DOMINO SUGAR SITE E 317-329 KENT AVENUE BROOKLYN, NEW YORK Remedial Investigation Report NYC VCP Site Number: 15CVCP002K Prepared for: Two Trees Management, LLC 45 Main Street, Suite 602 Brooklyn, NY 11201 Prepared by: EBC 1808 Middle Country Road Ridge, NY 11961 September 2014 Environmental Business Consultants
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DOMINO SUGAR SITE E
317-329 KENT AVENUE BROOKLYN, NEW YORK
Remedial Investigation Report
NYC VCP Site Number: 15CVCP002K
Prepared for:
Two Trees Management, LLC
45 Main Street, Suite 602
Brooklyn, NY 11201
Prepared by:
EEBB CC
1808 Middle Country Road
Ridge, NY 11961
September 2014
Environmental Business Consultants
REMEDIAL INVESTIGATION REPORT
TABLE OF CONTENTS
LIST OF ACRONYMS
CERTIFICATION
EXECUTIVE SUMMARY ...................................................................................................... i
FIGURES Figure 1 - Site Location Map Figure 2 - Site Boundary Map Figure 3 - Redevelopment Plan Figure 4 - Surrounding Land Use Figure 5 - Site Sampling Locations Figure 6 - Soil Exceedences Map Figure 7 - Groundwater Exceedences Map Figure 8 - Soil Vapor Detections
ATTACHMENTS Attachment A - Soil Boring Logs Attachment B - Groundwater Sampling Logs Attachment C - Soil Gas Sampling Logs Attachment D - Laboratory Reports in Digital Format Attachment E - EHI 2004 Phase I Report Attachment F - Emteque 2012 Phase I Report Attachment G - Nova 2004 Phase III Report Attachment H - AKRF 2009 Phase II Report
LIST OF ACRONYMS Acronym Definition
AOC Area of Concern
CAMP Community Air Monitoring Plan
COC Contaminant of Concern
CPP Citizen Participation Plan
CSM Conceptual Site Model
DER-10 New York State Department of Environmental Conservation Technical Guide 10
FID Flame Ionization Detector
GPS Global Positioning System
HASP Health and Safety Plan
HAZWOPER Hazardous Waste Operations and Emergency Response
IRM Interim Remedial Measure
NAPL Non-aqueous Phase Liquid
NYC VCP New York City Voluntary Cleanup Program
NYC DOHMH New York City Department of Health and Mental Hygiene
NYC OER New York City Office of Environmental Remediation
NYS DOH ELAP
New York State Department of Health Environmental Laboratory Accreditation Program
OSHA Occupational Safety and Health Administration
DOMINO SUGAR SITE E 317-329 Kent Avenue, Brooklyn, NY Remedial Investigation Report
vi Environmental Business Consultants
EEBB CC 1808 Middle Country Road Ridge, NY 11961
Phone 631.504.6000 Fax 631.924.2870
above GQS included benzo(a)anthracene (max of 0.49 µg/L), benzo(b)fluoranthene (max
of 0.48 µg/L), benzo(k)fluoranthene (0.08 µg/L), bis(2-ethylhexyl)phthalate (max of 42
µg/L), chrysene (max. of 0.49 µg/L), and indeno(1,2,3-cd)pyrene (3.7 µg/L) in one or
more of the three groundwater samples collected by EBC in 2014 and the groundwater
sample collected by AKRF in 2008. Dissolved metals present in groundwater at levels
above GQS included iron, lead, magnesium, manganese, selenium and sodium. The
presence of some of these metals in groundwater, specifically those that are common
salinity indicators, can be attributed to the proximity to the East River and the intrusion of
road salting.
7. Soil vapor samples collected during the 2014 EBC RI indicated petroleum related VOCs
and chlorinated VOCs were present at low concentrations. Petroleum-related VOCs
(BTEX) were detected at a maximum concentration of 141.43 μg/m3. Overall the highest
reported concentrations was for acetone (maximum of 7693 μg/m3). Trichloroethylene
(TCE) was detected in three of the five soil vapor samples at a concentration ranging
from 241 to 61.2 μg/m3. The New York State Department of Health (NYSDOH) Final
Guidance on Soil Vapor Intrusion (October 2006) notes mitigation is the recommended
action for a TCE concentrations above 250 μg/m3 in soil gas.Tetrachloroethylene (PCE)
was detected in all five soil vapor samples, and ranged in concentration from 2.03 to 28.3
μg/m3. Carbon tetrachloride was detected within three of the five soil vapor samples at a
maximum concentration of 0.566 μg/m3, and 1,1,1-trichloethylene (TCA) was detected in
three of the five soil vapor samples at a maximum concentration of 3.54 μg/m3. The PCE,
carbon tetrachloride and TCA concentrations are below the monitoring level ranges
established within the NYSDOH Final Guidance on Soil Vapor Intrusion.
DOMINO SUGAR SITE E 317-329 Kent Avenue, Brooklyn, NY Remedial Investigation Report
1
EEBB CC Environmental Business Consultants 1808 Middle Country Road
Ridge, NY 11961
Phone 631.504.6000 Fax 631.924.2870
REMEDIAL INVESTIGATION REPORT 1.0 SITE BACKGROUND
Two Trees Management LLC has applied to enroll in the New York City Voluntary Cleanup
Program (NYC VCP) to investigate and remediate a 1.32-acre Site located at 317 to 329 Kent
Avenue in the Williamsburg-South Side section of Brooklyn, New York. Site E will be
redeveloped with a 15-story mixed use building that will have 5 cellar levels for community
facility space and parking. The portion of the RI work conducted on Site E was performed
between April 2, 2014, and May 8, 2014. This RIR summarizes the nature and extent of
contamination and provides sufficient information for establishment of remedial action
objectives, evaluation of remedial action alternatives, and selection of a remedy that is protective
of human health and the environment consistent with the use of the property pursuant to RCNY§
43-1407(f).
1.1 Site Location and Current Usage
Domino Sugar Site E is located at 317 to 329 Kent Avenue in the Williamsburg-South Side
section of Brooklyn, New York, and is currently identified as a portion of Block 2428, Lot 1 on
the New York City Tax Map. Figure 1 shows the Site location. Lot 1 is a 57,600 ft2 lot located
on the east side of Kent Avenue between South 3rd Street to the north and South 4th Street to the
south. Site E has been undeveloped and utilized for parking for employees of the Domino Sugar
Company and other sugar refinery companies since the 1940's. The former parking lot is
currently being utilized as The Brooklyn Bike Park, a recreational bicycle track.
Site A is currently bordered by South 3rd Street to the north, South 4th Street to the south,
several residential apartment buildings and a scrap metal facility to the east and Kent Avenue to
the west. Site A is an rectangular shaped lot consisting of 180 ft of street frontage on Kent
Avenue and 320 ft of street frontage on both South 3rd Street and South 4th Street, for a total of
approximately 57,600 ft2.A map of the site boundary is shown on Figure 2.
1.2 Proposed Redevelopment Plan
Redevelopment of the former Domino Sugar properties (Block 2414, Lot 1 and Block 2428, Lot
1) will include four new mixed-use buildings (Sites A, B, D, E), adaptively reuse the existing
DOMINO SUGAR SITE E 317-329 Kent Avenue, Brooklyn, NY Remedial Investigation Report
2 Environmental Business Consultants
EEBB CC 1808 Middle Country Road Ridge, NY 11961
Phone 631.504.6000 Fax 631.924.2870
landmarked Refinery building (Site F), create a one acre inland green space to be called Domino
Square (Site C) and develop a new waterfront park.
The proposed future use of Site E will consist of a new 15-story mixed-use building with 5 cellar
levels. The new building will have a total floor area of approximately 774,003 ft2, consisting of
approximately 20,612 ft2 of retail space, a 178,718 ft2 parking facility, and 114,369 ft2 of
community facility uses. This building would rise to a maximum height of approximately 435
feet.
The lowest cellar level (C5) will occupy the majority of the Site E footprint, with the exception
of areas in the northwest and southwest corners. Cellar level C5 will consist of three separate
community facility areas that will be used as a soccer field, gymnasium, and an aquatic center.
Cellar level C5 will also have four elevator pits, and five stairwells. The next lowest cellar level
(C4) will consist of a locker room for the community facilities on C5, and an additional
recreation space for the community facility. Cellar level C3 will consist of a storage room and
office space for the community facilities, and several large mechanical rooms. Cellar levels C2
and C1 will consist of an underground parking garage, but will also contain the the electrical
room, telecom room, plumbing room, gas meter room, water and sewer room, fire protection
room, two compactor rooms, bike storage room, men's and women's lockers and lunch room, the
building supers' office, workshop and storage room.
The building's first floor will consist of three retail spaces on the west end of the building, the
building's residential lobby, and additional parking. The second floor will have apartments along
the west end of the building, additional ground level retail spaces along the eastern end of South
3rd Street and South 4th Street, and additional parking spaces within the middle of the building.
The third floor will consist of residential apartments along Kent Avenue, South 3rd Street and
South 4th Street, and parking within the center of the building. After the 3rd floor, the building
divides into two separate towers. The two residential towers rise from the 4th floor to the 12th
floor before joining again at the 13th floor. The 4th through 15th floors consist solely of
residential apartments.
DOMINO SUGAR SITE E 317-329 Kent Avenue, Brooklyn, NY Remedial Investigation Report
3 Environmental Business Consultants
EEBB CC 1808 Middle Country Road Ridge, NY 11961
Phone 631.504.6000 Fax 631.924.2870
Assuming an excavation depth of approximately 52 ft for the entire 57,600 ft2 lot for
construction of the new building's five cellar levels, a total of approximately 111,000 cubic yards
(166,400 tons) of soil will require excavation. Layout of the proposed site development is
presented in Figure 3. The current zoning designation is C6-2. The proposed use is consistent
with existing zoning for the property.
Layout of the proposed site development is presented in Figure 3. The current zoning designation
is C6-2. The proposed use is consistent with existing zoning for the property.
1.3 Description of Surrounding Property
The area immediately surrounding Site E consists of the former Domino Sugar facility buildings
to west, and industrial buildings to the north, south and east. Figure 4 shows the surrounding land
usage of the adjacent properties listed below as well as additional properties located up to 500
feet away from the Site. No hospitals, schools or daycare facilities are located within a 250 ft
radius of the Site.
Surrounding Property Usage
Direction Property Description
North – Opposite side of South 3rd Street
Block 2415, Lot 1 - 315 Kent Avenue Developed with a 1-story industrial/manufacturing building
Block 2415, Lot 7501 - 29 South 3rd Street Developed a new 4-story, 26-unit residential apartment building.
Block 2415, Lot 38 - 37 South 3rd Street Developed a 4-story, 8-unit residential apartment building, with first floor retail space.
Block 2415, Lots 36 and 37 - 41 and 43 South 3rd Street Two small undeveloped lots
South – Opposite side of South 4th Street
Block 2441, Lot 8 - 331 Kent Avenue Developed with a 2-story commercial/office building consisting of 3 commercial spaces and one residential unit.
Block 2441, Lot 12 - 34 South 4th Street Developed with a 1-1/2-story industrial/manufacturing building constructed in 1996.
Block 2441, Lot 15 - 48 South 4th Street Developed with former 2-1/2 story industrial/manufacturing building converted into residential apartments.
DOMINO SUGAR SITE E 317-329 Kent Avenue, Brooklyn, NY Remedial Investigation Report
4 Environmental Business Consultants
EEBB CC 1808 Middle Country Road Ridge, NY 11961
Phone 631.504.6000 Fax 631.924.2870
Block 2441, Lot 21 - 47 South 5th Street Developed with a small one-story industrial/manufacturing building converted into a bar/restaurant.
East – Adjacent Property
Block 2428, Lot 24 - 56 South 3rd Street Developed with a new 4-story residential/apartment building. Block 2428, Lot 30 - 55 South 4th Street Developed with a one industrial/manufacturing building utilized for scrap metal sorting/storage. Block 2428, Lots 36 and 27 - 376 and 378 Wythe Avenue Two thin lots developed with multi-family walk-ups with rear yards.
West –
Block 2414, Lot 1 (SITE C) - 314 Kent Avenue Former industrial buildings associated with the Domino Sugar Factory.
DOMINO SUGAR SITE E 317-329 Kent Avenue, Brooklyn, NY Remedial Investigation Report
5 Environmental Business Consultants
EEBB CC 1808 Middle Country Road Ridge, NY 11961
Phone 631.504.6000 Fax 631.924.2870
2.0 SITE HISTORY
2.1 Past Uses and Ownership
Two Phase I Environmental Site Assessment (ESA) Reports have been completed for Sites A, B,
C, D, E and F. Both reports are summarized below.
2.1.1 Phase I Environmental Site Assessment Report (EHI, 2004)
A Phase I Environmental Site Assessment Report was completed by Environmental Health
Investigations, Inc. in 2004, for Sites A, B, C, D, E, and F. A copy of the Phase I Report is
attached in Attachment E. The Phase I Environmental Site Assessment Report identified the
vacant lot as parking for Domino Sugar employees, but did not thoroughly investigate the Site E
history prior to use as parking. The Phase I Report did not reveal any on-Site Recognized
Environmental Conditions in connection with Site E.
2.1.2 Phase I Environmental Site Assessment Report (Emteque LLC, 2012)
A Phase I Environmental Site Assessment Report was completed by Emteque LLC in 2012, for
Sites A, B, C, D, E, and F. A copy of the Phase I Report is attached in Attachment F. Historic
Sanborn maps provided within the report were reviewed to determine the following historic use
of Site E:
1887 Sanborn Map - The 1887 Sanborn map indicates Site E formerly consisted of multiple
20 or 25ft wide lots along South 3rd Street and South 4th Street that were developed with 3
story houses. The northwest corner of Site E was developed with a 9-story building used as
the kiln and filter house for the Havemeyer & Elder Sugar Refinery. The building contained
numerous coal fired boilers and two large smoke stacks.
1904 Sanborn Map - The 1904 Sanborn map indicates the sugar refinery operation
expanded to several of the lots along South 4th Street. The facility was now operated under
the name American Sugar Refinery. It consisted of a 7-story building at 29 to 35 South 4th
Street that housed 16 engines, a 2-story building at 38-40 South 3rd Street that was utilized
for coal storage, a 2 and 4-story building at 42-44 South 3rd Street that housed numerous
boilers, and a 10-story building at 317-323 Kent Avenue that consisted of 14 boilers, and was
utilized as the kiln and filter house. Several of the 3-story houses at 37, 39 and 41 South 4th
DOMINO SUGAR SITE E 317-329 Kent Avenue, Brooklyn, NY Remedial Investigation Report
6 Environmental Business Consultants
EEBB CC 1808 Middle Country Road Ridge, NY 11961
Phone 631.504.6000 Fax 631.924.2870
Street are labeled as pattern storage. A small lot at 325 Kent Avenue is developed with three
buildings labeled as a plating room, paints, and saw-dust house.
1918 Sanborn Map - The 1918 Sanborn map indicates the American Sugar Refining
Company of NY utilized nearly the entire footprint of Site E, with the exception of a 3-story
apartment building w/first floor store on the corner of South 4th Streetn and Kent Avenue
(329 Kent Avenue). Site E is shown as being developed with the following:
o Section G - Consists of two buildings and an open space area - 1) 317 - 323 Kent
Avenue - A 9-story building with a basement that was used as the kiln and filter
house, 2) 32-36 South 3rd Street - labeled as the old boiler house, and as vacant and
partly removed, and 3) 38-40 South 3rd Street - a coal yard.
o Section Q - Consists of three buildings 1) 46-54 South 3rth Street - A 68ft high
building consisting of six large syrup tanks, 2) 42-44 South 3rd Street - a 2-story
building used for storage of bone black and 3) 49 South 4th Street - a 1-story building
labeled as a filling house.
o Section P - Developed with two adjacent seven story buildings. The building at 37-49
South 4th Street was labeled as the filter house, and the building at 29-35 South 4th
Street was labeled as the filler house.
o Section T - Developed with a former 3-story residential building labeled as the
pattern shop, and an open lot likely used for parking.
1935 Sanborn Map - The 1935 Sanborn map appears to label most buildings as the same as
those depicted on the 1918 Sanborn map, but most buildings are labeled as vacant.
1947, 1950 and 1965 Sanborn Maps - The 1947, 1950 and 1965 Sanborn maps depict the
majority of Site E as being undeveloped with the exception of two 3-story buildings on the
corner of South 4th Street and Kent Avenue (327 and 329 Kent Avenue).
1977-2007 Sanborn Maps - All Sanborn maps from 1977 to 2007 depict the entire footprint
of Site E as undeveloped.
DOMINO SUGAR SITE E 317-329 Kent Avenue, Brooklyn, NY Remedial Investigation Report
7 Environmental Business Consultants
EEBB CC 1808 Middle Country Road Ridge, NY 11961
Phone 631.504.6000 Fax 631.924.2870
The Emteque LLC Phase I Environmental Site Assessment Report identified multiple recognized
environmental conditions in connection with Lot 1. However, only one is believed to be
associated with Site E:
Historic / Urban fill (Site A) - Emteque LLC stated previous environmental investigations
have identified soil and groundwater contamination attributed to previous filling of the
property prior to development. Emteque LLC recommended additional sampling of soil and
groundwater to fully characterize the site to aid in the development and implementation both
engineering and institutional controls. Additionally, further characterization of the site soil
will be required prior to its off-site disposal.
2.2 Previous Investigations
EBC was provided digital copies of previous investigations performed at the Site. A summary of
each is provided below.
2.2.1 Phase III Environmental Site Assessment (Nova, 2004)
A Phase III Environmental Site Assessment was performed at Site E, as well as the remainder of
the Domino Sugar property (Sites A, B, C, D and F) by Nova Consulting & Engineering, LLC
(Nova) in June of 2004. The Phase III Environmental Site Assessment included the installation
of five evenly spaced soil borings across Site E. From each of the five soil borings, Nova
retained soil samples in 4 ft intervals from 0-4 feet below grade to 16 to 20 feet below grade or
refusal.
Each of the soil samples were submitted for laboratory analysis of VOCs, and SVOCs, and the
soil samples retained from soil borings B-4 and B-5 were also submitted for laboratory analysis
of RCRA metals. The laboratory results are compared to NYSDEC Unrestricted Use Soil
Cleanup Objectives (UUSCOs) and Restricted Residential Use Soil Cleanup Objectives
(RRSCOs) as presented in 6NYCRR Part 375-6.8 and CP51 on Tables 2a, 3a, and 5. Figure 6
shows the location and posts the values for soil that exceeds UUSCOs and RRSCOs. A copy of
the report is included in Attachment G.
DOMINO SUGAR SITE E 317-329 Kent Avenue, Brooklyn, NY Remedial Investigation Report
Vinyl Chloride 20 900 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 1.5 U 1.4 U 1.5 U 1.5 U
Notes:* - 6 NYCRR Part 375-6 Remedial Program Soil Cleanup Objectives
ND - Not-detected
BDL - Delow Detection Limit
Dash - Not Analyzed
J - The value is estimated. This flag is used: a) on form 1 when the compound is reported above the MDL, but below the PQL, and b) on the Tentatively Identified Compounds (TIC) form for all compounds identified.
S - This compound is a solvent that is used in the laboratory. Laboratory contamination is suspected if concentration is less than five times the reporting level.
N - The concentration is based on the response fo the nearest internal. This flag is used on the TIC form for all compounds identified.
U - The compound was anlayzed for but not detected at or above the MDL.
Bold/highlighted- Indicated exceedance of the NYSDEC UUSCO Guidance Value
Bold/highlighted- Indicated exceedance of the NYSDEC RRSCO Guidance Value
Notes:* - 6 NYCRR Part 375-6 Remedial Program Soil Cleanup Objectives
Dash- Not Analyzed
BDL - Delow Detection Limit
ND - Not-detected
J - The value is estimated. This flag is used: a) on form 1 when the compound is reported above the MDL, but below the PQL, and b) on the Tentatively Identified Compounds (TIC) form for all compounds identified.
S - This compound is a solvent that is used in the laboratory. Laboratory contamination is suspected if concentration is less than five times the reporting level.
N - The concentration is based on the response fo the nearest internal. This flag is used on the TIC form for all compounds identified.
U - The compound was anlayzed for but not detected at or above the MDL.
Bold/highlighted- Indicated exceedance of the NYSDEC UUSCO Guidance Value
Bold/highlighted- Indicated exceedance of the NYSDEC RRSCO Guidance Value
Heptachlor 42 2,100 0.36 U 0.34 U 0.36 U 0.38 U < 1.8 1.8 < 1.9 1.9 < 1.9 1.9 < 1.8 1.8 < 1.8 1.8 < 1.8 1.8 < 1.8 1.8
Heptachlor epoxide 0.34 U 0.32 U 0.34 U 0.36 U < 1.8 1.8 < 1.9 1.9 < 1.9 1.9 < 1.8 1.8 < 1.8 1.8 < 1.8 1.8 < 1.8 1.8
Methoxychlor 4.1 U 3.9 U 14 J 4.3 U < 7.1 7.1 < 92 92 < 7.6 7.6 < 22 22 < 7.3 7.3 < 7.0 7 < 18 18
Toxaphene 13 U 12 U 13 U 13 U < 180 180 < 190 190 < 190 190 < 180 180 < 180 180 < 180 180 < 180 180
Notes:* - 6 NYCRR Part 375-6 Remedial Program Soil Cleanup Objectives
ND - Not-detected
Dash - Not analyzed
N - The concentration is based on the response fo the nearest internal. This flag is used on the TIC form for all compounds identified.
Bold/highlighted- Indicated exceedance of the NYSDEC UUSCO Guidance Value
Bold/highlighted- Indicated exceedance of the NYSDEC RRSCO Guidance Value
(1-3')(16-18')
AKRF Phase IIAKRF Phase II
S - This compound is a solvent that is used in the laboratory. Laboratory contamination is suspected if concentration is less than five times the reporting level.
J - The value is estimated. This flag is used: a) on form 1 when the compound is reported above the MDL, but below the PQL, and b) on the Tentatively Identified Compounds (TIC) form for all compounds identified.
AKRF Phase II AKRF Phase IICOMPOUNDNYSDEC Part 375.6
Notes:* - 6 NYCRR Part 375-6 Remedial Program Soil Cleanup Objectives
ND - Not-detected
Dash - Not analyzed
BDL - Below Detection Limit
J - The value is estimated. This flag is used: a) on form 1 when the compound is reported above the MDL, but below the PQL, and b) on the Tentatively Identified Compounds (TIC) form for all compounds identified.
S - This compound is a solvent that is used in the laboratory. Laboratory contamination is suspected if concentration is less than five times the reporting level.
N - The concentration is based on the response for the nearest internal. This flag is used on the TIC form for all compounds identified.
U - The compound was anlayzed for but not detected at or above the MDL.
Bold/highlighted- Indicated exceedance of the NYSDEC UUSCO Guidance Value
Bold/highlighted- Indicated exceedance of the NYSDEC RRSCO Guidance Value
6/23/2004 6/23/2004 6/23/2004 6/23/2004
SB-12
NOVA Phase III
B-5
(0-4') (4-8') (8-12') (12-16')
NOVA Phase III
(1-3') (16-18')
ResultsResultsResultsResults
SB-13
6/23/2004 6/23/2004
mg/Kg
11/7/2008 11/7/2008
mg/Kg mg/Kg
(1-3')
mg/Kg
(27-29')
11/7/2008
AKRF Phase II
11/7/2008
AKRF Phase II
ResultsResults
6/23/2004
mg/Kg mg/Kg
6/23/2004
mg/Kg mg/Kg
AKRF Phase II
COMPOUND
NYSDEC Part 375.6 Unrestricted Use
Soil Cleanup Objectives
NYDEC Part 375.6 Restricted
Residential Soil Cleanup
Objectives*
EBC RI(0-2')
mg/Kg
EBC RI EBC RI EBC RI EBC RI EBC RI
COMPOUND
NYSDEC Part 375.6 Unrestricted Use
Soil Cleanup Objectives
NYDEC Part 375.6 Restricted
Residential Soil Cleanup
Objectives*
mg/Kg
B-3
(0-4') (4-8') (8-12') (12-16')
NOVA Phase III
mg/Kg
NOVA Phase III
mg/Kg mg/Kg
NOVA Phase III NOVA Phase IIINOVA Phase III NOVA Phase III
U - The compound was anlayzed for but not detected at or above the MDL.
N - The concentration is based on the response fo the nearest internal. This flag is used on the TIC form for all compounds identified.
Bold/highlighted- Indicated exceedance of the NYSDEC Groundwater Standard
S - This compound is a solvent that is used in the laboratory. Laboratory contamination is suspected if concentration is less than five times the reporting level.
5/8/2014
µg/L µg/L µg/L
Results Results Results
4/9/2014 4/9/2014
COMPOUNDNYSDEC Groundwater
Quality Standards
J - The value is estimated. This flag is used: a) on form 1 when the compound is reported above the MDL, but below the PQL, and b) on the Tentatively Identified Compounds (TIC) form for all compounds identified.
U - The compound was anlayzed for but not detected at or above the MDL.
N - The concentration is based on the response fo the nearest internal. This flag is used on the TIC form for all compounds identified.
Bold/highlighted- Indicated exceedance of the NYSDEC Groundwater Standard
S - This compound is a solvent that is used in the laboratory. Laboratory contamination is suspected if concentration is less than five times the reporting level.
J - The value is estimated. This flag is used: a) on form 1 when the compound is reported above the MDL, but below the PQL, and b) on the Tentatively Identified Compounds (TIC) form for all compounds identified.
4/9/2014 4/9/2014 5/8/2014
µg/L µg/L µg/L
Compound NYSDEC Groundwater Quality Standards
E-MW1 E-MW2 E-MW3
EBC RI EBC RI EBC RI
TABLE 8Site E
Former Domino Sugar SiteBrooklyn, New York
Groundwater Analytical ResultsPesticides / PCBs
SB-13
AKRF Phase II
11/7/2008
µg/L
Results Result RL
PCB-1016 0.09 0.084 U < 0.069 0.069
PCB-1221 0.09 0.36 U < 0.069 0.069
PCB-1232 0.09 0.084 U < 0.069 0.069
PCB-1242 0.09 0.084 U < 0.069 0.069
PCB-1248 0.09 0.084 U < 0.069 0.069
PCB-1254 0.09 0.051 U < 0.069 0.069
PCB-1260 0.09 0.053 U < 0.069 0.069
PCB-1262 0.09 - < 0.069 0.069
PCB-1268 0.09 - < 0.069 0.069
4,4-DDD 0.3 0.012 U < 0.14 0.14
4,4-DDE 0.2 0.011 U < 0.14 0.14
4,4-DDT 0.11 0.016 U < 0.14 0.14
a-BHC 0.94 - < 0.069 0.069
a-Chlordane 1.94 0.0089 U < 0.14 0.14
Alachlor 0.0054 U < 1.0 1
Aldrin 0.0092 U < 0.021 0.021
b-BHC 0.04 0.0084 U < 0.069 0.069
Chlordane 0.05 - < 1.4 1.4
d-BHC 0.04 0.0064 U < 0.069 0.069
Dieldrin 0.004 0.011 U < 0.021 0.021
Endosulfan I 0.0052 U < 0.14 0.14
Endosulfan II 0.011 U < 0.14 0.14
Endosulfan Sulfate 0.015 U < 0.14 0.14
Endrin 0.016 U < 0.14 0.14
Endrin aldehyde 5 0.010 U < 0.14 0.14
Endrin ketone 0.012 U < 0.14 0.14
gamma-BHC 0.05 0.0060 U < 0.069 0.069
g-Chlordane 0.0054 U < 0.14 0.14
Heptachlor 0.04 0.0084 U < 0.14 0.14
Heptachlor epoxide 0.03 0.0065 U < 0.14 0.14
Methoxychlor 35 0.10 U < 1.4 1.4
Toxaphene 0.24 U < 3.5 3.5
Notes:U - The compound was anlayzed for but not detected at or above the MDL.
DASH - Not analyzed
Bold/highlighted- Indicated exceedance of the NYSDEC Groundwater Standard
COMPOUNDNYSDEC Groundwater
Quality Standards
E-MW3
EBC RI
5/8/2014
µg/L
TABLE 9Site E
Former Domino Sugar SiteBrooklyn, New York
Groundwater Analytical ResultsMetals
SB-13
AKRF Phase II
11/7/2008
mg/L
Results Result RL Result RL
Aluminum NS 61 2.43 0.01 3.68 0.01
Antimony 0.003 0.0088 U < 0.003 0.003 < 0.003 0.003
Cadmium 0.005 0.0028 U < 0.004 0.004 < 0.004 0.004
Calcium NS 141 110 0.01 124 0.01
Chromium 0.05 0.5 0.004 0.001 0.008 0.001
Cobalt NS 0.099 < 0.005 0.005 < 0.005 0.005
Copper 0.2 0.58 0.007 0.005 0.014 0.005
Iron 0.5 178 2.89 0.01 3.89 0.01
Lead 0.025 0.16 < 0.002 0.002 0.031 0.002
Magnesium 35 65 31.2 0.01 30.9 0.01
Manganese 0.3 3 2.65 0.05 0.229 0.005
Mercury 7.00E-04 0.00009 U < 0.0002 2.00E-04 < 0.0002 2.00E-04
Nickel 0.1 0.39 0.014 0.004 0.005 0.004
Potassium NS 23 12.9 0.1 11.8 0.1
Selenium 0.01 0.0053 J 0.009 0.004 0.007 0.004
Silver 0.05 0.0013 U < 0.005 0.005 < 0.005 0.005
Sodium 2 213 237 1 249 1
Thallium 0.0005 0.008 U < 0.002 0.002 < 0.002 0.002
Vanadium NS 0.21 < 0.010 0.01 < 0.010 0.01
Zinc 2 8 < 0.010 0.01 0.031 0.01
Notes:Dash - Not Analyzed
U - The compound was anlayzed for but not detected at or above the MDL. NS - No Standard
Bold/highlighted- Indicated exceedance of the NYSDEC Groundwater Standard
mg/L
J - The value is estimated. This flag is used: a) on form 1 when the compound is reported above the MDL, but below the PQL, and b) on the Tentatively Identified Compounds (TIC) form for all compounds identified.
U - The compound was anlayzed for but not detected at or above the MDL.
Bold/highlighted- Indicated exceedance of the NYSDEC Groundwater Standard
J - The value is estimated. This flag is used: a) on form 1 when the compound is reported above the MDL, but below the PQL, and b) on the Tentatively Identified Compounds (TIC) form for all compounds identified.
4/9/2014 4/9/2014 5/8/2014
mg/L mg/L mg/L
COMPOUNDNYSDEC Groundwater
Quality Standards
E-MW1 E-MW2 E-MW3
EBC RI EBC RI EBC RI
TABLE 11Site E
Former Domino Sugar SiteBrooklyn, New York
Soil Gas Analytical ResultsVolatile Organic Compounds
NYSDOH Soil OutdoorBackground Levels
(µg/m3) (a) (µg/m3) (b) Result RL Result RL Result RL Result RL Result RL
Notes:NA No guidance value or standard available(a) Final Guidance for Evaluating Soil Vapor Intrusion in the State of New York. October 2006. New York State Department of Health.(b) NYSDOH Guidance for Evaluating Soil Vapor Intrusion in the State of New York, February 2005, Summary of Background Levels for Selected Compounds (NYSDOH Database, Outdoor values)Value detected above NYSDOH Air Guidance Value of 5 µg/m3, which according to Soil Vapor/Indoor Air Matrix 1 would require at a minimum, mitigation. Value detected above NYSDOH Air Guidance Value of 100 µg/m3, which according to Soil Vapor/Indoor Air Matrix 2 would require at a minimum, mitigation.
E-SG4(µg/m³)
E-SG5(µg/m³) COMPOUNDS
NYSDOH Maximum Sub-Slab Value
E-SG1(µg/m³)
E-SG2(µg/m³)
E-SG3(µg/m³)
FIGURES
EEBBCCEnvironmental Business Consultants Phone 631.504.6000
Fax1808 Middle Country Road. Ridge. NY 11961 631.924.2780
Attn: Mr. Charles B. Sosik, P.G.Environmental Business Consultants1808 Middle Country RdRidge NY 11961-2406
Project ID: DOMINO SUGAR SITE E
Sincerely yours,
Laboratory DirectorPhyllis Shiller
Enclosed are revised Analysis Report pages. Please replace and discard the original pages. If you have any questions concerning this testing, please do not hesitate to contact Phoenix Client Services at ext. 200.
This laboratory is in compliance with the NELAC requirements of procedures used except where indicated.
This report contains results for the parameters tested, under the sampling conditions described on the Chain Of Custody, as received by the laboratory.
All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments.
A scanned version of the COC form accompanies the analytical report and is an exact duplicate of the original.
Polychlorinated BiphenylsNDPCB-1016 35 05/02/14 AW SW 8082ug/Kg35NDPCB-1221 35 05/02/14 AW SW 8082ug/Kg35NDPCB-1232 35 05/02/14 AW SW 8082ug/Kg35NDPCB-1242 35 05/02/14 AW SW 8082ug/Kg35NDPCB-1248 35 05/02/14 AW SW 8082ug/Kg35NDPCB-1254 35 05/02/14 AW SW 8082ug/Kg35NDPCB-1260 35 05/02/14 AW SW 8082ug/Kg35NDPCB-1262 35 05/02/14 AW SW 8082ug/Kg35NDPCB-1268 35 05/02/14 AW SW 8082ug/Kg35
QA/QC Surrogates97% DCBP 05/02/14 AW 30 - 150 %%82% TCMX 05/02/14 AW 30 - 150 %%
Pesticides - SoilND4,4' -DDD 2.5 05/05/14 CE SW8081ug/Kg2.5ND4,4' -DDE 2.5 05/05/14 CE SW8081ug/Kg2.5ND4,4' -DDT 2.5 05/05/14 CE SW8081ug/Kg2.5NDa-BHC 1.8 05/05/14 CE SW8081ug/Kg1.8NDa-Chlordane 3.5 05/05/14 CE SW8081ug/Kg3.5NDAldrin 1.8 05/05/14 CE SW8081ug/Kg1.8NDb-BHC 1.8 05/05/14 CE SW8081ug/Kg1.8NDChlordane 21 05/05/14 CE SW8081ug/Kg21NDd-BHC 1.8 05/05/14 CE SW8081ug/Kg1.8NDDieldrin 1.8 05/05/14 CE SW8081ug/Kg1.8NDEndosulfan I 3.5 05/05/14 CE SW8081ug/Kg3.5NDEndosulfan II 3.5 05/05/14 CE SW8081ug/Kg3.5NDEndosulfan sulfate 3.5 05/05/14 CE SW8081ug/Kg3.5NDEndrin 1.8 05/05/14 CE SW8081ug/Kg1.8NDEndrin aldehyde 3.5 05/05/14 CE SW8081ug/Kg3.5NDEndrin ketone 1.8 05/05/14 CE SW8081ug/Kg1.8NDg-BHC 1.8 05/05/14 CE SW8081ug/Kg1.8NDg-Chlordane 3.5 05/05/14 CE SW8081ug/Kg3.5NDHeptachlor 1.8 05/05/14 CE SW8081ug/Kg1.8NDHeptachlor epoxide 1.8 05/05/14 CE SW8081ug/Kg1.8NDMethoxychlor 7.0 05/05/14 CE SW8081ug/Kg7.0NDToxaphene 180 05/05/14 CE SW8081ug/Kg180
QA/QC Surrogates101% DCBP 05/05/14 CE 30 - 150 %%90% TCMX 05/05/14 CE 30 - 150 %%
VolatilesND1,1,1,2-Tetrachloroethane 7.3 04/11/14 U SW8260ug/Kg1.2ND1,1,1-Trichloroethane 7.3 04/11/14 U SW8260ug/Kg1.5ND1,1,2,2-Tetrachloroethane 7.3 04/11/14 U SW8260ug/Kg1.0ND1,1,2-Trichloroethane 7.3 04/11/14 U SW8260ug/Kg0.71ND1,1-Dichloroethane 7.3 04/11/14 U SW8260ug/Kg1.4
Page 2 of 6 Ver 2
E-SB6 15-17Phoenix I.D.: BG30367
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
ND1,1-Dichloroethene 7.3 04/11/14 U SW8260ug/Kg1.6ND1,1-Dichloropropene 7.3 04/11/14 U SW8260ug/Kg1.4ND1,2,3-Trichlorobenzene 7.3 04/11/14 U SW8260ug/Kg1.5ND1,2,3-Trichloropropane 7.3 04/11/14 U SW8260ug/Kg1.0ND1,2,4-Trichlorobenzene 7.3 04/11/14 U SW8260ug/Kg1.5ND1,2,4-Trimethylbenzene 7.3 04/11/14 U SW8260ug/Kg1.0ND1,2-Dibromo-3-chloropropane 7.3 04/11/14 U SW8260ug/Kg2.0ND1,2-Dibromoethane 7.3 04/11/14 U SW8260ug/Kg1.9ND1,2-Dichlorobenzene 7.3 04/11/14 U SW8260ug/Kg0.80ND1,2-Dichloroethane 7.3 04/11/14 U SW8260ug/Kg0.64ND1,2-Dichloropropane 7.3 04/11/14 U SW8260ug/Kg1.0ND1,3,5-Trimethylbenzene 7.3 04/11/14 U SW8260ug/Kg0.96ND1,3-Dichlorobenzene 7.3 04/11/14 U SW8260ug/Kg1.1ND1,3-Dichloropropane 7.3 04/11/14 U SW8260ug/Kg0.77ND1,4-Dichlorobenzene 7.3 04/11/14 U SW8260ug/Kg1.2ND2,2-Dichloropropane 7.3 04/11/14 U SW8260ug/Kg1.2ND2-Chlorotoluene 7.3 04/11/14 U SW8260ug/Kg1.2ND2-Hexanone 36 04/11/14 U SW8260ug/Kg3.3ND2-Isopropyltoluene 7.3 04/11/14 U SW8260ug/Kg 11.0ND4-Chlorotoluene 7.3 04/11/14 U SW8260ug/Kg0.84ND4-Methyl-2-pentanone 36 04/11/14 U SW8260ug/Kg1.7NDAcetone 50 04/11/14 U SW8260ug/Kg7.2NDAcrylonitrile 15 04/11/14 U SW8260ug/Kg4.1NDBenzene 7.3 04/11/14 U SW8260ug/Kg1.4NDBromobenzene 7.3 04/11/14 U SW8260ug/Kg0.95NDBromochloromethane 7.3 04/11/14 U SW8260ug/Kg1.1NDBromodichloromethane 7.3 04/11/14 U SW8260ug/Kg0.90NDBromoform 7.3 04/11/14 U SW8260ug/Kg1.0NDBromomethane 7.3 04/11/14 U SW8260ug/Kg5.6NDCarbon Disulfide 7.3 04/11/14 U SW8260ug/Kg1.2NDCarbon tetrachloride 7.3 04/11/14 U SW8260ug/Kg0.84NDChlorobenzene 7.3 04/11/14 U SW8260ug/Kg1.1NDChloroethane 7.3 04/11/14 U SW8260ug/Kg1.7NDChloroform 7.3 04/11/14 U SW8260ug/Kg1.3NDChloromethane 7.3 04/11/14 U SW8260ug/Kg3.8NDcis-1,2-Dichloroethene 7.3 04/11/14 U SW8260ug/Kg1.6NDcis-1,3-Dichloropropene 7.3 04/11/14 U SW8260ug/Kg0.79NDDibromochloromethane 7.3 04/11/14 U SW8260ug/Kg0.82NDDibromomethane 7.3 04/11/14 U SW8260ug/Kg0.92NDDichlorodifluoromethane 7.3 04/11/14 U SW8260ug/Kg1.9NDEthylbenzene 7.3 04/11/14 U SW8260ug/Kg1.3NDHexachlorobutadiene 7.3 04/11/14 U SW8260ug/Kg1.5NDIsopropylbenzene 7.3 04/11/14 U SW8260ug/Kg1.4NDm&p-Xylene 7.3 04/11/14 U SW8260ug/Kg2.9NDMethyl Ethyl Ketone 44 04/11/14 U SW8260ug/Kg6.3NDMethyl t-butyl ether (MTBE) 15 04/11/14 U SW8260ug/Kg2.0NDMethylene chloride 7.3 04/11/14 U SW8260ug/Kg1.2NDNaphthalene 7.3 04/11/14 U SW8260ug/Kg2.0NDn-Butylbenzene 7.3 04/11/14 U SW8260ug/Kg1.3
Page 3 of 6 Ver 2
E-SB6 15-17Phoenix I.D.: BG30367
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
NDn-Propylbenzene 7.3 04/11/14 U SW8260ug/Kg1.3NDo-Xylene 7.3 04/11/14 U SW8260ug/Kg2.8NDp-Isopropyltoluene 7.3 04/11/14 U SW8260ug/Kg1.0NDsec-Butylbenzene 7.3 04/11/14 U SW8260ug/Kg1.4NDStyrene 7.3 04/11/14 U SW8260ug/Kg2.1NDtert-Butylbenzene 7.3 04/11/14 U SW8260ug/Kg1.2NDTetrachloroethene 7.3 04/11/14 U SW8260ug/Kg1.5NDTetrahydrofuran (THF) 15 04/11/14 U SW8260ug/Kg 16.6NDToluene 7.3 04/11/14 U SW8260ug/Kg1.2NDtrans-1,2-Dichloroethene 7.3 04/11/14 U SW8260ug/Kg1.5NDtrans-1,3-Dichloropropene 7.3 04/11/14 U SW8260ug/Kg1.5NDtrans-1,4-dichloro-2-butene 15 04/11/14 U SW8260ug/Kg14NDTrichloroethene 7.3 04/11/14 U SW8260ug/Kg1.5NDTrichlorofluoromethane 7.3 04/11/14 U SW8260ug/Kg1.6NDTrichlorotrifluoroethane 7.3 04/11/14 U SW8260ug/Kg1.1NDVinyl chloride 7.3 04/11/14 U SW8260ug/Kg2.4
QA/QC Surrogates105% 1,2-dichlorobenzene-d4 04/11/14 U 70 - 130 %%100% Bromofluorobenzene 04/11/14 U 70 - 130 %%114% Dibromofluoromethane 04/11/14 U 70 - 130 %%100% Toluene-d8 04/11/14 U 70 - 130 %%
Per 1.4.6 of EPA method 8270D, 1,2-Diphenylhydrazine is unstable and readily converts to Azobenzene. Azobenzene is used for the calibration of 1,2-Diphenylhydrazine.
Please be advised that the NY unrestricted soil criteria for chromium is based on hexavalent chromium and trivalent chromium.
All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments.
Phyllis Shiller, Laboratory DirectorMay 07, 2014
1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.B = Present in blank, no bias suspected.
If there are any questions regarding this data, please call Phoenix Client Services at extension 200.This report must not be reproduced except in full as defined by the attached chain of custody.
Reviewed and Released by: Greg Lawrence, Assistant Lab Director
RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level LOD=Limit of Detection MDL=Method Detection Limit
Additional 8270 criteria: 20% of compounds can be outside of acceptance criteria as long as recovery is at least 10%. (Acid surrogates acceptance range for aqueous samples: 15-110%, for soils 30-130%)
Additional 8260 criteria: 10% of LCS/LCSD compounds can be outside of acceptance criteria as long as recovery is 40-160%.
Comment:
l = This parameter is outside laboratory lcs/lcsd specified recovery limits.m = This parameter is outside laboratory ms/msd specified recovery limits.r = This parameter is outside laboratory rpd specified recovery limits.
MS - Matrix SpikePhyllis Shiller, Laboratory Director
If there are any questions regarding this data, please call Phoenix Client Services at extension 200.
May 07, 2014MS Dup - Matrix Spike Duplicate
RPD - Relative Percent Difference
LCS - Laboratory Control SampleLCSD - Laboratory Control Sample Duplicate
NC - No Criteria
Intf - Interference
Page 8 of 8
Sample Criteria Exceedences ReportWednesday, May 07, 2014 Page 1 of 2
Phoenix Laboratories does not assume responsibility for the data contained in this report. It is provided as an additional tool to identify requested criteria exceedences. All efforts are made to ensure the accuracy of the data (obtained from appropriate agencies). A lack of exceedence information does not necessarily suggest conformance to the criteria. It is ultimately the site professional's responsibility to determine appropriate compliance.
The samples in this delivery group were received at 4°C.(Note acceptance criteria is above freezing up to 6°C)
Page 1 of 1
1
Sarah - Phoenixlabs
From: Sarah - Phoenixlabs [[email protected]]Sent: Wednesday, April 30, 2014 11:10 AMTo: 'Shannon - Phoenixlabs'Subject: Can you take off hold BG30367Attachments: GBG30363-ChainofCustody-1.pdf
Importance: High
Please run per Dominick BG30367 for PCB and Pest. I will scan to COC
This laboratory is in compliance with the NELAC requirements of procedures used except where indicated.
This report contains results for the parameters tested, under the sampling conditions described on the Chain Of Custody, as received by the laboratory.
A scanned version of the COC form accompanies the analytical report and is an exact duplicate of the original.
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
Comments:
Per 1.4.6 of EPA method 8270D, 1,2-Diphenylhydrazine is unstable and readily converts to Azobenzene. Azobenzene is used for the calibration of 1,2-Diphenylhydrazine.
1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.
If there are any questions regarding this data, please call Phoenix Client Services at extension 200.This report must not be reproduced except in full as defined by the attached chain of custody.
Reviewed and Released by: Bobbi Aloisa, Vice President
RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level LOD=Limit of Detection MDL=Method Detection Limit
Page 6 of 15 Ver 1
Sample Information Custody InformationMatrix:Location Code:Rush Request:P.O.#:
Collected by:Received by:Analyzed by:
GROUND WATEREBC72 Hour
04/09/14SWsee "By" below
Laboratory Data
E-MW2
Phoenix ID: BG31852
04/11/140:00
17:36
Parameter ResultRL/PQL Units Date/Time By Reference
FOR: Attn: Mr. Charles B. Sosik, P.G.Environmental Business Consultants1808 Middle Country RdRidge NY 11961-2406
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
Comments:
Per 1.4.6 of EPA method 8270D, 1,2-Diphenylhydrazine is unstable and readily converts to Azobenzene. Azobenzene is used for the calibration of 1,2-Diphenylhydrazine.
1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.
If there are any questions regarding this data, please call Phoenix Client Services at extension 200.This report must not be reproduced except in full as defined by the attached chain of custody.
Reviewed and Released by: Bobbi Aloisa, Vice President
RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level LOD=Limit of Detection MDL=Method Detection Limit
Page 12 of 15 Ver 1
Sample Information Custody InformationMatrix:Location Code:Rush Request:P.O.#:
Collected by:Received by:Analyzed by:
GROUND WATEREBC72 Hour
04/09/14SWsee "By" below
Laboratory Data
TRIP BLANK
Phoenix ID: BG31853
04/11/140:00
17:36
Parameter ResultRL/PQL Units Date/Time By Reference
FOR: Attn: Mr. Charles B. Sosik, P.G.Environmental Business Consultants1808 Middle Country RdRidge NY 11961-2406
1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.
If there are any questions regarding this data, please call Phoenix Client Services at extension 200.This report must not be reproduced except in full as defined by the attached chain of custody.
Reviewed and Released by: Bobbi Aloisa, Vice President
RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level LOD=Limit of Detection MDL=Method Detection Limit
Additional 8270 criteria: 20% of compounds can be outside of acceptance criteria as long as recovery is at least 10%. (Acid surrogates acceptance range for aqueous samples: 15-110%, for soils 30-130%)
$8260DP25R Trichloroethene 524 1.0 ug/LBG31851 NY / TAGM - Volatile Organics / Groundwater Standards 5$8260DP25R 1,2-Dibromo-3-chloropropane 0.04ND 1.0 ug/LBG31851 NY / TOGS - Water Quality / GA Criteria 0.04$8260DP25R 1,2-Dibromoethane 0.0006ND 1.0 ug/LBG31851 NY / TOGS - Water Quality / GA Criteria 0.0006$8260DP25R 1,2-Dichloroethane 0.6ND 2.0 ug/LBG31851 NY / TOGS - Water Quality / GA Criteria 0.6$8260DP25R Hexachlorobutadiene 0.5ND 1.0 ug/LBG31851 NY / TOGS - Water Quality / GA Criteria 0.5$8260DP25R Trichloroethene 524 1.0 ug/LBG31851 NY / TOGS - Water Quality / GA Criteria 5$8260DP25R 1,2,3-Trichloropropane 0.04ND 1.0 ug/LBG31851 NY / TOGS - Water Quality / GA Criteria 0.04$DP8270-SIMF Nitrobenzene 0.4ND 1.0 ug/LBG31851 NY / TOGS - Water Quality / GA Criteria 0.4$DP8270-SIMF Hexachlorobutadiene 0.5ND 1.0 ug/LBG31851 NY / TOGS - Water Quality / GA Criteria 0.5$DP8270-SIMF Benzidine 5ND 10 ug/LBG31851 NY / TOGS - Water Quality / GA Criteria 5$DP8270-SIMR Benz(a)anthracene 0.0020.03 0.02 ug/LBG31851 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$DP8270-SIMR Benz(a)anthracene 0.0020.03 0.02 ug/LBG31851 NY / TOGS - Water Quality / GA Criteria 0.002$DP8270-SIMR Chrysene 0.0020.03 0.02 ug/LBG31851 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$DP8270-SIMR Chrysene 0.0020.03 0.02 ug/LBG31851 NY / TOGS - Water Quality / GA Criteria 0.002$DP8270-SIMR Benzo(b)fluoranthene 0.002ND 0.02 ug/LBG31851 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$DP8270-SIMR Benzo(b)fluoranthene 0.002ND 0.02 ug/LBG31851 NY / TOGS - Water Quality / GA Criteria 0.002$DP8270-SIMR Benzo(k)fluoranthene 0.002ND 0.02 ug/LBG31851 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$DP8270-SIMR Benzo(k)fluoranthene 0.002ND 0.02 ug/LBG31851 NY / TOGS - Water Quality / GA Criteria 0.002$DP8270-SIMR Benzo(a)pyrene 0.002ND 0.02 ug/LBG31851 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$DP8270-SIMR Indeno(1,2,3-cd)pyrene 0.002ND 0.02 ug/LBG31851 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$DP8270-SIMR Indeno(1,2,3-cd)pyrene 0.002ND 0.02 ug/LBG31851 NY / TOGS - Water Quality / GA Criteria 0.002AL-WM Aluminum 0.12.43 0.010 mg/LBG31851 NY / TOGS - Water Quality / GA Criteria 0.1D-AL Aluminum (Dissolved) 0.10.90 0.01 mg/LBG31851 NY / TOGS - Water Quality / GA Criteria 0.1DFE-WMDP Iron, (Dissolved) 0.30.88 0.01 mg/LBG31851 NY / TOGS - Water Quality / GA Criteria 0.3DMN-WMDP Manganese, (Dissolved) 0.32.89 0.053 mg/LBG31851 NY / TOGS - Water Quality / GA Criteria 0.3D-NA Sodium (Dissolved) 20255 1.1 mg/LBG31851 NY / TOGS - Water Quality / GA Criteria 20DTL-WMDP Thallium , (Dissolved) 0.0005BRL 0.001 mg/LBG31851 NY / TOGS - Water Quality / GA Criteria 0.0005FE-WMDP Iron 0.32.89 0.01 mg/LBG31851 NY / TOGS - Water Quality / GA Criteria 0.3MN-WMDP Manganese 0.32.65 0.050 mg/LBG31851 NY / TOGS - Water Quality / GA Criteria 0.3NA-WM Sodium 20237 1.0 mg/LBG31851 NY / TOGS - Water Quality / GA Criteria 20TL-WMDP Thallium - LDL 0.0005BRL 0.002 mg/LBG31851 NY / TOGS - Water Quality / GA Criteria 0.0005
$8260DP25R Trichloroethene 520 1.0 ug/LBG31852 NY / TAGM - Volatile Organics / Groundwater Standards 5$8260DP25R 1,2-Dichloroethane 0.6ND 2.0 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 0.6$8260DP25R 1,2-Dibromoethane 0.0006ND 1.0 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 0.0006$8260DP25R 1,2-Dibromo-3-chloropropane 0.04ND 1.0 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 0.04$8260DP25R 1,2,3-Trichloropropane 0.04ND 1.0 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 0.04$8260DP25R Trichloroethene 520 1.0 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 5$DP8270-SIMF Phenol 1ND 1.3 ug/LBG31852 NY / TAGM - Semi-Volatiles / Groundwater Standards 1$DP8270-SIMF Phenol 1ND 1.3 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 1$DP8270-SIMF Bis(2-chloroethyl)ether 1ND 1.3 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 1$DP8270-SIMF 2-Chlorophenol 1ND 1.3 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 1
Sample Criteria Exceedences ReportMonday, April 21, 2014 Page 2 of 3
$DP8270-SIMF 2-Methylphenol (o-cresol) 1ND 1.3 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 1$DP8270-SIMF 2-Nitrophenol 1ND 1.3 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 1$DP8270-SIMF 2,4-Dimethylphenol 1ND 1.3 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 1$DP8270-SIMF Bis(2-chloroethoxy)methane 5ND 6.3 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 5$DP8270-SIMF 2,4-Dichlorophenol 1ND 1.3 ug/LBG31852 NY / TAGM - Semi-Volatiles / Groundwater Standards 1$DP8270-SIMF 2,4-Dichlorophenol 1ND 1.3 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 1$DP8270-SIMF 4-Chloro-3-methylphenol 1ND 1.3 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 1$DP8270-SIMF Hexachlorocyclopentadiene 5ND 6.3 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 5$DP8270-SIMF 2,4,6-Trichlorophenol 1ND 1.3 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 1$DP8270-SIMF 2,4,5-Trichlorophenol 1ND 1.3 ug/LBG31852 NY / TAGM - Semi-Volatiles / Groundwater Standards 1$DP8270-SIMF 2,4,5-Trichlorophenol 1ND 1.3 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 1$DP8270-SIMF 4-Nitroaniline 5ND 6.3 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 5$DP8270-SIMF 2,6-Dinitrotoluene 5ND 6.3 ug/LBG31852 NY / TAGM - Semi-Volatiles / Groundwater Standards 5$DP8270-SIMF 2,6-Dinitrotoluene 5ND 6.3 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 5$DP8270-SIMF 3-Nitroaniline 5ND 6.3 ug/LBG31852 NY / TAGM - Semi-Volatiles / Groundwater Standards 5$DP8270-SIMF 3-Nitroaniline 5ND 6.3 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 5$DP8270-SIMF 2,4-Dinitrophenol 1ND 1.3 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 1$DP8270-SIMF Dibenzofuran 5ND 6.3 ug/LBG31852 NY / TAGM - Semi-Volatiles / Groundwater Standards 5$DP8270-SIMF 2,4-Dinitrotoluene 5ND 6.3 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 5$DP8270-SIMF 4-Nitrophenol 1ND 1.3 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 1$DP8270-SIMF 2-Nitroaniline 5ND 6.3 ug/LBG31852 NY / TAGM - Semi-Volatiles / Groundwater Standards 5$DP8270-SIMF 2-Nitroaniline 5ND 6.3 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 5$DP8270-SIMF 4,6-Dinitro-2-methylphenol 1ND 1.3 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 1$DP8270-SIMF Benzidine 5ND 5.6 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 5$DP8270-SIMF 3,3'-Dichlorobenzidine 5ND 6.3 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 5$DP8270-SIMR Benz(a)anthracene 0.0020.19 0.03 ug/LBG31852 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$DP8270-SIMR Benz(a)anthracene 0.0020.19 0.03 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 0.002$DP8270-SIMR Chrysene 0.0020.29 0.03 ug/LBG31852 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$DP8270-SIMR Chrysene 0.0020.29 0.03 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 0.002$DP8270-SIMR Benzo(b)fluoranthene 0.0020.29 0.03 ug/LBG31852 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$DP8270-SIMR Benzo(b)fluoranthene 0.0020.29 0.03 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 0.002$DP8270-SIMR Benzo(k)fluoranthene 0.0020.08 0.03 ug/LBG31852 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$DP8270-SIMR Benzo(k)fluoranthene 0.0020.08 0.03 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 0.002$DP8270-SIMR Benzo(a)pyrene 0.002ND 0.03 ug/LBG31852 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$DP8270-SIMR Indeno(1,2,3-cd)pyrene 0.0020.05 0 ug/LBG31852 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$DP8270-SIMR Indeno(1,2,3-cd)pyrene 0.0020.05 0 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 0.002AL-WM Aluminum 0.13.68 0.010 mg/LBG31852 NY / TOGS - Water Quality / GA Criteria 0.1D-AL Aluminum (Dissolved) 0.10.39 0.01 mg/LBG31852 NY / TOGS - Water Quality / GA Criteria 0.1D-NA Sodium (Dissolved) 20247 1.1 mg/LBG31852 NY / TOGS - Water Quality / GA Criteria 20DTL-WMDP Thallium , (Dissolved) 0.0005BRL 0.001 mg/LBG31852 NY / TOGS - Water Quality / GA Criteria 0.0005FE-WMDP Iron 0.33.89 0.01 mg/LBG31852 NY / TOGS - Water Quality / GA Criteria 0.3NA-WM Sodium 20249 1.0 mg/LBG31852 NY / TOGS - Water Quality / GA Criteria 20
Sample Criteria Exceedences ReportMonday, April 21, 2014 Page 3 of 3
PB-WM Lead 0.0250.031 0.002 mg/LBG31852 NY / TOGS - Water Quality / GA Criteria 0.025TL-WMDP Thallium - LDL 0.0005BRL 0.002 mg/LBG31852 NY / TOGS - Water Quality / GA Criteria 0.0005
$8260DP25R Hexachlorobutadiene 0.5ND 1.0 ug/LBG31853 NY / TOGS - Water Quality / GA Criteria 0.5$8260DP25R 1,2,3-Trichloropropane 0.04ND 1.0 ug/LBG31853 NY / TOGS - Water Quality / GA Criteria 0.04$8260DP25R 1,2-Dibromo-3-chloropropane 0.04ND 1.0 ug/LBG31853 NY / TOGS - Water Quality / GA Criteria 0.04$8260DP25R 1,2-Dibromoethane 0.0006ND 1.0 ug/LBG31853 NY / TOGS - Water Quality / GA Criteria 0.0006$8260DP25R 1,2-Dichloroethane 0.6ND 2.0 ug/LBG31853 NY / TOGS - Water Quality / GA Criteria 0.6$8260DP25R 1,3-Dichlorobenzene 3ND 5.0 ug/LBG31853 NY / TOGS - Water Quality / GA Criteria 3
Phoenix Laboratories does not assume responsibility for the data contained in this report. It is provided as an additional tool to identify requested criteria exceedences. All efforts are made to ensure the accuracy of the data (obtained from appropriate agencies). A lack of exceedence information does not necessarily suggest conformance to the criteria. It is ultimately the site professional's responsibility to determine appropriate compliance.
This laboratory is in compliance with the NELAC requirements of procedures used except where indicated.
This report contains results for the parameters tested, under the sampling conditions described on the Chain Of Custody, as received by the laboratory.
All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments.
A scanned version of the COC form accompanies the analytical report and is an exact duplicate of the original.
Polychlorinated BiphenylsNDPCB-1016 35 04/10/14 AW SW 8082ug/Kg35NDPCB-1221 35 04/10/14 AW SW 8082ug/Kg35NDPCB-1232 35 04/10/14 AW SW 8082ug/Kg35NDPCB-1242 35 04/10/14 AW SW 8082ug/Kg35NDPCB-1248 35 04/10/14 AW SW 8082ug/Kg35NDPCB-1254 35 04/10/14 AW SW 8082ug/Kg35NDPCB-1260 35 04/10/14 AW SW 8082ug/Kg35NDPCB-1262 35 04/10/14 AW SW 8082ug/Kg35NDPCB-1268 35 04/10/14 AW SW 8082ug/Kg35
QA/QC Surrogates38% DCBP 04/10/14 AW 30 - 150 %%41% TCMX 04/10/14 AW 30 - 150 %%
Pesticides - SoilND4,4' -DDD 2.6 04/14/14 CE SW8081ug/Kg2.6ND4,4' -DDE 2.6 04/14/14 CE SW8081ug/Kg2.6ND4,4' -DDT 2.6 04/14/14 CE SW8081ug/Kg2.6NDa-BHC 1.8 04/14/14 CE SW8081ug/Kg1.8NDa-Chlordane 3.5 04/14/14 CE SW8081ug/Kg3.5NDAldrin 1.8 04/14/14 CE SW8081ug/Kg1.8NDb-BHC 1.8 04/14/14 CE SW8081ug/Kg1.8NDChlordane 21 04/14/14 CE SW8081ug/Kg21NDd-BHC 1.8 04/14/14 CE SW8081ug/Kg1.8NDDieldrin 1.8 04/14/14 CE SW8081ug/Kg1.8NDEndosulfan I 3.5 04/14/14 CE SW8081ug/Kg3.5NDEndosulfan II 3.5 04/14/14 CE SW8081ug/Kg3.5NDEndosulfan sulfate 3.5 04/14/14 CE SW8081ug/Kg3.5NDEndrin 1.8 04/14/14 CE SW8081ug/Kg1.8NDEndrin aldehyde 3.5 04/14/14 CE SW8081ug/Kg3.5NDEndrin ketone 1.8 04/14/14 CE SW8081ug/Kg1.8NDg-BHC 1.8 04/14/14 CE SW8081ug/Kg1.8NDg-Chlordane 3.5 04/14/14 CE SW8081ug/Kg3.5NDHeptachlor 1.8 04/14/14 CE SW8081ug/Kg1.8NDHeptachlor epoxide 1.8 04/14/14 CE SW8081ug/Kg1.8NDMethoxychlor 7.1 04/14/14 CE SW8081ug/Kg7.1NDToxaphene 180 04/14/14 CE SW8081ug/Kg180
QA/QC Surrogates40% DCBP 04/14/14 CE 30 - 150 %%47% TCMX 04/14/14 CE 30 - 150 %%
VolatilesND1,1,1,2-Tetrachloroethane 9.3 04/11/14 U SW8260ug/Kg1.5ND1,1,1-Trichloroethane 9.3 04/11/14 U SW8260ug/Kg1.9ND1,1,2,2-Tetrachloroethane 9.3 04/11/14 U SW8260ug/Kg1.3ND1,1,2-Trichloroethane 9.3 04/11/14 U SW8260ug/Kg0.92ND1,1-Dichloroethane 9.3 04/11/14 U SW8260ug/Kg1.9
Page 2 of 49 Ver 1
E-SB1 0-2Phoenix I.D.: BG30363
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
ND1,1-Dichloroethene 9.3 04/11/14 U SW8260ug/Kg2.0ND1,1-Dichloropropene 9.3 04/11/14 U SW8260ug/Kg1.8ND1,2,3-Trichlorobenzene 9.3 04/11/14 U SW8260ug/Kg1.9ND1,2,3-Trichloropropane 9.3 04/11/14 U SW8260ug/Kg1.3ND1,2,4-Trichlorobenzene 9.3 04/11/14 U SW8260ug/Kg1.9ND1,2,4-Trimethylbenzene 9.3 04/11/14 U SW8260ug/Kg1.3ND1,2-Dibromo-3-chloropropane 9.3 04/11/14 U SW8260ug/Kg2.5ND1,2-Dibromoethane 9.3 04/11/14 U SW8260ug/Kg2.5ND1,2-Dichlorobenzene 9.3 04/11/14 U SW8260ug/Kg1.0ND1,2-Dichloroethane 9.3 04/11/14 U SW8260ug/Kg0.82ND1,2-Dichloropropane 9.3 04/11/14 U SW8260ug/Kg1.3ND1,3,5-Trimethylbenzene 9.3 04/11/14 U SW8260ug/Kg1.2ND1,3-Dichlorobenzene 9.3 04/11/14 U SW8260ug/Kg1.4ND1,3-Dichloropropane 9.3 04/11/14 U SW8260ug/Kg0.99ND1,4-Dichlorobenzene 9.3 04/11/14 U SW8260ug/Kg1.5ND2,2-Dichloropropane 9.3 04/11/14 U SW8260ug/Kg1.6ND2-Chlorotoluene 9.3 04/11/14 U SW8260ug/Kg1.5ND2-Hexanone 47 04/11/14 U SW8260ug/Kg4.2ND2-Isopropyltoluene 9.3 04/11/14 U SW8260ug/Kg 11.3ND4-Chlorotoluene 9.3 04/11/14 U SW8260ug/Kg1.1ND4-Methyl-2-pentanone 47 04/11/14 U SW8260ug/Kg2.2NDAcetone 50 04/11/14 U SW8260ug/Kg9.3NDAcrylonitrile 19 04/11/14 U SW8260ug/Kg5.3NDBenzene 9.3 04/11/14 U SW8260ug/Kg1.9NDBromobenzene 9.3 04/11/14 U SW8260ug/Kg1.2NDBromochloromethane 9.3 04/11/14 U SW8260ug/Kg1.4NDBromodichloromethane 9.3 04/11/14 U SW8260ug/Kg1.2NDBromoform 9.3 04/11/14 U SW8260ug/Kg1.3NDBromomethane 9.3 04/11/14 U SW8260ug/Kg7.2NDCarbon Disulfide 9.3 04/11/14 U SW8260ug/Kg1.5NDCarbon tetrachloride 9.3 04/11/14 U SW8260ug/Kg1.1NDChlorobenzene 9.3 04/11/14 U SW8260ug/Kg1.4NDChloroethane 9.3 04/11/14 U SW8260ug/Kg2.2NDChloroform 9.3 04/11/14 U SW8260ug/Kg1.7NDChloromethane 9.3 04/11/14 U SW8260ug/Kg4.9NDcis-1,2-Dichloroethene 9.3 04/11/14 U SW8260ug/Kg2.0NDcis-1,3-Dichloropropene 9.3 04/11/14 U SW8260ug/Kg1.0NDDibromochloromethane 9.3 04/11/14 U SW8260ug/Kg1.0NDDibromomethane 9.3 04/11/14 U SW8260ug/Kg1.2NDDichlorodifluoromethane 9.3 04/11/14 U SW8260ug/Kg2.5NDEthylbenzene 9.3 04/11/14 U SW8260ug/Kg1.7NDHexachlorobutadiene 9.3 04/11/14 U SW8260ug/Kg2.0NDIsopropylbenzene 9.3 04/11/14 U SW8260ug/Kg1.8NDm&p-Xylene 9.3 04/11/14 U SW8260ug/Kg3.7NDMethyl Ethyl Ketone 56 04/11/14 U SW8260ug/Kg8.1NDMethyl t-butyl ether (MTBE) 19 04/11/14 U SW8260ug/Kg2.6NDMethylene chloride 9.3 04/11/14 U SW8260ug/Kg1.5NDNaphthalene 9.3 04/11/14 U SW8260ug/Kg2.5NDn-Butylbenzene 9.3 04/11/14 U SW8260ug/Kg1.7
Page 3 of 49 Ver 1
E-SB1 0-2Phoenix I.D.: BG30363
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
NDn-Propylbenzene 9.3 04/11/14 U SW8260ug/Kg1.7NDo-Xylene 9.3 04/11/14 U SW8260ug/Kg3.6NDp-Isopropyltoluene 9.3 04/11/14 U SW8260ug/Kg1.3NDsec-Butylbenzene 9.3 04/11/14 U SW8260ug/Kg1.8NDStyrene 9.3 04/11/14 U SW8260ug/Kg2.7NDtert-Butylbenzene 9.3 04/11/14 U SW8260ug/Kg1.5NDTetrachloroethene 9.3 04/11/14 U SW8260ug/Kg2.0NDTetrahydrofuran (THF) 19 04/11/14 U SW8260ug/Kg 18.4NDToluene 9.3 04/11/14 U SW8260ug/Kg1.5NDtrans-1,2-Dichloroethene 9.3 04/11/14 U SW8260ug/Kg1.9NDtrans-1,3-Dichloropropene 9.3 04/11/14 U SW8260ug/Kg1.9NDtrans-1,4-dichloro-2-butene 19 04/11/14 U SW8260ug/Kg17NDTrichloroethene 9.3 04/11/14 U SW8260ug/Kg2.0NDTrichlorofluoromethane 9.3 04/11/14 U SW8260ug/Kg2.1NDTrichlorotrifluoroethane 9.3 04/11/14 U SW8260ug/Kg1.5NDVinyl chloride 9.3 04/11/14 U SW8260ug/Kg3.0
QA/QC Surrogates107% 1,2-dichlorobenzene-d4 04/11/14 U 70 - 130 %%92% Bromofluorobenzene 04/11/14 U 70 - 130 %%104% Dibromofluoromethane 04/11/14 U 70 - 130 %%100% Toluene-d8 04/11/14 U 70 - 130 %%
Per 1.4.6 of EPA method 8270D, 1,2-Diphenylhydrazine is unstable and readily converts to Azobenzene. Azobenzene is used for the calibration of 1,2-Diphenylhydrazine.
Please be advised that the NY unrestricted soil criteria for chromium is based on hexavalent chromium and trivalent chromium.
All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments.
1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.B = Present in blank, no bias suspected.
If there are any questions regarding this data, please call Phoenix Client Services at extension 200.This report must not be reproduced except in full as defined by the attached chain of custody.
Reviewed and Released by: Greg Lawrence, Assistant Lab Director
RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level LOD=Limit of Detection MDL=Method Detection Limit
Page 6 of 49 Ver 1
Sample Information Custody InformationMatrix:Location Code:Rush Request:P.O.#:
Collected by:Received by:Analyzed by:
SOLIDEBC72 Hour
04/08/14SWsee "By" below
Laboratory Data
E-SB1 29-31
Phoenix ID: BG30364
04/09/140:00
16:26
Parameter ResultRL/PQL Units Date/Time By Reference
FOR: Attn: Mr. Charles B. Sosik, P.G.Environmental Business Consultants1808 Middle Country RdRidge NY 11961-2406
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
VolatilesND1,1,1,2-Tetrachloroethane 5.7 04/11/14 U SW8260ug/Kg0.94ND1,1,1-Trichloroethane 5.7 04/11/14 U SW8260ug/Kg1.1ND1,1,2,2-Tetrachloroethane 5.7 04/11/14 U SW8260ug/Kg0.81ND1,1,2-Trichloroethane 5.7 04/11/14 U SW8260ug/Kg0.56ND1,1-Dichloroethane 5.7 04/11/14 U SW8260ug/Kg1.1ND1,1-Dichloroethene 5.7 04/11/14 U SW8260ug/Kg1.2ND1,1-Dichloropropene 5.7 04/11/14 U SW8260ug/Kg1.1ND1,2,3-Trichlorobenzene 5.7 04/11/14 U SW8260ug/Kg1.1ND1,2,3-Trichloropropane 5.7 04/11/14 U SW8260ug/Kg0.81ND1,2,4-Trichlorobenzene 5.7 04/11/14 U SW8260ug/Kg1.1ND1,2,4-Trimethylbenzene 5.7 04/11/14 U SW8260ug/Kg0.82ND1,2-Dibromo-3-chloropropane 5.7 04/11/14 U SW8260ug/Kg1.5ND1,2-Dibromoethane 5.7 04/11/14 U SW8260ug/Kg1.5ND1,2-Dichlorobenzene 5.7 04/11/14 U SW8260ug/Kg0.63ND1,2-Dichloroethane 5.7 04/11/14 U SW8260ug/Kg0.50ND1,2-Dichloropropane 5.7 04/11/14 U SW8260ug/Kg0.81ND1,3,5-Trimethylbenzene 5.7 04/11/14 U SW8260ug/Kg0.76ND1,3-Dichlorobenzene 5.7 04/11/14 U SW8260ug/Kg0.85ND1,3-Dichloropropane 5.7 04/11/14 U SW8260ug/Kg0.61ND1,4-Dichlorobenzene 5.7 04/11/14 U SW8260ug/Kg0.90ND2,2-Dichloropropane 5.7 04/11/14 U SW8260ug/Kg0.96ND2-Chlorotoluene 5.7 04/11/14 U SW8260ug/Kg0.92ND2-Hexanone 29 04/11/14 U SW8260ug/Kg2.6ND2-Isopropyltoluene 5.7 04/11/14 U SW8260ug/Kg 10.79ND4-Chlorotoluene 5.7 04/11/14 U SW8260ug/Kg0.66ND4-Methyl-2-pentanone 29 04/11/14 U SW8260ug/Kg1.4NDAcetone 50 04/11/14 U SW8260ug/Kg5.7NDAcrylonitrile 11 04/11/14 U SW8260ug/Kg3.2NDBenzene 5.7 04/11/14 U SW8260ug/Kg1.1NDBromobenzene 5.7 04/11/14 U SW8260ug/Kg0.74NDBromochloromethane 5.7 04/11/14 U SW8260ug/Kg0.84NDBromodichloromethane 5.7 04/11/14 U SW8260ug/Kg0.71NDBromoform 5.7 04/11/14 U SW8260ug/Kg0.80NDBromomethane 5.7 04/11/14 U SW8260ug/Kg4.4NDCarbon Disulfide 5.7 04/11/14 U SW8260ug/Kg0.93NDCarbon tetrachloride 5.7 04/11/14 U SW8260ug/Kg0.66NDChlorobenzene 5.7 04/11/14 U SW8260ug/Kg0.85NDChloroethane 5.7 04/11/14 U SW8260ug/Kg1.3NDChloroform 5.7 04/11/14 U SW8260ug/Kg1.0NDChloromethane 5.7 04/11/14 U SW8260ug/Kg3.0NDcis-1,2-Dichloroethene 5.7 04/11/14 U SW8260ug/Kg1.2NDcis-1,3-Dichloropropene 5.7 04/11/14 U SW8260ug/Kg0.62NDDibromochloromethane 5.7 04/11/14 U SW8260ug/Kg0.64NDDibromomethane 5.7 04/11/14 U SW8260ug/Kg0.72NDDichlorodifluoromethane 5.7 04/11/14 U SW8260ug/Kg1.5NDEthylbenzene 5.7 04/11/14 U SW8260ug/Kg1.0NDHexachlorobutadiene 5.7 04/11/14 U SW8260ug/Kg1.2NDIsopropylbenzene 5.7 04/11/14 U SW8260ug/Kg1.1
Page 8 of 49 Ver 1
E-SB1 29-31Phoenix I.D.: BG30364
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
NDm&p-Xylene 5.7 04/11/14 U SW8260ug/Kg2.3NDMethyl Ethyl Ketone 34 04/11/14 U SW8260ug/Kg5.0NDMethyl t-butyl ether (MTBE) 11 04/11/14 U SW8260ug/Kg1.6NDMethylene chloride 5.7 04/11/14 U SW8260ug/Kg0.94NDNaphthalene 5.7 04/11/14 U SW8260ug/Kg1.5NDn-Butylbenzene 5.7 04/11/14 U SW8260ug/Kg1.0NDn-Propylbenzene 5.7 04/11/14 U SW8260ug/Kg1.0NDo-Xylene 5.7 04/11/14 U SW8260ug/Kg2.2NDp-Isopropyltoluene 5.7 04/11/14 U SW8260ug/Kg0.82NDsec-Butylbenzene 5.7 04/11/14 U SW8260ug/Kg1.1NDStyrene 5.7 04/11/14 U SW8260ug/Kg1.6NDtert-Butylbenzene 5.7 04/11/14 U SW8260ug/Kg0.92NDTetrachloroethene 5.7 04/11/14 U SW8260ug/Kg1.2NDTetrahydrofuran (THF) 11 04/11/14 U SW8260ug/Kg 15.1NDToluene 5.7 04/11/14 U SW8260ug/Kg0.90NDtrans-1,2-Dichloroethene 5.7 04/11/14 U SW8260ug/Kg1.1NDtrans-1,3-Dichloropropene 5.7 04/11/14 U SW8260ug/Kg1.2NDtrans-1,4-dichloro-2-butene 11 04/11/14 U SW8260ug/Kg11NDTrichloroethene 5.7 04/11/14 U SW8260ug/Kg1.2NDTrichlorofluoromethane 5.7 04/11/14 U SW8260ug/Kg1.3NDTrichlorotrifluoroethane 5.7 04/11/14 U SW8260ug/Kg0.89NDVinyl chloride 5.7 04/11/14 U SW8260ug/Kg1.9
QA/QC Surrogates107% 1,2-dichlorobenzene-d4 04/11/14 U 70 - 130 %%94% Bromofluorobenzene 04/11/14 U 70 - 130 %%104% Dibromofluoromethane 04/11/14 U 70 - 130 %%101% Toluene-d8 04/11/14 U 70 - 130 %%
Per 1.4.6 of EPA method 8270D, 1,2-Diphenylhydrazine is unstable and readily converts to Azobenzene. Azobenzene is used for the calibration of 1,2-Diphenylhydrazine.
Please be advised that the NY unrestricted soil criteria for chromium is based on hexavalent chromium and trivalent chromium.
All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments.
1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.B = Present in blank, no bias suspected.
If there are any questions regarding this data, please call Phoenix Client Services at extension 200.This report must not be reproduced except in full as defined by the attached chain of custody.
Reviewed and Released by: Greg Lawrence, Assistant Lab Director
RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level LOD=Limit of Detection MDL=Method Detection Limit
Page 11 of 49 Ver 1
Sample Information Custody InformationMatrix:Location Code:Rush Request:P.O.#:
Collected by:Received by:Analyzed by:
SOLIDEBC72 Hour
04/08/14SWsee "By" below
Laboratory Data
E-SB2 29-31
Phoenix ID: BG30365
04/09/140:00
16:26
Parameter ResultRL/PQL Units Date/Time By Reference
FOR: Attn: Mr. Charles B. Sosik, P.G.Environmental Business Consultants1808 Middle Country RdRidge NY 11961-2406
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
VolatilesND1,1,1,2-Tetrachloroethane 8.1 04/11/14 U SW8260ug/Kg1.3ND1,1,1-Trichloroethane 8.1 04/11/14 U SW8260ug/Kg1.6ND1,1,2,2-Tetrachloroethane 8.1 04/11/14 U SW8260ug/Kg1.1ND1,1,2-Trichloroethane 8.1 04/11/14 U SW8260ug/Kg0.79ND1,1-Dichloroethane 8.1 04/11/14 U SW8260ug/Kg1.6ND1,1-Dichloroethene 8.1 04/11/14 U SW8260ug/Kg1.8ND1,1-Dichloropropene 8.1 04/11/14 U SW8260ug/Kg1.6ND1,2,3-Trichlorobenzene 8.1 04/11/14 U SW8260ug/Kg1.6ND1,2,3-Trichloropropane 8.1 04/11/14 U SW8260ug/Kg1.1ND1,2,4-Trichlorobenzene 8.1 04/11/14 U SW8260ug/Kg1.6ND1,2,4-Trimethylbenzene 8.1 04/11/14 U SW8260ug/Kg1.2ND1,2-Dibromo-3-chloropropane 8.1 04/11/14 U SW8260ug/Kg2.2ND1,2-Dibromoethane 8.1 04/11/14 U SW8260ug/Kg2.2ND1,2-Dichlorobenzene 8.1 04/11/14 U SW8260ug/Kg0.89ND1,2-Dichloroethane 8.1 04/11/14 U SW8260ug/Kg0.71ND1,2-Dichloropropane 8.1 04/11/14 U SW8260ug/Kg1.1ND1,3,5-Trimethylbenzene 8.1 04/11/14 U SW8260ug/Kg1.1ND1,3-Dichlorobenzene 8.1 04/11/14 U SW8260ug/Kg1.2ND1,3-Dichloropropane 8.1 04/11/14 U SW8260ug/Kg0.86ND1,4-Dichlorobenzene 8.1 04/11/14 U SW8260ug/Kg1.3ND2,2-Dichloropropane 8.1 04/11/14 U SW8260ug/Kg1.4ND2-Chlorotoluene 8.1 04/11/14 U SW8260ug/Kg1.3ND2-Hexanone 40 04/11/14 U SW8260ug/Kg3.6ND2-Isopropyltoluene 8.1 04/11/14 U SW8260ug/Kg 11.1ND4-Chlorotoluene 8.1 04/11/14 U SW8260ug/Kg0.94ND4-Methyl-2-pentanone 40 04/11/14 U SW8260ug/Kg1.9NDAcetone 50 04/11/14 U SW8260ug/Kg8.0NDAcrylonitrile 16 04/11/14 U SW8260ug/Kg4.5NDBenzene 8.1 04/11/14 U SW8260ug/Kg1.6NDBromobenzene 8.1 04/11/14 U SW8260ug/Kg1.1NDBromochloromethane 8.1 04/11/14 U SW8260ug/Kg1.2NDBromodichloromethane 8.1 04/11/14 U SW8260ug/Kg1.0NDBromoform 8.1 04/11/14 U SW8260ug/Kg1.1NDBromomethane 8.1 04/11/14 U SW8260ug/Kg6.2NDCarbon Disulfide 8.1 04/11/14 U SW8260ug/Kg1.3NDCarbon tetrachloride 8.1 04/11/14 U SW8260ug/Kg0.94NDChlorobenzene 8.1 04/11/14 U SW8260ug/Kg1.2NDChloroethane 8.1 04/11/14 U SW8260ug/Kg1.9NDChloroform 8.1 04/11/14 U SW8260ug/Kg1.5NDChloromethane 8.1 04/11/14 U SW8260ug/Kg4.2NDcis-1,2-Dichloroethene 8.1 04/11/14 U SW8260ug/Kg1.8NDcis-1,3-Dichloropropene 8.1 04/11/14 U SW8260ug/Kg0.87NDDibromochloromethane 8.1 04/11/14 U SW8260ug/Kg0.91NDDibromomethane 8.1 04/11/14 U SW8260ug/Kg1.0NDDichlorodifluoromethane 8.1 04/11/14 U SW8260ug/Kg2.2NDEthylbenzene 8.1 04/11/14 U SW8260ug/Kg1.5NDHexachlorobutadiene 8.1 04/11/14 U SW8260ug/Kg1.7NDIsopropylbenzene 8.1 04/11/14 U SW8260ug/Kg1.6
Page 13 of 49 Ver 1
E-SB2 29-31Phoenix I.D.: BG30365
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
NDm&p-Xylene 8.1 04/11/14 U SW8260ug/Kg3.2NDMethyl Ethyl Ketone 49 04/11/14 U SW8260ug/Kg7.0NDMethyl t-butyl ether (MTBE) 16 04/11/14 U SW8260ug/Kg2.2NDMethylene chloride 8.1 04/11/14 U SW8260ug/Kg1.3NDNaphthalene 8.1 04/11/14 U SW8260ug/Kg2.2NDn-Butylbenzene 8.1 04/11/14 U SW8260ug/Kg1.5NDn-Propylbenzene 8.1 04/11/14 U SW8260ug/Kg1.5NDo-Xylene 8.1 04/11/14 U SW8260ug/Kg3.1NDp-Isopropyltoluene 8.1 04/11/14 U SW8260ug/Kg1.2NDsec-Butylbenzene 8.1 04/11/14 U SW8260ug/Kg1.5NDStyrene 8.1 04/11/14 U SW8260ug/Kg2.3NDtert-Butylbenzene 8.1 04/11/14 U SW8260ug/Kg1.3NDTetrachloroethene 8.1 04/11/14 U SW8260ug/Kg1.7NDTetrahydrofuran (THF) 16 04/11/14 U SW8260ug/Kg 17.3NDToluene 8.1 04/11/14 U SW8260ug/Kg1.3NDtrans-1,2-Dichloroethene 8.1 04/11/14 U SW8260ug/Kg1.6NDtrans-1,3-Dichloropropene 8.1 04/11/14 U SW8260ug/Kg1.7NDtrans-1,4-dichloro-2-butene 16 04/11/14 U SW8260ug/Kg15NDTrichloroethene 8.1 04/11/14 U SW8260ug/Kg1.7NDTrichlorofluoromethane 8.1 04/11/14 U SW8260ug/Kg1.8NDTrichlorotrifluoroethane 8.1 04/11/14 U SW8260ug/Kg1.3NDVinyl chloride 8.1 04/11/14 U SW8260ug/Kg2.6
QA/QC Surrogates103% 1,2-dichlorobenzene-d4 04/11/14 U 70 - 130 %%95% Bromofluorobenzene 04/11/14 U 70 - 130 %%106% Dibromofluoromethane 04/11/14 U 70 - 130 %%100% Toluene-d8 04/11/14 U 70 - 130 %%
Per 1.4.6 of EPA method 8270D, 1,2-Diphenylhydrazine is unstable and readily converts to Azobenzene. Azobenzene is used for the calibration of 1,2-Diphenylhydrazine.
Please be advised that the NY unrestricted soil criteria for chromium is based on hexavalent chromium and trivalent chromium.
All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments.
1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.B = Present in blank, no bias suspected.
If there are any questions regarding this data, please call Phoenix Client Services at extension 200.This report must not be reproduced except in full as defined by the attached chain of custody.
Reviewed and Released by: Greg Lawrence, Assistant Lab Director
RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level LOD=Limit of Detection MDL=Method Detection Limit
Page 16 of 49 Ver 1
Sample Information Custody InformationMatrix:Location Code:Rush Request:P.O.#:
Collected by:Received by:Analyzed by:
SOLIDEBC72 Hour
04/08/14SWsee "By" below
Laboratory Data
E-SB6 0-2
Phoenix ID: BG30366
04/09/140:00
16:26
Parameter ResultRL/PQL Units Date/Time By Reference
FOR: Attn: Mr. Charles B. Sosik, P.G.Environmental Business Consultants1808 Middle Country RdRidge NY 11961-2406
Polychlorinated BiphenylsNDPCB-1016 36 04/10/14 AW SW 8082ug/Kg36NDPCB-1221 36 04/10/14 AW SW 8082ug/Kg36NDPCB-1232 36 04/10/14 AW SW 8082ug/Kg36NDPCB-1242 36 04/10/14 AW SW 8082ug/Kg36NDPCB-1248 36 04/10/14 AW SW 8082ug/Kg36210PCB-1254 36 04/10/14 AW SW 8082ug/Kg36NDPCB-1260 36 04/10/14 AW SW 8082ug/Kg36NDPCB-1262 36 04/10/14 AW SW 8082ug/Kg36NDPCB-1268 36 04/10/14 AW SW 8082ug/Kg36
QA/QC Surrogates86% DCBP 04/10/14 AW 30 - 150 %%76% TCMX 04/10/14 AW 30 - 150 %%
Pesticides - SoilND4,4' -DDD 2.6 04/14/14 CE SW8081ug/Kg2.6ND4,4' -DDE 2.6 04/14/14 CE SW8081ug/Kg2.6244,4' -DDT 2.6 04/14/14 CE SW8081ug/Kg2.6NDa-BHC 1.8 04/14/14 CE SW8081ug/Kg1.8NDa-Chlordane 3.6 04/14/14 CE SW8081ug/Kg3.6NDAldrin 1.8 04/14/14 CE SW8081ug/Kg1.8NDb-BHC 1.8 04/14/14 CE SW8081ug/Kg1.8NDChlordane 22 04/14/14 CE SW8081ug/Kg22NDd-BHC 1.8 04/14/14 CE SW8081ug/Kg1.8NDDieldrin 1.8 04/14/14 CE SW8081ug/Kg1.8NDEndosulfan I 3.6 04/14/14 CE SW8081ug/Kg3.6NDEndosulfan II 3.6 04/14/14 CE SW8081ug/Kg3.6NDEndosulfan sulfate 3.6 04/14/14 CE SW8081ug/Kg3.6NDEndrin 1.8 04/14/14 CE SW8081ug/Kg1.8NDEndrin aldehyde 3.6 04/14/14 CE SW8081ug/Kg3.6NDEndrin ketone 1.8 04/14/14 CE SW8081ug/Kg1.8NDg-BHC 1.8 04/14/14 CE SW8081ug/Kg1.8NDg-Chlordane 3.6 04/14/14 CE SW8081ug/Kg3.6NDHeptachlor 1.8 04/14/14 CE SW8081ug/Kg1.8NDHeptachlor epoxide 1.8 04/14/14 CE SW8081ug/Kg1.8NDMethoxychlor 7.3 04/14/14 CE SW8081ug/Kg7.3NDToxaphene 180 04/14/14 CE SW8081ug/Kg180
QA/QC Surrogates140% DCBP 04/14/14 CE 30 - 150 %%83% TCMX 04/14/14 CE 30 - 150 %%
Per 1.4.6 of EPA method 8270D, 1,2-Diphenylhydrazine is unstable and readily converts to Azobenzene. Azobenzene is used for the calibration of 1,2-Diphenylhydrazine.
Please be advised that the NY unrestricted soil criteria for chromium is based on hexavalent chromium and trivalent chromium.
Semi-Volatile Comment:Due to a matrix interference and/or the presence of a large amount of non-target material in the sample, a dilution was required resulting in an elevated RL for the semivolatile analysis.
Volatile Comment:There was a suppression of the last internal standard in the low level analysis, all affected compounds are reported from the methanol preserved high level analysis which did not exhibit this interference.
For Pesticides, due to matrix interference caused by the presence of PCBs in the samples an elevated MDL was reported.
All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments.
1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.B = Present in blank, no bias suspected.
If there are any questions regarding this data, please call Phoenix Client Services at extension 200.This report must not be reproduced except in full as defined by the attached chain of custody.
Reviewed and Released by: Greg Lawrence, Assistant Lab Director
RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level LOD=Limit of Detection MDL=Method Detection Limit
Page 22 of 49 Ver 1
Sample Information Custody InformationMatrix:Location Code:Rush Request:P.O.#:
Collected by:Received by:Analyzed by:
SOLIDEBC72 Hour
04/08/14SWsee "By" below
Laboratory Data
E-SB6 15-17
Phoenix ID: BG30367
04/09/140:00
16:26
Parameter ResultRL/PQL Units Date/Time By Reference
FOR: Attn: Mr. Charles B. Sosik, P.G.Environmental Business Consultants1808 Middle Country RdRidge NY 11961-2406
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
VolatilesND1,1,1,2-Tetrachloroethane 7.3 04/11/14 U SW8260ug/Kg1.2ND1,1,1-Trichloroethane 7.3 04/11/14 U SW8260ug/Kg1.5ND1,1,2,2-Tetrachloroethane 7.3 04/11/14 U SW8260ug/Kg1.0ND1,1,2-Trichloroethane 7.3 04/11/14 U SW8260ug/Kg0.71ND1,1-Dichloroethane 7.3 04/11/14 U SW8260ug/Kg1.4ND1,1-Dichloroethene 7.3 04/11/14 U SW8260ug/Kg1.6ND1,1-Dichloropropene 7.3 04/11/14 U SW8260ug/Kg1.4ND1,2,3-Trichlorobenzene 7.3 04/11/14 U SW8260ug/Kg1.5ND1,2,3-Trichloropropane 7.3 04/11/14 U SW8260ug/Kg1.0ND1,2,4-Trichlorobenzene 7.3 04/11/14 U SW8260ug/Kg1.5ND1,2,4-Trimethylbenzene 7.3 04/11/14 U SW8260ug/Kg1.0ND1,2-Dibromo-3-chloropropane 7.3 04/11/14 U SW8260ug/Kg2.0ND1,2-Dibromoethane 7.3 04/11/14 U SW8260ug/Kg1.9ND1,2-Dichlorobenzene 7.3 04/11/14 U SW8260ug/Kg0.80ND1,2-Dichloroethane 7.3 04/11/14 U SW8260ug/Kg0.64ND1,2-Dichloropropane 7.3 04/11/14 U SW8260ug/Kg1.0ND1,3,5-Trimethylbenzene 7.3 04/11/14 U SW8260ug/Kg0.96ND1,3-Dichlorobenzene 7.3 04/11/14 U SW8260ug/Kg1.1ND1,3-Dichloropropane 7.3 04/11/14 U SW8260ug/Kg0.77ND1,4-Dichlorobenzene 7.3 04/11/14 U SW8260ug/Kg1.2ND2,2-Dichloropropane 7.3 04/11/14 U SW8260ug/Kg1.2ND2-Chlorotoluene 7.3 04/11/14 U SW8260ug/Kg1.2ND2-Hexanone 36 04/11/14 U SW8260ug/Kg3.3ND2-Isopropyltoluene 7.3 04/11/14 U SW8260ug/Kg 11.0ND4-Chlorotoluene 7.3 04/11/14 U SW8260ug/Kg0.84ND4-Methyl-2-pentanone 36 04/11/14 U SW8260ug/Kg1.7NDAcetone 50 04/11/14 U SW8260ug/Kg7.2NDAcrylonitrile 15 04/11/14 U SW8260ug/Kg4.1NDBenzene 7.3 04/11/14 U SW8260ug/Kg1.4NDBromobenzene 7.3 04/11/14 U SW8260ug/Kg0.95NDBromochloromethane 7.3 04/11/14 U SW8260ug/Kg1.1NDBromodichloromethane 7.3 04/11/14 U SW8260ug/Kg0.90NDBromoform 7.3 04/11/14 U SW8260ug/Kg1.0NDBromomethane 7.3 04/11/14 U SW8260ug/Kg5.6NDCarbon Disulfide 7.3 04/11/14 U SW8260ug/Kg1.2NDCarbon tetrachloride 7.3 04/11/14 U SW8260ug/Kg0.84NDChlorobenzene 7.3 04/11/14 U SW8260ug/Kg1.1NDChloroethane 7.3 04/11/14 U SW8260ug/Kg1.7NDChloroform 7.3 04/11/14 U SW8260ug/Kg1.3NDChloromethane 7.3 04/11/14 U SW8260ug/Kg3.8NDcis-1,2-Dichloroethene 7.3 04/11/14 U SW8260ug/Kg1.6NDcis-1,3-Dichloropropene 7.3 04/11/14 U SW8260ug/Kg0.79NDDibromochloromethane 7.3 04/11/14 U SW8260ug/Kg0.82NDDibromomethane 7.3 04/11/14 U SW8260ug/Kg0.92NDDichlorodifluoromethane 7.3 04/11/14 U SW8260ug/Kg1.9NDEthylbenzene 7.3 04/11/14 U SW8260ug/Kg1.3NDHexachlorobutadiene 7.3 04/11/14 U SW8260ug/Kg1.5NDIsopropylbenzene 7.3 04/11/14 U SW8260ug/Kg1.4
Page 24 of 49 Ver 1
E-SB6 15-17Phoenix I.D.: BG30367
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
NDm&p-Xylene 7.3 04/11/14 U SW8260ug/Kg2.9NDMethyl Ethyl Ketone 44 04/11/14 U SW8260ug/Kg6.3NDMethyl t-butyl ether (MTBE) 15 04/11/14 U SW8260ug/Kg2.0NDMethylene chloride 7.3 04/11/14 U SW8260ug/Kg1.2NDNaphthalene 7.3 04/11/14 U SW8260ug/Kg2.0NDn-Butylbenzene 7.3 04/11/14 U SW8260ug/Kg1.3NDn-Propylbenzene 7.3 04/11/14 U SW8260ug/Kg1.3NDo-Xylene 7.3 04/11/14 U SW8260ug/Kg2.8NDp-Isopropyltoluene 7.3 04/11/14 U SW8260ug/Kg1.0NDsec-Butylbenzene 7.3 04/11/14 U SW8260ug/Kg1.4NDStyrene 7.3 04/11/14 U SW8260ug/Kg2.1NDtert-Butylbenzene 7.3 04/11/14 U SW8260ug/Kg1.2NDTetrachloroethene 7.3 04/11/14 U SW8260ug/Kg1.5NDTetrahydrofuran (THF) 15 04/11/14 U SW8260ug/Kg 16.6NDToluene 7.3 04/11/14 U SW8260ug/Kg1.2NDtrans-1,2-Dichloroethene 7.3 04/11/14 U SW8260ug/Kg1.5NDtrans-1,3-Dichloropropene 7.3 04/11/14 U SW8260ug/Kg1.5NDtrans-1,4-dichloro-2-butene 15 04/11/14 U SW8260ug/Kg14NDTrichloroethene 7.3 04/11/14 U SW8260ug/Kg1.5NDTrichlorofluoromethane 7.3 04/11/14 U SW8260ug/Kg1.6NDTrichlorotrifluoroethane 7.3 04/11/14 U SW8260ug/Kg1.1NDVinyl chloride 7.3 04/11/14 U SW8260ug/Kg2.4
QA/QC Surrogates105% 1,2-dichlorobenzene-d4 04/11/14 U 70 - 130 %%100% Bromofluorobenzene 04/11/14 U 70 - 130 %%114% Dibromofluoromethane 04/11/14 U 70 - 130 %%100% Toluene-d8 04/11/14 U 70 - 130 %%
Per 1.4.6 of EPA method 8270D, 1,2-Diphenylhydrazine is unstable and readily converts to Azobenzene. Azobenzene is used for the calibration of 1,2-Diphenylhydrazine.
Please be advised that the NY unrestricted soil criteria for chromium is based on hexavalent chromium and trivalent chromium.
All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments.
1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.B = Present in blank, no bias suspected.
If there are any questions regarding this data, please call Phoenix Client Services at extension 200.This report must not be reproduced except in full as defined by the attached chain of custody.
Reviewed and Released by: Greg Lawrence, Assistant Lab Director
RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level LOD=Limit of Detection MDL=Method Detection Limit
Page 27 of 49 Ver 1
Sample Information Custody InformationMatrix:Location Code:Rush Request:P.O.#:
Collected by:Received by:Analyzed by:
SOLIDEBC72 Hour
04/08/14SWsee "By" below
Laboratory Data
E-SB7 0-2
Phoenix ID: BG30368
04/09/140:00
16:26
Parameter ResultRL/PQL Units Date/Time By Reference
FOR: Attn: Mr. Charles B. Sosik, P.G.Environmental Business Consultants1808 Middle Country RdRidge NY 11961-2406
Polychlorinated BiphenylsNDPCB-1016 36 04/10/14 AW SW 8082ug/Kg36NDPCB-1221 36 04/10/14 AW SW 8082ug/Kg36NDPCB-1232 36 04/10/14 AW SW 8082ug/Kg36NDPCB-1242 36 04/10/14 AW SW 8082ug/Kg36NDPCB-1248 36 04/10/14 AW SW 8082ug/Kg36NDPCB-1254 36 04/10/14 AW SW 8082ug/Kg36NDPCB-1260 36 04/10/14 AW SW 8082ug/Kg36NDPCB-1262 36 04/10/14 AW SW 8082ug/Kg36NDPCB-1268 36 04/10/14 AW SW 8082ug/Kg36
QA/QC Surrogates54% DCBP 04/10/14 AW 30 - 150 %%44% TCMX 04/10/14 AW 30 - 150 %%
Pesticides - SoilND4,4' -DDD 2.6 04/14/14 CE SW8081ug/Kg2.6ND4,4' -DDE 2.6 04/14/14 CE SW8081ug/Kg2.6ND4,4' -DDT 2.6 04/14/14 CE SW8081ug/Kg2.6NDa-BHC 1.8 04/14/14 CE SW8081ug/Kg1.8NDa-Chlordane 3.6 04/14/14 CE SW8081ug/Kg3.6NDAldrin 1.8 04/14/14 CE SW8081ug/Kg1.8NDb-BHC 1.8 04/14/14 CE SW8081ug/Kg1.8NDChlordane 22 04/14/14 CE SW8081ug/Kg22NDd-BHC 1.8 04/14/14 CE SW8081ug/Kg1.8NDDieldrin 1.8 04/14/14 CE SW8081ug/Kg1.8NDEndosulfan I 3.6 04/14/14 CE SW8081ug/Kg3.6NDEndosulfan II 3.6 04/14/14 CE SW8081ug/Kg3.6NDEndosulfan sulfate 3.6 04/14/14 CE SW8081ug/Kg3.6NDEndrin 1.8 04/14/14 CE SW8081ug/Kg1.8NDEndrin aldehyde 3.6 04/14/14 CE SW8081ug/Kg3.6NDEndrin ketone 1.8 04/14/14 CE SW8081ug/Kg1.8NDg-BHC 1.8 04/14/14 CE SW8081ug/Kg1.8NDg-Chlordane 3.6 04/14/14 CE SW8081ug/Kg3.6NDHeptachlor 1.8 04/14/14 CE SW8081ug/Kg1.8NDHeptachlor epoxide 1.8 04/14/14 CE SW8081ug/Kg1.8NDMethoxychlor 18 04/14/14 CE SW8081ug/Kg18NDToxaphene 180 04/14/14 CE SW8081ug/Kg180
QA/QC Surrogates46% DCBP 04/14/14 CE 30 - 150 %%45% TCMX 04/14/14 CE 30 - 150 %%
VolatilesND1,1,1,2-Tetrachloroethane 7.2 04/11/14 U SW8260ug/Kg1.2ND1,1,1-Trichloroethane 7.2 04/11/14 U SW8260ug/Kg1.4ND1,1,2,2-Tetrachloroethane 7.2 04/11/14 U SW8260ug/Kg1.0ND1,1,2-Trichloroethane 7.2 04/11/14 U SW8260ug/Kg0.70ND1,1-Dichloroethane 7.2 04/11/14 U SW8260ug/Kg1.4
Page 29 of 49 Ver 1
E-SB7 0-2Phoenix I.D.: BG30368
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
ND1,1-Dichloroethene 7.2 04/11/14 U SW8260ug/Kg1.6ND1,1-Dichloropropene 7.2 04/11/14 U SW8260ug/Kg1.4ND1,2,3-Trichlorobenzene 7.2 04/11/14 U SW8260ug/Kg1.4ND1,2,3-Trichloropropane 7.2 04/11/14 U SW8260ug/Kg1.0ND1,2,4-Trichlorobenzene 7.2 04/11/14 U SW8260ug/Kg1.4ND1,2,4-Trimethylbenzene 7.2 04/11/14 U SW8260ug/Kg1.0ND1,2-Dibromo-3-chloropropane 7.2 04/11/14 U SW8260ug/Kg1.9ND1,2-Dibromoethane 7.2 04/11/14 U SW8260ug/Kg1.9ND1,2-Dichlorobenzene 7.2 04/11/14 U SW8260ug/Kg0.79ND1,2-Dichloroethane 7.2 04/11/14 U SW8260ug/Kg0.63ND1,2-Dichloropropane 7.2 04/11/14 U SW8260ug/Kg1.0ND1,3,5-Trimethylbenzene 7.2 04/11/14 U SW8260ug/Kg0.95ND1,3-Dichlorobenzene 7.2 04/11/14 U SW8260ug/Kg1.1ND1,3-Dichloropropane 7.2 04/11/14 U SW8260ug/Kg0.76ND1,4-Dichlorobenzene 7.2 04/11/14 U SW8260ug/Kg1.1ND2,2-Dichloropropane 7.2 04/11/14 U SW8260ug/Kg1.2ND2-Chlorotoluene 7.2 04/11/14 U SW8260ug/Kg1.1ND2-Hexanone 36 04/11/14 U SW8260ug/Kg3.2ND2-Isopropyltoluene 7.2 04/11/14 U SW8260ug/Kg 10.99ND4-Chlorotoluene 7.2 04/11/14 U SW8260ug/Kg0.83ND4-Methyl-2-pentanone 36 04/11/14 U SW8260ug/Kg1.7NDAcetone 50 04/11/14 U SW8260ug/Kg7.1NDAcrylonitrile 14 04/11/14 U SW8260ug/Kg4.0NDBenzene 7.2 04/11/14 U SW8260ug/Kg1.4NDBromobenzene 7.2 04/11/14 U SW8260ug/Kg0.93NDBromochloromethane 7.2 04/11/14 U SW8260ug/Kg1.0NDBromodichloromethane 7.2 04/11/14 U SW8260ug/Kg0.89NDBromoform 7.2 04/11/14 U SW8260ug/Kg1.0NDBromomethane 7.2 04/11/14 U SW8260ug/Kg5.5NDCarbon Disulfide 7.2 04/11/14 U SW8260ug/Kg1.2NDCarbon tetrachloride 7.2 04/11/14 U SW8260ug/Kg0.83NDChlorobenzene 7.2 04/11/14 U SW8260ug/Kg1.1NDChloroethane 7.2 04/11/14 U SW8260ug/Kg1.7NDChloroform 7.2 04/11/14 U SW8260ug/Kg1.3NDChloromethane 7.2 04/11/14 U SW8260ug/Kg3.8NDcis-1,2-Dichloroethene 7.2 04/11/14 U SW8260ug/Kg1.6NDcis-1,3-Dichloropropene 7.2 04/11/14 U SW8260ug/Kg0.77NDDibromochloromethane 7.2 04/11/14 U SW8260ug/Kg0.80NDDibromomethane 7.2 04/11/14 U SW8260ug/Kg0.90NDDichlorodifluoromethane 7.2 04/11/14 U SW8260ug/Kg1.9NDEthylbenzene 7.2 04/11/14 U SW8260ug/Kg1.3NDHexachlorobutadiene 7.2 04/11/14 U SW8260ug/Kg1.5NDIsopropylbenzene 7.2 04/11/14 U SW8260ug/Kg1.4NDm&p-Xylene 7.2 04/11/14 U SW8260ug/Kg2.8NDMethyl Ethyl Ketone 43 04/11/14 U SW8260ug/Kg6.2NDMethyl t-butyl ether (MTBE) 14 04/11/14 U SW8260ug/Kg2.0NDMethylene chloride 7.2 04/11/14 U SW8260ug/Kg1.2NDNaphthalene 7.2 04/11/14 U SW8260ug/Kg1.9NDn-Butylbenzene 7.2 04/11/14 U SW8260ug/Kg1.3
Page 30 of 49 Ver 1
E-SB7 0-2Phoenix I.D.: BG30368
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
NDn-Propylbenzene 7.2 04/11/14 U SW8260ug/Kg1.3NDo-Xylene 7.2 04/11/14 U SW8260ug/Kg2.7NDp-Isopropyltoluene 7.2 04/11/14 U SW8260ug/Kg1.0NDsec-Butylbenzene 7.2 04/11/14 U SW8260ug/Kg1.3NDStyrene 7.2 04/11/14 U SW8260ug/Kg2.1NDtert-Butylbenzene 7.2 04/11/14 U SW8260ug/Kg1.1NDTetrachloroethene 7.2 04/11/14 U SW8260ug/Kg1.5NDTetrahydrofuran (THF) 14 04/11/14 U SW8260ug/Kg 16.5NDToluene 7.2 04/11/14 U SW8260ug/Kg1.1NDtrans-1,2-Dichloroethene 7.2 04/11/14 U SW8260ug/Kg1.4NDtrans-1,3-Dichloropropene 7.2 04/11/14 U SW8260ug/Kg1.5NDtrans-1,4-dichloro-2-butene 14 04/11/14 U SW8260ug/Kg13NDTrichloroethene 7.2 04/11/14 U SW8260ug/Kg1.5NDTrichlorofluoromethane 7.2 04/11/14 U SW8260ug/Kg1.6NDTrichlorotrifluoroethane 7.2 04/11/14 U SW8260ug/Kg1.1NDVinyl chloride 7.2 04/11/14 U SW8260ug/Kg2.3
QA/QC Surrogates109% 1,2-dichlorobenzene-d4 04/11/14 U 70 - 130 %%94% Bromofluorobenzene 04/11/14 U 70 - 130 %%86% Dibromofluoromethane 04/11/14 U 70 - 130 %%100% Toluene-d8 04/11/14 U 70 - 130 %%
Per 1.4.6 of EPA method 8270D, 1,2-Diphenylhydrazine is unstable and readily converts to Azobenzene. Azobenzene is used for the calibration of 1,2-Diphenylhydrazine.
Please be advised that the NY unrestricted soil criteria for chromium is based on hexavalent chromium and trivalent chromium.
Semi-Volatile Comment:Due to a matrix interference and/or the presence of a large amount of non-target material in the sample, a dilution was required resulting in an elevated RL for the semivolatile analysis.
Due to a matrix interference and/or the presence of a large amount of non-target material in the sample, an elevated RL was reported for the pesticide analysis.
All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments.
1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.B = Present in blank, no bias suspected.
If there are any questions regarding this data, please call Phoenix Client Services at extension 200.This report must not be reproduced except in full as defined by the attached chain of custody.
Reviewed and Released by: Greg Lawrence, Assistant Lab Director
RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level LOD=Limit of Detection MDL=Method Detection Limit
Page 33 of 49 Ver 1
Sample Information Custody InformationMatrix:Location Code:Rush Request:P.O.#:
Collected by:Received by:Analyzed by:
SOLIDEBC72 Hour
04/08/14SWsee "By" below
Laboratory Data
E-SB7 15-17
Phoenix ID: BG30369
04/09/140:00
16:26
Parameter ResultRL/PQL Units Date/Time By Reference
FOR: Attn: Mr. Charles B. Sosik, P.G.Environmental Business Consultants1808 Middle Country RdRidge NY 11961-2406
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
VolatilesND1,1,1,2-Tetrachloroethane 12 04/11/14 U SW8260ug/Kg2.0ND1,1,1-Trichloroethane 12 04/11/14 U SW8260ug/Kg2.4ND1,1,2,2-Tetrachloroethane 12 04/11/14 U SW8260ug/Kg1.7ND1,1,2-Trichloroethane 12 04/11/14 U SW8260ug/Kg1.2ND1,1-Dichloroethane 12 04/11/14 U SW8260ug/Kg2.4ND1,1-Dichloroethene 12 04/11/14 U SW8260ug/Kg2.7ND1,1-Dichloropropene 12 04/11/14 U SW8260ug/Kg2.4ND1,2,3-Trichlorobenzene 12 04/11/14 U SW8260ug/Kg2.4ND1,2,3-Trichloropropane 12 04/11/14 U SW8260ug/Kg1.7ND1,2,4-Trichlorobenzene 12 04/11/14 U SW8260ug/Kg2.4ND1,2,4-Trimethylbenzene 12 04/11/14 U SW8260ug/Kg1.8ND1,2-Dibromo-3-chloropropane 12 04/11/14 U SW8260ug/Kg3.3ND1,2-Dibromoethane 12 04/11/14 U SW8260ug/Kg3.2ND1,2-Dichlorobenzene 12 04/11/14 U SW8260ug/Kg1.3ND1,2-Dichloroethane 12 04/11/14 U SW8260ug/Kg1.1ND1,2-Dichloropropane 12 04/11/14 U SW8260ug/Kg1.7ND1,3,5-Trimethylbenzene 12 04/11/14 U SW8260ug/Kg1.6ND1,3-Dichlorobenzene 12 04/11/14 U SW8260ug/Kg1.8ND1,3-Dichloropropane 12 04/11/14 U SW8260ug/Kg1.3ND1,4-Dichlorobenzene 12 04/11/14 U SW8260ug/Kg1.9ND2,2-Dichloropropane 12 04/11/14 U SW8260ug/Kg2.0ND2-Chlorotoluene 12 04/11/14 U SW8260ug/Kg1.9ND2-Hexanone 61 04/11/14 U SW8260ug/Kg5.5ND2-Isopropyltoluene 12 04/11/14 U SW8260ug/Kg 11.7ND4-Chlorotoluene 12 04/11/14 U SW8260ug/Kg1.4ND4-Methyl-2-pentanone 61 04/11/14 U SW8260ug/Kg2.9NDAcetone 50 04/11/14 U SW8260ug/Kg12NDAcrylonitrile 24 04/11/14 U SW8260ug/Kg6.8NDBenzene 12 04/11/14 U SW8260ug/Kg2.4NDBromobenzene 12 04/11/14 U SW8260ug/Kg1.6NDBromochloromethane 12 04/11/14 U SW8260ug/Kg1.8NDBromodichloromethane 12 04/11/14 U SW8260ug/Kg1.5NDBromoform 12 04/11/14 U SW8260ug/Kg1.7NDBromomethane 12 04/11/14 U SW8260ug/Kg9.4NDCarbon Disulfide 12 04/11/14 U SW8260ug/Kg2.0NDCarbon tetrachloride 12 04/11/14 U SW8260ug/Kg1.4NDChlorobenzene 12 04/11/14 U SW8260ug/Kg1.8NDChloroethane 12 04/11/14 U SW8260ug/Kg2.8NDChloroform 12 04/11/14 U SW8260ug/Kg2.2NDChloromethane 12 04/11/14 U SW8260ug/Kg6.4NDcis-1,2-Dichloroethene 12 04/11/14 U SW8260ug/Kg2.7NDcis-1,3-Dichloropropene 12 04/11/14 U SW8260ug/Kg1.3NDDibromochloromethane 12 04/11/14 U SW8260ug/Kg1.4NDDibromomethane 12 04/11/14 U SW8260ug/Kg1.5NDDichlorodifluoromethane 12 04/11/14 U SW8260ug/Kg3.2NDEthylbenzene 12 04/11/14 U SW8260ug/Kg2.2NDHexachlorobutadiene 12 04/11/14 U SW8260ug/Kg2.6NDIsopropylbenzene 12 04/11/14 U SW8260ug/Kg2.3
Page 35 of 49 Ver 1
E-SB7 15-17Phoenix I.D.: BG30369
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
NDm&p-Xylene 12 04/11/14 U SW8260ug/Kg4.8NDMethyl Ethyl Ketone 73 04/11/14 U SW8260ug/Kg11NDMethyl t-butyl ether (MTBE) 24 04/11/14 U SW8260ug/Kg3.4NDMethylene chloride 12 04/11/14 U SW8260ug/Kg2.0NDNaphthalene 12 04/11/14 U SW8260ug/Kg3.3NDn-Butylbenzene 12 04/11/14 U SW8260ug/Kg2.2NDn-Propylbenzene 12 04/11/14 U SW8260ug/Kg2.2NDo-Xylene 12 04/11/14 U SW8260ug/Kg4.6NDp-Isopropyltoluene 12 04/11/14 U SW8260ug/Kg1.8NDsec-Butylbenzene 12 04/11/14 U SW8260ug/Kg2.3NDStyrene 12 04/11/14 U SW8260ug/Kg3.5NDtert-Butylbenzene 12 04/11/14 U SW8260ug/Kg1.9NDTetrachloroethene 12 04/11/14 U SW8260ug/Kg2.6NDTetrahydrofuran (THF) 24 04/11/14 U SW8260ug/Kg 111NDToluene 12 04/11/14 U SW8260ug/Kg1.9NDtrans-1,2-Dichloroethene 12 04/11/14 U SW8260ug/Kg2.4NDtrans-1,3-Dichloropropene 12 04/11/14 U SW8260ug/Kg2.5NDtrans-1,4-dichloro-2-butene 24 04/11/14 U SW8260ug/Kg23NDTrichloroethene 12 04/11/14 U SW8260ug/Kg2.6NDTrichlorofluoromethane 12 04/11/14 U SW8260ug/Kg2.7NDTrichlorotrifluoroethane 12 04/11/14 U SW8260ug/Kg1.9NDVinyl chloride 12 04/11/14 U SW8260ug/Kg3.9
QA/QC Surrogates103% 1,2-dichlorobenzene-d4 04/11/14 U 70 - 130 %%98% Bromofluorobenzene 04/11/14 U 70 - 130 %%103% Dibromofluoromethane 04/11/14 U 70 - 130 %%101% Toluene-d8 04/11/14 U 70 - 130 %%
Per 1.4.6 of EPA method 8270D, 1,2-Diphenylhydrazine is unstable and readily converts to Azobenzene. Azobenzene is used for the calibration of 1,2-Diphenylhydrazine.
Please be advised that the NY unrestricted soil criteria for chromium is based on hexavalent chromium and trivalent chromium.
All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments.
1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.B = Present in blank, no bias suspected.
If there are any questions regarding this data, please call Phoenix Client Services at extension 200.This report must not be reproduced except in full as defined by the attached chain of custody.
Reviewed and Released by: Greg Lawrence, Assistant Lab Director
RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level LOD=Limit of Detection MDL=Method Detection Limit
Page 38 of 49 Ver 1
Sample Information Custody InformationMatrix:Location Code:Rush Request:P.O.#:
Collected by:Received by:Analyzed by:
SOLIDEBC72 Hour
04/08/14SWsee "By" below
Laboratory Data
SOIL DUPLICATE 2
Phoenix ID: BG30370
04/09/140:00
16:26
Parameter ResultRL/PQL Units Date/Time By Reference
FOR: Attn: Mr. Charles B. Sosik, P.G.Environmental Business Consultants1808 Middle Country RdRidge NY 11961-2406
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
VolatilesND1,1,1,2-Tetrachloroethane 7.7 04/11/14 U SW8260ug/Kg1.3ND1,1,1-Trichloroethane 7.7 04/11/14 U SW8260ug/Kg1.5ND1,1,2,2-Tetrachloroethane 7.7 04/11/14 U SW8260ug/Kg1.1ND1,1,2-Trichloroethane 7.7 04/11/14 U SW8260ug/Kg0.76ND1,1-Dichloroethane 7.7 04/11/14 U SW8260ug/Kg1.5ND1,1-Dichloroethene 7.7 04/11/14 U SW8260ug/Kg1.7ND1,1-Dichloropropene 7.7 04/11/14 U SW8260ug/Kg1.5ND1,2,3-Trichlorobenzene 7.7 04/11/14 U SW8260ug/Kg1.5ND1,2,3-Trichloropropane 7.7 04/11/14 U SW8260ug/Kg1.1ND1,2,4-Trichlorobenzene 7.7 04/11/14 U SW8260ug/Kg1.5ND1,2,4-Trimethylbenzene 7.7 04/11/14 U SW8260ug/Kg1.1ND1,2-Dibromo-3-chloropropane 7.7 04/11/14 U SW8260ug/Kg2.1ND1,2-Dibromoethane 7.7 04/11/14 U SW8260ug/Kg2.1ND1,2-Dichlorobenzene 7.7 04/11/14 U SW8260ug/Kg0.85ND1,2-Dichloroethane 7.7 04/11/14 U SW8260ug/Kg0.68ND1,2-Dichloropropane 7.7 04/11/14 U SW8260ug/Kg1.1ND1,3,5-Trimethylbenzene 7.7 04/11/14 U SW8260ug/Kg1.0ND1,3-Dichlorobenzene 7.7 04/11/14 U SW8260ug/Kg1.1ND1,3-Dichloropropane 7.7 04/11/14 U SW8260ug/Kg0.82ND1,4-Dichlorobenzene 7.7 04/11/14 U SW8260ug/Kg1.2ND2,2-Dichloropropane 7.7 04/11/14 U SW8260ug/Kg1.3ND2-Chlorotoluene 7.7 04/11/14 U SW8260ug/Kg1.2ND2-Hexanone 39 04/11/14 U SW8260ug/Kg3.5ND2-Isopropyltoluene 7.7 04/11/14 U SW8260ug/Kg 11.1ND4-Chlorotoluene 7.7 04/11/14 U SW8260ug/Kg0.90ND4-Methyl-2-pentanone 39 04/11/14 U SW8260ug/Kg1.8NDAcetone 50 04/11/14 U SW8260ug/Kg7.7NDAcrylonitrile 15 04/11/14 U SW8260ug/Kg4.3NDBenzene 7.7 04/11/14 U SW8260ug/Kg1.5NDBromobenzene 7.7 04/11/14 U SW8260ug/Kg1.0NDBromochloromethane 7.7 04/11/14 U SW8260ug/Kg1.1NDBromodichloromethane 7.7 04/11/14 U SW8260ug/Kg0.96NDBromoform 7.7 04/11/14 U SW8260ug/Kg1.1NDBromomethane 7.7 04/11/14 U SW8260ug/Kg6.0NDCarbon Disulfide 7.7 04/11/14 U SW8260ug/Kg1.3NDCarbon tetrachloride 7.7 04/11/14 U SW8260ug/Kg0.90NDChlorobenzene 7.7 04/11/14 U SW8260ug/Kg1.1NDChloroethane 7.7 04/11/14 U SW8260ug/Kg1.8NDChloroform 7.7 04/11/14 U SW8260ug/Kg1.4NDChloromethane 7.7 04/11/14 U SW8260ug/Kg4.1NDcis-1,2-Dichloroethene 7.7 04/11/14 U SW8260ug/Kg1.7NDcis-1,3-Dichloropropene 7.7 04/11/14 U SW8260ug/Kg0.84NDDibromochloromethane 7.7 04/11/14 U SW8260ug/Kg0.87NDDibromomethane 7.7 04/11/14 U SW8260ug/Kg0.97NDDichlorodifluoromethane 7.7 04/11/14 U SW8260ug/Kg2.1NDEthylbenzene 7.7 04/11/14 U SW8260ug/Kg1.4NDHexachlorobutadiene 7.7 04/11/14 U SW8260ug/Kg1.6NDIsopropylbenzene 7.7 04/11/14 U SW8260ug/Kg1.5
Page 40 of 49 Ver 1
SOIL DUPLICATE 2Phoenix I.D.: BG30370
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
NDm&p-Xylene 7.7 04/11/14 U SW8260ug/Kg3.0NDMethyl Ethyl Ketone 46 04/11/14 U SW8260ug/Kg6.7NDMethyl t-butyl ether (MTBE) 15 04/11/14 U SW8260ug/Kg2.1NDMethylene chloride 7.7 04/11/14 U SW8260ug/Kg1.3NDNaphthalene 7.7 04/11/14 U SW8260ug/Kg2.1NDn-Butylbenzene 7.7 04/11/14 U SW8260ug/Kg1.4NDn-Propylbenzene 7.7 04/11/14 U SW8260ug/Kg1.4NDo-Xylene 7.7 04/11/14 U SW8260ug/Kg3.0NDp-Isopropyltoluene 7.7 04/11/14 U SW8260ug/Kg1.1NDsec-Butylbenzene 7.7 04/11/14 U SW8260ug/Kg1.5NDStyrene 7.7 04/11/14 U SW8260ug/Kg2.2NDtert-Butylbenzene 7.7 04/11/14 U SW8260ug/Kg1.2NDTetrachloroethene 7.7 04/11/14 U SW8260ug/Kg1.6NDTetrahydrofuran (THF) 15 04/11/14 U SW8260ug/Kg 17.0NDToluene 7.7 04/11/14 U SW8260ug/Kg1.2NDtrans-1,2-Dichloroethene 7.7 04/11/14 U SW8260ug/Kg1.5NDtrans-1,3-Dichloropropene 7.7 04/11/14 U SW8260ug/Kg1.6NDtrans-1,4-dichloro-2-butene 15 04/11/14 U SW8260ug/Kg14NDTrichloroethene 7.7 04/11/14 U SW8260ug/Kg1.6NDTrichlorofluoromethane 7.7 04/11/14 U SW8260ug/Kg1.7NDTrichlorotrifluoroethane 7.7 04/11/14 U SW8260ug/Kg1.2NDVinyl chloride 7.7 04/11/14 U SW8260ug/Kg2.5
QA/QC Surrogates106% 1,2-dichlorobenzene-d4 04/11/14 U 70 - 130 %%96% Bromofluorobenzene 04/11/14 U 70 - 130 %%107% Dibromofluoromethane 04/11/14 U 70 - 130 %%102% Toluene-d8 04/11/14 U 70 - 130 %%
Per 1.4.6 of EPA method 8270D, 1,2-Diphenylhydrazine is unstable and readily converts to Azobenzene. Azobenzene is used for the calibration of 1,2-Diphenylhydrazine.
Please be advised that the NY unrestricted soil criteria for chromium is based on hexavalent chromium and trivalent chromium.
All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments.
1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.B = Present in blank, no bias suspected.
If there are any questions regarding this data, please call Phoenix Client Services at extension 200.This report must not be reproduced except in full as defined by the attached chain of custody.
Reviewed and Released by: Greg Lawrence, Assistant Lab Director
RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level LOD=Limit of Detection MDL=Method Detection Limit
Page 43 of 49 Ver 1
Sample Information Custody InformationMatrix:Location Code:Rush Request:P.O.#:
Collected by:Received by:Analyzed by:
SOLIDEBC72 Hour
04/08/14SWsee "By" below
Laboratory Data
TRIP BLANK HIGH
Phoenix ID: BG30371
04/09/140:00
16:26
Parameter ResultRL/PQL Units Date/Time By Reference
FOR: Attn: Mr. Charles B. Sosik, P.G.Environmental Business Consultants1808 Middle Country RdRidge NY 11961-2406
VolatilesND1,1,1,2-Tetrachloroethane 250 04/10/14 U SW8260ug/Kg41ND1,1,1-Trichloroethane 250 04/10/14 U SW8260ug/Kg50ND1,1,2,2-Tetrachloroethane 250 04/10/14 U SW8260ug/Kg36ND1,1,2-Trichloroethane 250 04/10/14 U SW8260ug/Kg25ND1,1-Dichloroethane 250 04/10/14 U SW8260ug/Kg50ND1,1-Dichloroethene 250 04/10/14 U SW8260ug/Kg55ND1,1-Dichloropropene 250 04/10/14 U SW8260ug/Kg49ND1,2,3-Trichlorobenzene 250 04/10/14 U SW8260ug/Kg50ND1,2,3-Trichloropropane 250 04/10/14 U SW8260ug/Kg36ND1,2,4-Trichlorobenzene 250 04/10/14 U SW8260ug/Kg50ND1,2,4-Trimethylbenzene 250 04/10/14 U SW8260ug/Kg36ND1,2-Dibromo-3-chloropropane 250 04/10/14 U SW8260ug/Kg67ND1,2-Dibromoethane 250 04/10/14 U SW8260ug/Kg67ND1,2-Dichlorobenzene 250 04/10/14 U SW8260ug/Kg28ND1,2-Dichloroethane 250 04/10/14 U SW8260ug/Kg22ND1,2-Dichloropropane 250 04/10/14 U SW8260ug/Kg36ND1,3,5-Trimethylbenzene 250 04/10/14 U SW8260ug/Kg33ND1,3-Dichlorobenzene 250 04/10/14 U SW8260ug/Kg37ND1,3-Dichloropropane 250 04/10/14 U SW8260ug/Kg27ND1,4-Dichlorobenzene 250 04/10/14 U SW8260ug/Kg40ND2,2-Dichloropropane 250 04/10/14 U SW8260ug/Kg42ND2-Chlorotoluene 250 04/10/14 U SW8260ug/Kg40ND2-Hexanone 1300 04/10/14 U SW8260ug/Kg110ND2-Isopropyltoluene 250 04/10/14 U SW8260ug/Kg 135ND4-Chlorotoluene 250 04/10/14 U SW8260ug/Kg29
Page 44 of 49 Ver 1
TRIP BLANK HIGHPhoenix I.D.: BG30371
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
ND4-Methyl-2-pentanone 1300 04/10/14 U SW8260ug/Kg60NDAcetone 2500 04/10/14 U SW8260ug/Kg250NDAcrylonitrile 500 04/10/14 U SW8260ug/Kg140NDBenzene 250 04/10/14 U SW8260ug/Kg50NDBromobenzene 250 04/10/14 U SW8260ug/Kg33NDBromochloromethane 250 04/10/14 U SW8260ug/Kg37NDBromodichloromethane 250 04/10/14 U SW8260ug/Kg31NDBromoform 250 04/10/14 U SW8260ug/Kg35NDBromomethane 250 04/10/14 U SW8260ug/Kg190NDCarbon Disulfide 250 04/10/14 U SW8260ug/Kg41NDCarbon tetrachloride 250 04/10/14 U SW8260ug/Kg29NDChlorobenzene 250 04/10/14 U SW8260ug/Kg37NDChloroethane 250 04/10/14 U SW8260ug/Kg59NDChloroform 250 04/10/14 U SW8260ug/Kg46NDChloromethane 250 04/10/14 U SW8260ug/Kg130NDcis-1,2-Dichloroethene 250 04/10/14 U SW8260ug/Kg55NDcis-1,3-Dichloropropene 250 04/10/14 U SW8260ug/Kg27NDDibromochloromethane 250 04/10/14 U SW8260ug/Kg28NDDibromomethane 250 04/10/14 U SW8260ug/Kg32NDDichlorodifluoromethane 250 04/10/14 U SW8260ug/Kg67NDEthylbenzene 250 04/10/14 U SW8260ug/Kg46NDHexachlorobutadiene 250 04/10/14 U SW8260ug/Kg53NDIsopropylbenzene 250 04/10/14 U SW8260ug/Kg48NDm&p-Xylene 250 04/10/14 U SW8260ug/Kg99NDMethyl Ethyl Ketone 1500 04/10/14 U SW8260ug/Kg220NDMethyl t-butyl ether (MTBE) 500 04/10/14 U SW8260ug/Kg69NDMethylene chloride 250 04/10/14 U SW8260ug/Kg41NDNaphthalene 250 04/10/14 U SW8260ug/Kg67NDn-Butylbenzene 250 04/10/14 U SW8260ug/Kg46NDn-Propylbenzene 250 04/10/14 U SW8260ug/Kg45NDo-Xylene 250 04/10/14 U SW8260ug/Kg96NDp-Isopropyltoluene 250 04/10/14 U SW8260ug/Kg36NDsec-Butylbenzene 250 04/10/14 U SW8260ug/Kg47NDStyrene 250 04/10/14 U SW8260ug/Kg72NDtert-Butylbenzene 250 04/10/14 U SW8260ug/Kg40NDTetrachloroethene 250 04/10/14 U SW8260ug/Kg53NDTetrahydrofuran (THF) 500 04/10/14 U SW8260ug/Kg 1230NDToluene 250 04/10/14 U SW8260ug/Kg40NDtrans-1,2-Dichloroethene 250 04/10/14 U SW8260ug/Kg50NDtrans-1,3-Dichloropropene 250 04/10/14 U SW8260ug/Kg51NDtrans-1,4-dichloro-2-butene 500 04/10/14 U SW8260ug/Kg460NDTrichloroethene 250 04/10/14 U SW8260ug/Kg53NDTrichlorofluoromethane 250 04/10/14 U SW8260ug/Kg56NDTrichlorotrifluoroethane 250 04/10/14 U SW8260ug/Kg39NDVinyl chloride 250 04/10/14 U SW8260ug/Kg81
QA/QC Surrogates105% 1,2-dichlorobenzene-d4 04/10/14 U 70 - 130 %%95% Bromofluorobenzene 04/10/14 U 70 - 130 %%103% Dibromofluoromethane 04/10/14 U 70 - 130 %%
Page 45 of 49 Ver 1
TRIP BLANK HIGHPhoenix I.D.: BG30371
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
101% Toluene-d8 04/10/14 U 70 - 130 %%
Comments:
TRIP BLANK INCLUDED. %SOLIDS ASSUMED 100%
This sample was not collected in accordance with EPA method 5035. NELAC requires the laboratory to qualify the volatile soil data as biased low.
All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments.
1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.
If there are any questions regarding this data, please call Phoenix Client Services at extension 200.This report must not be reproduced except in full as defined by the attached chain of custody.
Reviewed and Released by: Greg Lawrence, Assistant Lab Director
RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level LOD=Limit of Detection MDL=Method Detection Limit
Page 46 of 49 Ver 1
Sample Information Custody InformationMatrix:Location Code:Rush Request:P.O.#:
Collected by:Received by:Analyzed by:
SOLIDEBC72 Hour
04/08/14SWsee "By" below
Laboratory Data
TRIP BLANK LOW
Phoenix ID: BG30372
04/09/140:00
16:26
Parameter ResultRL/PQL Units Date/Time By Reference
FOR: Attn: Mr. Charles B. Sosik, P.G.Environmental Business Consultants1808 Middle Country RdRidge NY 11961-2406
VolatilesND1,1,1,2-Tetrachloroethane 5.0 04/11/14 U SW8260ug/Kg0.82ND1,1,1-Trichloroethane 5.0 04/11/14 U SW8260ug/Kg1.0ND1,1,2,2-Tetrachloroethane 5.0 04/11/14 U SW8260ug/Kg0.71ND1,1,2-Trichloroethane 5.0 04/11/14 U SW8260ug/Kg0.49ND1,1-Dichloroethane 5.0 04/11/14 U SW8260ug/Kg0.99ND1,1-Dichloroethene 5.0 04/11/14 U SW8260ug/Kg1.1ND1,1-Dichloropropene 5.0 04/11/14 U SW8260ug/Kg0.97ND1,2,3-Trichlorobenzene 5.0 04/11/14 U SW8260ug/Kg1.0ND1,2,3-Trichloropropane 5.0 04/11/14 U SW8260ug/Kg0.71ND1,2,4-Trichlorobenzene 5.0 04/11/14 U SW8260ug/Kg1.0ND1,2,4-Trimethylbenzene 5.0 04/11/14 U SW8260ug/Kg0.72ND1,2-Dibromo-3-chloropropane 5.0 04/11/14 U SW8260ug/Kg1.3ND1,2-Dibromoethane 5.0 04/11/14 U SW8260ug/Kg1.3ND1,2-Dichlorobenzene 5.0 04/11/14 U SW8260ug/Kg0.55ND1,2-Dichloroethane 5.0 04/11/14 U SW8260ug/Kg0.44ND1,2-Dichloropropane 5.0 04/11/14 U SW8260ug/Kg0.71ND1,3,5-Trimethylbenzene 5.0 04/11/14 U SW8260ug/Kg0.66ND1,3-Dichlorobenzene 5.0 04/11/14 U SW8260ug/Kg0.74ND1,3-Dichloropropane 5.0 04/11/14 U SW8260ug/Kg0.53ND1,4-Dichlorobenzene 5.0 04/11/14 U SW8260ug/Kg0.79ND2,2-Dichloropropane 5.0 04/11/14 U SW8260ug/Kg0.84ND2-Chlorotoluene 5.0 04/11/14 U SW8260ug/Kg0.80ND2-Hexanone 25 04/11/14 U SW8260ug/Kg2.3ND2-Isopropyltoluene 5.0 04/11/14 U SW8260ug/Kg 10.69
Page 47 of 49 Ver 1
TRIP BLANK LOWPhoenix I.D.: BG30372
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
ND4-Chlorotoluene 5.0 04/11/14 U SW8260ug/Kg0.58ND4-Methyl-2-pentanone 25 04/11/14 U SW8260ug/Kg1.2NDAcetone 50 04/11/14 U SW8260ug/Kg5.0NDAcrylonitrile 10 04/11/14 U SW8260ug/Kg2.8NDBenzene 5.0 04/11/14 U SW8260ug/Kg0.99NDBromobenzene 5.0 04/11/14 U SW8260ug/Kg0.65NDBromochloromethane 5.0 04/11/14 U SW8260ug/Kg0.73NDBromodichloromethane 5.0 04/11/14 U SW8260ug/Kg0.62NDBromoform 5.0 04/11/14 U SW8260ug/Kg0.70NDBromomethane 5.0 04/11/14 U SW8260ug/Kg3.9NDCarbon Disulfide 5.0 04/11/14 U SW8260ug/Kg0.81NDCarbon tetrachloride 5.0 04/11/14 U SW8260ug/Kg0.58NDChlorobenzene 5.0 04/11/14 U SW8260ug/Kg0.74NDChloroethane 5.0 04/11/14 U SW8260ug/Kg1.2NDChloroform 5.0 04/11/14 U SW8260ug/Kg0.91NDChloromethane 5.0 04/11/14 U SW8260ug/Kg2.6NDcis-1,2-Dichloroethene 5.0 04/11/14 U SW8260ug/Kg1.1NDcis-1,3-Dichloropropene 5.0 04/11/14 U SW8260ug/Kg0.54NDDibromochloromethane 5.0 04/11/14 U SW8260ug/Kg0.56NDDibromomethane 5.0 04/11/14 U SW8260ug/Kg0.63NDDichlorodifluoromethane 5.0 04/11/14 U SW8260ug/Kg1.3NDEthylbenzene 5.0 04/11/14 U SW8260ug/Kg0.91NDHexachlorobutadiene 5.0 04/11/14 U SW8260ug/Kg1.1NDIsopropylbenzene 5.0 04/11/14 U SW8260ug/Kg0.96NDm&p-Xylene 5.0 04/11/14 U SW8260ug/Kg2.0NDMethyl Ethyl Ketone 30 04/11/14 U SW8260ug/Kg4.3NDMethyl t-butyl ether (MTBE) 10 04/11/14 U SW8260ug/Kg1.4NDMethylene chloride 5.0 04/11/14 U SW8260ug/Kg0.82NDNaphthalene 5.0 04/11/14 U SW8260ug/Kg1.3NDn-Butylbenzene 5.0 04/11/14 U SW8260ug/Kg0.91NDn-Propylbenzene 5.0 04/11/14 U SW8260ug/Kg0.90NDo-Xylene 5.0 04/11/14 U SW8260ug/Kg1.9NDp-Isopropyltoluene 5.0 04/11/14 U SW8260ug/Kg0.72NDsec-Butylbenzene 5.0 04/11/14 U SW8260ug/Kg0.94NDStyrene 5.0 04/11/14 U SW8260ug/Kg1.4NDtert-Butylbenzene 5.0 04/11/14 U SW8260ug/Kg0.80NDTetrachloroethene 5.0 04/11/14 U SW8260ug/Kg1.1NDTetrahydrofuran (THF) 10 04/11/14 U SW8260ug/Kg 14.5NDToluene 5.0 04/11/14 U SW8260ug/Kg0.79NDtrans-1,2-Dichloroethene 5.0 04/11/14 U SW8260ug/Kg1.0NDtrans-1,3-Dichloropropene 5.0 04/11/14 U SW8260ug/Kg1.0NDtrans-1,4-dichloro-2-butene 10 04/11/14 U SW8260ug/Kg9.3NDTrichloroethene 5.0 04/11/14 U SW8260ug/Kg1.1NDTrichlorofluoromethane 5.0 04/11/14 U SW8260ug/Kg1.1NDTrichlorotrifluoroethane 5.0 04/11/14 U SW8260ug/Kg0.78NDVinyl chloride 5.0 04/11/14 U SW8260ug/Kg1.6
QA/QC Surrogates103% 1,2-dichlorobenzene-d4 04/11/14 U 70 - 130 %%93% Bromofluorobenzene 04/11/14 U 70 - 130 %%
Page 48 of 49 Ver 1
TRIP BLANK LOWPhoenix I.D.: BG30372
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
91% Dibromofluoromethane 04/11/14 U 70 - 130 %%102% Toluene-d8 04/11/14 U 70 - 130 %%
Comments:
TRIP BLANK INCLUDED. %SOLIDS ASSUMED 100%
All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments.
1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.
If there are any questions regarding this data, please call Phoenix Client Services at extension 200.This report must not be reproduced except in full as defined by the attached chain of custody.
Reviewed and Released by: Greg Lawrence, Assistant Lab Director
RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level LOD=Limit of Detection MDL=Method Detection Limit
Additional 8270 criteria: 20% of compounds can be outside of acceptance criteria as long as recovery is at least 10%. (Acid surrogates acceptance range for aqueous samples: 15-110%, for soils 30-130%)
Additional 8260 criteria: 10% of LCS/LCSD compounds can be outside of acceptance criteria as long as recovery is 40-160%.
Comment:
l = This parameter is outside laboratory lcs/lcsd specified recovery limits.m = This parameter is outside laboratory ms/msd specified recovery limits.r = This parameter is outside laboratory rpd specified recovery limits.
MS - Matrix SpikePhyllis Shiller, Laboratory Director
If there are any questions regarding this data, please call Phoenix Client Services at extension 200.
April 16, 2014MS Dup - Matrix Spike Duplicate
RPD - Relative Percent Difference
LCS - Laboratory Control SampleLCSD - Laboratory Control Sample Duplicate
NC - No Criteria
Intf - Interference
Page 7 of 7
Sample Criteria Exceedences ReportWednesday, April 16, 2014 Page 1 of 2
Phoenix Laboratories does not assume responsibility for the data contained in this report. It is provided as an additional tool to identify requested criteria exceedences. All efforts are made to ensure the accuracy of the data (obtained from appropriate agencies). A lack of exceedence information does not necessarily suggest conformance to the criteria. It is ultimately the site professional's responsibility to determine appropriate compliance.
This laboratory is in compliance with the NELAC requirements of procedures used except where indicated.
This report contains results for the parameters tested, under the sampling conditions described on the Chain Of Custody, as received by the laboratory.
A scanned version of the COC form accompanies the analytical report and is an exact duplicate of the original.
CompletedDissolved Mercury Digestion 05/12/14 I/I SW7470CompletedPCB Extraction (2 Liter) 05/09/14 L SW3510CompletedExtraction for Pest (2 Liter) 05/09/14 L SW3510CompletedSemi-Volatile Extraction 05/09/14 E/X SW3520
Page 1 of 6 Ver 1
E-MW 3Phoenix I.D.: BG43036
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
CompletedDissolved Metals Preparation 05/09/14 AG SW846-3005
PesticidesND4,4' -DDD 0.14 05/13/14 CE SW8081ug/L0.14ND4,4' -DDE 0.14 05/13/14 CE SW8081ug/L0.14ND4,4' -DDT 0.14 05/13/14 CE SW8081ug/L0.14NDa-BHC 0.069 05/13/14 CE SW8081ug/L0.069NDa-chlordane 0.14 05/13/14 CE SW8081ug/L0.14NDAlachlor 1.0 05/13/14 CE SW8081ug/L 11.0NDAldrin 0.021 05/13/14 CE SW8081ug/L0.021NDb-BHC 0.069 05/13/14 CE SW8081ug/L0.069NDChlordane 1.4 05/13/14 CE SW8081ug/L1.4NDd-BHC 0.069 05/13/14 CE SW8081ug/L0.069NDDieldrin 0.021 05/13/14 CE SW8081ug/L0.021NDEndosulfan I 0.14 05/13/14 CE SW8081ug/L0.14NDEndosulfan II 0.14 05/13/14 CE SW8081ug/L0.14NDEndosulfan Sulfate 0.14 05/13/14 CE SW8081ug/L0.14NDEndrin 0.14 05/13/14 CE SW8081ug/L0.14NDEndrin Aldehyde 0.14 05/13/14 CE SW8081ug/L0.14NDEndrin ketone 0.14 05/13/14 CE SW8081ug/L0.14NDg-BHC (Lindane) 0.069 05/13/14 CE SW8081ug/L0.069NDg-chlordane 0.14 05/13/14 CE SW8081ug/L0.14NDHeptachlor 0.14 05/13/14 CE SW8081ug/L0.14NDHeptachlor epoxide 0.14 05/13/14 CE SW8081ug/L0.14NDMethoxychlor 1.4 05/13/14 CE SW8081ug/L1.4NDToxaphene 3.5 05/13/14 CE SW8081ug/L3.5
QA/QC SurrogatesDiluted Out%DCBP (Surrogate Rec) 05/13/14 CE SW8081%Diluted Out%TCMX (Surrogate Rec) 05/13/14 CE SW8081%
Polychlorinated BiphenylsNDPCB-1016 0.069 05/12/14 AW 608/ 8082ug/L0.069NDPCB-1221 0.069 05/12/14 AW 608/ 8082ug/L0.069NDPCB-1232 0.069 05/12/14 AW 608/ 8082ug/L0.069NDPCB-1242 0.069 05/12/14 AW 608/ 8082ug/L0.069NDPCB-1248 0.069 05/12/14 AW 608/ 8082ug/L0.069NDPCB-1254 0.069 05/12/14 AW 608/ 8082ug/L0.069NDPCB-1260 0.069 05/12/14 AW 608/ 8082ug/L0.069NDPCB-1262 0.069 05/12/14 AW 608/ 8082ug/L0.069NDPCB-1268 0.069 05/12/14 AW 608/ 8082ug/L0.069
QA/QC Surrogates53% DCBP 05/12/14 AW 608/ 8082%67% TCMX 05/12/14 AW 608/ 8082%
Per 1.4.6 of EPA method 8270D, 1,2-Diphenylhydrazine is unstable and readily converts to Azobenzene. Azobenzene is used for the calibration of 1,2-Diphenylhydrazine.
Due to a matrix interference and/or the presence of a large amount of non-target material in the sample, an elevated RL was reported for the pesticide analysis.
Phyllis Shiller, Laboratory DirectorMay 16, 2014
1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.3 = This parameter exceeds laboratory specified limits.
If there are any questions regarding this data, please call Phoenix Client Services at extension 200.This report must not be reproduced except in full as defined by the attached chain of custody.
Reviewed and Released by: Bobbi Aloisa, Vice President
RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level LOD=Limit of Detection MDL=Method Detection Limit
Page 6 of 6 Ver 1
Sample Criteria Exceedences ReportFriday, May 16, 2014 Page 1 of 2
D-AL Aluminum (Dissolved) 0.10.39 0.01 mg/LBG43036 NY / TOGS - Water Quality / GA Criteria 0.1DFE-WMDP Iron, (Dissolved) 0.30.38 0.01 mg/LBG43036 NY / TOGS - Water Quality / GA Criteria 0.3D-NA Sodium (Dissolved) 2087.5 1.1 mg/LBG43036 NY / TOGS - Water Quality / GA Criteria 20DSE-WMDP Selenium, (Dissolved) 0.010.068 0.004 mg/LBG43036 NY / TOGS - Water Quality / GA Criteria 0.01DTL-WMDP Thallium , (Dissolved) 0.0005BRL 0.001 mg/LBG43036 NY / TOGS - Water Quality / GA Criteria 0.0005
Phoenix Laboratories does not assume responsibility for the data contained in this report. It is provided as an additional tool to identify requested criteria exceedences. All efforts are made to ensure the accuracy of the data (obtained from appropriate agencies). A lack of exceedence information does not necessarily suggest conformance to the criteria. It is ultimately the site professional's responsibility to determine appropriate compliance.
This laboratory is in compliance with the NELAC requirements of procedures used except where indicated.
This report contains results for the parameters tested, under the sampling conditions described on the Chain Of Custody, as received by the laboratory.
A scanned version of the COC form accompanies the analytical report and is an exact duplicate of the original.
1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.
If there are any questions regarding this data, please call Phoenix Client Services at extension 200.This report must not be reproduced except in full as defined by the attached chain of custody.
Reviewed and Released by: Greg Lawrence, Assistant Lab Director
RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level
Page 3 of 12 Ver 1
Sample Information Custody InformationMatrix:Location Code:Rush Request:P.O.#:
Collected by:Received by:Analyzed by:
AIREBC72 Hour
04/09/14SWsee "By" below
DM
Laboratory Data
E-SG3
Phoenix ID: BG31848
04/11/1410:4317:36
Parameterppbv
ResultppbvRL
ug/m3Result Date/Time By Reference
FOR: Attn: Mr. Charles B. Sosik, P.G.Environmental Business Consultants1808 Middle Country RdRidge NY 11961-2406
1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.
If there are any questions regarding this data, please call Phoenix Client Services at extension 200.This report must not be reproduced except in full as defined by the attached chain of custody.
Reviewed and Released by: Greg Lawrence, Assistant Lab Director
RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level
Page 6 of 12 Ver 1
Sample Information Custody InformationMatrix:Location Code:Rush Request:P.O.#:
Collected by:Received by:Analyzed by:
AIREBC72 Hour
04/09/14SWsee "By" below
DM
Laboratory Data
E-SG4
Phoenix ID: BG31849
04/11/1410:4617:36
Parameterppbv
ResultppbvRL
ug/m3Result Date/Time By Reference
FOR: Attn: Mr. Charles B. Sosik, P.G.Environmental Business Consultants1808 Middle Country RdRidge NY 11961-2406
1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.
If there are any questions regarding this data, please call Phoenix Client Services at extension 200.This report must not be reproduced except in full as defined by the attached chain of custody.
Reviewed and Released by: Greg Lawrence, Assistant Lab Director
RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level
Page 9 of 12 Ver 1
Sample Information Custody InformationMatrix:Location Code:Rush Request:P.O.#:
Collected by:Received by:Analyzed by:
AIREBC72 Hour
04/09/14SWsee "By" below
DM
Laboratory Data
E-SG5
Phoenix ID: BG31850
04/11/1410:2517:36
Parameterppbv
ResultppbvRL
ug/m3Result Date/Time By Reference
FOR: Attn: Mr. Charles B. Sosik, P.G.Environmental Business Consultants1808 Middle Country RdRidge NY 11961-2406
1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.
If there are any questions regarding this data, please call Phoenix Client Services at extension 200.This report must not be reproduced except in full as defined by the attached chain of custody.
Reviewed and Released by: Greg Lawrence, Assistant Lab Director
RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level
Phoenix Laboratories does not assume responsibility for the data contained in this report. It is provided as an additional tool to identify requested criteria exceedences. All efforts are made to ensure the accuracy of the data (obtained from appropriate agencies). A lack of exceedence information does not necessarily suggest conformance to the criteria. It is ultimately the site professional's responsibility to determine appropriate compliance.
BG29068 - BG29075
Tuesday, April 15, 2014
Sample ID#s:
Attn: Mr. Charles B. Sosik, P.G.Environmental Business Consultants1808 Middle Country RdRidge NY 11961-2406
Project ID: DOMINO SUGAR SITE
Sincerely yours,
Laboratory DirectorPhyllis Shiller
If you have any questions concerning this testing, please do not hesitate to contact Phoenix Client Services at ext. 200.
This laboratory is in compliance with the NELAC requirements of procedures used except where indicated.
This report contains results for the parameters tested, under the sampling conditions described on the Chain Of Custody, as received by the laboratory.
All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments.
A scanned version of the COC form accompanies the analytical report and is an exact duplicate of the original.
Polychlorinated BiphenylsNDPCB-1016 38 04/08/14 AW SW 8082ug/Kg38NDPCB-1221 38 04/08/14 AW SW 8082ug/Kg38NDPCB-1232 38 04/08/14 AW SW 8082ug/Kg38NDPCB-1242 38 04/08/14 AW SW 8082ug/Kg38NDPCB-1248 38 04/08/14 AW SW 8082ug/Kg38NDPCB-1254 38 04/08/14 AW SW 8082ug/Kg38NDPCB-1260 38 04/08/14 AW SW 8082ug/Kg38NDPCB-1262 38 04/08/14 AW SW 8082ug/Kg38NDPCB-1268 38 04/08/14 AW SW 8082ug/Kg38
QA/QC Surrogates113% DCBP 04/08/14 AW 30 - 150 %%88% TCMX 04/08/14 AW 30 - 150 %%
Pesticides - SoilND4,4' -DDD 2.8 04/09/14 CE SW8081ug/Kg2.8ND4,4' -DDE 2.8 04/09/14 CE SW8081ug/Kg2.8ND4,4' -DDT 2.8 04/09/14 CE SW8081ug/Kg2.8NDa-BHC 1.9 04/09/14 CE SW8081ug/Kg1.9NDa-Chlordane 3.8 04/09/14 CE SW8081ug/Kg3.8NDAldrin 1.9 04/09/14 CE SW8081ug/Kg1.9NDb-BHC 1.9 04/09/14 CE SW8081ug/Kg1.9NDChlordane 23 04/09/14 CE SW8081ug/Kg23NDd-BHC 1.9 04/09/14 CE SW8081ug/Kg1.9NDDieldrin 1.9 04/09/14 CE SW8081ug/Kg1.9NDEndosulfan I 3.8 04/09/14 CE SW8081ug/Kg3.8NDEndosulfan II 3.8 04/09/14 CE SW8081ug/Kg3.8NDEndosulfan sulfate 3.8 04/09/14 CE SW8081ug/Kg3.8NDEndrin 1.9 04/09/14 CE SW8081ug/Kg1.9NDEndrin aldehyde 3.8 04/09/14 CE SW8081ug/Kg3.8NDEndrin ketone 1.9 04/09/14 CE SW8081ug/Kg1.9NDg-BHC 1.9 04/09/14 CE SW8081ug/Kg1.9NDg-Chlordane 3.8 04/09/14 CE SW8081ug/Kg3.8NDHeptachlor 1.9 04/09/14 CE SW8081ug/Kg1.9NDHeptachlor epoxide 1.9 04/09/14 CE SW8081ug/Kg1.9NDMethoxychlor 92 04/09/14 CE SW8081ug/Kg92NDToxaphene 190 04/09/14 CE SW8081ug/Kg190
QA/QC SurrogatesInterference% DCBP 04/09/14 CE 30 - 150 %%
Per 1.4.6 of EPA method 8270D, 1,2-Diphenylhydrazine is unstable and readily converts to Azobenzene. Azobenzene is used for the calibration of 1,2-Diphenylhydrazine.
Please be advised that the NY unrestricted soil criteria for chromium is based on hexavalent chromium and trivalent chromium.
Semi-Volatile Comment:Due to a matrix interference and/or the presence of a large amount of non-target material in the sample, a dilution was required resulting in an elevated RL for the semivolatile analysis.
Due to a matrix interference and/or the presence of a large amount of non-target material in the sample, an elevated RL was reported for the pesticide analysis.
All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments.
1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.B = Present in blank, no bias suspected.
If there are any questions regarding this data, please call Phoenix Client Services at extension 200.This report must not be reproduced except in full as defined by the attached chain of custody.
Reviewed and Released by: Greg Lawrence, Assistant Lab Director
RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level LOD=Limit of Detection MDL=Method Detection Limit
Page 6 of 40 Ver 1
Sample Information Custody InformationMatrix:Location Code:Rush Request:P.O.#:
Collected by:Received by:Analyzed by:
SOLIDEBC72 Hour
04/02/14SWsee "By" below
Laboratory Data
E-SB4 0-2
Phoenix ID: BG29069
04/07/140:00
17:33
Parameter ResultRL/PQL Units Date/Time By Reference
FOR: Attn: Mr. Charles B. Sosik, P.G.Environmental Business Consultants1808 Middle Country RdRidge NY 11961-2406
Polychlorinated BiphenylsNDPCB-1016 38 04/08/14 AW SW 8082ug/Kg38NDPCB-1221 38 04/08/14 AW SW 8082ug/Kg38NDPCB-1232 38 04/08/14 AW SW 8082ug/Kg38NDPCB-1242 38 04/08/14 AW SW 8082ug/Kg38NDPCB-1248 38 04/08/14 AW SW 8082ug/Kg38NDPCB-1254 38 04/08/14 AW SW 8082ug/Kg38NDPCB-1260 38 04/08/14 AW SW 8082ug/Kg38NDPCB-1262 38 04/08/14 AW SW 8082ug/Kg38NDPCB-1268 38 04/08/14 AW SW 8082ug/Kg38
QA/QC Surrogates96% DCBP 04/08/14 AW 30 - 150 %%88% TCMX 04/08/14 AW 30 - 150 %%
Pesticides - SoilND4,4' -DDD 2.7 04/09/14 CE SW8081ug/Kg2.7ND4,4' -DDE 2.7 04/09/14 CE SW8081ug/Kg2.7ND4,4' -DDT 2.7 04/09/14 CE SW8081ug/Kg2.7NDa-BHC 1.9 04/09/14 CE SW8081ug/Kg1.9NDa-Chlordane 3.8 04/09/14 CE SW8081ug/Kg3.8NDAldrin 1.9 04/09/14 CE SW8081ug/Kg1.9NDb-BHC 1.9 04/09/14 CE SW8081ug/Kg1.9NDChlordane 23 04/09/14 CE SW8081ug/Kg23NDd-BHC 1.9 04/09/14 CE SW8081ug/Kg1.9NDDieldrin 1.9 04/09/14 CE SW8081ug/Kg1.9NDEndosulfan I 3.8 04/09/14 CE SW8081ug/Kg3.8NDEndosulfan II 3.8 04/09/14 CE SW8081ug/Kg3.8NDEndosulfan sulfate 3.8 04/09/14 CE SW8081ug/Kg3.8NDEndrin 1.9 04/09/14 CE SW8081ug/Kg1.9NDEndrin aldehyde 3.8 04/09/14 CE SW8081ug/Kg3.8NDEndrin ketone 1.9 04/09/14 CE SW8081ug/Kg1.9NDg-BHC 1.9 04/09/14 CE SW8081ug/Kg1.9NDg-Chlordane 3.8 04/09/14 CE SW8081ug/Kg3.8NDHeptachlor 1.9 04/09/14 CE SW8081ug/Kg1.9NDHeptachlor epoxide 1.9 04/09/14 CE SW8081ug/Kg1.9NDMethoxychlor 7.6 04/09/14 CE SW8081ug/Kg7.6NDToxaphene 190 04/09/14 CE SW8081ug/Kg190
QA/QC SurrogatesInterference% DCBP 04/09/14 CE 30 - 150 %%
91% TCMX 04/09/14 CE 30 - 150 %%
VolatilesND1,1,1,2-Tetrachloroethane 8.0 04/10/14 U SW8260ug/Kg1.3ND1,1,1-Trichloroethane 8.0 04/10/14 U SW8260ug/Kg1.6ND1,1,2,2-Tetrachloroethane 8.0 04/10/14 U SW8260ug/Kg1.1ND1,1,2-Trichloroethane 8.0 04/10/14 U SW8260ug/Kg0.78ND1,1-Dichloroethane 8.0 04/10/14 U SW8260ug/Kg1.6
Page 8 of 40 Ver 1
E-SB4 0-2Phoenix I.D.: BG29069
Client ID:DOMINO SUGAR SITEProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
ND1,1-Dichloroethene 8.0 04/10/14 U SW8260ug/Kg1.7ND1,1-Dichloropropene 8.0 04/10/14 U SW8260ug/Kg1.5ND1,2,3-Trichlorobenzene 8.0 04/10/14 U SW8260ug/Kg1.6ND1,2,3-Trichloropropane 8.0 04/10/14 U SW8260ug/Kg1.1ND1,2,4-Trichlorobenzene 8.0 04/10/14 U SW8260ug/Kg1.6ND1,2,4-Trimethylbenzene 8.0 04/10/14 U SW8260ug/Kg1.1ND1,2-Dibromo-3-chloropropane 8.0 04/10/14 U SW8260ug/Kg2.1ND1,2-Dibromoethane 8.0 04/10/14 U SW8260ug/Kg2.1ND1,2-Dichlorobenzene 8.0 04/10/14 U SW8260ug/Kg0.88ND1,2-Dichloroethane 8.0 04/10/14 U SW8260ug/Kg0.70ND1,2-Dichloropropane 8.0 04/10/14 U SW8260ug/Kg1.1ND1,3,5-Trimethylbenzene 8.0 04/10/14 U SW8260ug/Kg1.1ND1,3-Dichlorobenzene 8.0 04/10/14 U SW8260ug/Kg1.2ND1,3-Dichloropropane 8.0 04/10/14 U SW8260ug/Kg0.84ND1,4-Dichlorobenzene 8.0 04/10/14 U SW8260ug/Kg1.3ND2,2-Dichloropropane 8.0 04/10/14 U SW8260ug/Kg1.3ND2-Chlorotoluene 8.0 04/10/14 U SW8260ug/Kg1.3ND2-Hexanone 40 04/10/14 U SW8260ug/Kg3.6ND2-Isopropyltoluene 8.0 04/10/14 U SW8260ug/Kg 11.1ND4-Chlorotoluene 8.0 04/10/14 U SW8260ug/Kg0.92ND4-Methyl-2-pentanone 40 04/10/14 U SW8260ug/Kg1.9NDAcetone 50 04/10/14 U SW8260ug/Kg7.9NDAcrylonitrile 16 04/10/14 U SW8260ug/Kg4.5NDBenzene 8.0 04/10/14 U SW8260ug/Kg1.6NDBromobenzene 8.0 04/10/14 U SW8260ug/Kg1.0NDBromochloromethane 8.0 04/10/14 U SW8260ug/Kg1.2NDBromodichloromethane 8.0 04/10/14 U SW8260ug/Kg0.99NDBromoform 8.0 04/10/14 U SW8260ug/Kg1.1NDBromomethane 8.0 04/10/14 U SW8260ug/Kg6.1NDCarbon Disulfide 8.0 04/10/14 U SW8260ug/Kg1.3NDCarbon tetrachloride 8.0 04/10/14 U SW8260ug/Kg0.92NDChlorobenzene 8.0 04/10/14 U SW8260ug/Kg1.2NDChloroethane 8.0 04/10/14 U SW8260ug/Kg1.9NDChloroform 8.0 04/10/14 U SW8260ug/Kg1.4NDChloromethane 8.0 04/10/14 U SW8260ug/Kg4.2NDcis-1,2-Dichloroethene 8.0 04/10/14 U SW8260ug/Kg1.7NDcis-1,3-Dichloropropene 8.0 04/10/14 U SW8260ug/Kg0.86NDDibromochloromethane 8.0 04/10/14 U SW8260ug/Kg0.89NDDibromomethane 8.0 04/10/14 U SW8260ug/Kg1.0NDDichlorodifluoromethane 8.0 04/10/14 U SW8260ug/Kg2.1NDEthylbenzene 8.0 04/10/14 U SW8260ug/Kg1.4NDHexachlorobutadiene 8.0 04/10/14 U SW8260ug/Kg1.7NDIsopropylbenzene 8.0 04/10/14 U SW8260ug/Kg1.5NDm&p-Xylene 8.0 04/10/14 U SW8260ug/Kg3.1NDMethyl Ethyl Ketone 48 04/10/14 U SW8260ug/Kg6.9NDMethyl t-butyl ether (MTBE) 16 04/10/14 U SW8260ug/Kg2.2NDMethylene chloride 8.0 04/10/14 U SW8260ug/Kg1.3NDNaphthalene 8.0 04/10/14 U SW8260ug/Kg2.1NDn-Butylbenzene 8.0 04/10/14 U SW8260ug/Kg1.4
Page 9 of 40 Ver 1
E-SB4 0-2Phoenix I.D.: BG29069
Client ID:DOMINO SUGAR SITEProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
NDn-Propylbenzene 8.0 04/10/14 U SW8260ug/Kg1.4NDo-Xylene 8.0 04/10/14 U SW8260ug/Kg3.0NDp-Isopropyltoluene 8.0 04/10/14 U SW8260ug/Kg1.1NDsec-Butylbenzene 8.0 04/10/14 U SW8260ug/Kg1.5NDStyrene 8.0 04/10/14 U SW8260ug/Kg2.3NDtert-Butylbenzene 8.0 04/10/14 U SW8260ug/Kg1.3NDTetrachloroethene 8.0 04/10/14 U SW8260ug/Kg1.7NDTetrahydrofuran (THF) 16 04/10/14 U SW8260ug/Kg 17.2NDToluene 8.0 04/10/14 U SW8260ug/Kg1.3NDtrans-1,2-Dichloroethene 8.0 04/10/14 U SW8260ug/Kg1.6NDtrans-1,3-Dichloropropene 8.0 04/10/14 U SW8260ug/Kg1.6NDtrans-1,4-dichloro-2-butene 16 04/10/14 U SW8260ug/Kg15NDTrichloroethene 8.0 04/10/14 U SW8260ug/Kg1.7NDTrichlorofluoromethane 8.0 04/10/14 U SW8260ug/Kg1.8NDTrichlorotrifluoroethane 8.0 04/10/14 U SW8260ug/Kg1.2NDVinyl chloride 8.0 04/10/14 U SW8260ug/Kg2.6
QA/QC Surrogates100% 1,2-dichlorobenzene-d4 04/10/14 U 70 - 130 %%89% Bromofluorobenzene 04/10/14 U 70 - 130 %%97% Dibromofluoromethane 04/10/14 U 70 - 130 %%101% Toluene-d8 04/10/14 U 70 - 130 %%
Per 1.4.6 of EPA method 8270D, 1,2-Diphenylhydrazine is unstable and readily converts to Azobenzene. Azobenzene is used for the calibration of 1,2-Diphenylhydrazine.
Please be advised that the NY unrestricted soil criteria for chromium is based on hexavalent chromium and trivalent chromium.
All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments.
1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.B = Present in blank, no bias suspected.
If there are any questions regarding this data, please call Phoenix Client Services at extension 200.This report must not be reproduced except in full as defined by the attached chain of custody.
Reviewed and Released by: Greg Lawrence, Assistant Lab Director
RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level LOD=Limit of Detection MDL=Method Detection Limit
Page 12 of 40 Ver 1
Sample Information Custody InformationMatrix:Location Code:Rush Request:P.O.#:
Collected by:Received by:Analyzed by:
SOLIDEBC72 Hour
04/02/14SWsee "By" below
Laboratory Data
E-SB4 15-17
Phoenix ID: BG29070
04/07/140:00
17:33
Parameter ResultRL/PQL Units Date/Time By Reference
FOR: Attn: Mr. Charles B. Sosik, P.G.Environmental Business Consultants1808 Middle Country RdRidge NY 11961-2406
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
VolatilesND1,1,1,2-Tetrachloroethane 6.9 04/10/14 U SW8260ug/Kg1.1ND1,1,1-Trichloroethane 6.9 04/10/14 U SW8260ug/Kg1.4ND1,1,2,2-Tetrachloroethane 6.9 04/10/14 U SW8260ug/Kg0.98ND1,1,2-Trichloroethane 6.9 04/10/14 U SW8260ug/Kg0.67ND1,1-Dichloroethane 6.9 04/10/14 U SW8260ug/Kg1.4ND1,1-Dichloroethene 6.9 04/10/14 U SW8260ug/Kg1.5ND1,1-Dichloropropene 6.9 04/10/14 U SW8260ug/Kg1.3ND1,2,3-Trichlorobenzene 6.9 04/10/14 U SW8260ug/Kg1.4ND1,2,3-Trichloropropane 6.9 04/10/14 U SW8260ug/Kg0.98ND1,2,4-Trichlorobenzene 6.9 04/10/14 U SW8260ug/Kg1.4ND1,2,4-Trimethylbenzene 6.9 04/10/14 U SW8260ug/Kg0.99ND1,2-Dibromo-3-chloropropane 6.9 04/10/14 U SW8260ug/Kg1.8ND1,2-Dibromoethane 6.9 04/10/14 U SW8260ug/Kg1.8ND1,2-Dichlorobenzene 6.9 04/10/14 U SW8260ug/Kg0.76ND1,2-Dichloroethane 6.9 04/10/14 U SW8260ug/Kg0.61ND1,2-Dichloropropane 6.9 04/10/14 U SW8260ug/Kg0.98ND1,3,5-Trimethylbenzene 6.9 04/10/14 U SW8260ug/Kg0.91ND1,3-Dichlorobenzene 6.9 04/10/14 U SW8260ug/Kg1.0ND1,3-Dichloropropane 6.9 04/10/14 U SW8260ug/Kg0.73ND1,4-Dichlorobenzene 6.9 04/10/14 U SW8260ug/Kg1.1ND2,2-Dichloropropane 6.9 04/10/14 U SW8260ug/Kg1.2ND2-Chlorotoluene 6.9 04/10/14 U SW8260ug/Kg1.1ND2-Hexanone 34 04/10/14 U SW8260ug/Kg3.1ND2-Isopropyltoluene 6.9 04/10/14 U SW8260ug/Kg 10.95ND4-Chlorotoluene 6.9 04/10/14 U SW8260ug/Kg0.80ND4-Methyl-2-pentanone 34 04/10/14 U SW8260ug/Kg1.6NDAcetone 50 04/10/14 U SW8260ug/Kg6.8NDAcrylonitrile 14 04/10/14 U SW8260ug/Kg3.9NDBenzene 6.9 04/10/14 U SW8260ug/Kg1.4NDBromobenzene 6.9 04/10/14 U SW8260ug/Kg0.89NDBromochloromethane 6.9 04/10/14 U SW8260ug/Kg1.0NDBromodichloromethane 6.9 04/10/14 U SW8260ug/Kg0.85NDBromoform 6.9 04/10/14 U SW8260ug/Kg0.96NDBromomethane 6.9 04/10/14 U SW8260ug/Kg5.3NDCarbon Disulfide 6.9 04/10/14 U SW8260ug/Kg1.1NDCarbon tetrachloride 6.9 04/10/14 U SW8260ug/Kg0.80NDChlorobenzene 6.9 04/10/14 U SW8260ug/Kg1.0NDChloroethane 6.9 04/10/14 U SW8260ug/Kg1.6NDChloroform 6.9 04/10/14 U SW8260ug/Kg1.3NDChloromethane 6.9 04/10/14 U SW8260ug/Kg3.6NDcis-1,2-Dichloroethene 6.9 04/10/14 U SW8260ug/Kg1.5NDcis-1,3-Dichloropropene 6.9 04/10/14 U SW8260ug/Kg0.74NDDibromochloromethane 6.9 04/10/14 U SW8260ug/Kg0.77NDDibromomethane 6.9 04/10/14 U SW8260ug/Kg0.87NDDichlorodifluoromethane 6.9 04/10/14 U SW8260ug/Kg1.8NDEthylbenzene 6.9 04/10/14 U SW8260ug/Kg1.3NDHexachlorobutadiene 6.9 04/10/14 U SW8260ug/Kg1.4NDIsopropylbenzene 6.9 04/10/14 U SW8260ug/Kg1.3
Page 14 of 40 Ver 1
E-SB4 15-17Phoenix I.D.: BG29070
Client ID:DOMINO SUGAR SITEProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
NDm&p-Xylene 6.9 04/10/14 U SW8260ug/Kg2.7NDMethyl Ethyl Ketone 41 04/10/14 U SW8260ug/Kg6.0NDMethyl t-butyl ether (MTBE) 14 04/10/14 U SW8260ug/Kg1.9NDMethylene chloride 6.9 04/10/14 U SW8260ug/Kg1.1NDNaphthalene 6.9 04/10/14 U SW8260ug/Kg1.8NDn-Butylbenzene 6.9 04/10/14 U SW8260ug/Kg1.3NDn-Propylbenzene 6.9 04/10/14 U SW8260ug/Kg1.2NDo-Xylene 6.9 04/10/14 U SW8260ug/Kg2.6NDp-Isopropyltoluene 6.9 04/10/14 U SW8260ug/Kg0.99NDsec-Butylbenzene 6.9 04/10/14 U SW8260ug/Kg1.3NDStyrene 6.9 04/10/14 U SW8260ug/Kg2.0NDtert-Butylbenzene 6.9 04/10/14 U SW8260ug/Kg1.1NDTetrachloroethene 6.9 04/10/14 U SW8260ug/Kg1.4NDTetrahydrofuran (THF) 14 04/10/14 U SW8260ug/Kg 16.2NDToluene 6.9 04/10/14 U SW8260ug/Kg1.1NDtrans-1,2-Dichloroethene 6.9 04/10/14 U SW8260ug/Kg1.4NDtrans-1,3-Dichloropropene 6.9 04/10/14 U SW8260ug/Kg1.4NDtrans-1,4-dichloro-2-butene 14 04/10/14 U SW8260ug/Kg13NDTrichloroethene 6.9 04/10/14 U SW8260ug/Kg1.5NDTrichlorofluoromethane 6.9 04/10/14 U SW8260ug/Kg1.5NDTrichlorotrifluoroethane 6.9 04/10/14 U SW8260ug/Kg1.1NDVinyl chloride 6.9 04/10/14 U SW8260ug/Kg2.2
QA/QC Surrogates102% 1,2-dichlorobenzene-d4 04/10/14 U 70 - 130 %%93% Bromofluorobenzene 04/10/14 U 70 - 130 %%98% Dibromofluoromethane 04/10/14 U 70 - 130 %%98% Toluene-d8 04/10/14 U 70 - 130 %%
Per 1.4.6 of EPA method 8270D, 1,2-Diphenylhydrazine is unstable and readily converts to Azobenzene. Azobenzene is used for the calibration of 1,2-Diphenylhydrazine.
Please be advised that the NY unrestricted soil criteria for chromium is based on hexavalent chromium and trivalent chromium.
All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments.
1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.B = Present in blank, no bias suspected.
If there are any questions regarding this data, please call Phoenix Client Services at extension 200.This report must not be reproduced except in full as defined by the attached chain of custody.
Reviewed and Released by: Greg Lawrence, Assistant Lab Director
RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level LOD=Limit of Detection MDL=Method Detection Limit
Page 17 of 40 Ver 1
Sample Information Custody InformationMatrix:Location Code:Rush Request:P.O.#:
Collected by:Received by:Analyzed by:
SOLIDEBC72 Hour
04/02/14SWsee "By" below
Laboratory Data
E-SB5 0-2
Phoenix ID: BG29071
04/07/140:00
17:33
Parameter ResultRL/PQL Units Date/Time By Reference
FOR: Attn: Mr. Charles B. Sosik, P.G.Environmental Business Consultants1808 Middle Country RdRidge NY 11961-2406
Polychlorinated BiphenylsNDPCB-1016 36 04/08/14 AW SW 8082ug/Kg36NDPCB-1221 36 04/08/14 AW SW 8082ug/Kg36NDPCB-1232 36 04/08/14 AW SW 8082ug/Kg36NDPCB-1242 36 04/08/14 AW SW 8082ug/Kg36NDPCB-1248 36 04/08/14 AW SW 8082ug/Kg36NDPCB-1254 36 04/08/14 AW SW 8082ug/Kg36NDPCB-1260 36 04/08/14 AW SW 8082ug/Kg36NDPCB-1262 36 04/08/14 AW SW 8082ug/Kg36NDPCB-1268 36 04/08/14 AW SW 8082ug/Kg36
QA/QC Surrogates96% DCBP 04/08/14 AW 30 - 150 %%81% TCMX 04/08/14 AW 30 - 150 %%
Pesticides - SoilND4,4' -DDD 2.6 04/09/14 CE SW8081ug/Kg2.6ND4,4' -DDE 2.6 04/09/14 CE SW8081ug/Kg2.6ND4,4' -DDT 2.6 04/09/14 CE SW8081ug/Kg2.6NDa-BHC 1.8 04/09/14 CE SW8081ug/Kg1.8NDa-Chlordane 3.6 04/09/14 CE SW8081ug/Kg3.6NDAldrin 1.8 04/09/14 CE SW8081ug/Kg1.8NDb-BHC 1.8 04/09/14 CE SW8081ug/Kg1.8NDChlordane 22 04/09/14 CE SW8081ug/Kg22NDd-BHC 1.8 04/09/14 CE SW8081ug/Kg1.8NDDieldrin 1.8 04/09/14 CE SW8081ug/Kg1.8NDEndosulfan I 3.6 04/09/14 CE SW8081ug/Kg3.6NDEndosulfan II 3.6 04/09/14 CE SW8081ug/Kg3.6NDEndosulfan sulfate 3.6 04/09/14 CE SW8081ug/Kg3.6NDEndrin 1.8 04/09/14 CE SW8081ug/Kg1.8NDEndrin aldehyde 3.6 04/09/14 CE SW8081ug/Kg3.6NDEndrin ketone 1.8 04/09/14 CE SW8081ug/Kg1.8NDg-BHC 1.8 04/09/14 CE SW8081ug/Kg1.8NDg-Chlordane 3.6 04/09/14 CE SW8081ug/Kg3.6NDHeptachlor 1.8 04/09/14 CE SW8081ug/Kg1.8NDHeptachlor epoxide 1.8 04/09/14 CE SW8081ug/Kg1.8NDMethoxychlor 22 04/09/14 CE SW8081ug/Kg22NDToxaphene 180 04/09/14 CE SW8081ug/Kg180
QA/QC Surrogates140% DCBP 04/09/14 CE 30 - 150 %%89% TCMX 04/09/14 CE 30 - 150 %%
VolatilesND1,1,1,2-Tetrachloroethane 9.8 04/10/14 U SW8260ug/Kg1.6ND1,1,1-Trichloroethane 9.8 04/10/14 U SW8260ug/Kg2.0ND1,1,2,2-Tetrachloroethane 9.8 04/10/14 U SW8260ug/Kg1.4ND1,1,2-Trichloroethane 9.8 04/10/14 U SW8260ug/Kg0.96ND1,1-Dichloroethane 9.8 04/10/14 U SW8260ug/Kg1.9
Page 19 of 40 Ver 1
E-SB5 0-2Phoenix I.D.: BG29071
Client ID:DOMINO SUGAR SITEProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
ND1,1-Dichloroethene 9.8 04/10/14 U SW8260ug/Kg2.1ND1,1-Dichloropropene 9.8 04/10/14 U SW8260ug/Kg1.9ND1,2,3-Trichlorobenzene 9.8 04/10/14 U SW8260ug/Kg2.0ND1,2,3-Trichloropropane 9.8 04/10/14 U SW8260ug/Kg1.4ND1,2,4-Trichlorobenzene 9.8 04/10/14 U SW8260ug/Kg2.0ND1,2,4-Trimethylbenzene 9.8 04/10/14 U SW8260ug/Kg1.4ND1,2-Dibromo-3-chloropropane 9.8 04/10/14 U SW8260ug/Kg2.6ND1,2-Dibromoethane 9.8 04/10/14 U SW8260ug/Kg2.6ND1,2-Dichlorobenzene 9.8 04/10/14 U SW8260ug/Kg1.1ND1,2-Dichloroethane 9.8 04/10/14 U SW8260ug/Kg0.87ND1,2-Dichloropropane 9.8 04/10/14 U SW8260ug/Kg1.4ND1,3,5-Trimethylbenzene 9.8 04/10/14 U SW8260ug/Kg1.3ND1,3-Dichlorobenzene 9.8 04/10/14 U SW8260ug/Kg1.5ND1,3-Dichloropropane 9.8 04/10/14 U SW8260ug/Kg1.0ND1,4-Dichlorobenzene 9.8 04/10/14 U SW8260ug/Kg1.6ND2,2-Dichloropropane 9.8 04/10/14 U SW8260ug/Kg1.7ND2-Chlorotoluene 9.8 04/10/14 U SW8260ug/Kg1.6ND2-Hexanone 49 04/10/14 U SW8260ug/Kg4.4ND2-Isopropyltoluene 9.8 04/10/14 U SW8260ug/Kg 11.4ND4-Chlorotoluene 9.8 04/10/14 U SW8260ug/Kg1.1ND4-Methyl-2-pentanone 49 04/10/14 U SW8260ug/Kg2.312Acetone 50 04/10/14 U SW8260ug/Kg9.8JSNDAcrylonitrile 20 04/10/14 U SW8260ug/Kg5.5NDBenzene 9.8 04/10/14 U SW8260ug/Kg1.9NDBromobenzene 9.8 04/10/14 U SW8260ug/Kg1.3NDBromochloromethane 9.8 04/10/14 U SW8260ug/Kg1.4NDBromodichloromethane 9.8 04/10/14 U SW8260ug/Kg1.2NDBromoform 9.8 04/10/14 U SW8260ug/Kg1.4NDBromomethane 9.8 04/10/14 U SW8260ug/Kg7.6NDCarbon Disulfide 9.8 04/10/14 U SW8260ug/Kg1.6NDCarbon tetrachloride 9.8 04/10/14 U SW8260ug/Kg1.1NDChlorobenzene 9.8 04/10/14 U SW8260ug/Kg1.5NDChloroethane 9.8 04/10/14 U SW8260ug/Kg2.3NDChloroform 9.8 04/10/14 U SW8260ug/Kg1.8NDChloromethane 9.8 04/10/14 U SW8260ug/Kg5.2NDcis-1,2-Dichloroethene 9.8 04/10/14 U SW8260ug/Kg2.1NDcis-1,3-Dichloropropene 9.8 04/10/14 U SW8260ug/Kg1.1NDDibromochloromethane 9.8 04/10/14 U SW8260ug/Kg1.1NDDibromomethane 9.8 04/10/14 U SW8260ug/Kg1.2NDDichlorodifluoromethane 9.8 04/10/14 U SW8260ug/Kg2.6NDEthylbenzene 9.8 04/10/14 U SW8260ug/Kg1.8NDHexachlorobutadiene 9.8 04/10/14 U SW8260ug/Kg2.1NDIsopropylbenzene 9.8 04/10/14 U SW8260ug/Kg1.9NDm&p-Xylene 9.8 04/10/14 U SW8260ug/Kg3.9NDMethyl Ethyl Ketone 59 04/10/14 U SW8260ug/Kg8.5NDMethyl t-butyl ether (MTBE) 20 04/10/14 U SW8260ug/Kg2.7NDMethylene chloride 9.8 04/10/14 U SW8260ug/Kg1.6NDNaphthalene 9.8 04/10/14 U SW8260ug/Kg2.6NDn-Butylbenzene 9.8 04/10/14 U SW8260ug/Kg1.8
Page 20 of 40 Ver 1
E-SB5 0-2Phoenix I.D.: BG29071
Client ID:DOMINO SUGAR SITEProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
NDn-Propylbenzene 9.8 04/10/14 U SW8260ug/Kg1.8NDo-Xylene 9.8 04/10/14 U SW8260ug/Kg3.8NDp-Isopropyltoluene 9.8 04/10/14 U SW8260ug/Kg1.4NDsec-Butylbenzene 9.8 04/10/14 U SW8260ug/Kg1.8NDStyrene 9.8 04/10/14 U SW8260ug/Kg2.8NDtert-Butylbenzene 9.8 04/10/14 U SW8260ug/Kg1.6NDTetrachloroethene 9.8 04/10/14 U SW8260ug/Kg2.1NDTetrahydrofuran (THF) 20 04/10/14 U SW8260ug/Kg 18.9NDToluene 9.8 04/10/14 U SW8260ug/Kg1.6NDtrans-1,2-Dichloroethene 9.8 04/10/14 U SW8260ug/Kg2.0NDtrans-1,3-Dichloropropene 9.8 04/10/14 U SW8260ug/Kg2.0NDtrans-1,4-dichloro-2-butene 20 04/10/14 U SW8260ug/Kg18NDTrichloroethene 9.8 04/10/14 U SW8260ug/Kg2.1NDTrichlorofluoromethane 9.8 04/10/14 U SW8260ug/Kg2.2NDTrichlorotrifluoroethane 9.8 04/10/14 U SW8260ug/Kg1.5NDVinyl chloride 9.8 04/10/14 U SW8260ug/Kg3.2
QA/QC Surrogates103% 1,2-dichlorobenzene-d4 04/10/14 U 70 - 130 %%88% Bromofluorobenzene 04/10/14 U 70 - 130 %%98% Dibromofluoromethane 04/10/14 U 70 - 130 %%99% Toluene-d8 04/10/14 U 70 - 130 %%
Per 1.4.6 of EPA method 8270D, 1,2-Diphenylhydrazine is unstable and readily converts to Azobenzene. Azobenzene is used for the calibration of 1,2-Diphenylhydrazine.
Please be advised that the NY unrestricted soil criteria for chromium is based on hexavalent chromium and trivalent chromium.
Semi-Volatile Comment:Due to a matrix interference and/or the presence of a large amount of non-target material in the sample, a dilution was required resulting in an elevated RL for the semivolatile analysis.
Due to a matrix interference and/or the presence of a large amount of non-target material in the sample, an elevated RL was reported for the pesticide analysis.
All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments.
1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.B = Present in blank, no bias suspected.
If there are any questions regarding this data, please call Phoenix Client Services at extension 200.This report must not be reproduced except in full as defined by the attached chain of custody.
Reviewed and Released by: Greg Lawrence, Assistant Lab Director
RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level LOD=Limit of Detection MDL=Method Detection Limit
Page 23 of 40 Ver 1
Sample Information Custody InformationMatrix:Location Code:Rush Request:P.O.#:
Collected by:Received by:Analyzed by:
SOLIDEBC72 Hour
04/02/14SWsee "By" below
Laboratory Data
E-SB5 12-14
Phoenix ID: BG29072
04/07/140:00
17:33
Parameter ResultRL/PQL Units Date/Time By Reference
FOR: Attn: Mr. Charles B. Sosik, P.G.Environmental Business Consultants1808 Middle Country RdRidge NY 11961-2406
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
VolatilesND1,1,1,2-Tetrachloroethane 8.9 04/10/14 U SW8260ug/Kg1.5ND1,1,1-Trichloroethane 8.9 04/10/14 U SW8260ug/Kg1.8ND1,1,2,2-Tetrachloroethane 8.9 04/10/14 U SW8260ug/Kg1.3ND1,1,2-Trichloroethane 8.9 04/10/14 U SW8260ug/Kg0.88ND1,1-Dichloroethane 8.9 04/10/14 U SW8260ug/Kg1.8ND1,1-Dichloroethene 8.9 04/10/14 U SW8260ug/Kg1.9ND1,1-Dichloropropene 8.9 04/10/14 U SW8260ug/Kg1.7ND1,2,3-Trichlorobenzene 280 04/11/14 U SW8260ug/Kg56ND1,2,3-Trichloropropane 280 04/11/14 U SW8260ug/Kg40ND1,2,4-Trichlorobenzene 280 04/11/14 U SW8260ug/Kg56ND1,2,4-Trimethylbenzene 280 04/11/14 U SW8260ug/Kg41ND1,2-Dibromo-3-chloropropane 280 04/11/14 U SW8260ug/Kg75ND1,2-Dibromoethane 8.9 04/10/14 U SW8260ug/Kg2.4ND1,2-Dichlorobenzene 280 04/11/14 U SW8260ug/Kg31ND1,2-Dichloroethane 8.9 04/10/14 U SW8260ug/Kg0.79ND1,2-Dichloropropane 8.9 04/10/14 U SW8260ug/Kg1.3ND1,3,5-Trimethylbenzene 280 04/11/14 U SW8260ug/Kg37ND1,3-Dichlorobenzene 280 04/11/14 U SW8260ug/Kg42ND1,3-Dichloropropane 8.9 04/10/14 U SW8260ug/Kg0.95ND1,4-Dichlorobenzene 280 04/11/14 U SW8260ug/Kg44ND2,2-Dichloropropane 8.9 04/10/14 U SW8260ug/Kg1.5ND2-Chlorotoluene 280 04/11/14 U SW8260ug/Kg45ND2-Hexanone 45 04/10/14 U SW8260ug/Kg4.0ND2-Isopropyltoluene 280 04/11/14 U SW8260ug/Kg 139ND4-Chlorotoluene 280 04/11/14 U SW8260ug/Kg33ND4-Methyl-2-pentanone 45 04/10/14 U SW8260ug/Kg2.149Acetone 50 04/10/14 U SW8260ug/Kg8.9JS'NDAcrylonitrile 18 04/10/14 U SW8260ug/Kg5.0NDBenzene 8.9 04/10/14 U SW8260ug/Kg1.8NDBromobenzene 280 04/11/14 U SW8260ug/Kg37NDBromochloromethane 8.9 04/10/14 U SW8260ug/Kg1.3NDBromodichloromethane 8.9 04/10/14 U SW8260ug/Kg1.1NDBromoform 8.9 04/10/14 U SW8260ug/Kg1.3NDBromomethane 8.9 04/10/14 U SW8260ug/Kg6.9NDCarbon Disulfide 8.9 04/10/14 U SW8260ug/Kg1.4NDCarbon tetrachloride 8.9 04/10/14 U SW8260ug/Kg1.0NDChlorobenzene 8.9 04/10/14 U SW8260ug/Kg1.3NDChloroethane 8.9 04/10/14 U SW8260ug/Kg2.1NDChloroform 8.9 04/10/14 U SW8260ug/Kg1.6NDChloromethane 8.9 04/10/14 U SW8260ug/Kg4.7NDcis-1,2-Dichloroethene 8.9 04/10/14 U SW8260ug/Kg1.9NDcis-1,3-Dichloropropene 8.9 04/10/14 U SW8260ug/Kg0.97NDDibromochloromethane 8.9 04/10/14 U SW8260ug/Kg1.0NDDibromomethane 8.9 04/10/14 U SW8260ug/Kg1.1NDDichlorodifluoromethane 8.9 04/10/14 U SW8260ug/Kg2.4NDEthylbenzene 8.9 04/10/14 U SW8260ug/Kg1.6NDHexachlorobutadiene 280 04/11/14 U SW8260ug/Kg59NDIsopropylbenzene 280 04/11/14 U SW8260ug/Kg54
Page 25 of 40 Ver 1
E-SB5 12-14Phoenix I.D.: BG29072
Client ID:DOMINO SUGAR SITEProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
NDm&p-Xylene 8.9 04/10/14 U SW8260ug/Kg3.5NDMethyl Ethyl Ketone 54 04/10/14 U SW8260ug/Kg7.8NDMethyl t-butyl ether (MTBE) 18 04/10/14 U SW8260ug/Kg2.5NDMethylene chloride 8.9 04/10/14 U SW8260ug/Kg1.5NDNaphthalene 280 04/11/14 U SW8260ug/Kg75NDn-Butylbenzene 280 04/11/14 U SW8260ug/Kg51NDn-Propylbenzene 280 04/11/14 U SW8260ug/Kg51NDo-Xylene 8.9 04/10/14 U SW8260ug/Kg3.4NDp-Isopropyltoluene 280 04/11/14 U SW8260ug/Kg41NDsec-Butylbenzene 280 04/11/14 U SW8260ug/Kg53NDStyrene 8.9 04/10/14 U SW8260ug/Kg2.6NDtert-Butylbenzene 280 04/11/14 U SW8260ug/Kg45NDTetrachloroethene 8.9 04/10/14 U SW8260ug/Kg1.9NDTetrahydrofuran (THF) 18 04/10/14 U SW8260ug/Kg 18.0NDToluene 8.9 04/10/14 U SW8260ug/Kg1.4NDtrans-1,2-Dichloroethene 8.9 04/10/14 U SW8260ug/Kg1.8NDtrans-1,3-Dichloropropene 8.9 04/10/14 U SW8260ug/Kg1.8NDtrans-1,4-dichloro-2-butene 560 04/11/14 U SW8260ug/Kg520NDTrichloroethene 8.9 04/10/14 U SW8260ug/Kg1.9NDTrichlorofluoromethane 8.9 04/10/14 U SW8260ug/Kg2.0NDTrichlorotrifluoroethane 8.9 04/10/14 U SW8260ug/Kg1.4NDVinyl chloride 8.9 04/10/14 U SW8260ug/Kg2.9
QA/QC Surrogates99% 1,2-dichlorobenzene-d4 04/11/14 U 70 - 130 %%95% Bromofluorobenzene 04/11/14 U 70 - 130 %%108% Dibromofluoromethane 04/10/14 U 70 - 130 %%97% Toluene-d8 04/10/14 U 70 - 130 %%
Per 1.4.6 of EPA method 8270D, 1,2-Diphenylhydrazine is unstable and readily converts to Azobenzene. Azobenzene is used for the calibration of 1,2-Diphenylhydrazine.
Please be advised that the NY unrestricted soil criteria for chromium is based on hexavalent chromium and trivalent chromium.
Volatile Comment:There was a suppression of the last internal standard in the low level analysis, all affected compounds are reported from the methanol preserved high level analysis which did not exhibit this interference.
All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments.
1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.B = Present in blank, no bias suspected.
If there are any questions regarding this data, please call Phoenix Client Services at extension 200.This report must not be reproduced except in full as defined by the attached chain of custody.
Reviewed and Released by: Greg Lawrence, Assistant Lab Director
RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level LOD=Limit of Detection MDL=Method Detection Limit
Page 28 of 40 Ver 1
Sample Information Custody InformationMatrix:Location Code:Rush Request:P.O.#:
Collected by:Received by:Analyzed by:
SOLIDEBC72 Hour
04/02/14SWsee "By" below
Laboratory Data
SOIL DUPLICATE 1
Phoenix ID: BG29073
04/07/140:00
17:33
Parameter ResultRL/PQL Units Date/Time By Reference
FOR: Attn: Mr. Charles B. Sosik, P.G.Environmental Business Consultants1808 Middle Country RdRidge NY 11961-2406
Polychlorinated BiphenylsNDPCB-1016 38 04/08/14 AW SW 8082ug/Kg38NDPCB-1221 38 04/08/14 AW SW 8082ug/Kg38NDPCB-1232 38 04/08/14 AW SW 8082ug/Kg38NDPCB-1242 38 04/08/14 AW SW 8082ug/Kg38NDPCB-1248 38 04/08/14 AW SW 8082ug/Kg38NDPCB-1254 38 04/08/14 AW SW 8082ug/Kg38NDPCB-1260 38 04/08/14 AW SW 8082ug/Kg38NDPCB-1262 38 04/08/14 AW SW 8082ug/Kg38NDPCB-1268 38 04/08/14 AW SW 8082ug/Kg38
QA/QC Surrogates118% DCBP 04/08/14 AW 30 - 150 %%83% TCMX 04/08/14 AW 30 - 150 %%
Pesticides - SoilND4,4' -DDD 2.8 04/09/14 CE SW8081ug/Kg2.8ND4,4' -DDE 2.8 04/09/14 CE SW8081ug/Kg2.8ND4,4' -DDT 2.8 04/09/14 CE SW8081ug/Kg2.8NDa-BHC 1.9 04/09/14 CE SW8081ug/Kg1.9NDa-Chlordane 3.8 04/09/14 CE SW8081ug/Kg3.8NDAldrin 1.9 04/09/14 CE SW8081ug/Kg1.9NDb-BHC 1.9 04/09/14 CE SW8081ug/Kg1.9NDChlordane 23 04/09/14 CE SW8081ug/Kg23NDd-BHC 1.9 04/09/14 CE SW8081ug/Kg1.9NDDieldrin 1.9 04/09/14 CE SW8081ug/Kg1.9NDEndosulfan I 3.8 04/09/14 CE SW8081ug/Kg3.8NDEndosulfan II 3.8 04/09/14 CE SW8081ug/Kg3.8NDEndosulfan sulfate 3.8 04/09/14 CE SW8081ug/Kg3.8NDEndrin 1.9 04/09/14 CE SW8081ug/Kg1.9NDEndrin aldehyde 3.8 04/09/14 CE SW8081ug/Kg3.8NDEndrin ketone 1.9 04/09/14 CE SW8081ug/Kg1.9NDg-BHC 1.9 04/09/14 CE SW8081ug/Kg1.9NDg-Chlordane 3.8 04/09/14 CE SW8081ug/Kg3.8NDHeptachlor 1.9 04/09/14 CE SW8081ug/Kg1.9NDHeptachlor epoxide 1.9 04/09/14 CE SW8081ug/Kg1.9NDMethoxychlor 58 04/09/14 CE SW8081ug/Kg58NDToxaphene 190 04/09/14 CE SW8081ug/Kg190
QA/QC Surrogates128% DCBP 04/09/14 CE 30 - 150 %%76% TCMX 04/09/14 CE 30 - 150 %%
VolatilesND1,1,1,2-Tetrachloroethane 8.5 04/10/14 U SW8260ug/Kg1.4ND1,1,1-Trichloroethane 8.5 04/10/14 U SW8260ug/Kg1.7ND1,1,2,2-Tetrachloroethane 8.5 04/10/14 U SW8260ug/Kg1.2ND1,1,2-Trichloroethane 8.5 04/10/14 U SW8260ug/Kg0.83ND1,1-Dichloroethane 8.5 04/10/14 U SW8260ug/Kg1.7
Page 30 of 40 Ver 1
SOIL DUPLICATE 1Phoenix I.D.: BG29073
Client ID:DOMINO SUGAR SITEProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
ND1,1-Dichloroethene 8.5 04/10/14 U SW8260ug/Kg1.9ND1,1-Dichloropropene 8.5 04/10/14 U SW8260ug/Kg1.7ND1,2,3-Trichlorobenzene 8.5 04/10/14 U SW8260ug/Kg1.7ND1,2,3-Trichloropropane 8.5 04/10/14 U SW8260ug/Kg1.2ND1,2,4-Trichlorobenzene 8.5 04/10/14 U SW8260ug/Kg1.7ND1,2,4-Trimethylbenzene 8.5 04/10/14 U SW8260ug/Kg1.2ND1,2-Dibromo-3-chloropropane 8.5 04/10/14 U SW8260ug/Kg2.3ND1,2-Dibromoethane 8.5 04/10/14 U SW8260ug/Kg2.3ND1,2-Dichlorobenzene 8.5 04/10/14 U SW8260ug/Kg0.94ND1,2-Dichloroethane 8.5 04/10/14 U SW8260ug/Kg0.75ND1,2-Dichloropropane 8.5 04/10/14 U SW8260ug/Kg1.2ND1,3,5-Trimethylbenzene 8.5 04/10/14 U SW8260ug/Kg1.1ND1,3-Dichlorobenzene 8.5 04/10/14 U SW8260ug/Kg1.3ND1,3-Dichloropropane 8.5 04/10/14 U SW8260ug/Kg0.90ND1,4-Dichlorobenzene 8.5 04/10/14 U SW8260ug/Kg1.3ND2,2-Dichloropropane 8.5 04/10/14 U SW8260ug/Kg1.4ND2-Chlorotoluene 8.5 04/10/14 U SW8260ug/Kg1.4ND2-Hexanone 43 04/10/14 U SW8260ug/Kg3.8ND2-Isopropyltoluene 8.5 04/10/14 U SW8260ug/Kg 11.2ND4-Chlorotoluene 8.5 04/10/14 U SW8260ug/Kg0.99ND4-Methyl-2-pentanone 43 04/10/14 U SW8260ug/Kg2.030Acetone 50 04/10/14 U SW8260ug/Kg8.5JSNDAcrylonitrile 17 04/10/14 U SW8260ug/Kg4.8NDBenzene 8.5 04/10/14 U SW8260ug/Kg1.7NDBromobenzene 8.5 04/10/14 U SW8260ug/Kg1.1NDBromochloromethane 8.5 04/10/14 U SW8260ug/Kg1.2NDBromodichloromethane 8.5 04/10/14 U SW8260ug/Kg1.1NDBromoform 8.5 04/10/14 U SW8260ug/Kg1.2NDBromomethane 8.5 04/10/14 U SW8260ug/Kg6.6NDCarbon Disulfide 8.5 04/10/14 U SW8260ug/Kg1.4NDCarbon tetrachloride 8.5 04/10/14 U SW8260ug/Kg0.99NDChlorobenzene 8.5 04/10/14 U SW8260ug/Kg1.3NDChloroethane 8.5 04/10/14 U SW8260ug/Kg2.0NDChloroform 8.5 04/10/14 U SW8260ug/Kg1.5NDChloromethane 8.5 04/10/14 U SW8260ug/Kg4.5NDcis-1,2-Dichloroethene 8.5 04/10/14 U SW8260ug/Kg1.9NDcis-1,3-Dichloropropene 8.5 04/10/14 U SW8260ug/Kg0.92NDDibromochloromethane 8.5 04/10/14 U SW8260ug/Kg0.95NDDibromomethane 8.5 04/10/14 U SW8260ug/Kg1.1NDDichlorodifluoromethane 8.5 04/10/14 U SW8260ug/Kg2.3NDEthylbenzene 8.5 04/10/14 U SW8260ug/Kg1.5NDHexachlorobutadiene 8.5 04/10/14 U SW8260ug/Kg1.8NDIsopropylbenzene 8.5 04/10/14 U SW8260ug/Kg1.6NDm&p-Xylene 8.5 04/10/14 U SW8260ug/Kg3.4NDMethyl Ethyl Ketone 51 04/10/14 U SW8260ug/Kg7.4NDMethyl t-butyl ether (MTBE) 17 04/10/14 U SW8260ug/Kg2.3NDMethylene chloride 8.5 04/10/14 U SW8260ug/Kg1.4390Naphthalene 320 04/11/14 U SW8260ug/Kg84NDn-Butylbenzene 8.5 04/10/14 U SW8260ug/Kg1.5
Page 31 of 40 Ver 1
SOIL DUPLICATE 1Phoenix I.D.: BG29073
Client ID:DOMINO SUGAR SITEProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
NDn-Propylbenzene 8.5 04/10/14 U SW8260ug/Kg1.5NDo-Xylene 8.5 04/10/14 U SW8260ug/Kg3.3NDp-Isopropyltoluene 8.5 04/10/14 U SW8260ug/Kg1.2NDsec-Butylbenzene 8.5 04/10/14 U SW8260ug/Kg1.6NDStyrene 8.5 04/10/14 U SW8260ug/Kg2.5NDtert-Butylbenzene 8.5 04/10/14 U SW8260ug/Kg1.4NDTetrachloroethene 8.5 04/10/14 U SW8260ug/Kg1.8NDTetrahydrofuran (THF) 17 04/10/14 U SW8260ug/Kg 17.7NDToluene 8.5 04/10/14 U SW8260ug/Kg1.3NDtrans-1,2-Dichloroethene 8.5 04/10/14 U SW8260ug/Kg1.7NDtrans-1,3-Dichloropropene 8.5 04/10/14 U SW8260ug/Kg1.7NDtrans-1,4-dichloro-2-butene 17 04/10/14 U SW8260ug/Kg16NDTrichloroethene 8.5 04/10/14 U SW8260ug/Kg1.8NDTrichlorofluoromethane 8.5 04/10/14 U SW8260ug/Kg1.9NDTrichlorotrifluoroethane 8.5 04/10/14 U SW8260ug/Kg1.3NDVinyl chloride 8.5 04/10/14 U SW8260ug/Kg2.8
QA/QC Surrogates105% 1,2-dichlorobenzene-d4 04/10/14 U 70 - 130 %%84% Bromofluorobenzene 04/10/14 U 70 - 130 %%101% Dibromofluoromethane 04/10/14 U 70 - 130 %%97% Toluene-d8 04/10/14 U 70 - 130 %%
Per 1.4.6 of EPA method 8270D, 1,2-Diphenylhydrazine is unstable and readily converts to Azobenzene. Azobenzene is used for the calibration of 1,2-Diphenylhydrazine.
Please be advised that the NY unrestricted soil criteria for chromium is based on hexavalent chromium and trivalent chromium.
Due to a matrix interference and/or the presence of a large amount of non-target material in the sample, an elevated RL was reported for the pesticide analysis.
All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments.
1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.B = Present in blank, no bias suspected.
If there are any questions regarding this data, please call Phoenix Client Services at extension 200.This report must not be reproduced except in full as defined by the attached chain of custody.
Reviewed and Released by: Greg Lawrence, Assistant Lab Director
RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level LOD=Limit of Detection MDL=Method Detection Limit
Page 34 of 40 Ver 1
Sample Information Custody InformationMatrix:Location Code:Rush Request:P.O.#:
Collected by:Received by:Analyzed by:
SOLIDEBC72 Hour
04/02/14SWsee "By" below
Laboratory Data
TRIP BLANK HIGH
Phoenix ID: BG29074
04/07/140:00
17:33
Parameter ResultRL/PQL Units Date/Time By Reference
FOR: Attn: Mr. Charles B. Sosik, P.G.Environmental Business Consultants1808 Middle Country RdRidge NY 11961-2406
VolatilesND1,1,1,2-Tetrachloroethane 250 04/10/14 U SW8260ug/Kg41ND1,1,1-Trichloroethane 250 04/10/14 U SW8260ug/Kg50ND1,1,2,2-Tetrachloroethane 250 04/10/14 U SW8260ug/Kg36ND1,1,2-Trichloroethane 250 04/10/14 U SW8260ug/Kg25ND1,1-Dichloroethane 250 04/10/14 U SW8260ug/Kg50ND1,1-Dichloroethene 250 04/10/14 U SW8260ug/Kg55ND1,1-Dichloropropene 250 04/10/14 U SW8260ug/Kg49ND1,2,3-Trichlorobenzene 250 04/10/14 U SW8260ug/Kg50ND1,2,3-Trichloropropane 250 04/10/14 U SW8260ug/Kg36ND1,2,4-Trichlorobenzene 250 04/10/14 U SW8260ug/Kg50ND1,2,4-Trimethylbenzene 250 04/10/14 U SW8260ug/Kg36ND1,2-Dibromo-3-chloropropane 250 04/10/14 U SW8260ug/Kg67ND1,2-Dibromoethane 250 04/10/14 U SW8260ug/Kg67ND1,2-Dichlorobenzene 250 04/10/14 U SW8260ug/Kg28ND1,2-Dichloroethane 250 04/10/14 U SW8260ug/Kg22ND1,2-Dichloropropane 250 04/10/14 U SW8260ug/Kg36ND1,3,5-Trimethylbenzene 250 04/10/14 U SW8260ug/Kg33ND1,3-Dichlorobenzene 250 04/10/14 U SW8260ug/Kg37ND1,3-Dichloropropane 250 04/10/14 U SW8260ug/Kg27ND1,4-Dichlorobenzene 250 04/10/14 U SW8260ug/Kg40ND2,2-Dichloropropane 250 04/10/14 U SW8260ug/Kg42ND2-Chlorotoluene 250 04/10/14 U SW8260ug/Kg40ND2-Hexanone 1300 04/10/14 U SW8260ug/Kg110ND2-Isopropyltoluene 250 04/10/14 U SW8260ug/Kg 135
Page 35 of 40 Ver 1
TRIP BLANK HIGHPhoenix I.D.: BG29074
Client ID:DOMINO SUGAR SITEProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
ND4-Chlorotoluene 250 04/10/14 U SW8260ug/Kg29ND4-Methyl-2-pentanone 1300 04/10/14 U SW8260ug/Kg60NDAcetone 2500 04/10/14 U SW8260ug/Kg250NDAcrylonitrile 500 04/10/14 U SW8260ug/Kg140NDBenzene 250 04/10/14 U SW8260ug/Kg50NDBromobenzene 250 04/10/14 U SW8260ug/Kg33NDBromochloromethane 250 04/10/14 U SW8260ug/Kg37NDBromodichloromethane 250 04/10/14 U SW8260ug/Kg31NDBromoform 250 04/10/14 U SW8260ug/Kg35NDBromomethane 250 04/10/14 U SW8260ug/Kg190NDCarbon Disulfide 250 04/10/14 U SW8260ug/Kg41NDCarbon tetrachloride 250 04/10/14 U SW8260ug/Kg29NDChlorobenzene 250 04/10/14 U SW8260ug/Kg37NDChloroethane 250 04/10/14 U SW8260ug/Kg59NDChloroform 250 04/10/14 U SW8260ug/Kg46NDChloromethane 250 04/10/14 U SW8260ug/Kg130NDcis-1,2-Dichloroethene 250 04/10/14 U SW8260ug/Kg55NDcis-1,3-Dichloropropene 250 04/10/14 U SW8260ug/Kg27NDDibromochloromethane 250 04/10/14 U SW8260ug/Kg28NDDibromomethane 250 04/10/14 U SW8260ug/Kg32NDDichlorodifluoromethane 250 04/10/14 U SW8260ug/Kg67NDEthylbenzene 250 04/10/14 U SW8260ug/Kg46NDHexachlorobutadiene 250 04/10/14 U SW8260ug/Kg53NDIsopropylbenzene 250 04/10/14 U SW8260ug/Kg48NDm&p-Xylene 250 04/10/14 U SW8260ug/Kg99NDMethyl Ethyl Ketone 1500 04/10/14 U SW8260ug/Kg220NDMethyl t-butyl ether (MTBE) 500 04/10/14 U SW8260ug/Kg69NDMethylene chloride 250 04/10/14 U SW8260ug/Kg41NDNaphthalene 250 04/10/14 U SW8260ug/Kg67NDn-Butylbenzene 250 04/10/14 U SW8260ug/Kg46NDn-Propylbenzene 250 04/10/14 U SW8260ug/Kg45NDo-Xylene 250 04/10/14 U SW8260ug/Kg96NDp-Isopropyltoluene 250 04/10/14 U SW8260ug/Kg36NDsec-Butylbenzene 250 04/10/14 U SW8260ug/Kg47NDStyrene 250 04/10/14 U SW8260ug/Kg72NDtert-Butylbenzene 250 04/10/14 U SW8260ug/Kg40NDTetrachloroethene 250 04/10/14 U SW8260ug/Kg53NDTetrahydrofuran (THF) 500 04/10/14 U SW8260ug/Kg 1230NDToluene 250 04/10/14 U SW8260ug/Kg40NDtrans-1,2-Dichloroethene 250 04/10/14 U SW8260ug/Kg50NDtrans-1,3-Dichloropropene 250 04/10/14 U SW8260ug/Kg51NDtrans-1,4-dichloro-2-butene 500 04/10/14 U SW8260ug/Kg460NDTrichloroethene 250 04/10/14 U SW8260ug/Kg53NDTrichlorofluoromethane 250 04/10/14 U SW8260ug/Kg56NDTrichlorotrifluoroethane 250 04/10/14 U SW8260ug/Kg39NDVinyl chloride 250 04/10/14 U SW8260ug/Kg81
QA/QC Surrogates99% 1,2-dichlorobenzene-d4 04/10/14 U 70 - 130 %%95% Bromofluorobenzene 04/10/14 U 70 - 130 %%
Page 36 of 40 Ver 1
TRIP BLANK HIGHPhoenix I.D.: BG29074
Client ID:DOMINO SUGAR SITEProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
95% Dibromofluoromethane 04/10/14 U 70 - 130 %%100% Toluene-d8 04/10/14 U 70 - 130 %%
Comments:
TRIP BLANK INCLUDED. %SOLIDS ASSUMED 100%
This sample was not collected in accordance with EPA method 5035. NELAC requires the laboratory to qualify the volatile soil data as biased low.
All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments.
1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.
If there are any questions regarding this data, please call Phoenix Client Services at extension 200.This report must not be reproduced except in full as defined by the attached chain of custody.
Reviewed and Released by: Greg Lawrence, Assistant Lab Director
RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level LOD=Limit of Detection MDL=Method Detection Limit
Page 37 of 40 Ver 1
Sample Information Custody InformationMatrix:Location Code:Rush Request:P.O.#:
Collected by:Received by:Analyzed by:
SOLIDEBC72 Hour
04/02/14SWsee "By" below
Laboratory Data
TRIP BLANK LOW
Phoenix ID: BG29075
04/07/140:00
17:33
Parameter ResultRL/PQL Units Date/Time By Reference
FOR: Attn: Mr. Charles B. Sosik, P.G.Environmental Business Consultants1808 Middle Country RdRidge NY 11961-2406
VolatilesND1,1,1,2-Tetrachloroethane 5.0 04/10/14 U SW8260ug/Kg0.82ND1,1,1-Trichloroethane 5.0 04/10/14 U SW8260ug/Kg1.0ND1,1,2,2-Tetrachloroethane 5.0 04/10/14 U SW8260ug/Kg0.71ND1,1,2-Trichloroethane 5.0 04/10/14 U SW8260ug/Kg0.49ND1,1-Dichloroethane 5.0 04/10/14 U SW8260ug/Kg0.99ND1,1-Dichloroethene 5.0 04/10/14 U SW8260ug/Kg1.1ND1,1-Dichloropropene 5.0 04/10/14 U SW8260ug/Kg0.97ND1,2,3-Trichlorobenzene 5.0 04/10/14 U SW8260ug/Kg1.0ND1,2,3-Trichloropropane 5.0 04/10/14 U SW8260ug/Kg0.71ND1,2,4-Trichlorobenzene 5.0 04/10/14 U SW8260ug/Kg1.0ND1,2,4-Trimethylbenzene 5.0 04/10/14 U SW8260ug/Kg0.72ND1,2-Dibromo-3-chloropropane 5.0 04/10/14 U SW8260ug/Kg1.3ND1,2-Dibromoethane 5.0 04/10/14 U SW8260ug/Kg1.3ND1,2-Dichlorobenzene 5.0 04/10/14 U SW8260ug/Kg0.55ND1,2-Dichloroethane 5.0 04/10/14 U SW8260ug/Kg0.44ND1,2-Dichloropropane 5.0 04/10/14 U SW8260ug/Kg0.71ND1,3,5-Trimethylbenzene 5.0 04/10/14 U SW8260ug/Kg0.66ND1,3-Dichlorobenzene 5.0 04/10/14 U SW8260ug/Kg0.74ND1,3-Dichloropropane 5.0 04/10/14 U SW8260ug/Kg0.53ND1,4-Dichlorobenzene 5.0 04/10/14 U SW8260ug/Kg0.79ND2,2-Dichloropropane 5.0 04/10/14 U SW8260ug/Kg0.84ND2-Chlorotoluene 5.0 04/10/14 U SW8260ug/Kg0.80ND2-Hexanone 25 04/10/14 U SW8260ug/Kg2.3ND2-Isopropyltoluene 5.0 04/10/14 U SW8260ug/Kg 10.69
Page 38 of 40 Ver 1
TRIP BLANK LOWPhoenix I.D.: BG29075
Client ID:DOMINO SUGAR SITEProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
ND4-Chlorotoluene 5.0 04/10/14 U SW8260ug/Kg0.58ND4-Methyl-2-pentanone 25 04/10/14 U SW8260ug/Kg1.2NDAcetone 50 04/10/14 U SW8260ug/Kg5.0NDAcrylonitrile 10 04/10/14 U SW8260ug/Kg2.8NDBenzene 5.0 04/10/14 U SW8260ug/Kg0.99NDBromobenzene 5.0 04/10/14 U SW8260ug/Kg0.65NDBromochloromethane 5.0 04/10/14 U SW8260ug/Kg0.73NDBromodichloromethane 5.0 04/10/14 U SW8260ug/Kg0.62NDBromoform 5.0 04/10/14 U SW8260ug/Kg0.70NDBromomethane 5.0 04/10/14 U SW8260ug/Kg3.9NDCarbon Disulfide 5.0 04/10/14 U SW8260ug/Kg0.81NDCarbon tetrachloride 5.0 04/10/14 U SW8260ug/Kg0.58NDChlorobenzene 5.0 04/10/14 U SW8260ug/Kg0.74NDChloroethane 5.0 04/10/14 U SW8260ug/Kg1.2NDChloroform 5.0 04/10/14 U SW8260ug/Kg0.91NDChloromethane 5.0 04/10/14 U SW8260ug/Kg2.6NDcis-1,2-Dichloroethene 5.0 04/10/14 U SW8260ug/Kg1.1NDcis-1,3-Dichloropropene 5.0 04/10/14 U SW8260ug/Kg0.54NDDibromochloromethane 5.0 04/10/14 U SW8260ug/Kg0.56NDDibromomethane 5.0 04/10/14 U SW8260ug/Kg0.63NDDichlorodifluoromethane 5.0 04/10/14 U SW8260ug/Kg1.3NDEthylbenzene 5.0 04/10/14 U SW8260ug/Kg0.91NDHexachlorobutadiene 5.0 04/10/14 U SW8260ug/Kg1.1NDIsopropylbenzene 5.0 04/10/14 U SW8260ug/Kg0.96NDm&p-Xylene 5.0 04/10/14 U SW8260ug/Kg2.0NDMethyl Ethyl Ketone 30 04/10/14 U SW8260ug/Kg4.3NDMethyl t-butyl ether (MTBE) 10 04/10/14 U SW8260ug/Kg1.4NDMethylene chloride 5.0 04/10/14 U SW8260ug/Kg0.82NDNaphthalene 5.0 04/10/14 U SW8260ug/Kg1.3NDn-Butylbenzene 5.0 04/10/14 U SW8260ug/Kg0.91NDn-Propylbenzene 5.0 04/10/14 U SW8260ug/Kg0.90NDo-Xylene 5.0 04/10/14 U SW8260ug/Kg1.9NDp-Isopropyltoluene 5.0 04/10/14 U SW8260ug/Kg0.72NDsec-Butylbenzene 5.0 04/10/14 U SW8260ug/Kg0.94NDStyrene 5.0 04/10/14 U SW8260ug/Kg1.4NDtert-Butylbenzene 5.0 04/10/14 U SW8260ug/Kg0.80NDTetrachloroethene 5.0 04/10/14 U SW8260ug/Kg1.1NDTetrahydrofuran (THF) 10 04/10/14 U SW8260ug/Kg 14.5NDToluene 5.0 04/10/14 U SW8260ug/Kg0.79NDtrans-1,2-Dichloroethene 5.0 04/10/14 U SW8260ug/Kg1.0NDtrans-1,3-Dichloropropene 5.0 04/10/14 U SW8260ug/Kg1.0NDtrans-1,4-dichloro-2-butene 10 04/10/14 U SW8260ug/Kg9.3NDTrichloroethene 5.0 04/10/14 U SW8260ug/Kg1.1NDTrichlorofluoromethane 5.0 04/10/14 U SW8260ug/Kg1.1NDTrichlorotrifluoroethane 5.0 04/10/14 U SW8260ug/Kg0.78NDVinyl chloride 5.0 04/10/14 U SW8260ug/Kg1.6
QA/QC Surrogates100% 1,2-dichlorobenzene-d4 04/10/14 U 70 - 130 %%96% Bromofluorobenzene 04/10/14 U 70 - 130 %%
Page 39 of 40 Ver 1
TRIP BLANK LOWPhoenix I.D.: BG29075
Client ID:DOMINO SUGAR SITEProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
101% Dibromofluoromethane 04/10/14 U 70 - 130 %%101% Toluene-d8 04/10/14 U 70 - 130 %%
Comments:
TRIP BLANK INCLUDED. %SOLIDS ASSUMED 100%
All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments.
1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.
If there are any questions regarding this data, please call Phoenix Client Services at extension 200.This report must not be reproduced except in full as defined by the attached chain of custody.
Reviewed and Released by: Greg Lawrence, Assistant Lab Director
RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level LOD=Limit of Detection MDL=Method Detection Limit
Additional 8270 criteria: 20% of compounds can be outside of acceptance criteria as long as recovery is at least 10%. (Acid surrogates acceptance range for aqueous samples: 15-110%, for soils 30-130%)
$8270SMRDP Benzo(b)fluoranthene 10003700 270 ug/KgBG29073 NY / 375-6.8 Semivolatiles / Residential Restricted 1000$8270SMRDP Benzo(b)fluoranthene 10003700 270 ug/KgBG29073 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Benzo(k)fluoranthene 10001200 270 ug/KgBG29073 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Benzo(k)fluoranthene 8001200 270 ug/KgBG29073 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 800$8270SMRDP Benzo(a)pyrene 10002500 270 ug/KgBG29073 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Benzo(a)pyrene 10002500 270 ug/KgBG29073 NY / 375-6.8 Semivolatiles / Residential Restricted 1000$8270SMRDP Benzo(a)pyrene 10002500 270 ug/KgBG29073 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Indeno(1,2,3-cd)pyrene 500890 270 ug/KgBG29073 NY / 375-6.8 Semivolatiles / Residential 500$8270SMRDP Indeno(1,2,3-cd)pyrene 500890 270 ug/KgBG29073 NY / 375-6.8 Semivolatiles / Residential Restricted 500$8270SMRDP Indeno(1,2,3-cd)pyrene 500890 270 ug/KgBG29073 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 500CU-SM Copper 5051.2 0.36 mg/kgBG29073 NY / 375-6.8 Metals / Unrestricted Use Soil 50PB-SMDP Lead 63156 7.2 mg/KgBG29073 NY / 375-6.8 Metals / Unrestricted Use Soil 63
$8260-SMDPR Vinyl chloride 210ND 250 ug/KgBG29074 NY / 375-6.8 Volatiles / Residential 210$8260-SMDPR Vinyl chloride 20ND 250 ug/KgBG29074 NY / 375-6.8 Volatiles / Unrestricted Use Soil 20$8260-SMDPR 1,2-Dichloroethane 20ND 250 ug/KgBG29074 NY / 375-6.8 Volatiles / Unrestricted Use Soil 20$8260-SMDPR Acetone 50ND 2500 ug/KgBG29074 NY / 375-6.8 Volatiles / Unrestricted Use Soil 50$8260-SMDPR Benzene 60ND 250 ug/KgBG29074 NY / 375-6.8 Volatiles / Unrestricted Use Soil 60$8260-SMDPR Methyl Ethyl Ketone 120ND 1500 ug/KgBG29074 NY / 375-6.8 Volatiles / Unrestricted Use Soil 120$8260-SMDPR Methylene chloride 50ND 250 ug/KgBG29074 NY / 375-6.8 Volatiles / Unrestricted Use Soil 50$8260-SMDPR trans-1,2-Dichloroethene 190ND 250 ug/KgBG29074 NY / 375-6.8 Volatiles / Unrestricted Use Soil 190
Phoenix Laboratories does not assume responsibility for the data contained in this report. It is provided as an additional tool to identify requested criteria exceedences. All efforts are made to ensure the accuracy of the data (obtained from appropriate agencies). A lack of exceedence information does not necessarily suggest conformance to the criteria. It is ultimately the site professional's responsibility to determine appropriate compliance.
This laboratory is in compliance with the NELAC requirements of procedures used except where indicated.
This report contains results for the parameters tested, under the sampling conditions described on the Chain Of Custody, as received by the laboratory.
A scanned version of the COC form accompanies the analytical report and is an exact duplicate of the original.
1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.
If there are any questions regarding this data, please call Phoenix Client Services at extension 200.This report must not be reproduced except in full as defined by the attached chain of custody.
Reviewed and Released by: Greg Lawrence, Assistant Lab Director
RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level
Phoenix Laboratories does not assume responsibility for the data contained in this report. It is provided as an additional tool to identify requested criteria exceedences. All efforts are made to ensure the accuracy of the data (obtained from appropriate agencies). A lack of exceedence information does not necessarily suggest conformance to the criteria. It is ultimately the site professional's responsibility to determine appropriate compliance.