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Laucks Testing Laboratories, Inc. SFUND RECORDS CTR 167987 940 South Harney St. Seattle, WA 98108 (206) 767-5060 FAX (206) 767-5063 FAX Cover Sheet To: Company: From: "r~ FAX Number: Date: No. of Pages (including cover page): Q -"5^ 3 Preliminary Results for: Workorders(s); Analysis: Verified by: Do these samples need to be re-analyzed? If yes, which samples?:________________ Reason: Yes The preliminary results for the re-analysis will be faxed on (date): Laucks does not certify that these results meet NELAC Standards because all NELAC required elements are not included in the facsimile. Please refer to the full report to review all NELAC required elements. The information contained in or attached to this FAX message is intended only for >he confidential use of the individual(s) named above. If you are not the named recipient, or an agent responsible for delivering it to Ihe named recipient, you are hereby notified that you have received this document in error, and that review, dissemination, or copying of this communication is prohibited. If you have received this communication in error, please notify us immediately by telephone at 206-767-5060, and return the original documenls to us by mail at the address listed above.
25

Analytical data, SDG MAI01, soil samples received …MAI01 (g/ml) G decanted:(Y/N) (uL) N Lab Sample ID: 0308327-01 Lab File ID: L0902012.D Date Received: 08/21/03 _ Date Extracted:

Aug 28, 2020

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Page 1: Analytical data, SDG MAI01, soil samples received …MAI01 (g/ml) G decanted:(Y/N) (uL) N Lab Sample ID: 0308327-01 Lab File ID: L0902012.D Date Received: 08/21/03 _ Date Extracted:

LaucksTesting Laboratories, Inc.

SFUND RECORDS CTR167987

940 South Harney St.Seattle, WA 98108

(206) 767-5060 FAX (206) 767-5063

FAX Cover SheetTo:

Company:

From:

"r~FAX Number:

Date:

No. of Pages(including cover

page):

Q -"5 3

Preliminary Results for:

Workorders(s);

Analysis:

Verified by:

Do these samples need to be re-analyzed?If yes, which samples?:________________Reason:

Yes

The preliminary results for the re-analysis will be faxed on (date):

Laucks does not certify that these results meet NELAC Standards because all NELAC required elementsare not included in the facsimile. Please refer to the full report to review all NELAC required elements.

The information contained in or attached to this FAX message is intended only for >he confidential use of the individual(s)named above. If you are not the named recipient, or an agent responsible for delivering it to Ihe named recipient, you arehereby notified that you have received this document in error, and that review, dissemination, or copying of thiscommunication is prohibited. If you have received this communication in error, please notify us immediately by telephone at206-767-5060, and return the original documenls to us by mail at the address listed above.

Page 2: Analytical data, SDG MAI01, soil samples received …MAI01 (g/ml) G decanted:(Y/N) (uL) N Lab Sample ID: 0308327-01 Lab File ID: L0902012.D Date Received: 08/21/03 _ Date Extracted:

1BSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

Lab Name: Laucks Testing_Labs____ Contract: ________

SAMPLE NO.

072-002-001

Case No.:

SOIL

MED

Lab Code:

Matrix: (soil/water)

Sample wt/vol:

Level: (low/med)% Moisture: 7

Concentrated Extract Volume: 500_

Injection Volume: 2.0 (uL)GPC Cleanup: (Y/N) Y pH:

SAS No.: SDGNo.: MAI01

(g/ml) G

decanted:(Y/N)(uL)

N

Lab Sample ID: 0308327-01

Lab File ID: L0902012.D

Date Received: 08/21/03 _

Date Extracted: 08/26/03

CAS NO. COMPOUND

Date Analyzed: 09/02/03Dilution Factor: 1.0

CONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG Q

100-52-7108-95-2111-44-495-57-895-48-7108-60-198-86-2106-44-5621-64-767-72-198-95-378-59-188-75-5105-67-9111-91-1120-83-291-20-3106-47-887-68-3105-60-259-50-791-57-677-47-488-06-295-95-4, j92-52-4 " i91-58-7 !88-74-4 .131-11-3 ;606-20-2 !208-96-8 i99-09-2 '83-32-951-28-5 i100-02-7132-64-9121-14-2

BenzaldehydePhenolbis(2-Chloroethyl)ether2-Chlorophenol2-Methylphenol2,2'-oxybis(1 -Chloropropane)Acetophenone4-MethylphenolN-Nitroso-di-n-propylamineHexachloroethaneNitrobenzeneIsophorone2-Nitrophenol2,4-Dimethylphenolbis(2-ChloroethoxyJmethane2,4-DichlorophenolNaphthalene4-ChloroanilineHexachlorobutadieneCaprolactam4-Ch!oro-3-methylphenol2-MethylnaphthaleneHexachlorocyclopentadiene2,4,6-Trichlorophenol2,4,5-Trichlorophenol1,1'-Biphenyl2-Chloronaphthalene2-NitroanilineDimethylphthalate2.6-DinitrotolueneAcenaphthylene j3-Nitroaniline !Acenaphthene j2,4-Dinitrophenol4-NitrophenolDibenzofuran2,4-Dinitrotoluene

2700270027002700270027002700270027002700276627002700270027002700270027002700270027002700270027002700270027002700270027002700270027002700270027002700

UUU

, UUUUUUUUUU JUUUUUr uUuuuuuuu

• uuuuuuuuuu

FORM I SV-1

Page 3: Analytical data, SDG MAI01, soil samples received …MAI01 (g/ml) G decanted:(Y/N) (uL) N Lab Sample ID: 0308327-01 Lab File ID: L0902012.D Date Received: 08/21/03 _ Date Extracted:

1CSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

SAMPLE NO.

Lab Name: Laucks Testing Labs Contract:072-002-001

Case No.:

SOIL

2

MED

Lab Code:Matrix: (soil/water)

Sample wt/vol:

Level: (low/med)% Moisture; 7

Concentrated Extract Volume: 500Injection Volume: 2.0 (uL)

GPC Cleanup: (Y/N) Y pH:

SAS No.: SDGNo.: MAI01

(g/ml) G

decanted:(Y/N)

(uL)

Lab Sample ID: 0308327-01Lab File ID: L0902012.D

N

CAS NO. COMPOUND

Date Received: 08/21/03

Date Extracted: 08/26/03

Date Analyzed: 09/02/03Dilution Factor: 1.0

CONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG Q

84-66-286-73-77005-72-3100-01-6534-52-186-30-6101-55-3118-74-11912-24-987-86-585-01-8120-12-786-74-884-74-2206-44-0129-00-085-68-791-94-156-55-3218-01-9117-81-7117-84-6205-99-2207-08-950-32-8_^193-39-5"53-70-3191-24-2

I Diethylphthalatej Fluorenei 4-Chlorophenyl-phenylether; 4-Nitroaniline

4,6-Dinitro-2-methvlphenotN-Nitrosodiphenylamine4-Brornophenyl-phenyletherHexachlorobenzeneAtrazinePentachlorophenolPhenanthreneAnthraceneCarbazoleDi-n-butylphthalateFluoranthenePyreneButylbenzylphthalate3t3'-DichlorobenzidineBenzo[alanthraceneChrysenebis(2-Ethylhexyl)phthalateDi-n-octylphthalateBenzolb]fluorantheneBenzofklfluorantheneBenzola]pyrenelndeno[1 ,2,3-cd]pyreneDibenzo[a,hjanthraceneBenzo^h.ijperylene

1100r _..,_

270027002700270027002700

I 27002700120027002700840

2700890

2700270027002700160027002700 I27002700270027002700

JU ,u

,ui U

uuuuuJuU J

JBUJuuuuJuu

.. u_JuU _|u

" U

FORM I SV-2

Page 4: Analytical data, SDG MAI01, soil samples received …MAI01 (g/ml) G decanted:(Y/N) (uL) N Lab Sample ID: 0308327-01 Lab File ID: L0902012.D Date Received: 08/21/03 _ Date Extracted:

18SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

SAMPLE NO.

Lab Name: Laucks Testing Labs

Lab Code: Case No.:

Matrix: (soil/water) SOILSample wt/vol: 15

Level: (low/med) LOW

% Moisture: 7

Concentrated Extract Volume: 500

Injection Volume: 2.0 (uL)GPC Cleanup: (Y/N) Y pH:

072-002-001 RE

(g/ml) G_

decanted:(Y/N)

(uL)

Contract: __ _ _SAS No.: _ SDG No.: MAI01

Lab Sample ID: 0308327-01 RELab File ID: L0904020.D

Date Received: 08/21/03N Date Extracted: 08/25/03

Date Analyzed: 09/04/03

Dilution Factor: 4.0

CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG Q

100-52-7j 108-95-2

il1_44_495-57-895-48-7108-60-198-86-2106-44-5621-64-767-72-198-95-378-59-188-75-5105-67-9111-91-1120-83-291-20-3106-47-887-68-3105-60-259-50-791-57-6 •;77-47-488-06-295-95-4.,92-52-4 '91-58-788-74-4131-11-3606-20-2208-96-899-09-283-32-951-28-5100-02-7132-64-9121-14-2

| Benzaldehyde; Phenoli bis(2-Chloroethyl)ether! 2-Chlorophenol! 2-Methylphenol

2,2'-oxybis(1 -Chloropropane)i Acetophenone1 4-Methylphenol

N-Nitroso-di-n-propylamineHexachtoroethaneNitrobenzeneIsophorone2-Nitrophenol2,4-Dimethylphenolbis(2-Chloroethoxy)methane

i 2,4-DichlorophenolNaphthalene

; 4-Chloroaniline: Hexachlorobutadiene1 Caprolactam| 4-Chloro-3-methylphenolI 2-Methylnaphthalene

Hexachlorocyclopentadiene2,4,6-Trichlorophenol2,4,5-TrichlorophenolIJ'-Biphenyl2-Chloronaphthalene2-NitroanilineDimethylphthalate2,6-Dinitrotoluene

I Acenaphthylene; 3-Nitroaniline: Acenaphthene; 2,4-Dinitrophenol

4-NitrophenolDibenzofuran2,4-Dinitrototuene

1400140014001400140014001400

I 140014001400140014001400140014001400140014001400140014001400140014001400140014001400140014001400140014001400140014001400

UUU

, UUUUUUUUUUUU

I— uI u

uuuuuuuuuu

- uuuuuuuuuu

FORM I SV-1

Page 5: Analytical data, SDG MAI01, soil samples received …MAI01 (g/ml) G decanted:(Y/N) (uL) N Lab Sample ID: 0308327-01 Lab File ID: L0902012.D Date Received: 08/21/03 _ Date Extracted:

1CSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

SAMPLE NO.

Lab Name: Laucks Testing LabsLab Code:

Contract:072-002-001 RE

Case No.: SAS No.: SDGNo.: MAI01

SOIL

15_

LOW

Matrix: (soil/water)

Sample wt/vol:

Level: (low/med)% Moisture: 7

Concentrated Extract Volume: 500Injection Volume: 2.0 (uL)

GPC Cleanup: (Y/N) Y pH:

_ (g/ml) G

decanted:(Y/N)

(uL)

Lab Sample ID: 0308327-01 RELab File ID:

Date Received: 08/21/03N Date Extracted: 08/25/03

GAS NO. COMPOUND

Date Analyzed: 09/04/03Dilution Factor: 4.0

CONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG Q

84-66-286-73-7

! 7005-72-3100-01-6534-52-186-30-6101-55-3118-74-11912-24-9

I 87-86-5i 85-01-8

120-12-7i 86-74-8

84-74-2206-44-0129-00-685-68-791-94-156-55-3218-01-9117-81-7117-84-0=205-99-2207-08-950-32-8.193-39-5 -53-70-3191-24-2

DiethylphthalateFluorene4-Chlorophenyl-phenylether4-Nitroaniline4,6-Dinitro-2-metrtylphenolN-Nitrosodiphenylamine4-Bromophenyl-phenyIetherHexachlorobenzeneAtrazinePentachlorophenolPhenanthreneAnthraceneCarbazoleDi-n-butylphthalateFluoranthenePyreneBulylbenzylphthalate3,3'-DichlorobenzidineBenzo[a]anthraceneChrysenebis(2-Ethylhexyl}phthalateDi-n-octylphtnaiateBenzo[b]fluorantheneBenzo[k]fluorantheneBenzo[a]pyrene!ndeno[1 ,2,3-cd]pyreneDibenzofohjanthraceneBenzolg.h.ijperylene I

140014001400140014001400140014001400

1 14002100140014001400690

1100140014001400460900

1400140014001400140014001400

UUU

,Ur uUUUUU

UUUJJUuuJJuuuuuu

" U

FORM I SV-2

Page 6: Analytical data, SDG MAI01, soil samples received …MAI01 (g/ml) G decanted:(Y/N) (uL) N Lab Sample ID: 0308327-01 Lab File ID: L0902012.D Date Received: 08/21/03 _ Date Extracted:

1BSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

SAMPLE NO.

Lab Name: Laucks_Testing_Labs_____Lab Code: Case No.:

Matrix: (soil/water) SOILSample wt/vol:

Level: (low/med)

Contract:SAS No.:

072-002-002

15 _ (g/ml) G

LOW

decanted:(Y/N)

(uL)

% Moisture: 9

Concentrated Extract Volume: 500Injection Volume: 2.0 (uL)GPC Cleanup: (Y/N) Y pH:

N

SDG No.: MAJ01

Lab Sample ID: 0308327-02Lab File ID: L0904021.D

Date Received: 08/21/03Date Extracted: 08/25/03

CAS NO. COMPOUND

Date Analyzed: 09/04/03Dilution Factor: 4.0

CONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG Q

100-52-7108-95-2111-44-495-57-895-48-7108-60-198-86-2106-44-5621-64-767-72-198-95-378-59-188-75-5105-67-9111-91-1120-83-291-20-3106-47-887-68-3105-60-259-50-791-57-677-47-488-06-295-95-4,92-52-4 *"91-58-788-74-4131-11-3606-20-2208-96-899-09-283-32-951-28-5100-02-7132-64-9121-14-2

I Benzaldehydei Phenoli bis(2-Chloroethyl)ether! 2-Chlorophenol! 2-Methylphenolj 2,2'-oxybis(1-Chloropropane)i Acetophenonei 4-Methylphenoli N-Nitroso-di-n-propylaminej Hexachloroethanei Nitrobenzene; Isophorone

2-Nitrophenoli 2,4-Dimethylphenol; bis(2-Chloroethoxy)methaneI 2,4-Dichlorophenoli Naphthalene

4-ChloroanilineHexachlorobutadiene

i Caprolactam4-Chloro-3-methylphenol

! 2-Methylnaphthalene! Hexachlorocyclopentadienej 2,416-Trichlorophenoli 2,4,5-trichlorophenoi

1.1'-BiphenylI 2-Chloronaphthalene

2-NitroanilineDimethylphthalate

I 2,6-DinitrotolueneAcenaphthylene3-NitroanilineAcenaphthene

i 2,4-Dinitrophenol! 4-Nitrophenol1 Dibenzofuran

2,4-Dinitrotoluene

1500150015001500150015001500320

15001500150015001500150015001500150015001500150015001500150015001500150015001500150015001500150015001500150015001500 j

UUU

,uUUUJUUUUUUU ju 1Uuuuuuuuuuu

" Uuuuuuuuuu

FORM I SV-1

Page 7: Analytical data, SDG MAI01, soil samples received …MAI01 (g/ml) G decanted:(Y/N) (uL) N Lab Sample ID: 0308327-01 Lab File ID: L0902012.D Date Received: 08/21/03 _ Date Extracted:

1CSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

SAMPLE NO.

Lab Name: Laucks Testing Labs Contract:072-002-002

Case No.:SOIL

15

LOW

Lab Code:Matrix: (soil/water)Sample wt/vol:Level: (low/med)

% Moisture: 9

Concentrated Extract Volume: 500

Injection Volume: 2.0 (uL)

GPC Cleanup: (Y/N) Y pH:

SAS No.: SDGNo.: MAI01

__ (g/ml) G

decanted:(Y/N)(uL)

N

Lab Sample ID: 0308327-02Lab File ID: L090402TI .DDate Received: 08/21/03

Date Extracted: 08/25/03

Date Analyzed: 09/04/03Dilution Factor: 4.0

CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG Q

, 84-66-286-73-77005-72-3100-01-6534-52-186-30-6101-55-3118-74-11912-24-987-86-585-01-8120-12-786-74-884-74-2206-44-0129-00-085-68-791-94-156-55-3218-01-9117-81-7117-84-0^205-99-2207-08-950-32-8^193-39-5"'53-70-3191-24-2

' DiethylphthalateI Fluorene| 4-Chlorophenyl-phenyletherI 4-Nitroaniline! 4,6-Dinitro-2-methylphenol

N-Nitrosodiphenylamine4-Bromophenyl-phenyletherHexachlorobenzeneAtrazinePentachlorophenolPhenanthreneAnthraceneCarbazoleDi-n-butylphthalateFluoranthenePvreneButylbenzyjphthalate3,3'-DichlorobenzidineBenzolajanthraceneChrysene

i bis(2-Ethylhexyl)phthalateI Di-n-octylphthalate! Benzo[b]fluoranthene} Benzo[k]fluoranthene

Benzoralpyrenei lndeno[1,2,3-cd]pyrenei Dibenzo[a,hlanthracene

Benzo[g,h,i]perylene

15001500150015001500150015001500150015001500150015001500150015001500 ,15001500150035001500150015001500150015001500

UUr u

,uuuuuuuuuu

u uuuuuuu

uuuuuu

" u ,

FORM I SV-2

Page 8: Analytical data, SDG MAI01, soil samples received …MAI01 (g/ml) G decanted:(Y/N) (uL) N Lab Sample ID: 0308327-01 Lab File ID: L0902012.D Date Received: 08/21/03 _ Date Extracted:

1BSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

SAMPLE NO.

Lab Name: Laucks Testing LabsLab Code: _ Case No.:Matrix: (soil/water) SOILSample wt/vol: 15 _ _Level: (low/med) LOW% Moisture: 0Concentrated Extract Volume: 500Injection Volume: 2.0 (uL)GPC Cleanup: (Y/N) Y pH:

Contract:SAS No.:

072-002-003

SDGNo.: MAI01

(g/ml) G_

decanted:(Y/N)(uL)

N

Lab Sample ID: 0308327-03Lab File ID: L0904018.DDate Received: 08/21/03Date Extracted: 08/25/03Date Analyzed: 09/04/03Dilution Factor: 2.0

CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG Q

! 100-52-7i 108-95-2

1 1 1-44-495-57-8

i 95-48-7108-60-198-86-2106-44-5621-64-767-72-1 i98-95-3 i78-59-1 !

88-75-5105-67-9 ;

\ 111-91-1 i; 120-83-2i 91-20-3 ;

106-47-8 !87-68-3 i105-60-2 i59-50-791-57-6 ••--77-47-488-06-295-95-4,92-52-4 *"'91-58-788-74-4131-11-3606-20-2208-96-899-09-2 !83-32-9 !51-28-5 j100-02-7 I132-64-9121-14-2

BenzaldehydePhenolbis(2-Chloroethyl)ether2-Chlorophenol2-Methylphenol2,2'-oxybis(1 -Chloropropane)Acetophenone4-MethylphenolN-Nitroso-di-n-propylamineHexachloroethaneNitrobenzeneIsophorone2-Nitrophenol2,4-Dimethylphenolbis(2-Chloroethoxy)methane2,4-DichlorophenolNaphthalene4-ChloroanilineHexachlorobutadieneCaprolactam4-Chloro-3-methylphenol2-MethylnaphthaleneHexachlorocyclopentadiene2,4,6-Trichiorophenol2,4,5-Trichlorophenol1,1'-Biphenyl2-Chloronaphthalene2-NitroanilineDimethylphthalate2,6-DinitrotolueneAcenaphthylene3-NitroanilineAcenaphthene2,4-Dinitrophenol4-NitrophenolDibenzofuran2,4-Dinitrotoluene

670670670670670670670670670670670670670670670670670670670670670670670„

670670670670670670670670670670670670670

UUU

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" UU 1

UUUUUUUU

FORM I SV-1

Page 9: Analytical data, SDG MAI01, soil samples received …MAI01 (g/ml) G decanted:(Y/N) (uL) N Lab Sample ID: 0308327-01 Lab File ID: L0902012.D Date Received: 08/21/03 _ Date Extracted:

1CSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

SAMPLE NO.

Lab Name: Laucks Testing Labs ____

Lab Code: _ Case No.:Matrix: (soil/water) SOIL

Sample wt/vol: 15

Level: (low/med) LOW

% Moisture: 0

Contract:SAS No.:

072-002-003

(g/ml) G

decanted :(Y/N)

Concentrated Extract Volume: 500 (uL)

Injection Volume: 2.0 (uL)

GPC Cleanup: (Y/N) Y pH:

N

__ SDG No.: MAJ01_Lab Sample ID: 0308327-03Lab File ID: L0904018.D

Date Received: 08/21/03

Date Extracted: 08/25/03 _Date Analyzed: 09/04/03Dilution Factor: 2.0

CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG Q

84-66-286-73-77005-72-3100-01-6

[ 534-52-1i 86-30-6

101-55-3118-74-11912-24-987-86-5

| 85-01-8120-12-786-74-884-74-2206-44-0129-00-0

[ 85-68-791-94-156-55-3218-01-9117-81-7117-84-6205-99-2207-08-950~-32-8,193-39-5'"'53-70-3191-24-2

i DiethylphthaiateFluorene4-Chlorophenyl-phenylether4-Nitroaniline4,6-Dinitro-2-methylphenolN-Nitrosodiphenylamine4-Bromoj3henyl-phenyletherHexachlorobenzeneAtrazinePentachlorophenolPhenanthreneAnthraceneCarbazoleDi-n-butylphthalateFluoranthenePyreneButylbenzylphthalate3,3'-DichlorobenzidineBenzo[ajanthraceneChrysenebis(2-Ethylhexyl)phthalateDi-n-octylphthalateBenzo[b]fiuorantheneBenzo[kjfluorantheneBenzo[a]pyreneIndenofl^.S-cdJpyreneDibenzo[a,h]anthraceneBenzo[g,h,i]perylene

670 U670 U670 U670 , U

r~ 670 U670 U670 U670 U670 U670 U220 J670 U670 U670 U400 ' J480 J440 J670 U210 J340 J

2900670350 J670 U170 J140 J670 U n

170 ]- J

FORM I SV-2

Page 10: Analytical data, SDG MAI01, soil samples received …MAI01 (g/ml) G decanted:(Y/N) (uL) N Lab Sample ID: 0308327-01 Lab File ID: L0902012.D Date Received: 08/21/03 _ Date Extracted:

1BSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

SAMPLE NO.

Lab Name: Laucks *festing_J.absLab Code: _ _ Case No.: __

Matrix: (soil/water) SOIL _

Sample wt/vol: 15 (g/ml) GLevel: (low/med) LOW

% Moisture: 18 decanted:(Y/N)

Concentrated Extract Volume: 500 (uL)

Injection Volume: 2.0 (uL)

GPC Cleanup: (Y/N) Y pH:

Contract:072-002-004

N

SAS No.: _ SDG No.: MAJ01

Lab Sample ID: 0308327-04

Lab File ID: LP?02021^p

Date Received: 08/21/03^ _

Date Extracted: 08/25/03

Date Analyzed: 09/02/03

Dilution Factor: 1.0

CAS NO. COMPOUNDCONCENTRATION UNJTS:(ug/L or ug/Kg) UG/KG Q

100-52-7108-95-2111-44-495-57-895-48-7108-60-198-86-2106-44-5621-64-767-72-198-95-378-59-188-75-5105-67-9111-91-1120-83-291-20-3106-47-887-68-3105-60-259-50-791-57-677-47-488-06-295-95-4,92-52-4 "91-58-788-74-4131-11-3606-20-2208-96-899-09-283-32-951-28-5100-02-7 ;

132-64-9 !121-14-2 I

BenzaldehydePhenolbis(2-ChloroethylJether2-Chlorophenol2-Methylphenol2,2'-oxybis(1 -Chloropropane)Acetophenone4-MethylphenolN-Nitroso-di-n-propylamineHexachloroethaneNitrobenzeneIsophorone2-Nitrophenol2,4-Dimethylphenolbis(2-Chloroethoxy)methane2,4-DichlorophenolNaphthalene4-ChloroanilineHexachlorobutadieneCaprolactam4-Chloro-3-methylphenol2-MethylnaphthaleneHexachlorocyclopentadiene2,4,6-Trichlorophenol2,4^5-Trichlorophenol1,1'-Biphenyl2-Chloronaphthalene2-NitroanilineDimethylphthalate2L6-DinitrototueneAcenaphthylene3-NitroanilineAcenaphthene2,4-Dinitrophenol4-NitrophenolDibenzofuran2,4-Dinitrotoluene I

150 J410 U410 U410 aU410 U410 U130 J410 U410 [_ U410 U410 U410 U410 U410 U410 U410 U410 U410 U410 i U410 U410 U410 U410 U410 U410 i U410 U410 U410 ^ U410 U410 U410 U410 U410 U410 U410 U410 U410 U

FORM I SV-1

Page 11: Analytical data, SDG MAI01, soil samples received …MAI01 (g/ml) G decanted:(Y/N) (uL) N Lab Sample ID: 0308327-01 Lab File ID: L0902012.D Date Received: 08/21/03 _ Date Extracted:

1CSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

SAMPLE NO.

Lab Name: Laucks Testing Labs _____Lab Code: Case No.: __Matrix: (soil/water) SOILSample wt/vol: 15 (g/ml) GLevel: (low/med) LOW% Moisture: 18 decanted:(Y/N)Concentrated Extract Volume: 500 (uL)

Injection Volume: 2.0 (uL)GPC Cleanup: (Y/N) Y pH:

Contract:072-002-004

SAS No.: SDGNo.: MAI01

N

Lab Sample ID: 0308327-04Lab File ID: L0902021 .D

Date Received: 08/21/03Date Extracted: 08/25/03 __Date Analyzed: 09/02/03Dilution Factor: 1.0

CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG Q

[ 84-66-286-73-77005-72-3100-01-6534-52-186-30-6101-55-3118-74-11912-24-987-86-585-01-8120-12-786-74-884-74-2206-44-0129-00-085-68-7

""91-94:156-55-3218-01-9117-81-7

| 117-84-0205-99-2207-08-950-32-8-

, 193-39-5"*53-70-3191-24-2

! DiethylphthalateFluorene4-Chlorophenyi-phenylether4-Nitroaniline4,6-Dinitro-2-methylphenolN-Nitrosodiphenylamine4-Bromophenyl-phenyletherHexachlorobenzeneAtrazinePentachlorophenolPnenanthreneAnthraceneCarbazoleDi-n-butylphthatateFluoranthenePyrene

........_ Butylbenzylphthalate _._...._.__.,.„__...._._...3,3'-DichloroDenzidineBenzo[a]anthracene

i Chrysenebis(2-Ethylhexyl)phthalateD i-n -octy IphthalateBenzo[b]fluorantheneBenzo[k]fluorant!i6neBenzofa]pyrenelndeno[1 ,2,3-cd]pyreneDibenzo[a,h]anthraceneBenzo[g,h,ijpery!.ene . ._ .___.._..___.._.

410410410410410410

I 410410410410410

r 410410410410410410410410410

19000650410410410410410410

UUU

,UUUUUUUUUUUUUUUUUE

UUUUU

" U

FORM I SV-2

Page 12: Analytical data, SDG MAI01, soil samples received …MAI01 (g/ml) G decanted:(Y/N) (uL) N Lab Sample ID: 0308327-01 Lab File ID: L0902012.D Date Received: 08/21/03 _ Date Extracted:

1BSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

SAMPLE NO.

Lab Name: Laycks Testing LabsLab Code: _ Case No.:

Matrix: (soil/water) SOIL

Sample wt/vol: 15 _ (Q/ml) G_

Level: (low/med) LOW_

% Moisture: 18 decanted:(Y/N)

Concentrated Extract Volume: 500_ (uL)

Injection Volume: 2.0_ (uL)

GPC Cleanup: (Y/N) Y pH:

Contract:072-002-004DL

SAS No.: SDGNo.: MA101

N

Lab Sample ID: 0308327-04DLLab File ID: W903Q09.D_

Date Received: 08/21/03Date Extracted: 08/25/03

CAS NO. COMPOUND

Date Analyzed: 09/03/03

Dilution Factor: 5.0

CONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG

I 100-52-7108-95-2111-44-4

i 95-57-895-48-7108-60-198-86-2106-44-5621-64-767-72-1

I 98-95-3I 78-59-1! 88-75-5

165-67-9111-91-1

I 120-83-2! 91-20-3

106-47-887-68-3-Og_g— ' j

59-50-791-57-6 :77-47-488-06-295-95-4, ;92-52-4 '"- :

91-58-7 I88-74-4 l131-11-3 :

606-20-2 ;

208-96-8 i99-09-283-32-951-28-5 i100-02-7 !132-64-9 i121-14-2 i

BenzaidehydePhenolbis(2-Chloroethyl)ether2-Chlorophenol2-Methylphenol2,2'-oxybis(1-Chloropropane)Acetophenone4-MethylphenolN-Nitroso-di-n-propylamineHexachloroethaneNitrobenzeneIsophorone2-Nitrophenol2j4-Dimethylphenolbis(2-Chloroethoxy)methane2,4-DichlorophenolNaphthalene4-ChtoroanilineHexachlorobutadieneCaprolactam4-Chloro-3-methylphenol2-MethylnaphthaleneHexachlorocyclopentadiene2,4,6-Trichlorophenol2,4,5-Trichlorophenol1,1'-Biphenyl2-Chloronaphthalene2-NitroanilineDimethylphthalate2,6-DinitrotolueneAcenaphthylene3-NitroanilineAcenaphthene2,4-Dinitrophenol4-NitrophenolDibenzofuran2,4-Dinitrotoluene

200020002000200020002000"2000200020002000200020002000200020002000

I 20002000

i 2000r 2000

20002000200020002000200020002000200020002000200020002000200020002000

UUU

,uUUUUUUUUUuUuuuuuuuuuuuu

- uuuuuuuuuu

FORM I SV-1

Page 13: Analytical data, SDG MAI01, soil samples received …MAI01 (g/ml) G decanted:(Y/N) (uL) N Lab Sample ID: 0308327-01 Lab File ID: L0902012.D Date Received: 08/21/03 _ Date Extracted:

1CSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

SAMPLE NO.

Lab Name: Laucks Testing Labs __

Lab Code: Case No.: __Matrix: (soil/water) SOIL

Sample wt/vol: 15 (g/ml) G

Level: (low/med) LOW __

% Moisture: 18 decanted:(Y/N)

Concentrated Extract Volume: 500 (uL)

Injection Volume: 2.0 _ (uL)

GPC Cleanup: (Y/N) Y pH:

Contract:SAS No.:

072-002-004DL

SDGNo.: MAI01

N

Lab Sample ID: 0308327-04DL

Lab File tD: L0903009.DDate Received: 08/21/03Date Extracted: 08/25/03_ _

Date Analyzed: 09/03/03Dilution Factor: 5.0

GAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG

84-66-286-73-77005-72-3100-01-6534-52-186-30-6101-55-3118-74-11912-24-9

! 87-86-585-01-8120-12-786-74-884-74-2206-44-0129-00-085-68-791-94-156-55-3218-01-9117-81-7117-84-0205-99-2207-08-950-32-8,193-39-5"53-70-3191-24-2

DiethylphthalateFluorene4-Chlorophenyl-phenylether4-Nitroanlline4,6-Dinitro-2-methylphenolN-Nitrosodiphenylamine4-Bromophenyl-phenyletherHexachlorobenzeneAtrazinePentachlorophenol

I Phenanthrene ^AnthraceneCarbazoleDi-n-butylphthalateFluoranthenePyreneButylbenzylphthalate3,3'-DichlorobenzidineBenzo£a]anthraceneChrysenebis{2-Ethylhexyl)phthalateDi-n-octylphthalateBenzo[b]f1uorantheneBenzo[k)fluorantheneBenzo[ajpyrenelndeno[1 ,2,3-cdJpyreneDibenzofa,h]anthraceneBenzofa,h,i]perylene

2000 U2000 U2000 U2000 ,U2000 U2000 U2000 U2000 U2000 U2000 U2000 U2000 U

u 2000 U2606 u2000 U2000 U2000 U2000 U2000 U2000 U

22000 D800 JD

2000 U2000 U2000 U2000 U2000 i U2660" r u

FORM I SV-2

Page 14: Analytical data, SDG MAI01, soil samples received …MAI01 (g/ml) G decanted:(Y/N) (uL) N Lab Sample ID: 0308327-01 Lab File ID: L0902012.D Date Received: 08/21/03 _ Date Extracted:

1BSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

SAMPLE NO.

072-002-005Lab Name: Laucks Testing Labs ___ Contract:

Lab Code: _ Case No.: SAS No.: SDG No.: MAI01

Matrix: (soil/water)

Sample wt/vol:Level: (low/med)

% Moisture:

(g/ml) GSOIL _

15

LOW_

14 decanted:(Y/N)

Lab Sample ID: 0308327-05

Lab File ID: L0902010.D

Date Received: 08/21/03N

Concentrated Extract Volume: 500_

Injection Volume: 2.0 (uL)

GPC Cleanup: (Y/N) Y pH:

(uL)Date Extracted: 08/25/03

Date Analyzed: 09/02/03

Dilution Factor: 1.0

CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG Q

100-52-7108-95-2111-44-495-57-895-48-7108-60-198-86-2106-44-5621-64-767-72-198-95-378-59-188-75-5105-67-9111-91-1120-83-291-20-3106-47-887-68-3105-60-259-50-791-57-6;

! 77-47-4: 88-66=2

95-95-492-52-4 -

! 91-58-788-74-4131-11-3

I 606-20-2I 208-96-8 j

99-09-2 '83-32-9 :51-28-5 ;100-02-7 i132-64-9 !

1 121-14-2 i

BenzaldehydePhenolbis(2-Chloroethyl)ether2-Chlorophenol2-Methylphenol2,2'-oxybis{1 -Chloropropane)Acetophenone4-MethylphenolN-Nitroso-di-n-propylamineHexachloroethaneNitrobenzeneIsophorone2-Nitrophenol2,4-DimethyJphenolbis(2-Chloroethoxy)methane2,4-DichlorophenolNaphthalene4-ChloroanilineHexachlorobutadieneCapjolactam4-Chioro-3-methylphenol2-MethylnaphthaleneHexachlorocyclopentadiene2,4,6-Trichlorophenol2,4, 5-Trich loropjnenol1,1'-Biphenyl2-Chloronaphthalene2-NitroanilineDimethylphthalate2J3-DinitrotolueneAcenaphthylene3-NitroanilineAcenaphthene2,4-Dinitrophenol4-NitrophenolDibenzofuran2,4-Dinitrotoluene

390390390390390390390390390390390390390390390390390390390390390390390390390390390390390390390390390390390390390

UUUUUUUUUUUUUUUUUUUUUUUUUUU

- uUuuuuuuuu

FORM I SV-1

Page 15: Analytical data, SDG MAI01, soil samples received …MAI01 (g/ml) G decanted:(Y/N) (uL) N Lab Sample ID: 0308327-01 Lab File ID: L0902012.D Date Received: 08/21/03 _ Date Extracted:

1CSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

Lab Name: Laucks Testing Labs Contract:

Lab Code: __ Case No.: ____ SAS No.:Matrix: (soil/water) SOIL

Sample wt/vol: 15 (g/ml) G

Level: (low/med) LOW

% Moisture: 14 decanted:(Y/N) N

Concentrated Extract Volume: 500 (uL)

Injection Volume: 2.0 (uL)GPC Cleanup: (Y/N) Y pH:

SAMPLE NO.

072-002-005

SDGNo.: JMAK>1_

Lab Sample ID: 0308327-05Lab File ID: L0902p1IO.p

Date Received: 08/21/03Date Extracted: 08/25/03Date Analyzed: 09/02/03^Dilution Factor: 1.0

GAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG

84-66-286-73-77005-72-3100-01-6534-52-186-30-6

! 101-55-3i 118-74-1

1912-24-987-86-585-01-8120-12-786-74-884-74-2206-44-0129-00-0

| 85-68-7! 91-94-1

56-55-3218-01-9

I 117-81-7117-84-6

> 205-99-2207-08-950-32-8.,193-39-5'"- 153-70-3 i191-24-2

DiethylghthalateFluorene4-Chlorophenyl-phenylether4-Nitroaniline4,6-Dinitro-2-methylphenolN-Nitrosodiphenylamine4-Bromophenyl-phenyletherHexachlorobenzeneAtrazinePentachlorophenolPhenanthreneAnthraceneCarbazoleDi-n-butylphthalateFluoranthenePyreneButylbenzylphthalate3 L3'-DichlorobenzidineBenzo]a]anthraceneChrysenebis(2-Ethylhexyl)phthalateDi-n-octylphthalateBenzo[bjfluorantheneBenzo[k]fluorantheneBenzo[a]pyrenelndeno[1 ,2t3-cd]pyreneDibenzo[a,h]anthraceneBenzofg,h,i]perylene

390390390390390390390390390390390390390150390390390390390390230390390390390390390390

UuU

^uuuu •uuuuuu

JBuuuuuuJuuuuuu

- u

FORM I SV-2

Page 16: Analytical data, SDG MAI01, soil samples received …MAI01 (g/ml) G decanted:(Y/N) (uL) N Lab Sample ID: 0308327-01 Lab File ID: L0902012.D Date Received: 08/21/03 _ Date Extracted:

18SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

SAMPLE NO.

Lab Name: Laucks Testing LabsLab Code: Case No.:Matrix: (soil/water) SOILSample wt/vol: 2 (g/ml) GLevel: (low/med) MED

% Moisture: 12 decanted:(Y/N)Concentrated Extract Volume: 500 (uL)Injection Volume: 2.0 (uL)

GPC Cleanup: (Y/N) Y pH:

Contract:SAS No.:

072-002-006

N

SDGNo.: MAI01

Lab Sample ID: 0308327-06Lab File ID: Lp9p2015.D

Date Received: 08/21/03Date Extracted: 08/26/03Date Analyzed: 09/02/03Dilution Factor: 1.0

GAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG Q

100-52-7108-95-2111-44-495-57-895-48-7108-60-198-86-2106-44-5621-64-767-72-198-95-378-59-188-75-5105-67-9111-91-1120-83-291-20-3106-47-887-68-3105-60-259-50-791-57-677-47-488-06-295-95-492-52-491-58-788-74-4131-11-3606-20-2208-96-899-09-2 ]83-32-951-28-5100-02-7132-64-9121-14-2 :

BenzaldehydePhenolbis(2-Chloroethy|)ether2-Chlorophenol2-Methylphenol2,2'-pxybis(1-Chlprpprppane)Acetophenone4-MethylphenolN-Nitroso-di-n-propylarnineHexachloroethaneNitrobenzeneIsophorone2-Nitrophenol2,4-Dimethylphenolbis(2-Chloroethoxy)methane2,4-DichlorophenolNaphthalene4-ChloroanilineHexachlorobutadieneCaprolactam4-Chloro-3-methylphenol2-MethylnaphthajeneHexachlorocyclopentadiene2,4,6-Trichlorophenol2,4t5-Trichlorophenol1,1'-Bipnenyl2-Chloronaphthalene2-NitroanilineDirnethylphthalate2,6-DinitrotolueneAcenaphthylene3-NitroanilineAcenaphthene2,4-Dinitrophenol4-Nitrophenol !Dibenzofuran2,4-Dinitrptpluene _ __._._

2800 U2800 U2800 U2800 U2800 U2800 U2800 U

r 2800 U2800 U2800 U2800 U2800 jj2800 U2800 U2800 ! U2800 I U2800 I U2800 U"2800 U2800 U2800 U2800 j U |2800 ! U2800 U2800 U2800 U i2800 U2800 U2800 U2800 U2800 U2800 U2800 I U2800 i U2800 ! U2866 11 U2800 \ U

FORM I SV-1

Page 17: Analytical data, SDG MAI01, soil samples received …MAI01 (g/ml) G decanted:(Y/N) (uL) N Lab Sample ID: 0308327-01 Lab File ID: L0902012.D Date Received: 08/21/03 _ Date Extracted:

1CSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

SAMPLE NO.

Lab Name: Laucks Testing Labs

Lab Code: Case No.:Matrix: (soil/water) SOIL

Sample wt/voi: 2 (g/ml) GLevel: (low/med) MED

% Moisture: 12 decanted:{Y/N)Concentrated Extract Volume: 500 (uL)

Injection Volume: 2.0 (uL)

GPC Cleanup: (Y/N) Y pH:

Contract:

SAS No.:

072-002-006

N

SDGNo.: MAI01Lab Sample ID: 0308327-06Lab File ID: 1.0902015.0

Date Received: 08/21/03

Date Extracted: 08/26/03Date Analyzed: 09/02/03

Dilution Factor: 1.0

CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG Q

I 84-66-2i 86-73-7

7005-72-3i 100-01-6! 534-52-1'• 86-30-6; 101-55-3! 118-74-1! 1912-24-9

87-86-585-01-8

i 120-12-7I 86-74-8

84-74-2206-44-0129-00-0

i 85-68-7! 91-94-1

56-55-321g_Q1_g

i 117-81-7! 117-84-0

205-99-2; 207-08-9! 50-32-8i 193-39-5

53-70-3191-24-2

piethylphthalateFluorene4-Chlorophenyl-phenyletherl:y)ACpanJiLQe .4,6-Dinitro-2-methylphenolN-Nitrosodiphenylamine4-Bromophenyl-phenyletherHexachlorobenzeneAtrazinePentachlorophenolPhenanthreneAnthracene

! CarbazoleDi-n-buty!phthalateFluoranthene

; Pyrenei Butylbenzylphthalate

3,3'-Dichlorobenzidinej Benzq[a]anthracene; Chrysene! bis(2-Ethylhexyliphthalatei Di-n-octylphthalateI Benzofbjfluoranthene; Benzo[k]fluoranthene

........ i Benzplajpyrene! lndeno[1,2,3-cdipyrene; Dibenzo[a,h]anthracene

Benzolg,h,i]perylene

j 2800 [ U2800 U2800 U2800 U2800 U2800 U2800 U2800 U2800 [ U2800 U !2800 U2800 U2866 U2800 U2800 U2800 U2800 U2800 U2800 U2800 U800 J ""]

2800 U j2800 U2800 U2800 U2800 U2866 U I2800 i U

FORM I SV-2

Page 18: Analytical data, SDG MAI01, soil samples received …MAI01 (g/ml) G decanted:(Y/N) (uL) N Lab Sample ID: 0308327-01 Lab File ID: L0902012.D Date Received: 08/21/03 _ Date Extracted:

1BSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

Laucks Testing Labs Contract:

SAMPLE NO.

Lab Name:Lab Code: Case No.: _____

Matrix: (soil/water) SOIL

Sample wt/voi: 15 (g/ml) GLevel: (low/med) LOW

% Moisture: 11 decanted:(Y/N)

Concentrated Extract Volume: 500 _ (uL)

Injection Volume: 2.0 (uL)

GPC Cleanup: (Y/N) Y pH:

072-002-007

N

SAS No.: ___ SDG No.: MAI01

Lab Sample ID: 0308327-07Lab File ID: L0902019.D_Date Received: 08/21/03Date Extracted: 08/25/03Date Analyzed: 09/02/03

Dilution Factor: 1.0

CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG

100-52-7108-95-2111-44-495-57-8

| 95-48-7108-60-198-86-2106-44-5621-64-767-72-198-95-378-59-188-75-5105-67-9111-91-1120-83-291-20-3106-47-887-68-3105-60-259-50-791-57-677-47-488-06-295-95-4,92-52-4 x~91-58-788-74-4131-11-3606-20-2208-96-899-09-283-32-951-28-5100-02-7132-64-9121-14-2

BenzaldehydeI Phenol! bis(2-Chloroethyl)ether

2-Chtorophenol2-Methylphenol

I 2,2'-oxybis(1-Chloropropane)! AcetophenoneI 4-MethylphenolI N-Nitroso-di-n-propylamine

HexachloroethaneNitrobenzene

! Isophorone2-Nitrophenol2,4-Dimethylphenolbis(2-Chloroethoxy)methane

• 2,4-Dichlorophenol: Naphthalene

4-ChloroanilineI Hexachlorobutadiene

Caprolactam: 4-Chloro-3-methylphenol\ 2-Methylnaphthalene! Hexachlorocyclopentadiene

2 ,4,6-Trichlorophenol2,4,5-Trichlorophenol

; 1,1'-Biphenyl2-Chloronaphthalene2-NitroanilineDirnethylphthatate2,6-DinitrotolueneAcenaphthylene

i 3-Nitroanilinej Acenaphthenei 2,4-Dinitrophenol: 4-Nitrophenol

Dibenzofuran: 2,4-Dinitrotoluene

370370370370370370370370370370

I 370370370370370370370370370370370370370370370370370370370370370 1370 J370 '370370370370

UU

1 U, U

UUUUUUUUr u

™u —uuuuuuuuuuuuu

" Uuuuuuuuuu

FORM I SV-1

Page 19: Analytical data, SDG MAI01, soil samples received …MAI01 (g/ml) G decanted:(Y/N) (uL) N Lab Sample ID: 0308327-01 Lab File ID: L0902012.D Date Received: 08/21/03 _ Date Extracted:

Lab Name:

Lab Code:

1CSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

Laucks TestingJ_abs ___ _ Contract: ___ _

Case No.: SAS No.:

SAMPLE NO.

072-002-007

SDGNo.: MAI01Matrix: (soil/water) SOIL

Sampie wt/vol: 15 (g/ml) G_Level: (low/med) LOW _

% Moisture: 11 decanted:(Y/N)

Concentrated Extract Volume: 500 (uL)

Injection Volume: 2.0 (uL)

GPC Cleanup: (Y/N) Y pH:

Lab Sample ID: 0308327-07

Lab File ID: L0902p19:DDate Received: 08/21/03

N Date Extracted: 08/25/03

Date Analyzed: 09/02/03Dilution Factor: 1.0

GAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG Q

84-66-286-73-77005-72-3100-01-6534-52-186-30-6101-55-3

[ 118-74-11912-24-987-86-585-01-8120-12-786-74-884-74-2206-44-0129-00-085-68-791-94-156-55-3218-01-9117-81-7117-84-0:205-99-2207-08-950-32-81 93-39-5 v-53-70-3191-24-2

j DiethylphthalateI Fluorene! 4-Chlorophenyl-phenylether! 4-Nitroaniline! 4,6-Dinitro-2-methylphenoli N-Nitrosodiphenylamine

4-BromophenyI-phenyletheri Hexachlorobenzene! Atrazine

Pentachlorophenol; PhenanthreneI Anthracene< Carbazole'• Di-n-butylphthalatei Fluoranthene

...... i Pjffene. __„„.,_ _ ... _ . _' Butylbenzylphthalate; 3,3'-Dichlorobenzidinei Benzo|a]anthracene! Chrysene

bis(2-EthylhexyJ)phthalate\ Di-n-octyjphthalate• Benzo[b]fluoranthenei Benzo[k]fiuoranthenei Benzo[a]pyrenei IndenoII S-cdlpyrene

Dibenzolajhjanthracene; Benzo[g,h,i]perylene

110370370370370370370370370370370370370280370370370370370370780370370370370370370370

JBUU

^uUUUUUU

i UUUJBUUUUUU

UUUUUU

- u

FORM I SV-2

Page 20: Analytical data, SDG MAI01, soil samples received …MAI01 (g/ml) G decanted:(Y/N) (uL) N Lab Sample ID: 0308327-01 Lab File ID: L0902012.D Date Received: 08/21/03 _ Date Extracted:

1BSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

SAMPLE NO.

Lab Name: Laucks Testing Labs ______Lab Code: _ Case No.:Matrix: (soil/water) SOIL_

Sample wt/vol: 15 (9/ml) G

Level: (low/rned) LOW

% Moisture: 11 decanted:(Y/N)

Concentrated Extract Volume: 500 (uL)Injection Volume: 2.0 (uL)

GPC Cleanup: (Y/N) Y pH:

Contract:

SAS No.:

072-002-010

SDGNo.: MAI01

Lab Sample ID: 0308327-08

Lab File ID: L0902020.D

N

CAS NO. COMPOUND

Date Received: 08/21/03Date Extracted: 08/25/03

Date Analyzed: 09/02/03

Dilution Factor: 1.0

CONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG_

j 100-52-7I 108-95-2! 111-44-4I 95-57-8! 95-48-7i 108-60-1I 98-86-2| 106-44-5i 621-64-7j 67-72-1i 98-95-3| 78-59-1! 88-75-5i 105-6>-9I 111-91-1i 120-83-2' 91-20-3: 106-47-8! 87-68-3

105-6~6-2i 59-50-7i 91-57-6 -:i 77-47-4' 86-06-2 ''! 95-95-4i 92-52-4 "--i 91-58-7i 88-74-4! 131-11-3\ 606-20-2

208-96-8i 99-09-2

83-32-9: 51-28-5; 100-02-7! 132-64-9'

121-14-2

BenzaldehydePhenolbis{2-Chloroethyl)ether2-Chlorophenol2-Methylphenol2,2'-oxybis(1-Chloropropane)Acetophenone4-MethylphenolN - N itroso-di-n-propylamin eHexachloroethaneNitrobenzeneIsophorone2-Nitrophenol2 ,4-Dimethylphenolbis(2-Chloroethoxy)methane2J4-DichlorophenolNaphthalene4-ChloroanilineHexachlorobutadieneCaprolactam4-Chloro-3-methylphenol2-MethylnaphthaleneHexachlorocyclopentadiene2,4,6-Trichlorophenol^^S-Trichlorophenol1,1'-Biphenyl2-Chloronaphthalene2-NitroanilineDimethylphthalate2,6-DinitrotolueneAcenaphthylene3-NitroanilineAcenaphthene2,4-Dinitrophenol4-NitrophenolDibenzofuran2,4-Dinitrotoluene

370370370370

1 370370370370370370370370370370370370370370

r~ 370370370370370370370370370370370370370370370370370 ,370370

UUU

, UUUUUUUU _iUUUUuUuuuuuuuuu 1u

- uuuuU juuuuu

FORM I SV-1

Page 21: Analytical data, SDG MAI01, soil samples received …MAI01 (g/ml) G decanted:(Y/N) (uL) N Lab Sample ID: 0308327-01 Lab File ID: L0902012.D Date Received: 08/21/03 _ Date Extracted:

1CSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

SAMPLE NO.

Lab Name: Laucks Testing Labs __Lab Code: Case No.:Matrix: (soil/water) SOIL

Sample wt/vol: 15 (g/ml) G

Level: (low/med) L°W

% Moisture: 11 decanted:(Y/N)

Concentrated Extract Volume: 500 (uL)

Injection Volume: 2.0 (uL)GPC Cleanup: (Y/N) Y pH:

Contract:SAS No.:

072-002-010

SDG No.: MAI01

N

Lab Sample ID: 0308327-08Lab File ID: L0902020.D

Date Received: 08/21/03

Date Extracted: 08/25/03

CAS NO. COMPOUND

Date Analyzed: 09/02/03

Dilution Factor: 1.0

CONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG Q

84-66-286-73-7

L 7005-72-3100-01-6534-52-186-30-6

, 101-55-3I 118-74-1

1912-24-987-86-585-01-8120-12-786-74-884-74-2266-44-0129-00-085-68-7

, 91-94-156-55-3218-01-9117-81-7117-84-6265-99-2207-08-950-32-8193-39-5 -53-70-3 i191-24-2 I

DiethylpnthalateFluorene4-Chloropheny!-phenylether4-Nitroaniline4,6-Dinitro-2-methylphenolN-Nitrosodiphenylamine4-Bromopher>yl-phenyletherHexachlorobenzeneAtrazinePentachlorophenolPhenanthreneAnthraceneCarbazoleDi-n-butylphthalateFtuoranthenePyreneButylbenzylphthalate3,3'-DichlorobenzidineBenzo[a]anthraceneChrysenebis(2-Ethylhexyl)phthalateDi-n-octylpjithalateBenzo[b]fluorantneneBenzo[klfluorantheneBenzo[a]pyrenelndeno{1 ,2.3-cd]pyreneDibenzo[a,h]anthraceneBenzoIg.hJlperylene ___

370 U370 U370 U370 3U370 U370 U I370 U370 U370 1 U370 U370 U370 U370 U100 JB370 ~1~ U370 U370 I U370 I U370 U370 U600370 U370 U370 U370 U370 U370 U370 I" U J

FORM I SV-2

Page 22: Analytical data, SDG MAI01, soil samples received …MAI01 (g/ml) G decanted:(Y/N) (uL) N Lab Sample ID: 0308327-01 Lab File ID: L0902012.D Date Received: 08/21/03 _ Date Extracted:

18SEMIVOLATiLE ORGANICS ANALYSIS DATA SHEET

SAMPLE NO.

Lab Name: Laucks Testing Labs _

Lab Code: Case No.:

Matrix: (soil/water) SOIL

Sample wt/vol: 2 _ (g/rnl) G_

Level: (low/med) MED

% Moisture: 10 decanted:(Y/N)

Concentrated Extract Volume: 500 (uL)

Injection Volume: 2.0 (uL)

GPC Cleanup: (Y/N) Y pH:

Contract:SAS No.:

072-002-008

SDGNo.: MAI01

N

Lab Sample ID: 0308327-09

Lab File ID: L09030Q5.D

Date Received: 08/21/03

Date Extracted: 08/26/03

Date Analyzed: 09/03/03

Dilution Factor: 1.0

CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG Q

i 100-52-7108-95-2

| 111-44-495-57-8

r 95-48-7108-60-1

I 98-86-2106-44-5621-64-767-72-198-95-378-59-188-75-5105-67-9111-91-1120-83-291-20-3106-47-887-68-3105-60-259-50-791-57-6 ,77-47-488-06-295-95-492-52-4 x-91-58-788-74-4131-11-3606-20-2208-96-899-09-283-32-951-28-5100-02-7132-64-9121-14-2

BenzaldehydePhenolbis(2-Chloroethyl)ether2-Chlorophenol2-Methylphenol2,2'-oxybis(1-Chloropropane)Acetophenone4-MethylphenolN-Nitroso-di-n-propylamineHexachloroethaneNitrobenzeneIsophorone2-Nitropjienol2,4-Dimethylpheno!bis(2-Chloroethoxy)methane2,4-DichlorophenolNaphthalene4-ChloroanilineHexachlorobutadieneCaprolactam4-Chloro-3-methylphenol2-MethylnaphthaleneHexachlorocyclopentadiene2 ,4 ,6-Trichlorophenol2,4,5-Trichlorophenol1,1'-Btphenyl2-Chloronaphthalene2-NitroanilineDimethylphthalate2,6-DinitrotolueneAcenaphthylene3-NitroanilineAcenaphthene2,4-Dinitrophenol4-NitrophenolDibenzofuran2,4-Dinitrotoluene

2800280028002800280028002800280028002800280028002800280028002800280028002800280028002800280028002800280028002800280028002800280028002800280028002800

UUU

^UUUUUUUUUUUU

I U

UUUUUUU 1UU JUU

- uU~Ju Iuuuuuuu

FORM I SV-1

Page 23: Analytical data, SDG MAI01, soil samples received …MAI01 (g/ml) G decanted:(Y/N) (uL) N Lab Sample ID: 0308327-01 Lab File ID: L0902012.D Date Received: 08/21/03 _ Date Extracted:

1CSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

SAMPLE NO.

072-002-008Lab Name: Laucks Testing Labs _____ Contract:Lab Code: Case No.: ____ SAS No.: _ _ SDG No.: MAI01Matrix: (soil/water)

Sample wt/vol:Level: (low/med)

% Moisture:

SOIL __

.2.__„..... (g/ml) G_MED

10 decanted:(Y/N)

Lab Sample ID: 0308327-09

Lab File ID: JrP_9030°Date Received: 08/21/03

N Date Extracted: 08/26/03Concentrated Extract Volume: 500

Injection Volume: 2.0 (uL)

GPC Cleanup: (Y/N) Y pH:

(uL)

CASNO. COMPOUND

Date Analyzed: 09/03/03Dilution Factor: 1.0

CONCENTRATION UNITS:{ug/L or ug/Kg) UG/KG

84-66-286-73-7

! 7005-72-3100-01-6534-52-1

j 86-30-6| 101-55-3i 118-74-1f 1912-24-9' 87-86-5

85-01-8120-12-786-74-884-74-2206-44-0129-00-085-68-791-94-156-55-3218-01-9117-81-71 1 7-84-0.205-99-2207-08-950-32-8193-39-5"-

i 53-70-3191-24-2

DiethyiphthalateFluorene4-Chlorophenyl-phenylether4-Nitroaniline4,6-Dinitro-2-methylphenolN-Nitrosodiphenylamine4-Bromophenyl-phenyletherHexachlorobenzeneAtrazinePentachlorophenolPhenanthreneAnthraceneCarbazoleDi-n-butylphthalateFluoranthenePyreneButylbenzylphthalateSjS'-DichlorobenzidineBenzo[ajanthraceneChrysenebis(2-Ethylhexyl)phthalateDi-n-octyfphthalateBenzo[blfluorantheneBenzofk]fluorantheneBenzo[a]pyrenelndeno[1 ,2,3-cd]pyreneDibenzo[afh]anthraceneBenzo[q,h,i]perylene

8602800280028002800280028002800280028002800280028002800280028002800280028002800

6302800280028002800280028002800

JUU

,UUUUUUUUUUUUUUUUUJUUUUUU

• u

FORM I SV-2

Page 24: Analytical data, SDG MAI01, soil samples received …MAI01 (g/ml) G decanted:(Y/N) (uL) N Lab Sample ID: 0308327-01 Lab File ID: L0902012.D Date Received: 08/21/03 _ Date Extracted:

18SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

Laucks Testing Labs______ Contract:, ___

SAMPLE NO.

Lab Name:Lab Code: __ Case No.:Matrix: (soil/water) SOIL

Sample wt/vol: 15 __ (9/rnl) GLevel: (low/med) LOW ___

% Moisture: 12 decanted:(Y/N)

Concentrated Extract Volume: 500 (uL)Injection Volume: 2.0 (uL)

GPC Cleanup: (Y/N) Y pH:

072-002-009

SAS No.: SDGNo.: MAI01

Lab Sample ID: 0308327-10Lab File ID: L0902011.D

Date Received: 08/21/03N Date Extracted: 08/25/03

Date Analyzed: 09/02/03Dilution Factor: 1.0

CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG Q

I 100-52-7108-95-2

! 111-44.4t 95-57-8

95-48-7t 108-60-1! 98-86-2! 106-44-5I 621-64-7| 67-72-1i 98-95-3

78-59-188-75-5105-67-9111-91-1120-83-291-20-3106-47-887-68-3105-60-259-50-791-57-6 :77-47-488-06-295-95-492-52-4 "--91-58-788-74-4131-11-3606-20-2208-96-899-09-283-32-951-28-5100-02-7132-64-9121-14-2

! Benzaldehydei Phenolj bis(2-Chloroethyl)etherI 2-Chlorophenol! 2-Methylphenol• 2,2'-oxybis(1-Chloropropane)

Acetophenone4-MethylphenolN-Nitroso-di-n-propylamineHexachloroethaneNitrobenzeneIsophorone2-Nitrophenol

: 2,4-Dimethylphenol; bis(2-Chloroethoxy)methanei 2,4-Dichlorophenol

Naphthalene! 4-Chloroaniline

HexachlorobutadieneCaprolactam4-Chloro-3-methylphenol

! 2-Methylnaphthalene' Hexachlorocyclopentadiene

2j4i6-Trichlorophenol2,4,5-Trichlorophenol1.1'-Biphenyl2-Chloronaphthalene

', 2-Nitroaniline; Dimethylphthalate: 2,6-Dinitrotoluenei AcenaphthyleneI 3-NitroanilineI Acenaphthenei 2,4-Dinitrophenol\ 4-Nitrophenol! Dibenzofuran: 2J4-Dinitrotoluene

380 T~ U380 | U380 U380 _U380 U380 U380 U380 U380 U380 U380 U380 U380 U380 U380 U380 U380 U ~~*380 U380 U380 I U380 U380 U380 U380 U380 U380 U380 U380 - U380 U380 U380 U380 U380 U380 U380 U380 U380 U

FORM I SV-1

Page 25: Analytical data, SDG MAI01, soil samples received …MAI01 (g/ml) G decanted:(Y/N) (uL) N Lab Sample ID: 0308327-01 Lab File ID: L0902012.D Date Received: 08/21/03 _ Date Extracted:

1CSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

SAMPLE NO.

Lab Name: Laucks T®.?l!n.9.J l5..-.. ____Lab Code: _ Case No.: __Matrix: (soil/water) SOIL_ _

Sample wt/vol: 15_ _ (g/ml) G

Level: (low/med) LOW% Moisture: 12. decanted:(Y/N)

Concentrated Extract Volume: 500 (uL)Injection Volume: 2.0 (uL)GPC Cleanup: (Y/N) Y pH:

Contract:072-002-009

SAS No.: ___ SDG No.: MAI01

Lab Sample ID: 0308327-10Lab File ID: L0902011.D

Date Received: 08/21/03

N

CAS NO. COMPOUND

Date Extracted: 08/25/03Date Analyzed: 09/02/03Dilution Factor: 1.0

CONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG

84-66-286-73-77005-72-3100-01-653452-186-30-6

"101-55-3118-74-11912-24-987-86-585-01-8120-12-786-74-884-74-2206-44-0129-00-685-68-791-94-156-55-3218-01-9117-81-7117-84-0. 4

205-99-2207-0&950-32-8193-39-5 -53-70-3191-24-2

DiethylphthalateFluorene4-Chlorophenyl-phenylether4-Nitroaniline4,6-Dinitro-2-methylphenolN-Nitrosodiphenylamine4-Bromophenyl-phenyletherHexachlorobenzeneAtrazinePentachlorophenolPhenanthreneAnthraceneCarbazoleDi-n-butylphthalateFluoranthenePyreneButylbenzylpjithalate3,3'-DichlorobenzidineBenzojajanthraceneChrysenebis(2-Ethylhexyl)phthalateDi-n-octylphthalateBenzoMfiuorantheneBenzofk]fluorantheneBenzgjalpyrenelndeno[1 ,2,3-cdJp.yreneDibenzofa,h|anthraceneBenzp[g1h,i]pe.ryjene ....._ ..,„_.._. .. _,

140380380380380380380380380380380380

* 380190380380380 "*380380380

r 110380380380380380380380

JB' U

u-,uuu

I UU 1uuuuu

JBUU ]uuuuJuuuuu •

, U |

- u

FORM I SV-2