basis mol

7/24/2019 basis mol

1/380

GPM (GROSS PROFIT MARGIN)

KOMPONEN $/kg $ / Lb BM $ /Lb molCH3OH 0.801 0.36332749 32.042 11.6417395HCl 0.4 0.18143695 36.461 6.61537263

CH3Cl 2 0.90718475 50.488 45.8019436H2O 0 0 18.015 0

1 Kg = 2.204623 Lb

reaksi :

GPM P!o"#k %&'k(') *1 + CH3Cl , 1 + H2O- *1 + CH3OH , 1 + HCl-

27.5448315

CH3OH + HCl CH3Cl + H2O

7/24/2019 basis mol

2/380

Komponen BM perr!"s #$emi#al engineers" $an%book&'($ e%i(ion) (a

CH3OH 32.042

HCl 36.461

CH3Cl 0.4''

H2O 1'.01

Kapasi(as 42000 (on,(a$-n reaksi CH3OH +

1 (a$-n = 330 $ari

24 /am

(on = 1000 Kg

7/24/2019 basis mol

3/380

le 2*13

Cl ** CH3Cl + H2O

7/24/2019 basis mol

4/380

rasio mol CH3OH : HCl HCl e#ess 1

1 : 1.1

ak(or s#ale*-p pabrik = 1

as-msi basis CH3OH : 100 Kmol,/am

3204.2 Kg,/am

konersi CH3OH = .00 Kirk o($mer)

kem-rnian CH3OH = .0 5llman& 40 ol)

CH3OH reaksi = Konersi m-la*m-la

komponen mol Kmol,/am Kg,/am bereaksi Kmol) sisa kmol)

CH3OH . . 3200.64.0 4.

H2O 0.1 0.1 1.'01

CH3OH + HCl CH3Cl

m-la . 114.''

reaksi 4.0 4.0 4.0

sisa 4. 1.' 4.0

kon%isi operasi:

7 = 300 Ckomponen8 = 3 bar = 2.6 a(m

CH3OH

pro%-k HCl

CH3Cl

H2O

7o(al Kg,/am)

-mpan

7/24/2019 basis mol

5/380

gar (i%ak (erben(-k pro%-k samping& !ai(- %ime(il e($er pa(en( 4&22&043)

HCl (eori(is = . kmol,/am 3642.43 Kg,/am

HCl e#ess = 14.' Kmol,/am 46.36'0' Kg,/am

HCl (o(al = 114.'' Kmol,/am 41''.'21' Kg,/am

kem-rnian HCl = 31

komponen mol Kmol,/am Kg,/am bereaksi kmol) sisa Kmol)

HCl 31 114.'' 41''.'224.0 1.'

H2O 6 2.91199 4606.64'

+ H2O

4.0 H2O (o(al pro%-k = H2O %ari me(anol + H2O %ari H

4.0

;857 O57857 np-(

Kmol,/am Kg,/am Kmol,/am Kg,/am raksi b

. 3200.' 4. 160.049 CH3OH 26.69''

114.'' 41''.'21 1.' 92'.409' HCl 34.11

0 0 4.0 491.636 CH3Cl 0.0000

2.'11' 460'.4411 30.916994 631'.1629 H2O 3'.403

490.6' 11'.266 490.6994 11'.269 100.0000

kem-rnian C$3Cl =

7/24/2019 basis mol

6/380

l + H2O reaksi

O-(p-(

era(

1.333

6.0916

3.3

2.60

100.0000

3.346

7/24/2019 basis mol

7/380

7/24/2019 basis mol

8/380

bera(

CH3OH 1.33341 0.430623 1.363

HCl 6.091633 0.09''4' 9.91312

CH3Cl 3.346 61.22'24 2.6223

H2O 2.6'6 3'.2432039 39.16416

7/24/2019 basis mol

9/380

ang bers-$- 10 * 20 C

r $ar-s bers-$- 30*40 C

77OM

Kg,/am

12'.03'32

921.20'92223.9'1'2

3494.'49'

463.'134 Kmol !ang (erserap : 221.419 Kmol

49'6.640' H2O %ari -(ili(as !ang %ib-(-$kan : 7o(al Kmol !aang (ers

30.3994 3''.'03 Kg,/am

169'4.'30'

H2O e#ess 20 agar pen%inginan semp-rna = 49'6.64

7/24/2019 basis mol

10/380

7/24/2019 basis mol

11/380

erap @ BM Kmol

Kg,/am

7/24/2019 basis mol

12/380

7/24/2019 basis mol

13/380

ke %is(ilasi

CA

(op pro%-#(

%ari -en#$er

ke -(ili(as

?s-msi: me(il klori%a (erserap ole$ H2O

inp-( komponen Kmol (erserap kmol) Kg

CH3OH 0.0 0.92 32.0100

HCl 0.1' 0.1' 9.2'4

CH3Cl 0.1' 4.0'0 41.'

H2O 19.'22 126.2'0 2'43.1932

7O7?L 131.921

maka kebutuhan H2O :

(o(al Kmol BM H2O = 2393.0291 Kg,/am

%ig-nakan air proses berlebi$ 20 -n(-k men!emp-rnakan pen!erapan

(o(al air proses = 2'49.6324'1320'Kg,/am

H2O pro%-k baa$ = air proses + H2O !ang (erserap

293.'0Kmol,/am

komponeninp-( 7

Kmol,/am Kg,/am Kmol,/am

CH3OH 0.0 32.0100 0.1'

7/24/2019 basis mol

14/380

HCl 0.1' 9.2'4 0.0400

CH3Cl 0.1' 41.' '.61'

H2O 19.'22 2'43.1932 31.64

>5ML?H 9434.43

C 1'.0901 2'49.632

7O7?L 102'2.0'60

komponeninp-(

o-(p-(

(op bo((om

bera(

CH3OH 0.43062321 0.13062431 1.010944'64'

HCl 0.09''4991 0.0292'99 0.230029'16

CH3Cl 61.22'24463 ''.2363624 '.'3323

H2O 3'.24320390' 11.602903311 '.99'9''9'

100 100 100

7/24/2019 basis mol

15/380

lolos kmol) Kg

0.1' 6.401

0.0400 1.46'

'.61' 4324.3'61

31.64 6'.63464

400.'9'0

p Bo((om

Kg,/am Kmol,/am Kg,/am

6.4020 0.92 2.60'0

7/24/2019 basis mol

16/380

1.490 0.1' .'29

4324.3'62 4.0'0 229.3

6'.6346 126.2'0 2294.3'6

400.'9' 233.939

2'49.632

3'1.2062

102'2.0'60

7/24/2019 basis mol

17/380

D

A

NM OVER ALL : F = D + W

komponen 7i(ik %i%i$ C ) 1 a(m)

CH3OH 64.4 CH3Cl

HCl 0. HCl

CH3Cl *24.3 CH3OH

H2O 100 H2O

DEE

komponen Kmol Kg Fi @i

? CH3OH 0.1' 6.40116 0.0019010621 0.001306

B HCl 0.036 1.46'16 0.0003402124 0.00029

C CH3Cl '.61962 4324.3'61' 0.922240416 0.''236

H2O 31.6406' 6'.634641' 0.26'9346'3 0.116029

7O7?L 119.460322 400.'9' 1 1

NM komponen CH3OH (A

mol CH3OH . D = !?. + @? . A

!?. + @? . A = 0.1' Kmol . . . . 3)

karena . CH3OH bera%a %i %is(ila( maka:

. mol CH3OH . D = !? .

F?. = 0.19'002Kmol . . . . 4)

7/24/2019 basis mol

18/380

s-bs(i(-si 4) ke 3)

@?. A= 0.00001' Kmol

komponen @. D @. @A. A

CH3OH 0.1' 0.19'002 0.00001'

HCl 0.036 0.036 0CH3Cl '.61962 '.61962 0

H2O 31.6406' 3.16406' 2'.40'0'909

7O7?L 119.460322 '.04934 2'.40'09'6'9

LA!" AL#R D# D#$%#LA% = '.04934'99Kmol

LA!" AL#R D# &O%%OM = 2'.40'09'6'9Kmol

7 ee% = 24 K 20.' C

8 = 960 mmHg 1 a(m

komponen @D 8sa( Ki G

CH3OH 0.001901062 101.'69441 0.134033'93' .699'9

HCl 0.000340212 3146.691'9 42.0304603 1946.144

CH3Cl 0.92224042 3'1'.00'9' .0239114' 20'.6'94

H2O 0.26'9346'4 1'.234 0.02409306' 1

7 (rial = 300 K

% 'e = 7 soler = 303.3139K 30.1639201C

8 = 960 mmHg 1 a(mkomponen ! 8sa( Ki G

CH3OH 0.00224311 16.1'96' 0.2193209 .16'2

HCl 0.00044'949 3'30.6'34 1.22412414 121'.40

CH3Cl 0.61'611 4''.1432 6.63346433' 16.112'

H2O 0.03446642 31.21662 0.0420423232 1

7rial = 30 K

% bub)e 7 soler = 393.1201K 100.00200C

8 = 960 mmHg 1 a(m

komponen @ 8sa( Ki GCH3OH 9.03321E*009 26'.09462 3.494699132 3.49493

HCl 0 12361.90 162.693263 162.696

CH3Cl 0 23332.2291 30.9003'1429 30.90043

H2O 0.29 9.'' 0.'446 1

7/24/2019 basis mol

19/380

D*t,*bu* komponen

komponen inp-( is(ila( as(e

CH3OH 0.1' 0.19'002 0.00001'

HCl 0.036 0.036 4.'134'E*022

CH3Cl '.61962 '.61962 2.419'1E*012

H2O 31.6406' 3.16406' 2'.40'0'909

119.460322 '.04934 2'.40'09'6'9

komponen;857

O57

Kmol,/am Kg,/am Kmol,/am Kg,/am

CH3OH 0.1' 6.40116 0.19'002 6.40131

HCl 0.036 1.46'16 0.036 1.46'2

CH3Cl '.61962 4324.3'61' '.61962 4324.3'6

H2O 31.6406' 6'.634641' 3.1640699 6.'634643'.10'

400.'9'

komponen inp-( (op bo((om

bera(

CH3OH 0.1306243 0.14'4626 0.00012046

HCl 0.0292'' 0.033131 3.423E*021

CH3Cl ''.236362 '.239 2.3'2E*011

H2O 11.6029033 1.2'6 .'9403

men-h*tun- ,e.u/

7 ae = 7%e + 7b-bl = 33'.232'2'2'' K

2

8 = 1 a(m 960 mmHg

komponen @ @% @ 8sa(

C$3OH 0.001901062 0.00224311 9.033211E*009 999.214

HCl 0.000340212 0.00044'949 1.6442E*023 93'32.64

CH3Cl 0.92224042 0.61'611 '.11012E*014 11991.'9H2O 0.26'9346'4 0.03446642 0.269 1''.331

-mpan mas-k %alam kea%aan /en-$ 1*=0)& maka = 1

0.

soler = 0.000

(rial =

7/24/2019 basis mol

20/380

komponen @ G G.@ , G*

CH3OH 0.0019 4.1293 0.001

HCl 0.0003 32.0366 0.0003

CH3Cl 0.922 62.063 0.931

H2O 0.26'9 1.0000 0.39

7O7?L 1.0000 1.294'

maka : = 0.

komponen @% G G.@% , G*

CH3OH 0.0022 4.1293 0.0026

HCl 0.0004 121'.403 0.0004

CH3Cl 0.61 16.112' 0.60

H2O 0.034 1.0000 0.090

7O7?L 1.0000 1.03''

Komposisi reI- L)

komponen @L kmol,/am

CH3OH 0.0022 0.011641194

HCl 0.0004 0.00232'46'

CH3Cl 0.61 4.0243

H2O 0.034 0.1'3262'

.1'''201

Komposisi -ap )

komponen F Kmol,/am

CH3OH 0.0022 0.21142114

HCl 0.0004 0.0422''46'

CH3Cl 0.61 0.6426'94

H2O 0.034 3.340399249

4.2369944

7/24/2019 basis mol

21/380

*24.3

0.

011L

455H

F = raksi mol

@ = raksi bera(

NM komponen H2O (D

!B . + @B . A = 31.6406994

karena 0 H2O bera%a %ibo((om maka:

0.0 mol H2O . D = @B . A

@B . A = 2'.40'0'909

mol H2O D = !B. + @

B. A

7/24/2019 basis mol

22/380

s-bs(i(-si 2) ke 1)

!B. 3.1640699

an(oine grain 7oler& C$emi#al enginee

komponen ?

CH3OH 1'.'9HCl 16.04

CH3Cl 16.102

H2O 1'.3036

!D D#$%R#&"$# OM6ONEN

0.00022' GL. = .16'200'

0.014300'61 GL. A = 3.494929'3

3.663440121 GL. ?e =

0.00646296 4.2222046

3.6'4

;m = 4.41099'

0.62'6162413

9.''111'4'2@

0.010321'9

'.9603'E*006

0.146040'

0.'4311'092

1.0000 untuk komponen HC) (&

GHCl. ?e =

44.1993332906

!A @B. = '.3016909E+012.4'4E*006 @B.A

0 @B. = '.3016909E+01

0

0.991 @B.D = @B. + @B.A

1.0000 s-bs(i(-si 1) ke 2)

@BA.A = 4.'1349043E*022

@B. = 0.036

GL. GL. A)J0.

G HCl. GHCl. A)J0.

CT

BAPsat

+=l)

7/24/2019 basis mol

23/380

untuk komponen met*) k)o,*'a ( C

G CH3Cl. ?e =

6.2266

@C. = 342296402.1

@[email protected] = 342296402.1

@C.D = @C. + @C. A

57 s-bs(i(-si 3) ke 4)

A @C.A = 2.419'143'4E*012

Kmol,/am Kg,/am @C. = '.61962

0.00001' 0.0006402

4.'13E*022 1.96E*020

2.419'1E*012 1.22E*010

2'.40'0'91 11.9911' kem-rnian CH3Cl %i%is(ila( =11.991'2 kem-rnian C$H3Cl %i bo((om =

400.'9'

ki G

1.02291'0 4.1292622

9.14'209 32.036'

1.4'3029 62.06230.249'033 1

geankoplis& persamaan 11.9*1)

G CH3Cl. G CH3Cl. A

= fX

q.

1

7/24/2019 basis mol

24/380

m,m+1 = 0.03934

m + 1 = G.@ , G*

m 0.03''

= 1.000 %m

= 0.0'3

eI-ks %is(ila(

L = .1''' Kg,/am

-ap !ang kel-ar %is(ila( men-/- kon%ensor

= L +

= 4.236'Kg,/am

7/24/2019 basis mol

25/380

Kmol . . . . 1)

Kmol . . . . 2)

7/24/2019 basis mol

26/380

Kmol

ing %esign)

B C

3626. *34.21914.2 *14.4

2099.9 *2.

3'16.44 *46.13

8 = mmHg

7 = Kelin

?& B& C = kons(an(a ?n(oine

Meng$i(-ng s(age (eori(is ;m)

s(age

@?.A . . . 1)

. . . 2)

WLDLAverageL x ... =

AverageL

WL

wH

DH

DL

m

Log

WX

WXx

DX

DXLog

N

.

.

.

.

. -.

.*-

.

./*

=

WBDBAverageL x ... =

X

Xx

WX

DX

WH

DH

average

WB

DB mN

.

.-*

.

.

.

.

.

. =

7/24/2019 basis mol

27/380

@C.A . . . . . 3)

. . . . 4)

'.23931 2.3'22'9E*011

men-h*tun- kapa*taCH3Cl !ang %i%apa( %ari %is(ila( = 4324.3'61'1 Kg,/am

1039'.26'44Kg,$ari

342413'.'6Kg,(a$-n

3424.13''67on,(a$-n

kapasi(as !ang %i$arapkan = 2000 (on,(a$-n

ak(or s#ale *-p pabrik = 0.0'3623

maka keb-(-$an: me(anol .'363Kmol,/am 1'9.1113Kg,/amHCl 6.9149 Kmol,/am 244.'39 Kg,/am

)J0.

7/24/2019 basis mol

28/380

7/24/2019 basis mol

29/380

7/24/2019 basis mol

30/380

7/24/2019 basis mol

31/380

7/24/2019 basis mol

32/380

7/24/2019 basis mol

33/380

komponen;857 O578


CH3OH . 3200.' 4.

HCl 114.'' 41''.'21' 1.'

CH3Cl 0 0 4.0

H2O 2.'11994 460'.4411206' 30.91699413

11'.266'906' 11'.266

komponen ;857 7O


CH3OH 4. 160.049 0.

HCl 1.' 92'.409' 0.1'

CH3Cl 4.0 491.6364 0.19

H2O 30.916994 631'.1626'906' 19.'224'3'91

air pen%ingin 26.6''11 49'6.6409'3 0

169'4.'30966'06

komponen;857

?8


CH3OH 0. 32.00' 0.1'

HCl 0.1' 9.2'409' 0.036CH3Cl 0.19 41.'4' '.61962

H2O 19.'224' 2'43.19320136 31.6406994

CA 1'.09009 2'49.6324'1320'

102'2.0'60143144

komponen;857

7


CH3OH 0.1' 6.40116 0.19'002

HCl 0.036 1.46'16 0.036

CH3Cl '.61962 4324.3'61'1 '.61962

H2O 31.6409 6'.634641'3'9 3.1640699

400.'9'000'9

7/24/2019 basis mol

34/380

komponen ;857 Kg,/am)

reak(or CA

7/24/2019 basis mol

35/380

57

Kg,/am REA%160.049

92'.409'

491.6364

631'.1626'906'

906'

O57857

BO77OM

Kg,/am Kmol,/am Kg,/am

32.00' 3.6 12'.03'32

9.2'409' 1.9'02 921.20'922 "EN41.'4' 4.942 23.9'1'2

2'43.19320136 12.'422'06 3494.'49903

0 26.6''106' 49'6.6409'4

9434.433236 30.3994436'9

169'4.'30966'06

O57857

L

7/24/2019 basis mol

36/380

O57857 Kg,/am)

bo((om -en#$er L s#r-bber %is(ila( as(e NM OV12'.03'32 2.609664 6.40131400' 0.00064012

921.20'922 .'292624 1.46'16 1.9069924222E*020

23.9'1'2 229.292 4324.3'61'1 1.22090643411E*010

'261.394'91 122.19104'6' 6.'634641'3 11.99119964'

30.3994436'91 3'1.20621422 43'.109'224 11.991'19'41

470321031895548

7/24/2019 basis mol

37/380

OR

H $;$%EM

&ER

$#

7/24/2019 basis mol

38/380

ER ALL

7/24/2019 basis mol

39/380

basis per$i(-ngan 1 /am operasi

sa(-an operasi /o-le,/am

7empera(-r basis 2 2'.1K

;E mi($& 2001)

%eal gas

komponen ? B C

CH3OH 21.1 9.0E*02 2.E*0 *2.'E*0'

HCl 30.69 *9.20E*03 1.2E*0 *3.0E*0

CH3Cl 13.'' 1.01E*01 *3.'E*0 2.9E*0

H2O 32.24 1.2E*03 1.06E*0 *3.60E*0

CH3OCH3 9.4 1.69E*01 .E*06 *3.34E*0'

Cp li-i%

ase li-i% #1 #2 #3 #4 #

CH3OH 1.06E+0 *362.23 0.39 0 0HCl 49300 0 0 0 0

CH3Cl 610 *209. 0.3946 0.0004'' 0

H2O 296390 *200.1 '.12 *0.014116 .3901E*006

0C

==T

T

pii dTCnHQ0

..

432

32

432T

DT

CT

BATCp

DTCTBTACpdtT

To

+++=

+++=

5432

432

5

5

4

4

3

3

2

21

54321

TC

TC

TC

TC

TCCp

TCTCTCTCCCpdt

T

To

++++=

++++=

7/24/2019 basis mol

40/380

gain 7oler& C$emi#al engineering %esign)

Cp gas

ase gas

HCl

8err!& (able 2*16 $al 220)

Cp = >,Kmol K

+= -&+*..

DT

CBAdTCp

7/24/2019 basis mol

41/380

H2O

L&b =

7# =

7b =

L = la(en( $ea( (empera(-re 7& K/,Kmol

L&b = la(en( $ea( a( ($e normal boiling poin(& K/,Kmol 7 =

7# = #ri(i#al (empera(-re & K

7b = boiling poin(& K L =7 = 7empera(-re& K

6.9+0.000'47 8err!&(able 2*14 $al 211)

=bc

c

bvvTT

TTLL .

7/24/2019 basis mol

42/380

406'3 K/,kmol

649.3K

100C

393.1K

30 C

303.1K

1090.9'

7/24/2019 basis mol

43/380

s(eam

7s = 300 C

7i = 30 C 7o = 20 C

s(eam kon%ensa(

7= 300 C

Ne,a

7/24/2019 basis mol

44/380

N s(eam = 31'' K/,Kg 1312.03' b(-,lb

< s(eam =

M s(eam = 0.6261342Kg

NERACA ENER>#

inp-( o-(p-(Komponen H K/,/am) H K/,/am)

CH3OH 6426.1'61309 19202.1'621

H2O 166.24963092' 2149.41336192

< s-ppl! 1936.16 0

< loss 0 '996.'096

1'1'1 1'1'1

Ms(eam . Ns(eam

7/24/2019 basis mol

45/380

D-ngsi : meng-apkan me($anol %engan ba

kon%isi operasi : 7 = 20

8 = 1.'

li-i%

komponen

CH3OH

HCl

CH3Cl

H2O

as

komponen

CH3OH

HCl

CH3Cl

H2O

enta)p* k2 C 7 =

2'.1K

komponen

CH3OH

H2O

enta)p* k

gan maksim-m 10 ) -lri#$& $al 432)

N CH3OH

N H2O

1 a(m = 101.32 Kpa

komponen

=T

T

p

ref

dCH

7/24/2019 basis mol

46/380

geankoplis& s(eam (able ?.2*10 CH3OH

H2O

= bvv LL .

7/24/2019 basis mol

47/380

(-an s(eam

C

a(m

C4 C2 C3 C1 C8

1.06E+0 *3.62E+02 .3'E*01 0.00E+00 0

4.93E+04 .00E+01 0.00E+00 0.00E+00 0

.6E+04 *2.0'E+02 3.9E*01 4.''E*04 0

2.96E+0 *2.0E+03 '.13E+00 *1.41E*02 .39E*006

A & C D

2.12E+01 9.0E*02 2.E*0 *2.'E*0'

3.09E+01 *9.20E*03 1.2E*0 *3.0E*0

1.3E+01 1.01E*01 *3.'E*0 2.9E*0

3.22E+01 1.2E*03 1.06E*0 *3.60E*0

mponen ke)ua,20 C 7re = 2 C

23.1 K 2'.1 K

n Kmol,/am) H K/,/am)

6633.'642461 122.0'1069 '12902.9

9340.442426 0.122630'21 00.16

'13602.

mponen

(er/a%i per-ba$an ase

329' K/,Kmol gain 7oler& C$emi#al engineering %esign)

406'3 K/,Kmol

n Kmol,/am) H

Cp %7

Cp %7

+ nT -.*

7/24/2019 basis mol

48/380

6633.'642461 122.0'1069 19202

9340.442426 0.122630'21 2149.413

193200

H2O

L&b =

7# =

7b =

L = la(en( $ea( (empera(-re 7& K/,Kmol

L&b = la(en( $ea( a( ($e normal boiling poin(& K/,Kmol 7 =

7# = #ri(i#al (empera(-re & K

7b = boiling poin(& K L =

7 = 7empera(-re& K

CH3OHL&b =

7# =

7b =

7 =

L =

bc

c

TT

TT

7/24/2019 basis mol

49/380

7/24/2019 basis mol

50/380

406'3 K/,kmol

93.1K

100C

393.1K

20C

23.1K

10190.9

329' K/,kmol 329'

93.1K

64.4C

339.K

20C

23.1K

94'6.'42

7/24/2019 basis mol

51/380

s(eam

7s = 300 C

7i = 30 C 7o = 20 C

s(eam kon%ensa(

7 = 300 C

;era#a energi (o(al:

H inp-( + < s-ppl! = H o-(p-( + < loss

enta)p* komponen *nput7 = 30 C 7re =

303.1K

komponen n Kmol,/am) H K/,/am)

HCl 23962 140.''4412' 33499.66

H2O 136060.01'9' 313.'144366 4223.3

4'912.

ne,a

7/24/2019 basis mol

52/380

M s(eam = 213.'10932060Kg

NERACA ENER>#inp-( o-(p-(

Komponen H K/,/am) H K/,/am)

HCl 33499.660131493 1436040.299

H2O 4223.2'04442 411''.'063

< s-ppl! 6'0'64.613'0'4 0

< loss 0 34044'.2306

926969' 926969'

7/24/2019 basis mol

53/380

D-ngsi : meng-apkan HCl %engan ban(-an s(eam

kon%isi operasi : 7 = 20 C

8 = 1.' a(m

komponen ? B

CH3OH 21.1 9.0E*02

HCl 30.69 *9.20E*03

CH3Cl 13.'' 1.01E*01

H2O 32.24 1.2E*03

komponen C1 C2CH3OH 1.06E+0 *3.62E+02

HCl 4.93E+04 .00E+01

CH3Cl .6E+04 *2.0'E+02

H2O 2.96E+0 *2.0E+03

enta)p* komponen ke)ua,2 C 7 = 20 C

2'.1 K 23.1 K

komponen n Kmol,/am)

HCl 6963.2'6 140.''4412'

H2O 9340.44 313.'14439

enta)p* komponengan maksim-m 10 ) -lri#$& $al 432)

N HCl 16161 K/,Kmol

N H2O 406'3 K/,Kmol

komponen n Kmol,/am)

& s(eam (able ?.2*10 HCl 6963.2'6 140.''4412'

H2O 9340.44 313.'14439

Cp %7

Cp %7

+=T

T

p

ref

ndTCH -.*

7/24/2019 basis mol

54/380

L = la(en( $ea( (em

L&b = la(en( $ea( a( (

7# = #ri(i#al (empera

7b = boiling poin(& K

7 = 7empera(-re& K

=

bc

cbvv

TT

TTLL .

7/24/2019 basis mol

55/380

C

2.E*0 *2.'E*0'

1.2E*0 *3.0E*0

*3.'E*0 2.9E*0

1.06E*0 *3.60E*0

C3 C4 C.3'E*01 0.00E+00 0

0.00E+00 0.00E+00 0

3.9E*01 4.''E*04 0

'.13E+00 *1.41E*02 .39E*006

7re = 2 C

2'.1K

H

2'41.9

2301'30

324692


gain 7oler& C$emi#al engineering %esign)

H

1436041

411'

7/24/2019 basis mol

56/380

62922

H2O

L&b = 406'3 K/,kmol

7# = 93.1 K

7b = 100 C

era(-re 7& K/,Kmol 393.1 K

e normal boiling poin(& K/,Kmol 7 = 20 C

(-re & K 23.1 K

L = 10190.9

CH3OH

L&b = 16161 K/,kmol

7# = 93.1 K

7b = 64.4 C

339.K

7 = 20 C

23.1K

L = 342.94

7/24/2019 basis mol

57/380

7i = 20 C 7o = 300 C

Ne,a

7/24/2019 basis mol

58/380

NERACA ENER>#komponen inp-( K/,/am) o-(p-( K/,/am)

CH3OH '12902.909 10'03'.9316403

HCl 0 1161299.139'1

H2O 2302930.44632 2'242.9'93'

< s-ppl! 2030'9.39

< loss 10143.96'961

7O7?L 146312.6' 146312.6'

7/24/2019 basis mol

59/380

D-ngsi : memanaskan me($anol %an HCl %engan ban(-an s(eam

kon%isi operasi : 7 = 300 C

8 = 3 a(m

komponen ?

CH3OH 21.1

HCl 30.69

CH3Cl 13.''

H2O 32.24

enta)p* kompone2 C 7 = 300

2'.1 K 93.1

Me($anol

komponen

CH3OH '636.493

H2O 006.94

HCl

komponen

HCl '242.96

H2O 006.94

%O%AL O"%6"% =

keb-(-$an s(eam

gan maksim-m 10 ) -lri#$& $al 432) s(eam !ang %ig-nakan

N s(eam = 31''

< s(eam =

M s(eam = 639.03''

Cp %7

Cp %7

Ms(eam .

7/24/2019 basis mol

60/380

7/24/2019 basis mol

61/380

B C

9.0E*02 2.E*0 *2.'E*0'

*9.20E*03 1.2E*0 *3.0E*0

1.01E*01 *3.'E*0 2.9E*0

1.2E*03 1.06E*0 *3.60E*0

n outputC 7re = 2 C

K 2'.1 K

n Kmol,/am) H

122.0'109 10'03

0.122630'22 1104.0

10143

n Kmol,/am) H

140.''4413 1161299

313.'1444 2'2434'

3'62

04496K/,>am

a%a (ekanan a(m %engan s-$- 360 C

K/,Kg eankoplis& s(eam (able ?.2*10

Kg

s(eam

7/24/2019 basis mol

62/380

7/24/2019 basis mol

63/380

7o = 330 C

7i = 300 C

300 C

2 C PH reaksi 2 C

Ne,a

7/24/2019 basis mol

64/380

ber%asarkan Himmelbla- $alaman 46:

panas reaksi s(an%ar& 2 C

reaksi !ang (er/a%i :

CH3OH + HCl ** CH3Cl + H2O

%a(a en(alpii pemben(-kan ain 7oler& #$emi#al engineering %esig

komponen PH K/,mol) K/,Kmol

CH3OH *201.3 *201300

HCl *2.36 *2360

CH3Cl *'6.39 *'6390

H2O *242 *242000

*622030

komponen n kmol) PH K/,/am) PH reaksi K/,/am)

CH3OH 6.124034 *1233044.319 *110636'.012392

HCl 24.0163'14 *226291.2'213

CH3Cl 116.3'29'11 *1001'0.'0946

H2O 430.0'6'613 *1040'1020.4423

*111201.012392

Ne,a

7/24/2019 basis mol

65/380

-ngsi : mereaksikan me(anol %an HCl

kon%isi operasi : 8 = 3 a(m

7 = 300 C

330 C

komponen ?

CH3OH 21.1

HCl 30.69

CH3Cl 13.''

H2O 32.24

enta)p* ke)ua,

7 = 330

603.1

04496'.9130K/,/am

komponen Cp %7

7/24/2019 basis mol

66/380

CH3OH 32.3'2936

HCl 12'.'21494133

CH3Cl ''9.191'4'92

H2O 10014.6'94'269

NERACA ENER>#komponen inp-( K>,/am)

n) CH3OH 10'03'.93164

HCl 1161299.139'

CH3Cl 0

H2O 2'242.9'936

PHr 110636'.01

< serap

116'193.923

ekso(ermis

110636'.01

kebutuhan a*, pen'*n-*n:

m = ,kmol K

7/24/2019 basis mol

70/380

NERACA ENER>#

komponeninp-( K/,/am) o-(p-( K/,/am)

(op bo((om

CH3OH 60'3.10131 1913.1'669 2943.10026

HCl 223691.0'036 449.200063 61.100'

CH3Cl 43.133102 1114'.'06 0

H2O 43091'.0664 3919.033 14106'.9

CA 9'0.349 0

< serap *10964.0

7O7?L 4'306.43 13061634.099

13041.026 13041.026

kebutuhan a*, pen'*n-*n: Cp air = 4.1'6'

7in = 20

m = < 7 o-( = 30

Cp.P7

26224.420Kg

< = m.Cp.P7

7/24/2019 basis mol

71/380

D-ngsi : men%inginkan se#ara men%a%ak %engan ban(-an air pen%ingin !a

kon%isi operasi :

7 = ' C

8 = 1 a(m

komponen C4 C2 C3

CH3OH 10'00 *362.23 0.39

HCl 49300 0 0

CH3Cl 610 *209. 0.3946

H2O 296390 *200.1 '.12

komponen ? B C

CH3OH 21.1 9.0E*02 2.E*0

HCl 30.69 *9.20E*03 1.2E*0

CH3Cl 13.'' 1.01E*01 *3.'E*0

H2O 32.24 1.2E*03 1.06E*0

CH3OCH3 9.4 1.69E*01 .E*06

enta)p* output%O6 6ROD"C%

7 = ' C 7re =

3'.1K

komponen n kmol) H

CH3OH 13'.426 1.220'106' 1913.1'669'9

C HCl 1'2'.123 0.240163'14 449.200063

K CH3Cl 1012.2' 110.636420 1114'.'061

H2O 13'.611 13.30'96 3919.032'

4'306.429&O%%OM 6ROD"C%

7 = 30 C 7re =

303.1K

N CH3OH 329' K/,Kmol

N HCl 16161 K/,Kmol gain 7oler& C

N H2O 406'3 K/,Kmol

Cp %7

7/24/2019 basis mol

72/380

komponen n Kmol,/am) H

CH3OH 2411.2 4.003296291 2943.10026

HCl 23962 24.2662194 61.100'

H2O 136060 10131.2106 14106'.92

141'.113

L = la(en( $ea( (empera(-re 7& K/,K

L&b = la(en( $ea( a( ($e normal boilin

K/,Kg K 7# = #ri(i#al (empera(-re & K

C 23.1 K 7b = boiling poin(& K

C 303.1 K 7 = 7empera(-re& K

Cp %7

=bc

c

bvvTT

TTLL .

7/24/2019 basis mol

73/380

g bers-$- 10 s,% 20 C

C1 C8

0 0

0 0

0.0004'' 0

*0.014116 .39E*006

*2.'E*0'

*3.0E*0

2.9E*0

*3.60E*0

*3.34E*0'

2 C

2'.1K

2 C

2'.1K

$emi#al engineering %esign)

7/24/2019 basis mol

74/380

H2O

L&b = 406'3 K/,kmol

7# = 303.1K

7b = 100 C

ol 393.1 K

poin(& K/,Kmol 7 = ' C

3'.1K

L = 316.21

CH3OH

L&b = 406'3 K/,kmol

7# = 303.1K

7b = 64.4 C

339.K

7 = ' C

3'.1K

L = 604.4

7/24/2019 basis mol

75/380

CA

7# = 30 C

7i= ' 7o = 0 C

CA

7#o = 4 C

NERACA ENER># %O%AL : H *nput = H o

enta)p* *nputH o-(p-( %ari (op

7/24/2019 basis mol

76/380

m = 4632.'243093Kg

7/24/2019 basis mol

77/380

D-ngsi = men%inginkan -ap kel-aran -en#$er %engan ban(-an CA

kon%isi operasi =

7 = 0 C

8 = 1 a(m

utput + e,ap

komponen ? B

CH3OH 21.1 9.0E*02

HCl 30.69 *9.20E*03

CH3Cl 13.'' 1.01E*01

H2O 32.24 1.2E*03

NERACA ENER>#

komponen inp-( K>,/am) o-(p-( K/,>am)CH3OH 1913.1'669'92 69.09402'

HCl 449.200062' 1'9.33094231

CH3Cl 1114'.'060' 41'46.90203339

H2O 3919.032' 1611.436'6

< serap 2049'.4030'21

4'306.4292 4'306.429249

7/24/2019 basis mol

78/380

7/24/2019 basis mol

79/380

C

2.E*0 *2.'E*0'

1.2E*0 *3.0E*0

*3.'E*0 2.9E*0

1.06E*0 *3.60E*0

7/24/2019 basis mol

80/380

7/24/2019 basis mol

81/380

CA

7# = 20 C 7o = 3 C

7i = 0 C 7 = 30 C

enta)p* *nputH o-(p-( %ari #ooler = 1''2'.436 K/,/am

Cooling a(er = 493463.6'' K/,/am

1731272232K/,/am

H2O %ari -(ili(as

7 = 20 C 7re = 2

23.1 K 2'.1

komponen kg,/am Kmol,/am HH2O 342.091014 13.'42639 136060.01 493464

H *nput = H output + e,ap< serap = *''1292.1K/,/am

Cp %7

7/24/2019 basis mol

82/380

NERACA ENER>#

komponeninp-( K/,/am) o-(p-( K/,/am)

(op bo((om

CH3OH 69.09403 263.44409 260.212296

HCl 1'9.3309423 9.032126 963.99444

CH3Cl 41'46.9020334 10.3'62 0

H2O 1611.436'6 62416.219 1393'30.1

CA 493463.6'' 0

< serap *''1292.1

7O7?L 9'660.1966 4'632.04

43422.2316 43422.2320

kebutuhan a*, pen'*n-*n: Cp air = 4.1'6'

7in = 20

m = < 7 o-( = 30

Cp.P7

212364.3'4Kg

< = m.Cp.P7

7/24/2019 basis mol

83/380

D-ngsi : men!erap HCl e#ess %an komponen lainn!a %engan ban(-an CA

kon%isi operasi :

7 = 3 C

8 = 1 a(m

komponen C4 C2 C3

CH3OH 10'00 *362.23 0.39

HCl 49300 0 0

CH3Cl 610 *209. 0.3946

H2O 296390 *200.1 '.12

komponen ? B C

CH3OH 21.1 9.0E*02 2.E*0

HCl 30.69 *9.20E*03 1.2E*0

CH3Cl 13.'' 1.01E*01 *3.'E*0

H2O 32.24 1.2E*03 1.06E*0

CH3OCH3 9.4 1.69E*01 .E*06

enta)p* output%O6 6ROD"C%

7 = 3 C 7re =

30'.1K

komponen n kmol) H

CH3OH 21.046 1.220'106' 263.444069

C HCl 306.3441 0.240163'14 9.0321261

K CH3Cl 143.'9 110.636420 10.3'623

H2O 322.49 13.30'96 62416.219

9'660.1966&O%%OM 6ROD"C%

7 = 30 C 7re =

303.1K


N HCl 16161 K/,Kmol gain 7oler& C

N H2O 406'3 K/,Kmol

Cp %7

7/24/2019 basis mol

84/380

komponen n Kmol,/am) H

CH3OH 2411.2 4.003296291 260.212296

HCl 23962 24.2662194 963.99444

H2O 136060 10131.2106 1393'30.1

1394604.109

L = la(en( $ea( (empera(-re 7& K/,K

L&b = la(en( $ea( a( ($e normal boilin

K/,Kg K 7# = #ri(i#al (empera(-re & K

C 23.1 K 7b = boiling poin(& K

C 303.1 K 7 = 7empera(-re& K

Cp %7

=bc

c

bvvTT

TTLL .

7/24/2019 basis mol

85/380

C1 C8

0 0

0 0

0.0004'' 0

*0.014116 .39E*006

*2.'E*0'

*3.0E*0

2.9E*0

*3.60E*0

*3.34E*0'

2 C

2'.1K

2 C

2'.1K

$emi#al engineering %esign)

7/24/2019 basis mol

86/380

H2O

L&b = 406'3 K/,kmol

7# = 23.1K

7b = 100 C

ol 393.1 K

poin(& K/,Kmol 7 = 30 C

303.1K

L = 0'.39

CH3OH

L&b = 329' K/,kmol

7# = 23.1K

7b = 64.4 C

339.K

7 = 30 C

303.1K

L = 94.4

HCl

L&b = 16161 K/,kmol

7# = 23.1K

7b = 0. C

323.6K

7 = 30 C

303.1K

L = 2'.6'

7/24/2019 basis mol

87/380

CA

7# = 30 C

7i= 3 7o = 32. C

CA

7#o = 4 C

NERACA ENER># %O%AL : H *nput = H o

enta)p* *nputH o-(p-( %ari (op s#r-bber = 9'660.1'K/,>am

enta)p* output

7 = 20.' C 7re = 2 C

24 K 2'.1 K

komponen n kmol) HCH3OH *442211.'0469 0.24016 *10'.341

HCl *11.'9 0.04003 *.'112

CH3Cl *4039.66639914 10.03 *42431.99

H2O *11612'.4640'4 3'.909'2 *40.'

*'964.2'



N HCl 16161 K/,Kmol gain 7oler& C$emi#al enginee

N CH3Cl 21436 K/,Kmol

N H2O 406'3 K/,Kmol

komponen n kmol) H

CH3OH ''.3'3'2611 0.24016 *904.'99

HCl 129.21'9'9239 0.04003 *'030.02

CH3Cl '.4942421 10.03 1'362

Cp %7

Cp %7

+=T

T

p

ref

ndTCH -.*

7/24/2019 basis mol

88/380

H2O 133.'12'13'3 3'.909'2 *910349

112'12

;era#a energi (o(al

H inp-( = H o-(p-( + < serap

< serap = *10431.''2K/,/am 10432

keb-(-$an air pen%ingin:

H 4 C) = 1''.4 K/,Kg

H 30 C) = 12.9 K/,Kg

m =#komponen inp-( K>,/am) o-(p-( K/,>am)

CH3OH 263.444066' *904.'992'6

HCl 9.03212611 *'030.022349'4

CH3Cl 10.3'6233 1'3624.6491

H2O 62416.2194' *910349.42940'

< serap *10431.''2

9'660.1966 9'660.19660024

7/24/2019 basis mol

91/380

C

2.E*0 *2.'E*0'

1.2E*0 *3.0E*0

*3.'E*0 2.9E*0

1.06E*0 *3.60E*0

C3 C1 C8

0.39 0 0

0 0 0

0.3946 0.0004'' 0

'.12 *0.014116 .39E*006H2O

L&b = 406'3 K/,kmol

7# = 23.1 K

7b = 100 C

(empera(-re 7& K/,Kmol 393.1 K

a( ($e normal boiling poin(& K/,Kmol 7 = *16.3 C

pera(-re & K 26.' K

(& K L = *1'4'.34

re& K

CH3OH

L&b = 329' K/,kmol

7# = 23.1 K

7b = 64.4 C

339.K

7 = *16.3 C

26.' K

L = *2'''1.''

7/24/2019 basis mol

92/380

HCl

L&b = 16161 K/,kmol

7# = 23.1 K

7b = 0. C

323.6K

7 = 30 C

*16.3K

L = *1634

CH3Cl

L&b = 21436 K/,kmol

7# = 23.1 K

7b = *24.3 C

24'.'K

7 = *16.3 C

26.' K

L = 19'.13

7/24/2019 basis mol

93/380

Ne,a

7/24/2019 basis mol

94/380

HCl 0.00044 1.9'9'4' 0.0403 222.1239

CH3Cl 0.61'61 306.412 10.1024 112.019

H2O 0.03449 6.9966 3.'932 234.919

< kon%ensasi = .H * .H% * L.HL 221639

keb-(-$an air pen%ingin

s-$- air pen%ingin mas-k = 30 C

s-$- air pen%ingin kel-ar = 4 C

Cp air pen%ingin = 4.1'4 K/,Kg

< serap =

m air pen%ingin = < serap

3314.'Kg

Ne,a

7/24/2019 basis mol

95/380

-ngsi : memisa$kan me(il klori%a %ari imp-ri(iesn!a.

kon%isi operasi = 8 = 1 a(m

7 = (rial boiling poin( ee%

kon'ena* + )o

n'ena* + )o

@9017294348308K/,/am

7 = 2. C

enta)p* '*t*)at

C 7 = 30.163'322

K 303.313'322

N H komponen Kg,/am

329' '693.' CH3OH 9.'002'1

7/24/2019 basis mol

96/380

16161 '03.33'9 HCl 1.9'690'461

21436 226494 CH3Cl 303.030303620

406'3 1'4'4.9 H2O 6.932133262

2294226

K/,/am enta)p* bottom

7 = 100.00200'6393.1200'6

komponen Kg,/am

CH3OH 0.0009'0'1

HCl 2.1223033E*020

CH3Cl 1.4661'0E*010

H2O 629.'13'4

NERACA ENER>#loss komponen inp-( K>,/am)

ss

CH3OH *10'.340'496

m 10) HCl *.'11164

CH3Cl *42431.963'4

H2O *40.'1226191

< reboiling 306'6.'1022

< kon%ensasi

< loss

- 10 C m (able D*2 2'1010.3169306

7/24/2019 basis mol

97/380

komponen ? B C

CH3OH 21.1 9.0E*02 2.E*0 *2.'E*0'

HCl 30.69 *9.20E*03 1.2E*0 *3.0E*0

CH3Cl 13.'' 1.01E*01 *3.'E*0 2.9E*0

H2O 32.24 1.2E*03 1.06E*0 *3.60E*0

komponen C4 C2 C3 C1 C8

CH3OH 10'00 *362.23 0.39 0 0

HCl 49300 0 0 0 0

CH3Cl 610 *209. 0.3946 0.0004'' 0

H2O 296390 *200.1 '.12 *0.014116 .39E*006

enta)p* ,e.u/

C 7re = 2 C 7 = 30.163' C

K 2'.1 K 303.3136 K

n kmol) H komponen Kg,/am n kmol)

0.2441'99 4121.2 132.66'3 CH3OH 0.00006 0.00016

Cp %7

7/24/2019 basis mol

98/380

0.040032963 24439.3 12.02923 HCl 0.00113 3.12E*00

10.034' 4964'.6 2290.9 CH3Cl 3.3'161 0.0669'

3.'909'192 1366 419.416 H2O 0.044466 0.00246'

9'32.'6

C 7re = 2 CK 2'.1 K

n kmol) H

2.40164E*00 904'23 0.1926

.02'1E*022 3'00936 2.24E*01'

2.64'E*012 6940236 2.00E*00'

34.'390396' 1''039 33'9.6

33'9.'

o-(p-( K/,/am)

%is(ila( bo((om

132.66'302 0.1926

12.029233609 2.24E*01'

2290.913' 2.00E*00'

419.4191 33'9.6

221639

13433

9'32.'62613 2231992'1010.31693063

Cp %7

7/24/2019 basis mol

99/380

7re = 2 C

2'.1K

H

4121.2 0.0'4

Cp %7

7/24/2019 basis mol

100/380

24439.3 0.00966

4964'.6 33.33196

1366 3.441

36.'9''

7/24/2019 basis mol

101/380

7ipe (angki silin%er (egak %engan %asar %a(ar %an a(asn!a b

%asar pemili$an 5m-mn!a %ig-nakan -n(-k li-i% pa%a (ekanan a(mos

8er$i(-ngan :

MEN>H#%"N> DEN$#%A$ CAM6"RAN:

komponen mol kmol,/am massa Kg,/am) Q Kg,m3) ol-me m

CH3OH 0. 122.0'11 32.40944920 9'3. .00936

H2O 0.001 0.122630'2 2.2014243 0.00222

329.616636' .0096

ensi(as #amp-ran = 9'3.3' Kg,m3

4'.44919'lb,(3

%iren#anakan pen!impanan -n(-k 10 $ari %engan 3 b-a$ (angki mem-%a$kan

se$ingga ol-me masing*masing:

pen!impanan = 10 $ari

/-mla$ (angki = 6 b-a$

keb-(-$an me(anol = 329.61664 Kg,/am selama 1 $ari

42629.4 Kg selama 10 $ari

259449 lb

Bo)ume metano) pa'a tan-k*:

ol-me (angki = 424'.4669 (3

ol-me me(anol %alam 1 (angki = 9096.41112266 (3

as-msi ba$an isi '0 ol-me (angki ak(or keamanan)

se$ingga ol-me (angki = '41.6334949 (3

'41.6334949(3

MENEN%"AN D#MEN$# %AN>#

rasio H, = 3,'

= iame(er Brownel,1

H = 7inggi 7angki

R = 3.1413

H = 11.4'''3 (

3.04'm

= 30.6636'' (

.34622 m

HDvo!me ...4

1 2

=

7/24/2019 basis mol

102/380

%ig-nakan %iame(er 3 ( %an (inggi 16 ( &maka

MENEN%"AN !"MLAH 6LA%E DAN %E&AL $HELL

"Browne and $o!ng% pers &'()%(*++ , -./

( = (ebal s$ell S in

8 = (ekanan in(ernal S psi

% = insi%e %iame(er S in

C = ak(or korosi S in 1,' in)

E = ak(or pengelasan& %ig-nakan %o-ble el%

= s(ress alloable& ba$an kons(r-ksi Carbon

ra%e C& maka = 1260 psi

8 = (ekanan in(ernal S 8si = %ensi(as air pa%a s-$- 30 Cel#i-s =H = (inggi #o-rseS (

Cou,e 4

H = 16 (

(1 = 0.214' in

%ipili$ (ebal s$ell s(an%ar = 0.2' in BronellS

meng$i(-ng pan/ang pla(e%iren#anakan mengg-nakan 10 pla(e -n(-k (iap #o-rse& alloan#e -n(-k er(i#al

/arak samb-ng an(ar pla(e) = ,32 in %an lebar = ' (

L = pan/ang (iap pla(e S (

% =%iame(er %alam (ang

n = /-mla$ pla(e

el% leng($ = n alloable el%e% /oin(

L1 = 10.'''4 in

/a%i = pan/ang pla(e = 10.'''3'3'in

lebar pla(e = ' (

(ebal pla(e = 0.2'

Cou,e 2

H = 16 ( * ' (

(2 = 0.124431

%ipili$ (ebal s$ell s(an%ar = 0.1 in

%iren#anakan akan mengg-nakan s$ell pla(e %engan 6 in ' () butt-weldes cou

C0f

dP

t += ..2.

144-1* = HP

n

engt1weddL

12

.. =

7/24/2019 basis mol

103/380

meng$i(-ng pan/ang pla(e

%iren#anakan mengg-nakan 10 pla(e -n(-k (iap #o-rse& alloan#e -n(-k er(i#al




n = /-mla$ pla(e


L1 = 10.'92' in

/a%i = pan/ang pla(e = 10.'929644in

lebar pla(e = ' (

(ebal pla(e = 0.1

MENEN%"AN %O6 AN>LE "N%" CON#CAL ROOF

bila %ig-nakan 10 pla(e (iap angle& maka pan/ang (iap angle :

L = 10.093 (

"MENEN%"AN %E&AL DAN %#N>># HEAD %AN>#

"Browne and $o!ng% Pers')'(.-% (*++ , ((2/

(ekanan pen!impanan = 1 a(m = 14.9 psi

%an %iambil ak(or keamanan 10 maka:

8 = 16.19 8si #os 30 = 0.'66

($ = 0.36001 in

7op angle -n(-k (angki #oni#al %engan %iame(er an(ara 3 ( $ingga 60 ( a%ala$

n

engt1weddL

12

.. =

-6.0.*o.2.

P0fDPt1

=

7/24/2019 basis mol

104/380

-%-( a%ala$ s-%-( #one roo (er$a%ap garis $oriTon(al.

"Browne and $o!ng% Pers'-')% (*++ , )-/

= %iame(er (angki s(an

($ = #one s$ell ($i#knessS i

0.2230004

= 12.'' %era/a(

Men-h*tun- t*n--* hea' (h

$ = 3.02064 ( 1.1'4'321 m

MENEN%"AN D#AME%ER 6#6A 6EN>#$#AN DAN 6EN>EL"ARAN

= I-i% Io ra(e S (3 ,sQ = I-i% %ensi(! S lb,(3

i = %iame(er op(im-m S in#$

%iren#anakan ak(- pengisian selama ' /am.

7/24/2019 basis mol

105/380

erben(-k ker-#-(

$erik

ONVER$#

1Kg,m3 = 0.06243lbm,(3 3,/am) 1 Kg 2.2046 lb

1 $ari 24 /am

1 ( 12 in#$

0.304'm

roses pengisian %an pengosongan)

77:41-43

7/24/2019 basis mol

106/380

l = 2940 bbl = 133.' (3

43.033m3

e% & E = '

(eel ?*2'3

.6 Kg,m3

62.1'43 lb,(3

al 34'

el%e% /oin(

i + (ebal s$ellSin

ses.

7/24/2019 basis mol

107/380

el%e% /oin(

i + (ebal s$ellSin

21,2 21,

2 ,

16

7/24/2019 basis mol

108/380

arS (

n

%(**( , &)./

7/24/2019 basis mol

109/380

7ipe (angki silin%er (egak %engan %asar %a(ar %an a(asn!a b

%asar pemili$an 5m-mn!a %ig-nakan -n(-k li-i% pa%a (ekanan a(mos

8er$i(-ngan :


komponen mol kmol,/am massa Kg,/am) Q Kg,m3) ol-me m

HCl 31 140.''441 136.9'6'1139'1 113 4.30993

H2O 6 313.'144 64.16'103244 .699'

109'.6621902 .'333

ensi(as #amp-ran = 10'0.366 Kg,m3

69.44163lb,(3

%iren#anakan pen!impanan -n(-k 9 $ari %engan b-a$ (angki mem-%a$kan pr



/-mla$ (angki = 9 b-a$

keb-(-$an HCl = 109'.66 Kg,/am selama 1 $ari

1'12040.91 Kg selama 9 $ari

3771928 lb


ol-me (angki = 229.1'3 (3

ol-me HCl %alam 1 (angkki = '461.02'32'3'2(3


se$ingga ol-me (angki = 1013.2334069 (3

1013.2334069(3


rasio H, = 3,'

= iame(er Brownel,1

H = 7inggi 7angki

R = 3.1413

H = 12.20466 (

3.91'03m

= 32.496 (

.1496m

HDvo!me ...4

1 2

=

7/24/2019 basis mol

110/380









=s(ress alloable& ba$an kons(r-ksi Lo all

ra%e B& maka = 1'90 psi

8 = (ekanan in(ernal S 8si = %ensi(as air pa%a s-$- 30 Cel#i-s =H = (inggi #o-rseS (

Cou,e 4

H = 16 (

(1 = 0.21031 in


meng$i(-ng pan/ang pla(e%iren#anakan mengg-nakan 10 pla(e -n(-k (iap #o-rse& alloan#e -n(-k er(i#al




n = /-mla$ pla(e


L1 = 10.'''4 in

/a%i = pan/ang pla(e = 10.'''3'3'in

lebar pla(e = ' (

(ebal pla(e = 0.2'

Cou,e 2

H = 16 ( * ' (

(2 = 0.164'13


%iren#anakan akan mengg-nakan s$ell pla(e %engan 6 in ' () butt-weldes cou

C0f

dP

t += ..2.

144-1* = HP

n

engt1weddL

12

.. =

7/24/2019 basis mol

111/380


%iren#anakan mengg-nakan 10 pla(e -n(-k (iap #o-rse& alloan#e -n(-k er(i#al




n = /-mla$ pla(e


L1 = 10.'92' in


lebar pla(e = ' (

(ebal pla(e = 0.1



L = 10.093 (





8 = 16.19 8si #os 30 = 0.'66

($ = 0.2461'19 in

7op angle -n(-k (angki #oni#al %engan %iame(er an(ara 3 ( $ingga 60 ( a%ala$

n

engt1weddL

12

.. =

-6.0.*o.2.

P0fDPt1

=

7/24/2019 basis mol

112/380





0.3306313

= 1.26' %era/a(


$ = .9'6049 ( 1.963'91133 m


= I-i% Io ra(e S (3 ,sQ = I-i% %ensi(! S lb,(3



7/24/2019 basis mol

113/380

erben(-k ker-#-(

$erik

ONVER$#

1Kg,m3 = 0.06243lbm,(3 3,/am) 1 Kg 2.2046 lb

1 $ari 24 /am

1 ( 12 in#$

0.304'm

oses pengisian %an pengosongan)

77:41-43

7/24/2019 basis mol

114/380

l = 3'0 bbl = 133.' (3

43.033m3

e% & E = '

! (eel ?*22

.6 Kg,m3

62.1'43 lb,(3

al 34'

el%e% /oin(

i + (ebal s$ellSin

ses.

7/24/2019 basis mol

115/380

el%e% /oin(

i + (ebal s$ellSin

21,2 21,

2 ,

16

7/24/2019 basis mol

116/380

arS (

n

%(**( , &)./

7/24/2019 basis mol

117/380

pompa 1

D-ngsi : Mengalirkan me(anol %ari (angki me(anol

7-/-an 8eran#angan :

1. Menen(-kan (ipe pompa

2. menen(-kan %imensi pipa

a. Meng$i(-ng kapasi(as %ebi() pemompaan

b. Meng$i(-ng %iame(er op(imal pipa

#. Menen(-kan pemili$an /enis pipa

3. Meng$i(-ng ke$ilangan energi akiba( gesekan

a. Meng$i(-ng ke#epa(an linier I-i%

b. Meng$i(-ng bilangan e!nol%

#. meng$i(-ng pan/ang ek-ialen pipa

%. Meng$i(-ng risi %alam pemipaan

4. Meng$i(-ng (enaga pompa

a. Meng$i(-ng pres-re $ea%

b. Meng$i(-ng po(ensial $ea%

#. Meng$i(-ng elo#i(! $ea%

%. Meng$i(-ng poer pompa

Langka$ 8eran#angan :


alam peran#angan ini %ipili$ pompa #en(ri-gal %engan per(imbanga

a. kons(r-ksi se%er$ana

b. Ke#epa(an p-(aran s(abil

#. Dl-i%a %ialirkan pa%a (ekanan !ang -niorm

%. 7i%ak memel-kan areal !ang l-as

e. Bia!a peraa(ann!a paling m-ra$ %iban%ingkan (ipe pompa lain.

4 Menentukan kapa*ta pemompaan (6e,an

7/24/2019 basis mol

118/380

Komponen Q kg,m3) Q . @ M kg,/am)

CH3OH 0.43923 9'3. 9'3.4094234 32.409446

H2O 0.00062499 0.664691 2.201424

>-mla$ 9'4.01'93'06' 329.61664

La/- alir ee%

7/24/2019 basis mol

119/380

0.0009119lb,(.s

U #amp = 0.000344 lb,(.s Kern, fg 14, 1965 : 823

46.434

(Peters,198,

5n(-k komersial s(eel :

46.434

1.3 in 0.040661' m

e = 0.000046 m ($e"n%o&l's 'g)2)1-3 &)88#

e, = 0.0003'

*"nn'ng *r'ct'on *"ctor (* # + 0.03 ($e"n%o&l's '

1 Men-h*tun- tena-a pompa

")enentu%"n &ressure !e"d

a(a :

g = 32.2

g# = 32.194

1 a(m 2116.1

1.1 a(m 2329.91

211.61

4.320196322(.lb,lbm

b) enentu%"n &otens'"l !e"d

%iren#anakan :

1 m 3.2' (

3 m .'4 (

V = 2 m 6.6 (

Potens'"l e"d + 6.63012 (.lb,lbm

c) enentu%"n .eloc't/ !e"d

;e

=

;e

W 2100 berar(i aliran !ang mas-k men-/- (angki pro%-k a%ala$ alira

;e

=

in =

5n(-k e, s ;e

)& maka :

Kons(an(a ke#epa(an grai(asi (,s2

Dak(or konersi& lb (,lbs2

81 =8 #airan %lm (angki

82= 8 mas-k aporiTer

V1 =

V2 =

vD

N

=%&

cg

g5eadpotensiaH =

2

=

P

7/24/2019 basis mol

120/380

Karena ke#epa(an linear #airan (i(ik 1 %an (i(ik 2 rela(i sama& maka :

1 = 2

.eloc't/ e"d + 0 (.lb,lbm

d) r'ct'on e"d (0#


&46.4

1.3 in 0.040661' m

e = 0.000046 m ($e"n%o&l's 'g)2)1-3 &)88#e, = 0.0003'


Menen(-kan 8an/ang ek-ialen :

Komponen L, >-mla$ 8an/ang Le)

8ipa l-r-s 1 12

3 2 11.26

a(e ale& -ll! open 13 1 2.021'1

C$e#k ale& -ll! open 13 1 21.9264$arp e%ge en(ran#e 2' 1 4.06236

k = 0&

$arp e%ge ei( k=1&0) ' 1 .334346

pipa l-r-s er(ikal 1 '.

7o(al 8an/ang ekialen Le) 1'2.424'4'

Ke$ilangan energi karena riksi

($e"n%o&l's s)2)1-6 &)89#

14.69369' (.lb,lbm

e. Menen(-kan 8oer Hea% *A)

*A) = 2.'2'40'(.lb,lbm

Kapasi(as

7/24/2019 basis mol

121/380

iskosi(as kinema(ik = 9.14E*006 (2,s = 0.662'42

ari Dig.14*36 pe(ers p.20& -n(-k kapasi(as 24.2 gallon,mn( %iperole$

20

B$p = Bro%e orse&ower + 0.61322H8

ari Yg 14*3' 8e(ers p.21& -n(-k B$p = 1.3 %iperole$

eZsiensi mo(or = '1

8oer mo(or = 0.96619

ipakai poer mo(or = 4

Reume :

Ko%e : 8*01

D-ngsi : Mengalirkan me(anol %ari (angki me(anol

7ipe : #en(ri-gal

>-mla$ : 1

Kapasi(as : 24.243613gallon,meni(

7enaga 8ompa : 0.61326 H8

Ba$an Kon(r-ksi : oerc'"l 0teel

8ipa : 2 in

O = 2.3' in

= 1.3 in

#$ = '0

X pompa=

nominal

=

motor

B1pPowermotor

=

=550

-* fQWfB1p

7/24/2019 basis mol

122/380

1 kg = 2.2046 lb

1 gr = 0.001 kg

3.31469

0.0000011 /am = 3600 %(k

1 #-( = 9.4'01 gallon

Ba$an bak- :

Me(anol

Kem-rnian .0

0.10

:

(&eters, &)521#

*u-a)

1 m3 = in2

1 #m3

= m3

H2O

7/24/2019 basis mol

123/380

100

#-(,%(k

gallon,mn(

0.194

0.16039 (

0.0204'4'

(,%(k

(2

7/24/2019 basis mol

124/380

"l 496#

)2)1-3 &)88#

7-rb-len

(,s2

lb (,lbs2

lb,(2

lb,(2

7/24/2019 basis mol

125/380

0.16039 (

)2)1-3 &)88#

()

gallon,mn(

f+

7/24/2019 basis mol

126/380

Cs

eisiensi X)

H8

7/24/2019 basis mol

127/380

1 meni( = 60 se#on%

0.00644

1 m = 3.2' (

1 a(m = 2116.11 in = 0.0'3 (

1 Kg,m.s = 0.6919lb,(.s

1 in2= (2

lb,(2

7/24/2019 basis mol

128/380

7/24/2019 basis mol

129/380

7/24/2019 basis mol

130/380

7/24/2019 basis mol

131/380

7/24/2019 basis mol

132/380

pompa 2

D-ngsi : Mengalirkan HCl %ari (angki HCl


























7/24/2019 basis mol

133/380

Komponen Q Q . @ M kg,/am)

HCl 0.49624969 113 6'.1634'144 136.9'6'11

H2O 0.2392321 21.133''01 64.16'1

>-mla$ 10'.29040246 109'.662

La/- alir ee%

7/24/2019 basis mol

134/380

7/24/2019 basis mol

135/380


1 = 2


d) r'ct'on e"d (0#


6120'.321

2.323 in 0.0'9'32319 m

e = 0.000046 m ($e"n%o&l's 'g)2)1-3 &)88#e, = 0.0009'3




8ipa l-r-s 1 12

3 2 13.4663

a(e ale& -ll! open 13 1 2.0619

C$e#k ale& -ll! open 13 1 26.0221$arp e%ge en(ran#e 2' 1 .3'62

k = 0&

$arp e%ge ei( k=1&0) ' 1 11.1'222


7o(al 8an/ang ekialen Le) 12.11336


($e"n%o&l's s)2)1-6 &)89#

32.93130'9 (.lb,lbm


*A) = 42.406129'3(.lb,lbm

Kapasi(as

7/24/2019 basis mol

136/380

iskosi(as kinema(ik = 1.14E*00 (2,s = 1.0636149

ari Dig.14*36 pe(ers p.20& -n(-k kapasi(as 4.4 gallon,mn( %iperole$

39

B$p = Bro%e orse&ower + 1.140219H8

ari Yg 14*3' 8e(ers p.21& -n(-k B$p = 1. %iperole$

eZsiensi mo(or = '3

8oer mo(or = 1.'241699

ipakai poer mo(or = 4

Reume :

Ko%e : 8*02

D-ngsi : Mengalirkan HCl %ari (angki HCl

7ipe : #en(ri-gal

>-mla$ : 1

Kapasi(as : 49.1'22gallon,meni(

7enaga 8ompa : 1.1402 H8


8ipa : 2 1,2 in

O = 2.'' in

= 2.323 in

#$ = '0

X pompa=

nominal

=

motor

B1pPowermotor

=

=550

-* fQWfB1p

7/24/2019 basis mol

137/380

1 kg = 2.2046 lb

1 gr = 0.001 kg

3.31469

0.0000011 /am = 3600 %(k

1 #-( = 9.4'01 gallon

Ba$an bak- :

HCl

Kem-rnian 31.00

6.00

:

(&eters, &)521#

*u-a)

1 m3 = in2

1 #m3

= m3

H2O

7/24/2019 basis mol

138/380

100

#-(,%(k

gallon,mn(

0.2304 (

0.12'0 (

0.023931

(,%(k

(2

7/24/2019 basis mol

139/380

"l 496#

)2)1-3 &)88#

7-rb-len

(,s2

lb (,lbs2

lb,(2

lb,(2

7/24/2019 basis mol

140/380

0.12'0 (

)2)1-3 &)88#

()

gallon,mn(

f+

7/24/2019 basis mol

141/380

Cs

isiensi X)

H8

7/24/2019 basis mol

142/380

1 meni( = 60 se#on%

0.00644

1 m = 3.2' (

1 a(m = 2116.11 in = 0.0'3 (

1 Kg,m.s = 0.6919lb,(.s

1 in2= (2

lb,(2

7/24/2019 basis mol

143/380

7/24/2019 basis mol

144/380

7/24/2019 basis mol

145/380

7/24/2019 basis mol

146/380

7/24/2019 basis mol

147/380

'o!&! *01-

#)g M&)g#'k') m&(')ol "'! '! m&)'" #'

:& Do!be pipe 0xc1anger:##')

*;-

Ko)" O&!' l#"' P')' : *oC- : *K- : *o-:'o!&! ?! 1667626.386 K/'m

1580604.805 B(#/'m;m') m'#k 'o!&! 3927.62 kg/'m

8658.823644 lb/'mK&b#(#

7/24/2019 basis mol

148/380

:enent!;an Temprat!r ;aori;

572 "pers' .'

7/24/2019 basis mol

149/380

N( 688= D

7/24/2019 basis mol

150/380

%& 46.15014496H 16 -Fig&'" ern! hal "#$.

0.105

d. Menghitung ho

7/24/2019 basis mol

151/380

7/24/2019 basis mol

152/380

7/24/2019 basis mol

153/380

0.006809379

774.7118273

k. Menentukan Pressure Drop ditube

"'! Ag.29

7/24/2019 basis mol

154/380

2.94825E005 P

9APORI:ING

Bl')g') !&)ol" *%&- 1847.980136"'! Ag 29 k&!) ""''(A 0.0016 A(2/)2D 0.79 3ern% tabe ) 1a 2

=umlah 8rosses dan ba!!le

L> 9.523714233 A(

#ml'< !o&N , 1 N + L>/B 3.847965347

#ml'< b'AAl&

N 2.847965347= 0.00498 A(

2.41633E007 P

2.97241E005 P

menentukan ?Ps

PP

menentukan P dishell (Ps)

menentukan ?Ps

PP

Menentukan ?Ps total

PP (o('l

3

10

2

-=&.3.*522.10

1-.=3.*NA.G3OP3

+=

3

10

2

-=&.3.*522.10

1-.=3.*NA.G3OP3

+=

7/24/2019 basis mol

155/380

1 kg

1 g!

1 'm 1 #A(

a'2*/

1 m

3

ficient 1 m3

7/24/2019 basis mol

156/380

a' *.4*)/

A(A(

28.2690092 )2

m'll 100

7/24/2019 basis mol

157/380

2*

21.2031188

! %ig&'"

5 K&!)

lb*n+&%+'

7/24/2019 basis mol

158/380

3ern%fig () 1a 2

7/24/2019 basis mol

159/380

ern.

! %ig&'"

5 K&!)

7/24/2019 basis mol

160/380

3ern%fig () 1a 2

7/24/2019 basis mol

161/380

7/24/2019 basis mol

162/380

=2

7/24/2019 basis mol

163/380

2.2046 lb 1 m&)( 60 &o)" 1

0.001 kg 0.006944

35.31467 1 m 3.28 A(0.000001 1 '(m 2116.1

3600 "(k 1 ) 0.083 A(7.480519 g'llo) 1 kk'l 3.968321 B(#

1 KF 0.9478171 B(#

1 )2 A(2

)

2

m3 lbA/A(2

7/24/2019 basis mol

164/380

k&!) .103

(o 200 A(2 o! l&.

7/24/2019 basis mol

165/380

7/24/2019 basis mol

166/380

7/24/2019 basis mol

167/380

7/24/2019 basis mol

168/380

7/24/2019 basis mol

169/380

7/24/2019 basis mol

170/380

7/24/2019 basis mol

171/380

2.42 lb/A(.'m

7/24/2019 basis mol

172/380

7/24/2019 basis mol

173/380

7/24/2019 basis mol

174/380

7/24/2019 basis mol

175/380

7/24/2019 basis mol

176/380

7/24/2019 basis mol

177/380

7/24/2019 basis mol

178/380

7/24/2019 basis mol

179/380

'o!&! *02-

#)g M&)g#'k') HCl "'! '! m&)'" #'

:& Do!be pipe 0xc1anger:##')

*;-

Ko)" O&!' l#"' P')' : *oC- : *K- : *o-:'o!&! ?! 6468516.383 K/'m

6130970.44 B(#/'m;m') m'#k 'o!&! 10785.96 kg/'m

23778.71997 lb/'mK&b#(#

7/24/2019 basis mol

180/380

:enent!;an Temprat!r ;aori;

572 "pers' .'

7/24/2019 basis mol

181/380

N( 1024= D

7/24/2019 basis mol

182/380

%& 31.45671719H 11 -Fig&'" ern! hal "#$.

0.16 3ern%fig () 1a 2& >ol'(l(' (' komo)&)

')' #)(#k &)g#') 1 mol #m') H> HH> H

L

+=

1mx

i

iDi

=

i

i9ixq1

( )( )

( )( )

+

+

=+

5.0

m) 1

U117.211

4.541

11

0XPN

NN

7/24/2019 basis mol

293/380

Komo)&) A *kmol/'m- + PCH3OH 0.245 0.0017 9.5469HCl 0.049 0.0003 12301.0388CH3Cl 105.035 0.7292 1036.0150H2O 38.708 0.2687 1.1609:o('l 144.037 1.000

Komo)&) k kU+ 'lA'CH3OH 0.0126 0.000021 8.2234365137HCl 16.1856 0.005507 10595.7797387032CH3Cl 1.3632 0.994062 892.3950727796H2O 0.0015 0.000411 1

:o('l 1.000

Penen+uan Te*pera+ur de6+ila+

:&m&!'(#! "&(l'( "'! "&)g') (!'l "& o)( (&m&!'(#!. :&k')') o&!'"')gg' ko)(') '"' ko)" 1 '(m:&k')') 1 '(m 101.325:&m&!'(#! :!'l 30.1635975201 C 303.3136Komo)&) Akmol/'m PCH3OH 0.2449918797 0.0022 165.1879

HCl 0.0490032763 0.0004 38930.6785CH3Cl 105.035459983 0.9619 4988.1414H2O 3.870781752 0.0354 31.9521:o('l 109.200 1.000

Komo)&) k +/k 'lA'CH3OH 0.2174 0.0103 5.16985HCl 51.2246 0.0000 1218.40596CH3Cl 6.5633 0.1466 156.11290H2O 0.0420 0.8431 1.00000

:o('l 1.000

Penen+uan Te*pera+ur 4o++o* De6+ila6i

:&m&!'(#! bo((om "&(l' m&!#'k') (&m&!'(#! b#bbl& o)( "'! #)(#km&)&)(#k') (&m&!'(#! o&!' !&bol&! *!&bol&! '!'l-:&k')') 1 '(m 101.325:&m&!'(#! :!'l 100.0020555086 C 373.1520555086Komo)&) Akmol/'m + PCH3OH 2.450163813569E005 7.03321059416E007 2658.0751643188

HCl 5.902890849928E022 0 123619.564695223CH3Cl 2.964984906363E012 0 23332.2912520951H2O 34 8370357679 0 9999992967 759 9987597097

7/24/2019 basis mol

294/380

:o('l 34.8371 1.000

Komo)&) k kU+ 'lA'CH3OH 3.4974673215 2.45984242181E006 3.4974730292HCl 162.6573219674 0 162.6575874182CH3Cl 30.7003832264 0 30.7004333283H2O 0.999998368 0.9999976647 1:o('l 1.000

Menghi+ung Bu*lah Pla+e Mini*u* Pada To+al Re%lu

;)(#k m&)g!

L=

Log

WLog

= LB

HB

HD X

X

X

Nm

WLDLAverageL x ... =

7/24/2019 basis mol

295/380

%m) , 1 0.9043%m) 0.0957

Menen+uan Bu*lah Pla+e Teori+i6 (N +eori+i6)

Nm) 8% m) 0.0957

=&)g') &!'m'')

% T + %m)Y *% %m)-/*%,1-W *N Nm)-/*N,1-

N *Nm) , W-/ *1 W-

T % Y W1.05 0.1005131758 0.00434919 0.80250765661.1 0.1052995175 0.00866071 0.7286357419

1.15 0.1100858592 0.01293506 0.6931379242

1.2 0.1148722009 0.01717270 0.67201555791.25 0.1196585426 0.02137411 0.65766706741.3 0.1244448843 0.02553976 0.6469563344

1.35 0.129231226 0.02967009 0.63837652911.4 0.1340175677 0.03376556 0.6311273522

1.45 0.1388039094 0.03782660 0.6247522951.5 0.1435902511 0.04185364 0.618976578

='mbl T 1.25%&Al#k 0.1244448843

F#ml'< Pl'(& :&o!( 24.94 25

Menen+uan Bu*lah Pla+e a+ual

M&)gg#)'k') OJCo))&llJ o!!&l'(o) Eo 51325 log *'.Z'- *o#lo) >ol.6g '"' #

7/24/2019 basis mol

296/380

CH3OH 2.2'' 2.6E*01 .13E+02

HCl 3.342 0.292 324.6CH3Cl 1.'19 2.E*01 416.2

Aa(er 5.459 3.05@01 647.13

: (o 303.3136 K komo)&) (o kmol/'m +" CH3OH 0.245 0.002 3.95E,00HCl 0.049 0.000 7.6784121084CH3Cl 105.035 0.962 3.3605984571H2O 3.871 0.035 9.9792504193

#ml'< 109.200 1.000

: bo((om 373.1520555086 K komo)&) bo((om kmol/'m +b CH3OH 2.450163813569E005 7.03321059416E007 0.03HCl 5.902890849928E022 0 0.75CH3Cl 2.964984906363E012 0 0.1H2O 34.8370357679 0.9999992967 0.2838

#ml'< 34.8370602695 1

Bu*lah Pla+e a+ual

'>g 1.0105648667 1.0105648667

Eo 50.8517 [

N '(#'l N (&o!( 1 !&bol&! EAA

47.0781057744 ('g& \ 47

Menen+uan Loa6i ;*pan Ma6u

P&!

7/24/2019 basis mol

297/380

Log N!/N 3.112010322N!/N 22.4661632551N'( 1 N! , NN 2.0062123178

F'" #m') m'#k '"' l'(& "'! 12 "''! m&)'!'.

-M2T2: M2D:

1. iame(er 8-n#ak Menara

= eI-k a(io

, = ? 1.6'00'433 kmol,/am

= Lo + 122.9'6 kmol,/am

B&!'( mol&k#l ;' =&(l'(

Komo)&) X Bm X. BmCH3OH 0.0022 32.0420 0.0718865639

HCl 0.0004 36.4610 0.0163617636CH3Cl 0.9619 50.4880 48.5624432199H2O 0.0354 18.0150 0.6385712636

:o('l 1.0000 4.2'262'111

49.2892628111 kg/kmolP 1.2 '(m 121.59 k': 294.000000 K M'k' "&)(' #' "&(l'(

2.0432411242

Menen+uan Den6i+a6

7/24/2019 basis mol

298/380

;)(#k m&)g

7/24/2019 basis mol

299/380

#m :!' ')g ')g "g#)'k') 18='! g. 16.6 P&(&! ] :mm&!ol#m& '!')

0.0106884

'& Dia*e+er olo* 4a@ah

M&)&)(#k') =&)(' ;' C'm#!') Bo((om=&)(' #' 'm#!') "

7/24/2019 basis mol

300/380

B&!'( mol&k#l ;' bo((om

Komo)&) X Bm X. BmCH3OH 0.0000025 32.0420 7.881827088E005HCl 0.0000000 36.4610 0CH3Cl 0.0000000 50.4880 0H2O 1.0000 18.0150 18.0149579299:o('l 1.0000 137.0060 18.0150367482

18.0150367482 kg/kmolP 1 '(m 101.325 k'

: 100.00 373.15

M'k' "&)(' #' bo((om

0.5883881842

Menen+uan Den6i+a6

7/24/2019 basis mol

301/380

="''( "&)(' lI#" 'm#!') 99.49999

=&)(' lI#" bo((om

1792.4932141449

#m :!' ')g ')g "g#)'k') 18='! g. 16.6 P&(&! ] :mm&!ol#m& #' m'km#m

#m 418.083 kmol/'m + 31.131 kg/kmol 1.3774690356

L'# l! >ol#m& '!') 305.091 kmol/'m + 28.8696kg/kmol 0.0000500

='! &!

#'Bm+)+4

"='m&(&!

=

=

v

vL3v6m

-* =

7/24/2019 basis mol

302/380

:o 2.3555085796

Bo((om 0.1485754537

F'" )&( '!&' ')g "&!ol&< &k('! 1.2520420166

;)(#k "'&!'< "o)om&! "'mbl 20[ l#' k&&l#!#

7/24/2019 basis mol

303/380

2.1146373 m

Menghi+ung Pre66uree Drop

Dr7 Pate Pres!re Drop 13.24453574830.76790482497.0062202866m/

2

K.H "'! Ag 16.12 P&(&! ]

7/24/2019 basis mol

304/380

1.2 + 14.7 17.64

15.644264998 0.002760 P'

P P" , P< 17.64 , 0.0026 17.642760 P='m&(&! kolom 1.0836 m 41.633 )llo'bl& (!& D 13750 PFo)( &AA&) E 0.8Co!oo) A'(o! C 0.125 )/10 ('

7/24/2019 basis mol

305/380

21.5190257663)2 2

18.2690257663

BC ! ! 603.625 50.75

47.3477053039)

=&

7/24/2019 basis mol

306/380

7/24/2019 basis mol

307/380

7/24/2019 basis mol

308/380

P'K

P'K

7/24/2019 basis mol

309/380

OC

7/24/2019 basis mol

310/380

N43.969430260231.7276636413

27.941726144

26.077864133624.94292665424.155863220123.559020295823.076380333322.667348376122.3085885292

l'(&

7/24/2019 basis mol

311/380

2.4E*01

3.22E*01

'.10E*02

8.10@02

.+"8.85E033.45E033.23E,003.54E013.60E,00

.+b2.11E08 g&') kol Ag .34 .3

0.00E,00 g&') kol Ag .34 .40.00E,00 g&') kol Ag .34 .52.84E01 g&') kol ('bl& .24 .22.84E01

mN/mR2

('g&

=3''.

7/24/2019 basis mol

312/380

7/24/2019 basis mol

313/380

K

mmHg

ol

7/24/2019 basis mol

314/380

)A(.

7/24/2019 basis mol

315/380

K

Q. @i

.133339'E*00

0

0.430016

4'12

7/24/2019 basis mol

316/380

)

m/

mol

m3/

m3/

7/24/2019 basis mol

317/380

m2m2

mm

mm

kg/

m2

m2

m2

m2

m2

m2

m2

7/24/2019 basis mol

318/380

m

mm

L#b')g

7/24/2019 basis mol

319/380

42.6630515327)

Xo#)g

42.6630515327)

] Xo#)g-

Xo#)g

7/24/2019 basis mol

320/380

)

)

))

7/24/2019 basis mol

321/380

7# = 30 C

7i= 32. 7o=30 C

CA

7#o = 4 C

%ari nera#a massa %an nera#a panas %iperole$ :

ba$an = 3'2.31914'6

panas !g %ib-(-$kan&

7/24/2019 basis mol

322/380

Menghitung density campuran

Fluida panas

Komponen BM Massa Massa

(kmol) (kg)

CH3OH 32.042 0.24 9.

HCl 36.461 0.04 1.'CH3Cl 50.488 10.03 &303.0

18.015 3.'91 6.9

Total !09." 53#".$

P! P/PJ 0.0022152319:! :/:J 0.1601936129T 1

D&

7/24/2019 basis mol

323/380

Total

Mengitung konduktiitas te+mal *ampu+an

7?BLE 2*31 7$ermal Con%-#(ii(! o norgani# an% Organi# Li-i%s A,mK)_

Fluida /anas

Komponen k i i.k

1(m.K) 1(m.K)

CH3OH !.09203 0.00!5 !.59206

HCl ".9$20$ 0.0003 9.%520#

CH3Cl $.5"20$ 0.9#53 $.$520$

3.9#20$ 0.0!30 5.!5206

Total !.00000 $.5020$

Fluida -ingin

Komponen k k i

1(m.K) 1(m.K)

2E+02 1.0E+02 1

Total !

Menentukan 4-

Dari Tabel 8 Kern, Ud 50-125

Ud = !"5

Menghitung Luas Permukaan

2++E50"

Menentukan spesifikasi dan layout tube

-s-nan Triangular

8ass $ell 1

8ass 7-be 2

O-(si%e iame(er = 3/4 in#$ = 0.062

8i(#$ 0.9375 in#$ = 0.09'12BA ;o. 16

nsi%e iame(er = 0.62 in#$ = 0.016666669

Dlo area per (-be = 0.302 0.002092222

Outside sura!e / lin t = 0.163 2'.2692

"nside sura!e / lin t = 0.1623 23.3912

8an/ang = "5 (

H"O

H"O (B)

#tu/ja$.t2.`%

& = '/(Ud)PT* t2

in2 =

(2=

(2=

7/24/2019 basis mol

324/380

Menentukan jumlah tube

+t = &/(,.a-* @rr>502

ari (abel Kern& maka /-mla$ (-be %ib-la(kan men/a%i

;( = #"" (-be

Menentukan diameter shell

ari (abel Kern& /-mla$ (-be %ia(as& %i%apa(kan %iame(er s$ell

s = 3! in#$ ".5#33333333

Koreksi luas permukaan dan Ud

? = ;(.L.a = $033.965

5% =

7/24/2019 basis mol

325/380

7/24/2019 basis mol

326/380

at = +t ? at / n = 0.#6"0

Mengitung ke*epatan massa (8a)

!3%66.369#6!!! l/r.t2

et = .t/ = "6%0.!!353%960#

Mengitung koeisien pe+pindaan panas

H 92 -Fig&'" ern! hal "#$.

0.07 3ern%fig () 1a 2

7/24/2019 basis mol

327/380

N'm' l'( CON=ENDO%Ko"& l'( C01F#ml'< 1 B#'am.(2.0D

B(-,>am.(2.

DDlo area :

aT (2

DMass elo#i(! :

T Kg,/am (2

lb,/am (2

De!nol% ;-mber :

aoLNA t UU=

TmA

Q>D

=U

n

taNa TT

U144

JU=

ta

WT

J=

T

t

DU%& =

7/24/2019 basis mol

352/380

/e+itungan sell side E

ell side Cold luid (Cai+an medium o+ganik)

?s-msi $o = 300

Kern& ')

7 = 2'.6666669

P7 =

ari Yg 1&11 kern& maka %ig-nakan $o = 129

D Fengitung lean O;erall ei!ient

Kern&106)

5# = 119.0'66626

d = 0.0117

d $ini$u$ = 0.001

/+essu+e -+op tue

Kern&14')

ari Yg 2& kern %i%apa( :

Dak(or rik = 0.001'

Bt = 3.2615252895 sia

B(-,>am.(2.0D

D7empera(-r %in%ing (-be

0D

0D

B(-,>am.(2.0D

B(-,/am (20D

Dir( Da#(or

Aa$ t20%/#tu

Aa$ t20%/#tu

(2,in2

( )cccW tT1o1io

1otT

++=

-*

-.*

1o1io

1o1io>c

+

=

DC

DCD>>>>B

U=

s

t

De

LnfPt

10

2

10U22.5=

7/24/2019 basis mol

353/380

pesiYk ol-me s(ea = 0.64

g s(eam = 0.024446142

Kern&14')

P8r = 1.49262 8sia

Kern&14')

BT = 4.7341502895 sia

8ress-re rop s(an%a = 10 8sia

(3,lb

gs

n6

2

4P!

2

=

rT PPPT +=

7/24/2019 basis mol

354/380

= 302

= 302

= 20

= 20

0D0D0D0D

7/24/2019 basis mol

355/380

7/24/2019 basis mol

356/380

kern& 91).0D

7/24/2019 basis mol

357/380

7/24/2019 basis mol

358/380

7/24/2019 basis mol

359/380

pompa 4

D-ngsi : Mengalirkan me(il klori%a ke (angki pro%-k


























7/24/2019 basis mol

360/380

Komponen Q Q . M kg,/am)

CH3OH 0.0014'463 9'3. 1.1432'111 9.'002'1

HCl 0.0003314 113 0.36021019 1.9'690'46

CH3Cl 0.'23' 1 01.09409940 303.030304

H2O 0.012'6 12.'0'09694' 6.93213326

>-mla$ 1.39242 3'2.319

La/- alir ee%

7/24/2019 basis mol

361/380

0.0003 lb,(.s 0.001009

U air = 0.' Kg,m.s U me(il klori%= 0.1'

0.0009119 lb,(.s 0.000120

U #amp = 0.00012941 lb,(.s Kern, fg 14, 1965 : 823

22362.909

(Peters,198,


22362.909

1.3 in 0.040661' m

e = 0.000046 m ($e"n%o&l's 'g)2)1-3 &)88#

e, = 0.0003'


1 Men-h*tun- tena-a pompa

")enentu%"n &ressure !e"d

a(a :

g = 32.2

g# = 32.194

1 a(m 2116.1

1 a(m 2116.1

0 (.lb,lbm

b) enentu%"n &otens'"l !e"d

%iren#anakan :

1 m 3.2' (

2 m 6.6 (

V = 1 m 3.2' (

Potens'"l e"d + 3.2'2606 (.lb,lbm

;e

=

;e

W 2100 berar(i aliran !ang mas-k men-/- (angki pro%-k a%ala$ alira

;e

=

in =

5n(-k e, s ;e

)& maka :

Kons(an(a ke#epa(an grai(asi (,s2

Dak(or konersi& lb (,lbs2

81=8 #airan %lm (angki

82= 8 mas-k (angki

V1 =

V2 =

vDN

=%&

cg

g5eadpotensiaH =

=

P

7/24/2019 basis mol

362/380

c) enentu%"n .eloc't/ !e"d


1 = 2


d) r'ct'on e"d (0#


223&62.9

1.3 in 0.040661' m

e = 0.000046 m ($e"n%o&l's 'g)2)1-3 &)88#

e, = 0.0003'




8ipa l-r-s 1 12

3 1 .6329a(e ale& -ll! open 13 1 2.021'1

C$e#k ale& -ll! open 13 1 21.9264

$arp e%ge en(ran#e 2' 1 4.06236

k = 0&

$arp e%ge ei( k=1&0) ' 1 .334346


7o(al 8an/ang ekialen Le) 196.9203


($e"n%o&l's s)2)1-6 &)89#

6.32'9''1 (.lb,lbm


;e

=

in =

Elbo 0o

* =

=cg

6ad6eocit7He

2

2

cg

v

D

Lff

24

2

=

adveocit71eeadpotensia1adpress!re1eWf ++=

7/24/2019 basis mol

363/380

*A) = .'163'46(.lb,lbm

Kapasi(as -mla$ : 1

Kapasi(as : 2'.43'393gallon,meni(

7enaga 8ompa : 0.2'1331 H8


8ipa : 2 in

O = 2.3' in

= 1.3 in

#$ = '0

X pompa=

nominal

=

motor

B1pPowermotor

=

=550

-* fQWfB1p

7/24/2019 basis mol

364/380

1 kg = 2.2046 lb

1 gr = 0.001 kg

3.31469

0.0000011 /am = 3600 %(k

1 #-( = 9.4'01 gallon

Ba$an bak- :

Me(anol

Kem-rnian .0

0.10

:

(&eters, &)521#

*u-a)

1 m3 = in2

1 #m3

= m3

H2O

7/24/2019 basis mol

365/380

100

#-(,%(k

gallon,mn(

0.194 (

0.16039 (

0.0204'4'

(,%(k

Kg,m.s

(2

7/24/2019 basis mol

366/380

lb,(.s

Kg,m.s

lb,(.s

"l 496#

)2)1-3 &)94#

7-rb-len

(,s2

lb (,lbs2

lb,(2

lb,(2

7/24/2019 basis mol

367/380

0.16039 (

)2)1-3 &)94#

()

f+

7/24/2019 basis mol

368/380

gallon,mn(

Cs

isiensi X)

H8

7/24/2019 basis mol

369/380

1 meni( = 60 se#on%

0.00644

1 m = 3.2' (

1 a(m = 2116.11 in = 0.0'3 (

1 Kg,m.s = 0.6919lb,(.s

1 in2= (2

lb,(2

7/24/2019 basis mol

370/380

7/24/2019 basis mol

371/380

7/24/2019 basis mol

372/380

7/24/2019 basis mol

373/380

7/24/2019 basis mol

374/380

7ipe (angki silin%er (egak %engan %asar %a(ar %an a(asn!a berbe

%asar pemili$an 5m-mn!a %ig-nakan -n(-k li-i% pa%a (ekanan a(mosp$eri

8er$i(-ngan :


komponen kmol,/am massa Kg,/am) Q Kg,m3) ol-me m3,/am)

CH3OH 0.2441 9.'002'1 9'3. 0.010014

HCl 0.040033 1.9'690'461 113 0.0014'

CH3Cl 10.0346 303.03030362 1 .9662

H2O 3.'909'1' 6.932133262 0.0900'3

10.20024 3'2.31914 .'9926

ensi(as #amp-ran = 1.'01412''6 Kg,m3

9.1934'2206lb,(3

%iren#anakan pen!impanan -n(-k 9 $ari %engan b-a$ (angki mem-%a$kan proses p



/-mla$ (angki = b-a$

keb-(-$an HCl = 3'2.31914 Kg,/am selama 1 $ari

04243.06142 Kg selama 9 $ari

477317128322 lb


ol-me (angki = 34'69.46261193 (3


se$ingga ol-me (angki = 41'40.134091' (3

'36'.11026'144(3


rasio H, = 3,'

= iame(er Brownel,1

H = 7inggi 7angki

R = 3.1413

H = 11.442'64 (

3.4'99'm

HDvo!me ...4

1 2=

7/24/2019 basis mol

375/380

= 30.1430 (

.3009601m









= s(ress alloable& ba$an kons(r-ksi Carbon

ra%e C& maka = 1260 psi

8 = (ekanan in(ernal S 8si

= %ensi(as air pa%a s-$- 30 Cel#i-s =H =(inggi #o-rseS (

Cou,e 4

H = 16 (

(1 = 0.214' in



%iren#anakan mengg-nakan 10 pla(e -n(-k (iap #o-rse& alloan#e -n(-k er(i#al el%e




n = /-mla$ pla(e


L1 = 10.'''4 in

/a%i = pan/ang pla(e = 10.'''3'3' in

lebar pla(e = ' (

(ebal pla(e = 0.2'

Cou,e 2

H = 24 ( * ' (

(2 = 0.1'40129

%iren#anakan akan mengg-nakan s$ell pla(e %engan 6 in ' () butt-weldes courses.

C0f

dPt +=

..2

.

144

-1* =

HP

n

engt1weddL

12

.. =

7/24/2019 basis mol

376/380



%iren#anakan mengg-nakan 10 pla(e -n(-k (iap #o-rse& alloan#e -n(-k er(i#al el%e



% =%iame(er %alam (angn = /-mla$ pla(e


L1 = 10.'92' in


lebar pla(e = ' (

(ebal pla(e = 0.1



L = 10.093 (





8 = 16.19 8si #os 30 = 0.'66

7op angle -n(-k (angki #oni#al %engan %iame(er an(ara 3 ( $ingga 60 ( a%ala$ 21,2

n

engt1wedd

L 12

.. =

-6.0.*o.2

.

P0f

DPt1

=

7/24/2019 basis mol

377/380

($ = 0.36001 in





0.2230004

= 12.'' %era/a(


$ = 3.02064 (


= I-i% Io ra(e S (3 ,s

Q = I-i% %ensi(! S lb,(3



7/24/2019 basis mol

378/380

(-k ker-#-(

ONVER$#

1Kg,m3 = 0.06243lbm,(31 Kg 2.2046 lb

1 $ari 24 /am

1 ( 12 in#$

0.304'm

engisian %an pengosongan)

77:41-43

7/24/2019 basis mol

379/380

l = 2940 bbl = 133.' (3

43.033m3

e% & E = '

(eel ?*2'3

.6 Kg,m3

62.1'43 lb,(3

al 34'

% /oin(

i + (ebal s$ellSin

7/24/2019 basis mol

380/380

% /oin(

i + (ebal s$ellSin

21,2 ,

16

basis mol

Documents