Separation, Purification and Characterization of Organic Liquid and Solid Unknowns by means of Simple Distillation, Extraction and Recrystallization Anna Zurek CHE 231L Section 202 Department of Chemistry, DePaul University, 1110 W. Belden Avenue, Chicago, IL 60614 [email protected] 2/12/2015 Abstract: Simple distillation is used to separate clear, homogenous mixture of two unknown liquids (unknown #6). The mixture is highly viscous and has mildly sweet odor. Once the products are distilled, small sample of each product is heated to determine its boiling point range. The boiling point of the lower boiling liquid (LB) is determined to be 84.3-86.1 (°C) and the boiling 1