I INC. February 18, 1985 Paula Ausserer Viar and Company Sample Management Office P.O. Box 818 300 North Lee Street Alexandria, VA 22313 Reference: Dioxin Case 3089, Versar Project 868.001 EPA Contract 68-01-6929 Dear Ms. Ausserer; Enclosed is the final dioxin data package for Case 3089 which consisted of twenty foul: soil samples out of Region VI. The samples were received at Versar on 8/21/84. Should you require additional information or have questions, please contact me. Charles W. Carter ____/ M.^^.^Ci^ Organic Laboratory Manager Laboratory Operations Versar, Inc. cc: US EPA EMSL/LV, Data Audit Staff US EPA REGION VI, William Langley 80442 6850 VERSAR CENTER • P.O. BOX 1549 * SPRINGFIELD, VIRGINIA 22151 • TELEPHONE: I703) 750-3000 • TELEX: 901125
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I INC.
February 18, 1985
Paula AussererViar and CompanySample Management OfficeP.O. Box 818300 North Lee StreetAlexandria, VA 22313
Reference: Dioxin Case 3089, Versar Project 868.001EPA Contract 68-01-6929
Dear Ms. Ausserer;Enclosed is the final dioxin data package for Case 3089 which consisted
of twenty foul: soil samples out of Region V I . The samples were received atVersar on 8/21/84.
Should you require additional information or have questions, pleasecontact me.
Charles W. Carter _ _ _ _ /M.^^.^Ci^
Organic Laboratory ManagerLaboratory OperationsVersar, Inc.
cc: US EPA EMSL/LV, Data Audit StaffUS EPA REGION VI, William Langley
804426850 VERSAR CENTER • P.O. BOX 1549 * SPRINGFIELD, VIRGINIA 22151 • TELEPHONE: I703) 750-3000 • TELEX: 901125
USEPA Contract Laboratory ProgramCASE NO: ^ BATCH NO: ]Sample Management Office
P.O. Box 818 Alexandria, Virginia 22313FTS 8-557-2490 703/557-2490 (;LP DIOXIN SHIPMENT RECORD
WHITE—SMO Copy YELLOW—Region Copy PINK—Lab Copy for Return to SMO GOLI>—Lab Copy
»••• INC.
I. NARRATIVECASE 3089, VERSAR PROJECT 868.001EPA CONTRACT 68-01-6929
CMm\o
Enclosed is the data report for Case 3089 for dioxin analysis.Since this was our first case, we had some initial difficulties with
the standard curve and the chromatography checks. Once these were solved, -\the analysis proceeded without difficulty. 0
If you have any questions, feel free to contact me. °
Charles w. CarterOrganic Laboratory ManagerLaboratory OperationsVersar, Inc.
000001
6850 VERSAR CENTER .P.O. BOX 1549 • SPRINGFIELD, VIRGINIA 221S1 • TELEPHONE: I703I 760-3000 • TELEX: 901125
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Sorr.cteil (or contribution by n»tlv« ICDO, 0.»X o( •/« 322 lubtruted., 5 k«: 5/8t
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FORM B-2. INITIAL CALIBRATION SUWARY
Insti,..ID
^CftoHoos'/tap
. ytw; «tC• %CT
yew
^-
^0 (?!.»
4000•iOOO
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sDate Tinie1-"W (A^f)-M-tf /t.;'/7/-/y-fy niiil-/f-lfS /W<-H-» 2c^ti-H-ls^ V-'ct
/-/'/•4T ils'i
'-is-»5 ""«1-lS-^S Ir-lt'-15-» O'01*MS-i-S 134t, l-15-l.i '335 GILS
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301.IDPC^(cc<Ctl
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Peak Area320 322 323
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7fnso %Stf/IOM5 1 3 1 1 1 .fSl1353B3) aTK.yloZ<?!i&>a>31?^3»•iOMxfl A7?iiaool5iss1iiat> t niHO(,2>10730 7? 41530IMSISO UOK130 3(5isltal ill i a a? ""
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111»l5 11'mi31114 ^H3
Heas. Mean HiRF KF
lative Native S>
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Surr. Hesolut'n;•f.S-^
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Solution ID Codes;
PCCC1OC2CC3CC4
, OS^ <
Perfonnance check solutionConcentration calibration solution tl « 0.2 ng/mlConcentration calibration solution »2 « 1.0 no nlConcentration calibration solution •3 m 5.0 ng/talConcentration calibration solution t4 « 20.0 ng/U.Concentration calibration solution »5 » 40.0 ng/telCOMftW f(»/ae- £» Ay 000004
Rev: 5/84
PQRM B-3. CONTINUING CALIBRATION SUMMARY
Instr.ID Date Time
•4WO i-'W K--^ K. ll</il mVI /^l iSf^WW '/32-How 1-15-15 om fc loaa? laifi JIS? 151.^ 3cobz jtios
' fooo 1-15-S5 l-<3l PC. W(,i '21 1 3 3855 i51io SlISM 44713f i--)0a \-1^-&S~,
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' \<it\ ac^b^> a-TSu, i^tesi io55"n isasia/ /^
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Heas. MeanSol. Peak Area (or Height) RF RFID 320 322 323 328'*' 332 334 Native Native
Ft. '\ii-s >i,30» i5S(, io»n SsaolaaMa£ci leaks 13333 fcTjb ^a-ii boiai, i.tiba i.t>^
Heas. Mean TCDDRF RF Isomers
Surr. Surr. Resolut'nE
4^%,a.<»<L. o. n. <».Ty<>0.175 G-lffa lfl.l5>
LT!
O.q 41 0.1 It. "W°0
1,0 Offtt. S',^2,
0.^1,1 0.<ilb 1-W-
0.151 O.m H.O-/.
ID.1'
Solution ID codes;
K:OC1CC2CC3CC4CC5
Perfonnance check solutionOonoentration calibration solution *l « 0.2 ng/mlOoncentration calita-ation solution «2 ' 1.0 ng/mlConcentration calibration solution »3 » 5.0 ng/nlConcentration calibration solution «4 - 20.0 nj/nlConcentration calitaation solution 45 » 40.0 ng/tal 000005
Rev: 5/84
FORM B-4. TCDD DMA REPORT - PARTIAL SCAN OONFIBMATICN
^-^ Response Ratios % Relative AbundancesS^ (relative to m/e 322)No. 320/322 320/324 257/322 257/259 194/196 160 161 194 196 257 259 320 322 324
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LAB 9/2&/64
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003302
00330;
003304
oc^or.(,'033'C'6
C'03307 ' \ .
003305
003305+- 'flo
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FROJECT: B68.0000 CASE: 306? DATE 8/21/&i ACIi;
•'^ATCH; 1 SITE! REGIOh c. I M I T ; RAN
DUE BATES: LAE. 9/20/84 REQUEST 9/2J/6-. CHAIN OF CUSTODY N:.
BATCH COMMENIsRERUN SAMPLES DUE 9-30
PARAMETER
LABSAMPLE
*FIELD SAMPLE
« SAMPLE REM.iiSKS
7971797;797379747975
' ?7A
DP 00333'?
EF &03320
FF 00332i
riF 003322
[.F 0;.332S
:iF 003324
000015
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«
7953
7954
7955
7956
7957
r)795E.
••••'- 7-95;- •
756'..
7961
796;
7963
7964
7965
79A6
7567
796E
7969
7970
0
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COMMENT ••AMPLES DUE
MATRIX
SOIL
SOIL
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SOIL
SOIL
SOIL
SOIL
SOIL
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SOIL
SOIL
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868.01
9/2u/84
9-30
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PARAMETER RE&UEST SHEET ?A6E 2-
PROJECT: 86B.OOOO CASE! 3089 DATE 8/21/64 AC&: CARTE?>
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DUE I'ATES! LAP- 9/20/84 REQUEST 9/£&/S-i CHAIN OF CUS'iaDi N:.
BATCH COMMENTSRERUN SAMPLES DUE 9-30
PARAMETEK
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7971
7?7;
7973
7974
7975
976
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INITIAL CAUBHAIIOM - PAGE 1
CHMMATOOUFm CHECK
Criteria
PC SolutionFile • tata/Ti—
375-i I/^/S'Tl '/f.-/f
37-70 ' ( 1 5 ( 2 5
01((
377 7 '('5^5
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334
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INITIAL CM.IBRM10N - PACE I
CHRDNMOGRNW CHECK
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PC SolutionFile* Oite/Tlir
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^ L 9 S 00HtDMASS CHROHATOGRAH DATAl 3736 *1 SCANS 958 TO 1286 0ei/H/ss isi49iw ca-ii 373114 ^SAMPLEl CCUJUN PERFORMANCE CHECK 1-939 2 UL 4808 JK/BO 0COHDS.l G«n SP2338 79/4>2eetl5>24864 0RflNGEl G 1,138(1 LABEL) H 2-J9.B MMHl fl 0. 1.8 J 8 BASE) U 20, 3 0
iee.e-i Ik-—— a,0',''''3-'1''-00 e3G1
r ~^ - ^^7.«ye /^ ' f,S41B15 1 fl '
I T329 . | 319.396323 J | , 322.S9E
: 1146ft
I ft ..,^^AAi _^y——p, / V 7 L..^-,-r.^.n.f|i.^^-A.^ . •^-^^-"j .^^-yJ/V--^-
9S8 ieee iese nee use izee SCAN23l47 25:93 26(18 27:33 28:48 38(83 TIHE
0 0 0
6 L 9 S 0 0MOVES CHRCHATOGRA11 DATAl 3756 11 SCANS 1888 TO 1868 '081/14/83 15t49)» CALIi 3731 14 0SAMPLEl COLUMN PERFORMANCE CHECK 1-833 2 UL 4888 JK/BO 0COHDS.I 6811 SP2338 78/4>288»15>24884 0RAHGEl G 1.1309 LABEL! H 2,18.8 OUAHiA 2. 2.8 J 8 BASEi U 28, 3
18253761.
188.8-, 15594.-1^- 154^ ^
n n ^ -.. ( ' - -\ i<i~ -,.v -^
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! 328 . / I 328.998t 8.589
_/' . / ' . ^^ '~ts^__^_ l s^^^ —' ^s^ _rf^^-w- —•^^^
1888 1818 1020 1030 1848 1859 1869 SCAN25103 25)18 25)33 25)48 26)83 26)18 26i33 Tilt( ^ • ")1. •^ •—'
£ /- 9 5 0 0HIDtttSS CHRWBTOGIWtS OATAl 3756 tl SCflHS 1080 TO 1068 N
91/14/8S 15«9:99 CALI: 3751 *4 "-SttfLEl COLUMN PERFOHMNCE CHECK 1-039 2 UL 4880 JK/BO ~CONDS.t Een SP2339 78/4>2BM1S>24«4 0RANGE: G l<138e LABELl H 2.18.0 QUWl A 2, 2.9 J B BASE! U 26- 3 0
19248871.
75.9-1 "y8' 8888.
332 / 1 " ^OOZQ 332.999f l ± 9.599
— — — — 1924 —
11691., 1BB.9-1 l32' 11G95.
334 / I 334.199; " 1 1 t 9.5W
1999 1919 1929 1939 1948 1959 1969 SCAH23163 25ll8 25:33 25:48 26:93 26(18 26(33 TIME
I, 0 .:)
MOHflSS CHROMftTOCRflHS DATA: 3756 tl SCAMS 1000 TO 1868 w
01/14/85 i5»49«ee CALI: 3751 M oSAMPLE: COLUMN PERFOmCE CHECK 1-833 2 UL 4880 JK/BO 0COOS. I EOl SP23» 79/4>2fle»15>24W4 0RAHGEl G 1,1308 UBELl H 2,18.9 OWN! ft 2, 2.6 J 0 BASEl U 20, 3 -0
10261510.
43.9-, w49- 1035 1578.
1015 /\ ^•.1067. / \ f\
A / \ /\ h^
237 / \ / V \ 257.877
: , ALLV. , "'^. ,_^~_. ^L^—^-——"——^^^_ ^ ;r 1026
3487.100 0-, 'i?89- "•' ^ ' 3592. !
/ I 1035 '1815 / 1 26M- ;2396. / 1 "i132- A I96". / 1 A / \ !
322 / \ I \ I Y \ 322.896 i: /\j\J\\ ' " ' .1000 1019 1820 1838 1048 1BS8 1860 SCAN25103 25118 25:33 25:48 26103 26:18 26;33 TIME
C 0 0 ;
0 0 5 6 7 4
MIDMASS CHROIATOGRAffi DATA! 3756 *1 SCANS 1800 TO 1060 '?'81/14/85 15l49!8a CftLl! 3751 114 ?1
SAHPLEl COLUMN PERFOWMCE CHECK 1-033 2 UL 4800 JK/BO —CONOS.I 6m SP2338 79/4>29W15> 24884 5RANGE: G 1,1388 UBELt H 2,19.9 QUAN: A 2, 2.8 J 8 BASEl U 28, 3 .A
18252728.
77 l 1815 "?1. 1835 ,,CB \"•'n 2137. r\ 2183. 2'~• )
A / \ 18217. .
320 . / \ / '/ \ 328.896• , ./ V i \ •"";ie2G3487.
198.8-1 1015 t 89- ^ 3592.
: / \ ^ /\322. / \ / \ / V' \ 322.896- Ay V T \
1825 /
497.14.4-1 1821' S1B
323. /^ j \ / \ / \ 323•e9?'
1880 1010 1820 1830 1048 1058 1060 SCAN25(83 25:18 25f33 25:48 26:03 26:18 26:33 TIIC
C 0 00 0 5 6 7 5
9 I- 9 ? 0 0HIOmSS CHROIMTOGRWIS DATA: 3756 tt SCANS 959 TO 1180 „,91/14/85 15:43108 CflLIl 3751 •4 w
SMPLEl COLUMN PERFORMANCE CHECK 1-633 2 UL 4000 JK/BO ^CONDS.I Cfll SP2330 79/4>29e»15>249*4 ~RflNGEl G 1.1386 UflELl H 2.10.8 CUftHi A 2, 2.0 J 0 BrtSEl U 28, 3 Q
0— , IBIS • 1935"""] 2137. h 2148. 2'68-
8793. / 1 lfl56S.
329. i\ \\ i \ \ 329.996
, 1949190.0-1 IBIS n. 2939. 3592.
2436. I I i 13177.
322 . A I I I Y I 322.99G
»-«-1 1915 f. le3s »8-339- 1\ l%1935. I 1 lw3.
323. A AA 3a-897
- .,.... . _.AML,....^.''""^^^v^^^^r-^ ^ tf ii.i i*- i -——~'> > ' ' 1 ~^^ .__J-^|^^<^ -->\JS^^.-^^^A
969 989 1990 1929 1049 I960 19B9 1190 SCM24l92 24l33 25:03 25:33 26:93 26t33 27:93 27:33 TIME
( 0 l:'
L L 9 5 0 0M1UMSS CMROtWrOGRftMS DATA: 3756 tl SCANS 958 TO 1100 COBl/14/85 15l49i88 CALIi 3751 *4 CMSAHPLEl COLUMH PERFORMANCE OECK 1-033 2 UL 4888 JK/BO 0COHOS.I 601 SP2338 7B/4>2eeB15>248(4 0RANGEl G 1.138B LAEELl N 2,18.8 WMl A 2, 2.8 J 8 BASEl U 28, 3 0
1825 03772.
32.5-1 1E198• 3796.
328 J | 328.898J I t 8.588
——— —— - ^ r ^ ' '"— "" ~—
8888.75.9-, 3OT7- 8888.
332 | I 332.999I 1 i 8.388
- ,— - - — _ _ - ^^ — — r . — , — —
; 11696.188.8-1 m7e- 11696.
: 334 1 \ 334.188I I i 8.588
SEE / I 187957. I \ 78.
_^_233. _ _ ^ _^ _^_ / V • | __..___^__.__l*3•__„_968 988 1888 1828 1848 18G8 1088 1188 SCAH
24:82 24)33 25)83 25)33 26:83 26:33 27:83 27(33 TIME
(•• 0 0
8 L 9 S 00NIDHASS CHROHATOGRM DATAl 3776 tl SCANS 959 TO 1299 r*91/15/85 Sllliee CALIl 37E9 *9 w
SlWLEl CCLUMH PERFORMflNCE OCCK 1-939 2UL 4809 JK —CONDS.i 601 SPSOS 7e/4>2«MIS>24(M4 nRflNGEi cieee,iB4e U«ELI H 2, 4.e BUAN! A e, i.e J e BASE! u a, 3 o
iee.e-i l¥l 5984.1<-7
'-— 3,3,~i,'i Td-raP'
1605
jll clil_r,co. ny,1 '5l/
328 . 319.S96324 323.S97
.1., j.^Av^^vM^^y/ » 1 \A^W^^VV^ T^^J V^W'Wy^rtft^^
350 1909 1859 1180 1150 1208 SCAN23l47 25lB3 26:18 27:33 28:48 38:83 TIME
C " 0 0
6 L 9 5 0 0HIDHASS CHROmTOGRAMS DATA: 3779 tl SCMS 359 TO 1188 mBl/15/83 SllllM CALIf 3769 t3 CMSMPLEl COLUm fEWWSWVX. CHECK 1-839 2UL 4888 JK 0CONOS.l 6W SP2338 78/4>2ee»15>248*4 0RANGE) G 1,1308 LABEL) N 2.1B.B QUWl A 2> 2.9 J 0 BASEl U 29, 3 0
1921 03133
3^ 13752- . - IM. .3^3 3176.
s\ ir. y^-0^- .0.^3328 1 1 l,«4b1*o i 328.836
I i t fl SM/ I ••IT/, C»/ii,fcio i how- nii ,
, - / \ tF «( ff. fX.
'\y"w« - /*- ^_ - 'S -J - hri >• .•' u ' J ——^*^-f—— - ~- — -T- - - ~_ • ^LCUUC" " ^ "* '
16206796.
79.4-i 3e?62' 6832.
; - A ^^. O.T8
332. ^"'mi,7 / ^^ ,3M.eM~—VH I 1 * 8.588
, j ' ' ' .828 rn •" '8686.
188.8-1 ^ays• 8688.
' 3 3 4 f \ 334.188I I t 8.588
968 988 1888 1828 1048 1668 1888 1188 SCAN24f82 24:33 25i83 25:33 26.83 26>33 27:83 27:33 TIME
( • 0 0
0 G 9 ? 0 0
HIOHASS CHROMftTOGfMMS DATA) 377B «1 SCAMS 968 TO 1960 _Bl/15/85 9lllt88 CALll 3769 «3 <"SAHPLEl COLtm PERFORfWCE OECK 1-039 2UL 4809 JK M
COHDS.I EM SP2338 70/4>288*l5>248*4 °RMttEl GIBM.lftU LWal N 2, 2.0 BUAHl A 1< 4.6 J 0 BASE: U 2B, 3 §
1821 g. 1835
77.2n 1811 le^- I924- 2328.1679. n 817B. "'"'•723B. / \ /-\ A
328. A / \ / Y \ ^^°0^ 328.896/ \ \ / \ 335 * 8.S88
: ^•^-o,^"t"188.8-1 1811 12!41- ^a. 3816.
2119- A 18457. '9669. / \ A A
A / \ /Y\/ \ / \ / \ .s95— • ° l1 * e•5Be
^_ \/_v_J_^."'. 1821
•»"% 183822.5-1 1811 W"' 488. • 679.
394. / \ 2833. A: - T' / \ A /l
323 /\ / \ / \/ 1 323.897: ^^^^A^vl ^ '""988 998 1888 1818 1828 1838 1048 1858 1868 SCAN
24:33 24:48 23(83 25:18 25l33 25:48 26l83 26:18 26(33 T11C
( 0 0
t- 9 9 S 0 0MDMftSS CHROMATOGRflH DATAt 3777 *1 SCANS 989 TO 1200 0ei/15/65 14131:08 CflLi! 3769 •9 MSflWLEl COLUMN PEKFOBMNCE CHECK 1-039 2UL 4080 JK 0COHOS.l E8H SP2338 79/4>28e»lS>24884 0RflNGEl G 1.1288 LABELl N 2. 4.8 eWNi.P 9, 1.8 J 8 BASEl U 28< 3 0
.88.8. J^a,^,^00 0 7984-
: T ' -1 ' c—————• * im ^ •M'/.
^ " 1814 • |
: "r: 328 A 319.S95: 324 323.337
! "f
1 TA I \ I A"
rV^ lv^AM^ .J j r V^v^^A^ '- ' y^W L^A/Vyy.988 958 1888 1859 1100 1158 1208 SCAN
22l32 23(47 25)83 28:18 27:33 28:48 38)83 TinE
C 0 0
6 f: 9 'S 0 0
MIOHASS CHROHATOGRAMS DATA: 3777 11 SCANS 950 TO 1188 _: ei/15/85 i4i3iiae CALI: 3759 is ' •SAMPLEl COLUMN PERFORMANCE CHECK 1-839 2UL 4000 JK QCOTOS.l 601 SP2338 79/4>2eM15>24Bt4 5RANGEl G 1,1200 LffiELl H 2.10.B QUAHl A 2, 2.8 J 8 BASE) U 26, 3 0
1824 0: 31.Sn {^•.-.^,5^. ^
/I ^^ • '^-lu^-..o.-s
I I J Sl^in * o »328 - / I K r - o . ' \ - i s ^F.ofn. i :
I l k,. 1 1 . r^cii^w^^^^^^f^^-.^——^.——r^^-,^,,^ •^ •^-^^•^~^—^A^-^——.^^-^\^.^-^-r, - - -
10238224.
; 76.7-1 ^P4' 8224. ;^a- - 0 . 2 3 A ^ _ '\^ ^^asM- ° °"
332 ' I \ 332.B99 ,/ 1 1 B.SW
1823: 18647. '
198.8-1 4<?13' 18728. i
334 I 334.188 ': A968 988 1898 1829 1848 1860 1888 1188 SCAN
24:82 24l33 25l83 2Sl33 26i83 26:33 27:93 27l33 TIME
C 0 0
£ 9 9 S 0 0i ku: HIOHASS CHROHATOOWHS DATAl 3777 tl SCAMS 388 TO 1088 2
81/IS/8S 14l31l88 CALIl 3763 •3 . °SMTLEl COUJMM PERPORWiMCE CHECK 1-033 2UL 4800 JK °COOS. I 68H SP2338 78/4>2Batl5>24B«4 —RANGEl Gl«2e,ie38 LABELl H 2,10.0 OUWl fl 1, 4.0 J 0 BASE) I) 29, 3 ———————
1025; 3178.
80.8-1 l3968' 3224.
320 . A / \ /V \ 32e'996
1025
1«.0-, s30- - 0.^ •. ". ^ ^ ^39S> / I
322. A / \ /V\ ^a•B96; \ . - ^ - /WiV l"1024888.
"•^ za-^ IT' 9t3-^E -- -o.ib /I33.3 / A .
323 . A / 1 /\ / \ 323.037 i
f\\/\.^^^^-^A^\ A—7 V/>1^- V V^\/\/^-/\^^^^/V^\ \980 1000 1020 1840 lOEB 1080 SCAN
24833 23:03 2Sl33 28:83 26:33 27:03 TIME
( - 0 0
17 ?; 9 5 0 0HIOUSS CHROMTOCRAM DATA* 3788 «1 SCANS 358 TO 1290 _81/15/eS 22l29l88 CALIl 3769 *9 w
SAMPLE) COLUHH PEFORWNCe CHECK 1-618 2UL CME(3089 4998 UY n
CONDS.I 601 SP233e70'4>2ee«lS>24W4 - 0
RAHGEl G 1,1200 lfBB.1 H i.lO.OIMMIl A 0, 1.0 J 0 BASEl U 29, 3 5
""•i iL^^-^00 w2-
: IBS? <:L1__ / "0 - 1 1 ">'•
- I I '"T •; I320. | 319.596
323 N ^ 322.B96
: • I T" V Au\ ' \1\ L.IJ \.J 1 i \ I \J ^N/ \^^^950 1000 1030 1100 1150 1200 SCAM
23)47 23)03 26)18 27l33 28)48 30)83 TIW
C 0 0
G 8 9 5 0 0HIDHASS CHROHATOGRAMS DATAl 3788 «1 SCANS 1888 TO 1188 —81/1S/CS 22123188__ CALK 3769 *9 (5
i SttPLEl COLUMN PEFCRMWCE CHECK 1-816 2U. CASE*38e9 4888 W 0COOS. l 68H SP2338 7B/4>2eB«15>24»4 0
: RANGEl G 1.1288 100.1 H 2.18.8 WHt A 1, 8.8 J 8 BASEl U 28> 3 01841 0
31.1-, ^.-^.'S^3 ^
] A ^ e!!"-*-05 -/ \ ^5^0'1 1 nr * 8.S88/ \ ^F.O.Uz. _/ \ (-OT. O.yi l;; fmw 1{F
184823868.
i JWflf
• 75.4-1 -•y— 24992.H 2 •: 335^5%
332 ( \ 332.899A "1848
31722.188.8-1 128642. gg^
334 \ 334.188/ I i 8.S88
1888 1828 1848 1868 1888 1188 SOW25i83 2Sl33 26(83 26l33 27i93 27l33 TIME
- C 0 0
9 b 9 S 0 0HIBttSS CHROMATOGRAH OATfll 3788 *1 SCANS IW TO 1199 S
; B1/1S/85 22l29lW__ CflLIl 3769 « 0SAMPLEl COLUMH PEFCRMflHCE CHECK M18 2UL CflSEt3989 4800 W 0CONDS.l 6811 SP2330 78/4>2eetl5>24M4 <-3
] RAHCEl G 1.12M UtBELl H 2,19.9 WM^t,A l'2e•e J e wx1 U 20, 3
'' leSsso' o.r/.-" w?188.8-1 "'i88- qi-y. 29696.
| lo98oi: | 111659.
1831 | 113785. | [ I
• 322 - / I / U \ 322-"6
: I 1 I I \ I * e•see
'; !—-^—V—^^\ T
: 1980 1829 1948 1968 1888 1108 SOW25163 25133 26(83 26:33 27lB3 27l33 TIME
(.. 0 -J
/- R 9 S 0 0MIDMftSS CHROMATOGRAH DATA) 3788 tl SCANS 1880 TO 1188 "?
: 81/15/85 22i29iW CTLIl 3769 IS. Q; SflWLEl COLUtM PEFORMAHCE CtCCK 1-818 2UL CflSE«3e83 4908 VY 0
CCTOS.I G8M SP2338 78/4>2e8(l!>248(4 0; RflNGEl G 1.1288 LABELl N 2.18.8 WtHiA 1 ' 8.8 J 8 BASEt U 28, 3 0
16E88.199.8-1 '"I156- 18888.
\ I IB5711859.
1931 ^•11566. , f\S9288. X U
328. / / U 328.89E
' I V * e•58B
1^ . ^1880 1828 1848 1868 1888 1180 SCAN25i83 25(33 2Gl83 26t33 27i83 27)33 TIME
C' 0 0
9 9 9 5 0 0 ' •i~
HIOHA5S CtfiOMATOGRAM OATAi 3788 «1 SCANS 1988 TO 1100 MBl/15/83 22l29lM CALIl 3769 t3 °
: SMfLEl CO.UMM PEFOIWNCE CHECK I-fll9 2UL CASEt3B83 4800 W 0CCTBS.l 60) SP233B 7B/4>28M15>24M4 0
RAHXl G 1<12B8 LABEL) H 2,10.0 OlMHl ft 1> 8.0 J 9 BASEl U 28, 3 —'i. 2S43.
189.6-1 12?2- 3524.1\ 1858I 2133.
1B31 \ ( \1384. 1444fl [ J I
323 . J I I 1 ' j \ 323.897
^/^-\J^\./ __ ^ __ ^ \/V^ \1888 1828 1848 1BG8 1888 1188 SCAN2Sl03 25l33 26)83 26133 27103 27l33 TIIE
C 0 0
6 9 9 5 0 0'K IQ> (0
MIDMRSS OfiOMATOGfWH DATAl 3807 tl SOWS 989 TO 1958 rtBl/17/84- 12l23iee CALK 3886 t3 0SMTLEl COLUMN PERFORMANCE CHECK 1-039 2UL 4000 SEP/JK 0COWS. l 601 SP2330 78/2>219t20>240»6 0RAHGEl G 1,1200 LABELl H 2,10.0 OUANi ft .2, 2.8 J 0 BASE) U 20, 3 0
4514.100.9. "F. ^ 4S28.
,. ^——^\l<fS»~. 4038.TC-C^ 18369.
3, ^ I958 _^ to^K- ^ 7-<¥',///3448. Y ' n— I CaYa//^
n"' ^ -=^A ^A—
320. 319.596' 323 322.S96
988 920 940 968 988 1880 1828 1B4« SCAN22l33 23l03 23l33 24lB3 24l33 23lB3 25:33 26l83 TIME
C 0 0
0 '6 9 S 0 0MIOIWfiS'CHROMTOCRAMS DATA) 3807 (1 SCANS 349 TO 1820 oei/17-<4 12)23)88 CALIl 3886 (3 -tSWLEl OXJUfM PERFORMANCE CHECK 1-839 2UL 4888 SEP/JK 0CONDS.I EW SP2338 78/2>218128>248« 0RAHGEl G 1,1200 LflBELl H 2,18.0 WMl fl 2, 2.9 J 8 BASEl U 29, 3 0
369 0194G.7G•91 S5- ^ l%- ^978- / \ 6878. / \
328 / \ / \ / T \ 328.896: / V / V I V' ' ' 969 ' ' ' ' '
2S1E.188.8. .»> 11?91.» 0^979 /£" 2548. I
<%4: A ^:^ ^°,^S>(
322 /\ / \ /V \ 32'2' •"6\ A /v rv . ••" i968 4 .
"•S-l 31. l '. T" 323 , w3-
X A A A "fe '4323. A / \ ^V \ 323•()971.^.A./\/i\^^_./^
948 958 968 978 988 938 1088 1818 1828 SCAN23)33 23)48 24)83 24)18 24)33 24)48 23)83 25)18 25)33 TIME
; C1' 0 0
I. 6 9 S 0 0•!=> W Q
HtOttSS CHROMATOGRANS DATAl 3887 *1 SCANS 906 TO 1050 «!91/17/84 12l23l8e CALIl 3806 t3 0S<WLEl COLUMH PERFORWiHCE CHECK 1-633 2UL 4888 SEP/JK 0CONDS.I SW SP2338 79/2>2iat29>248»6 . 0RAHGEl G 1,1288 UflELl H 2,19.8 OMHl A 2, 2.8 J 8 BftSEl U 28. 3 0
9692311.
33.1-1 l8938.-/^-/^?7 2332.
/ \ tos"j7 o,r328 . / \ - 7^7 " zTT ' 0•<?4' 32B.898
/ I 1 0 ^ g g^
S6BS4S1.
76.8-1 25?83- 5464.
332 / I 77'Z 332.899I \ t 8.588 ;
9687182.
'"•1 T ^-wf334 I I 334.188
I 1 t 8.388
988 928 948 968 988 1888 1828 1848 SCAN22l33 23l83 23l33 24l83 24l33 25(83 25:33 26:83 TIME
C. 1 0 0
6 6 9 ? 0 0MIOMflSS CHROHATOCRAH DATA) 3815 11 SCTNS 1980 TO 1280 _
: 81/17/85 28(26(88 CflLll 3769 t9 "•SMFLEl CTLUMH PERFOMIMKE CHECK 1-839 2UL MSE13883 4806 W ^COOS.l 68M SP2338 76^>218t28> 24886 0RAHGEt G 1.12M. LABELl N 8, 4.8 OUAHl A 8. 1.8 J 8 BASE) U 28, 3 0
188.8-1 'T";) •>,,I|I-T^OD 0 8144.
p^ ^•-/^
1849^ t rt328 . |( 319.S96324 J 323.SS7
L | 1162
^ v i ^\ ^J i ^-^-LJ \^^ k^LA1888 1838 1188 1158 1288 SCAN25(83 26119 27l33 28(48 38(84 TIME
(. /:\• 0
£ 6 9 ^ 0 0MIDHASS CHMmOGRlWS DATA: 3815 tl SCANS 95B TO 1108 CM81/17/85 28l26lW CflLli 3763 t3 <3<SfWLEl CCUJMH PERFORfttNCE CHECK 1-839 2UL CASE13889 4008 W 0COtOS.I E8H SP233B 7B/»218»2B>24et6 0RAHGEl 01039,1833 LABELl H 2,10.8 QlMHl A 2, 2.0 J B BASEi U 201 3 0
1034 02959.
78.9-1 "t84- 2964.
J^-sc.si A A A»: ^ A \ N\• _.. . ^ / V V i \ .
1934l q > o-Vft-- '"•iee.e-i "T-" 3756.
322 M / \ /V I 322.B96: „ A/VIv ""1034888.
22•4-| 3^.0.^ T' 8<()-
„: " A M; - /l/V I/^f~^^\/^\/^\^^/^\^^^/\J^f\/^\^^f 1 ' ^ A^/vs/^^^^v^^^^^V^^A^^see 988 isee 1820 1848 leee tesa nw SCAN
24(83 24l33 25l83 25t33 26;B3 2€!33 27:B3 27l33 TIME
• (.; 0 U
^ 69 c. 00maWS CHROMTOGRAMS OATfll 3815 *1 SCANS 950 TO 1100 ^01/17/85 28l2El88 CflLIl 3769 *9 0SAMPLE) COLUM PERFCIWlHCE CHECK 1-039 2UL CASE»3889 4888 W 0COtCS.l Vm SP2336 TW>nW«t>WSK 0RANGEl G 1,1288 LABELl H 2,18.0 QUAHl A 2, 2.8 J 0 BASEl U 28, 3 0
18343SB7.
38.8-, 16284.-/.-^" ^
328 I \ 328.898I I t 8.S88
1832852E.
74.3-1 39fl73• 8592.S2-'. o.if \\ sss £: fo^i'/3^ J I Jl»
332 / 1 332.899I \ t 9.S89
1832! 11517. . _ i / •}
188.8. ^1- - '
n : 0,g97334 I | 334.189
\ s.m f/'O ± B•'iM
968 988 1888 1828 1848 1868 1888 1188 SCAN24t83 24l33 25l83 25:33 26i83 26i33 27l93 27l33 Tilt
(/ 0 0
S 6 9 S 0 0HIOMASS CHRWATOGRAH DATA) 3836 (1 SCANS 950 TO 1200 ^61/21/85 15ll9lBe CALIl SCAN «3 °SAWLEl COLUm PERFOWtWCE CHECK 1-039 2UL 4998 JK §COWS.l 601 SP2338 7e/2>2iet28> 24996 CTRANGEl G 1.1286 LABELiM 9, 4.8 QUANi A 9, l.fl J 9 BASE) U 29, 3 • w
iae.B-1 "|16 _,-, S224.I ICfn, . q, -(-OO'OI «. ?>^1'
' I •<' if\- ft -<—*'°o =- ^AS'rs^&f
^ T'T II
- I I320 319.396
. 323 322.596
; 1139, " J
^L.J. g3 I..-,' *'""" 'T-T' 6--1 ' L'^J, ^-^"-l-' .^i^T-"63-!.^1^...
. 950 leee lese nee use • 1288 SCAN23(48 25183 26ll8 27|33 29:48 38l94 TIMEr • (T) n•^ •^/
9 6 9 5 0 0v^
MIDMASS CHRattTOGRflHS DATA: 3836 11015 SCANS 1608 TO 1940 S"61/21/65 ISllSlU CALIt SCAN t3 °SAMPLE) CM.UMN PERFORMANCE CHECK I-B39 2UL 4668 JK §CONDS.I 6BM SP2339 7e/2>21W2B>248K §RAHGEl G 1.12ee LffiELl H 2,10.0 QUAHl A 2, 2.0 J 0 BASE) U 29, 3
1B1E2343. .„-.QAWJl Jffv i-0'rfl
B2.8-, 1806 -T'8- "26 1892. 2396.17B6. / \ U26- 7634.
A / \ 0.63^ /829- /^\319 / \ / ^T \ 318.59S321 / \ / I \ 329.S96
1816283e" 1931
iee.e-, 1996 llce- "|5 2339. 2892.tOAo / \ /r\ i'y~^ ^B-ro* 9444.
A1948. / \ 0.10 99^ 9^
321 . / \ I / '1 \ 329.596323 / \ \ / | \ 322.596
'1916 ' 7 ' i i . - -
: 381. /iq q_ 1177. / AAJ.
^ / una -1"''/ \ / / HMO! _ / \ a 248-323 . / \ ,, /^\ 323.BS7
/\ / \ /A^ \
ieee lees 1910 IBIS 1029 i92S 1030 1935 iB4a SCAN25t93 2Slll 25ll8 25:26 23(33 25:41 25l48 25;56 26:03 TirE
( . 0 O
2 - 6 9 5 0 0MIDMflSS CHROmTOGRMIS DATA) 3836 11015 SCANS 1888 TO 1040 ^81/21/8513)13)88 CflLIl SOW •3 0SfWLEl COUJW FEKFORHAMX CHECK 1-833 2UL 4088 JK 0coos. i em smw n^>2iwns>uws oRAKXl G 1.128B LKELl N 2,18.9 OMHl A 2< 2.8 J 8 BASEl U 28, 3 0
18162835.
34.B-1 12P4.-^ - . ^
A -^-"^^327 / \ 32G.S36329 / \ 328.S98
-r- 18155446.
: 78.8-1 26M1' 64S6.
331 . / \ 338.339333 / \ 332.339
18138184.
lBe•e] /T ^o7333 / \ 332.688335 ' / V 334.688
1888 1885 1818 1815 1828 1825 1038 1835 1848 SCAN25)83 23)11 25)18 25i26 25:33 25:41 25:48 25)56 26)83 TIME
<' 0 0
8 6 9 5 0 0HIDHASS CHROMTOGRAHS DATA) 383S »1915 ' SCANS IBM TO 1040 Tr
Bl/21/85 15119)88 CALIl SCAN «3 °SAMPLEl COLUMN PERFORNWCE CHECK 1-833 2UL 4080 JK °COH1S. l 601 SP2338 78/2>218(28>248»6 °RAHGEl G 1,1288 LABEL) H 2,18.8 aJAHl A 2, 2.0 J 8 BflSEl U 28, 3
121S.
0-3-1 4^' ' / 1825 12S2.
/ ^ 0.4> ^ •.
256. / \ / \ / Y-7 \ 255.577258 / \ / \ / \ S?•V77
' ' ' ' " 'tei6 ' 1 - 1 ' ' 1 • • • - » -2838.
188.8-1 "I36' 1831 2892./\ 1B25 2338.
1806 / \ 2B96- 9444'
321 . / \ / \ / \/ \ 328.596. 323 / \ / \ / \ 322-596
1888 1885 1818 1815 1828 1825 1038 1835 1848 SCAN25l83 25lll 25118 25i26 25i33 25841 25l48 25!56 26(83 TinE
0 0
6 6 9 S 0 0HIDHASS CHROHATOGMM DATAl 3844 *1 SCflHS 959 TO 1280 2ei/21/85 23l2SlW CftLIl SCAN t3 QSAMPLEl TCCO COUDM PERFORMMCE CHECK 1-039 2UL CASE13889 4080 Vf 0COWS. l KBM SP233B 7B/2>21B(29>249»6 0lUMGEi G 1.1290 LAGELl N 9, 4.0 QUAHl A 9. 1.0 J 0 BftSEl 1) 29, 3 o
4nQ n_. 1914 0001'•""•'I j-t—3,1,,-t^, TLDR> '"""•
JU-——^—— /yr-"-'
1 J^--'/^T ^ -^
" I; 328 . | 313.S96323 322.396
; 1137i A
^^SL^JSU v r L^sgi sg—I w&^J L ' ^L^950 ieee 1050 nee use izee SCAN
23)48 25l93 26:18 27:33 28(48 30(94 TIME
(, 0 0
0 0 L S 0 0MIDMASS CHROHATOGRAHS DATAl 3844 tIBO? SCANS 1888 TO 1030 ^01/21/85 23l25l8e CALIl SCflH •3 0SWl£l TCOO COLUHN PHa-ORMWCE CtCCK 1-839 2UL 01SE»3e89 4990 UY 0COOS. l 501 SP2339 7e/2>21W2e> 24096 0RAHCEl G 1,1290 LfflELt H 2,19.9 QUAN) A 1, 3.8 J 8 BftSEl U 29, 3 0
18141837. -It W37 ®
35.4-1 8499.-M' ^tfe. ^g_
328 . / '\ 328.898
18124113.
76.4-1 18612_ ^3g_
; - / \ ^ '• ^^'703332 / \ 332.099
/ \ ± 8.598
18125413.
188.8-, 24898, 353/ .-O.-f-7 "'S-; / \ ''W
i 334 / \ 334.188/ \ * 8.588
1898 1985 1818 1815 1020 1825 1930 SCAH25803 25lll 25!l8 25:26 25l33 25l41 25l48 T11Cf: 0 0
\r 0 /- S 0 0
MIttWSS CHROMflTOGRflMS DATA) 3844 *1887 SCANS 360 TO 1089ei/21/95 23l25l98 CALtl SCAN t3 0
; SWLEi TCOO COLUMN PERFORMANCE CHECK 1-039 2UL CflSE»3889 4000 W 10CONDS.I 601 SP2338 70/2>2ie628> 24886 0RANGEl 01818,1820 LABELl H 2,10.9 OMHl A 2, 2.0 J 0 BASEl U 29, 3 0
1814 01538. °
79.2-1 ^P8' 1594.
A A M 3^°/^•0"329 . / \ S \ / ' \ 329.696
1\1\1 \19141948.
loo o- 8813.- 0.1^ s ^3 wiiIIW.U^ A A K » ZBlA./i 3^ 3/ - u. 10
A A M322 / \ I I I V \ 322.0961 A/Ay \1814
13.5-1 211. 1 272.
323 n / \ | 1 / I 323."97I \ / \ I v \ * B•sw
^<^: <^<i -i' -r \^~^—'• - ^^^^T^y^V^^-^^^368 980 1888 1828 1848 1868 1888 SCflH
24l83 24l33 23(83 25l33 26lB3 26)33 27(83 TIHE
C 0 •J
2 0 L S 0 0
IBB.B-i
313324 '
X22
HIDHASS CHROMATOGRAII OATAl 3848 tl SCANS 990 TO 1288 S91/22/8S 12:34:88 CALl! 3845 «6 oSAMPLEl COLUMN PERFORHME CHECK 1-039 2UL 4008 JK 0COHDS.I 601 SP233B 78/2>219»29> 248(6 0RANGEl G 1,1209 LAGELl H 2,19.9 OUlWi A 9, 1.8 J 8 BASEl U 28, 3
T 4736.
^\ 1.4 -f^'00-^
999
921
ee sse leee133 23:48 25:93
1
|
( 1893
'
1850 1189 1158 1288 SCAN26:18 27:33 28:48 38:84 TIME
318.593323.597
1 1
L—i
31
0
£ 0 L 5 00MIDMflSS CHROWTOGRW DATA) 3848 tl SCANS 33B TO 1040 KB1/22/8S 12l34l88 CALtl 3845 *6 0SMPLEl COUMI POfWWtW. CHECK 1-839 2UL W» JK 0CONDS.l 601 SP2338 7e/2>21W28>24B86 0RAHGEl G 1-1208 LABELl H 2,18.8 OWNt A 2> 8.8 J 8 BASEl U 28, 3 '=>
18892396.
: 188.8. y- - --'00^ 2484.
/ RJ'-O.^I
; 328 I I 328.898f \ t 8.588
998 1888 1B18 1828 1838 1848 SCAN24l48 25:63 25ll8 25:33 23:48 26(83 TIME
C 0 •J'
t7 0 /. ^ 0 0mawss wMiwma««s OATAI 3848 *i SCAMS see TO 1100 ^Bl/22/83 12l34lBe CALIl 3845 K °SAMPLE) COLUM FERFORfWC CHECK 1-833 2UL 4888 JK 0
COWS. l 681 SP2338 76^>218«8>248(e 0
RANGE) G l<128e LABELl H 2,18.8 QUAHl A t, 4.8 J O BASEi U 29, 3 —1B885468.
79.1n 22?16- 5472. :
^ ; ?3lSO
332 | 332.839
11> 1888 :
6917.188.8-1 29?64' 6928. !
1 - ^-"s ft I'. {
I: 334 334.188 '
t 8.588 ;; [: L _„_______ ./I II 988 958 1888 1859 1188 SCAN :
22:33 23l48 25:83 26; 18 27l33 TIME 1
0 0 •
S 0 /'. c o 0HIOMASS CHR01ATOGRAHS DATA( 3848 11 SCANS 950 TO 1089 <!•.91/22/85 12l34lM CftLIl 3843 K 10SAMPLEl COLUMN PERFORHAHE CHECK 1-839 2UL 4000 JK • 0CONOS, l 68H SP2339 78/2>218(28>248(6 0RANGE) Gi888,i8i8 LABEL) H 2,ie.e WMI A i. i.e J e BASEI u 29, 3 °
1099 0
19S3.79.9-1 S44S- 1956.
• / I A
329 S3Q / 1 / 1 / Y \ 329•9X
. -- 1\1\1\\ __________•-1 "- 1B99 1 '
2448.\ 18B.B-, l9^8• ^-O.^.qi, 2448.
i »: A A Ml i A/VI\ , , _ • "
' ( g g g ' ' r ,
382.12.8-1 "J?8- 314.
I - ^,0./, f. \ (\1\323. S22i / \ / 1 I V I 323.997
I - \ \ \\ - --^-^ —^\^^— /\^\.—/ L^-——^— \—>.A^^A^S^^•^^^^v--^^^A^1 968 988 1888 1828 1848 1968 1888 SCAN
24)83 24(33 2S|83 25l33 26:93 26:33 27(83 Tilt
(.'• 0 0
9 0 !.. S 0 0HIDMASS CHmmTOGRAM MTfll 3858 tl SCANS 958 TO 128091/22/85 28l57l88 Cffl-Il 3845 «6 1"SAMFLEl COLWH PCRFORHAHCE CHECK 1-839 2UL CftSE«3a89 4809 VY 10COMK.I EBM SP2338 78^0 2 ie»28> 24886 gRAHCEl G 1,1288 UfiELl H 8, 4.8 QUAHl A e> 1.8 J 8 GflSEl U 29, 3 §
1W-B-1 J3,' '>,1,2Tc-oO 0 5224.
I—————/^-~ ^3_ .
1822
• 1I T' 328 1 319.596
324 " 323.597
: 1129
^SS^SL^J • 1^^——'SS^lg&^J L l J LJ»p) Lll73_J
958 1888 1858 1188 1150 1288 SCAN23:48 25(83 26118 27l33 28:48 38(84 TIME
C. 0 0
/- 0 L S 0 0maims CHMHATOGRAHS DATA) ssss ti . SCANS sse TO iwe tD
ei/22/65 29157188 CALIl 3845 *6 0SAMPLEl COLUMH PERFORMANCE CHECK 1-039 2UL CflSE»3989 WWW oCONDS.i EBM SP2338 79/2>219»29>24986 0RflNGEl G 1,1208 LABELl M 2,19.9 WMl A 2, 2.8 J 8 GASEl U 28, 3 0
18882887. 1922
79 9-1 M7 ".i28- ^M- 2fl96'—1 1681. A , 7137. "*•
^-^.SO e75l• \ A A
A / / Y \A / V i v18892617. 1922w^ ^. T^""^.i1^-^ T A A A
322 / \ / \ I V \ 322.89G
\ 1 \ 1 \ 1 \ \ "1988
997 i%14. S-1 388. n 381-^2J---^^ 77«- n , ,323 l\ i \ \ /\ 323.897
/ \ M / V l * B'5Be
968 988 1888 1828 1949 1868 SCAN24l83 24)33 2Sl93 25l33 26l83 2El33 TIME
( 0 U
c o z - s o ' oMIDMASS CHROHATOGRAH DATA) 3858 11 SCANS 990 TO 1040 f'Bl/22/85 29157100 CALIl 3845 K ,-,SfWLEl COLUW PERFORHAHCE CHECK 1-939 2UL CftSE»3889 4900 UY r-,COOS. l 68n 5P2336 7e/2>21W2e>24e»6 0RANGEl G 1,1298 LABELl H 2,19.9 BUAHl A 2, 2.9 J 9 BftSEi U 26, 3 0
[9972599.
199.9-, "j06--/ct- "^ 2S69.
/ 1 J^L /^)-- ^ ^? -^f 1 -S-7^0? l
( 1 •?. 0 - ?
328 J I 328.939f I t 9.599
999 1909 1819 1829 1939 1949 SCttI24!4S 25i93 25!l8 25i33 25s48 26l93 TIHE
' • 0 J
6 0 /- S 0 0mUttSS CHR(MATOGRAHS DATAl 3858 11 SCftHS 959 TO 1868 (0 '01/22/83 2eiS7lOe Cft-Il 384S IE 10SAHPLEl COUJUN PERFORMCE CHECK I-B39 2UL CflSE»3889 4000 W 0CONOS.i 6eM SPi338 78/2>219»2fl>24e»6 0 1
RAHGEl G 1,1280 LABELl H 2,10.9 QUAHl A 2, 2.9 J 8 BflSEi U 20, 3 0 ;1006 0 15806. ;
74.1-1 24?35' S808. !
iT-^ I ^-— I332 J I 332.099 j
: i[1006 ~ !7827. •
100.0-, 32?74- 7840. |
334 334.108j t O.SOO
• , . f[ ,960 900 tOeO 1020 1040 1060 SCflN '
24l03 24l33 25:03 25S33 26l03 26l33 TIME( ^"i i'"') :'. \-_/ ^J
0 \. L S 0 0HIMflSS CMROMOTOGRW DATAl 3861 «1 SCANS 900 TO 1298 _
: 91/23/8S 8l21l9e CALIl 3860 t5 °-: SAMPLEl COLUMN PERFORMWCE CHECK 2UL 4806 JK ^
COOS. I 60M SP2339 78/2>21B»28>249»6 5i RANGE) G 1,1280 LABELl H 2,10.8 WMt A 8, 1.8 J 8 BASEi U 29, 3 o
: '"•I 3, rcoo-"^ , ° 362e-
| ^ -^-..00,3,^
: 1888 j |f l
1 'I
i 319 . 318.S3S323 322.536
i
1131;
\ . 1i —i—J\A,—r sn - . v»i. J ||. fe ' -AYI .I—f J \^.^t^-/ ^r^-i^^^-io-*-^398 318 1888 18S8 1188 1158 1288 SCAN
22)33 23l48 25)83 26ll8 27i33 28:48 38l84 TIMEI i' •\ , ')'. ^ '.J
t, I- /_ 5 0 0MIDMiISS CHMHATOGRAHS DATA) 3861 tl SCANS 988 TO 1180 —81/23/85 8121(80 CALIl 3868 15 —SflWLEl CCLUMN PERFORMANCE CHECK 2UL 4880 JK QCONOS.l E8H SP2339 78^>218628> 24886 oRAHGEl G 1.1280 LAB&1 H 2.18.8 WMl A 3, 2.8 J 8 BASEi U 29, 3 S
1889 ra4261.
79.6-1 la?19- 4264.
^"S ' 4on-/•»< )332 ( 332.033
: ) i 0.508
^-^o.^
; ——ac——J.J-I_-—i—l u.i - c - — • • ' • | ' • ^•->-'->—•i- -•r — i - _ ^ •T-- i • — i18895355.
108.0-1 22?6S• . 5360.
334 334.100' 1 8.500
908 950 1000 1051 1100 SCflH22(33 23(48 25103 26:18 27i33 TIME
( n n
Z [. L 0 0H1DMASS CffiOttTOGRAnS DATAl 3861 *19e5 SCANS 969 TO 1050 _i81/23/8S 8121108 CALIl 3S6B •S 3
; SAHPLEl CO.UHH PBiFORHAHCE CHECK 2UL 4088 JK 0CONDS.l 6811 SP2338 7B^>21BC6>24M6 0RAHXl GlB95,iei5 LABELl H 2,10.9 QUAHl A 1 . 3.8 J 0 BftSEi U 29, 3 0leie o
1453.88.3-1 "f78- 1496.
^o/ ^ o.-i'» A / \ r\/\328. '•^S / \ / I / V \ 329.996
_ _ _ ^^ -
: 1838.| 188.9-, 7re6.'»-o.°i-(. . 10. ^
\ . 333/ c 0,0'a < / \ A A"^3 /\ / \ / \ / \
322. / ^ / l / V V 322.B96) / \ / V \leie248.
13.5-1 , RB' 251.
323 [\ { \ !\ 1\ 323.097
: - \ \ v \
968 3S9 1880 1B28 1949 SCAN24(93 24:33 25:93 25:33 26)03 TIME
. 0 0
£ I- /.- S 0 0HIMASS CHROHATKRNI DATA) 3861 *1 SCAHS 959 TO IB58 -,,81/23/85 8l21lBe CALIl 3869 t5 enSAHPLEl COLUMN PERFOiHAHCE CHECK 2UL 4608 JK 0COCS. l WH SP2338 78/2>21Bt2e>24W6 0
; RANGEl G l<12ee LABEL) N 2.10.8 OUAHl A 3,13.9 J 0 MSEl U 29, 3 0; 1841. 0
i IM.O-, 7864.-^. «-17^ ^
' f?F '1']w; . nr - ^^
; fiF« 0.^51
'• 328 328.896; " t e.sea
960 388 im 1828 1848 SCAN! 24l83 24(33 2S|83 25:33 26:83 TIME
L 0 0
17 1. /- S 0 0HIDHASS CHROHATOGRAH DATfll 3869 «1 SCAMS 950 TO 1200 W91/23/85 15l44l88 CALIl 3S6B «5 5°SAHPLEl COLUMN PERFORmHCE CHECK 1-033 2UL 4006 JK 0
CONDS.I EW SP2330 79/2>21BK8> 24866 0
RANGE) G 1,1288 LABEL H B, 4.0 QUAHl A 9, 1.0 J 0 BASE) U 28, 3 §iw.e-i "^a^^.irc-oo 4929.
IK6 ^~~ ^^2,
1081 1
1895 i
I329 319.396324 323.S97
1133
J^^J v I'3" ' ^^^J ^^^J Vj J t358 1888 1859 1188 1158 1208 SCAN
23:48 23(83 26)18 27)33 28l48 38)84 TIME
c o y
S 1. L 5 0 0HIDHASS CHROMflTOGRflM DATAl 3869 *1 SCANS 350 TO 1068 _,M/23/85 lSl44l88 CALIl 3868 IS 'ySBWLEl COUm FERFOaWCE CHECK I-B39 2UL 4BBB JK "CONDS.i em SP2338 78^>21B»2e>248»6 ^RANGE) G 1.12M LAEELl N 2<lB.e QUflNl A 2- 4.8 J 0 BftSEl U 28, 3 o
24B3. 0
iee.B-, 18766.-9?.'W/ a48.
""I fiF- O.'K.O
328 . 328.898t 8.588
| _„— .,—.——^^^^v^^A 2^--^^^ /\^A-^^/^^/>^^^/\A^968 988 1888 1828 1848 1868 SCAN
24:83 24l33 25lB3 25:33 26t83 26(33 TIME
• : C. 0 0
9 U_ S 0 0KIMASS CffiOIWTOGRAHS DflTfll 3889 *1 SCANS 958 TO 1869 „,81/23/83 t5l44lU CftLIl 3868 »3 ws
SlWLEl COLtJMH PERFORWINCE CHECK 1-833 2UL 4888 JK °CONDS.l 6M1 SP2338 78/2>218e29>24886 "RAHGEl G 1.12B8 LABELl H 2.18.8 OMHi A 2. 2.8 J 0 BftSEl U 28. 3 Q
1818 ' (-»5693. -'
76.4-, 24^83• S712.
^-^ ^^^W \
332 1 332.899I A; 1818
7472.IB8.8-I 31?3®' 7488.
334 I 334.180
; , \
', 968 988 1800 1028 1848 1868 SCAN24:93 24l33 25:93 25l33 26|83 26l33 TIME
L. 0 0
L I- L S O OHIOmSS CHROMATOCRAMS IMTAl 3869 11 SCANS 958 TO 106081/23/8S 13i44l80 CALIl 3868 « c0
SWLEl COUtM VWVWtWS. CHECK 1-839 2UL 4888 JK ~CONDS.i 6811 SP2338 78/2>218Ke>248»6 u
RAHXl G 1,1288 LffiELl N 2.18.8 OUAHl A 2. 2.9 J 8 BASE) U 28, 3 Q '••1812 0I946- 1826 ;"•'] -.z i: ?r ^ "- :
^ A / \ /V\328 / \ / \ / 1 \ 328.896 ;i A / V l \1812 ,„,; 2325. 1826
i 180.8. ^ •" •"J : 2332. I
- - 7? A M ^: 322 / \ I I / \ 322.996 •
! 1 . . / \ / V | V " 1i ' ' 1 8 1 2 ;! TCC IttLD 11 ^Wl '5.41 '• ioai n.tc 44J* 1
1C •>_ 1""1 W0' IWM -M'1Ib.Z-i - . y yy^ r\ 1372. 382.-J^. y ITJ: /I . A
I 323: 3' A / M 323- 1
• ' / \ / \ / I \ * e''ie<l '^^-/<A>^^/^^^^A^^\^^^—--^^^ ' -'' I -\y\—A^^^—^\A_ I
: 968 988 1880 1828 1940 I860 SCAN24l83 24:33 25i83 2Sl33 26103 26(33 TIME
: C. 0 0
t \
NATIVE RF
320 332 Q .+ * + X " • RF
322 334 Q^————————————.—————.—————.—————.—————————————————————— Q-;
PC# FILE f ^-————————————————————————————————————————————————————————————————— !~~-
1 37S7 S7632- S-Wc/ _J__ £>.^_____________ in
2 S7il f-imo 'i7i,W 1___0.9')^_________________ ^3 J-7^ ztf^yto y/igJ?? Q-2 /.^________________* 3-1-11 SOSfoao 311, b^ 0-05 <.l7____________________5 3"7"?^ 1535-70^ 3.135T; 0-025 '•33.__________________
1 -?7?S loll^ io7S<,o s Q. gg 2__________________2 ^7fc?. ^jy^/g ^29^^/ 1___^c/___________________
( ) 3 37if____W3n7 J/oygy 0-2 /.IS__________________4 •3772- £.f{:/37o 28&&8S "0-05 /,/^_______________5 3')'?5 HIS250 39ni7 0-025 1,35
1 3 7*o____ fit'/S z if 361 5 Q.fss_________________2 J7kt S&e-K/l ilysti • '\___^______________3 J7^fe___ imi-if zfosn 0-2 /,/y_______________* 3~n^ I.KQWQ 3&<t.J> O-O5 /. 10_________________5 y?^ nat>3<g^o .aiifeo^ o-o25 i.3Q_____________
PC 111 RF' « o.SSO RSD • V.S L<t2 RF • t.ol RSO . 2./ _,'*3 RF . /./7 RSO - A? ^»4 RF . '•'3 Rsa -a . '? yff RF . ' -aS RSO - 3.5 -/ Criteria - s 10X
Hean R? . /. 0<? |h„ , A-^11
^ 0^ -/.^ / / \ A l ^b
( ' 000067
SURROGATE RF
332 Q c\
328' * + x " . RF —(0.009 x 322) 334 Q [--
———————————— ————————————1———————|———————|—————————————— LTiPCH FILE f 0
____________________________________________________ 0
1 3-7S-7 3/6¥6, ^-/S!"70/ 16.67 (.<5Z
2 -?76/ •^3lf ^7iiZ<i 8.33 "•^/
3 J76/ ^20^ %S^7 5 o.?75-
^ 1 ^73-^ ^^(0 6^60 16-67 o•'^so
2 J7&Z ^Y^1/ zzyz-yy 8.33 o'yss-3 ^7(;S- "/^ ?/<?%"/ 5 ^,,ySS
T 3W '^ssi tiSS6l ~\fi.VI t'W
2 37(,3 J?•}?-^ -r)'i"?// 8.33 O.'i'/f
3 J7^ .?^ z^J/7 5 ^%7
PC ^ Hean RF . o,m RSD ' (,.1K Mean RF . o.?os- RSD - ^'^ff Mean RF - o.'S7(, RSO . o'^f CrIterU - S 10X A
Mean RF' . O.^f, , '1r^^^
^ RSD RF . ^ ^(\JV\1
<—^ | ^
OOOOG8
0 6 L 5 0 0MIDWSS CHROHATOGRA11S DATA! 37S7 11 SCANS 95B TO 11BB O;81/14/85 16:47:88 CALI: 3751 •4 t0SAMPLE: TCOO CC1 1-615 2UL 4988 CASE13684 W °CONDS.l 6W SP2338 78/0 28W15> 24964 0
RflMGEl C 1.1108 LflBELl H 2,19.0 QUANi A 2, 2.0 J 0 BASE: U 2B, 3 °1827 °4313.
OB T_ 19214. .«—35.3-1 A 4328.
257 / | 257.B77
: /I __„___: "8"' ' ' 1 8 2 6 1 - —'
9876.74.2-1 38}?6' 9888.
ll /1'Z'; 328 Xf t - /^ 3 328.99C
1 1 ^ ± 8.588
-T-- - 1826
188.1h ^: *^0<,-W< 1^
322 . / | 322.996•____A . ~968 988 1888 1828 1848 I860 1888 1188 SCAN
24:82 24:33 25i83 25(33 26)83 26l33 27:83 27:33 TIME
t 0 0
I- Z L S 0 0MIMASS CHROHATOGRAHS DATAl 3757 11 SCWS 958 TO 1100 091/14/93 16l47;ee CALIl 3751 »4 lSAWLEl TCOO CC1 1-015 2UL 4000 CASE13684 W 0
CONOS.l Sen SP2338 7e/4>20e»15>24fl»4 0
RAHGEl 6 l.liee LABELl N 2.10.8 QUAHl A 2, 2.9 J 9 BASEi 1) 29, 3 —1626 —
32^1.-^^ ?/ <: ^
328 I | 326.096
: ^^________: ""IB25
55164.78.3-1 22?75- 55184.
. - l l ^ 4 SIM332 I I 332.M9:___A____•"
1925' JSSS:
188.8-1 298626. Tg^g
334 \ \ 334.1U• L^.^JL__-'968 988 1880 1828 1848 I860 1888 1188 SCAN
24i82 24l33 25l93 25l33 26:03 26(33 27:83 27l33 TIME
C 0 0
6 2 ,'- S 0 0MIDmSS CHROMflTOGRflMS DATA: 3758 »1 SCANS 958101100 ^i81/14/85 17lS2l88 CALI: 3751 *4 {s.SMFLEl TCOO CC1 1-013 2UL 4888 W 0COHOS.l WH SP233B 7a/4>2eW15>2«84 0RAHCEl C l>liee LABELl N 2.10.0 9WHi A 2, 2.B J 9 BASE: U 29, 3 0
1B23 04917.
3S.2-1 21?6' 4928.
237 / 1 257.877
•________IS_______•"1B2910684.
76.4-, 45156• lf^-^7^ 1WM-
329 I \ 328.896I I t 8.588
' ' W Q ' ' '14814.
; 188.8-, yaKS.^.^-.-.Sl. ^
322 ( 1 322.896A968 988 1888 1828 1848 I860 1888 1188 SCON
24182 24l33 25s83 25l33 26:83 26:33 27l83 27l33 TIME
(; 0 0
HIDHASS CHRONATOCRfllBl/14/85 17i52l88SAMPLEl TCOO CC1 1-1CONDS.I EM SP2338RANGE) G i.iiee
/ 1 328.098A-1-
/ \ 332.999A' ' ' 1927 '
85355.348918.
f \ 334.198A968 980 1898
24:82 24:33 25:83
us815 2UL478/4>298tu«ai H
cc
088 W15>248«42,18.9
MTfll 37"VLl: 37S
QUAHl A
1828 184825:33 26:83
58 tl31 t4
2> 2.8 J18287480.
1927fcaeM)OWW3«266656.
SCWS 951
8 BASEl U 28,
-W Jioi0
J"Sff
^
0 TO 1188
3
id7f60
1868 188826l33 27:83
CMr0000
7584.
66848.
85376.
1108 SCAN27133 TIME
0
t7 Z L ? 0 0
MIOHASS CHROMftTOGIMMS DflTfll 376B »1 SCANS 958101190 ?81/14/85 19l53l99 CALI: 3731 «4 QSAHPLEl TCOO CC1 1-015 2UL 4808 Vt QCONDS.I een spi33e 7e/4>29wi5>24e»4 0RANGEl G l.llW LABELl H 2.18.0 OUAHl A 2, 2.9 J 8 BASE! U 29, 3 0
18281976.
38.8-, 91?4- 2919.
257 / I 257.977I I t 9.599
_——^^——^-—Y^——^^'^^^'—^-r———.f 1^^^ _A^^-^~^^^^.^-^^a^-19284955.76-7] T .^-^
328 / I 320.896I \ ± 9.596
1827enAJ
yuw » a w < = 2//.199.9-1 "r-" 5296.
322 I I 322.996I I t 9.599
369 980 1909 1929 1949 I960 1888 1199 SCAN24:92 24i33 25:93 25l33 26:83 26l33 27:83 27l33 TIME
€ • 0 0
5 Z L c 0 0niDMASS CHROMftTOGRfttIS DATA) 3760 *I SCANS 358 TO 1108 'ei/14/85 19iS3:88 CALll 3751 «4 0SAMPLE) TCOO CC1 1-915 2UL 4099 W 0CONDS.l 681 SP2336 79/4>28a»15>!4B«4 0RANGE) G 1,1188 LABEL) N 2,18.8 WWl A 2. 2.9 J 8 BftSEl U 28, 3 0
10273046.
9.8-, 13793. z-'^ ^
328 / I 328.098) 1 * 8.S80
102624668.
78,0-1 wyl• 24704.A ^ ,z^332 | I 332.099: A ••"
; 102631634.
188.8-1 126848. 31688.
334 I I 334.180) 1 * 0.388
960 980 1880 1028 1840 I860 1888 1180 SCM24l02 24l33 25803 2Sl33 26:03 26833 27!B3 27i33 T1HE
: C 0 0
9 Z L (; 0 0HIDHASS CHRCTIftTOGRMIS DATAl 3761 tl SCANS 950 TO 1100 |n81/14/8S 20(32100 CALIi 37S1 M f.SMPLEt TCOO CC2 1-914 2UL WW W 0COOS. I Efln SP233B 79/4>29etl3>248»4 0RAHGEl G l.llM UBELl H 2,10.0 QUAHl A 2. 2.8 J 9 BASEi U 29, 3 0
1838 026436.
48.1-1 "I03- 26464.
257 1 1 257.977A "-193052975.
BB.4-, 2e?13- 52992.
|l <-= y7^7Jo
328 . / I 328.896- . , ,A . . -^1938
65929.199.9-, 266417./^^. ^
322 . I I 322.996A '•"969 989 1899 1929 1949 I960 1988 1189 SCAN
24f82 24|33 23lB3 25l33 26(93 26:33 27l83 27)33 TIME
L 0 0
/- g /.. S 0 0H1DHAS5 CHROHATOCRWIS DATA: 3761 11 SCANS 359 TO 1100 t0
91/14/8S 28l32l88 CALl! 37S1 *4 0SMPLEl TCOO CC2 1-014 2UL WM W 0COHDS.I 6eM SP233B 79/4>2e9«lS>24B«4 0RAHGEl G l.liee LffiELl N 2,18.0 BUAH: A 2, 2.0 J 0 BASEt U 29, 3 0
102913S22.
„, 52792.-ZJy».=-s-°"y ,-^2B.1-1 , jl 135S2.
328 . » I 328.098I l t e.see
1028329S7.
78.4-1 2wre3- S2992.|1 f~- </7t<,zo
: 332 . 1 1 332.833. A •""1828
67567.198.9-, 26?17- 67S84.
334 | I 334.18B• A368 3S8 1880 1820 1848 1B68 1888 1180 SCAN
24882 24133 25:03 25:33 26:83 26:33 27:83 27)33 TIME
G 0 0
, [, Z Z- s' 0 0MIDW6S CHROMftTOGRAMS DATA) 3762 *1 SCANS 358 TO 1106 r-81/14/85 21l86l88 CALIf 3751 *4 r;SAWLEl TCOO CC2 1-814 2UL 4688 UY °CONDS.l em SP2338 7B/4>2eedS>248»4 0
RANGEl G 1 ,1188 LABELl N 2,19.8 OUAHi A 2, 2.8 J 8 BASE; U 28, 3 ry1828 -
11812.35.6-1 48447' 11848.
257 1 1 257.877A1827
25283.76.1-, M?S9• 25312.n §--' ^7?/p328 j \ 328.896; A "
r - ' ' ^ 8 2 733258.
188. , 134949.^^7 . y^
322 I \ 322.896: A968 988 1888 1828 1848 1869 18S8 1189 5UN
24s82 24l33 25i83 25;33 26i83 26i33 27l83 27l33 TIME
C O O
6 3 /- S 0 0HIDHASS CHROMATOGRAMS DATA) 3762 11 SCANS 358 TO 1100 CO61/14/S5 21106)00 CM.1: 3731 14 t-~SAMPLEl TCOO CC2 1-814 2U. 4090 W 00X05.1 68H SP233B 7ft'4>2eMlS>24M4 0
RANGE) G 1,1180 LABEL) N 2,18.e QUAH) A 2. 2.9 J 8 BASE) U 26, 3 °1827 °3994.JKS79 -IZ15-- tlltf
18.6-1 z^'9- ' 6856.
328 ) I 328.898: , Iv^1826
25596.78.7-, "Y53- 25608.
n ^ ztfiyy332 ) I 332.899
i 1 A . '""'1826
32583.; 188.8-, 12?91- 32544.
334 1 I 334.180: ^ A ••"•968 988 1088 1028 1048 1069 1888 1180 SCAN
24:82 24l33 25:03 25:33 26:03 26133 27)03 27)33 TIMEc o • ;"^L V-^ •-..'
0 £ /, S 0 0HIOHASS CHROHTOGRAnS DATAl 37G3 *1 SCANS 959 TO 1108 ey
91/14/85 21l42iee CALIl 3731 t4 r-SMPLEi TCDO CC2 1-014 2UL 4080 VY °CONDS.I een SPSSM 7a/4>2eMis>24M4 0
RflNGEl G 1.11U LflBELl N 2,10.9 aUAHl A 2. 2.8 J 0 BASEl I) 28, 3 g102613496.
38.3-1 74]}56- 19329.
237 I I 257.977
A •""1026
41145.89.7-, 15S?24- 411S2.
A -- J667Y7
328 . f \ 329.836I I * e.see
1826S8983.
189.8-, 291623. «'. .-/ . g,
322 ( | 322.896) 1 t 8.389
968 988 1888 1829 1848 I860 1888 1189 SCAN24:02 24:33 25l93 25l33 26:83 26:33 27:03 27:33 TIME
L 0 0
I- £ L S 0 0MOHASS CHROMATOGRAHS DATA: 3763 tl SCANS 350 TO 1108 °81/14/85 21142:88 CALIl 3751 M QSAWLEl TCOO CC2 1-914 2UL 4080 W 0COWS.! Gen SP2338 7e/4>288815>24W4 0RflHGEl G liliee LAGELl H 2<18.8 WfHi A 2, 2.9 J 0 BASEl I) 29, 3 0
18239359.
19.1-, 4I2««.-^^ ^
328 1 1 328.096J t * e.see
: 1 , . , , •/^•1 , . - I ^
37881.; 77.2. l5l5a9• 37B24.
(1 ^ JffS/l
i 332 J I 332.999J I 1 e.see
1024: 49085.1B6.8-1 194552. ^g^
334 / \ 334.1W: A •••"966 999 IBM 1920 1848 1860 1888 1188 SCAN
24i82 24:33 23:83 25l33 26lB3 26:33 27|83 27l33 TIHE
C: 0 0
6 ? ./.. ^ 0 0
MIDMASS CHROMATOGRAHS DATAl 3?64 tl SCANS 950 TO 1100 *~!81/14/95 22fl6l88 CALI: 3751 »4 w
SAMPLEl TCCO CC3 1-913 2UL WOf Vt QCOWS. l GeH SP233B 79/4>2ee»15>24»l 3RAHGEl G 1.1180 lfiBB.1 H 2,10.0 BUAHl A 1, 2.0 J 0 BASEt U 29, 3 0
1823151822.
41.4-1 EM?85- 151040.
257 / I 257.B77I i t e.aee
1823231824.
; 89.1-1 1178888. 291848./l i'-- iaWt>
328 \\ 328.896
\ 1\________••-1823: 3G4544
\ 188.8-1 1482848. x CMf; /3W. WW.
322 I 1 322.896
1 i\_______•"968 988 1888 1828 1848 1860 1888 1188 SCAN
24l82 24l33 25:83 25)33 26:83 26l33 27(03 27)33 TIME
C 0 0
£ i L S 0 0HIDMASS CHMMATOGRAHS DATAl 3764 •I SCANS 958 TO 1189 CM91/14/85 22ll6iee CALIl 3731 *4 COSAITLEl TCOD CC3 1-813 2UL 4888 Wf 0CONDS.I 6m SP233B 79/4>2eeeiS>24et4 0RAHGEl G 1,1188 LABELl N 2.18.0 QUDNl A 2, 2.8 J 8 BASEl U 29, 3 °
1823 °24853.95368.-^.-^- ^
328 I 1 328.898; I i 8.388
1 ' ' ' J822 I I I I58543.
79.3-, vaw- 585G8.
H I ' WSSV7
332 I I 332.839: . A "' ' ' 1821 ' ' ' =^
6371S.188.8-1 7S3^3' 63744.
i 334 ( ( 334.188' I I 1 8.388
9G8 988 1888 1828 1848 I860 1888 1188 SCAN24:82 24l33 2Sl83 25:33 2Ef83 26l33 27:B3 27(33 TIKE
0 0 0'- . . . - . ^
fr £ Z- ? 0 0HIIMASS CHROmTOGRAHS DATA] 3765 tl •SCANS 950101108 S91/14/85 2Zl51iea CALIl 3751 t4 0SAMPLE) TCOO CC3 1-913 2UL 4899 W 0cows. i een sp233e 7a/4>2ewis>2W4 oRAHCEl G l.liee LABEL) H 2.10.8 aUAHl A 2. 2.8 J 0 BASEi U 29, 3 0
; 1823181228.
48.3-1 41%"• 181248.
257 ) 1 257.B77: A1823
138324.78.9-1 911105. IWW.
\ ^^ /f33//S-
328 \ \ 328.836J I t 8.988
' ^ 8 2 3231367.
188.8. ie21918.^.W- 1^. ^392.
322 J I 322.096:___A368 988 1888 1828 1848 I860 1888 1188 SCAN
24:82 24)33 25l83 2Sl33 26:83 26:33 27:83 27:33 TIME
C O Or
MIMASS CHROMATOGRAHS DATA: 3765 » SCANS 950 TO 1 in ^et/t4^s 22isiiee (MI.I« 3751 •4 gSAH>LEl TCtO CC3 1-913 2UL 4898 W oCCNDS.l 6»1 SP2339 7e/4>2eMlS>24W4 0RANGE) G I.liee LABELl N 2,10.8 Qumi A 2. 2.8 J 8 BflSEl U 20, 3 o
192316368.64126. - W7.--SfflV. ^^
1 1 328.996( 1 1 9.W9
J—^—^————————^——• - • • • •——————^34858.•3¥88• 34889.
A /--- 3/cW\ \ 332.999f 1 i 8.588yl
' ' ' 1822 ' ' ' '43699.172316- 43712.
/ 1 334.189A969 989 1899 182B 1849 1968 1988 1199 SCAN
24l82 24:33 25:83 25:33 26i93 26:33 27:83 27:33 TIME
0 0
9 £ I 5 0 0
maVB5 CHROMATOGRflMS DATA) 3766 tl SCANS 950 TO 1188 1081/14/85 23:2Slffi CALIt 3751 »4 c?SftWLEl TCOO CC3 1-813 2UL WW W °COHDS.I sen sma 7e/4>aeti5>24e»4 °RAHGEl G I'llBO LABEL) H 2,10.0 QUANi A 2, 2.9 J B BASEl U 29, 3 —
1924 —96123.
4B.4-1 3S3BS9. gg^
257 ) 1 257.977J I t 9.yW
1923184349.
77.6-1 764^59- 184S76.ll ,- /732?7r
320 f\ 329.896
:_______^________•"1023
: 237811.
Sit 0.00^'- S 7 / ' /1B9.B-1 ° " 237824.
322 322.696t 8.588
368 988 1888 1828 1848 1868 1888 1188 SCAN24:82 24:33 25:83 25l33 2Ei83 26s 33 27:83 27l33 TIME
C 0 0
L £ /- S 0 0MIDMflSS CMROHflTOGRWS DATA: 375E tl SCANS 958 TO 11B8 CO61/14/85 23l25l09 CflLls 3731 14 0SAMPLEl TCOD CC3 1-013 2UL 4000 W 0COOS. l 601 SP2330 7e/4>2e9»15>24%4 0
1 RAHGEl G l.liee UBELl H 2.10.0 QUAHl ft 2, 2.0 J 0 BASEl U 29, 3 °182315156.
3S.5. •T7- -"^--SB^ 1K1E.
328 . ) I 328.838A ••"^ ' ' [yQ I ' I I
33876.; 77.3-, 12?9S• 33888.
; - A f -- 2'fO-Sn332 I 1 332.099\ A
' ' ' ' J822 1 . 1 142786.
188.8-, 1KK2- 42816.
334 J I 334.188I \ t 8.588
968 988 1888 1828 1848 1060 1888 1188 SCAN' 24182 24l33 25l83 25l33 2E!83 26:33 27;83 27l33 TIME
(„ 0 0
a £ /- s o oHIUttSS CHROMTOXAHS OflTfti 3771 «1 SCANS 958 TO llBfl ^Bl/15/85 l8)41i88 CALIf 3769 »9 0SIWLEl CC4 1-912 2UL 4080 JK 0CONDS.l 601 SP2338 78/4>29B»15>248t4 0RttCEl G 1,1258 LABELl H 2,10.0 BUAHl A 2, 2.0 J 0 BftSEi U 28, 3 0
18233698.
12.3-1 l^w' 3772.
328 / 1 328.998
: - /I^
23324.76.8-, "JS68- _ 23368.
/I ^^^-^W
332 J I 332.B991 1 1 8.388
1 1 ' ' .821 • ''30748.
188.8-1 12146S. gg^
334 \\ 334.180I I 1 8.380
960 980 1080 1828 1840 1860 1088 1188 SCAH24)02 24)33 23)83 23)33 26l03 26:33 27)83 27)33 TIME
G 0 0
6 £ L 5 0 0MIUttSS CHROMftTOGRflMS DATAf 3771 11 SCANS 958 TO 1199 CO91/15/85 10(41188 CftLIl 3769 B COSAWLEl CC4 1-812 2UL 4080 JK 0COMDS.1 601 SP2338 78/4>28W1^24W4 0RAHGEl G 1-1259 LABEL) H 2,18.9 WtUi A 2, 2.9 J 9 BASE) U 28, 3 0
' 1923 0281983.I I QIQA42.9-1 11358UO. 2BIW8.
! 257 / I 257.B77) \ ± 8.5B8
; ~ 1 9 2 35324E3.
: 81.2-1 2233558. S32W9.
: " / 1 £ ' 502C)OSO~» I I 333*335 __ ___328 I 1 328.896
( 1 * 8.5881 1 . A1023
ESS346.188.8-1 2796478. eSS3e».
322 / I 322.896 // 1 t 8.388
9G8 980 1888 1828 1848 1868 1888 1108 SCAN24l02 24l33 25(83 25:33 26l83 26«33 27l83 27(33 TIME
C 0 •• 0
O V L ^ O O'• HIUMSS CHRCMATOGRAHS MTft: 3772 tl SCANS 958 TO 1108 5
81/15/85 lll2B:ee CALIl 3769 « 0SflWLEl CC4 1-812 2UL 4899 JK 0CCTCS.l 68M SP2338 78/4>28etl5>24e«4 0RANGE: G 1.12S9 LABELl H 2,18.0 fiUMi A 2, 2.8 J 8 BASE: I) 29, 3 0
19235210.
13.1-1 22?93- 5298.
329 | I 328.099
/I . • ""'' ' tea ' ' -^
31310.77.5-1 1M?27- 31328.
; - /I -- 2^^' 332 I I 332.B99\ A____•-
102240401.
18B.0-, 169?61- 49448.
: 334 / I 334.190f I I 0.S99
9E0 988 1990 1028 1948 1960 1889 1190 SCAN24(02 24:33 25:93 25:33 26:93 26:33 27:93 27t33 TIME
C 0 0
I- 17 L S 0 0MIDMftSS CHROMftTOCRMB DATA) 3772 tl SCANS 950 TO 1169 §61/15/85 lll28in CALI: 3769 *9 0SMFLEl CC4 1-912 2UL 4809 JK 0CONOS.l 66M SP2338 76/4>26etl5>24a4 0
; RWGEi G 1.125B LABELl H 2.10.8 BUAHl A 2, 2.9 J 9 WBEs U 20, 3 0• 1824
371191.44.9-1 1491569. 371208.
257 i \ 257.S77I \ ± 8.S99
1024G9118S.
82.B-I 280629. 69109,
328 1 1 328.8361 1 i 0.S88
1 7 ^1024
642732.169.8-1 359535B. „,„;
, - f\ S - W376>322 I \ 322.B96:__a__•"
968 988 1888 1828 1846 1868 1888 1188 SCAN24i82 24i33 2Sl83 25l33 26i83 2S;33 27:63 27l33 TItt
C. 0 0
Z V L S 00HimftSS CHROMATOGRWtS DATAl 3773 tl SCANS 358 TO 1169 '-Iei/15/83 12)88:00 CALIl 37E9 *9 2SAHPLEl DIOXIH CC4 STANDARO 1-612 2UL 4808 SEP °CONDS.l 6eH SP2338 79/4>2e8»15> 24884 0
RANGEl G 1,1188 LABELl H 2,10.0 OUAHl A 2. 2.9 J 0 BASE) U 28, 3 ~1826 —
361972.41.4-, 1597178. 3g,gg^
; 237 / I 257.B77i A1825
: E9324S.79.3-1 3838348. 693248.
^ - n j'.l,^55^&
329 ) | 328.836" ( 1 * 8.598
1825874478.
188.8-1 3784288. 874496.
322 ( 1 322.896i A968 988 1888 1828 1848 1868 1888 1188 SCON
24i82 24833 25t83 25i33 26883 26:33 27l83 27l33 TINE
C 0 ' 0
£ v L 5 0 0MIDMflSS CHROHATOGRAHS DATAl 3773 11 SCANS 950 TO 1188 w
81/15/85 12188! 80 CflLIl 3769 «9 QSMFLEl DIOXIH CC4 STANDARD 1-812 2UL 4000 SEP 0COWS. I SW SP2330 78/4>288»15>248*4 0RAHGEl G Llim LAGELl N 2,18.9 QUAHl A 2, 2.9 J 9 BASEl U 28, 3 o
• 192S5342.
12.9-1 "I77- 5480.
328 I 1 328.636J 1 1 6.366
162433285.
; 79.9-, 13?57- 33344.
: - M 5T.33U31332 . ) l 332.699
I \ t 6.S06
162441711.
166.6-, "V72- 41728.
' 3 3 4 f 1 334.186\ , . . A9E6 988 1800 1626 1646 1660 1686 1100 SCMI
24102 24133 2Sl63 2Sl33 26:63 26:33 27:63 27<33 T11E
0 0
V I? L S 0 0mWASS CHUHATUXAHS DATA) 3774 *1 SCANS 358 TO 1168 S81/15/8S 12l48lM CALI) 3769 «3 0SAMPLEl CC5 I-flll 2UL 4000 JK 0COBS. I EBH SP2338 79''4>288C13>248t4 0RANGEl G 1,1188 LAGELl H 2,18.8 OUAHl A 2, 2.0 J 0 BASE) U 2fl, 3 0
182411949.RQ| QJ38.7-1 i i2eee.
328 / I 328.998/ 1 t 8.S88
! ^ _ ^ _ . ^ y \^_ -. . .1023
38685.\ 78.4-1 "y65- 38636.
i 332 S > 3'35T^ / | 332.999; ' '- 1 1 t 8.589
; I ^\ ,'• 1823; 39978.; 188.9-1 lre?14' 39194.
| 334 f \ 334.199" ) 1 i 8.589
; 969 988 1888 1829 1848 196B 1968 1188 SCAN; 24i82 24i33 25i83 25l33 26l93 26:33 27:83 27:33 TIME
C 0 0
S 7 Z. 5 0 0
HIBHASS CHROmTOGRAHS DftTfti 3774 »1 SCANS 958701189 §01/15/65 12:48(99 CftLIi 3769 »9 0SAHPLEl CCS 1-011 2UL 4888 JK 0CUDS.) 6811 SP2338 78/4>288eiS>248(4 0 'RMKEl G 1,1188 UBa> H 2,lB.e QUAHI A 2, 2.9 J e BOSEl U M, 3 ;
1024 I79S624. ,
43.8-1 3672490. 79SE48. :
257 I 1 TSI.Wn |I 1 t 9.5W i
J \—— I1824 I
1476668. |81.4-1 685988B. 147668B. \
329 - Z^ 535 -7030 J ^ :g§ ^
18241814528.OAq7qAa1B8.B-1 W30W. 1814S28. i
322 I 1 322.896 ':___A____•"968 988 1888 1828 1848 1068 1888 1188 SCAH
24:82 24:33 25:83 23:33 26:83 2Gi33 27:93 27:33 TIME
(: 0 0
9 v L -a 0 0 "*'MIOWSS CWfWTOGRWS DATA I 3775 *1 SCflHS 358101108 CT
81/15/85 13122:88 CALI: 3769 t3 "SttFLEl 03 1-011 2UL W» JK —CODS.! sen sp233e 79/4>2ee(is>24»» "RAHGEl G l.liee LABELi H 2,1B.B OUAH: fl 2, 2.8 J 0 BftSEi U 29, 3
• 1025753648.
M.l-i 3364580. 7S3EU.
: 257 / I 257.877A1825
1388548.81.2-1 6319738. 1388548.
3M- ?. 14,^50 / I ^SS
1 ^ V- ,1825
1718858.188.8-1 7841528. 1718878.
1 A322 I I 322.836i A ••"368 988 1888 1828 1848 I860 18S8 1188 SCAN
24:82 24:33 25:03 23:33 26:83 26:33 27:83 27|33 TIME
(_ 0 0
L v L 5 0 0HIDIWSS CHMMATOCRAHS DftTfll 3773 tl SCANS 958 TO 1100 ^81/1S/83 t3i22l88 CALIi 3763 19 0SAHPLEl CCS 1-911 2UL 4000 JK 0COHOS.I 6en sroao 7e/4>2B»i5> 240(4 oRAHGEl C 1,1180 LABELl H 2-18.9 QUANi A 2. 2.9 J 8 BASE: U 28, 3 0
102419758.dSUffC39.5-1 -H— 18864.
328 I \ 328.838•___A •"1823
27284.76.3-1 taae- 27232.
332. ^..33,-,^ n ^833
182335S57.
188.8-, 139,117- 35584.
334 I I 334.188; l A960 988 1888 1828 1848 1869 1888 1188 SCAN
24:92 24|33 25:83 25:33 26:83 26:33 27:83 27:33 TIHE
C 0 0
8 1; L ^ O OHIDMftSS CHROMATOGRAHS DftTfts 3776 tl SCANS 956 TO 110881/15/85 i3!f7:ee CTLII 3769 *9 fsMCLEi ccs i-eii 2UL 4888 JK oCONDS.I 68MSP2338 78/4>288«15>248e4 0RANGEl G l>liee LfflELt H 2,18.0 WMt A 2, 2.0 J 8 BASE) U 20. 3 0
1826 0617454. 0
'9CMKCA44.4-1 AWSbB. g^^
257 1 1 257.877I \ t 9.508
19261138689.
81.9-1 489S6Sa. 1138699.
II gr' 110t)3(-'i0
328 / I 329.836
:_______i\_______"1826
1398598.188.8-, 6188838. 1398398.
322 I I 322.89GI I t 9.599
968 988 1898 1828 1848 1860 1888 1188 SCAN24:82 24(33 25)83 25(33 26(83 26l33 27:83 27)33 TIHE
L- 0 0
6 \J L S 0 0- HIOHASS CHROHATOGRAHS DATA) 3776 tt SCANS 958 TO 1190 °0
91/15/83 t3i57l88 CALIl 3769 *9 nSAMPLE) CC5 1-011 2UL 4888 JK 0CONDS.l 68H SP2338 78/4>288C15>24884 0(iAHGEt G bliee LAGELi H 2,16.0 QUAH: A 2, 2.8 J 0 BASEl U 29, 3 o
: 18258675.
: 38.2-1 36)?6- 8784.
328 1 1 328.838
\ [1824
21982.75.7-, 3ly3• 22816.
332 i\ ^ . ,3111^ 332.899l A ""1824
29836.188.8-1 "?91- 29888.
334 I \ 334.180
\ 1[ ••"•368 988 1888 1828 1848 I860 1888 1188 SCAN
24102 24)33 25(83 25:33 26)83 26)33 27)83 27)33 TIIC
0 0 0
Q 0 0 : .taUTiMillMi ',
HITIM. CJUIUIA1101 - P*tt 2 . |
SENSiiuir
____^___^____j«EA ________ Nol» Ht Pull Ht 251 Unlit S)(. S/N 25125) 320 322 | Va* 332 | 334 251 2S» i/N 322 322 322 322
CrIfrlJ i Z.i ^ 10 0.20 ''.
0.45
Cone. Callb. •IFIl.t mun^m____________________________________________
1-I^V-^ •5;H 1^\'\ -to"" a721u' 1311c><i l(i5s71 1333t13 l•s 3'i ^ '•'s ^ 0(' 0•4•2>
"Stf'/CTB
i-n-SS W^> s^ '°w t^2•B (pw tSQi ^y> 4 62- /(. A £2. 33 ^S"3?J7
^".£S__^a_ 1233- am A2U- JfflL /5£Z2. iQ£i. _!____!7 j7 ^ ^7 '7^ o•-?y
I-^K I 0 "13 to'3 "'0(''1 :lw2 3'"sl 1 37 i7 05 ^ 71fl 0'3'1
M1'3 . 4i'?3 iom iais( -HM 5o-)!,s 1, 2 s- 14^ 51 i ii-s (,s 0.31 i
i0________________ ___ ' ____ ____________ !0——————————————————————————————————————————————————————————0g * fldL^stc"L ^CO
^ 5 L S 0 0MIOMASS CHR01ATOGRA11S DATA! 3778 11 SCANS 956 TO 1 1 TO _81/IS^S ISlHlOe CALIl37S9*9 °SAHHEl CC1 1-dS 2UL 4990 JK °COHDS.l GW SP233e 7e/4>2eeei5>24W4 '-,RANGEl G l.tlie LABELl N 2,18.9 SWHl A 2, 2.8 J 9 BASE: U 29, 3 a
1827 02433.
43.2. "P9- 24S6.
\ 0,^257 I I 257.B77
( \ t e.fee
19274385.
; 77.6-, 2e,69- ^W/z^ ««6.
' 3 2 0 I I 328.836: , ...„ JL . "18275675.
IW.Ih, 27366. X^?-^ ^
/I 0.76322 I I 322.896
I \ t 8.S88
368 388 1888 1828 1840 I860 1888 , 1188 SCAN24l82 24:33 2Si83 25l33 26883 26:33 27:83 27l33 T11Cc. o o
2 (- /'- 5 0 0HIOHASS CHROMATOGIWMS OATA8 3778 *1 . SCANS 936 TO 1180 ^B1/1S/8S 15114800 CALIs 3769 •9 0SWLEl CC1 I-eiS 2UL 4000 JK ^OHS.l SW SP2338 78/4>289tlS>249t4 0RflNGEl G l.liee UCELl N 2,10.0 aUAHl A 2, 2.0 J 0 BASE) U 28, 3 °
1027 . °2365.
; 9.2-, 13654.-^<<-^S ^
328 J \ 328.098I I t e.seo
: 182S26018.
! 78.8-1 tfls579- 26112.n ^- - zJ?7r?
332 f \ 332.939' i A102S
; 33331.: 180.0-, 1;B?3- 33472.
I - A 6,-^7334 I I 334.100i l ^ . A ••°"
960 980 1080 1020 1848 186B 1088 1180 SCAN24l02 24:33 25:83 25833 26l83 26833 27803 27833 TIfE
; ( 0 0
£ S ,L 5 0 0MIt)Mftsl'CHROt1flTOGRftMS OATft! 3898 tl SCANS 1060 TO 106881/17/64 13138)80 CftLIl 3886 »3 CUSAMPLE) CC1 1-913 2UL 4889 JK 0CONDS.l em SP2338 78/2>21882»>24a86 .-1RANGE) G 1,1288 LAGELl H 2*1B.8 QUANt A 2. 2.8 J 8 BOSEl U 29, 3 0
T637 02832. 0
81.9-1 ^63' 2852.
Z-2^6 _ a < S ~ / , — / \ 3^^2-</%, -,-„-•'•"> . ff,- ____—————— ^lf-———— » / 01,,;? I 1 32B.B»^"To^r ff-f \ t
183624B2.
188.8 ( 12233. (), oo?=//» ^gg^
fc^^/ \ /OZ(3/ \7^r0-^322 j \ 322.836
f 1 * 8.588
1 8 8 8 1 8 1 8 1 8 2 8 1 8 3 8 1 8 4 8 1 8 3 8 1 8 6 8 SCAN23:93 25; 18 23133 25)48 • 26)83 26)18 26l33 TIME
C 0 0
t7 5 Z. S 0 015 W _»
HIDMflSS CHROmTOGRflfIS DATA) 3888 11 SCANS 358 TO 1188 -"81/17/84 13139(80 CftLIl 3886 *3 -JSflMPLEl CC1 1-815 2UL 4008 JK 5CONOS.i EOl SP2338 78/2>21B»28>24B»6 0RAHCEl G 1,1288 LABEL) H 2,18.8 OWNl ft 2, 2.8 J 8 BASEl U 29, 3 o
18361395. .
18.3-, 689S.-^-^7^ ^
328 . / I 328.838A,J^A^.J————^J^VA^^AA/^^* ' -^ J^^^ \ ^S^^^-/^^^V*\. f^V~»W——-r~ •——•^J«tfV^~>/*^^^^% '———^ A- A J^—^.^^^
183518745.
75.1-1 45S71• 18768.
332 H ^5-^7 332.899: . A . ^ '"183514305.
180.0-1 ?}3e' 14336.
334 I I 334.10BA ••"360 988 1880 1820 1848 1868 1880 1188 SCAN
24183 24l33 2S103 25l33 26l03 26l33 27803 27l33 Tilt
C 0 0
5 5 /. S 0 0•SW ^-
mWASS CHROMATOGRAnS DATA) 3888 *1 SCANS 1098 TO 1860 '-'81/17/84 13138108 CfiLIi 3886 t3 "SAMPLEi (XI 1-915 2UL 4888 JK 0
COOS. l G8H SP2338 78^>21812e>248«E --'RANGEl G t<1288 LABEL) H 2.18.8 QUWi A 2, 2.8 J 9 l" 2e' 3
1175.49.4-1 5y4• 1238.
/ \ £Z<ut-
257 / \ 257.877I \ ± 8.388
' ^"^^^ i^~~^^ \ ^ I i936 ' • '2482.
188.8-1 l2W' 2S84.
Mi^^r^/ 'I ;^23S
322 / 1 322.836I \ ± 8.S88
1888 1818 1828 1838 1048 1958 1868 SCAN25:83 25l 18 25.33 25(48 26;e3 26:18 26l33 TIME
<„ 0 0
9 S /.. S 0 0MICHftSS CHROHATOGRAHS DATA) 3837 *1 SCANS 950 TO 119001x21/85 16l39iee CALIl SCAN »3 inSAHPLEl TCOO CCt STANDARD 1-015 2UL CASE13889 WWW 0COHDS.l 601 SP2339 78/2>21B»8>24W6 -<RANGEl G 1.1188 UCELl H 2,18.8 OJAHl A 2. 2.8 J 0 BASEl U 29, 3 0
IBIS 0697. 0
44.9-1 2M9- 717,n ^z. ^-r?J7^———-J 1 yiZ
256 I I "»"<' /— 255.577258 ' ) 1 257.577
"^ L-l-- '"le^1""""'" —^-"-xl-^^•^~cr -i" -- -1——11308.
86.7-1 58a' , 1314./ I ^^--/^t
/313 I I — <3foofc ^ „. 318.S95321- I 1 '"SispF" ( 32e-596
- —— ^^ - ——— - — — _
1613.189.9-, ("?3- •'""^ 1628.
321 | I 329.596323' M 322.596
969 988 1989 1928 1948 I860 1888 1188 SOW24)93 24:33 25l93 25)33 26f93 26(33 27:83 27l33 TIME
0 0
L S L 5 0 0HIOIttSS CHROtttTOCRftMS MTfll 3837 11 SCAHS 950 TO 1198 (081/21/83 lEl38l88 CflUl SCAN *3 0SAMPLE) TCOO CCl STANDARD 1-813 2UL CASE13889 4888 W T-ICOHDS.l eeM SP2338 78^>21B128>24816 0RAHGEl C 1,1108 LABEL) H 2.18.8 OMHl A 2< 2.6 J 9 BASEl U 29, 3 0
IBIS °1112.
14.6 'SEa.-ii^m ii3g_
327 1 1 326.398329 ' ( I 328.S98
^ - ' ~ H143972.
77.4-1 25?72' 3976.
A 41^-^331 J \ 338.S99333 " I I - 332.399
_ _ , — — — - — — - - - ^^ ———-.- - —— — _
7712.198. e-i 32ra6- 7728.
333 | \ 332.6B8333 " j I 334.688
968 388 1988 1828 1848 I860 1888 1188 SCAN24i83 24l33 25:83 25»33 26l93 26i33 27l83 27l33 TIME
(r- 0
S S /- S 0 0MIDMffiS CHROWlTOCRflMS DATAl 3843 11 SCANS 956 TO 1100 081/22/85 14(86(88 CflLIl 3845 »6 '-IEWLEl CC1 1-915 2UL 4999 JK 0CONDS.l 501 SP2339 78/2>21Bt2e>24Be6 0RftHGEl G 1'liee LABEL) N 2,16.8 QUANi A 2, 2.9 J 9 BftSEl U 2B, 3 '-'ieieless.
12.9-1 "l38- 1896.
327 I I 326.396329 ' 1 1 328.598
1883 '6278.
73.7-1 m92- 6272./ ^-- I.OS
33z <" .;.; u^''i I I331 ^ <- ' ' '^ ( I J.(,Y. Oev,^-^. -From- 338.599333 I \ W^- RF 332'599
- - — -,_ _ - ^^ - - - —
8389.IB8.8-1 "iF1' B512.
333 | I 332.688335 f I 334.688
968 988 1088 1828 1848 1868 1888 1188 SCANZ4fB3 24:33 25893 25:33 26)83 26(33 27183 27(33 TIME
L 0 0
6 S /- S 0 0HItMASS CHROHATOGRflnS DATA) 3849 tl SCANS 350 TO 1100 CO61/22/85 14)96199 CALIl 3845 «6 0SAMPLE) CCl I-9t5 2UL 4999 JK ^CONDS.l 6«1 SP233fl 79/2>21»29>24fl86 0RANGE) G 1.11M LABELl N 2,19.9 BUAHl A 2, 2.8 J 9 BASEl U 28. 3 0ieie °
' 756.• 45.7-, 27?3- 765.
; - ^Y =0.3'? 1\256 '33 3 fli 255.37725B " 1 257.S77
I \ ^se '- ^ ....,-, -i -y^-h- ^—, --4-'^+---^1387.
; 83.3-1 6S12• 1394.
; ' ai1' - . f307(» ( 1319 to I 1 318. S95321 ' t I 329.596
; — - —— ——-,- — - - T - ^ — - ——— —- — - • — —: . 1E6E.
199.0-1 7¥4• 1674.
321 / 1 329.536323 ' J 1 322.596
j \ rt^ »^
9S9 989 1999 1929 1949 I960 T 1989 1199 SCAN24i93 24l33 25)93 25l33 26:83 26:33 27:93 27(33 TIME
0 0
0 9 Z . S O OMIOMASS CHROIIATOCRflHS DATAl 3863 tl SCANS 990 TO 1328 A)91/23/85 18l31l88 CALIl 3868 «S 0SflWLEl CC1 1-915 2UL 4880 JK «-4CONOS.l 68H SP2338 78/2>2ie829>24886 0RANGEl G bliee LflBELl H 2,10.9 OUAHl A 1,28.0 J 0 BftSEi U 28. 3 0
1968 0• 13634.
76.6-1 5B^65- 13872.
': 2s n'2bo7 / \: 331 / \ 338.399
333 ' / \ 332.S99: KF-0 .18 / V
180817912.
188.8-1 e?y2' 18112.
333 / \ 332.68B; 333 " / \ 334.688
998 993 1888 188S 1818 1813 1828 SCAN24:46 24)35 25)83 25)11 25:18 25:26 25:33 T1HE
(. 0 0
I- 9 /- S 0 0
HIMASS CHRDHATOGRAH DATA) 3863 tl SCAMS 308 TO 1109 nBl/23/85 10131100 CALU 3668 «5 -^SAMPLE! CC1 1-915 2UL 4000 JK ,-1CONDS.l 68M SP2338 7»'2>218(20>24086 0RANGEt G 1,1180 LABELl H 2,18.0 OUANt A 3, 5.0 J 0 BASEl U 29, 3 0
100S o1210.
100.0-1 "jl3' 1240.
\ 1 ~ ^25f; ^^-- 0 3^
33^
: 256 . 255.577250 257.577
; A^A^^^A^^^\~^^^A~y^^ ^f^yy^A900 950 1000 1050 1100 SCAN
22! 33 23148 25i03 26ll8 27l33 TIME
< . 0
2 9 L S 0 0MIQHASS CHROtWTOGRflMS DflTfl: 3863 tl SOWS 900 TO 1100 _,01/23/S5 10131100 CALl! 3868 15 '.SAMPLEl CC1 1-915 2UL 4000 JK _|CONDS.I Em SP2338 79/2>2iee28> 24996 0RAHGEl G l<liee LflBELl H 2,10.8 QUAHl fl 3, l.B J e BASEl U 28, 3 0
1889 02454.
85.3-, wy8• 2468.
•E:' ^5351319 318. S3S321 ~ 328.5S6
i i.nm .- - - - - - -. -^—^-^—^——^^-^J _ •-^m^»in——i——^J——^—_^-^—,,^.,,1889
! 2879.168.0-1 l2^51' 2884.
321 328.396323 322.596
i ^ v-^ ^ 1 - • n • • .988 950 1889 1858 1188 SCAN
22133 23(48 25(03 26:18 27:33 TIME
C, 0 0 :
£ 9 L 9 0 0MIDMftSS CHROHATOGRAH DATA) 3863 11 • SCANS 998 TO 1050 CM91/23/83 18t31lM CftLIt 3869 15 ^SAMPLE) CC1 I-91S 2UL 4999 JK ^ :COHDS. I E9H SP233B 79^21W3S>2WHS 0
RAHGEl G 1 ,1198 LflBELl N 2_lB.a QUANi A 1 > 3.9 J 9 BASEl U 28, 3 0 ;
1757.199.9-1 77?9- 1914. !
I
i
327 | I 326.396 '329 I 1 329.399 I
: _j_L__.... I999 1999 1919 1929 1939 1949 1939 SCAN :
24)49 23i93 25(19 23)33 25)48 26)93 26)18 TI)C ;
c - Q o ;
0 ^ 0 0 ! •SMCLE COKXHIHAIION CMOIIMUK UO»BCU
USC I ^aS^ l»Tg /-/S'-gr Project <gfeg________ MMim;, / - ItT-^S^ |_____________„____________________________________,________________ [
320 Ml * E<tlited Estiinited . ,EM I FllE » t « , < l t * t RF t Wt • Cmc. Hulu •^ Ir— telamiirm IWii.- -'. i
322 * Ml CoiKlitrttlon ll»it«tloo I
?003311 377^ 2i!fyJg, <^g> f7W t-e^f /0-'f — /,'/ 3.!^
Of0p3313 i7So 116W 'S6 UOISS /•01 W.S ——— 0-78'_____ ____i-0
OFoom'l J7>/ ins'/i St seitil i.oi ic.l o.ti(,____ ____o.lS ;
OFccm-i J/iil 'Ib/l sv i -10531 /.HI ,c,i — ____(i, tt_____ _____CI.'/Q II
DFccjilS nt3 Utaf w 1 1 1 1 1 1 , 1 /.p; /c.i ~ ____P.of,______ _____O.IS \
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322 VH CoiKciitntlon Lintalian
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0 L I. 5 0 0HIOMASS CHROHATOGRAHS DATA) 3779 *i SCANS sse TO nee91/15/83 16l82l88 CALI: 3763 *9 dSATFLE: TCCO DF883311 2UL 4888 CftSE»38S9 W r-1CCNDS.: EM SP2338 76/4>28e»15>24»4 t-1RAHCEl G 1.1188 LABEL) H 2,19.8 BUANi A 1, 2.8 J 8 BASE: U 29, 3 0: 984 0
24816. 012.fri 119832. ^^g
A o-^ \ 1B39 '
257 - /V \ • ^1: 1957 ^•^
/T V\ A K!8'-1 ,—/ Y^v^^^V^y--^^.; . • 1883: 163985.! 81.1-1 1122488. j^gg^
VM 1869 / 1 —» aae' 32B . «JV» / l 328.BS6I839 aai39G / \ ± e•sw
24113. 3MMG- / I13^. y\ / \; ___ _ ^_______ __ ..^. ___ _^/V ^-^^ V V\^^^^^,^^^.^ ,--/,'. ,^,/ ,Y ^V,————,
282524.
! '"•'I •-32° ort/"/ "T®' 283264-; . -^^K^-"- j \
'• TM 1068 / ( Q44 oqcI A" _ CTTV) / I ACt«TObi <B™ 65722. / i * A <UM' . .^ 2^5. 4^1B• / \
11848. 148168. ./ \ / Ii _"25i^ _ . - i i ^48 . ^^^ y . ^.968 988 1888 1828 1848 1868 1888 1188 SCAN
24:82 24:33 2S;03 25:33 26:83 26:33 27:83 27l33 TIME
(..- 0 0
niDHASS CHMHATOGRAHS DATA) 3773 11 SCANS 950 TO 1109Bl/l-1/85 16)02100 CALl! 3769 •9SflMPLEi TCDO DFee3311 2UL WW CASEt3889 WCOHOS.I E8H SP2338 78/4>2Betl5>246(4RAHCEl G MIN LABELl H 2,10.8 (MAHl A 2, 2.9 J 0 BASEl U 29, 3
183325856.137048.
Z L L S 0 0HIIMASS OHROHATOCRAMS DATA) 3788 «1 SCANS 959 TO 11B0 ^81/15/85 16t38l88 CALIl 3769 *9 —1SfWLEl TCOO OFee3313 2UL CASB3089 4009 W 0CODS. l 60M SP233a 79/4>2WeiS> 24684 0RAHGEl Gie3B,l93S LflBELl H 2,lB.e eUKNl A 1, 2.B J B BflSEl U 29, 3 0
'"'•"I ^L-.l.-l A A w96-'"? S-1831 1\/\
H-2288 . / V I A2S7. rA . A. 18672 /\ / \ / \ y,^1/VA^^-A^AA/, S'"BS.9-1 A 4352./i ye-;?.^ w ^ ; z.ibof,
- i \ -Jil 1B32 w £-\ \ 1818.
328. / I 15474. 328.896
-/ \ A-N\ V^^^y^^_^M/^^—'-^^vvYwAT^^^S* 1B31H" 1772
88.4-1 <r 6134 . 4328.
322 . i \ A i \ •Sia.WKA A / W \ A * ".".
' /^ \ /\Av. ^\/ \ /^-—AA'Vi | C-^——— ^ W^_A^\^_——I. J \^A/~^ V ^ ^ ^: 969 988 18W 1028 1048 1068 1888 1188 SCAN| 24(82 24)33 25(83 2Sl33 26lB3 26)33 27103 27l33 TIME
0 0 0
£ /- /- S 0 0MIDMASS CHWWTOGRAMS OATAl 3788 tl SCANS 958 TO 1168 CM91/15/85 16l38l88 CALIi 3769 *3 WStfTLEl TCCO DF883313 2UL CASB3889 4999 W -1CONDS.I een SP23M rs/watwuw oliMKXl G l.HOe LABELl H 2,10.8 SWHl A 2, 2.8 J 8 BASEl U 29, 3 0
1832 0
36SE.; 33.1-1 19?12' 3796.
. 3 2 8 / ( 328.898' ; 1 * 8.588
, 1831' 19771.} 97-4-} T' ^ r-- fio^ me8-• 332 _ i I \ 332.899
/\ 1 1 * 8.588
; ~~ ~ " ^ ' 1 8 3 1 ' ' ' ~11336.; 189•e^ T-^-^^/ w
: 334 1 334.188
^ : ___\,______^__ <^~^^,___^^^^rts '——s> • ^ - w^ - ~^ - ^^_^^^^^ ^ ^
968 988 1888 1828 1848 186B 1888 1188 SCAN24(82 24:33 25:83 25l33 26:83 26(33 27l93 27|33 TIME
; C 0 0
•i7 L L^OOHIMASS CHROMATOGRAHS DATA) 3781 tl SCANS 950 TO 1168 nBl/15/85 17l12(08 CtLll 37E9 *9 WSAnPLEl TCDO DF003314 2UL CASEt3ee9 WWW ^COOS. l OM SP2338 78/4>!8«15>24W4 0RAHGEl G 1,1189 LABELl H 2,19.0 OlANi A -2, 2.6 J 9 BASE) U 28, 3 0
1834 <=>976 2848' 1B79•-*] . T «••" a."' /^A /L r\I \ ^ A / "V / 'v\ 1 1.S"
ft / \f\,/^\L \^ L—\\M , / i. -lr V • \^ ^V\^A/^^— "'^V
qa 5_ ,-/c3fi , S'lBSS vfn <V <X»; ""'I ^ <- A A= 726 ^°---o.^ 9W.
j 52Z. / \A=38S2 3Z2-
329 J f\^ A .
^ X/^'^Vw^ ^ \^A^^V^k-''""1377. S" 1834ama H== 1216
52.2-1 'Y8-, A* 6494 1S32./^322 .1 \ 322.096, A . r l * e•5B8
. ./\/^.,, ;^ .J I V- . . ._ . - _.^..ift^Av^ \y ^^v \^/— \ / -^- ^ v^w _^_,36B see ieee iB2e 1940 iwa ieee nee SCBN
24)02 24)33 25(03 25l33 26(03 26(33 27(03 27(33 TIME
c' o o
S L L S 0 0HIDHASS CHROHATOGRAHS DATA) 3781 11 SCANS 958 TO 1196 <y91/15/85 17ll2i88 CALIi 3769 13 C\}'SAHPLEl TCDO ?803314 2UL CflSE»3889 4080 W r-(COHK.I 68H SP233e 7e/4>2WlS>24«4 0RAHGEl G l.liee LABEL) H 2,18.0 QUANi A 2, 2.8 J 0 BASE) U 28, 3 0
1833 <=>i 3833S.
33.1-1 159^92' 38464.
329 _ / I 328.836A ••'"1834
8S3E4.78.5-1 3TO?68- 86816.
^.y^ \ 1^--^w \\ -"
332 I I 332.8S8I I * 8.588
J 1; ' I ' ' ' • 1 8 3 4 1 ' ' '
183483.180.8-1 44?44- 183568.
334 / 1 334.180: I I I 8.S88
968 988 1888 1828 1848 1066 1888 1188 SCAN24f82 24l33 25l83 25l33 26i83 26]33 27:83 27l33 TIME
C 0 0
9 L L ^ O OMIDMASS CHROHTOGRAMS DATA) 3782 *1 SCANS 359 TO 1108 ,_91/15/85 17l43iM CALIl 3769 «9 -5
SAMPLE! TCCO DFM3317 2UL CASE13889 4008 W ;-CONOS.l 6«1 SP2339 79/4>28B«lS>24aM ^RMNGEl 61830,1948 U«ELt H 2,10.0 OJAHl A 2, 2.0 J 8 BASEi U 28. 3 ea
\ 0
257 . / \f\ j \ r \ 257.977
26.9-1 A 4248.
' — / I 1835 ,„,.<,..328 I \ 1494 _ 328.836; " \ 12791. A t 8.S88
188.8-1 n 15768.
j 1 8 3 5 / 1I 8187, / (
! 322 J S286. I 1 322.896i i _^J\ _J\968 988 1888 1828 1848 I860 18S8 1188 SCAN
24182 24l33 25:83 25)33 26l83 26833 27l83 27l33 TIME
C 0 0
/- L L S 0 0MIIMASS CHROMOTOOWlllS DATAl 3782 tl SCWS 350 TO 1 188 t°81/15/83 17l49iee CALIi 3769 *9 CJ
SflMPLEl TCOO DFie3317 2UL CASB3889 4000 W ^CCMK.l 601 SP2338 78/4>2fl9»13> 24984 u
RAHCEl C 1,1180 LABELl H 2,19.8 OUANi A 2, 2.8 J 9 BASE) U 29, 3 —IBS ~
36538.37.4-, 2M?31- 56648.
328 j \ 328.B98I I * 0.580/ 1 1969
// \ 3858._ / I ^-LA^g-' 1 8 3 4
119274.78.8-1 7AWISS. ^^gg^
( I (•-- ^OSff t^,,!./
332 / I 332.899/ I t 8.388
975 ^ I: 1837. / Ii I , ^'-i i r • S i 1 — 1
1833151265.
\ •"•"i 'T7' -w-. lsla6-334 f 1 334.188
181S / I * !>•5ee
12689 / \ "»2, 1^003. /• I nalA! •CT74B / 1 2914.
I , , .Kz49- ^ \ - ,
I 968 988 1888 1828 1848 1860 1888 1188 SCANi 24l82 24133 23103 2Sl33 26:83 26t33 27883 27l33 TIIC; L 0 0
S L L S 0 0HIDHASS CHROHATOGRAnS DATAl 3783 tl SCANS 950 TO 1100 t^B1/15/8S 18l2Sl9e CALIt 3769 *9 CMSAMPLEl TCOO Cree331B 2UL CASE*3889 4000 W -ICONOS.I EOn SP2330 78/4>289tl5>248t4 5RAHGEl G M188 UCELl N 2,10.8 QUANi A 2, 2.9 J 9 BASE) U M, 3 0
1878 °1846.
91.3-, • %% 2929.
r / \^ .A — / \ ^
•f\ r\J V^^/ vw^^^/__\..'-,-' \^ i - ? ^ i ^^ i^*^ - ^-^^"?6^763.
lyy s 698*. nqa— — • 1 •,-, A J^O-•' - tiSBf 82°•
983 ^--.O^ l\ S»1936 ,zt ^ "'415. J;; ) I H= 763
1W 3888-, J 1 A. 3927328 _ t , / I 320»99b
•AAJ^^Ll ^ Wy^^V^,19362118.
186.9-, 12?78- 2212.
322 f t 322.936
: : /^^ AI^^Y'^^1 ^—^vi ^^^ ^ V.^^s^^^V^F^---,969 989 1898 1829 1849 1869 1889 1188 SCAN
24102 24i33 25)83 23)33 26(83 26:33 27|83 27l33 TIME
( -_ • 0 0
6 L L 5 0 0niUttSS CHROHATOGRAIIS DATA) 3783 11 SCANS 950 TO 1189 m
Bl/15/85 18l2StN CALI: 3769 19 'SAWLEl TCOO OF883318 2UL CASE13889 4008 W " • ' ;CONDS.l em SP2338 79/4>2eW15>248M g :RAHGEl G l.liee UKLl N 2.10.8 eUAHl A 2, 2.8 J 8 BASE) U 28, 3 5 ;
1836 i38847. ;
36.3-1 2^¥28• 56896. ;
328 I 1 328.898 :
1\ - ^1835 ,
125777.88,3-i W3X. ^y^^
n c- n^-nt332 . / I 332.999
- < 1\ '""1835
156588.189.8-1 6a(!?73- 156672.A ^-^334 . | I 334.198
1 I ± 8.589
I I I , ^ V , , I968 989 1888 1828 1849 1869 1988 1189 SCAN
24:82 24133 25:83 25:33 2Cl83 26:33 27:83 27:33 TIME
C 0 0__ i
0 8 L S 0 0
MDHASS CHROHATOGRAHS DATA! 3784 tl SCANS 950 TO 1108Bl/15/85 13)00)00 CALI: 3789 *3 ...SfWLEl TCDO DFe03319 2UL CASE13083 4000 W —COWS. l 60M SP2339 7e/4>20»11>24e»4 "RANGE) G 1.1100 LABEL) N 2.10.0 OlMNi A 2, 2.9 J 0 BASEl U 20, 3 o
103S 05812. 0
78.7-, 31?9- 5680.
257 . J I 2S7.077, S \ ± 0.500
1015191E.
26.B"i \ ^ , 1940.1\ ^£- -. l-f Si" ^: tWM
. - \ 1034 ^VM I \ 756. WA *****w&D I | fACQ SWOfWK
/ I T^A * 9'sw
^^^^^^^^r^^/ ^\r ^•^-^^^^^//^/^^^7^.' ' ' 1021 ' ' i l
7408.IBfl O-i ''K93- s" te34 7472llTOtIr' r\ t^ W! nrZ*
/I A«5348
322 1000 / \ 322.0961338. / \ t 0.50013188. / \
1.. ^-^^^v. ^ y \ / ^ ^^^i r^-i ——^ ^,360 388 1000 1020 1040 1068 1688 1100 SCAN
24:02 24(33 25(03 25)33 26l03 2E.-33 27)03 27)33 TIfC
: C 0 0
1. 8 L S 0 0HIUHSS CHROMflTOGRflKS DATAl 37B4 tl SCflMS 950 TO 1190 -,ei/15/es i9i89i89 caLii 3753 «9 —SMfLEl TCOO OF003313 2UL CftSE»3889 4898 W ^CONDS.l EeM SP2338 78/4>2flB»15>24e»4 0RANGEl G Miee UCB-t H 2,1B.B OUWl A 2, 2.9 J 8 BASEl U 28, 3 0
1B34 <_)44353.
34.8-, "'I?12- 44416.
328 I I 328.B38/ \ t e.see
1933191387.
79.4-1 42343S- 191376.A ^^.WS^'>
' \ ^! 332 I \ 332.999; . / \ J^ -- O.I/ * e•5eB/V l "\
1933127683.
199.9-1 WWl. Vin^.
334 / \ 334.199/ 1 1 9.999
1915 / \ 19823673. j \ 1904.H^^ \^_ ? ^
969 989 1898 1929 1949 1868 1989 1199 SCAN24182 24)33 25l83 25)33 26l93 26l33 27)93 27)33 TIME
C 0 0
g e / -s o oHIMASS CHMHATOGRAHS DATA! 3783 » SCANS 959 TO 1189 .81/15/83 19i36l88 CALI-. 3769 »9 ^SAMPLEl TCOO OFee332fl 2UL CASE*3889 4808 UY —COHD5.1 E8H SP2338 78/4>20M15> 24884 ^RlWGEl £1834,1835 LABEL) H 2,18.8 QWHl A 2, 2.8 J 8 BASE) U 28, 3 5
1835 01542.
49.7-, w7- -, 1786.A JH^.^^M A n "257 . / \ / \ I \ 257.877
/ \ fv\ \ A.yA^A^ \^W\^J \L\^^^^/\,.
41.9-1 S= 1833 .' » 1448.\ A: ills An ^ZJ^328 / [ 328.896
I 1 1 8.388! i -^A^^^^^^^V-^^^ .&= 1834H; 2528
188.8-1 »>' 15873 ?4 3tO!^Sl n 3448.JBUi. • "m I \fywa ' f \__ AloRW. , f I
322 / \ ( 1 322.896^ J \ \A^r^^y^^-, ^\y^^^1^ \'—-^ / y^--968 988 1888 1828 1848 I860 1888 1188 SCAN
24»82 24l33 23|83 23:33 26l83 26l33 27l83 27l33 TIME
C 0 C
£ 5 /- S 0 0
HIDmSS CHROdATOCMnS DATA! 3783 tl SCANS 958 TO 1198 n>91/15/85 19:36108 CALI: 3769 19 COSAMPLE: TCOO IlFBB332e 2UL CASE13989 4900 W ^CONOS.I Em SP2338 7e/4>2Be«15>24fll4 0RAHGEl G l.llW LABEL) H 2,19.9 QUAHt A 2, 2.0 J B BASE) U 29, 3 0
0
49-7-! 1'228. ws, f\ ^- .- ^ 17W-7% ^: /^^••' J"2S7- / \ / I / \ 257.977
^ - / \ /^U \ A^^^LJ^^^^^J- ^19491372.
| 41.9. ^- i«e,J-P.—JlH r--^-7^
^ 32e- J n ^i i-.-^A^^^V^^^y^^ .
1169; 3318.' 199.9-, JJ£- - 1 - 3 "34 ITS32- 3449.! 'fit 2516. (I: . ^/, 27?68- M; ^A /\ I
322 / \<——z.-l<~ I \ 322.996J\ \ .^A.A/'-V^V-^ ^V^^^ \——„ / ^
969 989 1980 1929 1949 1069 1989 1199 SCAN24:92 24:33 25(93 25(33 26(93 26(33 27:93 27(33 TIHE
C 0 0
17 & /. 5 0 0H1UIASS CHROHATOGRAMS OATAl 3785 tl SCANS 958 TO 1180 —81/15/83 19l36l8e CALI: 3769 «3 „SAMPLE) TCOD ?883328 2UL CASE13889 4808 UY ^COMDS.l f8n SP2338 78/4>288»15>248M 0RANGE) G 1 .1180 LABELl N 2,18.8 OUAHl A 2, 2.8 J 8 BASEl U 28, 3 0
1834 091578.
38.1-, m^a• 91648.
328 1 1 328.898I I t 8.588/ 1 1868/ \ 936.
^, \^ • "718. ^1833
192511.88.1-1 9e?ls23• 192312.
; 1 ^ : l t O t > Z ' i 3
332 \ 332.839f I t 8.580
- 974 , / \1693. /Y' \| .7318- . • ^ T \ ^
1832248362.
188.8-1 1192678. 2WSM.
' 1 A ^ "334 f I 334.180f 1 1 8.500
977 / \937. y \665 . ^ . \^
960 988 1888 1820 1848 I860 1888 1188 SCAN24:82 24:33 23:83 25l33 26:83 26:33 27:83 27)33 TIME
: L 0 0
5 9 Z. S 0 0MIDWiSS CHROWTOGRWS MTfti 3786 »1 SCWS 358 TO 1100 •M81/15/85 28llll88 CALIl 37G9 t9 COSMFLEl TCOD DF893321 2UL CA5Et398S 4008 W ^COBS. I E8K SP2339 79/4>29egl5>24eM 0RAHGEl 01930-1049 LWELl H 2,19.9 QWHl A 2, 2.0 J 9 BASE! U 28. 3 0
0
66.9-1 n zy7 - <?.7Z 2832.A ^ \ •--IB36 J^ "I V ^ / 1 H= 1457
257 / \ A /v/ I fl- 5323 /\ 257.977y \ . A n \ / \ * '•»»YV/ \^^^ ^VLl . /v, '19382931.
51.6-, 2184.
{-•yz./^329 329.99E
t 9.389
,—^^-^^^v^v./x^ ^^^^^/v^^^19384918,
199.9-1 4232.^ -- ^,5?J; .
322 ^" 322.998A n * B•^8()
A A fj\^J\ V\^^J ^A^ S. \^ ^/V^^^ \ / s_ __
369 988 1999 1929 1849 1060 1988 1199 SCAN24:92 24:33 25:83 25:33 26:83 26:33 27:83 27l33 TIW
L- 0 0
9 S 00
HIDHASS CtKOMATOCRAMS DATA: 3786 «1 SCflHS 958 TO 1198ei/15/85 2eiiiiee CALI: 3753 »3SAtFLEl TCIX) DFB83321 2UL CASE1388S 4989 WCOND5.1 601 SP2338 79/4>2e(l»15> 248*4RAHGEl G Lliee LftBELl H 2,10.8 QUANi A 2, 2.0 J 8 BASE) U 29, 3
1941976 2726.
l - Q L ^ O O
moves CHRmnOGRAHS DATA: 3786 tl SCANS 956 TO 1168 tO01/15^5 !Bsttl9B CALIi 37C9 t3 c"3
SMfLEl TCOO OF993321 2UL CASE13869 4998 W T^CONDS.l 6m SP233B 7e/4>2ee(15>24«4 "RAHGEl G 1<11M LffiELl H 2,19.9 WWt A 2, 2.0 J a BASEl U 29, 3 -
1836 -171264. --94?06- 171264.
/ 1- 328.B96
/ I1035
361984.'22^?'1B• 361984.
n i-^t/fS-f //
j \ f'-^Wio ^ "l:^977 / \1316. / \S842f ^/ \ , ,
1833443449.-261WB' 443449.
M J^i; 6-^
\ '" .»:s, , , , / \ , , ,
968 388 1990 1929 1648 1068 1988 1180 SCAN24!92 24i33 25:93 2Si33 26893 26:33 27:93 27;33 TIME
0
u y . Si u uMIDWSS CTROMATOGRWS DftTfil 3787 tl SCANS 950 TO 1189 ISei/iMs 28issi8e CALI: 3769«9 03SMPLEI TCflO OFee3323 2DL CASE13889 4888 UY '-ICOMOS.l 6m SP2338 78/4>288ei5>248(4 0RAHCEl G 1,1188 LABELl H 2,18.8 QUAHl A-2, 2.8 J 8 BASE) U 29, 3 0
3E9 0
7875.43.8-j ^y4- J5Z - / J 7488.
/ \ 4306 S= 1848 ?ZZ tt'ilI I 'M30. i.. <)«Q| ' '/ I ^TC^C n^ 2191/ T
/ 1 / 1 * 9.W- li . -.,. /^x^^386
l2^q S" 1M249.4-1 • •'-" H= 3379 8448.
( 1 A° 19655 -.- }i7fv
328 . _^"^ V „ 328.896/ \ r-\/\ ± e•SM
•-.^..^^^.-^^ /V^A.,Ayv.f v i , ——. v. . ^ Y , '^y , . \-/ . - ^.TO s"194116648. H. 3117
188.8-1 965 12%64• ft= 13125 7^ 17888.
J S. A ^ - /5 -
'- /\ , / \ . 'e:g1
' / . \^^V \. ^.^A_^^. .-- --.968 988 1888 1828 1848 1868 1888 1188 SCAH
24:82 24l33 25t83 25l33 26:83 26l33 27|B3 27t33 TIME
L . 0 0
6 Q L S 0 0MIDHftSS CHROmTOGRflnS DATA: 3787 tl SCANS 959 TO llfl9 „81/15/85 29155180 CALI: 3769 »9 00
SMFLEl TCOO OF883323 2UL CASE*3889 4088 W •.CONDS.1 G«l SP2339 78/4>2eMlS>24M4 c-)RAHGEi G 1 ,1100 LABELl H 2,18.8 BUWl A 2, 2.9 J 8 BASEl U 29, 3 o
969 0TOTS.
43.8-1 ^SP4- , , 7488.ll 933/ \ 4398./ I 27^6-
257. . / I /\ 257.977/ t / \ ± 8.588
r^-A^L--^^ ^ ^^rrc^^ .3867972.
49.4-1 189759. g^
339 - "• \ - 324.896/ \ r-\/\ * fl•WB
- ^^M^V^V ,/v\,999
16648.t88.8-i 965 IMW. ^^g
12947. / \125848. / I
322- / \ / \ 8:588• / _ \^^/\/ \_ -.^<\/^r\. -—--.968 988 1889 1828 1848 1968 1888 1188 SCAN
24:82 24l33 25:83 25:33 26:83 26:33 27i83 27:33 TIME
C 0 0
0 6 L S 0 0
M1DMASS CHiOHATOGRAHS DATA: 3787 11 SCANS 938 TO 1100 f81/15/8S 28)33:88 CALl! 37E9 (9SAWLEl TCDO B-883323 2UL CASE*3889 4866 W C.-Jcoros.i 6w sp233e 7e/4>2ee8i3>248»4 uRMKEl G 1,1198 LABELl H 2,10.0 WMl A 2, 2.8 J 8 BASE: U 29, 3 0
184812484.
36.8-1 l9Ja2• 126S6.
328 - 967 /-/ I 1868 328-898
237B. / \ 2<»- * B•MB
- • 7768: / \ 12293-l}f^Vr}(^^^^ ^ ^ / v -V ^- ,
1839: 29637.
86.9-1 A • c^ftlcTi 29929.
332. / 1 ,_, 332.B99/ 1 1B61 ^ 9 jag/ \ 3852.
'_..——-,^————..-.^ ,\-^ .-. ..-..34286.
1B8.8-1 2S7248. •jWSt.\ J-n\ ^ - ' • °
334 J \ 334.188r \ t 8.588
968 988 1808 1828 1848 1868 1888 1188 SCAN24l82 24:33 25i83 25|33 26iB3 26:33 27i83 27l33 TIME
L 0 0
I 6 L S 00hIDHASS CHROHRTOGRAMS DATAl 3889 «1 SCANS 930 TO 1199 ^81/17/85 14l23l89 CftLl; 3886 «3 ^SflHPLE) DIOXIN REAGENT BUWK 2UL 4890 JK 0CONDS.I een smw 7e^>2iw2e>24eK 0RAHGEl G l.liee LfCH-1 H 2.10.9 QUANi ft 1, 2.0 J 9 BftSEt U 29, 3 0
10358918. (?F. y^^^_?_Z
: 29.4-1 3&K6' 3?.oanto.f 8992.
, - A CF. 0,1?5
328 f \ 328.898•____A -1834
23987.78.6-1 lm72' 24832.
H ^ ^ - 3^917332 J I 332.099•____A
183430510.
188.8-1 138145. ggggg
334 | I 334.189: A968 988 1888 1928 1848 1868 1888 1188 SCAN
24lB3 24l33 2Sl83 23l33 26i83 26:33 27l83 27(33 TIME
: C- 0 0
2 6 L 5 0 0HIOMASS CHROHATOGRAHS OATAl 3809 tl SCANS 959 TO 1100 f-191/17/83 14i23i89 CALIl 3896 »3 <?SWLEl OIOXIH REAGENT BLANK 2UL 4809 JK '-ICOHDS.l EW SP2338 78/2>219Kfl> 24006 0RMKEl G 1,1189 LABELl H 0, 4.9 OUAHl A 9, 1.8 J 8 BASEl U 28> 3 §
IMt fl~i J? Idle
^ ^'^AX^' \^V<»^^s/^ .068 I B B I ^ .v/ ' A/ AA^^^——V^y i 9.S99
: 62.2-1 lc?6 632.
! »:V^^AX^^^\^^^
El 6 1<^3 626 :
; 322 VATW^W^V l V 6 , / \ .-, 322.996'vVJ'y^/ ^Ar^A* ^ 1974 * B•aB8
969 988 1898 1929 1949 1969 1889 1189 SCAH24(93 24i33 25i63 25i33 26(83 26:33 27:93 27(33 TIME
C 0 0
£ 6 L S 0 0HIDHASS CHROHATOXANS DATAl 3819 tl SCANS 959 TO 116081/17/85 ISllllW CALIl 3886 t3SAMPLEl RIHSOTE OF 863310 2UL 4808 JK w
CONDS.I 68M SP233B 78/2>2l8t28>24B»6 ^RftHGEl G 1.1180 LABELl H 2,10.0 QUAHl A 2, 2.0 J 0 BftSEi U 20. 3 "
1036 g•S4"1' 315""?0 •* "'S 0y, . 37578. f f f - , i^i.-;-'-——,— ^^"•n A "• 3&ow*-o^ M64-/ I f{F' 0.353
328 I I 328.090i i t e.soe
103522<67.
78.3-1 9a!14' 22496.
; " n £^.^':)3C''"^332 332.09S
i i t e.see
183528721.
100.0-1 "y84' 28736.
334 I I 334.100: A960 988 1000 1820 1848 1868 1088 1188 SCAN
24)03 24(33 2Si83 2Sl33 26i93 26:33 27i83 27(33 TIME
C 0 ' 0
17 6 L S 0 0HIDdASS CHROWTOGRAHS DATA) 3810 *1 SCANS 950 TO 1108 ^ ;91/17/85 ISllliee CALIl 3896 »3 r-\SAMPLEl RIH5ATE OF N3310 2UL 4898 JK 0 ;
: CONDS.l Em SP2339 7e/2>218Ce>248t6 0 1
: RANGEl G 1 ,1188 LABEL) H 2,10.0 QUAHl A 2, 2.0 J 8 BASEl U 2B, 3 0 '
44.8-1 n ^52_ , 1-7'?. Lo^ 372. \
A -A 3M \257- . / \ II 257.877
I \ I •\J| V^-A * B•^w !
-"^ LA^fW^M V^^y^^. I32.9-1 '*°«86.< 273. !
328 . fA A AftA* / I M A A 328.896 I
iA>WV \AAAA^. < •-1835 |785. j
188.8-1 i?3- 838. I
322 . / \ 322.896 !j \ 1 8.588 j
'/ . ^^^y^^^ /J^^ |968 980 18N 1828 1848 I860 1888 1180 SCAN :
24183 24i33 25l03 25l33 26l83 2Gl33 27l83 27l33 TIHE ;
0 0 0 '
S 6 L S 0 0HIDMASS CHROWTOGRMK DATA) 3811 tl SCflNS 950 TO 110991/17/83 15l33iee CALIt 3886 *3 „,S<WLEl DIOXIH SAMPLE DFW3381 2UL 4880 JK «COHDS.l 601 SP2338 78/2>2ie«28>248»6 ^RAHGEl G 1,1188 LABELl N 2,18.8 OUAHl A 2, 2.8 J 8 BASE) U 28, 3 0
1834 03372. 0
31.2-1 15?58- 34S8.
328 { \ 328.098- , ^ ^ A, . • •""18338264.
'• 74.8-1 36P1• 8384.
332 | I 332.899! f \ t 8.388
: ^ , - ^ 7 V ^ _ _ ^183311842.
188.8-1 47}94' 11184.
' 3 3 4 1 1 334.188
1 . . , 1\9E8 988 1888 1828 1848 1858 1888 1188 SCAN
24:83 24)33 2Sl83 25)33 2El83 26l33 27(83 27)33 TIMEI, Q f.J
HIDHASS CHROWTOGRlWS MTAl 3811 *1 SCANS 958 TO 110081/17/83 15l53i9e CflLI: 3806 *3SAMPLEl DIOX1H SWLE DFW3381 2UL 4000 JKCONDS.l OH SP2338 79/2>210t2fl> 24986RANGE) G 1,1180 LffiELl N 9, 4.8 BUAHl A 8, 1.8 J 8 BftSEl U 29, 3
97S
L 6 L S 0 0MIDMftSS CHROMATOOWIS DATA) 3812 11 SCONS 950 TO 1100 tD ;ei/17/83 i6i44)89 CALI) asae t3 T-SMCLEl 010XIN SAMPLE DF893393 2UL 4800 JK r1
caos.i sm SP2338 79/2>2i9«29>24M6 0 !RANGE) G l.liee UflELl N 2,10.8 OUAHl A 2, 2.B J 0 BASE) U 28, 3 0 '
974 '.1556. ;
! 89^ 12!28- 1B36 1E36. '[A la83- 1/'^ 7577. t\ A !2S7 / I / \ 257.B77 !
; - / \ / \ * B.5M 1
1^.^: V^^v^^-^J \^^^^—^ |1035 :731. ;
; 42.3-1 ly. - 0,'Si 3?7' 778. :
: " A ^ -- /<!?<? ;
: - / \ T' ;/ \ w^ !
^ 1^x^^^^^y\^A/-l ^^^^^ I101E '1737. |
19B.B-1 1094 n ' t»34 182e' !1877. H "28. ig56 S
i 81?1- / 1 7)?6- 886. ii , 322 A l l / I 3889- 322.B96 !' ' / \ / \ / \ A * 8.588 j
l/V^-V^y-A——^——— \ \•.^L——-^~^^ '—^-^^—f——.- —, !%e 980 1B8B 1929 1949 1060 1989 1189 SCAH •
24l83 24l33 25)83 25)33 26)83 26)33 27)93 27)33 TIME '
; C, 0 , 0 j
e o /. s o oHIDmSS CHROmTOGRflMS DATAl 3812 11 SCANS 95B TO 1188 r-91/17/63 16l44l88 CALIl 3886 13 TSftfPLEl DIOXIH SAMFLE OF0e3383 2UL 4000 JK •-ICOM)S.i GWI SP2330 70^>2ie82e>248t6 0WHBEl G l.liee LABEL) H 2,19.9 OUANi A 2, 2.8 J 0 BASE) U 29, 3 °
1B34 °b6885»
36,8-1 G6944.
328 _ 328.838
1833146146.
78.7-1 7TOMe- 146176./I Wf-.f-SN^
,/, 1 1 • "^•i- - C.lf I I332. ^r- ' " ( I 332.899; i A • •""
1833185836.
i88.8-i wasa*. twex.
334 I 1 334.188: J\ "968 988 1888 1828 1848 I860 1888 1188 SUM [
24(83 24<33 25:83 25i33 26i83 26)33 27l83 27i33 TIME I
^ 0 0
6 6 L S C OmnttSS CHROMATOGRAHS DATAl 3813 tl SCftMS 958 TO 1188 03B1/17/8S 17140)88 CflLIl 3886 (3 '0'
: SNTLEl TCOO SNTLE BF883384 2UL CASE«3883 4888 W •COOS. l E8H SP2338 78/2>218»28>248»6 0RAHGEl G 1.1188 LABELl N 2,18.9 BUWl A -2, 2.8 J 8 BASEl U 28, 3 °
1835 °1037
3S.8-, w8'- ^i--£>,?(, 1192.
1 A "2S7 / I 257.877
' " / \ (\ ± e'M'
: L-^^ A^^^ ^^^X l- ^^^^ \^ ^^-
', 1835: 2388.
79.2-1 ^P8' ,, 2496.
; ,7, S^ A ^--^' 328 803. j 1 328.89E
' ' f\ * 8.588
: - ^ . / ^^/__ __/V, , / - l — — ^ ^ , - A| / _ ' __ _ •^1 "^^^—M^1 ' -f ^ r^ '^^•y~~'"• •'s-T V~^~^^ •-.u- .
; ^1TO 193SH" 2931 2981.; 188.8. ft. 13328.^.^. ^ ^
A 29se-; - \ 9222.
: 322- \ f\ t3a9^A/v/v^J\^^Y^^^^L^ -^^ JA^^968 988 1888 1828 1848 1868 1888 1188 SCAN
24l83 24i33 25)83 25:33 2E<83 26:33 27(83 27l33 TIME
' C 0 0
o o r ^ o oMIOmSS CHROWTOOWMS DATOl 3813 tl SCANS 359 TO 1100 0391/17/83 17(48(98 CALI( 3896 *3 ^
: SMTLEl TCOD SMfLE DF»3384 2UL CflSE«3889 4009 UY •CONOS.I EM1 SP2339 7a/2>21B«29>248»6 0
MNGEl G l>liee LABEL) H 2.10.8 OUANi A 2, 2.0 J e BASEl U 29, 3 ~IB35 —1937.
33.8-, 4,19' lle2-
2S7 / \ 237.977
/ \ A * B'^Be'A^.^A^y\ ^^ViA. ^7 ^^^18332388.
79.2-1 M?8' 2496.
. 9 7 9 M1119. ( \ I
328 BS33- ) I 329.936 If\ | ± 8.399 g
^^^^AC^^^^ . !1933 j
i - 1
199.9-1 "I78' 1B79 3132. !A • 2B5e- !/ > °a??' \
322 M /I 322.996 [/ I I\ t 9.399 !
•^n^J^^v^AfiJA^-^2J^969 9e8 1999 1929 1949 1969 1989 1199 SCAN
24i93 24i33 23(93 23(33 26)93 26l33 27(83 27(33 TIME
c o o
HIDHASS CHROWTOCRflei/17/83 i7i4ei88aWLEl TCCO SAMPLECONDS.l 6WSP2338RflHGEl G Mim
see sea ieee IBM 1049 ieee iree nee SCAN24103 24l33 25103 25(33 28183 26>33 27103 27i33 TIME
MS DATAl 3813 «1 SCWS 350 TO 1100CflLIl 3806 <3 0
OFN33B4 2UL CASE*3889 4996 W 107e^2>21M2e>24aK '-1LABELl H 2,18.0 QUAHl A 2> 2.9 J B BASEl 1) 28. 3 °
1834 °16926.73115. -^'-nw ^
L -. 0-^?M
183342821.
I1833
SS3S3.241383.
A
1963 328.8364135. t 8.S8B
7L42888.
yii.i/nmSSt
332.899* 8.S88
59680.
334.199i e.see
o
20 i ^ 0 0HIIXUSS CHROWTOGRWS DATA) 3814 tl SCANS 958 TO 1100 .81/17/83 ISlMlW CALI: 3886 13 !*'SAHPLEl TCOO SAMPLE DF883305 2UL CA5E13889 4866 W --CONDS.l WH SP2338 7M>2\WW>2WK ^RAHGEl 01834,1634 LftBELl M 2,18.8 aiMHl A 2. 2.8 J 0 BASEl U 28, 3 o
0
180.8-1 5» 1034 ,< ^f-Z- ; ei.il 578.H« 343 / \ ^32-
A A' 17B6 A ; 1
2S7 . / \ / • \ 257.B77
i LW V^V^^^ ^^^A^' ''"": a S° 1833 ,,• ^--l .^/^ ^^^M -^"^ 344-
' 328 . , / V 329.996/ \ f \ A t\ i d SIM
-^r/^VVfA^^/ W^^V^^. '18344S1.
99.7-, 2^1- S17.
322 . I I . 322.996
-A A^AA^r^^ /\ ±8 '^ee/V/^^/y^^/ ^VJ^-^V VW ^AA.
969 989 1809 1828 1849 18E8 1889 lt89 SCAN24tB3 24:33 25)83 25(33 26)93 26l33 27l93 27(33 TIME
r o o
£ o f • g. o oMIUMSS CHROHATOdMHS DATA) 3814 »1 SCANS 958 TO 1100 S^ I81/17/85 18lS4l88 CALIl 3886 *3 ,2SAMPLE) TCOO SAMPLE OFB83385 2UL CASE»3889 4988 W 0CONDS.I 68H SP2338 78/2>218»2e>24W6 Q 1
RAHGEl G 1.1180 LAGai H 2.19.B OUAHl A 2, 2.0 J 0 BASEl U 28, 3 01840488.
' 1W.B-1 4^6- 578.
i - A /M ^; IW ly^V^^^ ^^ . A^j ".4-1 ^ .
I 328 _ . / \ 328.836A_A, .- \ /A A * e•s8e
L^V^VfA^^^ W'SA^MfS,,1834
; 451.; 98.7-1 2a§l• 517.
; 322 . / I . 322.896A / \ AA * A * "•sw
! - A A A r\ A t^l \ r^^^ \ /V\ ^r^^/^^f ^S./^A^ W^M,968 988 1888 1828 1848 1(68 1088 1188 SCAN
24l83 24l33 25)83 2Sl33 26l93 26l33 27lB3 27|33 TIME; (..; 0 0
t7 0 K S 0 0MIDMAS5 CHROMATOGRAHS DATA) 3814 11 SCANS 950 TO 1100 c'0Bl/17/85 18l54iee CftLIl 3806 »3 "SAHPLEl TCOO SAMPLE ?683383 2UL CASE»3B89 4080 UY 3CONDS.I BflM SP2338 78/2>21M29>248»6 0liANGEl G 1.1100 LABELl H 2,10.B QUANi A 2, 2.0 J 8 BASE l U 28, 3 o
103412869.
29.2-1 "S51- 12128.
328 I \ 328.036 I1 1 * B.5B8 |
: 183231919.
77 H-< 158663. ^loco^ ^-.-^ A ^^^ /w |^r / I !332 I 1 332.099 ;
, / I * 9.30)
^ ^1B32
41461.lOB-B-j M?69' 41S36.
334 ) \ 334.1M: A "see see leee 1020 ie4e leee i8f8 nee SCAH !
24)03 24l33 25l03 2Sl33 26)03 26l33 27)03 27l33 TIME
u 0 0
S 0 ;; '; o 0HIOHASS CHMtMTOGRAMS OATAl 3838 tl SCANS 958701180 'V.91/21/85 17129100 CALIl SCflHO 10SMFLEl TCDO SAMPLE* DF003386 2U- CASE*3883 4080 W •MCOOS.I 601 SP2338 70/2>21flK0> 240*6 0RAHGEt G L1100 LABELl H 2,10.0 QUAHl A -1, 2.0 J 9 BASE) U 28, 3 0
1013 0
299.19e•9^ tM' 5= 1913 ZS"7 . ^, ^ 223.
i i I H'~ 195 '^t?^-
256 i I i I , 255.377258 ' J v\ . A ^ ,/" l/\ , i A A 257.577
191CIflGB 5° 1916
68-9-! 1 H= 143 J2£. - A 2 f^ f^iol, ls5' !A ft'329 7^ ' 3?^ '
320 \\ 319.336 i322 " I » < 321.396 \
i \^^,^€^ \^^\.,J\, ^' S« 1B15
H=7252.B-, i A. 278 ^; ^^^ 117.
- \ » A ' 7£;
322 l /1 , A i\ 321.S96 I323 ' I ^ /I /~1* «/ '11 A / 1 A / \ 1 1 322.596]\^Jvyi^ v. ^^^
969 980 1888 1828 1848 I860 1888 1188 SCM24103 24(33 25)03 25l33 26:83 26l33 27l93 27l33 TIME
C- 0 0 i
9 0 i? S 0 0KIDHASS CHROdATOGRAMS DATA) 3838 11 SCANS 359 TO 1100 1001/21/85 17123160 CflLIl SCAN *3 ^SAMPLE) TCDO SAMPLE* WW33K 2UL CTSE»3889 4898 W ^CONOS.t E8M SP233B 7a^>218t2B>24W6 c>
RANGEl G I.IW UWELl H 2,10.0 (XMHl A 2. 2.8 J 9 BASEl U 29, 3 g
iee.9. „
256 M J \ 255.S77^Wwf WW^/A^ '""leie149.
68.4-1 ^e- . 1S4.
A319 / I 318.533321 I B i 1 / 320.896lWV^^vv^^V^KA^^M^55.1-1 i 124.
321 . A/Ill i /I / S 1 32B.S96^Wi^W^^A^960 988 1888 1828 1848 1868 1888 1188 SCAN
24(83 24133 25(83 25l33 26l83 26l33 27l83 27)33 TIME
0 0 0
L 0 n 5 0 0HIWASS CHROMOTOGRflMS DATA) 3838 11 SCANS 959 TO 1108 ID81/21/85 17l29i88 CALIl SOW t3 10SMFLEl TCOO SMTLE* DF8e3386 2UL CASEt3889 W» W ^CCNDS.l 6811 SP2338 78/2>219»29>24W6 0RANGEl G l.liee LABEL! H 2,18.0 QUMIl A 2. 2.0 J 8 BASEl U 28, 3 <-?
1915 c)
4128.30.9-1 1B?46' 4128.
327. [\ 326.398329 J 1 328.398
18149864.
73»3^ ) t ^ .• Q -i^i/'y 98i2« i« ^JZ ^ - 7Z^
331 (\ 339.S99333 I \ 332.799
—— _ - - — ^^ ^_
13343.
188.9-1 l83' /^^ . -7/ 1336e-
A 'sTt/""0'333 / \ 332.68B335 I \ 334.68B
968 388 1888 1828 1848 I860 1888 1109 SCAN24163 24)33 25l83 25)33 26l83 26:33 27:83 27:33 TIME
0 0
MWHBS CHROMATOGRA11S DATAl 3839 *1 SCANS 358 TO 110861/21/83 ISllElM CflLIl SCAN (3SflMPLEl TCOO SAMPLE* OFW3307 2UL CflSE»3889 WM WCWCS.l 6BH SP2338 79^>21W29>24W6RWOE.I G liliee LABELl H 2,ie.8 OUAHl A -2, 2.8 J 0 BflSEl U 29, 3
HIDHASS CHRWiTOGRMIS DATA) 3833 11 SOWS 958 TO 1108ei/21/85 isiieiee CALII SCAN 13SAMPLE) TCCO SAMPLE* CFee33e7 2UL CASE*3e89 4880 WCONDS.l SW SP2338 7e^>21BK9> 24886RANGEi C 1 - 1 1 M LABELl H 2.18.9 WMl A 2> 2.0 J 8 BASEl I) 29, 3
o I- e s 00 :
HIDMASS CtfiOMATOGRAHS DATAl 3839 tl SCANS 958 TO 1108 w •91/21/85 18lt6iee CALIl SCAN *3 l0
: SAMPLEl TCCO SAMPLE* DF983307 2UL CASEt3889 4088 W * 1
COHDS.l 68H5P2338 78^>;l0t28>24WE "RANGEl G 1<1188 LABELl H 2,16.9 QUAN) A 2, 2.9 J 9 BASEl U 29, 3 Q
19144755.
: 31.8-1 "I86- 4776.
A327 . f \ 326.596329 I 1 329.598
191311479.
: ^••h T- ^;^^ "472-
331 . H 339.599333 f 1 332.599
i ^ • ' 1813 ' - T - — — 1 - T — — — T: 14995.
IM fl-i b^36« mcuM; ^ /I 1 3 1 . o.'7'S •"""
- \ ^333 . I 1 332.608335 f 1 334.690
: 969 988 lew 1928 1948 1060 1968 1190 SCAN! 24103 24l33 25l03 25l33 26l83 26l33 27l93 27l33 TIME
C,' 0 0
I- I- & S 0 0MIOWSS CHROMftTOGRflMS DATA! 3848 tl SCANS 958101109 -91/21/83 19lB4l88 CAUl SCTN 13 "SAMPLEl TCOO SAMPLE* ?093324 2UL CASE*3883 4609 W —CONOS.I em SP233e 7a^>21M20>24et6 SPAHGEl G 1-liee LABEL) H 2,18.B QUAHl A-2, 2.0 J 0 BASE) U 28, 3 Q
Tloa *»_ 272. SB 1912
sf\A^^ ^1036
^i S-1815 43. J^, ,n,zz i76.2 145 Hs 3 7e' J^ 43. !
319 . , j II/ , f l l l l l l n fl A | 1 < < 1 ' il 1 « d fld I 318.59S '
S» 1B15 ^9, -y.y74 s-i H" 28 —'" TtS^ 41
968 388 1888 1928 1848 1868 1888 1188 SCAN24l83 24l33 25i83 25i33 2E193 26l33 27;83 27i33 T11C |
•,. 0 ' 0 I
HIEIWSS CHROHATOGRAHS DATA) 3848 11 SCANS 959 TO 110881/21/85 19184108 CALIl SCAN 13SAMPLEl TCOO SAMPLE* DFB83324 2UL CA5E«3889 4888 WCOMOS.l 68M SP2338 79/2>21M28> 240*6RAHGEl G 1.1188 LAGELl H 2,18.8 BUANi A 1. 2.8 J 8 BASEl U 28, 3
181251.272.
£ I- F 5 0 0HIDHASS CHHMATOGRMIS DATfti 3846 »1 SCANS 958 TO 1180ei/21/65 19l84l80 CALIl SOW 0 OlSlWLEl TCOO SMPLE* OFW3324 2UL CASE«3883 4009 W c0
CONDS.I Gen SP2338 7a^>21W29>24W6 ^RflHGEl G 1.11W LABELl H 2-18.0 flWNl A 2, 2.9 J a BASE) U 29, 3 0
1014 g2868. -
33.7-1 1^3' 2B72.
327 / I 326.539329 1 1 328.S98
' ' " 18134849.; 7B-7-] T .„ i- i \ v'1
331 . / I 338.S99333 I I 332.S99
/ \ 1936/ \ 32-
__——--- . - - 7 S Ax: ——— - - - . - - - — — _-18136145.
lee.e-i 26!87- 6152.J^.-^.s/
i iy'333 f I 332.680335 " I \ 334.6M
968 388 1808 1829 184B 1068 1888 1188 SCAH24(83 24)33 25:83 2Sl33 26:83 26(33 27:83 27:33 TIME
. 0 0 0
17 f/ p g o oMIDMASS CHROMftTOGRflMS DATAl 3841 11 SCANS 958 TO 11B0 _Bl/21/85 28131(80 CALIl SCAN 13 (nSAMPLEl TCOO REAGENT GLAHK 2UL CASE13883 4000 W ,-(CONDS.l 601 SP2339 79/2>21BK8> 24096 0RANGEi G 1'liee LABEL) N 2<19.e QUAHl A 2, 2.9 J 8 BASE) U 28. 3 0
0
_ - - r — — — — — — —— - — T - - —^— - — - - — ——
Sa tfll?168.B-1 979 H" 29 ^ . tf ; 2.6 3^ /: ?/ 46.
la 1B10 pp 24 n 'Si'^ 'i32
319 i it J l i J i n l i E i l 1 318>595
'" H!mW¥^ Wj/| AJ^A^jfe""'r - r" ~ ' ~ s* Tei3 ~r~~
H' 1171.7 ft" 12 33.
368 ^- 1880 1928 1848 I860 18S8 1188 SCAN24883 24i33 25!e3 25l33 26;83 26l33 27183 27t33 TIME
C 1 0 0
MIEMASS CHiOMTOGRAHS DATfll 3841 tl SCANS 930 TO UNei/21/83 2ei31lN CALIl SCAN t3SAMPLE) TCOD REAGENT BLANK 2UL CASE*3e89 4098 WCOWS. I Em SP2338 78/2>21W2e>24W6RttCEl G l.liee LABELl N 2,10.0 OUAHl A 2, 2.0 J 0 BASEi U 29, 3
O*CO'-I000
see see ieee 1020 ie4e ieee ieee nee SCAN24)83 24l33 25103 25l33 26!e3 26(33 27)93 27)33 TIME
C' 0 ^
9 !. h S 0 0HtDMASS CHROMATOGRAMS DATA: 3841 tl SCANS 950 TO 1109 10B1/21/B5 28l31l88 CALIl SCAN 13 COSfWLEi TCOD REAGEHT BLW. 2UL C«SE»3089 4808 W ^CONDS.I 6811 SP23M 78/2>218t28>24fla6 °RANGEl G 1,1180 LABELl H 2,18.8 QUAHl A 2, 2.0 J 0 BASEl U 28, 3 °
1013 --'1786.
43.6-, Y- 18W.
327 . I I 326.598329 M 328.398
1 T • ' 1 9 1 2 — — — — — ' — — — T • ^ - - ,
81.8-, 14?29- 3376.A ^-^331 . / I 330.399
; 333 ; 1 332.399
' ~ ~ ' ~ ~ r i a i i ' ~ r ~ ~411B.
: 189.8-1 'y^ J,i 4128.J A 4J7 ~- o-1'
333 I \ 332.680333 I \ 334.680
968 see leee 1828 1848 leee leea nee SCAH24l83 24)33 25:83 25l33 26)83 26)33 27)83 27)33 Tilt
C 0 0
L I- ° S 0 0HID RIC + SPECTRUM MflP DATA: 3842 tl SCWS 1085 TO 1028 iei/21/85 2ii2iiee CALI: sew R wes 325 TO 335 'SAMPLEi TCOC SWPLEt DFB833e2 2UL CflSE»3e89 Wm W \CONDS.i 601 SP2339 79/2>21W2e>248e6 i
rts IWB{ \^ ^. I
g L i0 »SS (
i l l /—335 ;
I I I ,4-334 [
. . . I I I I . . . . ^332
" . ' . ' ' " I ' . ' . ' • • . ^
i l l • j^-328
——————————————————————————————————I———.———i———————————————Z-326
^^-"~ ' -—^^^ RIC
1866 1098 leiB 1812 1814 1916 1B18 1020 SCAN |25:12 25ll5 25lt8 25:21 25:24 25:27 2S:3B 23l33 TIME ;
0 0 0 ;
MIDMftSS CHROHATOGRAMS DATAl 3842 11 SCftHS 95B TO 11B881/21/85 21l21l8e CALIl SCAN 13SATFLEl TCOO SAMPLE* DF993382 2UL CftSE»3889 4090 WCONOS.l E8M SP2338 7B^>21BKC>24B86RANGE) G 1-Iiee LABELl N 2,10.8 QUAHl A 2, 2.B J 8 BASEl U 2B, 3
1045
fr I- n 5 0 0MIDMftSS CHROmrOGRAHS DATfll 3842 *1013 SCANS 958 TO 1109 CO01/21/85 2ii2iiee CALI) SCAN »3 c0SMFLEl TCOO SAMPLE* DF803302 2UL CASH3089 4090 UY ^0X05.1 EBM SP233B 78^>21882B>24M6 u
RAHGEl G Lliee LABELl N 2,10.8 QUANi A -2, 2.8 J 9 BftSEl U 28, 3 ^
QA a— *^^ 'M-W.a ya I Jf.5= 1813 1B26 TI; 1f" 22» J I
256 I . 1 ti i \ J l l J i J l i ' l l A i l l i ' i l 2K.S77
. ii8 Ih/HK MAfll ^M^^I ~*™~ 1^*"*" ' * I t ~ ~ ~ t '~~ ~ '" " " I + ~ ^
1089963 982 £ }§14 31'-
, S» 1813 ,......H" 15 109S
M 9-i A^ 41 fc^' 97
I ^VAW^^
; 960 388 1000 1828 1840 1868 1888 1188 SCAN: 24:03 24)33 23(83 25(33 26(83 26:33 27(83 27(33 Tilt
C 0 0
0 Z .-.: GOOHIUIASS CHROHATOGRAMS DATAl 3842 tl SCANS 959 TO 1168 0;81/21/85 21(21180 CALIl SCAN 13 COSAWLEl TOD SWPLEt OF883382 2UL CflSE»3889 4888 W -<CONDS.t E8n SP2338 78/2>21Bt28>248*6 0RAHGEl G 1,1188 LABEL) N 2,18.8 OUAHl A 2, 2.8 J 8 BASEl U 28, 3 0
1813 c:3
943.4S.2-1 i56' 943.
327. ) , 326.398. „_ Ih_^^-^-> \ ^^-^^~->^^~~^s / n^*-- \ ~^—> - , ^A^v>^~^^^Y~^^s- .
; 1812"1786.
: 82.3-1 7?4' 1716.
331 / \ 338.399333 1 1 332.S99
_ - - - - —— — ^^ —, —T— _ _ —
2883.188.8-j 7? • 2884.
: 333 / 332.688335 ' f 334.688
! . 1.., __^_...__/J__._ ..__._.__.,.___,968 988 1888 1828 1848 1968 1888 1188 SOW
24(83 24i33 2Sl83 25l33 26:83 26:33 27:93 27l33 TIHE
C 0 0
HIDHASS CHMmTOGRAIIS DATAl 3843 11 SCANS 950 TO 110081/21/85 22llliee CflLll SCTM «3SflMPLEl TCOO SNTLE* OP9e33e8 2UL CASE»3B89 Wm WCONDS.I 601 SP2338 7B/2>21B»2B>248t6RANGEl G l.llie LABELl H 2,19.8 BUAHl A 2, 2.9 J 9 BASEl U 29, 3
101573.
0r-'-ioo0
78.
2SS.577 !257.S77 1
39.
310.393329.336
116.
329.596322.396
1199 SCAN27l33 TIME'^
C\!C\l
Ti00
£ 3 ; ? S O OHIOHASS CffiOnATOCRAIIS MTAl 3864 «1 SCAHS 950 TO 118091/23/85 ItiSllOO Cft-Il 3868 B toS(WLEl DKKIN SAMPLE tF98331E 2UL 4888 JK COCOHDS.l 68M SP2338 78/2>218628>248t6 '^RflHGEl G 1.1198 LAGELl N 2,18.0 QUAHl A 2. 8.9 J 0 BftSEl U 28, 3 °
1928 °1011 53-
ii.^'-? J.5n nois^ ^ 1 1256 _ . l l l l i l i J i A / ' l / ^ K5.577, "IkvA^ / ^ """
——,— - ^"1927 ' " ^1G9.
89.8-1 K3' 212.J 1B11 A.
1 ^t 1% IJ2?l ^^"o^ U A | |
ih^^A^^^1928210.
ipfi a. 64v 9'X
1812 11
321 . 2?3' I I 329.596323 / ' 1 1 1 A 322.396
^^^^^^^^^^^AA^vL^^9G9 989 1988 1029 1949 1060 1888 1188 SCAN
24l83 24t33 25l83 25l33 26:93 2G|33 2?!93 27l33 TIft/ 0 0
17 Z £ 5 0 0HIMASS CHROMftTOOWnS DATAl 3884 11 SCANS 958 TO 1108Bl/23/85 11(31)88 CALtl 3868 »5 r-SAHPLEl DIOXIH SAMPLE OFe83316 2UL 4188 JK 03COHDS.I 68M SP233e 78/2>218e28>248(6 '-<RANGE) G 1,11B0 LABELl N 2,18.8 OUAHl A 2, 2.8 J B BASE: U 2B, 3 0
1811 °1B11. c>
43.6-1 *ASa• 1828.
327 . ) 1 326.S98329 I I 328.S98
.-^ ^A^^-^^^^-^^^J^^f^^^^^^^^^^^^^^^^^^^^^w^^f^.f^^^———.J^^^-^ J^J^^.
1818: 1863.
68.9-, w?7- 1888.
331 / I 338.S99333 I I 332.599
' ~ ' W 3 ' ' —
2368.188.9-, 11?9- 2368.
333 f I 332.E8833S ' ) 1 334.688
9E8 988 1888 1828 1848 1868 1888 1188 SCAN24l83 24l33 2Sl83 25l33 26:83 26l33 27)83 27)33 TIME
L: 0 0
5 Z • - ^ 0 0H1DMASS CHROHATOGRAMS DATA) 3865 tl SCANS 388 TO 1068 c0
91/23/85 12l58l88 CALIl 3860 «S . °-SfWLEl DIOXIH SMPLE DFee3316 OUP 2UL 4000 JK •CONOS.l 601 SP2330 7e^>210K28>248»6 —RANGEl G l.liee LABEL) H 2,18.0 OUAHl A 3, E.B J 8 BASEl U 28, 3 o
1811 1829
^- ^- ^S735.3-1 -r- 'f1' •0-'. . 3(.«/, 195.
256 . / \ / \ 255.577258 / \ / \ 2S!''577
'„_^y\^^^^v^-—A^^—-V^A^^^A^^"II 1^.
: •l 1^- 1^' ^-mA /319. / I / 1 319-'5": 321 / I / \ 329.596
/^^^^^-y^^^~^^~^'~———>^^-J--^^-^• •S> - - ^^ __^V^-s^-^
IBll 1TOAOC OU3>
188.8-1 1543'.*°"'' l'' ""• 843.
321 _ / \ / \ 320.596323 ! \ I \ 322.596
988 998 1888 1818 1828 1838 1040 1058 1860 SCAN24f33 24i4B 25l03 25:18 25l33 25:48 26i83 26il8 26l33 TIME
(L-- 0 0
9 6 •; c: 0 0MIDW6S CHROIttTOCRflMS DATfll 3865 tl SCANS 958 TO 1160Bl/23/85 12l38l8e CALll 386B »S 05SAMPLEl DIOXIN SAMPLE DF883316 DUP 2UL 4888 JK CO 'caas.i ew snsaa 79^>iiMse>tWK ^RAHGEl G 1.1100 LMELi H 2,18.0 MMHl A 2, 2.0 J 0 BASEi U 28, 3 0 ;
1811 0 I2255. ° i
! 37.2-, 18631.-^-'^ ^
' 3 2 7 1 1 326.598 !329 ' 1 1 328,598 ;
; 1810 ;
; ^ '79.2-1 "X-" 4848. '
331 / \ 338.599 '333 ' ; 1 332.539
' 1 8 1 8E89B.
188.8-, 2%9S• 6112.
333 H 332.688 I: 335 ' I \ 334.688 !
; . 1 , , ,A I; 968 988 1888 1828 1848 1060 1888 1188 SCAN |
24lB3 24l33 25:83 25l33 26163 26l33 27(83 27)33 TIME |0 ;^ iu ^ j
L Z i' 5 0 0H10HA5S CNTOHATOGRAH DATftI 3S57 *1 SCANS 988 TO 1840 °91/23/85 14l2S;ee Cftt-Il 3S60 »5 2SlWLEl DIIMIHSMFLE DPBe3312 2UL 4388 JK ^COHDS.l 61111 SP2338 7e/2>218828> 24966 C-, ;RftHGEl 01819,1812 LflBal H 2,19.8 (lUWl A 2, 4.8 J 0 BflSEl U 28, 3 o
128.1B8.8-1 3?8- ^ 1GS.
: i : O.Zf^': J11
2S6 25S.577; 258 ' 257.S77
988 998 1888 1818 1828 1038 1848 SCAH24:33 24148 25! 03 25:18 23:33 25; 48 2El83 TIME
0 -.J
MIDMASS CHROMOTOCRAM DATAl 3867 tl SCANS 989 TO 104981/23/85 141261 N CALIl 3868 »5SAMPLEl DIOXIH SAMPLE DFBe3312 2UL 489B JKCONDS.I 68H SP2338 79^>2l»BS>2MKRAHGEl G181B.1B12 LflBELl N 2,18.B QUAHl A 2, 4.8 J a BflSEl U 2B, 3
1B12329.1105.
6 Z I S 0 0' HIDdASS CHROWTOGRAH DATA) 3867 tl SCANS 988 TO 1048 n,
Bl/23/85 14l2Giee CALl! 3868 15 3-SAHPLEl DIOXIN SAMPLE DFBe3312 2UL WSH JK ,-4COHDS.I 68H SP233B 7B/2>21B«29>24e86 0RAHGEl Gieie,lei2 LABEL; N 2,18.0 QUAHl A li 2.8 J 8 BASEl U 28i 3 0
1811 r~J338.
188.8-1 1311. X ^.ci)'?--/Z. „.
; 3lo <',Z'llle
; 321 . I A 32B.59G: 323 I J l 322.S9E
988 390 IBee 1816 1829 1030 1040 SCAN24)33 24148 25)03 25)18 25:33 25)48 26)03 T1HE
L- 0 0
0 £ ; • S 0 0MIDMASS CHROHftTOGRflMS DATA: 3867 11 SCANS 359 TO 1100 03B1/23/8S 14l2ElN CALI: 3868 13 '-1SflMPLEl DIOXIH SAMPLE DFe83312 2UL 4600 JK 0 ;CONDS.l 601 SP2338 78/2>218e28>248«6 <=> 1RAHGEl G Lliee LABELl H 2.18.8 WMl A 2, 5.8 J 8 BASEl U 28, 3 0 !
1011 ;535.
• 46.4^ WTi.-'t^crf ggg^
327 . / I 326.598 i329 I I 328.598 ;
^^A>/S / ^^-^ / ——\ / / ->^^A^^^-^^^ i1818 '
: 1845. |82.4-1 4^9' 1876.&''--"" A -^"^331 J I 338.593
; 333 ' ) I 332.599
i 1818; 1295.
180.8-1 5^17' 1386.
i 333 f t 332.686335 ' I \ 334.688
968 988 1888 1828 1848 1868 1888 1188 SCAN24t83 24l33 25103 25:33 26:83 26:33 27:83 27:33 TIME: r 0 o
I- £ t; S 0 0MIDMflSS CHROMATOGRM1S DATA) 3843 11 SCANS 959101180 'Bl/21/85 22llllBe CALtl SCAN t3 ^SWLEl TCOD SATPLEI DFB93388 2UL CASE»3889 4009 W t>COOS. l eOH SP2330 7B/2>219»2B>24866 ^RANGE) G 1,1199 LABELl N 2,10.8 OJANi A 2, 2.8 J 0 BASEi U 28, 3 §
1014 § •749. - ;
59.2-, 4?4- 765. :
A ^^4 i327 \ A•32e9 326.598 !329 J I 328.596 ;
/ \ '^A^A—^^^A^^—A^^^^^^^ ' ^ ^^^^^^^^JV^^^/^^^^V^w^v^^^^^^ •
18131213.
89.7-1 ysm' 1239. ;
^^————331 J ^ 338.599333 ; I 332.599 ;
'._^^^ ^ i V . - - ;-_^______ I1813 ;1583. !
18e.9n ^ Jir'0'5' 1S2*. I
333 | I 332.688 !
335 J \ 334.688 I
_ - — ---T-- --,^^- - i - - ^-T-——r-- , :-i , — ,_=.. r. , |968 988 1888 1828 1848 1068 1888 1180 SCAN
24183 24133 25l83 25;33 26S83 26i33 27i83 27l33 TIME
' 0 0 Ii
3 i: i 5 0 0MIOWSS CHROHATOGRM1S DflTAl 3859 11 SCANS 358 TO 1100 '81/22/8S 14l58l88 CflLIf 3845 t6 :SWLEl DIOXIH SAMPLE CF983382 2UL 4We JK W .COOS.) 6BM SP2338 7e/2>219»2B>24W6 ry. ,RAMXl G 1,1188 LflBELl N 2,10.0 QUflHt A 2. 2.8 J 8 BflSEl U 29, 3 ,-| ;
1818 0596. 0
41.4-, 2^6- . ° 68S. ;
327 . I 326.S98 ;329 I l ' 328.598
^^^y sst^mf^mi ^~"__—^^^J^^j ^--^f^^l'^f^^^^-f^^^f^^^^^^^'——^^^^V^^A^^-^^hA I
' — - - l e e s ' ~ ~ r- I: 1232. !
84.3-, 5?2- 1232. !
1 A ^"'^ |331 J I 338.399 •333 ' I I 332.599 .
9SG I \ 1087 '2B. / \ 24. ;
; i_ -.1——-. — — , - a — — — 4 - / v - f___^_4- - I - - . - - -———,- '^-___| ', ~ ~~ ~ 1889 ;
' 188.8-, ^ ^^^r0^5 IW!- i
333 ( 1 332.688 >335 ' 1 1 334.689 '- L.._.... JL-,^ -.-.-..._. i
960 988 1888 1828 1848 1869 1888 1188 SCAN :: 24183 24133 25:83 25l33 26i03 26l33 27!B3 27,33 TIME *; C 0 0
£ i 9 5 0 0HIOHASS CMROIWTOGRflnS DATAl 3850 «1 SCANS 95B TO 11B9 VS
: 01/22/85 HiSSiee CALI) 3845 K r^SflfFLEl OIIW1N SflHPLE DF9e3382 2>JL 4089 JK t^CONDS.I EM SP2338 78^>21B(2B>24Me 2RflHixi cieee.iB2e LAGELI N 2. s.e wiMi A 1, 4.e J e BASE) u 29, 3 S
69.4-1 i 25.I 1093 ' J
256. 1 B ? ' I t ^ l * f l i A A 2S5-577
^AA^^U^ |
iee.0-i i 36.1816 A
TS.B-i lm2, i , 2 7 . !
T' 1 i j
^^UM^^^ \368 388 1000 1820 1049 1060 1080 1100 SCMI :
24(03 24(33 23(83 25(33 25)03 26:33 27)03 27)33 TIME :
L 0 0
i 05 00
42.1-1
2S6258 "
85.6-1
319321
109.9-1
321323 "
MIDIttSS CHROttTOGRAHS DAT61/22/85 16t21iee CALSflMPLEl TCOO HETHOO STANDAliD »1 2U. CfiSCONDS. l BW SP2338 TVQ'l\W3S>V/eKRWGEt G t.llW LABELl H 2,18.0 OU
1
1S
•K
670.2622.x^W.2/ ^
1 \ 320.536| 1 322.S96
- -^ . ^ ^ ^ - - -.960 988 1000 1020 1040 1060 1080 1100 SCAN
24:03 24(33 25l03 2Sl33 26i03 26l33 27|03 27l33 TIME
Al 3852 *1 SCANS 959 TO 1100 •fII 3845 16 t<
X*3089 4000 W i-l0
JAHl A -2, 2.0 J 0 BASEl U 20i 3 0010 0280.V4- 293./> S» 1010 iS7 , „ ,,7
H= 278 ^ - C ' • J 3
\\ A= 8651 2S5.577
I 257.377
889 t— 1-
l65.
["• 5-1009 ^ - ., ., S76.\ A: ^ ' 76
I ? , 318. SSS1 ; -- %'^7 ^••ae
0
S ^" ^ : 0 0HIDHftSS CHROWTOGIWIMS MTfti 3852 «1 SCTNS 958 TO 1188 ....01/22/85 16l21l80 CALI! 3845 K R iSBMPLEl TCDD METHOO STflMMM) tl 211. CflSE»3989 4889 W i_, •COHDS.I 68M SP2330 78^>21Be29>248e6 SRflNGEl G 1,1188 LABELl H 2.18.0 WWl A 2, 2.8 J 9 BASE) U 28, 3 0
1818 0288.
42.1-, lj,14• 283. ;
256 J I 255.577258 ' j \ 257.577 ,
^^^J^f^^^\^/^/\-^f>/\/' ' "ny^V^ i A^A^^/^^A^^/s^^^^^^/s^A^ ;-+-——-——T———-——I ^g l —— - i - -——h——.——>——-————r ,
565. •85.6. 29.8- 576. \
319 | I 318.S95 i321 / 1 328.596 i
^f,_^.p^ , ^ ,,. > *. ^ ,, ^ ^v^ . . ^ »._^ ^ . ^-.A,.——^_ -^.^^__^—^^
^^f'^^———-r—————""'""IBM' ' " • ~"'——~————r" -————-» \67B. i
1B9.8-1 26?2' 673. ;
321 | I 320.596 >.323 ' 1 1 322.596
' -,-^ ^~-,_H.^__- -- .- 1960 988 1880 1028 1048 1869 1088 1100 SCAN ;
24l03 24l33 25)83 25:33 26:83 26l33 27l83 27i33 TIME i' c i ^ ;
9 £ h ? 0 0MIDMASS CHROMOTOGRWIS DATAl 3852 11 SCANS 950 TO 1109 .„ :
61/22/85 16121190 CALIl 3843 »6 w.SWLEl TCtX) METHOD STANDARD «1 2UL CflSE»3989 4000 W '. >COHDS.l 6ai SP2338 78^>210e2e> 24086 T ' :RflHGEl G 1-liee LABELl N 2,10.9 QUANi A 2, 2.8 J 8 BASE) U 2B, 3 Q 1
1899 0 ;
1264. ':43.4-, GB3E. -^ - ^^ ^_ ;
327 . J i 326.596323 I I 328.598
[^————^-p--,———^^ V - . - - , -^-^——————^-^ ^- I; 1888 i: 2382. ;; 88.8-, te?93- 2388. !
A ^^2^7 !
331 . / I 338.399 !
333 I I 332.399 :
——r————————— T - _ _^___ ——— ___- _-_^____ _
2931.188.8. « . ^.-^. . !
333 j \ 332.E88 :335 ' I 1 334.688
1 , , , / V , ^^.^^ i9E8 988 1888 1828 1848 1860 1988 1188 SCflN
24193 24133 25183 23l33 26:83 26l33 27l83 27l33 TIME
c.. 0 0 l
L£ ° 5 0 0niDNASS CHROHATOGRflHS DATAl 3854 *1 SCANS 350 TO 1106 r-Bl/22/85 l7l49l88 CflLIl 3845 «6 r-SAMPLE) TCDD SAMPLE! DFB833e9 2UL CflSE»3889 4988 W '-1 :
CTBS.l E»l SP2338 7ft >218«28> 24885 0 ;RflHGEi G 1 ,1180 LABELl H 2,18.8 aUAHl A •t, 2.8 J 8 BASE l U 28, 3 <=> ;
1883 0 - '38. ;
83.8-1 1?4- i . 31. I
i fl i ^ H ft d II 11 'i236 fl 1 I l A 1 1 i iJl A A (1 All til 1 ij « lIlH f 1 255.377 '
"|AkJM^^ Ii 996 i: 33.
188.8-1 1?5- 37.
^ 'N^4^^ I1679 i
<uIffX —* i' 97.3-1 i l^ 4B9. 36. i
321 A rt J l l f l i X I h il/t I ft i I i \ \ 328.596 !
968 998 IBee 1829 1848 1868 1888 1188 SCAN I24l83 24833 23)83 25)33 26l83 26l33 27:63 27l33 TIME
( 0 0
HlWtGS CWCtMTOGRflMS DATA) 3854 *1 SCANS 358 TO 118091/22/85 17l43iee CALtl 3845 t6SMPLEl TCDC SAMPLE* CFM3383 2UL CASE*3889 4880 WCONDS.l C8M SP2338 78/2>21M2fl>248»6RftHCEl G 1,1199 LABEL) H 2.16.0 QUAHt A 2. 2.9 J 9 BASEl U 20, 3
L- 0 • 0
6 £ P 5 0 0niOMASS CHROHATOCRAHS DATAl 3855 tl SCflHS 939 TO 110861/22/S5 18l32l9e CALIi 3845 «6 0,SAMPLE) TCOO SAWLE* OFBe3315 2UL CASE13889 4089 W .COHDS.I EOH SP2338 7e/2>21892fl>24966 ^RftNGEl G l.liee LABELl H 2,10.9 OUWl A 2, 2,9 J 8 BASEl U 20, 3 0• lees o
; 453. 0; <3-8-| 173' j57 ; .^o ^- • F/1 469.
256 I I - o, ^ 255,577258 ) 1 257.577
__ — - - , ^ ^ — — _ _ - _
885.84.8-1 4roe' „,, , 987,
J^-^Z^ n ^--^/Wfllo./ *' .»" " •""^ i- •°"^ A ••••""1: IIA ./r""i-.-^^x^^^^^^^ \ ' / ^-^^-i—^^^ - i ^ \lees1B58. xo.<»'!= /"•
198.0-, 4442. .^-<». ,
321 J \ 329.596\ 1^ . 322.596
1 . . ^ V ,X , ^ ^ A
960 988 1600 1020 1040 1060 1889 1109 SCAN24)83 24)33 25)83 25(33 26:83 26:33 27lB3 27(33 TIK
' | L 0 0
0 \! G S 0 0HIUttSS CHROMflTOGRflMS DftTfll 3855 11 SCANS 350 TO 1180Bl/22/83 18l32iee CflLIl 3843 •6 0SAHPLEl TCOO SAMPLE* DFee331S 2UL CflSE»3B89 4880 W 00CONOS.I eed SP2338 78^2>21W2e>24M6 '-I
: RANGEl G LllM LflBELl H 2.10.8 QUAHl ft 2, 2.0 J 0 BflSEl U 26, 3 01988 0
1841 .-/o: /ti3( '-'45.4-1 4y7• 1854.
' 3 2 7 / I 326.598; 329 ) \ 32B.598
^S^ -. ^_.7 - ''" / -»h^»M^^_^______J'•?S-J^^y^^^_^S^^S^^—J^^V/fs^^^J^^^^J^M^A^—^n^S*<*> \-rf*fc. \— J^ \
: — T ' 1 9 8 7 ' '1942.
84.1-1 91^E7• 19S2.^i^- .- if-ns ftW \ _ni .wy -- -itW ^-i^ \ W '
: 331 ) I 338.599333 I I 332.599
- - , — — ^^^ - -——,__ - _
: 2297.1B8.B-1 1%B8• 2328.
333 f I 332.688: 335 ' 1 1 334.688
968 988 1888 1828 1848 1BE8 1888 1188 SCON: 24iB3 24l33 25l83 25:33 26:83 26l33 27l83 27|33 TIfC
: G 0 0
If 8 S 0 0MIOMftSS CHROIWTOGfWS DATAl 3856 H1BB5 SCANS 950 TO 1188 ^81/22/85 19t21iee CALIl 3845 «6 oOSAMPLEl TCOO METHOO 5TAHMRD *2 2UL CASE«3e89 4009 W '-1COOS. I EW SP2338 78/2>21W2B>24fl96 0RAHGEl C l.lim UCELl H 2,10.0 QUANi A -2, 2.0 J 0 BASEl U 29, 3 g
168135.KA •i qq wq
^ "lh4^ a5! laa a- 7;a s= lea7 J^ / s CT100.0-1 J^*3 - / 7 H=17 ^ | b3"
s- leesH' 24
; see "MB leee 1920 i84e leee iesa nee SCHN, 24lB3 24|33 25l83 2Sl33 26:03 26:33 27:03 27l33 TIME
C 0 0
6 V £ c; 0 0HIOHASS CHROHATOGRAHS DATA] 3856 11 SCANS 9 5 8 1 0 1 1 6 6 ...01/22/83 19:21(00 CM-ll 3845 »6 cv
SAMPLE) TCOO METHOD STANDARD *2 2UL CASEt3883 4800 UY _-CONDS.I 601 SP2338 7e^>21K2B>24a« QRANGE) G Mim LABELl H 2,16.8 gUAHl A 2, 2.8 J 8 BASEl U 29, 3 Q
1991 0
35.
'Ih^xjrt! ^ ^198.9-, i 63.
319 . 1 1 [\ A I (\ || i A 310.393^kA^v^^ "•"
9E8 988 1888 1829 1848 1860 1888 1188 SCAN24:83 24)33 2Sl83 25(33 26:83 26l33 27l83 27833 TINE
; C 0 0
£ 17 8 5 0 0MIGMASS CHROMftTOGRflMS DATAl 3856 *1 SCWS 950 TO 1188 _91/22/85 19i21iee CALIl 3845 •6 „-SAMPLE) TCIB METHOD STANDARD *2 2UL CftSE»3889 4000 UY w
COtCS.l 60M SP2338 79/2>2iee28>24e96 0RAHGEl G 1,1100 LftBELl N 2,1B.B BUftMl fl 2, 2.0 J 8 BftSEl U 28, 3 Q
1B07 0835.
43.5-1 3^2- 863.
327 . / I 326.53B329 J 1 328.598
-^^A^.-^^ - — -._^f»i —i \^^-_ • \ •f^^v~^f^—^~^^\/^'—^^-~i—^-^^->^/*^~^/^~^^\A^s.' 1 8 0 6 ' ' r
1642.83.1-1 71^5' 1650.
n ^^-^'"i J^- .0^1. 331 . / I --T 338.S99' 3 3 3 I 1 3>'' 332.S99
I 1——t^=- . =--^- ^————i-^^- --l—— T- ^--p—i -- , ^^ -l.1 1974., 180.0-1 B3!9' 1986.
333 ) ( 332.600335 ' 1 1 334.600
960 980 1800 1020 1048 1060 1080 1100 SCAH24:03 24l33 25l83 25«33 26!03 26s33 27103 27l33 TIME
; C 0 0
'ff 17 8 S 0 0HIDMASS CHROHTOGRAHS DATA: 3857 11888 SCANS 938 TO 110891/22/85 20182108 CALIl 384S «6 •VSAMPLE! TCDO SAMPLE* DF983322 2UL CASE*3089 4888 W w
COMB.« EaN SP2338 78/2>2t8C9>248e6 3RANGE: G 1,1188 LABELl N 2,18.8 QUAHl A -2, 2.8 J 8 BASE) U 2B, 3 §
0
87.8-1 i 43.
ei.B-, , . sr ^^ ^-'"
\ ''V^ ssS= 1088H= 14
188.8-1 J A° 5 49.
321 X l A A i t l l l 328.336
^^AMW'MM^^^ ^9G8 988 1889 1828 1848 1968 1BS8 1188 SCAH
24183 24133 25:83 2Sl33 26:83 26:33 27l83 27l33 TIHE/ r'\ '•"•'' '^-1 •—/
5 17 e s o oMIDMftSS CHROMflTOGRWIS DATAi 3857 «1 SCANS 350 TO 1109 „-,91/22/85 20(02108 CALIl 3845 «6 —SAHPLEl TCCO SAMPLE* DF9e3322 2UL CASEt3889 4800 W _JCOMB. l 6811 SP2338 79/2>2iee29> 24886 0RANGEi G i-iiee Lpea-i H 2.ie.e axus A 2, 2.9 J a BASEI u a, 3 o
1806 0775.
42.8-1 44^4' 787.( I S' 1886( I H' 773
327 0.3786 ^^329 J 328.598
^J~-'\~^ys^>A>^^J^<\ ^^^a^^ '\<^y^^^A -/\/ / ^— - -w^^"~v^^w^ y>^^-_AA.' 1 8 0 6 '
; 1497.88.4-1 6?>19• -,-, 1588.
f\ 773 1 £- 'SOV5I \ jH-.OW 73V -
3St; 331 1 338.599
333 ' / I 332.599
1806 ' — ~ ' -
1868.188.8^ "I?4- 1876.
333 J \ 332.6B8335 ' I I 334.688
968 988 1888 1828 1848 1960 1888 1188 SCON24:83 24l33 25:83 25(33 26(83 26x33 27:83 27:33 TIME
ۥ 0 0
9 t7 8 S 0 0NIDMASS CHROHATOGRAHS DATAl 3864 tl SCANS 958 TO 1180Bl/23/85 IllSliee CflLI: 3868 *S COSATPLEl 010XIN SAMPLE DFe03316 2UL 4006 JK COCONDS.l 501 SP2338 78/2>2ie829>240*6 ^RflNGEl G hliee LftBal N 2,19.9 QUANt A 2, 8.8 J 8 BftSEl U 28, 3 °
1828 °CI 0
1811
i l ^ Sx Oo's^ )s* i I
"18271E3.
89.8-1 5?3' 212.J 1811 ^1 not 67; H
32?-I ...^"^T \ ^ jy:§|
ih^^^v^^1828218.
iee.8-i e¥' 236.1812 1 1183. J l
321 . 2?3' I 328.S96323 / • 1 1 1 A 322.396
^L ^^Vw^AA^Aw^9EB 990 1888 1828 1849 1068 1880 1180 SCAN
24:03 24i33 25)83 25l33 26:83 26:33 27:03 27l33 TIME
0 0
L V 8 5 0 0HIDHASS CHRCMftTOCRmS DATAl 3864 *1 SCANS 958 TO 119091/23/85 lltSliee CALIf 3868 »5 t^SflHPLEl DtOXIH SAMPLE CF983316 2UL 4900 JK °0COOS. I 6m SP2338 , 2>218829>24W6 '-IRAHGEl G l.liee LABELl H 2,18.8 SWHl A 2. 2.8 J 8 BASEl U 29, 3 °
1811 §1811. °
43.6-1 *y9' 1828.
327 / 1 326.598329 ' ; 1 328.598
1818: 1869.
88.8-1 "it?7' 1888.
331 I I 338.S99333 ' ; I 332.599
1 ^ - , / V - - , ^^18892368.
188.8-1 l1?9' 2368.
333 I I 332.688335 J 1 334.688
968 988 1888 1828 1848 1B6B 1888 1188 SUN24l83 24l33 25l83 25l33 26i83 26l33 27l83 27l33 TIME
C; 0 Q
8 fr 8 S 0 0HIDHASS CHROHATOGRAMS DATAl 3865 tl SCANS 388 TO 1068 oc
91/23/85 12lS8l8e CALIl 3860 »5 . 00
SAMPLEl D10X1N SAMPLE DF0e331G DUP 2UL 4000 JK S: CONOS.l Em SP2338 7e/2>21M29>24e»6 -: RAHGEl G 1,1190 LABEL) N 2.18.8 OUANi A 3, E.B J 8 BASE) U 29, 3 <-,
1811 1023172. 178.
3S.9-1 5S1• 5?6- %_7 * 31,% 19S.
2S6 . / l / \ 25S.S77259 / \ / \ 257.S77
c^^^^^^^'—\-yy^—^v^^^Ay^, - ^ , -^ - - , ,; 88-8] 1%- 1^' ^s-m 47B-
319 / 1 / I 318.S9S: 321 / I / \ 32B.396
<^^ - ^—s /'"'''-' /''-"—^•—s/— -v^-—^^" •^^-—s/ i i . ^--^^^-^1811 1^Jac 3i»*T^B" •• 1<J JAl J
189.8n ISO.*0"" ' 1^1- M3.
321 / \ / \ 32B.S96323 / \ / \ 322.S96
388 990 ieee icie 1020 leae 1040 iese ieeo SCAN24f33 24:49 25(03 25ll8 2Sl33 2Sf48 26lB3 26ll8 26l33 TIME
^ 0 0
6 17 8 S 0 0MIDHASS CHROMTOGMHS DflTfti 3865 »t SCONS 958101189Bl/23/85 12(58)88 CfiLII 3860 »5 gySAMPLEl DIOXIH SAMPLE CFM3316 DUP 2UL 4808 JK COCOHCS.I 681 SP233e 78^>21W28>24ee6 <-<KMIKI G i-iiee utB-i M z.ie.e euwi A 2, 2.e J e BASEI u a, 3 o
IBll 0' 2253. 0' 17^ 1BE31.*.1^--''••I1i 3f.Z-l rt 22r2>
327 1 1 326.396329 ' ) 1 328.598
! ' ijia ' r - i i —-r—- i; 4835.' 79.2-1 21*7' 4848.
331 . 1 ( 338.599 !' 333 ' f I 332.599
1818: 6898.
188.8-, aras- 6112. •
333 I I 332.688 || 335- 1 1 334.688 !
; 1 . . .A I- 968 988 1888 1828 1848 1860 1888 1188 SCAN \' 24)83 24)33 25)83 25)33 26)83 26l33 27)83 27)33 TIME |
I '- 0 ^ I
0 S P 5 0 0MIDHASS CHROMATOGRAM DATA: 3867 *1 SCftHS 989 TO 1048 °01/23/85 14)26)08 CflLIl 3S6B IS 2SAMPLE) D10KIN SAMPLE OF0e3312 2UL 4008 JK T 'COMB. i OTtI SP2338 7e/2>21Be29> 24086 = ;RftHGEl Giet9>lB12 LflBELl N 2,19.B QUAHl A 2, 4.9 J B BflSEl U 26, 3 Q
128.
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: ^2- . 0.2^. Jll
2K _ 1 2S5.577; 258 | 257.577 i
988 999 1090 1810 1020 1030 1040 SCTN24(33 24;48 25l03 25f 18 25:33 23)48 26)03 TIME
0 U
I S 8 S 0 0MIDW6S CHROMATOGRflH MTAl 3867 tl SCANS 98B TO 1940 ^81/23/65 14:26188 CflLIl 3869 »5 2SflMPLEl D10XIN SMPLE CFBB3312 2UL 4009 JK ' •COWS. l eW SP2338 7e^>21W2e>2W8S 5RflNGEi Gleie.ieiz LABELI H 2,ie.e QUANI A 2. 4.e J a BASEI u a, 3 g
329.; iee.e-1 'i?5- 367.
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sse 930 ieee ieie 1920 ie3e ie4B SCAN24:33 24148 25103 25:18 25:33 25(48 26:03 TIME
C 0 0 !
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iBll c_i338.
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980 990 1808 1910 1020 1030 1049 SOW24l33 24l48 25l83 25)18 25:33 25(48 26l03 TIME
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1911 ;535. '
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