Customer Tracy Watson Avara Sharlnon Pharmaceutical Sevices Shannon Industrial Estate Shannon Clam Certificate Of Analysis Job Number: 17-35181 bueNumber: 1 Report Date: 14 November 2017 Site: Not Applicable PO Number: 4560436720 Date Samples Received: 0111 112U-17 Please find attached the results for the samples received at our laboratory on 01/13/2017. Should you have any queries regarding the report or require any further services, we would be happy to diseuss your requirements. For additional information about the company please lag-on to our website at the above address. Thank yau far choosing City Analysts Limited. We look forward to assisting you again.. Authorised By; Authorised Date: 14 November 201 7 Sham Reynolds Laboratory Manager Ndas: R@sulh relate only to the itams testad. Information on methods of analyds and pe~omance characteristics i5 available on request. Any opinfans or interpretations indioated are outside the scope of uur fNAB accreditation. This fqsi ppcifi shall ~ l ~ f be rq~p$ljc+g exmpt in full or with written approval of City .. Analysts . Limited. Page 1 of 7 For inspection purposes only. Consent of copyright owner required for any other use. EPA Export 16-03-2018:03:33:18
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Certificate Of Analysis Job Number: 17-35181 b u e N u m b e r : 1 Report Date: 14 November 2017
Site: Not Applicable PO Number: 4560436720 Date Samples Received: 0111 112U-17
Please find attached the results for the samples received at our laboratory on 01/13/2017.
Should you have any queries regarding the report or require any further services, we would be happy to diseuss your requirements. For additional information about the company please lag-on to our website at the above address.
Thank yau far choosing City Analysts Limited. We look forward to assisting you again..
Authorised By; Authorised Date: 14 November 201 7
Sham Reynolds Laboratory Manager
Ndas: R@sulh relate only to the itams testad. Information on methods of analyds and pe~omance characteristics i5 available on request. Any opinfans or interpretations indioated are outside the scope of uur fNAB accreditation. This fqsi ppcifi shall ~ l ~ f be rq~p$ljc+g exmpt in full or with written approval of City .. Analysts . Limited.
City Analysts Lifted, Pipm Hou&0 Road, Ringsend, Dublin 4.
t
Date of Sampling: 0 I I I t121117
Date Sample Received: Oi/l1/20~7
PV Value Analysis Parameter Result Units (Drinking
Start Date Water Only)
0911 1 /XI 7 Alkalinity CaC03 572.662 msn
06/11/2017 Copper e a.mo msn Cyclhexane 1-170 mgll
OlJllS2017 BOD5 31 mg/lO2
FOG
1 . 1 - 1 n-butanol I r 1 M O O I uan I - I
NOM: PV Value Is the parametric value, laken from European Cornmunitias, (Drlnklng Water) Regufahs, 201 4. S.I. No. 122 of 2U14 and relatee only to drlnking wter samples. For queries on results, please conlac! us wiffih ma weeks af the report date to ensure that we can acoornmtxiate your query as samples emnot be stored i*OiV3lY. NAC 8, RTC- Na abbnomal change and amptable to custnrners. TVC -Totar vlabIe count Site D = Analped at Ci& Analysts Dublin. Sk $ at City Analysts Shamon
nPrnpyl Acetate T lOO.0t) US11 iso-Prapyl Acetate < 100.00 ugll
Slte: Not Applicable
SampJe Description: ESO2 0211 1/2017
Sample Type: Effluent (Final)
Lab Reference Number: 376475
L
* *
Site I Method Ref.
t
*
*
*
MlBK < 1OO.OQ ugll -
THF 1oa.m ug/l - r: l a m w g t ten Butyl Abohol
1
"U
'U f
*U
Date of Sampling: OllllW017
Uate Sample Received; Qlll Id01 7
- Butyric acid < 10,000 mg/l
Iso-valeric Acid -z f 0.000 mg/l
Valeric acid < TO.DO0 mgll
Caproic Acid *. 10.000 mgll
PV Value (Drinking
Water Only]
I c I - I < 25.80 t uall I - I 1 . 1 - 1 &Butanone 1 c 100.00 I U d l I - I
I udl 1 - I r; 100.00 1 . 1 - 1 Isobutanol I
I *U- I - I Acetic Add I f0.000 I I - I I * u I - I Prmianic acid I <10.000 I mall I - I I * u I - I Iso-buMic Acid I < 10.000 I mall I - I
#= INAB Accredited, U = UKAS Accredited, * =Subcontracted
Nbk: PVVdue [S the parametric value, taken from European hrnmnitias, (Drlnklng Walsr) Regutatkxls, 20'14,5,1, No. 122 of 8014 and relates only lo drinking wafef samples. FW queries on results, pkam contact us within two weeks of the report date to ensure that we ean accommodate your query as samples cannot be stored Indefinitely. NAG d ATC - Nu abnormal change and acceptable to customws. TVG - Total viable munl Site D = Analysed at CUy Andyak Dublin. S b S = Analysed at Ciy Anarets Shannon
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Customer Tracy Watson
Site I Analysis Parameter Result Methad Ref. Start Date
l0.no t ua(l 1 - 1 1 . 1 - 1 1,3,5-Tri~hlorabenzene I
I - L U l - l 2-Chloroto bene
I * u I - I 6Ghlarotoluene r: 2.00 I Wfl I - I
Benzene I < 1,uo I U411 I - I
~
Bromoform I Bramomethane I c 2.00
I * U l - l Carbon Dlsulphide I 1.00
I I 1 1 I ugn "w ChIoro benzene .= 4.00 I # = INAE Accredlfed, U = UYAS Accredited, * = Subcontracted
Nom: PV Value Is the parmetic value, Taken from European Oommunities, (Drtnkirag Water) Reguhtims, 2p14. S.I. No. 122 of 2014 and relata only lo drlnking water samples. Far queries on reaulls, please c n n w us wlthin two weeks af the report date to ensure that we can accommodate your queq as samples cannot ba m t e d indefinitely. NAG a A X - No abnormal change and acceptable fo Gustomem. TVC - Totat viabb count Stta 0 = Analysed at ciiAflaIy6k D&lh. SikS = Anzdysed at City Analysfs Shannon
#= IMAB Accredited, U I UKAS Accredited, * = Subconwackd
Nota: PV Vahm is We parametricvalue, Wen from European Gomrnunlties, {Drinking Water) Regulations, 201 4. XI. No. 122 OF 2014 and mlabs only to drinking watm sanlpk. For guerbes on masuks, please contact us W'thfn two weeks d Ihe repoft dab to ensure that we can accomrndale your query as samples cannot be stored indefinitely. NAG B AT0 - No &nmmal change and awe&&[@ to C U S ~ C I ~ ~ O ~ S . TVC -Total viable count Sit8 0 = Analysed al City Analysts Oublin. Slle 3 t: Analysed at City Analysts Shannon
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TeILab Q
Certificate No: L117fI838 Date Redd: DYI1/2017
hsuc Date: OB12r2017 Our Rep ws-44316
€EKTlFICATE OF ANALYSIS Page 1 of 2
Project Description: Analysis of Aqueous SmpIe
Attention: I1 Company: Addre@:
Lab m: 142050
Project Summary: One $ample ws analysed for a i w g e ofdetemn~nmds. Please see page 2 krresdts. Tams 8t Cmditiow and methods used ai= outlined in the attached appendix.
No. of Pages:
Mr, Peter O’Byrne QiteIity Manager
Ms Breds Moore Technical Manager
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Page 2 of 2
Sample ID
Determ inand Lab It)
Nitrate as N nla
Tellab ES 02
0111112017
242050
4 . 5 6 (note I)
ANALYSIS OF AQUEOUS SAMPLE.
Date Sampled: O l / l ID017 Date Received: 0Y.t 1/2017 Date Analysis Commenced: 05/72/2017 Our Ref: WS-44316 Certificate No: U1 7/1838
Note I: LOD raised due to sample matrix interference.
Results expressed as mgd (ppm) unless stated otherwise
Certificate Of Analysis Job Number; 17'3541 3 lssue Number: 5 Report Date; -14 November 2037
Site: Not Applicable PO Number: 4500436720 Date Samples Received: 08/11 E201 7
Ptease find attaehed the results for the samples received at our laboratory on 08/11/2017,
Should you have any queries raqarding the report or require any further services, we would he happy to discuss your requirements. Far additional information about the company please log-on to our website at the above address.
Thank you far choosing City Analysts Limited. We look forward to assisting you again.
Sham Reynolds Laboratory Manager
Notes: Results relate only to the items tested. Information on methods of analysts and petformane characterlstlcs Is avaifable on request. Any opinions or interpretatiaDs Sndicated are out.side the scope of our ]NAB aecredltation. This test report shall nat be reproduced except in full or wjth written approval of City Analysts Limited.
PV Value Analysis Parameter Result Unit5 [Drinking
Start Date Water Only)
O&/11/2017 BOD5 22 mg/J 02
Site: Not Applicabls
Sample Description: ESQ2 OW1 1117
Sample Type: Effluent (Final)
Lab Referenm Numberr 3771 15
Gi!y Analysts Limited, Pigeon House Road, Ringsend. Dublin 4.
Date of Sempting; 08/11 /SO1 7
Date Sample Received: OBI1 1/2017
#- NAB Accrdltedx U = UKAS Accredited, * =Subcontracted
NOW PV Value Is lhe paramehlc value, faken from European Communities, (Drinking Water) RegukUons, 2014.S.l. No. 122 of 2014 and relates only to drfnklng water samples. Fbr qUBfie& on results, please contact us w.&in twa m k s of the report date to enare that we m accbrnmodale your query as samples cailna he stered Indefinitely. NAG & ATC - No abnormal ohange and ac~eptable to ~uskmtm~. TVC - Tqtal Ibiabte munt Site 0 = hnalysed at City Analysts Dublin. 'Site S = Analysed at City AnaptS Shannon
Page 2 of 2
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T,E. LABORATORIES T I I T E D 7iTading us
TeILab b LoughmartinBusiness Park, TSlow, CQ. Carlow
Phone: 05941 52881 Pax: 059-9152886
CERTIFICATE OF ANALYSIS Page1 of 2
Project Description: I Attention: ll Cornpnny: Address:
Certificate No:
Analysis oFAqueous Gample
Ms. Tracy Watson 142291
IssueDate: 11112~2017 Our Ref: WS-443 62 ll Pr6ject Summary; One sample was analysed for a range of determinands.
Pfease see page 2 for results. T m s & Conditions and methods used are autiined in the Efttaehed appendix.
No. of Pages:
Mr. Pder O'Byrne Quality Manager
Results page 2 plus 4 page a p p m d ~
& Bredr Moors Technical Manager
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Page 2 Qf 2
Determinand
Nitrate a5 N
Tellab 4b Sample ID ES 02
0813 112077
Lab ID 142291
nla 4.56 (note I)
ANALYSIS OF AQUEOUS SAMPLE.
Date Sampled: 09/11/2017 Date Received: 1011 11201 7 Date Analysis Commenced: 08M212017 Our Ref: WS-44362 Certificate No: L/'l7/1906
~.
Nate 1 : LOD raised due to sample matrix interference.
Results expressed as mg/l (ppm) unless stated otherwise
Certificate Of Analysis Job Number: 17-35754 Issue Number: 1 Report Date: 23 November 201 7
Site: Not Applicable PO Number: 4500436720 Date Samples Received: 1 5/1 i /2O17
PIease find attached the results for rhe samples received at our laboratory on 1541 1R017,
Should you have any queries regarding the report or require any further services, we would be happy to discuss your requirements. For additional information about the company please Iog-on to our website at the above address.
Thank you for choosing City Analysts Limited. We look forward to assisting you again.
Authorised By: Authorised bate: 23 November 2017
Sham Reynolds Laboratory Manager
Notes: Resutts relate only to the items teefed. Information an methods of analysis and performance characteristics Is available on request. Any opinions or interpretations indicated are outside the s ~ o p e of our INAB accredltation. Thls teest report shall not be reproduced except in full or with written approval of City Analysts Limited.
The above results relate only to the sample tested This report should not be regenerated except in full and with the consent of T.E. Laboratories Ltd.
T.E. Laboratories
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EPA Export 16-03-2018:03:33:19
Customer Tracy Watson A w a Shannon Pharmaceutical Sevices Shannan Industrial Estate Shannon Glare
IS0 I702
City Analysis Limited, Pipon House Road, Wings;8nd, Dublin 4.
Certificate Of Analysis Job Number; 17-35944 Issue Number: 1 Reporf Date: 28 November 261 7
Site: No1 Applicable PO Number: 4500436720 Date Samples Received; 22/1t120 17
Please find attached the results for the samples received at our laboratory on 2211 1/201?.
Should yau have any queries regarding the report or require any furZher seruice~, we would be happy to discuss your requirements. For additional informath about the company please log-on to our website at the above address.
Thank you for choosing City Anarysts Limited. We look forward to assisting you again.
Authorised By:
Caitlin Quinn Deputy Quality Manager
Authorised Date: 28 November 201 7
Notes:
Rewlts relate only to the Hams tested, lnformaticrn on methods of analysts and performance characteristics is available Any opinions or interpl'etations Indicated are outside the scope of our INAB accreditation. This test report shall hot be reproduced emept In full or with written approval of Glty Analysts Limited.
request,
Page 1 of2 Template: 1146 Ravislon: 016
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EPA Export 16-03-2018:03:33:19
Custorney Tracy Watson
Site I Analysis Par am et er RSi i l t Method Ref. Starl Rate
Project Summary: Ode sample was analyyed for a mgs: o f determinands. please s w page 2 forresults. Terms iEk Conditions and methods used are outlined in the attached appendix.
MO, of Paw:
Mr. Peter O’Bytnc Quality Mwnagcr
Results page 1 plus 4 page appendix
MsBreda Moore Tothnical Manager
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Page 2 ~f 2
Determinand
Nitrate as N
Tellab 4 Sample ID ES 02
2211112017
Lab ID 142699
x* <0,56 (note j)
ANALYSIS OF AQUEOUS SAMPLE.
-
Note I: LOD raised due to sample matrix interference.
Resutts expressed as mgll (ppm) unless stated otherwise
Certificate Of Analysis Job Numbet; 17-363-17 Issue Number: 1
Report Date: 6 December 2017
SZte: Not Applicable PO Number: 4500436720 Date Samples Received: 29J111-2017
Please find attached the results for the samples received at our laboratory on 29/11/2017.
Should you have any queries regarding the report or require any further services, we would be happy to discuss your requirements. Far additional informatton about the company please Iog-on ta our website at the above address.
Thahk you for choosing City Analysts Limited, We Icmk forward fa assisting YQU again.
Authorised By: Authorised Date: 6 December 2017
SRane Reynolds Laboratory Manager
Notes: Results relate only to the items tested. Information on methods of analysis and performance characteristics is available on request. Any aplnlans or inlerpretaffms indicated are outside the scope of our INAB accredltation, This test report shall not be reproduced except In full or with written approval of City Analysts Limited.
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Customer Tracy Watson
Site I Method Ref.
S/S1003#
Certificate Of Analysis
PV Value Analysis Parameter Result unit5 [Drinking
#= INAE Amrediled, U = UKAS Abcredited, ' = Subcontracted
IrlQta: PV Wue is tha paramwk gab@, taken ffum European Communities, (Drinking W-r) Regulallons, POI$. 6.1. No* 122 of 2014 and relab only to drinking water samples. For quaries an w~~lts, plea% conk& us within two weeks of the report date b ensure that we cm accommodate your quam as smpks m n o t be starad tndaflnilaiy. MAC & ATC - No abnnnal change and acceptable hs customers. TVC -Total vlable count Site D = AnalyM at Cify Analysts Dublin. Site S = Analped at City Analysts Shannon
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TelLab 4b
CERTTFICATE QF ANALYSIS Page 1 of 1
Project Description: Analysis afdqtreous Sample
Attention;
COmpRny: Address:
Laughmattin Business Park, Tullow, CO, Carlow Phone: 0594152881 Fax; 0594152886
One sample was analysed for a range of determinands. Please see pa& 2 Far resub. Teum & Conditions and methods used are outlined in the attached appendix.
Results page 2 plus 4 page appendix
Ms 3reda Moorc Technical Manager
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Page 2 of 2
Sample tD
Determinand Lab ID
Nitrate as N **
Tellab db ES 02
29/11/2017
142903
4 . 5 6 (note ?}
ANALYSIS OF AQUEOUS SAMPLE.
Date Sampled: 29/11/2017 Date Received: 04/12/2017 Date Analysis Commenced: 22/12/2017 Our Ref: WS-44494 Certificate No: U1 7/2039
Note 1: LOD raised due to sample matrix interference.
Results expressed as mg/l (ppm) unless stated otherwise