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Separation, Purification and Characterization of Organic Liquid and Solid Unknowns by means of Simple Distillation, Extraction and Recrystallization Anna Zurek CHE 231L Section 202 Department of Chemistry, DePaul University, 1110 W. Belden Avenue, Chicago, IL 60614 [email protected] 2/12/2015 Abstract: Simple distillation is used to separate clear, homogenous mixture of two unknown liquids (unknown #6). The mixture is highly viscous and has mildly sweet odor. Once the products are distilled, small sample of each product is heated to determine its boiling point range. The boiling point of the lower boiling liquid (LB) is determined to be 84.3-86.1 (°C) and the boiling 1
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Separation, Purification and Characterization of Organic Liquid and Solid Unknowns by meansof Simple istillation, !"traction and #ecrystallization $nna %urekC&! '()L Section '*'epartment of Chemistry, ePaul Uni+ersity, )))* ,- .elden $+enue, Chicago, /L 0*0)1a-k-zurek2gmail-com'3)'3'*)4Abstract:Simple distillation is used to separate clear, homogenous mi"ture of two unknown liquids 5unknown 607- 8he mi"ture is highly +iscous and has mildly sweet odor- Once the products are distilled, small sample of each product is heated to determine its boiling point range- 8he boiling point of the lower boiling liquid 5L.7 is determined to be 91-(:90-) 5C7 and the boiling point of the higher boiling compound 5&.7 ;'-(:;1-* 5C7- 8he density of the lower boiling liquid is found to be *-