Analytical Reference Materials Cat. # 31639 Lot #'s A056067 & A055797 Alternate BP/CN Distribution Marker Stock Solution 110 Benner Circle Bellefonte, PA 16823-8812 (814) 353-1300 FOR LABORATORY USE ONLY. READ MSDS PRIOR TO USE. MANUFACTURED UNDER RESTEK'S ISO 9001 REGISTERED QUALITY SYSTEM
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Analytical Reference Materials
Cat. # 31639Lot #'s A056067 & A055797
Alternate BP/CN Distribution Marker Stock Solution
110 Benner Circle Bellefonte, PA 16823-8812(814) 353-1300
FOR LABORATORY USE ONLY. READ MSDS PRIOR TO USE.
MANUFACTURED UNDER RESTEK'S ISO 9001 REGISTERED QUALITY SYSTEM
31639 A055797
Alternate BP/CN Distribution Marker Stock Solution
110 Benner CircleBellefonte, PA 16823-8812
Tel: (800)356-1688Fax: (814)353-1309
Catalog No. :
Description :
Expiration Date :
Lot No.:
Storage: Room Temperature
FOR LABORATORY USE ONLY-READ MSDS PRIOR TO USE.
November 2014
Certificate of Analysis
CAS #Percent Purity
2CompoundElution Order Concentration
(weight/volume)
Percent Uncertainty
43
n-Hexane (C6) 110-54-3 +/-0.08 %99% 1 200.000 ug/mln-Octane (C8) 111-65-9 +/-0.08 %99% 2 200.000 ug/ml
n-Decane (C10) 124-18-5 +/-0.08 %99% 3 200.000 ug/mln-Dodecane (C12) 112-40-3 +/-0.08 %99% 4 200.000 ug/ml
n-Hexadecane (C16) 544-76-3 +/-0.08 %98% 5 200.900 ug/mln-Heneicosane (C21) 629-94-7 +/-0.08 %99% 6 200.000 ug/mln-Octacosane (C28) 630-02-4 +/-0.08 %98% 7 199.920 ug/ml
n-Pentatriacontane (C35) 630-07-9 +/-0.08 %96% 8 200.640 ug/mln-Hexatriacontane (C36) 630-06-8 +/-0.08 %99% 9 200.000 ug/ml
PentaneSolvent:
Column: 30m x .25mm x .5um
hydrogen @ 40cm/sec.35°C (hold 2 min.) to 330°C
Rtx-5 (cat.#10238)
@ 10°C/min (hold 10 min.)250°C330°CFID
99%109-66-0
Carrier Gas:Temp. Program:
Inj. Temp:
Det. Type:Det. Temp:
Balance 1128342313
Lot #:A055797
Catalog #:Alternate BP/CN Distribution Marker Stock SolutionDescription:
Target:
PentaneSolvent: C19E42Solvent Lot: Final Volume:
Made by: Rebecca Lauver Date:Tested by: Diane Shaffer Date: 10/12/2007 1:42:05PM
By: Sara Eyster Date: 10/30/2007 10:51:49AMPackaged by: Staci Bodle / Date: 10/12/2007 11:35:17AMNo. Units: 67
Balance Used:ARMBALPC1 XP205 Serial #: 1128342313
Pass
100.00 ml
31639 200 ug/ml
10/12/2007 9:48:43AM
Pkg Size: 1 mL
Chemical Standard Batch Sheet
Compound CASStorageLocation Lot # Purity
Target Weight
ActualWeight
Target Conc(ug/ml)
Calc Conc(ug/ml)
20.9020.830.96 200.00 200.64n-Pentatriacontane (C35) 630-07-9 RA2D10C FIL02
20.0020.000.99 200.00 200.00n-Dodecane (C12) 112-40-3 RA1B3C 02552CE
20.0020.000.99 200.00 200.00n-Octane (C8) 111-65-9 RA1C11A 02637JD
20.0020.000.99 200.00 200.00n-Decane (C10) 124-18-5 RA1C11D 05257JD
20.0020.000.99 200.00 200.00n-Hexane (C6) 110-54-3 RA1C12A 06218EE
20.4020.410.98 200.00 199.92n-Octacosane (C28) 630-02-4 RA1C13D 07820PE
20.0020.000.99 200.00 200.00n-Heneicosane (C21) 629-94-7 RA1D13A 06931KD
20.5020.410.98 200.00 200.90n-Hexadecane (C16) 544-76-3 RA1G12A 04449DE
20.0020.000.99 200.00 200.00n-Hexatriacontane (C36) 630-06-8 RA1G12C 01222HH
31639 A056067
Alternate BP/CN Distribution Marker Stock Solution
110 Benner CircleBellefonte, PA 16823-8812
Tel: (800)356-1688Fax: (814)353-1309
Catalog No. :
Description :
Expiration Date :
Lot No.:
Storage: Room Temperature
FOR LABORATORY USE ONLY-READ MSDS PRIOR TO USE.
November 2014
Certificate of Analysis
CAS #Percent Purity
2CompoundElution Order Concentration
(weight/volume)
Percent Uncertainty
43
n-Hexane (C6) 110-54-3 +/-0.08 %99% 1 200.000 ug/mln-Octane (C8) 111-65-9 +/-0.08 %99% 2 200.000 ug/ml
n-Decane (C10) 124-18-5 +/-0.08 %99% 3 200.000 ug/mln-Dodecane (C12) 112-40-3 +/-0.08 %99% 4 200.000 ug/ml
n-Hexadecane (C16) 544-76-3 +/-0.08 %98% 5 199.920 ug/mln-Heneicosane (C21) 629-94-7 +/-0.08 %99% 6 200.000 ug/mln-Octacosane (C28) 630-02-4 +/-0.08 %98% 7 199.920 ug/ml
n-Pentatriacontane (C35) 630-07-9 +/-0.08 %96% 8 199.680 ug/mln-Hexatriacontane (C36) 630-06-8 +/-0.08 %99% 9 200.000 ug/ml
PentaneSolvent:
Column: 30m x .25mm x .5um
hydrogen @ 40cm/sec.35°C (hold 2 min.) to 330°C
Rtx-5 (cat.#10238)
@ 10°C/min (hold 10 min.)250°C330°CFID
99%109-66-0
Carrier Gas:Temp. Program:
Inj. Temp:
Det. Type:Det. Temp:
Balance 1128342313
Lot #:A056067
Catalog #:Alternate BP/CN Distribution Marker Stock SolutionDescription:
Target:
PentaneSolvent: C19E42Solvent Lot: Final Volume:
Made by: Rebecca Lauver Date:Tested by: Diane Shaffer Date: 10/24/2007 3:15:39PM
By: Sara Eyster Date: 10/30/2007 10:52:34AMPackaged by: / Staci Bodle Date: 10/24/2007 3:02:58PM No. Units: 64
Balance Used:ARMBALPC1 XP205 Serial #: 1128342313
Pass
100.00 ml
31639 200 ug/ml
10/24/2007 11:55:43AM
Pkg Size: 1 mL
Chemical Standard Batch Sheet
Compound CASStorageLocation Lot # Purity
Target Weight
ActualWeight
Target Conc(ug/ml)
Calc Conc(ug/ml)
20.8020.830.96 200.00 199.68n-Pentatriacontane (C35) 630-07-9 RA2D10C FIL02
20.0020.000.99 200.00 200.00n-Dodecane (C12) 112-40-3 RA1B3C 02552CE
20.0020.000.99 200.00 200.00n-Octane (C8) 111-65-9 RA1C11A 02637JD
20.0020.000.99 200.00 200.00n-Decane (C10) 124-18-5 RA1C11D 05257JD
20.0020.000.99 200.00 200.00n-Hexane (C6) 110-54-3 RA1C12A 06218EE
20.4020.410.98 200.00 199.92n-Octacosane (C28) 630-02-4 RA1C13D 07820PE
20.0020.000.99 200.00 200.00n-Heneicosane (C21) 629-94-7 RA1D13A 06931KD
20.4020.410.98 200.00 199.92n-Hexadecane (C16) 544-76-3 RA1G12A 04449DE
20.0020.000.99 200.00 200.00n-Hexatriacontane (C36) 630-06-8 RA1G12C 01222HH
QA Report: Alternate BP/CN Distribution Marker Stock Solution (Cat.#31639)
Peak Area in 1000: Runs of Lot # A055797 Runs of Lot # A056067COMPONENT 1 2 3 AVG StdDev %RSD 1 2 3 AVG Std... %RSD %D MEAN P/Fn-Hexane 152 163 142 157 155 152n-Octane 346 375 323 331 328 317n-Decane 414 447 380 397 393 378n-Dodecane 425 458 388 405 402 387Fluorene (IS) 392 425 358 369 371 355n-Hexadecane 457 492 415 423 425 408n-Heneicosane 467 494 420 420 434 414n-Octacosane 488 504 432 420 443 439n-Pentatriacontane 460 492 417 411 417 432n-Hexatriacontane 444 477 403 404 409 422
Retention Time:n-Hexane 1.01 1.01 1.00 1.01 0.01 0.74 1.01 1.01 1.02 1.01 0.00 0.25 -0.66n-Octane 1.97 1.97 1.95 1.96 0.01 0.65 1.97 1.97 1.97 1.97 0.00 0.09 -0.45n-Decane 4.82 4.82 4.81 4.82 0.00 0.07 4.82 4.82 4.82 4.82 0.00 0.01 -0.05n-Dodecane 7.09 7.09 7.09 7.09 0.00 0.02 7.09 7.09 7.09 7.09 0.00 0.01 0.01Fluorene (IS) 10.25 10.25 10.25 10.25 0.00 0.01 10.25 10.25 10.25 10.25 0.00 0.01 0.01n-Hexadecane 10.69 10.69 10.69 10.69 0.00 0.01 10.69 10.69 10.69 10.69 0.00 0.00 0.01n-Heneicosane 14.22 14.22 14.22 14.22 0.00 0.00 14.22 14.22 14.22 14.22 0.00 0.01 0.01n-Octacosane 18.05 18.05 18.05 18.05 0.00 0.01 18.05 18.05 18.05 18.05 0.00 0.00 0.00n-Pentatriacontane 21.05 21.05 21.05 21.05 0.00 0.01 21.05 21.05 21.05 21.05 0.00 0.00 0.01n-Hexatriacontane 21.43 21.43 21.43 21.43 0.00 0.00 21.43 21.43 21.43 21.43 0.00 0.00 0.00
Relative Response Factors:n-Hexane 0.387 0.382 0.397 0.389 0.008 1.968 0.426 0.418 0.427 0.423 0.005 1.112 -8.87 Passn-Octane 0.883 0.882 0.904 0.890 0.012 1.353 0.897 0.884 0.892 0.891 0.007 0.736 -0.19 Passn-Decane 1.056 1.053 1.063 1.057 0.005 0.500 1.076 1.060 1.065 1.067 0.008 0.735 -0.95 Passn-Dodecane 1.086 1.078 1.085 1.083 0.004 0.378 1.097 1.083 1.089 1.090 0.007 0.649 -0.63 PassFluorene (IS) 1.000 1.000 1.000 1.000 0.000 0.000 1.000 1.000 1.000 1.000 0.000 0.000 0.00 Passn-Hexadecane 1.167 1.156 1.159 1.161 0.005 0.462 1.146 1.145 1.150 1.147 0.002 0.197 1.19 Passn-Heneicosane 1.193 1.161 1.175 1.176 0.016 1.345 1.137 1.170 1.166 1.158 0.018 1.555 1.58 Passn-Octacosane 1.247 1.186 1.208 1.214 0.031 2.542 1.138 1.194 1.236 1.189 0.049 4.143 2.02 Passn-Pentatriacontane 1.174 1.157 1.166 1.166 0.009 0.737 1.112 1.126 1.218 1.152 0.057 4.985 1.18 Passn-Hexatriacontane 1.134 1.123 1.128 1.128 0.005 0.466 1.093 1.103 1.187 1.128 0.051 4.550 0.03 Pass
Page 1 of 2 Area % Report
Data File: \\Morty\Ezchrom\Projects\standards\Data\n-Hexane (C6) Lot#06218EE--Rep2 Method: \\Morty\Ezchrom\Projects\standards\Method\VOl-NFH-HP7f.met Acquired: 1/5/2007 12:25:31 PM Printed: 1/5/2007 1:32:23 PM n-Hexane (C6) Lot#06218EE-
HP-7
Page 2 of 2
Minutes0.0 2.5 5.0 7.5 10.0 12.5 15.0 17.5 20.0 22.5 25.0
Vol
t
0.5
1.0
1.5
2.0
Vol
t
0.5
1.0
1.5
2.0
8.78
10.1
4
Front FID ResultsRetention Time Area Area Percent
8.78 8448157 99.69710.14 25707 0.303
Totals8473864 100.000
File :\\Morty\Ezchrom\Projects\standards\Data\06218EE-.DOperator : ARM QAAcquired : 5 Jan 2007 14:16 using AcqMethod VOL-NFH.MInstrument : Instrument #8Sample Name: n-Hexane (C6) Lot#06218EE- Misc Info : Vial Number: 5
28 30 32 34 36 38 40 42 44 46 48 50 52 54 56 58 60 62 64 66 68 70 72 74 76 78 80 82 84 86 88 90 92 94 960
1000
2000
3000
4000
5000
6000
7000
8000
9000
m/z-->
Abundance Scan 1893 (8.592 min): 06218EE-.D\data.ms41 57
43
8655
715351 696763 6549 77 7959 746145
28 30 32 34 36 38 40 42 44 46 48 50 52 54 56 58 60 62 64 66 68 70 72 74 76 78 80 82 84 86 88 90 92 94 960
1000
2000
3000
4000
5000
6000
7000
8000
9000
m/z-->
Abundance #112279: Hexane57
43
41
8639
55 715351
Page 1 of 1 Area % Report
Data File: \\MORTY\ezchrom\Projects\standards\Data\Octane Lot#02637JD Method: \\Morty\Ezchrom\Projects\standards\Method\VOLRAW-HP7.met Acquired: 12/21/2005 4:47:41 PM Printed: 12/22/2005 12:22:17 PM Octane Lot#02637JD
40°C (hold 2 min.) to 240° C @ 8 C/min. (hold 10 min.)Column: Rtx-502.2 105m x .53mm x 3.0um Cat.#10910Inj: 200 C Split @ 5 ml/min.Det: FID @ 250 CCarrier Gas: Hydrogen @ 40 cm/sec.
HP-7
Minutes0 5 10 15 20 25 30 35
Vol
ts
0
5
10
Vol
ts
0
5
10
8.09
13.3
114
.10
Back FID ResultsRetention Time Area Area Percent
8.09 150961 0.32513.31 211649 0.45614.10 46050966 99.219
Totals46413576 100.000
File : G:\MSDATA\02637JD.DOperator : SEEAcquired : 22 Dec 2005 10:41 am using AcqMethod VOL Instrument : GCDSample Name: Octane 02637JD Misc Info : Vial Number: 22
0 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 115 1200
1000
2000
3000
4000
5000
6000
7000
8000
9000
m/z-->
Abundance Scan 1333 (14.472 min): 02637JD.D43
8557
7139
1145367 7763
0 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 115 1200
1000
2000
3000
4000
5000
6000
7000
8000
9000
m/z-->
Abundance #109231: Octane43
29 5785
71
39114
15 532 67 77 81 91 97 101
Page 1 of 2 Area % Report
Data File: \\Morty\Ezchrom\Projects\standards\Data\n-Decane Lot#05257JD Method: \\Morty\Ezchrom\Projects\standards\Method\svraw-HP4.met Acquired: 5/2/2007 1:20:14 PM Printed: 5/2/2007 2:04:30 PM n-Decane Lot#05257JD
HP-4a
Minutes0 5 10 15 20 25 30 35 40
Vol
t
0.0
2.5
5.0
7.5
Vol
t
0.0
2.5
5.0
7.5
7.09
7.29
8.05
8.51
9.55
11.1
8
26.1
1
HP 6890 ResultsRetention Time Area Area Percent
7.09 13628 0.0277.29 110709 0.2188.05 50635361 99.7098.51 7961 0.0169.55 5637 0.011
11.18 4019 0.00826.11 5627 0.011
Totals50782942 100.000
Library Searched : G:\Nist98.lQuality : 94ID : Decane
5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 115 120 125 130 135 140 145 1500
1000
2000
3000
4000
5000
6000
7000
8000
9000
m/z-->
Abundance Scan 913 (9.304 min): 05257JD.D\data.ms57
71
85
1429911353
67 7763 81 91 12795
5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 115 120 125 130 135 140 145 1500
1000
2000
3000
4000
5000
6000
7000
8000
9000
m/z-->
Abundance #112241: Decane57
43
71
8529
39
99 14253 1136714 77
Page 1 of 1 Area % Report
Data File: \\MORTY\ezchrom\Projects\standards\Data\n-Dodecane Lot#02552CE Method: \\Morty\Ezchrom\Projects\standards\Method\svraw.met Acquired: 6/6/2007 3:26:06 PM Printed: 6/6/2007 4:16:02 PM n-Dodecane Lot#02552CE
HP-3
Minutes0 5 10 15 20 25 30 35 40
Volts
0
1
2
3
Volts
0
1
2
3
10.6
210
.87
11.3
811
.44
11.5
5
FID ResultsRetention Time Area Area Percent
10.62 3331 0.06010.87 14255 0.25711.38 5523215 99.56011.44 3660 0.06611.55 3152 0.057
Totals5547613 100.000
File :\\Morty\ezchrom\Projects\standards\Data\02552CE.DOperator : ARM QAAcquired : 6 Jun 2007 18:06 using AcqMethod SVRAW.MInstrument : Instrument #1Sample Name: n-Dodecane Lot#02552CE Misc Info : Vial Number: 12
20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 115 120 125 130 135 140 145 150 155 160 165 170 175 1800
1000
2000
3000
4000
5000
6000
7000
8000
9000
m/z-->
Abundance Scan 1468 (12.480 min): 02552CE.D\data.ms57
71
85
17099113 127
1416551 77 91 155105
20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 115 120 125 130 135 140 145 150 155 160 165 170 175 1800
1000
2000
3000
4000
5000
6000
7000
8000
9000
m/z-->
Abundance #112318: Dodecane57
43
71
85
29
17099 113 127141
51 65 7938 91 155136
Page 1 of 1 Area % Report
Data File: \\MORTY\ezchrom\Projects\standards\Data\n-Heneicosane Lot#06931KD Method: \\MORTY\ezchrom\Projects\standards\Method\svraw.met Acquired: 3/19/2007 10:23:07 PM Printed: 3/20/2007 8:48:31 AM n-Heneicosane Lot#06931KD
HP-3
Minutes0 5 10 15 20 25 30 35 40
Volts
0
1
2
3
Volts
0
1
2
38.
05
21.3
922
.46
23.3
2
31.8
932
.44
38.0
5
FID ResultsRetention Time Area Area Percent
8.05 7689 0.087
21.39 18060 0.20522.46 8743480 99.34823.32 12005 0.136
31.89 4920 0.05632.44 5905 0.067
38.05 8809 0.100
Totals8800868 100.000
File :\\Morty\Ezchrom\Projects\standards\Data\06931KD.DOperator : ARM QAAcquired : 19 Mar 2007 17:02 using AcqMethod SVRAW.MInstrument : Instrument #1Sample Name: n-Heneicosane Lot#06931KD Misc Info : Vial Number: 1
30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 220 230 240 250 260 270 280 290 3000
1000
2000
3000
4000
5000
6000
7000
8000
9000
m/z-->
Abundance Scan 3262 (22.731 min): 06931KD.D\data.ms57
71
85
99
113127
141 155 296169 183 197 211 225 239 253 267 281
30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 220 230 240 250 260 270 280 290 3000
1000
2000
3000
4000
5000
6000
7000
8000
9000
m/z-->
Abundance #112581: Heneicosane57
71
43
85
99
113127 141 296155 169 183 211197 225 239 253 267
Page 1 of 1 Area % Report
Data File: \\Morty\Ezchrom\Projects\standards\Data\n-Octacosane (C28) Lot#07820PE Method: \\Morty\Ezchrom\Projects\standards\Method\svraw.met Acquired: 7/17/2007 4:37:23 AM Printed: 7/17/2007 10:39:36 AM n-Octacosane (C28) Lot#07820PE
HP-3
Minutes0 5 10 15 20 25 30 35 40
Volts
0
1
2
Volts
0
1
2
13.7
4
26.1
426
.57
26.9
227
.73
28.0
629
.09
FID ResultsRetention Time Area Area Percent
13.74 2216 0.043
26.14 38367 0.74826.57 2693 0.05226.92 19881 0.38827.73 5042149 98.28028.06 3651 0.07129.09 21430 0.418
Totals5130387 100.000
File :\\Morty\ezchrom\Projects\standards\Data\07820PE.DOperator : ARM QAAcquired : 16 Jul 2007 18:59 using AcqMethod SVRAW.MInstrument : Instrument #1Sample Name: n-Octacosane Lot#07820PE Misc Info : Vial Number: 4
20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 4000
1000
2000
3000
4000
5000
6000
7000
8000
9000
m/z-->
Abundance Scan 4219 (28.198 min): 07820PE.D\data.ms57
71
85
99
113127 141 155 169 183 197 211 225 394239 253 267 337295281 323309 351 365
20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 4000
1000
2000
3000
4000
5000
6000
7000
8000
9000
m/z-->
Abundance #16409: Octacosane57
43
71
85
9929
113127
141 155 169 183 197 211 225 239 281253 267 309 394337295 323 351 365
Page 1 of 1 Area % Report
Data File: \\Morty\Ezchrom\Projects\standards\Data\n-Pentatriacontane (C35) Lot#FIL02- Method: \\Morty\Ezchrom\Projects\standards\Method\svraw.met Acquired: 10/3/2006 8:48:04 AM Printed: 10/3/2006 9:44:12 AM n-Pentatriacontane (C35) Lot#FIL02-
HP-2
Minutes0 5 10 15 20 25 30 35 40
Volts
0.0
0.1
0.2
Volts
0.0
0.1
0.2
24.3
9
30.3
2
38.0
1
FID ResultsRetention Time Area Area Percent
24.39 8227 2.30830.32 342354 96.02838.01 5934 1.664
Totals356515 100.000
File :\\Morty\Ezchrom\Projects\standards\Data\FIL02.DOperator : ARM QAAcquired : 3 Oct 2006 3:49 using AcqMethod SVRAW.MInstrument : Instrument #1Sample Name: n-Pentatriacontane Lot#FIL02 Misc Info : Vial Number: 13
40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 440 460 480 5000
50000
100000
150000
200000
250000
300000
350000
400000
450000
500000
550000
600000
650000
700000
m/z-->
Abundance Scan 5062 (33.013 min): FIL02.D\data.ms57
71
85
99
113
127
141155
169183 197 211 225 239 253 281267 295 323 337 379309 393365 421 435351 407 493449
Page 1 of 1 Area % Report
Data File: \\Morty\Ezchrom\Projects\standards\Data\n-Hexatriacontane -Lot#01222HH Method: \\Morty\Ezchrom\Projects\standards\Method\31095.met Acquired: 8/8/2007 9:16:42 AM Printed: 8/8/2007 10:01:49 AM n-Hexatriacontane Lot#01222HH
HP-3
Minutes0 5 10 15 20 25 30 35 40
Vol
ts
0.00
0.25
0.50
0.75
Vol
ts
0.00
0.25
0.50
0.75
34.1
1
FID ResultsRetention Time Area Area Percent
34.11 2706922 100.000
Totals2706922 100.000
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