .. .. .. .. ..222244 -- 224433AAggiilleenntt HHPPLLCC IInnssttrruummeenntt PPaarrttss .. .. .. .. .. .. .. .. .. ..332277,, 333322AAggiilleenntt SSuupppplliieess,, GGCC

Air Diverter . . . . . . . . . . . . . . . . . . . . . . . . . . . .230Autosampler Supplies . . . . . . . . . . . . . . . . . . .243Backpressure Regulator Kit . . . . . . . . . . . . . . .229Cables . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .242Capillary Column Nuts . . . . . . . . . . . . . . . . . . .221Capillary Installation Gauge . . . . . . . . . . . . . . .221Chemical Traps . . . . . . . . . . . . . . . . . . . . .229, 303Column Hanger . . . . . . . . . . . . . . . . . . . . .231, 277Compact Ferrules . . . . . . . . . . . . . . . . . . . . . . .284Detector Supplies

Cables . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .242ECD/FID Dual-Purpose Make-Up Gas Kit . . . . . . .241EZ No-Vent GC Column-Mass

Spectrometer Connector . . . . . . . . . . . . . . . . . . .234FID Collector Assemblies . . . . . . . . . . . . . . . . . . . .239FID Flow Measuring Adaptor . . . . . . . . . . . . .239, 275FID Gauge Pack . . . . . . . . . . . . . . . . . . . . . . . . . . .239FID Ignitor . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .239FID Jets . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .240FID Maintenance Kits . . . . . . . . . . . . . . . . . . . . . . .239FID/Injector Cleaning Kit . . . . . . . . . . . . . . . . . . . .241FID/NPD Adaptor Fitting . . . . . . . . . . . . . . . . . . . .241

GC/MS Consumables . . . . . . . . . . . . . . .234 - 237MSD Conversion Fitting . . . . . . . . . . . . . . . . . . . . .235MSD Source Nut . . . . . . . . . . . . . . . . . . . . . . . . . . .235Plug Nut, Injector/Detector . . . . . . . . . .219, 241, 278

Diffusion Pump Assemblies for MS . . . . . . . . .237Direct Injection Inserts . . . . . . . . . . . . . . . . . .232Dual-Column Analysis

Capillary Inlet Adaptor Fitting Kits . . . . . . . .233, 269Dual-Column Direct Injection Tee . . . . . . . . .233, 269Ferrules . . . . . . . . . . . . . . . . . . . . . . . . .233, 269, 285mini-Lam Direct Injection Tee . . . . . . . . . . . .233, 269Reducing Nut . . . . . . . . . . . . . . . . . . . . . . . . . . . . .228

Electron Multipliers . . . . . . . . . . . . . . . . . . . . .236EPC Test Kit . . . . . . . . . . . . . . . . . . . . . . . . . . . .228Finger-Tight Nuts . . . . . . . . . . . . . . . . . . . . . . .221Injection Ports . . . . . . . . . . . . . . . . . . . .224 - 226Injectors . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .232Inlet Adaptor Fitting Kits . . . . . . . . .228, 233, 269Inlet Liner Seals . . . . . . . . . . . . . . . . . . . .219, 227Inlet Liners . . . . . . . . . . . . . . . . . . .210, 216 - 218

Base-Deactivated . . . . . . . . . . . . . . . . . . . . . . . . . .213CIS4 and PTV . . . . . . . . . . . . . . . . . . . . . . . . . . . . .217Direct Injection . . . . . . . . . . . . . . . . . . . . . . . .210, 218Packing Materials and Tools . . . . . . . . . . . . .214, 215Siltek Metal . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .218Sky . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .210Split . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .210, 217Split/Splitless . . . . . . . . . . . . . . . . . . . . . . . . .210, 217Splitless . . . . . . . . . . . . . . . . . . . . . . . . . . . . .210, 216SPME . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .217Uniliner . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .210, 218

Inlet Maintenance Kits . . . . . . . . . . .221, 239, 275Inlet Seals . . . . . . . . . . . . . . . . . . . . . . . . . . . .223Interface Guide Tube for MS . . . . . . . . . . . . . .236Interface with Bellows for MS . . . . . . . . . . . . .235Microseal Septa . . . . . . . . . . . . . . . .219, 247, 262O-Rings, Inlet Liner . . . . . . . . . . . . . . . . . . . . .219

Oven Flapper Assemblies . . . . . . . . . . . . . . . . .230PTV Seals . . . . . . . . . . . . . . . . . . . . . . . . . . . . .223Septa . . . . . . . . . . . . . . . . . . . . . . . . . . . . .205, 219Septum Nuts . . . . . . . . . . . . . . . . . . . . . . . . . . .220Septum-Purged Packed Column

Port Weldment . . . . . . . . . . . . . . . . . . . . . . . .232Syringes . . . . . . . . . . . . . . . . . . . . . . . . . .370 - 372Tool Kit, MLE . . . . . . . . . . . . . . . . . . . . . . . . . . .231

AAggiilleenntt SSuupppplliieess,, HHPPLLCCSyringes, Autosampler . . . . . . . . . . . . . . . . . . .349

AAggiilleenntt SSyysstteemm RReeppllaacceemmeenntt PPaarrttss,, GGCC .. .. ..222244 -- 224433AAggiilleenntt SSyysstteemm RReeppllaacceemmeenntt PPaarrttss,, HHPPLLCC .. ..332277,, 333322AAiirr CCoommpprreessssoorr TTrraappss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..229988AAiirr DDiivveerrtteerr .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..223300AAiirr ((ZZeerroo)) GGeenneerraattoorrss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..330055,, 330088AAiirr MMoonniittoorriinngg

Section Table of Contents . . . . . . . . . . . . . . . . .408Canister Supplies . . . . . . . . . . . . . . . . . . .419, 420Canisters . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .421

Carrying Box Kit . . . . . . . . . . . . . . . . . . . . . . . . . . .419Carrying Case . . . . . . . . . . . . . . . . . . . . . . . . . . . . .419Cleaning System . . . . . . . . . . . . . . . . . . . . . . . . . . .418Dual Canister Sampling Manifold . . . . . . . . . . . . . .416Gauges . . . . . . . . . . . . . . . . . . . . . . . . . . . . .411 - 413Heating Jacket . . . . . . . . . . . . . . . . . . . . . . . . . . . .419Humidification Chamber . . . . . . . . . . . . . . . . . . . . .419Miniature . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .421Reconditioning Service . . . . . . . . . . . . . . . . . . . . . .422Sampling Timer . . . . . . . . . . . . . . . . . . . . . . . . . . .418SilcoCan . . . . . . . . . . . . . . . . . . . . . . . . . . . . .408 - 410TO-Can . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .411Valves . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .412

Gas StandardsBTEX Gas Mixture . . . . . . . . . . . . . . . . . . . . . . . . . .428Cylinder Stand . . . . . . . . . . . . . . . . . . . . . . . . . . . .430Japan Calibration . . . . . . . . . . . . . . . . . . . . . . . . . .428Natural Gas . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .431Ozone Precursor . . . . . . . . . . . . . . . . . . . . . . . . . . .430Refinery Gas . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .431Scott Transportable Gases . . . . . . . . . . . . . . . . . .432TO-14A . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .427, 428TO-15 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .428

PUF Cartridges . . . . . . . . . . . . . . . . . . . . . . . . .426Resin . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .426Sample Inlets . . . . . . . . . . . . . . . . . . . . . . . . . .415Sampling Bags . . . . . . . . . . . . . . . . . . . . . . . . .423Sampling Kits, Passive Air . . . . . . .414 - 417, 420Syringes . . . . . . . . . . . . . . . . . . . . . . . . . .385, 437Test Gauges . . . . . . . . . . . . . . . . . . . . . . . . . . .413Thermal Desorption Unit Tubes . . . . . . . . . . . .424Ultra-Clean Resin . . . . . . . . . . . . . . . . . . . . . . .426Vacuum Bag Sampler . . . . . . . . . . . . . . . . . . . .423

AAllaasskkaa UUSSTT RReeffeerreennccee SSttaannddaarrddss .. .. .. .. .. .. .. .. ..550055,, 550066AAlllleenn ((HHeexx KKeeyy)) WWrreenncchheess .. .. .. .. .. .. .. .. .. ..225577,, 228811,, 332233AAlllluurree HHPPLLCC CCoolluummnnss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..117788 -- 118811AAmmiinnee CCoolluummnn TTeesstt MMiixx .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..553388AAnnaallyyttiiccaall RReeffeerreennccee MMaatteerriiaallss.. SSeeee RReeffeerreennccee

SSttaannddaarrddss..AAnnttiiffooaamm AAggeenntt ffoorr

PPuurrggee && TTrraapp SSaammpplleess .. .. .. .. .. .. .. .. .. ..445522,, 445566,, 446688AAPPEEXX SSuupppplliieess .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..224444AApppplliiccaattiioonnss ((CChhrroommaattooggrraammss))

Table of Contents . . . . . . . . . . . . . . . . . . . . . . .541GC Applications . . . . . . . . . . . . . . . . . . . .545 - 707

GC Applications by Phase Index . . . . . . . . . .543, 544GC Compound Index for Applications . . . . .752 - 758

HPLC Applications . . . . . . . . . . . . . . . . . .710 - 751HPLC Applications by Phase Index . . . . . . . . . . . .709HPLC Compound Index . . . . . . . . . . . . . . . . . .759, 760

AArroocclloorr RReeffeerreennccee SSttaannddaarrddss .. .. .. ..446699,, 448822,, 449955,, 449966AArriizzoonnaa UUSSTT RReeffeerreennccee SSttaannddaarrddss .. .. .. .. .. .. .. .. .. .. .. ..550077

AASSEE EExxttrraaccttiioonn SSyysstteemmss,, PPaarrttss aanndd SSuupppplliieess .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..440000 -- 440033

AASSTTMM RReeffeerreennccee SSttaannddaarrddssClinical, Forensic & Toxicology . . . . . . . . . . . . .523Environmental . . . . . . . . . . . . . . . . . . . . . . . . . .513Foods, Flavors & Fragrances . . . . . . . . . . . . . .536Petroleum & Petrochemical . . . . . . . . . .515 - 517Pharmaceutical . . . . . . . . . . . . . . . . . . . . . . . . .529

AATTAASS AAcccceessssoorriieess .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..224444AATTAASS IInnjjeeccttoorr LLiinneerrss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..224444AAuuttoossaammpplleerr

Supplies for Agilent GCs . . . . . . . . . . . . . . . . .243Syringes . . . . . . . . . . . . . . . . . . . . . . . . . .370 - 377Syringes, HPLC . . . . . . . . . . . . . . . .346 - 349, 384Vials . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .363

AAvviiaattiioonn GGaass RReeffeerreennccee SSttaannddaarrddss .. .. .. .. .. .. .. .. .. .. .. ..550022

BBBaacckkpprreessssuurree RReegguullaattoorrss

Gas . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .312Gas Kit . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .229Mobile Phase . . . . . . . . . . . . . . . . . . . . . . . . . .345

BBaallll VVaallvveess .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..332222BBaassee--DDeeaaccttiivvaatteedd GGCC AAcccceessssoorriieess

Inlet Liners . . . . . . . . . . . . . . . . . . . . . . . . . . . .213Wool . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .214Fused Silica Guard Columns . . . . . . . . . . . . . . . .34

BBeecckkmmaann HHPPLLCC IInnssttrruummeenntt RReeppllaacceemmeenntt PPaarrttss .. ..332288BBeenncchh OOrrggaanniizzeerrss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..335500BBeennddeerr,, TTuubbiinngg .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..332255BBiiooddiieesseell RReeffeerreennccee SSttaannddaarrddss .. .. .. .. .. ..550022 -- 550044,, 551166BBiipphheennyyll HHPPLLCC CCoolluummnnss .. .. .. .. .. .. .. ..117700,, 117766,, 118800,, 119922BBllaannkk FFeerrrruulleess .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..228855BBoonnddeedd SSttaattiioonnaarryy PPhhaasseess,,

PPaacckkeedd CCoolluummnn .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..112233,, 112244,, 112266BBooookk HHoollddeerrss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..335500BBoottttllee TToopp,, PPTTFFEE ((EEccoo--CCaapp)) .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..333388BBoottttlleess,, MMoobbiillee PPhhaassee .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..333388BBrruusshheess,, TTuubbee .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..228811BBTTEEXX RReeffeerreennccee SSttaannddaarrddss .. .. ..442299,, 447711,, 7766,, 550033,, 550044BBTTOO SSeeppttaa .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..220055BBuubbbbllee FFlloowwmmeetteerrss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..227755BBuullkk AAddssoorrbbeennttss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..339988BBuullkk PPaacckkiinngg MMaatteerriiaallss

GC . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .134 - 137HPLC (Silica) . . . . . . . . . . . . . . . . . . . . . . . . . . .194

BBuurreettss,, GGllaasssswwaarree .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..440066BByy--PPaassss LLiinnee ffoorr TTeekkmmaarr PPuurrggee && TTrraapp .. .. .. .. .. .. .. ..227711

CCCaabblleess ffoorr AAggiilleenntt GGCCss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..224422CCaalliibbrraattiioonn MMiixxttuurreess.. SSeeee RReeffeerreennccee SSttaannddaarrddss..CCaalliiffoorrnniiaa UUSSTT RReeffeerreennccee SSttaannddaarrddss .. .. .. .. .. .. .. .. .. ..550077CCaanniisstteerr SSuupppplliieess .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..442200CCaanniisstteerrss

Carrying Cases . . . . . . . . . . . . . . . . . . . . . . . . .419Cleaning System . . . . . . . . . . . . . . . . . . . . . . . .418Dual Canister Sampling Manifold . . . . . . . . . . .416Gauges . . . . . . . . . . . . . . . . . . . . . . . . . .411 - 413Heating Jacket . . . . . . . . . . . . . . . . . . . . . . . . .419Humidification Chamber . . . . . . . . . . . . . . . . . .419Miniature . . . . . . . . . . . . . . . . . . . . . . . . . . . . .421Reconditioning Service . . . . . . . . . . . . . . . . . . .422Sampling Timer . . . . . . . . . . . . . . . . . . . . . . . . .418

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INDEX

AlphabeticalSilcoCan . . . . . . . . . . . . . . . . . . . . . . . . . .408 - 410TO-Can . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .411Tripod . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .419Valves . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .412

CCaappiillllaarryy GGCC CCoolluummnnBubble Flowmeters . . . . . . . . . . . . . . . . . . . . . .275Caps . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .278Cutting Tools

Sapphire Scribe . . . . . . . . . . . . . . . . . . . . . . . . . . .277Scoring Wafer . . . . . . . . . . . . . . . . . . . . . . . . . . . .277Tubing Cutter . . . . . . . . . . . . . . . . . . . . . . . . . . . . .324

Evaluation Mixtures . . . . . . . . . . . . . . . . . . . . .538Ferrules . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .284Inlet Liners. See Inlet Liners.Installation Gauge . . . . . . . . . . . . . . . . . . . . . .278Installation Tools . . . . . . . . . . . . . . . . . . .276 - 283Nuts . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .221Rinsing Reservoir . . . . . . . . . . . . . . . . . . . . . . .275

CCaappiillllaarryy GGCC CCoolluummnnssSection Table of Contents . . . . . . . . . . . . . . . . . .19Application-Specific Columns

Chiral Compounds . . . . . . . . . . . . . . . . . . . . . . . . . .68Clinical, Forensic & Toxicology . . . . . . . . . . . . . . . .82Environmental . . . . . . . . . . . . . . . . . . . . . . . . .87 - 103Foods, Flavors & Fragrances . . . . . . . . . . . . . .69 - 73Petroleum & Petrochemical . . . . . . . . . . . . . . .74 - 81Pharmaceutical . . . . . . . . . . . . . . . . . . . . . . . . .83 - 86Specially Acid Deactivated . . . . . . . . . . . . . . . . . . . .67Specially Base Deactivated . . . . . . . . . . . . . . .63 - 66

Applications (Chromatograms) . . . . . . . .490 - 703Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . .541GC Applications by Phase Index . . . . . . . . . .543, 544GC Compound Index for Applications . . . . .752 - 758

Chiral Columns . . . . . . . . . . . . . . . . . . . . . . . . . .68Column Installation Instructions . . . . . . . . . . . .30Column Selection . . . . . . . . . . . . . . . . . . . .23 - 29Cross-Reference Chart . . . . . . . . . . . . . . . . .28, 29FAMEWAX . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .70Fast GC . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .60GCxGC Selectivity Kit . . . . . . . . . . . . . . . . . . . . .61General Purpose Columns . . . . . . . . . . . . .49 - 59Guard Columns

Overview . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .31Base-Deactivated . . . . . . . . . . . . . . . . . . . . . . . . . . .34Hydroguard . . . . . . . . . . . . . . . . . . . . . . . . . . . .34, 114Integra-Guard (Built-in) . . . . . . . . . . . . . . . . . . . . . .35Intermediate-Polarity Deactivated . . . . . . . . .33, 114Polar Deactivated . . . . . . . . . . . . . . . . . . . . . . . . . . .33Siltek-Deactivated . . . . . . . . . . . . . . . . . . . . . . . . . .33

MXT ColumnsMXT-1 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .115MXT-1 Sim Dist . . . . . . . . . . . . . . . . . . . . . . . . .79, 120MXT-1301 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .117MXT-1701 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .118MXT-1HT Sim Dist . . . . . . . . . . . . . . . . . . .77, 78, 120MXT-20 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .116MXT-200 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .118MXT-2887 . . . . . . . . . . . . . . . . . . . . . . . . . . . . .77, 119MXT-35 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .117MXT-5 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .116MXT-50 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .117MXT-500 Sim Dist . . . . . . . . . . . . . . . . . . . . . . .79, 120MXT-502.2 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .121MXT-624 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .121MXT-65 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .117MXT-65TG . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .119MXT-Alumina BOND . . . . . . . . . . . . . . . . . . . . . . . .108MXT-Biodiesel TG . . . . . . . . . . . . . . . . . . . . . . .81, 119MXT-Msieve 5A . . . . . . . . . . . . . . . . . . . . . . . . . . . .109MXT-Q-BOND . . . . . . . . . . . . . . . . . . . . . . . . . . . . .110MXT-S-BOND . . . . . . . . . . . . . . . . . . . . . . . . . . . . .110MXT-Volatiles . . . . . . . . . . . . . . . . . . . . . . . . . . . . .121MXT-WAX . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .118

MXT Tubing Scorer . . . . . . . . . . . . . .114, 277, 324PLOT Column Particle Trap . . . . . . . . . . . . . . . .111Retention Gaps . . . . . . . . . . . . . . . . . . . . . .31 - 35Rt- Columns

Rt-2330 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .57Rt-2560 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .57, 69Rt-Alumina BOND PLOT . . . . . . . . . . . . . . .74, 76, 108Rt-βDEXcst . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .68Rt-βDEXm . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .68Rt-βDEXsa . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .68Rt-βDEXse . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .68Rt-βDEXsm . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .68Rt-βDEXsp . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .68Rt-CW20M F&F . . . . . . . . . . . . . . . . . . . . . . . . . . . . .71Rt-Msieve 5A PLOT . . . . . . . . . . . . . . . . . . . . . . . . .109Rt-Q-BOND PLOT . . . . . . . . . . . . . . . . . . . . . . . . . .110Rt-QS-BOND PLOT . . . . . . . . . . . . . . . . . . . . . . . . .110Rt-S-BOND PLOT . . . . . . . . . . . . . . . . . . . . . . . . . . .110Rt-TCEP . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .80Rt-U-BOND PLOT . . . . . . . . . . . . . . . . . . . . . . . . . .110Rt-XLSulfur Micropacked . . . . . . . . . . . . . . . . . . . .131Rt-XLSulfur Packed . . . . . . . . . . . . . . . . . . . . . . . . .131Rt-γDEXsa . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .68

Rtx- ColumnsRtx-1 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .49Rtx-1 F&F . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .71Rtx-1301 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .55Rtx-1614 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .92Rtx-1701 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .56Rtx-20 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .51Rtx-200 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .54Rtx-200MS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .54Rtx-225 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .56Rtx-2887 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .77Rtx-35 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .51Rtx-35 Amine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .65Rtx-440 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .53Rtx-5 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .50, 85Rtx-5 Amine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .64Rtx-5 DHA Tuning . . . . . . . . . . . . . . . . . . . . . . . . . . .75Rtx-5MS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .50Rtx-50 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .52Rtx-502.2 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .102Rtx-624 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .55Rtx-65 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .52Rtx-65TG . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .72Rtx-BAC1 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .82Rtx-BAC2 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .82Rtx-Biodiesel TG . . . . . . . . . . . . . . . . . . . . . . . . . . . .81Rtx-CLPesticides . . . . . . . . . . . . . . . . . . . . . . . . . . . .88Rtx-CLPesticides2 . . . . . . . . . . . . . . . . . . . . . . . . . . .88Rtx-DHA . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .75Rtx-Dioxin2 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .96Rtx-G27 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .86Rtx-G43 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .86Rtx-Mineral Oil . . . . . . . . . . . . . . . . . . . . . . . . . . . . .99Rtx-OPPesticides . . . . . . . . . . . . . . . . . . . . . . . . . . .91Rtx-OPPesticides2 . . . . . . . . . . . . . . . . . . . . . . . . . .91Rtx-PCB . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .93Rtx-VMS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .100Rtx-Volatile Amine . . . . . . . . . . . . . . . . . . . . . . . . . .63Rtx-Volatiles . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .102Rtx-VRX . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .101Rtx-Wax . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .58, 60

Rxi- ColumnsRxi-1HT . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .47Rxi-1ms . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .41Rxi-5HT . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .47Rxi-5ms . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .41Rxi-5Sil MS . . . . . . . . . . . . . . . . . . . . . . .42, 87, 95, 97Rxi-17 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .44Rxi-17Sil MS . . . . . . . . . . . . . . . . . . . . . . . . .45, 73, 98Rxi-35Sil MS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .44Rxi-624Sil MS . . . . . . . . . . . . . . . . . . . . . . .46, 83, 103Rxi-XLB . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .44, 94

Selecting a Column . . . . . . . . . . . . . . . . . . .23 - 29

Stabilwax ColumnsStabilwax . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .59, 84Stabilwax-DA . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .67Stabilwax-DB . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .66

Stx- ColumnsStx-CLPesticides . . . . . . . . . . . . . . . . . . . . . . . . . . . .90Stx-CLPesticides2 . . . . . . . . . . . . . . . . . . . . . . . . . . .90

Tubing Scorer, MXT . . . . . . . . . . . . . .114, 277, 324Tubing Scorers, Fused Silica . . . . . . . . . . . . . .277

CCaappiillllaarryy HHPPLLCC CCoolluummnnss .. .. .. .. .. .. .. .. .. .. .. ..pplleeaassee iinnqquuiirreeCCaappiillllaarryy TTuubbiinngg .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..331199 -- 332211CCaappiillllaarryy--GGrraaddee HHyyddrrooccaarrbboonn TTrraapp .. .. .. .. .. .. .. .. .. .. .. ..229988CCaappss,, CCoolluummnn EEnndd,, CCaappiillllaarryy GGCC .. .. .. .. .. .. .. .. .. .. .. .. .. ..227788CCaarrbbaammaattee RReeffeerreennccee SSttaannddaarrddss .. .. .. .. .. .. .. .. .. .. .. .. ..446611CCaarrbbooBBllaacckk

Packings . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .134Solid Supports . . . . . . . . . . . . . . . . . . . . . . . . .127

CCaarrbbooFFrriitt IInnlleett LLiinneerr PPaacckkiinngg MMaatteerriiaall .. .. .. .. .. .. .. .. ..221144CCaarrbbooFFrriitt IInnsseerrttss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..221144CCaarrbbooPPrreepp CCaarrttrriiddggeess .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..339933CCaarrbbooxxyylliicc AAcciidd CCaarrttrriiddggeess .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..339922CCaarrlloo EErrbbaa SSuupppplliieess.. SSeeee TThheerrmmoo SScciieennttiiffiicc GGCC

SSuupppplliieess..CCaarrrriieerr GGaass PPuurriiffiieerrss.. SSeeee GGaass PPuurriiffiieerrss..CCaattaalloogg NNuummbbeerr IInnddeexx .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..776611 -- 777799CCDD--RROOMMss

Pro ezGC . . . . . . . . . . . . . . . . . . . . . . . . . . .24, 580CCEE IInnssttrruummeennttss//TThheerrmmooQQuueesstt SSuupppplliieess..

SSeeee TThheerrmmoo SScciieennttiiffiicc GGCC SSuupppplliieess..CCeennttrriiffuuggee,, QQ--sseepp 33000000 .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..339900CCeerraammiicc SSccoorriinngg WWaaffeerr .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..227777CCeerrttiiffiieedd VViiaallss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..335577CCGGAA FFiittttiinnggss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..331111CChheecckk VVaallvveess,, HHPPLLCC .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..333322CChheemmiiccaall SSttaannddaarrddss.. SSeeee RReeffeerreennccee SSttaannddaarrddss..CChheemmiiccaall TTrraappss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..222299,, 330033CChhiirraall CCaappiillllaarryy GGCC CCoolluummnnss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..6688CChhlloorrddaannee SSoolluuttiioonnss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..446699,, 449955CChhlloorroopprreennee RReeffeerreennccee SSttaannddaarrddss .. .. .. .. .. .. .. .. .. .. .. ..447788CChhrroommaattooggrraapphh IInnssttaallllaattiioonn KKiitt .. .. .. .. .. .. .. .. .. .. .. .. .. ..332233CChhrroommaattooggrraammss ((AApppplliiccaattiioonnss))

Table of Contents . . . . . . . . . . . . . . . . . . . . . . .541GC Applications . . . . . . . . . . . . . . . . . . . .545 - 707

GC Applications by Phase Index . . . . . . . . . .543, 544GC Compound Index for Applications . . . . .752 - 758

HPLC Applications . . . . . . . . . . . . . . . . . .710 - 751HPLC Applications by Phase Index . . . . . . . . . . . .709HPLC Compound Index . . . . . . . . . . . . . . . . . .759, 760

CChhrroommaattooggrraapphhyy CCoolluummnnss.. SSeeee CCaappiillllaarryy GGCCCCoolluummnnss,, HHPPLLCC CCoolluummnnss,, PPLLOOTT CCoolluummnnss,, PPaacckkeeddCCoolluummnnss.. SSeeee aallssoo ccoolluummnn nnaammeess ((ee..gg..,, RRttxx))..

CChhrroommaattooggrraapphhyy SSeemmiinnaarrss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..1122,, 1133CChhrroommoossoorrbb PPaacckkiinnggss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..113366CClleeaann--CCuutt TTuubbiinngg CCuutttteerr .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..333333CCLLPP RReeffeerreennccee SSttaannddaarrddss .. .. .. .. .. .. .. .. .. .. .. .. .. ..448866 -- 449955CCooaattiinnggss,, TTuubbiinngg ((SSuurrffaaccee TTrreeaattmmeennttss))

Frequently Asked Questions . . . . . . . . . . . . . .318CCoolllleeccttoorr AAsssseemmbblliieess,, FFIIDD .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..223399CCoolluummnn HHaannggeerr ffoorr AAggiilleenntt GGCCss .. .. .. .. .. .. .. .. .. ..223311,, 227777CCoolluummnn HHeeaatteerr,, HHPPLLCC .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..334433CCoolluummnn IInnssttaallllaattiioonn IInnssttrruuccttiioonnss,, GGCC .. .. .. .. .. .. .. .. .. .. ..3300CCoolluummnn IInnssttaallllaattiioonn,, GGCC

Section Table of Contents . . . . . . . . . . . . . . . . .201Gauge . . . . . . . . . . . .221, 235, 252, 257, 263, 278Kits

Micropacked Columns . . . . . . . . . . . . . . . . . . . . . .133Packed Columns . . . . . . . . . . . . . . . . . . . . . . . . . . .133

Tools . . . . . . . . . . . . . . . .215, 221, 231, 239, 248, 275 - 277, 279, 281, 282, 367


782 www.restek.com

INDEX

AlphabeticalCCoolluummnn SSeelleeccttiioonn

GC . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .23 - 29HPLC . . . . . . . . . . . . . . . . . . . . . . . . . . . .150 - 152

CCoolluummnn TTeesstt MMiixxeessGC . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .538HPLC . . . . . . . . . . . . . . . . . . . . . . . . . . . . .199, 539

CCoolluummnnss.. SSeeee CCaappiillllaarryy GGCC CCoolluummnnss,, HHPPLLCC CCoolluummnnss,,PPLLOOTT CCoolluummnnss,, PPaacckkeedd CCoolluummnnss.. SSeeee aallssooccoolluummnn nnaammeess ((ee..gg..,, RRttxx))..

CCoommppaacctt FFeerrrruulleess ffoorr AAggiilleenntt GGCCss .. .. .. .. .. .. .. .. .. .. .. ..228844CCoommppaacctt SStteeeell RRuulleerr .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..228811CCoommppoossiittee FFuueell RReeffeerreennccee SSttaannddaarrddss ..550011,, 550022,, 550055CCoommppoouunndd IInnddeexx ffoorr AApppplliiccaattiioonn CChhrroommaattooggrraammss

GC Applications . . . . . . . . . . . . . . . . . . . .752 - 758HPLC Applications . . . . . . . . . . . . . . . . . . 759, 760

CCoonnnneeccttiiccuutt UUSSTT RReeffeerreennccee SSttaannddaarrddss .. .. .. .. .. .. .. .. ..550077CCoonnnneeccttoorrss,, CCoolluummnn

Gerstel GRAPHPACK 3D/2 . . . . . . . . . . . .227, 291MXT

MXT Low Dead-Volume . . . . . . . . . . . . . . . . . . . . .292MXT Low Dead-Volume “Y” . . . . . . . . . . . . . . . . . .292Replacement Nuts and Ferrules . . . . . . . . . . . . . .292

PEEK, HPLC . . . . . . . . . . . . . . . . . . . . . . . . . . . .334Press-Tight

Deactivated Universal . . . . . . . . . . . . . . . . . .288, 289Polyimide Resin . . . . . . . . . . . . . . . . . . . . . . .270, 288Siltek-Deactivated . . . . . . . . . . . . . . . . .270, 288 - 290Universal . . . . . . . . . . . . . . . . . . . . . . . . . . . .288, 289Universal Angled . . . . . . . . . . . . . . . . . . . . . . . . . .288Universal Angled “Y” . . . . . . . . . . . . . . . . . . .270, 288Universal “Y” . . . . . . . . . . . . . . . . . . . . .270, 288, 290

SeCure “Y” . . . . . . . . . . . . . . . . . . . . . . . .270, 290Valco . . . . . . . . . . . . . . . . . . . . . . . . .292, 293, 335Vu-Union, Vacuum . . . . . . . . . . . . . . . . . .227, 291Vu2-Union . . . . . . . . . . . . . . . . . . . . . . . . . . . . .289

CCoonnnneeccttoorrss,, TTuubbiinnggBrass . . . . . . . . . . . . . . . . . . . . . . . . .313, 314, 316PEEK . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .335Pipe . . . . . . . . . . . . . . . . . . . . . . . . . . . . .313 - 317Reducing . . . . . . . . . . . . . . . . . . . . . . . . .313 - 317Silcosteel-CR-Treated . . . . . . . . . . . . . . . .315, 317Siltek-Treated . . . . . . . . . . . . . . . . . . . . . .315, 317Stainless Steel . . . . . . . . . . . . . . . . .313, 314, 316Sulfinert-Treated . . . . . . . . . . . . . . . . . . .315, 317Transfer Line Reducing Kit . . . . . . . . . . . . . . . .258Tube . . . . . . . . . . . . . . . . . . . . . . . . . . . . .313 - 317Valco

Male Pipe to Valco Internal Adaptor . . . . . . . . . . .293Nuts and Ferrules . . . . . . . . . . . . . . . . . . . . . . . . .293One-Piece Fused Silica Adaptor . . . . . . . . . . . . . . .293Treated . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .317Zero Dead-Volume Internal Cross . . . . . . . . . . . . .293Zero Dead-Volume Internal Reducing Union . . . . .293Zero Dead-Volume Internal Tee . . . . . . . . . . . . . .293Zero Dead-Volume Internal Union . . . . . . . . .293, 335

Zero Dead-Volume . . . . . . . . . . . . . . . . . .293, 335CCoonnttrroolllleerrss,, FFllooww .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..441155CCooppppeerr TTuubbiinngg .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..331199CCrriimmpp--TToopp VViiaallss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..335566,, 336655

Aluminum Crimp Seals w/Septa . . . . . . . . . . .356Convenience Kits . . . . . . . . . . . . . . . . . . . . . . .356Limited Volume Inserts . . . . . . . . . . . . . . . . . .356Limited Volume Vials . . . . . . . . . . . . . . . . . . . .356Snap Seal Style . . . . . . . . . . . . . . . . . . . . .356, 365

CCrriimmpp--TToopp WWIISSPP VViiaallss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..336611Aluminum Seals w/Septa . . . . . . . . . . . . . . . . .361WISP 48 (Snap Seal) . . . . . . . . . . . . . . . . . . . .361

CCrriimmppeerrss,, VViiaall CCaappElectronic . . . . . . . . . . . . . . . . . . . . . . . . . . . . .366Squeeze-Type . . . . . . . . . . . . . . . . . . . . . . . . . .366

CCrroossss--RReeffeerreennccee CChhaarrttssGC Columns . . . . . . . . . . . . . . . . . . . . . . . . .28, 29PLOT Columns . . . . . . . . . . . . . . . . . . . . . . . . . .105Syringes . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .372USP (GC) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .139USP (HPLC) . . . . . . . . . . . . . . . . . . . . . . . . . . . .153

CCrroossss UUnniioonnss.. SSeeee CCoonnnneeccttoorrss,, UUnniioonnss..CCuussttoomm

Coated Packing Materials . . . . . . . . . . . . . . . .140Columns

Capillary GC . . . . . . . . . . . . . . . . . . . . .please inquire.HPLC . . . . . . . . . . . . . . . . . . . . . . . . . . .please inquire.Micropacked GC . . . . . . . . . . . . . . . . . . . . . . . . . . .141Packed GC . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .141

Request FormsReference Standards . . . .www.restek.com/solutionsPacked GC Columns . . . . . . . . . . . . . . . . . . . . . . . .142

CCuutttteerrss,, TTuubbiinngg .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..333333CCyyaannoopprrooppyyll SSPPEE CCaarrttrriiddggee .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..339922CCyycclloohheexxyyll SSPPEE CCaarrttrriiddggee .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..339922CCyylliinnddeerr HHoollddeerr .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..331122CCyylliinnddeerr SSttaanndd .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..443300CCyylliinnddeerr VVaallvvee WWrreenncchh .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..331122CCyylliinnddeerrss,, SSaammppllee .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..443355

DDD33660066 AApppplliiccaattiioonn CCoolluummnn SSeett,,

PPaacckkeedd CCoolluummnnss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..112288DDeeaaccttiivvaattiioonn

Guard Columns . . . . . . . . . . . . . . . . . . .33, 34, 114Liner Packings

Deactivated Wool . . . . . . . . . . . . . . . . . . . . . .214, 244Liners

Base-Deactivated . . . . . . . . . . . . . . . . . . . . . . . . . .213Siltek-Deactivated . . . . . . . . . . . . . . . . . . . . . . . . .213

DDeebbuubbbblleerrss,, HHPPLLCC .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..334400DDeeccaappppeerrss,, VViiaall

Electronic . . . . . . . . . . . . . . . . . . . . . . . . . . . . .366Squeeze-Type . . . . . . . . . . . . . . . . . . . . . . . . . .366

DDeeggaasssseerr,, HHPPLLCC .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..334411DDeerriivvaattiizzaattiioonn RReeaaggeennttss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..553377DDeetteeccttoorr SSuupppplliieess

Agilent GCsCables . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .242ECD/FID Dual-Purpose Make-Up Gas Kit . . . . . . .241EZ No-Vent GC Column-Mass Spectrometer

Connector . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .234FID/NPD Adaptor Fitting . . . . . . . . . . . . . . . . . . . .241FID Base Weldment . . . . . . . . . . . . . . . . . . . . . . . .238FID Collector Assemblies . . . . . . . . . . . . . . . . . . . .239FID Collector Housing Kit . . . . . . . . . . . . . . . . . . . .238FID Collector Mount . . . . . . . . . . . . . . . . . . . . . . . .238FID Flow Measuring Adaptor . . . . . . . . . . . . .239, 275FID Gauge Pack . . . . . . . . . . . . . . . . . . . . . . . . . . .239FID Ignitor . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .239FID Jet Removal Tool . . . . . . . . . . . . . . . . . . . . . . .240FID Jets . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .240FID Maintenance Kits . . . . . . . . . . . . . . . . . . .239, 275FID Spanner Wrench . . . . . . . . . . . . . . . . . . . . . . .238MSD Conversion Fitting . . . . . . . . . . . . . . . . . . . . .235MSD Source Nut . . . . . . . . . . . . . . . . . . . . . . . . . . .235Plug Nut, Injector/Detector . . . . . . . . . .219, 241, 278

Jet Reamers . . . . . . . . . . . . . . . . . . . . . . . . . . .282PerkinElmer GCs

FID Jet . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .248FID Part Kit . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .248Nozzle Insulator . . . . . . . . . . . . . . . . . . . . . . . . . . .248

PID Lamps . . . . . . . . . . . . . . . . . . . . . . . . . . . .271DDiiaapphhrraaggmm VVaallvveess .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..441100 -- 441122DDiiaattoommaacceeoouuss EEaarrtthh .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..339988

DDiiaattoommiittee PPaacckkiinnggss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..113344DDiieesseell RReeffeerreennccee SSttaannddaarrddss

Biodiesel Calibration Standards . . . . . . . . . . . .516Diesel Fuel #2 . . . . . . . . . . . .500 - 502, 506, 523Diesel Internal Standards . . . . . . . . . . . . . . . .504Diesel Surrogate Standards . . . . . . . . . . . . . . .504Diesel/Biodiesel Blend . . . . . . . . . .502 - 504, 516Low Sulfur . . . . . . . . . . . . . . . . . . . . . . . . .518, 519

DDiirreecctt IInnjjeeccttiioonn IInnlleett LLiinneerrssFor Agilent GCs . . . . . . . . . . . . . . . . . . . . .210, 218For PerkinElmer GCs . . . . . . . . . . . . . . . . . . . .246For Shimadzu GCs . . . . . . . . . . . . . . . . . . . . . .250For Thermo Scientific GCs . . . . . . . . . . . .253, 254For Varian GCs . . . . . . . . . . . . . . . . . . . .259 - 261

DDiirreecctt IInnjjeeccttiioonn IInnsseerrttss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..223322DDiisskkccoovveerr--4477

Extraction Disk Holder . . . . . . . . . . . . . . . . . . .397Reservoir . . . . . . . . . . . . . . . . . . . . . . . . . . . . .397

DDiisskkss,, SSPPEE .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..339977DDiissttrriibbuuttoorrss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..44,, 55DDNNPPHH RReeffeerreennccee SSttaannddaarrddss .. .. .. .. .. .. .. .. .. .. .. .. ..448833,, 551133DDrreessssiinngg TTooooll .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..332255,, 333333DDrriinnkkiinngg WWaatteerr RReeffeerreennccee MMaatteerriiaallss .. .. .. .. ..445511 -- 446633DDrruugg PPrreepp II SSPPEE CCaarrttrriiddggee .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..339944DDrruugg PPrreepp IIII SSPPEE CCaarrttrriiddggee .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..339944DDrruugg RReeffeerreennccee SSttaannddaarrddss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..552255DDuuaall--CCoolluummnn AAnnaallyyssiiss

ConnectorsSeCure “Y” . . . . . . . . . . . . . . . . . . . . . . . . . . .270, 290Siltek Press-Tight . . . . . . . . . . . . . . . . .270, 288 - 290Universal Angled Press-Tight . . . . . . . . . . . . . . . .288Universal Angled “Y” Press-Tight . . . . . . . . .270, 288Universal “Y” Press-Tight . . . . . . . . . . .270, 288, 290

Direct Injection Tee . . . . . . . . . . . . . . . . .233, 269Ferrules . . . . . . . . . . . . . . . . . . . . . .233, 269, 285For Agilent GCs

Capillary Inlet Adaptor Fitting Kit . . . . . . . . .233, 269Dual-Column Direct Injection Tee . . . . . . . . .233, 269mini-Lam Direct Injection Tee . . . . . . . . . . . .233, 269Reducing Nut . . . . . . . . . . . . . . . . . . . . . . . . . . . . .228

Inlet Adaptor Fitting Kits . . . . . . . . . . . . .233, 269Overview . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .268Packed Column Inlet Fittings

Direct Injection Tees . . . . . . . . . . . . . . . . . . .233, 269Graphite Ferrules . . . . . . . . . . . . . . . . . . . . . . . . . .269

DDuuaall--PPuurrppoossee MMaakkee--UUpp GGaass KKiitt .. .. .. .. .. .. .. .. .. .. .. .. .. ..224411DDuuaall VVeessppeell RRiinngg IInnlleett SSeeaallss .. .. .. .. .. .. .. .. .. .. .. ..222222,, 222233

EEECCDD//FFIIDD DDuuaall--PPuurrppoossee MMaakkee--UUpp GGaass KKiitt .. .. .. .. .. .. ..224411EECCDD VVeenntt TTrraapp .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..229988EELLCCDD SSuupppplliieess

Hall 1000 Replacement Accessories . . . . . . . .271Nickel Reaction Tubes . . . . . . . . . . . . . . . . . . . .271Teflon Transfer Lines . . . . . . . . . . . . . . . . . . . .271

EElleeccttrroonn MMuullttiipplliieerrss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..223366,, 225588EEnnccaappssuullaatteedd FFeerrrruulleess .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..228844EEnnvviirroonnmmeennttaall AAnnaallyyssiiss RReeffeerreennccee SSttaannddaarrddss.. SSeeee

RReeffeerreennccee SSttaannddaarrddss..EEPPAA MMeetthhoodd RReeffeerreennccee SSttaannddaarrddss

1311 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4701664 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .470418.1 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .470500 Series Methods . . . . . . . . . . . . . . . .451 - 463600 Series Methods . . . . . . . . . . . . . . . .464 - 4698000 Series Methods . . . . . . . . . . . . . . .470 - 485CLP . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .486 - 495

EEuurrooppeeaann PPhhaarrmmaaccooppooeeiiaa MMeetthhoodd .. .. .. .. .. .. .. ..552288,, 552299


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INDEX

AlphabeticalEEvvaalluuaattiioonn MMiixxttuurreess,, CCoolluummnn .. .. .. .. .. .. .. .. .. .. .. ..553388,, 553399EEvvaappoorraattoorr AAppppaarraattuuss,, GGllaasssswwaarree .. .. .. .. .. .. .. .. .. .. .. ..440044EExxpplloossiivveess RReeffeerreennccee SSttaannddaarrddss .. .. .. .. .. .. .. .. .. .. .. .. ..447733EExxttrraaccttiioonn AAppppaarraattuuss,, GGllaasssswwaarree .. .. .. .. .. .. .. .. .. .. .. .. ..440044EExxttrraaccttiioonn SSyysstteemm PPaarrttss

ASE . . . . . . . . . . . . . . . . . . . . . . . . . . . . .400 - 403SPE . . . . . . . . . . . . . . . . . . . . . . . . . . . . .395 - 397

EEZZ NNoo--VVeenntt GGCC CCoolluummnn--MMaassss SSppeeccttrroommeetteerrCCoonnnneeccttoorr .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..223344,, 225588,, 226644

FFFAAMMEEWWAAXX CCaappiillllaarryy GGCC CCoolluummnn .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..7700FFaattttyy AAcciidd MMeetthhyyll EEsstteerr MMiixxttuurreess .. .. .. .. .. .. .. .. ..553322,, 553333FFeerrrruullee RReemmoovvaall KKiitt .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..229911FFeerrrruulleess

Alumaseal . . . . . . . . . . . . . . . . . . . . . . . . . . . . .285Blank . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .285Capillary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .284Compact—for Agilent GCs . . . . . . . . . . . . . . . .284Dual-Column . . . . . . . . . . . . . . . . . . .233, 269, 285Encapsulated . . . . . . . . . . . . . . . . . . . . . . . . . .284EZ No-Vent . . . . . . . . . . . . . . . . . . . .234, 258, 264For Agilent GCs . . . . . . . . . . . . . . . . . . . . . . . . .284For MXT Connectors . . . . . . . . . . . . . . . . . . . . .292For Shimadzu GCs . . . . . . . . . . . . . . . . . .251, 286For Thermo Scientific GCs . . . . . . . . . . . .256, 286M4 Fitting . . . . . . . . . . . . . . . . . . . . . . . . .256, 286Reducing . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .285SeCure “Y” Connector . . . . . . . . . . . . . . . . . . .290Standard . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .285Two-Hole . . . . . . . . . . . . . . . . . . . . . .233, 269, 285Vu2-Union Connector . . . . . . . . . . . . . . . .289, 291

FFIIDD PPaarrttss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..224477,, 224488FFIIDD PPeerrffoorrmmaannccee EEvvaalluuaattiioonn SSttaannddaarrdd .. .. .. .. .. .. .. .. ..553399FFIIDD SSuupppplliieess.. SSeeee DDeetteeccttoorr SSuupppplliieess..FFiilltteerrss

For ASE Extraction Cells . . . . . . . . . . . . . .400, 401Gas. See Gas Purifiers.In-Line, Air Sampling . . . . . . . . . . . . . . . . . . . .415Inlet, HPLC . . . . . . . . . . . . . . . . . . . . . . . . . . . .342Last Drop, HPLC . . . . . . . . . . . . . . . . . . . . . . . .342Mobile Phase . . . . . . . . . . . . . . . . . . . . . . . . . .342Passive Air Sampling . . . . . . . . . . . . . . . . . . . .415Resprep SPE Flow Filter . . . . . . . . . . . . . . . . . .397Syringe Filters . . . . . . . . . . . . . . . . . . . . . . . . .399UHPLC . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .195

FFiillttrraattiioonn GGllaasssswwaarree .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..334433FFiinnggeerr--TTiigghhtt NNuuttss,, GGCC .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..222211FFiirree DDeebbrriiss RReeffeerreennccee SSttaannddaarrddss .. .. .. .. ..550022,, 551133,, 552233FFiissoonnss SSuupppplliieess.. SSeeee TThheerrmmoo SScciieennttiiffiicc GGCC SSuupppplliieess..FFiittttiinnggss

Brass . . . . . . . . . . . . . . . . . . . . . . . . .313, 314, 316CGA . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .311Column End, HPLC . . . . . . . . . . . . . . . . . . . . . .351Kits . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .313MSD Conversion . . . . . . . . . . . . . . . . . . . . . . . .235Packed Column . . . . . . . . . . . . . . . . . . . . . . . . .142Packed Column Inlet Adaptor Kit . . . . . . . . . . .133Packed Column Reduction . . . . . . . . . . . . . . . .125Pipe (Parker) . . . . . . . . . . . . . . . . . . . . . .316, 317Pipe (Swagelok) . . . . . . . . . . . . . . . . . . .313 - 315Pipe-to-Tube . . . . . . . . . . . . . . . . . .310, 313 - 317Reduction . . . . . . . . . . . . . . . . . . . .125, 313 - 316Secure-Fit, HPLC . . . . . . . . . . . . . . . . . . . . . . . .335Silcosteel-CR-Treated . . . . . . . . . . . . . . . .315, 317Siltek-Treated . . . . . . . . . . . . . . . . . . . . . .315, 317

Stainless Steel . . . . . . . . . . . . . . . . .313, 314, 316Sulfinert-Treated . . . . . . . . . . . . . . . . . . .315, 317Tube (Parker) . . . . . . . . . . . . . . . . . . . . . .316, 317Tube (Swagelok) . . . . . . . . . . . . . . . . . . .313 - 315Valco (Treated) . . . . . . . . . . . . . . . . . . . . . . . . .317Welded Reducers, Packed Column . . . . . . . . .125Welded VCR, Packed Column . . . . . . . . . . . . . .125

FFllaasshh AArrrreessttoorr .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..331111FFllaasshhlliigghhtt .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..228822,, 332255FFllaasskkss,, GGllaasssswwaarree .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..440055,, 440066FFlleexxiibbllee SSttaaiinnlleessss SStteeeell HHoossee .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..331111FFlloorriiddaa UUSSTT RReeffeerreennccee SSttaannddaarrddss .. .. .. .. .. .. .. .. .. .. .. .. ..550077FFlloorriissiill CCaarrttrriiddggee QQuuaalliittyy CCoonnttrrooll SSttaannddaarrdd .. .. .. .. ..550000FFlloorriissiill SSPPEE CCaarrttrriiddggee .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..339922FFllooww CCoonnttrroolllleerr,, VVeerriiffllooww AAiirr SSaammpplliinngg .. .. .. .. .. .. .. ..441155FFlloowwmmeetteerrss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..220033,, 227744,, 227755FFoooodd TTeessttiinngg RReeffeerreennccee SSttaannddaarrddss .. .. .. .. .. .. .. .. .. .. ..553366FFrriittss

Air Sampling . . . . . . . . . . . . . . . . . . . . . . . . . . .415HPLC . . . . . . . . . . . . . . . . . . . . . . . . .196, 197, 351SPE . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .394

FFuueell OOiill DDeeggrraaddaattiioonn MMiixx .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..550033FFuueell RReeffeerreennccee SSttaannddaarrddss.. SSeeee RReeffeerreennccee SSttaannddaarrddss..FFuunnnneellss,, GGllaasssswwaarree .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..440066FFuusseedd SSiilliiccaa

Adaptors. See Connectors.Capillary Columns. See Capillary GC Columns.

See also column names (e.g., Rtx).GCxGC Selectivity Kit . . . . . . . . . . . . . . . . . . . . .61Guard Columns . . . . . . . . . . . . . . . .31, 33, 34, 114Retention Gaps . . . . . . . . . . . . . . . . . . . . . .31 - 35

GGGaass

Cylinder Holder . . . . . . . . . . . . . . . . . . . . . . . . .312Filters. See Gas Purifiers.Flowmeters . . . . . . . . . . . . . . . . . . . .203, 274, 275Generators

Hydrogen . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .304Hydrogen/Zero Air (FID Stations) . . . . . . . . . . . . .305International Power Cord Sets . . . . . . . . . . .305 - 308Nitrogen . . . . . . . . . . . . . . . . . . . . . . . . . . . . .306, 307Zero Air . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .305, 308Zero Air/Hydrogen (FID Stations) . . . . . . . . . . . . .305

Leak Detectors . . . . . . . . . . . . . . . . .204, 273, 296Management System . . . . . . . . . . . . . . . . . . . .296Pressure Regulators. See Regulators.Purifiers

Chemical and Vent Traps . . . . . . . . . . . . . . . .297, 298Overview . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .295Restek Gas Management System . . . . . . . . . . . . .296Super-Clean Gas Purifiers . . . . . . . . . . . . . . .299, 300Thermal Gas Purifier . . . . . . . . . . . . . . . . . . . . . . .303VICI/Matsen Modules . . . . . . . . . . . . . . . . . . . . . .303

Reference Standards . . .427 - 432, 471, 476, 503Sampling

Cylinders . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .435Loops . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .437Valves . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .436, 437

GGaass PPuurriiffiiccaattiioonn EEsssseennttiiaallssSection Table of Contents . . . . . . . . . . . . . . . . .201Fittings . . . . . . . . . . . . . . . . . . . . . . . . . . .313 - 317Flowmeters . . . . . . . . . . . . . . . . . . . . . . . .203, 274Gas Purification . . . . . . . . . . . . . . . . . . . .295 - 303Generators . . . . . . . . . . . . . . . . . . . . . . .304 - 308Installation Tools . . . . . . . . . . . . . . . . . . . . . . .323Leak Detector . . . . . . . . . . . . . . . . . . . . . . . . . .296Overview . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .295

Regulators & Accessories . . . . . . . . . . .309 - 312Tubing & Fitting Tools . . . . . . . . . . . . . . .324 - 325Tubing & Valves . . . . . . . . . . . . . . . . . . . .318 - 322

GGaass--TTiigghhtt SSyyrriinnggeess .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..337711,, 338811,, 338833GGaassoolliinnee RReeffeerreennccee SSttaannddaarrddss

Gasoline Internal Standards . . . . . . . . . . . . . .504Gasoline Range Organics . . . . . . . . . . . . . . . . .503Gasoline Surrogate Standards . . . . . . . . . . . . .504Gasoline, Low Sulfur . . . . . . . . . . . . . . . . . . . . .519Gasoline, Unleaded . . . . . . . . .501, 502, 505, 523

GGaauuggeessFID . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .239Gap Inspection Gauge . . . . . . . . . . . . . . . . . . .325Test, Air . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .413Vacuum . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .412Vacuum/Pressure . . . . . . . . . . . . . . . . . .411, 412

GGCC AAcccceessssoorriieess.. SSeeee IInnssttrruummeenntt SSuupppplliieess,, GGCC..GGCC CChhrroommaattooggrraapphh IInnssttaallllaattiioonn KKiitt .. .. .. .. .. .. .. .. .. .. .. ..332233GGCC CCoolluummnn TTeesstt MMiixxeess .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..553388GGCC CCoolluummnnss.. SSeeee CCaappiillllaarryy GGCC CCoolluummnnss,, PPLLOOTT

CCoolluummnnss,, PPaacckkeedd CCoolluummnnss.. SSeeee aallssoo ccoolluummnn nnaammeess ((ee..gg..,, RRttxx))..

GGCC PPhhaasseess CCrroossss--RReeffeerreennccee .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..2288GGCC//MMSS CClleeaanniinngg KKiitt .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..223377GGCC//MMSS TTuunniinngg MMiixxttuurree .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..446699,, 447799GGCCxxGGCC SSeelleeccttiivviittyy KKiitt .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..6611GGeenneerraattoorrss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..330044 -- 330088GGeerrsstteell GGRRAAPPHHPPAACCKK CCoonnnneeccttoorrss .. .. .. .. .. .. .. .. ..222277,, 229911GGllaassss IImmppiinnggeerrss,, MMiiddggeett .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..440077GGllaasssswwaarree .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..440044 -- 440077

Burets . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .406Evaporator Apparatus . . . . . . . . . . . . . . . . . . .404Extraction Apparatus . . . . . . . . . . . . . . . . . . . .404Flasks . . . . . . . . . . . . . . . . . . . . . . . . . . . .405, 406Funnels . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .406Glass Impingers, Midget . . . . . . . . . . . . . . . . .407Membrane Filtration . . . . . . . . . . . . . . . . . . . . .343Pipets . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .407Stopper . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .407

GGlloovvee BBooxx DDiissppeennsseerrss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..335500GGrraapphhiittee OO--RRiinnggss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..221199,, 224477,, 225511GGrraapphhiittee SSeeaalliinngg RRiinngg .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..225555GGRRAAPPHHPPAACCKK 33DD//22 FFeerrrruulleess .. .. .. .. .. .. .. .. .. .. .. .. ..222277,, 229911GGrroobb TTeesstt MMiixx .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..553388GGuuaarrdd CCoolluummnn HHoollddeerrss,, HHPPLLCC .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..119977GGuuaarrdd CCoolluummnn PPaarrttss,, HHPPLLCC .. .. .. .. .. .. .. .. .. .. .. .. .. ..119966,, 119977GGuuaarrdd CCoolluummnnss

GCBase-Deactivated . . . . . . . . . . . . . . . . . . . . . . . . . . .34Built-In (Integra-Guard) . . . . . . . . . . . . . . . . . . . . . .35Capillary GC . . . . . . . . . . . . . . . . . .31, 33, 34, 40, 114Fused Silica . . . . . . . . . . . . . . . . . . . . .31, 33, 34, 114Hydroguard Water-Resistant . . . . . . . . . . . . . .34, 114Integra-Guard . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .35Intermediate-Polarity Deactivated . . . . . . . . . . . . .33MXT Stainless Steel . . . . . . . . . . . . . . . . . . . . . . . .114Overview . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .31Polar-Deactivated . . . . . . . . . . . . . . . . . . . . . . . . . . .33SFC/CE Narrow-Bore . . . . . . . . . . . . . . . . . . . . . . . .33Siltek-Deactivated . . . . . . . . . . . . . . . . . . . . . . . . . .33

HPLCAllure . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .178 - 181Pinnacle DB . . . . . . . . . . . . . . . . . . . . . . . . . .166 - 172Pinnacle II . . . . . . . . . . . . . . . . . . . . . . . . . . .173 - 177Trident . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .196 - 198Ultra . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .182 - 189Ultra II . . . . . . . . . . . . . . . . . . . . . . . . . . . . .157 - 165Viva (Wide-Pore) . . . . . . . . . . . . . . . . . . . . . .190 - 193


784 www.restek.com

INDEX

Alphabetical

HHHaallll EELLCCDD RReeppllaacceemmeenntt AAcccceessssoorriieess .. .. .. .. .. .. .. .. .. ..227711HHaallooaacceettiicc AAcciidd RReeffeerreennccee SSttaannddaarrddss .. .. .. .. .. .. .. .. ..446622HHaayyeeSSeepp PPaacckkiinnggss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..113377HHeeaaddssppaaccee VViiaallss

20mm Aluminum Seals w/Septa, Assembled .363Headspace Autosampler Vials . . . . . . . . . . . . .363Screw Thread . . . . . . . . . . . . . . . . . . . . . . . . . .363Screw Thread Caps . . . . . . . . . . . . . . . . . . . . . .363

HHeelliiuumm SSppaarrggeerrss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..334422HHeerrbbiicciiddee RReeffeerreennccee SSttaannddaarrddss .. .. .. .. .. ..445555,, 445588,, 446622,,

446633,, 446666,, 447700,, 447755,, 448844HHeexx KKeeyy ((AAlllleenn)) WWrreenncchheess .. .. .. .. .. .. .. .. .. ..225577,, 228811,, 332233HHiigghh--PPuurriittyy VV..OO..CC.. RReegguullaattoorr .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..443333HHiigghh--TTeemmppeerraattuurree SSttrriinngg .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..228811HHiittaacchhii HHPPLLCC IInnssttrruummeenntt PPaarrttss .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..332288HHoossee,, FFlleexxiibbllee SSttaaiinnlleessss SStteeeell .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..331111HHPPLLCC

Section Table of Contents, Accessories . . . . . .326Section Table of Contents, Columns . . . . . . . . .144Accessories . . . . . . . . . . . . . . . . . . . . . . .326 - 351Applications (Chromatograms) . . . . . . . .710 - 751

Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . .708HPLC Applications by Phase Index . . . . . . . . . . . .709HPLC Compound Index . . . . . . . . . . . . . . . . . .759, 760

Biphenyl HPLC Columns . . . . . .160, 170, 176, 180Bottle Tops . . . . . . . . . . . . . . . . . . . . . . . .338, 339Bulk Packing Materials . . . . . . . . . . . . . . . . . . .194Capillary Columns . . . . . . . . . . . . . .please inquireColumn Hardware

Column End Fittings . . . . . . . . . . . . . . . . . . . .334, 351Column Tubing . . . . . . . . . . . . . . . . . . . . . . . . . . . .351Empty Columns . . . . . . . . . . . . . . . . . . . . . . . . . . . .351Frits . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .351

Column Heater . . . . . . . . . . . . . . . . . . . . . . . . .343Column Packing Kit . . . . . . . . . . . . . . . . . . . . . .351Column Selection . . . . . . . . . . . . . . . . . .145 - 149Column Test Mixes . . . . . . . . . . . . . . . . . .199, 539Columns

Section Table of Contents . . . . . . . . . . . . . . . . . . .144Allure AK . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .181Allure Aqueous C18 . . . . . . . . . . . . . . . . . . . . . . . .179Allure Basix . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .178Allure Biphenyl . . . . . . . . . . . . . . . . . . . . . . . . . . . .180Allure C18 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .178Allure Organic Acids . . . . . . . . . . . . . . . . . . . . . . . .180Allure PFP Propyl . . . . . . . . . . . . . . . . . . . . . . . . . .179Allure Silica . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .181Capillary Columns . . . . . . . . . . . . . . . . .please inquirePinnacle DB Aqueous C18 . . . . . . . . . . . . . . . . . . .171Pinnacle DB Biphenyl . . . . . . . . . . . . . . . . . . . . . . .170Pinnacle DB C18 . . . . . . . . . . . . . . . . . . . . . . . . . . .166Pinnacle DB C8 . . . . . . . . . . . . . . . . . . . . . . . . . . . .167Pinnacle DB Cyano . . . . . . . . . . . . . . . . . . . . . . . . .168Pinnacle DB IBD . . . . . . . . . . . . . . . . . . . . . . . . . . .171Pinnacle DB PAH . . . . . . . . . . . . . . . . . . . . . . . . . .172Pinnacle DB PFP Propyl . . . . . . . . . . . . . . . . . . . . .169Pinnacle DB Phenyl . . . . . . . . . . . . . . . . . . . . . . . .168Pinnacle DB Silica . . . . . . . . . . . . . . . . . . . . . . . . . .172Pinnacle II Amino . . . . . . . . . . . . . . . . . . . . . . . . . .176Pinnacle II Biphenyl . . . . . . . . . . . . . . . . . . . . . . . .176Pinnacle II C18 . . . . . . . . . . . . . . . . . . . . . . . . . . . .173Pinnacle II C8 . . . . . . . . . . . . . . . . . . . . . . . . . . . . .174Pinnacle II Cyano . . . . . . . . . . . . . . . . . . . . . . . . . .175Pinnacle II PAH . . . . . . . . . . . . . . . . . . . . . . . . . . .174Pinnacle II Phenyl . . . . . . . . . . . . . . . . . . . . . . . . .175Pinnacle II Silica . . . . . . . . . . . . . . . . . . . . . . . . . .177Prep Columns . . . . . . . . . . . . . . . . . . . . . . . .157 - 191Small Particle Columns . . . . . . . . . . . . . . . . .166 - 172UHPLC . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .166 - 172Ultra Amino . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .186Ultra Aqueous C18 . . . . . . . . . . . . . . . . . . . . . . . . .183

Ultra C1 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .185Ultra C18 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .182Ultra C4 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .184Ultra C8 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .183Ultra Carbamate . . . . . . . . . . . . . . . . . . . . . . . . . . .188Ultra Cyano . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .185Ultra IBD . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .184Ultra II Aromax . . . . . . . . . . . . . . . . . . . . . . . . . . .161Ultra II Aqueous C18 . . . . . . . . . . . . . . . . . . . . . . .159Ultra II Biphenyl . . . . . . . . . . . . . . . . . . . . . . . . . . .160Ultra II C18 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .157Ultra II C8 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .158Ultra II Carbamate . . . . . . . . . . . . . . . . . . . . . . . . .165Ultra II IBD . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .162Ultra II PFP Propyl . . . . . . . . . . . . . . . . . . . . . . . . .163Ultra II Quat . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .165Ultra II Silica . . . . . . . . . . . . . . . . . . . . . . . . . . . . .164Ultra PFP . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .187Ultra Phenyl . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .186Ultra Quat . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .189Ultra Silica . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .188Viva Biphenyl (Wide-Pore) . . . . . . . . . . . . . . . . . . .192Viva C18 (Wide-Pore) . . . . . . . . . . . . . . . . . . . . . . .190Viva C4 (Wide-Pore) . . . . . . . . . . . . . . . . . . . . . . . .191Viva C8 (Wide-Pore) . . . . . . . . . . . . . . . . . . . . . . . .191Viva PFP Propyl (Wide-Pore) . . . . . . . . . . . . . . . . .192Viva Silica (Wide-Pore) . . . . . . . . . . . . . . . . . . . . .193

FiltersFilter Kit . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .339Last Drop Filter . . . . . . . . . . . . . . . . . . . . . . . . . . .342Low-Pressure CPI Inlet Filter . . . . . . . . . . . . . . . .342Low-Pressure Slip-on Inlet Filter . . . . . . . . . . . . . .342Membrane Filtration Glassware . . . . . . . . . . . . . .343UHPLC . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .195

Fittings & ToolsCheck Valves . . . . . . . . . . . . . . . . . . . . . . . . . . . . .332PEEK Fitting Extractor . . . . . . . . . . . . . . . . . . . . . .337PEEK Performance Kit . . . . . . . . . . . . . . . . . . . . . .336PEEK Union Connector . . . . . . . . . . . . . . . . . . . . . .335Piston Seal Insertion Tool . . . . . . . . . . . . . . . . . . .337Piston Seals . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .332Rheodyne Style Nut and Ferrule . . . . . . . . . . . . . .334Secure-Fit Fittings . . . . . . . . . . . . . . . . . . . . . . . . .335Survival Kit . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .336Tube Fittings . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .335Tubing Cutter . . . . . . . . . . . . . . . . . . . . . . . . . . . . .333Tubing Cutter Dressing Tool . . . . . . . . . . . . . . . . .333Universal Column Connector . . . . . . . . . . . . . . . . .334ValvTool Wrench for 1/4-Inch Nuts . . . . . . . . . . . .337

Guard ColumnsAllure . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .178 - 181Pinnacle DB . . . . . . . . . . . . . . . . . . . . . . . . . .166 - 172Pinnacle II . . . . . . . . . . . . . . . . . . . . . . . . . . .173 - 177Trident . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .196 - 198Ultra . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .182 - 189Ultra II . . . . . . . . . . . . . . . . . . . . . . . . . . . . .157 - 165Viva (Wide-Pore) . . . . . . . . . . . . . . . . . . . . . .190 - 193

Instrument Replacement Parts . . . . . . .327 - 332Lamps . . . . . . . . . . . . . . . . . . . . . . . . . . .327 - 330Mobile Phase

Accessories . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .338Backpressure Regulators . . . . . . . . . . . . . . . . . . . .345Bottle Tops . . . . . . . . . . . . . . . . . . . . . . . . . . .338, 339Bottles . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .338Debubblers . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .340Degasser . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .341Filter Kit . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .339Filters . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .342Flow Splitters . . . . . . . . . . . . . . . . . . . . . . . . . . . . .344Mixers, In-Line . . . . . . . . . . . . . . . . . . . . . . . . . . . .344Pre-heater . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .343Pulse Dampers . . . . . . . . . . . . . . . . . . . . . . . . . . . .340Restek Survival Kit for HPLC . . . . . . . . . . . . . . . . .336Waste Overflow Indicator . . . . . . . . . . . . . . . . . . .338

OrganizersBook Holders . . . . . . . . . . . . . . . . . . . . . . . . . . . . .350Deluxe BenchBooster Organizer . . . . . . . . . . . . . .350Glove Box Dispensers . . . . . . . . . . . . . . . . . . . . . .350

HPLC 30 Column Storage Cabinet . . . . . . . . . . . . .350LCLocker HPLC Organizer . . . . . . . . . . . . . . . . . . .350Mini pHPerch Storage Unit . . . . . . . . . . . . . . . . . .350Open Supply Bins . . . . . . . . . . . . . . . . . . . . . . . . . .350TopLoader BalanceBank Storage Unit . . . . . . . . . .350

Prep Columns . . . . . . . . . . . . . . . . . . . . .157 - 191Pump Parts . . . . . . . . . . . . . . . . . . . . . . . .327, 331Small Particle Columns . . . . . . . . . . . . . .166 - 172Survival Kit for HPLC . . . . . . . . . . . . . . . . . . . .336Syringes

Autosampler . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .349Gas-Tight Syringes for

Rheodyne & Valco Valves . . . . . . . . . . . . . .347, 384Microliter Liquid-Type Syringes . . . . . . . . . . . . . . .348Priming Syringes for Waters HPLC Pumps . . . . . .348Syringes for Waters U6K Valves . . . . . . . . . . . . . .346

Tools . . . . . . . . . . . . . . . . . . . . . . . . . . . . .336, 337Trident Direct Guard Column System . . . . . . . .197Trident Guard Cartridges and Holders . .197, 198Trident Integral Guard Column System . . . . . .196Tubing

PEEK Tubing . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .332PEEK Tubing Elbows . . . . . . . . . . . . . . . . . . . . . . . .333Stainless Steel Tubing . . . . . . . . . . . . . . . . . . . . . .332Teflon Tubing . . . . . . . . . . . . . . . . . . . . . . . . . . . . .333Tubing Clip . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .333

UHPLC Columns . . . . . . . . . . . . . . . . . . . .166 - 172US Pharmacopeia Cross Reference . . . . . . . . .153Valves . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .345Wide-Pore Columns . . . . . . . . . . . . . . . .190 - 193

HHPPLLCC AAcccceessssoorriieess .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..332266 -- 335511HHPPLLCC PPuummpp PPrreessssuurree CCoonnvveerrssiioonn TTaabbllee .. .. .. .. .. .. .. ..114499HHuubb--CCaapp .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..333399HHuummiiddiiffiiccaattiioonn CChhaammbbeerr,, CCaanniisstteerr .. .. .. .. .. .. .. .. .. .. .. ..441199HHyyddrrooccaarrbboonn TTrraappss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..229988HHyyddrrooggeenn GGeenneerraattoorrss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..330044HHyyddrroogguuaarrdd TTuubbiinngg .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..3344,, 111144

IIIcceeBBlluuee SSeeppttaa .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..220055IIggnniittoorr,, FFIIDD .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..223399IInn--LLiinnee FFiilltteerrss

Air Sampling . . . . . . . . . . . . . . . . . . . . . . . . . . .415IInnddiiccaattiinngg GGaass PPuurriiffiieerrss

Hydrocarbon Trap . . . . . . . . . . . . . . . . . . . . . . .298Moisture Trap . . . . . . . . . . . . . . . . . . . . . . . . . .297Oxygen Trap . . . . . . . . . . . . . . . . . . . . . . . . . . .297

IInnjjeeccttiioonn PPoorrtt RReeppaaiirr TTooooll .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..222200IInnjjeeccttiioonn PPoorrttss,, AAggiilleenntt GGCC .. .. .. .. .. .. .. .. ..222200,, 222244 -- 222266IInnjjeeccttiioonn TTeeee,, DDuuaall--CCoolluummnn .. .. .. .. .. .. .. .. .. .. .. .. .. ..223333,, 226699IInnlleett AAddaappttoorr KKiittss

Capillary GC . . . . . . . . . . . . . . . . . . .228, 233, 269Micropacked Inlet Conversion Kits . . . . .133, 232Packed Column . . . . . . . . . . . . . . . . . . . . . . . . .133

IInnlleett CCoonnvveerrssiioonnInlet Adaptor Kits . . . . . . . . . . . . . . . . . . . . . . .133Packed Column to Capillary Column . . . .265 - 267

IInnlleett LLiinneerrPacking Tool . . . . . . . . . . . . . . . . . . . . . . .215, 279Removal Tool . . . . . . . . . . . . . .215, 231, 244, 279Seals

For Agilent (Gerstel/CIS) . . . . . . . . . . . .219, 223, 227For Thermo Scientific . . . . . . . . . . . . . . . . . . . . . . .255For Varian . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .262

IInnlleett LLiinneerrssOverview . . . . . . . . . . . . . . . . . . . . . . . . .206 - 213APEX Liners . . . . . . . . . . . . . . . . . . . . . . . . . . .244ATAS Liners . . . . . . . . . . . . . . . . . . . . . . . . . . . .244


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INDEX

AlphabeticalFor Agilent GCs

Base-Deactivated . . . . . . . . . . . . . . . . . . . . . . . . . .213CIS4 and PTV . . . . . . . . . . . . . . . . . . . . . . . . . . . . .217Direct Injection . . . . . . . . . . . . . . . . . . . . . . . .210, 218Siltek Metal . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .218Sky . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .210Split . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .210, 217Split/Splitless . . . . . . . . . . . . . . . . . . . . . . . . .210, 217Splitless . . . . . . . . . . . . . . . . . . . . . . . . . . . . .210, 216SPME . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .217Uniliner . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .210, 218

For PerkinElmer GCsDirect Injection . . . . . . . . . . . . . . . . . . . . . . . . . . . .246PSS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .210, 245PTV . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .246Sky . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .210Split . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .245Splitless . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .245Uniliner . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .246Zero Dilution . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .246

For Shimadzu GCsDirect Injection . . . . . . . . . . . . . . . . . . . . . . . .249, 250PTV . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .250Siltek Metal . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .250Sky . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .211Split . . . . . . . . . . . . . . . . . . . . . . . . . . . . .211, 249, 250Splitless . . . . . . . . . . . . . . . . . . . . . . . . .211, 249, 250SPME . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .250Uniliner . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .249, 250

For Thermo Scientific GCsDirect Injection (4000-5000-6000 Series GCs) . . .253Direct Injection (TRACE & Focus SSL) . . . . . . . . . .254Siltek Metal . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .254Sky . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .211Split (4000-5000-6000 Series GCs) . . . . . . . . . . . .253Split (TRACE & Focus SSL) . . . . . . . . . . . . . . .211, 253Splitless (4000-5000-6000 Series GCs) . . . . . . . . .253Splitless (TRACE & Focus SSL) . . . . . . . . . . . .211, 253Uniliner (4000-5000-6000 Series GCs) . . . . . . . . .253Uniliner (TRACE & Focus SSL) . . . . . . . . . . . . . . . .254

For Varian GCsDirect Injection . . . . . . . . . . . . . . . . . . . . . . .259 - 261For 1075/1077 GCs . . . . . . . . . . . . . . . . . . . . . . . .259For 1078/1079 GCs . . . . . . . . . . . . . . . . . . . .211, 261For 1177 GCs . . . . . . . . . . . . . . . . . . . . . . . . .211, 260Siltek Metal . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .261Sky . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .211SPI . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .260Split . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .259Splitless . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .259SPME . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .259Uniliner . . . . . . . . . . . . . . . . . . . . . . . . . . . . .259 - 261

Deactivations . . . . . . . . . . . . . . . . . . . . . . . . . .213Packing Materials & Tools . . . . . . . . . . . .214, 215Prepacked . . . . . . . . . . . . . . . . . . . . . . . . . . . . .214Siltek . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .213Uniliner Liners for Packed Injection

Port Conversion . . . . . . . . . . . . . . . . . . . . . . .266Vu-Tight . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .265

IInnlleett MMaaiinntteennaannccee KKiittss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..222211,, 227755IInnlleett SSeeaall WWaasshheerrss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..222233IInnlleett SSeeaallss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..225555IInnlleett SSuupppplliieess.. SSeeee IInnssttrruummeenntt SSuupppplliieess,, GGCC..IInnssttaallllaattiioonn KKiittss

Chromatograph . . . . . . . . . . . . . . . . . . . . . . . . .323Packed and Micropacked Columns . . . . .133, 232

IInnssttrruummeenntt SSuupppplliieess,, GGCCSection Table of Contents . . . . . . . . . . . . . . . . .201Air Diverter . . . . . . . . . . . . . . . . . . . . . . . . . . . .230Backpressure Regulator Kit . . . . . . . . . . . . . . .229Capillary Column Caps . . . . . . . . . . . . . . . . . . .278Capillary Installation

Gauges . . . . . . . . .221, 235, 252, 257, 263, 278Capillary Nuts . . . . . . . . . . . . . . . . . . . . . .221, 263Chemical Traps for Agilent GCs . . . . . . . .229, 303

Claw and Holder Tool . . . .215, 231, 248, 279, 367Cold Sensor for Agilent MS . . . . . . . . . . . . . . .236Detector Supplies. See Detector Supplies.Diffusion Pump Assemblies for Agilent MS . . .237Direct Injection Inserts . . . . . . . . . . . . . . . . . .232Direct Injection Liner Adaptor . . . . . . . . . . . . .232Dual-Column Analysis. See Dual-Column Analysis.ELCD Supplies . . . . . . . . . . . . . . . . . . . . . . . . . .271Electron Multipliers . . . . . . . . . . . . . . . . .236, 258Finger-Tight Column Nuts . . . . . . . . . . . . . . . .221Flowmeters . . . . . . . . . . . . . . . . . . . . . . . .203, 274For Agilent GCs . . . . . . . . . . . . . . . . . . . .216 - 243For APEX Injectors . . . . . . . . . . . . . . . . . . . . . .244For ATAS Injectors . . . . . . . . . . . . . . . . . . . . . .244For PerkinElmer GCs . . . . . . . . . . . . . . . .245 - 248For Shimadzu GCs . . . . . . . . . . . . . . . . . .249 - 252For Thermo Scientific GCs . . . . . . . . . . . .253 - 258For Varian GCs . . . . . . . . . . . . . . . . . . . .259 - 264GC/MS Cleaning Kit . . . . . . . . . . . . . . . . . . . . .237Injection Port Repair Tool . . . . . . . . . . . . . . . . .220Injection Ports . . . . . . . . . . . . . . . . . . . .224 - 226Inlet Adaptor Fitting Kits . . . . . . . . .228, 233, 269Inlet Liner Packing Tool . . . . . . . . . . . . . .215, 279Inlet Liner Removal Tool . . . . .215, 231, 244, 279Inlet Liners. See Inlet Liners.Inlet Maintenance Kits . . . . . . . . . . .221, 239, 275Inlet Seals . . . . . . . .219, 222, 223, 227, 255, 262Installation Gauges, Capillary . . . . . . . . . . . . .278Interface Guide Tube for Agilent MS . . . . . . . .236Interface with Bellows for Agilent MS . . . . . .235Leak Detectors . . . . . . . . . . . . . . . . .204, 273, 296Liner Packing Materials

Base-Deactivated Wool . . . . . . . . . . . . . . . . . . . . .214CarboFrit Inlet Liner Packing . . . . . . . . . . . . . . . . .214CarboFrit Puller/Inserter Tool . . . . . . . . . . . . . . .214Deactivated Wool . . . . . . . . . . . . . . . . . . . . . .214, 244Inlet Liner Packing Tool . . . . . . . . . . . . . . . . .215, 279Inlet Liner Removal Tool . . . . . . . .215, 231, 244, 279Wool Puller/Inserter Tool, Mini . . . . . . . . . .215, 279

Maintenance Kits . . . . . . . . . . . . . . .221, 239, 275Microseal Septa . . . . . . . . . . . . . . . .219, 247, 262Moisture Control By-Pass Line

for Tekmar Instruments . . . . . . . . . . . . . . . .271O-Rings, Inlet Liner . . . . . . . . . . . . . . . . . . . . .219PID Lamps . . . . . . . . . . . . . . . . . . . . . . . . . . . .271Pump Oil . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .237Purge & Trap Spargers . . . . . . . . . . . . . . . . . . .271Reducing Nut . . . . . . . . . . . . . . . . . . . . . . . . . .228Septa

BTO Septa . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .205IceBlue Septa . . . . . . . . . . . . . . . . . . . . . . . . . . . . .205Microseal Septa . . . . . . . . . . . . . . . . . . .219, 247, 262Thermolite Septa . . . . . . . . . . . . . . . . . . . . . . . . . .205

Septum Nut Removal Tool for Agilent GCs . . . . . . . . . . . . . . . . . . .220, 283

Septum Nuts . . . . . . . . . . . . . . . . . . . . . . . . . . .220Septum-Purged Packed Column

Port Weldment . . . . . . . . . . . . . . . . . . . . . . . .232Split Vent Line for Agilent GCs . . . . . . . . .229, 303Tees, Direct Injection . . . . . . . . . . . . . . . .233, 269Wool, Deactivated . . . . . . . . . . . . . . . . . .214, 244

IInnssttrruummeenntt--GGrraaddee TTuubbiinngg .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..331199IInntteeggrraa--GGuuaarrdd CCoolluummnnss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..3355IInntteerrmmeeddiiaattee--PPoollaarriittyy DDeeaaccttiivvaatteedd

GGuuaarrdd CCoolluummnnss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..3333IInntteerrnnaall SSttaannddaarrddss.. SSeeee RReeffeerreennccee SSttaannddaarrddss..IInntteerrnnaattiioonnaall RReeffeerreennccee MMaatteerriiaallss .. .. .. .. .. .. ..449988 -- 550000IIoonn EExxcchhaannggee PPhhaasseess,, SSPPEE .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..339922IIssootthheerrmmaall CCoolluummnn TTeesstt MMiixx .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..553388

JJJaappaann CCaalliibbrraattiioonn MMiixx .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..442299,, 449999JJeett FFuueell RReeffeerreennccee SSttaannddaarrddss .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..550022JJeett RReeaammeerrss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..228822JJeettss,, FFIIDD.. SSeeee DDeetteeccttoorr SSuupppplliieess..

KKKeerroosseennee RReeffeerreennccee SSttaannddaarrddss .. ..550011,, 550022,, 550066,, 552233KKuuddeerrnnaa--DDaanniisshh EEvvaappoorraattoorr CCoonncceennttrraattoorr .. .. .. .. .. ..440044

LLLaabb OOrrggaanniizzeerrss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..335500LLaammpp,, PPIIDD .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..227711LLaammppss,, HHPPLLCC DDeetteeccttoorr .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..332277 -- 333300LLaasstt DDrroopp FFiilltteerr,, HHPPLLCC .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..334422LLCCLLoocckkeerr HHPPLLCC OOrrggaanniizzeerr .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..335500LLeeaakk DDeetteeccttoorrss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..220044,, 227733,, 229966LLiimmiitteedd VVoolluummee IInnsseerrttss ffoorr VViiaallss .. .. .. .. ..335566,, 336600 -- 336622LLiimmiitteedd VVoolluummee VViiaallss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..335566,, 336600LLiinneerr DDeeaaccttiivvaattiioonnss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..221133LLiinneerr PPaacckkiinngg MMaatteerriiaallss aanndd TToooollss .. .. .. .. .. .. .. ..221144,, 221155LLiinneerrss.. SSeeee IInnlleett LLiinneerrss..LLiiqquuiidd PPhhaassee CCrroossss--RReeffeerreennccee ((UUSSPP--GGCC)) .. .. .. .. .. .. ..113399LLiiqquuiidd PPhhaasseess,, GGCC .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..113388LLOO--PPuullssee PPuullssee DDaammppeerr .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..334400LLooss AAnnggeelleess CCoouunnttyy WWIIPP RReeffeerreennccee SSttaannddaarrddss .. ..550077LLooww--PPrreessssuurree IInnlleett FFiilltteerr,, HHPPLLCC

CPI . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .342Slip-on . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .342

MMM44 FFiittttiinngg FFeerrrruulleess .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..225566,, 228866MMaakkee--UUpp GGaass KKiittss ffoorr AAggiilleenntt GGCCss .. .. .. .. .. .. .. .. .. .. .. ..224411MMaanniiffoolldd,, SSPPEE .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..339955,, 339966MMaassss SSppeeccttrroommeettrryy EElleeccttrroonn MMuullttiipplliieerrss .. .. ..223366,, 225588MMaassssaacchhuusseettttss UUSSTT RReeffeerreennccee SSttaannddaarrddss .. ..550088,, 550099MMeerrlliinn MMiiccrroosseeaall SSeeppttaa .. .. .. .. .. .. .. .. .. .. .. .. ..221199,, 224477,, 226622MMeesshh SSiizzeess,, GGCC CCoolluummnn PPaacckkiinnggss .. .. .. .. .. .. .. .. .. .. .. .. ..114400MMeetteerriinngg VVaallvveess .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..332222MMeetthhaannee CCyylliinnddeerr .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..227755MMeetthhooddss DDeevveellooppmmeenntt SSooffttwwaarree .. .. .. .. .. .. .. .. .. ..2244,, 558800MMiicchhiiggaann UUSSTT RReeffeerreennccee SSttaannddaarrddss .. .. .. .. .. .. .. .. .. .. ..550099MMiiccrroo--VViiaallss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..336655MMiiccrrooppaacckkeedd CCoolluummnnss

Custom Columns . . . . . . . . . . . . . . . . . . . . . . . .141Installation Kits . . . . . . . . . . . . . . . . . . . .133, 232Rt-XLSulfur . . . . . . . . . . . . . . . . . . . . . . . . . . . .131ShinCarbon . . . . . . . . . . . . . . . . . . . . . . . . . . . .130

MMiiccrroosseeaall SSeeppttaa .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..221199,, 224477,, 226622MMiilliittaarryy FFuueell RReeffeerreennccee SSttaannddaarrddss .. .. .. .. .. .. .. .. .. .. .. ..550022MMiinneerraall SSppiirriittss RReeffeerreennccee SSttaannddaarrddss .. .. .. .. .. ..550033,, 552233MMiinnii ppHHPPeerrcchh SSttoorraaggee UUnniitt .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..335500mmiinnii--LLaamm DDiirreecctt IInnjjeeccttiioonn TTeeee .. .. .. .. .. .. .. .. .. .. ..223333,, 226699MMiinnii--RReegguullaattoorr,, GGaass CCyylliinnddeerr .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..443333MMiinniiaattuurree CCaanniisstteerrss && AAcccceessssoorriieess .. .. .. .. .. .. ..442200,, 442211MMIINNIICCYYLL RReegguullaattoorr,, GGaass CCyylliinnddeerr .. .. .. .. .. .. .. .. .. .. .. .. ..331122MMiissssiissssiippppii UUSSTT RReeffeerreennccee SSttaannddaarrddss .. .. .. .. .. .. .. .. ..550099MMLLEE TTooooll KKiitt .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..227766MMoobbiillee PPhhaassee AAcccceessssoorriieess,,

HHPPLLCC .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..333366,, 333388,, 334400 -- 334444


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INDEX

AlphabeticalMMooiissttuurree CCoonnttrrooll BByy--PPaassss LLiinnee ffoorr

TTeekkmmaarr IInnssttrruummeennttss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..227711MMooiissttuurree TTrraappss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..229977MMoolleeccuullaarr SSiieevvee

Packed Columns . . . . . . . . . . . . . . . . . . . . . . . .127PLOT Columns . . . . . . . . . . . . . . . . . . . . . . . . . .109

MMoottoorr OOiill RReeffeerreennccee SSttaannddaarrddss .. .. .. .. .. .. .. .. .. ..550011,, 550066MMSS CCoolluummnnss,, GGCC .. .. .. .. .. .. .. ..4411,, 4422,, 4444,, 5500,, 5544,, 8877 -- 9977MMSS//GGCC CClleeaanniinngg KKiitt .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..223377MMSSDD AAcccceessssoorriieess .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..223355

Capillary Installation Tool . . . . . . . . . . . . .235, 278Conversion Fitting . . . . . . . . . . . . . . . . . . . . . .235Ion Source Cleaning Materials . . . . . . . . . . . .237Rough Pump Oil . . . . . . . . . . . . . . . . . . . . . . . .237Source Nut . . . . . . . . . . . . . . . . . . . . . . . . . . . .235

MMXXTTCapillary GC Columns

MXT-1 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .115MXT-1 Sim Dist . . . . . . . . . . . . . . . . . . . . . . . . .79, 120MXT-1HT Sim Dist . . . . . . . . . . . . . . . . . . .77, 78, 120MXT-1301 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .117MXT-1701 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .118MXT-20 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .116MXT-200 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .118MXT-2887 . . . . . . . . . . . . . . . . . . . . . . . . . . . . .77, 119MXT-35 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .117MXT-5 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .116MXT-50 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .117MXT-500 Sim Dist . . . . . . . . . . . . . . . . . . . . . . .79, 120MXT-502.2 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .121MXT-624 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .121MXT-65 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .117MXT-65TG . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .119MXT-Alumina BOND . . . . . . . . . . . . . . . . . . . . . . . .108MXT-Biodiesel TG . . . . . . . . . . . . . . . . . . . . . . .81, 119MXT-Msieve 5A PLOT . . . . . . . . . . . . . . . . . . . . . . .109MXT-Q-BOND . . . . . . . . . . . . . . . . . . . . . . . . . . . . .110MXT-S-BOND . . . . . . . . . . . . . . . . . . . . . . . . . . . . .110MXT-Volatiles . . . . . . . . . . . . . . . . . . . . . . . . . . . . .121MXT-WAX . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .118

ConnectorsConnector Kits . . . . . . . . . . . . . . . . . . . . . . . .270, 292For Fused Silica . . . . . . . . . . . . . . . . . . . . . . .270, 292For Metal . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .292Low Dead-Volume . . . . . . . . . . . . . . . . . . . . . . . . .292Low Dead-Volume “Y” . . . . . . . . . . . . . . . . . . . . . .292Replacement Ferrules and Nuts . . . . . . . . . . . . . .292

Guard Columns and Transfer Lines . . . . . . . . .114Needle Files . . . . . . . . . . . . . . . . . . . . . . . . . . .282Tubing Scorer . . . . . . . . . . . . . . . . . .114, 277, 324

Nnn--OOccttaannee oonn RReess--SSiill CC PPaacckkeedd CCoolluummnn .. .. .. .. .. .. .. .. ..113355NNeeaatt CCoommppoouunnddss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..444422 -- 444488NNeeeeddllee FFiillee,, MMXXTT .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..228822NNeeeeddlleess.. SSeeee SSyyrriinnggeess -- RReeppllaacceemmeenntt NNeeeeddlleess..NNEEWW PPRROODDUUCCTTSS .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..66--99NNiittrrooaarroommaattiicc RReeffeerreennccee SSttaannddaarrddss .. .. .. .. .. .. ..448844,, 448855NNiittrrooggeenn GGeenneerraattoorrss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..330066,, 330077NNoorrmmaall PPhhaassee SSPPEE CCaarrttrriiddggeess .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..339922NNoorrtthhwweesstt UUSSTT RReeggiioonnaall MMeetthhoodd

RReeffeerreennccee SSttaannddaarrddss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..551100NNuuttss,, GGCC

Capillary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .221Detector Plug . . . . . . . . . . . . . . . . . .219, 241, 278Finger-Tight Capillary . . . . . . . . . . . . . . . . . . . .221MSD Source . . . . . . . . . . . . . . . . . . . . . . . . . . .235Reducing . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .228

Septum . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .220For Agilent . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .220For Shimadzu . . . . . . . . . . . . . . . . . . . . . . . . . . . . .251

Stainless Steel . . . . . . . . . . . . . . . . . . . . .221, 263NNuuttss,, TTuubbee && PPiippee FFiittttiinnggss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..331166

OOO--RRiinnggss,, IInnlleett LLiinneerr .. .. .. .. .. .. .. .. .. .. .. ..221199,, 224444,, 224477,, 225511OO--RRiinnggss,, JJuummbboo SSyyrriinnggee .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..338855,, 443377OOiill && GGrreeaassee

Reference Standards . . . . . . . . . . . . . . . . . . . .470SPE Disk . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .397

OOiill--FFrreeee VVaaccuuuumm//PPrreessssuurree SSttaattiioonn .. .. .. .. .. .. .. .. .. .. ..339955OOppeenn SSuuppppllyy BBiinnss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..335500OOPPNN oonn RReess--SSiill CC PPaacckkeedd CCoolluummnnss .. .. .. .. .. .. .. .. .. .. .. ..113355OOppttii--CCaapp BBoottttllee CCaapp .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..333388OOrreeggoonn UUSSTT RReeffeerreennccee SSttaannddaarrddss .. .. .. .. .. .. .. .. .. .. .. ..551100OOrrggaanniizzeerrss,, LLaabb .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..335500OOrrggaannoocchhlloorriinnee PPeessttiicciiddee RReeffeerreennccee SSttaannddaarrddss..

SSeeee ppaaggeess 444400--444411..OOrrggaannoopphhoosspphhoorruuss PPeessttiicciiddee RReeffeerreennccee SSttaannddaarrddss..

SSeeee ppaaggeess 444400--444411..OOrrggaannoottiinn RReeffeerreennccee SSttaannddaarrddss .. .. .. .. .. .. .. .. .. .. .. .. .. ..449966OOrrggaannoottiinn SSPPEE CCaarrttrriiddggeess .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..339944OOrriiffiicceess,, AAiirr SSaammpplliinngg .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..441155OOvveenn FFllaappppeerr AAsssseemmbblliieess ffoorr AAggiilleenntt GGCCss .. .. .. .. .. ..223300OOxxyyggeenn TTrraappss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..229977OOzzoonnee PPrreeccuurrssoorr MMiixxttuurreess .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..443300

PPPaacckkeedd CCoolluummnn FFIIDD JJeettss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..224400PPaacckkeedd CCoolluummnn IInnlleett CCoonnvveerrssiioonn

Inlet Adaptor Kits . . . . . . . . . . . . . . . . . . . . . . .133Packed Column to Capillary Column . . . .265 - 267

PPaacckkeedd CCoolluummnnssBonded Stationary Phases . . . . . . . .123, 124, 126Bulk Packing Materials . . . . . . . . . . . . . . .134, 137CarboBlack

Packings . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .134Solid Supports . . . . . . . . . . . . . . . . . . . . . . . . . . . .127

ChromosorbPackings . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .136Solid Supports . . . . . . . . . . . . . . . . . . . . . . . . . . . .126

CustomCoated Packing Materials . . . . . . . . . . . . . . . . . . .140Column Configurations . . . . . . . . . . . . . . . . . . . . . .143Columns . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .141Micropacked Columns . . . . . . . . . . . . . . . . . . . . . .141Order Form . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .142

D3606 Application Column Set . . . . . . . . . . . . .128Diatomite Packings . . . . . . . . . . . . . . . . . . . . . .136Fittings . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .142Inlet Adaptor Kits . . . . . . . . . . . . . . . . . . . . . . .133Liquid Phase Cross-Reference . . . . . . . . . . . . .138Liquid Phases . . . . . . . . . . . . . . . . . . . . . . . . . .138Mesh Sizes . . . . . . . . . . . . . . . . . . . . . . . . . . . .140Micropacked Columns . . . . . . . . . . . . . . .130 - 132Molecular Sieves . . . . . . . . . . . . . . . . . . . . . . .127Packing Materials . . . . . . . . . . . . . . . . . .134 - 137Porous Polymer Packings

Chromosorb Century . . . . . . . . . . . . . . . . . . . . . . .137HayeSep Series . . . . . . . . . . . . . . . . . . . . . . . . . . .137Porapak Series . . . . . . . . . . . . . . . . . . . . . . . . . . . .137

Reduction Fittings . . . . . . . . . . . . . . . . . . . . . . .125Request Form, Custom . . . . . . . . . . . . . . . . . . .142Res-Sil Packings . . . . . . . . . . . . . . . . . . . . . . . .135

Rt-XLSulfur . . . . . . . . . . . . . . . . . . . . . . . . . . . .131ShinCarbon . . . . . . . . . . . . . . . . . . . . . . . . . . . .130Silcoport Packings . . . . . . . . . . . . . . . . . . . . . .134Solid Support Cross-Reference . . . . . . . . . . . .139Specialty Columns . . . . . . . . . . . . . . . . . .128 - 131Standard Column Configurations . . . . . . . . . . .143Stock Packed Columns . . . . . . . . . . . . . . .126, 127Tenax Packings . . . . . . . . . . . . . . . . . . . . . . . . .137Tubing . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .125Welded Tubing Reducers . . . . . . . . . . . . . . . . .125Welded VCR Fittings . . . . . . . . . . . . . . . . . . . . .125

PPaacckkiinngg MMaatteerriiaallssGC

CarboBlack . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .134Chromosorb . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .136Custom . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .140Diatomite . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .136Porous Polymer . . . . . . . . . . . . . . . . . . . . . . . . . . .137Res-Sil . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .135Silcoport . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .134Tenax . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .137

HPLC, Bulk . . . . . . . . . . . . . . . . . . . . . . . . . . . .194Inlet Liner . . . . . . . . . . . . . . . . . . . . . . . . .214, 215

PPaarrkkeerr FFiittttiinnggss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..331166,, 331177PPaarrkkeerr VVaallvveess .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..331177,, 332222PPaassssiivvee AAiirr SSaammpplliinngg KKiittss .. .. .. .. .. .. .. .. .. ..441144 -- 441177,, 442200PPCCBB RReeffeerreennccee SSttaannddaarrddss

Aroclor Solutions . . . . . . . . . . . . . . .469, 482, 495PCB Congeners . . . . . . . . . . . . . . . . . . . . . . . . .496PCB Standards in Oil . . . . . . . . . . . . . . . . . . . .516

PPEEEEKKColumn Connector . . . . . . . . . . . . . . . . . . . . . .334Fitting Extractor . . . . . . . . . . . . . . . . . . . . . . . .337Fittings, Secure-Fit . . . . . . . . . . . . . . . . . . . . . .335Tubing . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .332Tubing Cutter . . . . . . . . . . . . . . . . . . . . . . . . . .333Tubing Elbows . . . . . . . . . . . . . . . . . . . . . . . . . .333Union . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .335Washers for ASE Extraction Unit . . . . . . .400, 401

PPeennnnssyyllvvaanniiaa UUSSTT RReeffeerreennccee SSttaannddaarrddss .. .. .. .. .. .. ..551111PPeerrkkiinnEEllmmeerr GGCC SSuupppplliieess

FID Parts, Auto SYS . . . . . . . . . . . . . . . . .247, 248Injector Adapter, Auto SYS . . . . . . . . . . . . . . . .247Inlet Liners

Direct Injection . . . . . . . . . . . . . . . . . . . . . . . . . . . .246PSS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .210, 245PTV . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .246Sky . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .210Split . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .245Splitless . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .245Uniliner . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .246Zero Dilution . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .246

O-Rings, Inlet Liner . . . . . . . . . . . . . . . . . . . . .247Septa . . . . . . . . . . . . . . . . . . . . . . . . . . . . .205, 247Syringes . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .373Tool Kit, MLE . . . . . . . . . . . . . . . . . . . . . . . . . . .248Wrench Set . . . . . . . . . . . . . . . . . . . . . . . .248, 280

PPeerrkkiinnEEllmmeerr HHPPLLCC SSuupppplliieessInstrument Parts . . . . . . . . . . . . . . . . . . . . . . .328Syringes, Autosampler . . . . . . . . . . . . . . . . . . .349

PPeessttiicciiddee RReeffeerreennccee SSttaannddaarrddss.. SSeeee ppaaggeess 444400--444411..PPeettrroolleeuumm RReeffeerreennccee SSttaannddaarrddss

Low Sulfur . . . . . . . . . . . . . . . . . . . . . . . .518 - 521Simulated Distillation . . . . . . . . . . . . . . . . . . . .515UST Monitoring . . . . . . . . . . . . . . . . . . . .501 - 512

PPhhaarrmmaacceeuuttiiccaall RReeffeerreennccee SSttaannddaarrddss,, RReessiidduuaall SSoollvveennttss

European Pharmacopoeia . . . . . . . . . . . . . . . .528USP . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .528


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INDEX

AlphabeticalPPhhaassee CCrroossss RReeffeerreennccee

Capillary GC Columns . . . . . . . . . . . . . . . . . .28, 29HPLC . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .153PLOT Columns . . . . . . . . . . . . . . . . . . . . . . . . . .105

PPhheennooll RReeffeerreennccee SSttaannddaarrddss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..447722PPhhoottooiioonniizzaattiioonn ((PPIIDD)) LLaammppss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..227711PPiinnnnaaccllee DDBB HHPPLLCC CCoolluummnnss .. .. .. .. .. .. .. .. .. .. .. .. ..116666 -- 117722PPiinnnnaaccllee IIII HHPPLLCC CCoolluummnnss .. .. .. .. .. .. .. .. .. .. .. .. .. ..117733 -- 117777PPiippee FFiittttiinnggss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..331133 -- 331177PPiippeettss,, GGllaasssswwaarree .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..440077PPiissttoonn

Seal Insertion Tool . . . . . . . . . . . . . . . . . . . . . .337Seals . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .332

PPllaassttiicc SSyyrriinnggeess .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..336699PPlliieerr SSeett .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..332233PPLLOOTT CCoolluummnnss

MXT ColumnsMXT-Alumina BOND . . . . . . . . . . . . . . . . . . . . . . . .108MXT-Msieve 5A . . . . . . . . . . . . . . . . . . . . . . . . . . . .109MXT-Q-BOND . . . . . . . . . . . . . . . . . . . . . . . . . . . . .110MXT-S-BOND . . . . . . . . . . . . . . . . . . . . . . . . . . . . .110

Particle Trap . . . . . . . . . . . . . . . . . . . . . . . . . . .111Phase Cross-Reference Chart . . . . . . . . . . . . .105Rt- Columns

Rt-Alumina BOND . . . . . . . . . . . . . . . . . . . .74, 76, 108Rt-Msieve 5A . . . . . . . . . . . . . . . . . . . . . . . . . . . . .109Rt-Q-BOND . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .110Rt-QS-BOND . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .110Rt-S-BOND . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .110Rt-U-BOND . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .110

PPlluugg VVaallvveess .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..332222PPlluummbbiinngg CCoonnnneeccttoorrss.. SSeeee CCoonnnneeccttoorrss,, TTuubbiinngg..PPoocckkeett MMaaggnniiffiieerr .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..228822PPoollaarr DDeeaaccttiivvaatteedd FFuusseedd SSiilliiccaa GGuuaarrdd CCoolluummnnss .. .. ..3333PPoollyy CCrriimmpp VViiaallss

Cap with Septum . . . . . . . . . . . . . . . . . . . . . . .357Seals . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .357

PPoollyyccyycclliicc AArroommaattiicc HHyyddrrooccaarrbboonn RReeffeerreenncceeSSttaannddaarrddss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..446655,, 447744

PPoollyyiimmiiddee RReessiinn .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..227700,, 228888PPoollyywwaaxx

Calibration Materials . . . . . . . . . . . . . . . . . . . .516Chromatogram . . . . . . . . . . . . . . . . . . . . . .79, 120

PPoorraappaakk PPaacckkiinnggss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..113377PPoorroouuss PPoollyymmeerr

Packed Columns . . . . . . . . . . . . . . . . . . . . . . . .126Packings . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .137PLOT Columns . . . . . . . . . . . . . . . . . . . . . . . . . .110

PPrreeccoonnnneecctteedd GGuuaarrdd CCoolluummnn//TTrraannssffeerr LLiinnee .. .. .. .. ..228877PPrreepp CCoolluummnnss,, HHPPLLCC .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..115577 -- 119911PPrreessss--TTiigghhtt CCoonnnneeccttoorrss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..228877,, 228888PPrreessssuurree GGaauuggeess .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..330033,, 441122,, 441133PPrroo eezzGGCC SSooffttwwaarree .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..2244,, 558800PPrroottooccooll SSttaattiioonn .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..331122PPTTVV IInnlleett LLiinneerrss

For Agilent GCs . . . . . . . . . . . . . . . . . . . . . . . . .217For PerkinElmer GCs . . . . . . . . . . . . . . . . . . . .246For Shimadzu GCs . . . . . . . . . . . . . . . . . . . . . .250

PPuullssee DDaammppeerrss,, MMoobbiillee PPhhaassee .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..334400PPuummpp OOiill,, GGCC .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..223377PPuummpp PPaarrttss,, HHPPLLCC .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..332277,, 333311PPuurrggee && TTrraapp SSuupppplliieess

Moisture Control By-Pass Line . . . . . . . . . . . . .271Spargers . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .271

PPuurriiffiieerrss.. SSeeee GGaass PPuurriiffiieerrss..

QQQuuEECChhEERRSS PPrroodduuccttss,, QQ--sseepp

Centrifuge . . . . . . . . . . . . . . . . . . . . . . . . . . . . .390Packets . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .389Reference Standards . . . . . . . . . . . . . . . . . . . .534Tubes . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .389

RRReeaammeerrss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..228822RReecchhaarrggeeaabbllee SS--TTrraappss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..229977RReeccoonnddiittiioonniinngg SSeerrvviiccee:: AAiirr CCaanniisstteerrss .. .. .. .. .. .. .. .. ..442222RReedduucciinngg FFeerrrruulleess .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..228855RReedduucciinngg NNuutt .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..222288RReeffeerreennccee IInnffoorrmmaattiioonn

Pro ezGC Methods Development Software . . . . . . . . . . . . . .24, 580

Seminars . . . . . . . . . . . . . . . . . . . . . . . . . . . .12, 13RReeffeerreennccee SSttaannddaarrddss

Detailed Table of Contents . . . . . . . . . . . .440, 441500 Series Methods . . . . . . . . . . . . . . . .451 - 463600 Series Methods . . . . . . . . . . . . . . . .464 - 4698000 Series Methods . . . . . . . . . . . . . . .470 - 485Acrolein . . . . . . . . . . . . . . . . . . . . . . . . . . .464, 478Alaska UST . . . . . . . . . . . . . . . . . . . . . . . .505, 506Aldehydes/Ketones . . . . . . . . . . . . . . . . . . . . .483Amine Column Test Mix . . . . . . . . . . . . . . . . . .538Aroclor Solutions . . . . . . . . . . . . . . .469, 482, 495ASTM

D2887 Simulated Distillation Petrochemical . . . . .515D3710 Simulated Distillation Petrochemical . . . . .515D4059 PCB Standards in Oil . . . . . . . . . . . . . . . . . .516D6042 Plastic Container Testing . . . . . . . . . .529, 536D6352 Polywax . . . . . . . . . . . . . . . . . . . . . . . . . . . .516E1387 Fire Debris Analysis . . . . . . . . . . . . . .513, 523E1618 Fire Debris Analysis . . . . . . . . . . . . . .513, 523Fire Debris Mixtures . . . . . . . . . . . . . . . . . . .513, 523PCBs in Oil . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .516Petroleum & Petrochemical Mixtures . . . . .515 - 517Simulated Distillation . . . . . . . . . . . . . . . . . . .515, 516

Aviation Gas . . . . . . . . . . . . . . . . . . . . . . . . . . .502Bank Dye (MAAQ) . . . . . . . . . . . . . . . . . . . . . . .524Benzidine Mix . . . . . . . . . . . . . . . . . . . . . . . . . .490Biodiesel . . . . . . . . . . . . . . . . . . . . . .502, 504, 516Blood Alcohol . . . . . . . . . . . . . . . . . . . . . . . . . .524BTEX Gas Mixtures . . . . .429, 471, 476, 503, 504Canadian Environmental Methods . .488, 498, 499Carbamates . . . . . . . . . . . . . . . . . . . . . . . . . . .461Chlordane . . . . . . . . . . . . . . . . . . . . . . . . .469, 495Chlorinated Acid Herbicides . . . . . . . . . . .463, 484Chloroprene . . . . . . . . . . . . . . . . . . . . . . . . . . .478CLP

GPC Calibration Mix . . . . . . . . . . . . . . . . . . . . . . . .492Pesticides . . . . . . . . . . . . . . . . . . . . . . . . . . .493 - 495Semivolatiles . . . . . . . . . . . . . . . . . . . . . . . . .488 - 492Volatiles . . . . . . . . . . . . . . . . . . . . . . . . . . . .486 - 488

CLP Low ConcentrationPesticides . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .494Semivolatiles . . . . . . . . . . . . . . . . . . . . . . . . .489 - 492Volatiles . . . . . . . . . . . . . . . . . . . . . . . . . . . .486 - 488

CLP Methods . . . . . . . . . . . . . . . . . . . . . .486 - 495Column Evaluation Mixtures

GC Column Test Mixes . . . . . . . . . . . . . . . . . . . . . .538HPLC Column Test Mixes . . . . . . . . . . . . . . . .199, 539

Composite FuelsDiesel Fuel #2 Composite . . . . . . . . . . . . . . .501, 506Kerosene Composite . . . . . . . . . . . . . . . . . . .501, 506Unleaded Gasoline Composite . . . . . . . . . . . .501, 505

Connecticut UST . . . . . . . . . . . . . . . . . . . . . . . .507Creosote Oil . . . . . . . . . . . . . . . . . . . . . . . . . . .502Custom Request

Form . . . . . . . . . . . . .www.restek.com/solutionsDerivatization Reagents . . . . . . . . . . . . . . . . . .537Diesel

Diesel Fuel #2 . . . . . . . . . . . . . . . .501, 502, 506, 523Diesel Internal Standards . . . . . . . . . . . . . . . . . . .504Diesel Range Organics (DRO) . . . . . . . . . . . . . . . .512Diesel Surrogate Standards . . . . . . . . . . . . . . . . . .504

Diesel/Biodiesel Blend . . . . . . . . . . .502, 504, 516Disinfection Byproducts . . . . . . . . . . . . . . . . . .462DNPH Reference Standards . . . . . . . . . . .483, 513Drinking Water (500 Series) . . . . . . . . . .451 - 463Drinking Water Odor Standard . . . . . . . .463, 499Drugs (Exempt) . . . . . . . . . . . . . . . . . . . . . . . . .525EPA Methods

1311 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4701664 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .470418.1 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .470500 Series (Drinking Water) . . . . . . . . . . . . .451 - 463600 Series (Wastewater) . . . . . . . . . . . . . . .464 - 4698000 Series (Solid Waste) . . . . . . . . . . . . . .470 - 485CLP . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .486 - 495

Ethanol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .507Ethylene Oxide . . . . . . . . . . . . . . . . . . . . . . . . .528European Pharmacopoeia Method . . . . . .528, 529Evaluation Mixtures, Column . .199, 531, 538, 539Explosives by GC . . . . . . . . . . . . . . . . . . . . . . . .473Explosives by HPLC . . . . . . . . .473, 474, 485, 524Fatty Acid Methyl Esters . . . . . . . . . . . . .532, 533Fire Debris . . . . . . . . . . . . . . . . . . . .502, 513, 523Florida UST . . . . . . . . . . . . . . . . . . . . . . . . . . . .507Food Testing . . . . . . . . . . . . . . . . . . . . . . . . . . .536Forensic . . . . . . . . . . . . . . . . . . . . . . . . . .524, 525Formaldehyde-DNPH Mix . . . . . . . . . . . . . . . . .483Fragrance Materials Test Mix . . . . . . . . . . . . .531Fruit Juice Organic Acid . . . . . . . . . . . . . . . . . .531Fuel Oil Degradation Mix . . . . . . . . . . . . . . . . .503Gas Standards, Air Monitoring

BTEX Gas . . . . . . . . . . . . . . . .429, 471, 476, 503, 504Japan Calibration . . . . . . . . . . . . . . . . . .428, 429, 499Natural Gas . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .431Ozone Precursor . . . . . . . . . . . . . . . . . . . . . . . . . . .430Refinery Gas . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .431Scott Transportable Gases . . . . . . . . . . . . . . . . . .432TO-14A . . . . . . . . . . . . . . . . . . . . . . . . . . . . .427 - 429TO-15 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .428, 429

GasolineGasoline Internal Standards . . . . . . . . . . . . . . . . .504Gasoline Range Organics (GRO) . . . . . . . . . . . . . .503Gasoline Surrogate Standards . . . . . . . . . . . . . . . .504Gasoline, Unleaded . . . . . . . . . . . .501, 502, 505, 523

GC Column Test Mixtures . . . . . . . . . . . . . . . . .538GC/MS Tuning Mixture . . . . . . . . . . . . . . .469, 479Glycols . . . . . . . . . . . . . . . . . . . . . . .476, 507, 510Grob Test Mix . . . . . . . . . . . . . . . . . . . . . . . . . .538Haloacetic Acids . . . . . . . . . . . . . . . . . . . . . . . .462Herbicides . . . .455, 458, 462, 466, 470, 475, 484HPLC Column Test Mixtures . . . . . . . . . . .199, 539Hydraulic Oil . . . . . . . . . . . . . . . . . . . . . . . . . . .502International Reference Standards . . . .498 - 500Isothermal Column Test Mixture . . . . . . . . . . .538Japan Calibration Mixture . . . . . . . . . . . .429, 499Jet Fuel . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .502Kerosene . . . . . . . . . . . . . . . . .501, 502, 506, 523Los Angeles County WIP . . . . . . . . . . . . . . . . .507Massachusetts UST . . . . . . . . . . . . . . . . .508, 509Michigan UST . . . . . . . . . . . . . . . . . . . . . . . . . .509Military Fuels . . . . . . . . . . . . . . . . . . . . . . . . . .502Mineral Spirits . . . . . . . . . . . . . . . . . . . . .503, 523Mississippi UST . . . . . . . . . . . . . . . . . . . . . . . .509


788 www.restek.com

INDEX

AlphabeticalMotor Oil

Motor Oil Composite . . . . . . . . . . . . . . . . . . .501, 506Used Motor Oil Composite . . . . . . . . . . . . . . . . . . .501

Neat Compounds . . . . . . . . . . . . . . . . . . .442 - 448Nitroaromatics . . . . . . . . . . . . . . . . . . . . .484, 485Nitrogen/Phosphorus

Pesticides . . . . . . . . . . . . . . .454, 458, 481, 499Northwest UST Regional Method . . . . . . . . . . .510Oil & Grease . . . . . . . . . . . . . . . . . . . . . . . . . . .470Oregon UST . . . . . . . . . . . . . . . . . . . . . . . . . . .510Organic Acids . . . . . . . . . . . . . . . . . . . . . . . . . .531Organochlorine (OC) Pesticides.

See pages 440-441.Organometallics . . . . . . . . . . . . . . . . . . . . . . . .496Organophosphorus (OP) Pesticides.

See pages 440-441.Organotins . . . . . . . . . . . . . . . . . . . . . . . . . . . .496Oxygenates . . . . . . . . . . . . . . . . . . . . . . . . . . . .478Ozone Precursors . . . . . . . . . . . . . . . . . . . . . . .430Paraquat & Diquat . . . . . . . . . . . . . . . . . .189, 461PCB

Aroclor Solutions . . . . . . . . . . . . . .469, 482, 495, 496PCB Congeners . . . . . . . . . . . . . . . . . . . . . . . .496, 499PCB Standards in Oil . . . . . . . . . . . . . . . . . . . . . . .516

Pennsylvania UST . . . . . . . . . . . . . . . . . . . . . . .511Pesticides. See pages 440-441.Petroleums

Low Sulfur . . . . . . . . . . . . . . . . . . . . . . . . . . .518 - 521Simulated Distillation . . . . . . . . . . . . . . . . . . . . . . .515UST Monitoring . . . . . . . . . . . . . . . . . . . . . . .501 - 512

Pharmaceuticals, Residual SolventsEuropean Pharmacopoeia . . . . . . . . . . . . . . . . . . .528USP . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .528

Phenols . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .472Phenylurea Pesticide Mixes . . . . . . . . . . . . . . .461Plastic Container Testing . . . . . . . . . . . . .529, 536Polybrominated Diphenylethers (PBDEs) . . . . .459Polywax . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .516QuEChERS Standards . . . . . . . . . . . . . . . . . . . .534Residual Solvents . . . . . . . . . . . . . . . . . . .528, 529Retention Time Reference Standards . . . . . . .501Semivolatiles Mixtures. See pages 440-441.Single Component Solutions . . . . . . . . . .442 - 448Single Source Fuels

Aviation Gas . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .502Fuel Oils . . . . . . . . . . . . . . . . . . . . . . . . . . . . .502, 506Jet Fuel A . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .502

Solid Waste Methods (8000 Series) . . . .470 - 485State-Specific Environmental Methods . . . . . .497Stoddard Solvent . . . . . . . . . . . . . . . . . . .503, 523TCLP Solid Waste . . . . . . . . . . . . . . . . . . . . . . .470Tennessee UST . . . . . . . . . . . . . . . . . . . . . . . . .511Test Mixes . . . . . . . . . . . . . . . . . . . . . . . . .538, 539Texas TNRCC UST . . . . . . . . . . . . . . . . . . . . . . .511

Method 1005 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .511Method 1006 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .511

TO-14A . . . . . . . . . . . . . . . . . . . . . . . . . . .427, 428TO-15 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .428Toxaphene . . . . . . . . . . . . . . . .453, 454, 469, 495Toxicity Characteristic Leaching Procedure . .470Transformer Oil, PCB-Free . . . . . . . . . . . . . . . .516TRPH . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .470Tuning Mixture . . . . . . . . . . . . . . . . .469, 479, 489Unleaded Gasoline . . . . . . . . . .501, 502, 505, 523USP <467>Method . . . . . . . . . . . . . . . . . . . .528UST Monitoring . . . . . . . . . . . . . . . . . . . .501 - 512

Fuels . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .501, 502Military Fuels . . . . . . . . . . . . . . . . . . . . . . . . . . . . .502Mineral Spirits . . . . . . . . . . . . . . . . . . . . . . . .503, 523Motor Oil . . . . . . . . . . . . . . . . . . . . . . . . . . . . .501, 506Petroleum Hydrocarbons . . . . . . . . . . . . . . .504 - 512

Petroleum Volatiles . . . . . . . . . . . . . . . . . . . .503, 504Retention Time Reference Standard . . . . . . . . . . .501State-Specific Methods . . . . . . . . . . . . . . . . .505 - 512

Volatiles (VOA) Mixtures. See pages 440-441.Washington UST . . . . . . . . . . . . . . . . . . . . . . . .512Wastewater Methods (600 Series) . . . .464 - 469Weathered Petrochemical . . . . . . . . . . . .513, 523Well Investigation Program (WIP) . . . . . . . . .507Wisconsin UST . . . . . . . . . . . . . . . . . . . . .503, 512

RReeffiillllaabbllee HHyyddrrooccaarrbboonn TTrraapp .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..229988RReegguullaattoorrss

Backpressure Regulator, Gas . . . . . . . . . .229, 312Backpressure Regulator, HPLC . . . . . . . . . . . .345Dual-Stage Regulators . . . . . . . . . . . . . .309 - 311Flash Arrestor, Hydrogen . . . . . . . . . . . . . . . . .311Flexible Stainless Steel Hose . . . . . . . . . . . . . .311High-Purity V.O.C. . . . . . . . . . . . . . . . . . . . . . . .433Mini-Regulator . . . . . . . . . . . . . . . . . . . . . . . . .433MINICYL Regulator . . . . . . . . . . . . . . . . . . . . .312Protocol Station . . . . . . . . . . . . . . . . . . . . . . . .312Scott Transportable Gases . . . . . . . . . . . . . . . .434Silcosteel Regulators . . . . . . . . . . . . . . . . . . . .309Single-Stage Regulators . . . . . . . . . . . . .309 - 311Single-Stage V.O.C. Regulator

Syringe Adaptor Kit . . . . . . . . . . . . . . . . . . . .434Switchover Systems . . . . . . . . . . . . . . . . . . . . .312Tools

CGA Fittings . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .311Cylinder Valve Wrench . . . . . . . . . . . . . . . . . . . . . .312Universal Cylinder Wrench . . . . . . . . . . . . . . . . . .312Wall-Mount Cylinder Holder . . . . . . . . . . . . . . . . . .312

Ultra-High-PurityBrass Regulators . . . . . . . . . . . . . . . . . . . . . . . . . .310Stainless Steel Regulators . . . . . . . . . . . . . . . . . . .311

RReeppllaacceemmeenntt PPaarrttss,, GGCC IInnssttrruummeennttss.. SSeeee lliissttiinnggss ffoorriinnssttrruummeenntt mmaannuuffaaccttuurreerr..

RReeppllaacceemmeenntt PPaarrttss,, HHPPLLCC IInnssttrruummeennttss .. .. ..332277 -- 333311RReeqquueesstt FFoorrmmss

Reference Standards . . . . . . . .www.restek.com/solutions

Packed GC Columns . . . . . . . . . . . . . . . . . . . . .142RReess--SSiill PPaacckkiinnggss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..113355RReesseerrvvooiirr,, CCaappiillllaarryy GGCC .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..227755RReesseerrvvooiirrss,, SSPPEE .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..339944,, 339977RReessiidduuaall SSoollvveenntt RReeffeerreennccee SSttaannddaarrddss .. .. .. ..552288,, 552299RReessiinn

Polyimide . . . . . . . . . . . . . . . . . . . . . . . . .270, 288SDVB . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .426SPE Disk . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .397Ultra-Clean Adsorbent . . . . . . . . . . . . . . . . . . .426

RReesspprreepp SSPPEE12- & 24-Port Tube Manifold . . . . . . . . . . . . . .395Diskcover-47 Extraction Disk Holder . . . . . . . .397Diskcover-47 Reservoir . . . . . . . . . . . . . . . . . .397Disks . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .397Manifolds . . . . . . . . . . . . . . . . . . . . . . . . .395, 396Replacement Accessories . . . . . . . . . . . . . . . .394Sample Delivery System . . . . . . . . . . . . . . . . . .396SPE Flow Filter . . . . . . . . . . . . . . . . . . . . . . . . .397

RReetteennttiioonn GGaappss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..111144RReetthhrreeaaddiinngg TToooollss .. .. .. .. .. .. .. .. .. .. .. ..222200 ,, 223300,, 226633,, 228800RReevveerrsseedd PPhhaassee SSPPEE CCaarrttrriiddggee .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..339922RRiinnssiinngg RReesseerrvvooiirr,, CCaappiillllaarryy GGCC .. .. .. .. .. .. .. .. .. .. .. .. .. ..227755RRtt GGCC CCoolluummnnss

Rt-2330 Capillary . . . . . . . . . . . . . . . . . . . . . . . .57Rt-2560 Capillary . . . . . . . . . . . . . . . . . . . . .57, 69Rt-Alumina BOND PLOT . . . . . . . . . . . .74, 76, 108Rt-βDEXcst Chiral . . . . . . . . . . . . . . . . . . . . . . . .68Rt-βDEXm Chiral . . . . . . . . . . . . . . . . . . . . . . . . .68Rt-βDEXsa Chiral . . . . . . . . . . . . . . . . . . . . . . . .68

Rt-βDEXse Chiral . . . . . . . . . . . . . . . . . . . . . . . .68Rt-βDEXsm Chiral . . . . . . . . . . . . . . . . . . . . . . . .68Rt-βDEXsp Chiral . . . . . . . . . . . . . . . . . . . . . . . .68Rt-CW20M F&F Capillary . . . . . . . . . . . . . . . . . .71Rt-Msieve 5A PLOT . . . . . . . . . . . . . . . . . . . . . .109Rt-Q-BOND PLOT . . . . . . . . . . . . . . . . . . . . . . .110Rt-QS-BOND PLOT . . . . . . . . . . . . . . . . . . . . . .110Rt-S-BOND PLOT . . . . . . . . . . . . . . . . . . . . . . . .110Rt-TCEP Capillary . . . . . . . . . . . . . . . . . . . . . . . .80Rt-U-BOND PLOT . . . . . . . . . . . . . . . . . . . . . . .110Rt-XLSulfur Micropacked . . . . . . . . . . . . . . . . .131Rt-XLSulfur Packed . . . . . . . . . . . . . . . . . . . . . .131Rt-γDEXsa Chiral . . . . . . . . . . . . . . . . . . . . . . . .68

RRttxx CCaappiillllaarryy GGCC CCoolluummnnssRtx-1 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .49Rtx-1 F&F . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .71Rtx-1301 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .55Rtx-1614 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .92Rtx-1701 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .56Rtx-20 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .51Rtx-200 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .54Rtx-200MS . . . . . . . . . . . . . . . . . . . . . . . . . . . . .54Rtx-225 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .56Rtx-2887 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .77Rtx-35 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .51Rtx-35 Amine . . . . . . . . . . . . . . . . . . . . . . . . . . .65Rtx-440 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .53Rtx-5 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .50, 85Rtx-5 Amine . . . . . . . . . . . . . . . . . . . . . . . . . . . .64Rtx-5 DHA Tuning . . . . . . . . . . . . . . . . . . . . . . . .75Rtx-5MS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .50Rtx-50 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .52Rtx-502.2 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .102Rtx-624 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .55Rtx-65 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .52Rtx-65TG . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .72Rtx-BAC1 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .82Rtx-BAC2 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .82Rtx-Biodiesel TG . . . . . . . . . . . . . . . . . . . . . . . . .81Rtx-CLPesticides . . . . . . . . . . . . . . . . . . . . . . . . .88Rtx-CLPesticides Kits . . . . . . . . . . . . . . . . . . . . .88Rtx-CLPesticides2 . . . . . . . . . . . . . . . . . . . . . . . .88Rtx-DHA . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .75Rtx-Dioxin2 . . . . . . . . . . . . . . . . . . . . . . . . . . . . .96Rtx-G27 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .86Rtx-G43 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .86Rtx-Mineral Oil . . . . . . . . . . . . . . . . . . . . . . . . . .99Rtx-OPPesticides . . . . . . . . . . . . . . . . . . . . . . . .91Rtx-OPPesticides2 . . . . . . . . . . . . . . . . . . . . . . .91Rtx-PCB . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .93Rtx-VMS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .100Rtx-Volatile Amine . . . . . . . . . . . . . . . . . . . . . . .63Rtx-Volatiles . . . . . . . . . . . . . . . . . . . . . . . . . . .102Rtx-VRX . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .101Rtx-Wax . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .58

RRuulleerr,, CCoommppaacctt SStteeeell .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..228811RRuuppttuurree DDiisscc TTeeeess .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..443366RRxxii CCaappiillllaarryy GGCC CCoolluummnnss

Rxi-1HT . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .47Rxi-1ms . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .41Rxi-5HT . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .47Rxi-5ms . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .41Rxi-5Sil MS . . . . . . . . . . . . . . . . . . . .42, 87, 95, 97Rxi-17 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .44Rxi-17Sil MS . . . . . . . . . . . . . . . . . . . . . .45, 73, 98Rxi-35Sil MS . . . . . . . . . . . . . . . . . . . . . . . . . . . .44Rxi-624Sil MS . . . . . . . . . . . . . . . . . . . .46, 83, 103Rxi-XLB . . . . . . . . . . . . . . . . . . . . . . . . . . . . .44, 94


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INDEX

Alphabetical

SSSaammppllee CCyylliinnddeerr VVaallvveess .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..443366SSaammppllee CCyylliinnddeerrss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..443355SSaammppllee DDeelliivveerryy SSyysstteemm .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..339966SSaammppllee IInnlleettss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..441155SSaammppllee LLooooppss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..443377SSaammppllee PPrreeppaarraattiioonn

Section Table of Contents . . . . . . . . . . . . . . . . .387Accessories

Caps . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .394Connectors . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .394Female Luer End Cap . . . . . . . . . . . . . . . . . . . . . . .394Frits . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .394Resprep SPE Flow Filter . . . . . . . . . . . . . . . . . . . . .397Tubes, Empty . . . . . . . . . . . . . . . . . . . . . . . . . . . . .394

ASE, Parts and Supplies . . . . . . . . . . . . .400 - 403Bulk Adsorbents . . . . . . . . . . . . . . . . . . . . . . . .398Cartridges

Bonded Reversed Phase . . . . . . . . . . . . . . . . . . . .392CarboPrep . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .393Closed End . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .392Florisil . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .392Ion Exchange Phases . . . . . . . . . . . . . . . . . . . . . . .392Method Specific . . . . . . . . . . . . . . . . . . . . . . . . . . .394Normal Phase . . . . . . . . . . . . . . . . . . . . . . . . . . . . .392Pesticide Residue Cleanup . . . . . . . . . . . . . . . . . . .393Polymeric Adsorbents . . . . . . . . . . . . . . . . . . . . . .392Reversed Bonded Phase . . . . . . . . . . . . . . . . . . . .392Specialty Cartridges . . . . . . . . . . . . . . . . . . . .393, 394

Centrifuge . . . . . . . . . . . . . . . . . . . . . . . . . . . . .390Disks, Resprep . . . . . . . . . . . . . . . . . . . . . . . . .397Flow Filters . . . . . . . . . . . . . . . . . . . . . . . . . . . .397Glassware

Burets . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .406Evaporator Apparatus . . . . . . . . . . . . . . . . . . . . . .404Extraction Apparatus . . . . . . . . . . . . . . . . . . . . . . .404Flasks . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .405, 406Funnels . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .406Glass Impingers, Midget . . . . . . . . . . . . . . . . . . . .407Pipets . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .407Stopper . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .407

Manifolds, Resprep . . . . . . . . . . . . . . . . .395, 396Parts for ASE Systems . . . . . . . . . . . . . .400 - 403Parts for Diskcover-47 Extraction System . . . .397PEEK Washers . . . . . . . . . . . . . . . . . . . . .400, 401QuEChERS Products, Q-sep

Centrifuge . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .390Packets . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .389Reference Standards . . . . . . . . . . . . . . . . . . . . . . .534Tubes . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .389

Sample Delivery System . . . . . . . . . . . . . . . . . .396Syringe Filters . . . . . . . . . . . . . . . . . . . . . . . . .399Tools for ASE Systems . . . . . . . . . . . . . . . . . . .403Tubes

QuEChERS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .389Vacuum Pressure Station . . . . . . . . . . . . . . . . .395

SSaammpplliinngg BBaaggss,, AAiirr .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..442233SSaammpplliinngg KKiittss,, PPaassssiivvee AAiirr .. .. .. .. .. .. .. .. .. ..441144 -- 441177,, 442200SSaammpplliinngg VVaallvveess .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..443377SSaapppphhiirree SSccrriibbee .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..227777SSAAXX SSPPEE TTuubbeess .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..339922SSccoorriinngg WWaaffeerr .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..227777SSccootttt TTrraannssppoorrttaabbllee GGaasseess .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..443322SSccrreeww--TThhrreeaadd VViiaallss .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..335588 -- 336633,, 336655SSccrreewwddrriivveerrss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..224411,, 228811,, 332233SSCCXX SSPPEE TTuubbeess .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..339922SSDDVVBB RReessiinn .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..442266SSeeaallss

GC Inlet . . . . . . . . . . . . . . . . . . . . . .222, 223, 255InsertionTool, HPLC . . . . . . . . . . . . . . . . . . . . .337Pump, HPLC . . . . . . . . . . . . . . . . . . . . . . . . . . .332

SSeeCCuurree ““YY”” GGCC CCoolluummnn CCoonnnneeccttoorr .. .. .. .. .. .. .. ..227700,, 229900SSeemmiinnaarrss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..1122,, 1133SSeemmiivvoollaattiilleess RReeffeerreennccee SSttaannddaarrddss.. SSeeee RReeffeerreennccee

SSttaannddaarrddss..SSeeppttaa .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..220055,, 221199,, 224477,, 225511,, 225555,, 226622SSeeppttaa HHoollddeerr KKiittss,, TThheerrmmoo SScciieennttiiffiicc .. .. .. .. .. .. .. .. .. ..225555SSeeppttuumm CCaapp,, TThheerrmmoo SScciieennttiiffiicc .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..225555SSeeppttuumm NNuuttss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..222200SSeeppttuumm PPuulllleerr .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..222200,, 224444,, 228822,, 442233SSeeppttuumm PPuurrggeedd PPaacckkeedd CCoolluummnn

PPoorrtt WWeellddmmeenntt .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..223322SShhiimmaaddzzuu GGCC SSuupppplliieess

Capillary Installation Gauge . . . . . . . . . . . . . . .252Capillary Nut . . . . . . . . . . . . . . . . . . . . . . . . . . .251Ferrules . . . . . . . . . . . . . . . . . . . . . . . . . .251, 286Injector Nut Kit, GC . . . . . . . . . . . . . . . . . . . . .251Injector Wrench . . . . . . . . . . . . . . . . . . . .252, 280Inlet Liners

Direct Injection . . . . . . . . . . . . . . . . . . . . . . . .249, 250PTV . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .250Siltek Metal . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .250Sky . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .211Split . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .211, 249Split/Splitless . . . . . . . . . . . . . . . . . . . . . . . . . . . . .250Splitless . . . . . . . . . . . . . . . . . . . . . . . . .211, 249, 250SPME . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .250Uniliner . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .249

O-Rings, Inlet Liner . . . . . . . . . . . . . . . . . . . . .251Septa, Plug . . . . . . . . . . . . . . . . . . . . . . . .205, 251Septum Nut . . . . . . . . . . . . . . . . . . . . . . . . . . . .251Syringes . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .375Tool Kit, MLE . . . . . . . . . . . . . . . . . . . . . . . . . . .252Wrench Set . . . . . . . . . . . . . . . . . . . . . . . .252, 280

SShhiimmaaddzzuu HHPPLLCC IInnssttrruummeenntt PPaarrttss .. .. .. .. .. .. .. .. .. .. .. ..332299SShhiinnCCaarrbboonn CCoolluummnnss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..113300SShhoorrtt--CCaapp VViiaallss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..335588SShhuutt--OOffff VVaallvveess .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..332222SSiillccooCCaann AAiirr SSaammpplliinngg CCaanniisstteerrss

Canisters . . . . . . . . . . . . . . . . . . . . . . . . .408 - 410Carrying Cases . . . . . . . . . . . . . . . . . . . . . . . . .419Cleaning System . . . . . . . . . . . . . . . . . . . . . . . .418Gauges . . . . . . . . . . . . . . . . . . . . . . . . . .411 - 413Precleaned . . . . . . . . . . . . . . . . . . . . . . . . . . . .419Reconditioning Service . . . . . . . . . . . . . . . . . . .422Supplies . . . . . . . . . . . . . . . . . . . . . . . . . .418 - 419Valves & Gauges . . . . . . . . . . . . . . . . . . .411 - 413

SSiillccooppoorrtt PPaacckkiinnggss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..113344SSiillccoosstteeeell TTrreeaatteedd

Filter . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .415Orifice . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .415Regulators . . . . . . . . . . . . . . . . . . . . . . . . . . . .309Tubing . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .321

SSiillccoosstteeeell--CCRR TTrreeaatteeddFittings . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .317Tubing . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .321

SSiilliiccaa SSPPEE CCaarrttrriiddggee .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..339922SSiilliiccaa,, BBuullkk HHPPLLCC PPaacckkiinngg MMaatteerriiaallss .. .. .. .. .. .. .. .. .. .. ..119944SSiilltteekk TTrreeaatteedd

Filter . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .415Fittings . . . . . . . . . . . . . . . . . . . . . . . . . . .315, 317Guard Columns . . . . . . . . . . . . . . . . . . . . . . . . . .33Inlet Liners . . . . . . . . . . . . . . . . . . . . . . . . . . . .213Inlet Liners, Metal

For Agilent GCs . . . . . . . . . . . . . . . . . . . . . . . . . . .218For Shimadzu GCs . . . . . . . . . . . . . . . . . . . . . . . . .250For Thermo Scientific GCs . . . . . . . . . . . . . . . . . . .254For Varian GCs . . . . . . . . . . . . . . . . . . . . . . . . . . . .261

Orifice . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .415Press-Tight Connectors . . . . . . . . .270, 288 - 290Tubing . . . . . . . . . . . . . . . . . . . . . . . . . . . .320, 321Vials . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .353

SSiimmiillaarr PPeerrffoorrmmaannccee GGCC PPhhaasseess CCrroossss--RReeffeerreennccee .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..2288,, 2299

SSiimmuullaatteedd DDiissttiillllaattiioonn RReeffeerreennccee SSttaannddaarrddss .. .. .. .. ..551155SSiinnggllee CCoommppoonneenntt SSoolluuttiioonnss .. .. .. .. .. .. .. .. .. .. .. ..444422 -- 444488SSiinnggllee SSoouurrccee FFuueellss RReeffeerreennccee SSttaannddaarrddss .. .. .. .. .. ..550022SSkkyy LLiinneerrss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..220066 -- 221111SSlleeeevveess.. SSeeee IInnlleett LLiinneerrss..SSlliiddee--LLoocckk TTwweeeezzeerrss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..228811SSooaapp FFiillmm BBuubbbbllee FFlloowwmmeetteerr .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..227755SSooffttwwaarree

Pro ezGC Methods Development Software . . . . . . . . . . . . . .24, 580

SSoolliidd PPhhaassee EExxttrraaccttiioonn.. SSeeee SSaammppllee PPrreeppaarraattiioonn..SSoolliidd SSuuppppoorrttss,, GGCC

CarboBlack . . . . . . . . . . . . . . . . . . . . . . . . . . . .127Chromosorb . . . . . . . . . . . . . . . . . . . . . . . . . . .126Cross-Reference . . . . . . . . . . . . . . . . . . . . . . . .139Silcoport . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .134

SSoolliidd WWaassttee RReeffeerreennccee SSttaannddaarrddss .. .. .. .. .. .. ..447700 -- 448855SSoollvveenntt DDeebbuubbbblleerr .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..334400SSppaarrggeerrss,, PPuurrggee aanndd TTrraapp .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..227711SSPPEE.. SSeeee SSaammppllee PPrreeppaarraattiioonn..SSppeecciiaallttyy SSPPEE CCaarrttrriiddggeess .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..339933,, 339944SSPPII IInnlleett LLiinneerrss

For Varian GCs . . . . . . . . . . . . . . . . . . . . . . . . .260SSpplliitt IInnlleett LLiinneerrss

For Agilent GCs . . . . . . . . . . . . . . . . . . . . .210, 217For PerkinElmer GCs . . . . . . . . . . . . . . . .210, 245For Shimadzu GCs . . . . . . . . . . . . . . . . . .211, 249For Thermo Scientific GCs . . . . . . . .211, 253, 254For Varian GCs . . . . . . . . . . . . . . . .211, 259 - 261

SSpplliitt VVeenntt LLiinnee .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..222299,, 330033SSpplliittlleessss IInnlleett LLiinneerrss

For Agilent GCs . . . . . . . . . . . . . . . . . . . . .210, 216For PerkinElmer GCs . . . . . . . . . . . . . . . .210, 245For Shimadzu GCs . . . . . . . . . . . . . . . . . .211, 249For Thermo Scientific GCs . . . . . . . . . . . .211, 253For Varian GCs . . . . . . . . . . . . . . . . . . . .259 - 261

SSSSII TTuubbee CCuuttttiinngg MMaacchhiinnee .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..332244SSttaabbiillwwaaxx CCaappiillllaarryy GGCC CCoolluummnnss

Stabilwax . . . . . . . . . . . . . . . . . . . . . . . . . . .59, 84Stabilwax-DA . . . . . . . . . . . . . . . . . . . . . . . . . . .67Stabilwax-DB . . . . . . . . . . . . . . . . . . . . . . . . . . .66

SSttaaiinnlleessss SStteeeell TTuubbiinngg .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..331199 -- 332211SSttaannddaarrddss.. SSeeee RReeffeerreennccee SSttaannddaarrddss..SSTTAARR SSeerrvviiccee RReewwaarrddss PPrrooggrraamm ((UUSS OOnnllyy)) .. .. .. .. .. ..1111SSttaattee--SSppeecciiffiicc UUSSTT RReeffeerreennccee SSttaannddaarrddss .. ..550055 -- 551122SSttaattiioonnaarryy PPhhaasseess.. SSeeee CCaappiillllaarryy GGCC CCoolluummnnss,,

HHPPLLCC CCoolluummnnss,, PPLLOOTT CCoolluummnnss,, PPaacckkeedd CCoolluummnnss..SSeeee aallssoo ccoolluummnn nnaammeess ((ee..gg..,, RRxxii))..

SSttooppppeerr,, GGllaasssswwaarree .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..440077SSttoorraaggee RRaacckk ffoorr VViiaallss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..335588,, 336677SSttoorraaggee UUnniittss,, HHPPLLCC .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..335500SSttxx CCaappiillllaarryy GGCC CCoolluummnnss

Stx-CLPesticides . . . . . . . . . . . . . . . . . . . . . . . . .90Stx-CLPesticides2 . . . . . . . . . . . . . . . . . . . . . . . .90Stx-CLPesticides Kits . . . . . . . . . . . . . . . . . . . . .90

SSuullffiinneerrtt TTrreeaatteeddFittings . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .317Gas Sampling Valves & Replacement Rotors .437Rupture Disc Tee . . . . . . . . . . . . . . . . . . . . . . . .436Sample Cylinder Valves . . . . . . . . . . . . . . . . . .436Sample Cylinders . . . . . . . . . . . . . . . . . . . . . . .435Sample Loops . . . . . . . . . . . . . . . . . . . . . . . . . .437Tubing . . . . . . . . . . . . . . . . . . . . . . . . . . . .320, 321

SSuuppeerr--CClleeaann GGaass PPuurriiffiieerrss .. .. .. .. .. .. .. .. .. ..229999 -- 330022,, 335500SSWW--884466 .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..447711 -- 448855SSwwaaggeellookk FFiittttiinnggss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..331133 -- 331155SSwwaaggeellookk VVaallvveess .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..332222


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INDEX

AlphabeticalSSwwaaggiinngg TTooooll .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..332255SSwwiittcchhoovveerr SSyysstteemmss,, GGaass CCyylliinnddeerr .. .. .. .. .. .. .. .. .. .. .. ..331122SSyyrriinnggee FFiilltteerrss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..339999SSyyrriinnggeess

Section Table of Contents . . . . . . . . . . . . . . . . .368Overview (Syringe Basics) . . . . . . . . . . . . . . . .369A-2 Luer . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .385Air Monitoring

Jumbo . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .385, 437Spare O-rings . . . . . . . . . . . . . . . . . . . . . . . . .385, 437

AutosamplerFor Agilent GCs . . . . . . . . . . . . . . . . . . . . . . .370 - 372For HPLC . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .349For PerkinElmer GCs . . . . . . . . . . . . . . . . . . . . . . .373For Shimadzu GCs . . . . . . . . . . . . . . . . . . . . . . . . .375For Thermo Scientific GCs . . . . . . . . . . . . . . .376, 377For Varian 8000 Series GCs . . . . . . . . . . . . . . . . . .374

Cross-Reference Table for Agilent GCs . . . . . .372Gas-Tight . . . . . . . . . . . . . . . . . . . . .371, 381 - 385

Teflon Tip . . . . . . . . . . . . . . . . . . . . . . . . . . . .381, 382With Shut-Off Valves . . . . . . . . . . . . . . . . . . . . . . .383

HPLCAutosampler . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .349Gas-Tight for Rheodyne & Valco Valves . . . .347, 384Microliter Liquid-Type for

Rheodyne & Valco Valves . . . . . . . . . . . . . . . . . .348Priming for Waters HPLC Pumps . . . . . . . . . . . . . .348Syringes for Waters U6K Valves . . . . . . . . . . . . . .346

Large Volume . . . . . . . . . . . . . . . . . . . . . . . . . .371Luer-Lock Needles . . . . . . . . . . . . . . . . . .382, 383Micro-Volume . . . . . . . . . . . . . . . . . . . . . . . . . .380Microliter Syringes . . . . . . . . . . . . . .370, 378, 379Model V Valve . . . . . . . . . . . . . . . . . . . . . . . . .383Overview . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .369Plastic . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .369Precision Sampling

A-2 Luer Gas-Tight Syringes . . . . . . . . . . . . . . . . .385Heavy Duty Purge & Trap Syringe . . . . . . . . . . . . .385Luer-lock Valve Adaptor . . . . . . . . . . . . . . . . . . . . .385

Replacement NeedlesFor Agilent 7673/7683 Autosampler Syringes . . .371For Gas-Tight Syringes for

Rheodyne & Valco Valves . . . . . . . . . . . . . .347, 384For Gas-Tight Syringes with Shut-off Valves . . . . .383For HPLC Syringes . . . . . . . . . . . . . . . . .346, 347, 384For Luer-Lock Syringes . . . . . . . . . . . . . . . . . . . . .382For PerkinElmer Autosampler Syringes . . . . . . . . .373For Shimadzu Autosampler Syringes . . . . . . . . . . .375For Teflon Tip, Gas-Tight Syringes . . . . . . . . . . . .382For Thermo Scientific . . . . . . . . . . . . . . . . . . .376, 377For Varian 8000 Series Syringes . . . . . . . . . . . . . .374For Waters U6K Valves . . . . . . . . . . . . . . . . . . . . .346

Syringe Guides . . . . . . . . . . . . . . . . . . . . . . . . .383Syringe O-rings . . . . . . . . . . . . . . . . . . . . .385, 437

TTTaabbllee ooff CCoonntteennttss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..11TTCCLLPP SSoolliidd WWaassttee RReeffeerreennccee SSttaannddaarrddss .. .. .. .. .. .. .. ..447700TTDDUU ((TThheerrmmaall DDeessoorrppttiioonn UUnniitt)) TTuubbeess,,

AAiirr MMoonniittoorriinngg .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..442244TTeeddllaarr GGaass SSaammpplliinngg BBaaggss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..442233TTeeee WWrreenncchh .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..332255TTeeeess

Direct Injection . . . . . . . . . . . . . . . . . . . . .233, 269Pipe & Tube Fittings . . . . . . . . . . . . . . . .313 - 317Rupture Disc . . . . . . . . . . . . . . . . . . . . . . . . . . .436

TTeefflloonnFerrules, GC . . . . . . . . . . . . . . . . . . . . . . . . . . .286Syringes, Teflon-Tip . . . . . . . . . . . . . . . . .381, 382Transfer Lines for ELCDs . . . . . . . . . . . . . . . . .271

Tubing Cutter . . . . . . . . . . . . . . . . . . . . . . . . . .333Tubing, HPLC . . . . . . . . . . . . . . . . . . . . . . . . . . .333

TTeefflloonn TTaappee .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..332255TTeemmppeerraattuurree CCoonnttrroolllleerr,, HHPPLLCC .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..334433TTeennaaxx PPaacckkiinnggss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..113377TTeennnneesssseeee UUSSTT RReeffeerreennccee SSttaannddaarrddss .. .. .. .. .. .. .. .. ..551111TTeesstt GGaauuggeess,, AAiirr MMoonniittoorriinngg .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..441133TTeesstt MMiixxeess

GC . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .538HPLC . . . . . . . . . . . . . . . . . . . . . . . . . . . . .199, 539

TTeexxaass UUSSTT RReeffeerreennccee SSttaannddaarrddss .. .. .. .. .. .. .. .. .. .. .. .. ..551111TThheerrmmaall DDeessoorrppttiioonn UUnniitt TTuubbeess,,

AAiirr MMoonniittoorriinngg .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..442244TThheerrmmaall GGaass PPuurriiffiieerr .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..330033TThheerrmmoo SScciieennttiiffiicc GGCC SSuupppplliieess

Adaptors for Capillary Columns . . . . . . . . . . . .256Capillary Installation Gauge . . . . . . . . . . . . . . .257Electron Multiplier . . . . . . . . . . . . . . . . . . . . . .258EZ No-Vent GC/MS Connector . . . . . . . . . . . . .258FID Jet . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .256Fixing Nut for TRACE & Focus SSL . . . . . . . . . .256Graphite Ferrules for M4 Fittings . . . . . .256, 286Graphite Sealing Ring . . . . . . . . . . . . . . . . . . . .255Hex Key Set, Metric . . . . . . . . . . . . .257, 281, 323Inlet Liner Seals . . . . . . . . . . . . . . . . . . . . . . . .255Inlet Liners

Direct Injection (4000-5000-6000 GCs) . . . . . . . . .253Direct Injection (TRACE & Focus SSL) . . . . . . . . . .254Siltek Metal . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .254Sky . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .211Split (4000-5000-6000 GCs) . . . . . . . . . . . . . . . . . .253Split (TRACE & Focus SSL) . . . . . . . . . . . . . . .211, 253Split (TRACE 2000 GCs) . . . . . . . . . . . . . . . . . . . . .254Splitless (4000-5000-6000 GCs) . . . . . . . . . . . . . . .253Splitless (TRACE & Focus SSL) . . . . . . . . . . . .211, 253Uniliner (4000-5000-6000 GCs) . . . . . . . . . . . . . . .253

Liner Cap . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .255Liner Cap Removing Tool . . . . . . . . . . . . .257, 283Septa . . . . . . . . . . . . . . . . . . . . . . . . . . . . .205, 255Septa Holder Kits for TRACE & Focus SSL . . . .255Septum Cap for TRACE & Focus SSL . . . . . . . .255Syringes . . . . . . . . . . . . . . . . . . . . . . . . . .376, 377Terminal Fitting Nut . . . . . . . . . . . . . . . . . . . . .256Tool Kit, MLE . . . . . . . . . . . . . . . . . . . . . . . . . . .257Transfer Line Reducing Kit . . . . . . . . . . . . . . . .258Wrench Set, Metric . . . . . . . . . . . . . . . . .257, 280

TThheerrmmoo SScciieennttiiffiicc HHPPLLCC SSuupppplliieessSyringes, Autosampler . . . . . . . . . . . . . . . . . . .349

TThheerrmmoo SSeeppaarraattiioonn HHPPLLCC IInnssttrruummeenntt PPaarrttss .. .. .. .. ..333300TThheerrmmoolliittee SSeeppttaa .. .. .. .. .. .. .. .. .. .. .. .. .. ..220055,, 221199,, 225555,, 226622TThheerrmmoommeetteerr .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..228822TTOO AAiirr MMoonniittoorriinngg RReeffeerreennccee SSttaannddaarrddss

TO-14A . . . . . . . . . . . . . . . . . . . . . . . . . . .427, 428TO-15 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .428

TTOO--CCaann AAiirr SSaammpplliinngg CCaanniisstteerrssCanisters . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .411Carrying Cases . . . . . . . . . . . . . . . . . . . . . . . . .419Cleaning System . . . . . . . . . . . . . . . . . . . . . . . .418Gauges . . . . . . . . . . . . . . . . . . . . . . . . . .411 - 413Reconditioning Service . . . . . . . . . . . . . . . . . . .422Supplies . . . . . . . . . . . . . . . . . . . . . . . . . .418 - 419Valves & Gauges . . . . . . . . . . . . . . . . . . .411 - 413

TTooggggllee VVaallvveess .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..332222TToooollss

5-in-1 Magnetic Screwdriver . . . . . . . . . . . . . .32354-Piece Tool Kit . . . . . . . . . . . . . . . . . . . . . . . .323ASE Extraction System . . . . . . . . . . . . . . . . . . .403Brushes

Nylon . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .281Stainless Steel . . . . . . . . . . . . . . . . . . . . . . . . . . . .281

Capillary Column InstallationCapillary Installation

Gauge . . . . . . . . . . . . .221, 235, 252, 257, 263, 278Ceramic Scoring Wafer . . . . . . . . . . . . . . . . . . . . .277Compact Steel Ruler . . . . . . . . . . . . . . . . . . . . . . . .281High-Temperature String . . . . . . . . . . . . . . . . . . . .281MLE Tool Kits . . . . . . . . .231, 248, 252, 257, 263, 276Needle Files . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .282Pocket Magnifier . . . . . . . . . . . . . . . . . . . . . . . . . .282Rethreading Tool . . . . . . . . . . . . . .220 , 230, 263, 280Sapphire Scribe . . . . . . . . . . . . . . . . . . . . . . . . . . .277Slide-Lock Tweezers . . . . . . . . . . . . . . . . . . . . . . . .281Stainless Steel Tube Brushes . . . . . . . . . . . . . . . .281Wrench, Open-End, 1/4- to 3/16-Inch . . . . . . . . . . . .291Wrench, Open-End, 1/4- to 5/16-Inch . . . . . . . . . . . .280

Claw and Holder . . . . . . . .215, 231, 248, 279, 367Column Cutter, Capillary GC . . . . . . . . . . . . . . .277Cylinder Valve Wrench . . . . . . . . . . . . . . . . . . .312Flashlight . . . . . . . . . . . . . . . . . . . . . . . . .282, 325Gap Inspection Gauge . . . . . . . . . . . . . . . . . . .325GC Installation Kit . . . . . . . . . . . . . . . . . . . . . .323Hand Drill, Mini . . . . . . . . . . . . . . . . . . . . . . . . .282HPLC . . . . . . . . . . . . . . . . . . . . . . . . . . . . .336, 337Injection Port Repair Tool . . . . . . . . . . . . . . . . .220Injector Wrench . . . . . . . . . . . . . . . . . . . . . . . .280Inlet Liner Packing Tool . . . . . . . . . . . . . .215, 279Inlet Liner Removal Tool . . . . .215, 231, 244, 279Maintenance Kits, GC . . . . . . . . . . . . . . . .275, 276Maintenance Kits, HPLC . . . . . . . . . . . . . . . . . .336PEEK Fitting Extractor . . . . . . . . . . . . . . . . . . .337PEEK Performance Kit, HPLC . . . . . . . . . . . . . .336Piston Seal Insertion Tool . . . . . . . . . . . . . . . .337Plier Set . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .323Ruler, 15cm, Steel . . . . . . . . . . . . . . . . . . . . . . .281Screwdriver . . . . . . . . . . . . . . . . . . . . . . . . . . .323Septum Nut Removal Tool . . . . . . . . . . . .220, 283Survival Kit, HPLC . . . . . . . . . . . . . . . . . . . . . . .336Swaging Tool . . . . . . . . . . . . . . . . . . . . . . . . . . .325Tool Kits, MLE . . . . . . . . . . . . . . . . . . . . . . . . . .276Tubing

Bender . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .325Cutter Dressing Tool . . . . . . . . . . . . . . . . . . .325, 333Cutters . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .324, 333Reamers . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .325

ValvTool . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .337Wrenches

Adjustable . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .323Cylinder . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .312Cylinder Valve . . . . . . . . . . . . . . . . . . . . . . . . . . . . .312Injector . . . . . . . . . . . . . . . . . . . . . .220, 230, 252, 280Open-End . . . . . . . . . . . . . . . . . . . . . . . .248, 280, 291Tee . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .325ValvTool . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .337

TTooxxaapphheennee SSoolluuttiioonnss .. .. .. .. .. .. .. .. .. .. ..445533,, 445544,, 446699,, 449955TTRRAACCEE SSuupppplliieess.. SSeeee TThheerrmmoo SScciieennttiiffiicc GGCC SSuupppplliieess..TTrraaddeemmaarrkkss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..1155TTrraannssffeerr LLiinneess ((GGuuaarrdd CCoolluummnnss))

Capillary GC . . . . . . . . . . . . . . . . .33 - 35, 40, 114MXT Stainless Steel, GC . . . . . . . . . . . . . . . . . .114

TTrraappss Air Compressor Hydrocarbons . . . . . . . . . . . . .298Chemical Traps for Agilent GCs . . . . . . . .229, 303ECD Vent . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .298Gas Purifiers . . . . . . . . . . . . . . . . . . . . . .296 - 303Overview of Gas Purifiers . . . . . . . . . . . . . . . .295Rechargeable Gas Purifiers

Molecular Sieve S-Trap . . . . . . . . . . . . . . . . . . . . .297Refillable Hydrocarbon . . . . . . . . . . . . . . . . . . .298Restek Gas Management System . . . . . . . . . .296Super-Clean . . . . . . . . . . . . . . . . . . .299 - 302, 350VICI mat/sen Gas-Specific

Purifier Modules . . . . . . . . . . . . . . . . . . . . . .303


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INDEX

AlphabeticalTTrriiddeenntt HHPPLLCC GGuuaarrdd CCoolluummnnss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..119966TTRRPPHH RReeffeerreennccee SSttaannddaarrddss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..447700TTuubbee BBrruusshheess .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..228811TTuubbee FFiittttiinnggss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..331133 -- 331177TTuubbiinngg

Bender . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .325Clips . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .333Connectors. See Connectors, Tubing.Copper . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .319Cutter Dressing Tool . . . . . . . . . . . . . . . . .325, 333Cutters . . . . . . . . . . . . . . . . . . . . . . . . . . .324, 333Electropolished . . . . . . . . . . . . . . . . . . . . .320, 321HPLC Column . . . . . . . . . . . . . . . . . . . . . .332, 351Hydroguard . . . . . . . . . . . . . . . . . . . . . . . . .34, 321Instrument-Grade . . . . . . . . . . . . . . . . . . . . . . .319PEEK . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .332Reamers . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .325Scorer for MXT Columns . . . . . . . . .114, 277, 324Silcosteel-CR-Treated . . . . . . . . . . . . . . . .320, 321Silcosteel-Treated . . . . . . . . . . . . . . . . . . . . . . .321Siltek-Treated . . . . . . . . . . . . . . . . . . . . . .320, 321Stainless Steel . . . . . . . . . . . . . . . .319 - 321, 332Sulfinert-Treated . . . . . . . . . . . . . . . . . . .320, 321Swaging Tool . . . . . . . . . . . . . . . . . . . . . . . . . . .325Teflon . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .333

TTuunniinngg MMiixxttuurree .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..446699,, 447799,, 448899TTwwoo--HHoollee FFeerrrruulleess .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..223333,, 226699,, 228855

UUUHHPPLLCC FFiilltteerrss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..119955UUllttrraa HHPPLLCC CCoolluummnnss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..118822 -- 118899UUllttrraa IIII HHPPLLCC CCoolluummnnss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..115566 -- 116655UUllttrraa QQuuaatt RReeaaggeenntt SSoolluuttiioonn .. .. .. .. .. .. .. .. ..118899,, 119999,, 446611UUllttrraa--CClleeaann RReessiinn .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..442266UUnniilliinneerr IInnlleett LLiinneerrss

For Agilent GCs . . . . . . . . . . . . . . . . . . . . .210, 218For PerkinElmer GCs . . . . . . . . . . . . . . . . . . . .246For Shimadzu GCs . . . . . . . . . . . . . . . . . .249, 250For Thermo Scientific GCs . . . . . . . . . . . .253, 254For Varian GCs . . . . . . . . . . . . . . . . . . . .259 - 261

UUnniioonnss.. SSeeee aallssoo CCoonnnneeccttoorrss..Brass . . . . . . . . . . . . . . . . . . . . . . . . .313, 314, 316PEEK . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .335Pipe . . . . . . . . . . . . . . . . . . . . . . . . . . . . .313 - 317Reducing . . . . . . . . . . . . . . . . . . . . .293, 313 - 317Silcosteel-CR Treated . . . . . . . . . . . . . . . .315, 317Siltek/Sulfinert Treated . . . . . . . . . . . . . .315, 317Stainless Steel . . . . . . . . . . . . . . . . .313, 314, 316Transfer Line Reducing Kit . . . . . . . . . . . . . . . .258Tube . . . . . . . . . . . . . . . . . . . . . . . . . . . . .313 - 317Zero Dead-Volume . . . . . . . . . . . . . . . . . .293, 335

UUnnlleeaaddeedd GGaassoolliinnee RReeffeerreennccee SSttaannddaarrddss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..550011,, 550022,, 550055,, 552233

UUSS PPhhaarrmmaaccooppooeeiiaa CCrroossss RReeffeerreennccee .. .. .. .. .. .. .. .. .. ..115533UUSSLLCC .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..115544,, 115555UUSSPP <<446677>> RReeffeerreennccee SSttaannddaarrddss .. .. .. .. .. .. .. .. .. .. ..552288UUSSTT RReeffeerreennccee SSttaannddaarrddss .. .. .. .. .. .. .. .. .. .. .. .. .. ..550011 -- 551122

VVVaaccuuuumm

Bag Sampler, Air Monitoring . . . . . . . . . . . . . .423Gauge . . . . . . . . . . . . . . . . . . . . . . . . . . .411 - 413Pressure Station for Resprep SPE Systems . .395Vu-Union Connector . . . . . . . . . . . . . . . . .227, 291

VVaallccoo FFiittttiinnggss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..229933,, 331177,, 333355VVaallvvee AAddaappttoorr,, LLuueerr LLoocckk NNeeeeddlleess .. .. .. .. .. .. .. .. .. .. .. ..338855VVaallvvee PPaarrttss,, HHPPLLCC .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..332277 -- 333311VVaallvveess .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..332222

Ball . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .317Check, HPLC . . . . . . . . . . . . . . . . . . . . . . . . . . .332Diaphragm, Air Monitoring . . . . . . . . . . .410 - 412Metering, GC . . . . . . . . . . . . . . . . . . . . . . . . . . .322Plug . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .317Sampling, Sulfinert-Treated . . . . . . . . . . . . . . .437Shut-off, GC . . . . . . . . . . . . . . . . . . . . . . . . . . . .322

VVaarriiaann GGCC SSuupppplliieessCapillary Installaton Gauge . . . . . . . . . . . . . . .263Capillary Nuts . . . . . . . . . . . . . . . . . . . . . . . . . .263EZ No-Vent GC/MS Connector . . . . . . . . . . . . .264Inlet Liner Seals . . . . . . . . . . . . . . . . . . . . . . . .262Inlet Liners

Direct Injection . . . . . . . . . . . . . . . . . . . . . . . . . . . .259For 1075/1077 GCs . . . . . . . . . . . . . . . . . . . . . . . .259For 1078/1079 GCs . . . . . . . . . . . . . . . . . . . .211, 261For 1177 GCs . . . . . . . . . . . . . . . . . . . . . . . . .211, 260Siltek Metal . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .261Sky . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .211SPI . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .260Split . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .259Splitless . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .259SPME . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .259Uniliner . . . . . . . . . . . . . . . . . . . . . . . . .211, 259 - 261

Inlet Spring, Siltek . . . . . . . . . . . . . . . . . . . . . .263Rethreading Tool . . . . . . . . . . . . . . . . . . . . . . . .263Septa . . . . . . . . . . . . . . . . . . . . . . . . . . . . .205, 262Syringes . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .374Tool Kit, MLE . . . . . . . . . . . . . . . . . . . . . . . . . . .263

VVeenntt ffoorr GGCC//MMSS .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..223344,, 225588,, 226644VVeenntt TTrraapp .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..229988VVeerriifflloo FFllooww CCoonnttrroolllleerr .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..441155VVeerrnniieerr KKnnoobb .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..332222VVeessppeell RRiinngg IInnlleett SSeeaall,, DDuuaall .. .. .. .. .. .. .. .. .. .. .. .. ..222222,, 222233VViiaallss

Section Table of Contents . . . . . . . . . . . . . . . . .352Overview (Vial Basics) . . . . . . . . . . . . . . . . . . .3532.0mL Vials

8mm Screw-Thread . . . . . . . . . . . . . . . . . . . .359, 3609mm Short-Cap, Screw-Thread . . . . . . . . . . . . . . .35810mm Screw-Thread . . . . . . . . . . . . . . . . . . .360, 36111mm Crimp-Top . . . . . . . . . . . . . . . . . . . . . . . . . .35611mm Poly Crimp . . . . . . . . . . . . . . . . . . . . . . . . . .357

AccessoriesCrimpers and Decappers . . . . . . . . . . . . . . . . . . . .366Sampling Valves, Mininert . . . . . . . . . . . . . . . . . . .365Storage Racks . . . . . . . . . . . . . . . . . . . . . . . .358, 367

Certified . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .357Crimp Top . . . . . . . . . . . . . . . . . . . . .356, 361, 363Headspace . . . . . . . . . . . . . . . . . . . . . . . . . . . .363Micro-Vials . . . . . . . . . . . . . . . . . . . . . . . . . . . .365Mininert Precision Sampling . . . . . . . . . . . . . .365Poly Crimp . . . . . . . . . . . . . . . . . . . . . . . . . . . .357Precleaned VOA . . . . . . . . . . . . . . . . . . . . . . . .364Quick Reference Size Chart . . . . . . . . . . .354, 355Sample Collection Vials for ASE . . . . . . . . . . . .400Screw Thread . . . . . . . . . . . . . . . . . . . . .357 - 362Screw Thread Caps . . . . . . . . . . . . . . . . . . . . . .363Septum Selection Guide . . . . . . . . . . . . . . . . . .353Shell . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .362Short-Cap, Screw-Thread . . . . . . . . . . . . . . . . .358Siltek Deactivated . . . . . . . . . . . . . . . . . . . . . . .353Versa Vial . . . . . . . . . . . . . . . . . . . . . . . . . . . . .364VOA Sampling Vials . . . . . . . . . . . . . . . . . . . . .364WISP . . . . . . . . . . . . . . . . . . . . . . . . . . . . .361, 362

VVIICCII MMaatt//SSeenn GGaass--SSppeecciiffiicc PPuurriiffiieerr MMoodduulleess .. .. .. ..330033VViittoonn OO--RRiinnggss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..221199,, 225511

VViivvaa ((WWiiddee--PPoorree)) HHPPLLCC CCoolluummnnss .. .. .. .. .. .. .. .. ..119900 -- 119933VVoollaattiilleess ((VVOOAA)) RReeffeerreennccee SSttaannddaarrddss.. SSeeee RReeffeerreennccee

SSttaannddaarrddss..VVuu--TTiigghhtt .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..226655

Inlet Liners . . . . . . . . . . . . . . . . . . . . . . . . . . . .265Installation Fittings . . . . . . . . . . . . . . . . . . . . .265

VVuu--UUnniioonn CCoonnnneeccttoorrss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..222277,, 229911VVuu22--UUnniioonn CCoonnnneeccttoorrss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..228899

WWWaarrrraannttyy .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..1155WWaasshhiinnggttoonn UUSSTT RReeffeerreennccee SSttaannddaarrddss .. .. .. .. .. .. .. ..551122WWaassttee OOvveerrffllooww IInnddiiccaattoorr,, HHPPLLCC .. .. .. .. .. .. .. .. .. .. .. .. ..333388WWaasstteewwaatteerr MMeetthhooddss

RReeffeerreennccee SSttaannddaarrddss .. .. .. .. .. .. .. .. .. .. .. .. .. ..446644 -- 446699WWaatteerrss HHPPLLCC IInnssttrruummeenntt PPaarrttss .. .. .. .. .. .. .. .. .. ..333300,, 333311WWeeaatthheerreedd PPeettrroocchheemmiiccaall

RReeffeerreennccee SSttaannddaarrddss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..552233WWeellll IInnvveessttiiggaattiioonn PPrrooggrraamm

RReeffeerreennccee SSttaannddaarrddss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..550077WWiiddee--PPoorree HHPPLLCC CCoolluummnnss .. .. .. .. .. .. .. .. .. .. .. .. .. ..119900 -- 119933WWiissccoonnssiinn UUSSTT RReeffeerreennccee SSttaannddaarrddss .. .. .. .. .. .. .. .. .. ..551122WWIISSPP VViiaallss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..336611,, 336622WWiizzaarrdd DDoollllaarr PPrrooggrraamm ((UUSS OOnnllyy)) .. .. .. .. .. .. .. .. .. .. .. .. .. ..1100WWooooll PPuulllleerr//IInnsseerrtteerr .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..221155,, 227799WWooooll,, DDeeaaccttiivvaatteedd .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..221144,, 224444WWrreenncchheess

Adjustable . . . . . . . . . . . . . . . . . . . . . . . . . . . . .323Cylinder . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .312Cylinder Valve . . . . . . . . . . . . . . . . . . . . . . . . . .312Hex Key (Allen) . . . . . . . . . . . . . . . . .257, 281, 323Injector . . . . . . . . . . . . . . . . . . .220, 230, 252, 280Metric Set . . . . . . . . . . . . . . . . . . . . . . . . .257, 280Open-End . . . . . . . . . . . . . . . . .248, 252, 280, 291Spanner Wrench for Agilent GCs . . . . . . . . . . .238Tee . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .325ValvTool . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .337

XXXAADD EEqquuiivvaalleenntt RReessiinn .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..442266

ZZZeerroo AAiirr GGeenneerraattoorrss .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..330055,, 330088ZZeerroo DDeeaadd--VVoolluummee CCoonnnneeccttoorrss .. .. .. .. .. .. .. .. .. .. ..229933,, 333355


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