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Analysis of Frack Water By Kiersten Briggs and Schuyler Mincemoyer
12

Analysis of Frack Water

Feb 24, 2016

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Alvaro Federico

By Kiersten Briggs and Schuyler Mincemoyer. Analysis of Frack Water. Objective. An organic analysis of the effects of hydraulic fracturing on well water through GC-MS and FT-IR . - PowerPoint PPT Presentation
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Page 1: Analysis  of  Frack  Water

Analysis of Frack WaterBy Kiersten Briggs and Schuyler Mincemoyer

Page 2: Analysis  of  Frack  Water

Objective An organic analysis of the effects of

hydraulic fracturing on well water through GC-MS and FT-IR.

After GC-MS and FT-IR results were found, we also proceeded to run an XRF analysis to determine the metal and alloy makeup of the frack water.

Page 3: Analysis  of  Frack  Water

What is Hydraulic Fracturing? Drilling technique widely utilized for

collecting Natural Gas Energy from injecting highly-pressurized

fracking fluid cracks rocks to release gas Drilling occurs ~6,200 ft below the

surface Can produce fracturing at least 1,000-

1,500 ft away from the initial pressurization point

Page 4: Analysis  of  Frack  Water

What is Hydraulic Fracturing?

Page 5: Analysis  of  Frack  Water

What is Frack Water? Caused by Hydraulic Fracturing for

Natural Gas Well water speculated to be

contaminated by fracking fluid byproducts

http://www.youtube.com/watch?v=dZe1AeH0Qz8

Page 6: Analysis  of  Frack  Water

Suspected Contaminants We are testing for 5 out of a possible 353 dangerous components of fracking fluid

(632 total components) Xylene Benzene Ethylbenzene Naphthalene Toluene

Page 7: Analysis  of  Frack  Water

Procedure Extract components from water using

Separatory Funnel and Hexane Also attempted using Methylene

Chloride for extraction Run organic layer through the GC-MS

and FT-IR Standard Samples were mixed with

hexane and run through each instrument as a reference point

Page 8: Analysis  of  Frack  Water

Results GC-MS and FT-IR showed no benzene,

ethyl benzene, toluene, xylene, or naphthalene present.

An XRF analysis showed that of the metals/alloys in the water, 60% was Sulfur. The other 40% was Silica.

Page 9: Analysis  of  Frack  Water

Conclusions The benzene derivatives we tested for

were not present. Probable causes: Present in extremely low

concentrations Did not have a good water sample for

testing Gas samples may have left the

sample before testing

Page 10: Analysis  of  Frack  Water

Conclusions The XRF showed a surprising result with

60% sulfur contents within the Frack Water. Sulfur is present in the shale they

fracture during hydraulic fracturing Sulfur and CO2 are a byproducts of

processing natural gas

Page 11: Analysis  of  Frack  Water

For further studies

http://www.youtube.com/watch?v=4LBjSXWQRV8

Shows the breaks in the water from the tap system where the fire lights. Leads to a question of a gas trapped in the pipes, rather than a contaminant of the water itself.

Page 12: Analysis  of  Frack  Water

Questions?