Achillion Pharmaceuticals, Inc., Termination Request Ltr ...copy of the sewer disposal records for the long-lived isotopes (H-3 an~f C-14) disposed are attached. Regarding records

~- -_

"' ACHILLION -RESEARCH REALIZED_

November 11, 2019

Licensing Assistant Section Nuclear Safety Branch U.S. Nuclear Regulatory Commission, Region I 2100 Renaissance Boulevard, Suite 100 King of Prussia, PA 19406-2713

Re: Terrmnation of Materials License# 06-30628~01

To Whom it May Concern:

. www.achillion.com

RECRG11114'19AM05:39 .. --~-5

03035~70

I am writing to inform you that Achillion Pharmaceuticals, Inc. (Achillion) has decided to terminate radioactive materials license number 06-30628-01. Radioactive materials _used at and/or by Achillion ceased on October 30, 2019. Achillion no longer possesses any radioactive materials. A completed NRC form 314, "Certification of Disposition of Materials" and the associated radioactive waste manifest showing the proper -disposal of our remaining licensed material are attached.

No licensed radioactive materials were disposed of pursuant to 10 CFR 20.2002, 20.2004 or 20.2005. No evaluations of effluent releases were made pursuant to 20.2103 (b)(4).

Licensed radioactive materials were disposed of to the sanitary sewer system pursuant to 10 CFR 200.2003. A copy of the sewer disposal records for the long-lived isotopes (H-3 an~f C-14) disposed are attached.

Regarding records related to 10 CFR 30.35(g), there were no documented_ spills or contamination of the facility. There were no restricted areas at the facility and no known areas of inaccessible _contamination. Achillioii als_o never possessed quantities of radioactive material requiring a decommissioning funding plan.

Achillion contracted Radcor, LLC of Salem, Connecticut to perform a radiological survey of all areas where licensed radioactive materials_ had been used an/or stored over the years. A copy of this report is enclosed. ·

Should you have any questions regarding this license termination request, please contact Steven Podos, Ph.D., our current Radiation Safety Officer, at (203) 752-5458 or at [email protected].

Sincerely,

d of Research

Enclosures (4) 1. NRC Form 314-Certificate of Disposal of Materials 2. NRC Form 540-Uniform Low-Level Radioactive Waste Manifest 3. Sewer disposal records 4. Radiological Decommissioning Report, dates October 21, 2019

Achillion Pharmaceutica_ls, Inc. 300 George Street New Haven, CT 06_511

~\7JiJ· NMS8/RGN1 MP.TERIAl8°002

main 203.624.7000 fax 203.752.5454

NRC FORM 314 <,\.~\\JtEayl.., U.S. NUCLEAR REGULATORY COMMISSION APPROVED BY 0MB: NO. 3150-0028 EXPIRES: 02/29/2020 (02-2017) +.;, >o 10 CFR 30.360)(1 ); I,) '"°#~ Estimated burden per response to comply with this mandatory collection request: 30 minutes. This submittal is used by

~ " 40.420)(1 ); 70.380)(1 ); .. 0 CERTIFICATE OF DISPOSITION NRC as part of the basis for its determination that the facility is released for unrestricted use. Send comments regarding

and 72.54(k)(5)(1)(1) ~ : burden estimate to the FOIA, Privacy, and Information Co!Iections Branch (T-5 F53), U.S. Nuclear Regulatory Commission, ~ ~

OF MATERIALS Washington, DC 20555-0001, or by e-mail lo [email protected], and to the Desk Officer, Office of Information

~1,o,,. ~o,fj and Regulatory Affairs, NEOB-10202, (3150-0028), Office of Management and Budge!, Washington, DC 20503. If a

****"" means used to impose an information collection does not display a currently valid 0MB oontrol number, the NRC may not conduct or sponsor, and a person is not required to respond to, the information collection.

LICENSEE NAME AND ADDRESS LICENSE NUMB~R DOCKET NUMBER

Achillion Pharmaceuticals, Inc. 300 George Street

06-30628-01 030-35670

New Haven, CT 06511 LICENSE EXPIRATION DATE

April 30, 2021

A. LICENSE STATUS (Check the appropriate box)

D This license has expired. [Z] This license has not yet expired; please terminate it.

B. DISPOSAL OF RADIOACTIVE MATERIAL (Check the appropriate boxes and complete as necessary. If additional space is needed, provide attachments)

The licensee, or any individual executing this certificate on behalf of the licensee, certifies that:

D 1. No radioactive materials have ever been procured or possessed by the licensee under this license.

0 2. All activities authorized by this license have ceased, and all radioactive materials procured and/or possessed by the licensee under this license number cited above have been disposed of in the following manner.

D a. Transfer of radioactive materials to the licensee listed below:

[{]b. Disposal of radioactive materials:

D 1. Directly by the licensee:

D 2. By licensed disposal site:

[{]3. By waste contractor: I

Chase Environmental Group, Inc. 11450 Watterson Court, Louisville KY 40299 ( 665)250-4593

[Z]c. All radioactive materials have been removed such that any remaining residual radioactivity is within the limits of 10 CFR Part 20, Subpart E, and is ALARA.

C. SURVEYS PERFORMED AND REPORTED

0 1. A radiation survey was conducted by the licensee. The survey confirms:

[Z]a. the absence of licensed radioactive materials

[{]b. that any remaining residual radioactivity is within the limits of 10 CFR 20, Subpart E, and is ALARA.

[Z] 2. A copy of the radiation survey results:

[Z] a. is attached; or D b. is not attached (Provide explanation); or D c. was forwarded to NRG on:

D 3. A radiation survey is not required as only sealed sources were ever possessed under this license, and Date

D a. The results of the latest leak test are attached; and/or D b. No leaking sources have ever been identified.

The person to be contacted regarding the information provided on this form: NAME TITLE TELEPHONE (Include Area Code) E-MAIL ADDRESS

Steven Podos, Ph.D. Radiation Safety Officer 203-752-5458 [email protected]

Mail all future correspondence regarding this license to:

Achillion Pharmaceuticals, Inc. 300 George Street New Haven, CT 06511

C. CERTIFYING OFFICIAL I CERTIFY UNDER PENALTY OF PERJURY THAT THE FOREGOING IS TRUE AND CORRECT

PRINTED NAME AND TITLE

SIGNAJ~yj: ~r/ DATE

Mingjun Huang, Ph.D., Senior VP, Head of Research 11/11/1~ WARNING: FALSE STATEMENTS IN THIS CERTIFICATE MAY BE SUBJECT TO CIVIL i D(~R CRUii i) ALP •N ~LTIES. NRC REGULATIONS REQUIRE THAT SUBMISSIONS TO THE NRC BE COMPLETE AND ACCURATE IN ALL MATERIAL RESP T. 8 U.S.C. SECT 0 ~ 1001 MAKES IT A CRIMINAL OFFENSE TO MAKE A WILLFULLY FALSE STATEMENT OR REPRESENTATION TO ANY DEPARTMENT OR A NCY OF THE UNIT~[ STATES AS TO ANY MATIER WITHIN ITS JURISDICTION .

NRG FORM 314 (02 2017) •

HIICFORU~ !I. SHIPPfR• IWIE ANO l'ACIUtY SHIPPER ID• ..:,ica, ... -o.- PMle I _,_PMIE(II L l.bn!ml,.._

Chi .. -~-NI,\ MIICfCallllolllflO&,.li OF _t_P~ 1.1M ,._,..., .. _._._ ..... ,

UNIFORM LQW-UVl!L RAOIOACJM; 11450 Wat!mon Court X len..uc.,. NC~IGIIGMM --1...J'AGE(I)

WASTE MAHlfEST loullvllle, KY 40299 ~ -- lb>LJ'.<Glell T0.2019-:133

lff!rl'lflOPN'llll ...... _ ...... , ......... ---- . ..._. __ ,..,.,..,.......,

Cat!lcl

1 llll.JiNWCT 11U1tOa auacwcum ~ a::itlrJ T-KYIJOJ.L 111 W,\ TOXCO, Inc:. Ricki.aw iaoo,.c74.11300 .:[JflfM:f -· 109 Fl!nt Road ,....,._11ra.11o ..... ma1 -- .la1101Saur Mr..2$l-4511) Oalt Rk1aa TN 37830 8ISS-4B2-5532

CHEMTREC W5D5 I: CHEHOIRAD C11atamar I: 43115 14. ~IUI IW,IE Nm /IDORESS EP~ID• ~""' ................ ~-,__ µam ·---~~ ' l'DfM. NalllA O" SJ Tnm,ponalion Co., Inc. NJD07111299711

I I YES ~u.wma, 2 PO Boll 189 iw-a.11. 10. CMillCallon

lxl NO '"'-- Woodslawn NJ D80ll8 1DIJ0/20111 [Tlalol>-DIIIN_,_.,........,..,.,...,_, _ _,,_ i. ..... .......a JVES ... _............,. ~,'Cf ,m.a,oe• ~.-.-i.---.--.. --... .__.........i.v .. ....... ~·-- txJ NO MnmMIOl 1!55--.SIIB ........ - .. ----_..,_

NIA i".:r-1 C.J;, ~TE ,.. ~:iuRI! mu! DA'lli

I0/3M019 ,-J-J. :. Tachnk:llnlDflffl' 1D/30/2019

NM 11 Ut tllf'All'tl£l.lff DI TWNmlDlffA?OICJIICJIPnCN II ,,,. "" • " ,v 10 tr ..... ~ .... ~~ ..... ~ ...... --.LNID,..._ oar.,_ - ....-...- - lOTM. PACJ<MlE 1.-a ........ ..........

............ ~ - - ......,.._._, ._,...cu,u ACTMTYlllllllln CUlllll m• . ...._ UN29to Radlolcllve maleJlal. l!la!j)le(I padulJle- HJA HJA 5cllCIIO>lde C:-1'4; H-3 7.80E+02 NIA 0.114 TO-CT,E,1M11

X llmlle1t quarnlly of rnatmta~ 7 Ooe """" ..Ith DAW (lg(.u.n..a! ffOII UU I It~ Malelill HJA NIA C-14; H-3 7 ... --~ NIA 0.114 1u-Vl.0 E 0 1M12

nn.. rlntm with IIIYl,hu lSV 1or ~I

11•1 tJ:IIJUt ERG 11111 Gem1111tor Cerllliclllion Stmement The IDl!tilulltlls of 1h11 walUI 11111n!flllllld hall!IQ am known ID Ille gemll1lt0f, Them aie no EPA RCRA, p11thogelllc Ot other hazards pRIS!lnl OCher l!ian 1hoae apeelllcally llaleel on Ille FCIIIII 541.

Generator: ~hUHon Phannaceutlcala 5~ eeidoJ' ~ 10/30/2018

Prinlllllme ,,,..,,..luffl O,te

COK$10NEE OIUGINAL cuu:rr .OCCOIIPNfY w,sn; JNlJWIStt}

iNN!,,;t"UNM:14.· US NJ!Cl.E.AA~TORY~ l. IU . f'N\rtJrcOI NVl'f'IOl:a"\

""""""" ..,.,,..,. MatW"'4t1 SPECIAL NUCLEAR MATERIAL,~ -•'

UNIFORM LOW-LEVEL RADIOACTIVE '"""""· -- _.. .. U-233 U-235 Pu TOTAL T0-2019-333 WASTE MANIFEST 2 0228 ~3 NP NP NP NP 3.

CONTAINER AND WASTE DESCRIPTION 8.1 PAGE 1 OF 1 PAGE/SI

ACTIVITY IMRnlmr.i\ SOURCE 4. SHIPPER NAME

AIJ..NUCUOeS

:llD C-14 Tc-09 ~129 '""' Chase Environmental Groun

7.80E+02 MBQ 4.78E+02 NP NP O.OOE+OO SHIPPER 10 NUMBER

2.11E+01 mCI 1.29E+01 NA DISPOSAL CONTAINER DESCRIPTION WASTE DESCRIPTION FOR EACH WASTE TYi'!: IN CONTAINER ........

s.can~ 0 1 e l.tu5-f#a ....... ,.,,. f't!YSICA!. DESCRl!'TION t4.~De3CRlPTION ,s.~~ ...... IDENTll'.:>.TIOll --· ...... - ......... "'"'""'"""" 11.wnnt 11-

,._ - ···,ao~~~ AU&TAaS - - - ""'7A>CZR ...... llllol1D0""2 - ,.,.,._ ..,.....,. ..... ---· ~.,,..,.- (:OlffA!tsU T'QTA(..:CI CDfl"MIWt toTAl. ...ct'MTY .,......, ....

GENERATOA .... lillwill (m3) - .ft...o$h •m .. ..-- ..,......,...,.,. _,.,..,_,,,. """' --- -· - lkn) ....... ....... - P..,tl6t2) (m3) WIIUMClflo-.a P•Ot'A Nuclide MBo mCi C<:I.AMC

TO-CT-E-19-411 19 0.114 <5.0 <3.67E-8 <3.67E-5 39 0.114 100 Oxkla/NP NP C-14 4.7BEt02 1.29E+o1 NA 2044 Flberdrum i3 H-3 3.D1E+02 8.15E+OO

PmekAoe total T.80E+02 2,11E+o1

TO.Vl·E·1S-412 4 0.114 <5.0 <3.67E-8 <3.67E-5 59 0.114 89 Oxkla/NP NP C-14 3.70E-02 1.00E-03 NA

2044 '-/0 Non-haz Absorbent H-3 3.70E-02 1.00E-03

LSV Pads PackaM totDI 7..WE-02 2.00E-03

NOTEl;~-Col!IIL ... ..........., ~tw..~~~11!;11---....,.,.~ay---1 ..._).f'o~~N..-.,..,, ... ~~~-~lldlll!l!<llllMt--.o..,~4.•

J-~---IA ......... ~~ i..-

.._ __ .. ,~~ ,., .. ~~ht....,_~Mlt:f:NtaC<i«.tidOIIIMWilntlWh,_,.tJ. C..1~•"°'1~

1o...-............ _.,"OP·. ~·~"'* XI.CGllll\i:llt~IA4ICI ---1.~11=•°"*' ·- i,, ... Jt.1.-.b~ltd:II lll~lRdl So,p,n -h.-.. 10..0co~ '""' #2 ...... lbflca~t.bap -~·-- ldO ....... bn -- ..._,...,, ACl;W.~ .. .,.,,.. ""-

b.~D=i.-•Pd 11.&*.~"Wd:fa .. ,. ,.._,_ .. , . .,.,.,..~ 1&1.c-. .,,_. ·~- ll .... tl.• ft.ea-.~ -....... ~.,... ,,.~~ in_ ..... 3-1.°'P*l.liril,md~OI) 41.~~~k!!#ldC "'2. ""'°"' ... ......_ .......... -- "·-~ MilllfTMll•UW ta.Nijl!'I~~ i..-- $$.~-~ .,_ - .......... ... _ ., __ ia.~friolwr JI CWl'.CW-.IIIIWi\l. 1n-- ,._,,__ ... ,_ ...... 01110d '"""""""'

.,,......,. ... ._._.,.h=t~ ,.~t ......... ·-- t11-EP'A•DIIIII S,ht,,lp....., Sll0tw.~-~,1 .• ~ ............ ft. ari..e ,:XO 11.0,,,.,.~·-·1.

i,l~f-.tU:m - ............. <Id~ ,,_..._....,, ---

:coo:~542 U.S. l«JCI..EA/l AEGUV.TOR'fCOM!Jt:SS!OO I. WASTE COUECTORIPR()CE~ 'l. MANll'ES1 NU"9m

l IWJE 61<!M'SlllSeCU..Y

UNIFORM LOW-LEVEL RADIOACTIVE Chase Environmental Grouo, Inc. T0-2019-333 WASTE MANIFEST !DEIITIFICATIOH NUMl!l:R

T-KY003-L 19 3.

IMAU!FEST!NDEXANOl'1!GIOIW.COI.IPACTTASUI.ATIOfl PAGE_1_0F _1_PAGE(SJ

Usl oil orlQml '1'f!OCeSSal WAlm!' boloro "COI..I.ECTl:O WASl'E".

4, 5. a. ,a. lo. Ill. NJ.~EJJ

GVIEllATOR Gl!HlmAltlR,_E G£NEAATOR -- _.._.. WA6111 ...........

!!lElfflFICATIOO -IIITNUMEa> FN:4.llY WA8tl: ....,....,. ...... COOE - ... = IUJ>W C.AC'IMIY D.\/OUJ1dE

NUWIEJI N«>TaS'HONEN!Jl.l!lm - l""'""""1l ...... ,_, - "' IIATE/lW. - ~IZCl)*ff: - '"'' (MBql (1113)

'""' , ... ,,.., {l(g) (g}

2044 /\cn1111on Pharmaceuticals George St. U,&&U NF\ C I., I NP 7.80E+v, u.-u

Haven, CT 05511 203-624-7000

TOTALS Of Al.I. PAGES !NRC FORMS 1142 AND M2AJ "

....... ·_,·:::. ' .

Date .. .. .. -

7/n_ 1/1·~

I•

7/r;o x-lr iltr:. s-/1>

f ,,,/ 12/n1

I I

\o{ Is- (,H

l<Jl l'-F/t} \

\o\ ,.,(, , ,, u,

ta{ is/ O\

/,'1\2"\/ (\ I

II\ 0(,, /Ot Comments 7l~J0,2.

q{ll[ 01.. q{cJSi?>?

---··· I Q /.t ~/1' ~" ! ' }f .. , O!J,JC),,,L

l

111 il '):::?:. 1 u n'" -~, . JU 11 ,. , w,"'.

u .. : ',:; .. , .

\ _j

A chi/lion Plran,iffti!l1Cicals. Inc. 300 George Street, Suite 801

Newllave11, CT065/J.

Record of Sanitary Sewer Disposal

3H

··:. -·-·· ·····-· ·- - ·-•:::,:::: ...

Performed by (initials) Amount (µCi) .

Jf 2.}.w<.a

0- r-:: 4.5 7S-: S'F ). ,)

·'T -e: r z.s-· T'f' (.,~~

T'f- )

-r-1/ o~.'5 .u(}

"".\V Q. ' /.

5 .rLt t I

:rv .. ,,

,1#~,."r; "'.:;(../ 0. ,;;-(;

.. ·".!V o.s .... ,;·

, ...

,:f\/ ~$'A(i ....... ·······-·- ..

j'V 0.5vc; -:sv 0 . .5y.,, Ct ys zoµc..,~. ys .J '.) r, > '._", _lf'>,.J

ys f/\C -·-N,i J exceed: -t..!i),/> C/·

20 mCi/montb r ~ r-, \...-5 / .,

>}I~. . d \. y- .("' ,....., ", .. ./"'· ~

' .... ~ -::· ''7°J;·.

·····-··

. •

/

;I 1<-fi; i'>Y 3H

-· -··········

Date -

'6}31/01

CJ /10 / 01

\0)"2:3101

1DhD/ ()I

,ii c.,{o l

l\}t,\01

\I\ I~ IDt

l \ I J1 I o 1

2h/u 2...

:z.\,?\a') I

~ X

Comments

Achil/io11 Phar~1ai~11ticals, I11c. 300 George Street, Suite 801

New Hm•en, CT 065 /J


3H

... ,.. ........... --

·--,,,,, ...

---··-·-- ...........

Performed by (initials) ... ··---

jf

Jf jf ,1( Jf :Jf jr Jf -:sv

--sv ,

'-- ,-~ -'-- / ---·······

Not to exceed: 20 mCi/month

····-· .. --Amount (µCi)

--· -·······

2.5Y.C

:J.' <; f" c;

1,2)}'(;

l, '2 5 f" ('.

1.1:s )''(;

1.1s y<..,

i .)."5" }'(:

f.1-'r;,<(,

i. 25,,,,.C.·

f • 2t,;;M f.; '><_-

~ ·····-····· .···-· .... ,...

-- -- ···-·· ...

~

'

Cmnments

Achillion Phar;;,m.{111icals, Inc. 300 George Street, S11ite 801

New Haven, CT065t1


3H

... _._., ·=···· .. --,~. ··--Date

"""~ Performed by (initials) Amount (µCi)

""'"'"····· -·,=,. . -

,/2.<-J j {)?. <}f /, ,z_•'S"" Jt(;

I /Jo/De. j {;:;'. l, f 1':> r c.:

o1 I 1 /01 . .1 r=' 1:r1S" .rc1 i;;;,/r1/02 JF /, 'Z 5 1<,((1

2/1c:;/o z. Jf !. ZS,lfc; 2 \ :q \ <n. :sv I. 2.'$ A..li J.\.tl { 02, -;:'',/ Ll..!>A-4 C;

~L2s '"' ~ 1. 1r::AA,r: ::3/1)01. jf 1 ;2S )'1 c·1

_3/&(6? jf I. 2:s- fa( 1

3/ J&-}<r2 jf }.1":)j"(.;

qf_3/o?.. 1F t .i1S' Y<.:i ·=· """~ -········ ···~-- -·· .;r-=•••ss - ·::::,::= . ._

--

----· ------- -- ------ ----··--·-·----- ---·-----


---- ·------····---------····---

Comments

7( I

l z(iJ/) t{{(ti3

Date

1(2s1·0·s '1:.J 'tj/@l ' ,.\. / .. -

Achillio11 Pharn',,r"/euiicals, Inc. 300 George Street, Suite 801

New Haven, CT 06511


3H

Performed by (initials) Amount (µ.Ci)

Not to G

[ OP ti' _:3p,.<..; /

'1 ( t Iv (

Comments

Date

3/11.ltil 'i (! /03

Achillio11 Plwt11mceuticals, Inc. 300 George Street, Suite 801

New !fave11, CT 06511


3H

Performed by (initials) Amount (µCi)

[6

\}f (, J I fo 3

9!tt. (ot


jD

1-.......

Comments

1khillio11 Plrammce111icals. Inc. 300 George Streel. Suite 80 I

New Haven. CT 065/ I


3H ...

Date

c7/1("/ 03 1 )zf/ p3

Jo/z3/03 10/.?Jo/03

1ilur/03 { I -::,.i.J. -o <

/!'-flt-DJ.

l O - Ji:)' i.? J.

/ -IJ -15(/..

I -I .. -av: 1..- ,~-0\.\

.,J.-: 2. o- oc, ;l. - l 7_-C::,l( 3 - 3--L"'( ?::.- n- c(.\ ':t- {. -°?1

bf ~1\ or J-/1lf,(_or --f i (3 / 6.:'.)

T

"'·--·-··

Performed by (initials)

··-···

······· ·-

J( /J'/ JI" 1( _1r-: 1f ..,

Xr YT f. T

I- -r

YT

S:)1. \

,\L.J ·-··

Y'J. Not to exceed:

20 mCi/month '/"b 'Ir

·-.

-··

-

""''"'""-'"•·

Amount (µCi)

3. c;·/Jc ;

3. Y.rc i 3. <:;' ,r( i

_3, 5 _,µ(_ I

·-·······

5. 5-ytc .

/c t.t. {, ,'

/v "(. c/

{Jo v-U

' IO L<.. l.{

J. () (,L l 1

.;)Ci(,,.(' •

:1r\. r ' d-Du. Ql

Qc.."<A(:'; -z_,.oc .. (,:-

o20u.C ~

r-.,,UC;

(o /l ~ J.& ;ll Ct,"

'

I i

-A•==•

Date

!/-·,·,

Achillion Ph~'tmaceuticals, Inc. 300 George Street, Suite 801

New Haven, CT065JJ


3H Not to exceed: 20 mCi/montb


OZ }l C ·

. 02. }-'Ci

.o 2 Y c..

Date

t /31,1/07

~

_J:3 ~ ~ ~

'/:) ~ ~ ~

Ac/111/ion PhJh,.,,..Jeutica/s, Inc. 300 Geo,ge Street, Suite 801

New Haven. CT 0651 J

Record of Sanitary Sewer Disposal 14c



h1 '{ <XJb fl\ Ci' !

£pf'

"<t tt ·Ji~ * .~ l'.l. ~ 'f1 t!I ~ ~

~ ~ l',~ ~~ e ~ e.-, If'\ ~

\ u i

l I

~

~

RADIOLOGICAL DECOMMISSIONING REPORT

Achillion Pharmaceuticals, Inc. _300 George Street

New Haven, Connecticut 06511

October 21, 2019

Performed by Radcor, LLC

345 Laurelwood Drive Salem, CT 06420 (860) 887-1538

EXECUTIVE SUMMARY On October 14, 2019 a radiological assessment for the purpose of decommissioning was performed at the Achillion Pharmaceuticals, Inc. facility located at 300 George Street, New Haven, Connecticut. This assessment was conducted by Radcor, LLC of Salem, Connecticut.

After performing a radiological assessment and decontamination of the use and storage areas designated by the licensee, it is the opinion of Radcor, LLC that the areas assessed do not present any significant radiological hazard to facility personnel, the public, or the environment, and that once radioactive waste has been removed from the facility, these areas may be released for unrestricted use.

Radiological Decommissioning Report Achillion Pharmaceuticals, Inc.

SCOPE Radcor, LLC of Salem, Connecticut was contracted to perform a radiological assessment of selected areas of the Achillion Pharmaceuticals, Inc. (Achillion) facility located at 300 George Street, New Haven, Connecticut. This facility is licensed by the U.S. Nuclear Regulatory Commission (NRC) for the possession and use of radioactive materials under license No. 06-30628-01.

Achillion is ceasing licensed operations and is relocating to a different floor within the same building and therefore wishes to decommission their current facility and tenninate the radioactive materials license.

FACILITY DESCRIPTION Achillion leased approximately 20,150 square-feet of space on the 8th floor of the building located at 300 George Street, New Haven, CT. This space is composed of both laboratory and office space.

Affected Areas (Class 2) Facility personnel indicated that licensed radioactive material had been used and/or stored in only the following five (5) areas at the facility:

I. Tissue Culture lab with associated hallway;

2. Molecular Biology Lab;

3. Radioactive Waste Storage Area within the Glass Wash Room;

4. BL2 Lab; and

5. Biochemistry Lab.

Since no known radioactive contamination exists at the facility and the areas where licensed material had been used and/or stored had the potential to be contaminated to levels expected to be below the screening criteria, these areas were designated as Class 2 areas.

Floor plans showing the locations of these areas are provided as Attachment A of this report.

Identity of Potential Contaminants According to facility personnel, the following isotopes had been possessed under the license: hydrogen-3, carbon-14, phosphorus-32, phosphorus-33, sulfur-35, and iodine-125. The approximate dates that these isotopes were last used at the facility are provided in Table 1 below.

T bl 1 I t a e : so opes an d L t U D t as se a es Isotope Last use Isotope Last use

H-3 and C-14 2017 1-125 2004

S-35, P-32 and P-33 2016

Radiological Decommissioning Report I Achillion Pharmaceuticals, Inc.

Therefore, it was detennined that potential contamination from licensed material could only be due to H-3 and/or C-14, so survey and release criteria were based upon these isotopes.

ASSESSMENT PERSONNEL The radiological assessment was performed under the supervision of Mr. David J. Durkee, a professional health physicist. Mr. Durkee's resume is included as Attachment B to this report.

SURVEY PROCEDURES The survey was based upon the screening approach outlined in NRC's Consolidated Decommissioning Guidance (NUREG-1757) Section 6.6.3 (Vol. 1) "Criteria for Conducting Screening'' and Section 3.3 (Vol. 2) "Insignificant Radionuclides and Exposure Pathways." In this approach, the NRC allows the licensee to simplify decommissioning in cases where the licensee can demonstrate that low levels of radioactive contamination exist, e.g., academic research laboratories. All decomijlissioning survey measurements of any existing radioactive contamination found on building surfaces are then compared to radionuclide values found in a screening table developed by the NRC using appropriate dose modeling.

SCREENING CRITERIA 10 CFR 20, Subpart E specifies that a site will be considered acceptable for unrestricted use if the residual radioactivity that is distinguishable from background radiation results in a TEDE to an average member of the critical group that does not exceed 25 mrem (0.25 mSv) per year, including that from groundwater sources of drinking water, and the residual radioactivity has been reduced to levels that are as low as reasonably achievable (ALARA).

The screening criteria used were obtained from NRC's Consolidated Decommissioning Guidance (NUREG-1757) Volume 1, Table B.l. Since this screening criteria was based on a TEDE of 25 mrem and the State of Connecticut has established a limit of 19 mrem, the criteria provided in NUREG-1757 were reduced by 25% to ensure compliance with Connecticut's dose limits.

The screening values adopted are provided in Table 2.

Table 2 Screenino Values ,. Radionuclide Acceptable Screening Levels for Modified Screening Levels for

Unrestricted Release (dpm/100 cm2) Unrestricted release (dpm/100 cm2

) -

H-3 120,000,000 90,000,000

C-14 3,700,000 2,775,000

Radiological Decommissioning Report ] Achillion Pharmaceuticals, Inc.

INSTRUMENTATION Table 3 lists the instrument used in the performance of the surveys, along with parameters and detection sensitivities. The instrumentation used were calibrated using NIST-traceable standards. Instrument detection sensitivity calculations and calibration information are provided in Attachment C to this report.

T bl 3 S a e . urvey I t ns rumen t I fi f n orma 10n

Type of Instrumentation Measurement

Detector

Surface scans - ~ Gas Prop. Det. Ludlum model 43-68

Surface scans - ~ Gas Prop. Det. Ludlum model 43-37

Dose equivalent Scintillation rates Bicron Microrem LE

Smears, ~/y Perkin Elmer Microbeta 2450

"Nominal Values bMonitoring audible signal

RADIOLOGICAL SURVEY

Meter

Count-rate meterb Ludlum mod. 2241-2

Count-rate meterb Ludlum mod. 2241-2

(Same as detector)

(same as detector)

The survey of the Affected Areas was conducted as follows:

Bkgd.0 Eff& Cal Isotope

212 cpm 8.60% C-14

504 cpm 8.69% C-14

2-5 µrem/h 100%

23 cpm H-3 40% H-3

40 cpm C-14 75% Others

Dose-equivalent measurements were obtained throughout each Affected Area;

Minimum Detectable

Concentration

1,878 dpm/100 cm2

619 dpm/100 cm2

I µrem/h

63 dpm/100 cm2

43 dpm/100 cm2

100% of accessible lower surfaces were scanned for residual radioactivity using a gas-flow proportional counter; and,

Wipes samples for loose radioactivity were obtained throughout each Affected Area. Samples were obtained from areas where activity would have been likely to collect (i.e., sink drains, horizontal surfaces, inside cabinets, hood ducting, etc.). Samples were analyzed for beta activity using liquid scintillation analysis.

SURVEY FINDINGS AND RESULTS Survey documentation is provided as Attachment D to this report.

Dose-Equivalent Measurements Samples Dose-equivalent measurements were consistent with normal background levels for this area of the country.

Radiological Decommissioning Report 3 Achillion Pharmaceuticals, Inc.

Surface Scans A scan of area surfaces and equipment identified only one (1) area with a reading in excess of the minimum detectable concentration (MDC). This area was a small spot ( < 100 cm2) on a counter in the Molecular Biology Lab which was found to be contaminated to a level of 13,140 dpm/100 cm2 (C-14). This area was decontaminated to a level below the MDC.

Wipe Samples A total of 1,055 samples were obtained from the five (5) Affected Areas. Only two (2) areas were found to be contaminated to a level in excess of the MDC. These areas were both floor areas located within the Molecular Biology Laboratory. One area was found to be contaminated to a level of 1,312 dpm/100 cm2 (H-3) and the other area was found to be contaminated to a level of 251 dpm/100 cm2 (H-3). These areas were both decontaminated to levels below the MDC.

SUMMARY On October 14, 2019 a radiological assessment for the purpose of decommissioning was performed at the Achillion Pharmaceuticals, Inc. facility located at 300 George Street, New Haven, Connecticut. This assessment was conducted by Radcor, LLC of Salem, Connecticut.

After performing a radiological assessment and decontamination of the use and storage areas designated by the licensee, it is the opinion of Radcor, LLC that the areas assessed do not present any significant radiological hazard to facility personnel, the public, or the environment, and that once radioactive waste has been removed from the facility, these areas may be released for unrestricted use.

~--David J. Durkee Health Physicist, RRPT

Radiological Decommissioning Report 4 Achillion Pharmaceuticals, Inc.

Attachment A

Floor Plan

Radioactive Material Use/Storage Areas D

1aa@=-,1o#.~a=~~ .... ! .. N~G=PA=R::11=AL.,;8~TH~Fl,;,LO=OR.b=PLA"'=N========================~_, 0

-~ACHILLION

z 0 ~ e, z t! z 0 ::I :I:

~

BID DOOJMENlS

0 l'IIQALI + P A a 'T N E I S

St.t.LE:1/!,--1'-o"

D.\J[11/21/2C10

Al.01

Attachment B

Resume

RADCOR,LLC 345 Laurelwood Drive

Salem, CT 06420 (860) 887-1538

David J. Durkee

EDUCATION: Regents College, NY. - B.S. Technology (Nuclear/Health Physics) University of Phoenix, AZ. -A.A. Nuclear Technology Health Physics Technician Level I Basic - Radiation Safety Associates, Inc. Health Physics Technician Level II - Radiation Safety Associates, Inc. Respiratory Protection at Nuclear Facilities - Radiation Safety Associates, Inc. Environmental Monitoring for Radioactivity - Oak Ridge Associated Universities. Liquid Scintillation and Gamma Spectrum Analysis - Rutgers University Health Physics Audits - Radiation Safety Associates, Inc. Navy Naval Nuclear Power School (24 wks) Nuclear Prototype Training Unit (26 wks) Engineering Laboratory Technician School Machinist Mate "A" School

EXPERIENCE: December 1996 to Present Radcor, LLC, Salem, Connecticut

Diesel Operator/Maint. School Scuba Diver School Advanced Auxiliary Package Course Quality Assurance Inspector School

Health Physicist/Owner. Responsible for providing radiological consulting services to general industry, academic institutions, and companies involved in research and development. These services include: development and presentation of professional training; performance of program audits; performance of radiological surveys, decontamination and decommissioning; development of license applications, amendments and safety procedures; radiation protection program oversite; and, regulatory compliance.

Served as the Radiation Safety Officer (RSO) for ExxonMobil Research and Eng. Co., Paulsboro, NJ and ArQule, Inc. Woburn, Ma, and Agios Pharmaceuticals, Cambridge, MA. Currently serve as the RSO for Enanta Pharmaceuticals, Watertown, MA, Jnana Therapeutics, Boston, MA and Pfizer Inc., Groton, CT.

March 1994 to December 1996 Radiation Safety Associates, Inc., Hebron Connecticut Vice President-Technical Services. Responsible for the preparation of job proposals and operating budgets; making technical and manpower recommendations; supervising workers at job sites; perfonning technical evaluations as required; writing, editing, and developing course materials, working procedures and technical articles; and, performed duties as a health physicist.

Responsible for oversite of various site decontamination/decommissioning projects. These involved: the development of decommissioning plans; hiring and oversite of workers; hands-on performance of radiological surveys and site decontamination efforts; and the development and submittal of final reports.

Instructor for the following professional training courses: Fundamentals of Radiological Protection; Health Physics Technician Level I and II; Radiation Safety Officer; Radiation Safety Officer Refresher; and, Basic Radiation Worker.

Assistant Editor of Radiation Protection Management, the Journal of Applied Health Physics. Assistant RSO and Quality Control Officer for a radioanalytical laboratory.

October 1991 to March 1994 Radiation Safety Associates, Inc., Hebron, Connecticut Health Physicist. Responsible for providing consulting services to the nuclear industry; general industry; local, state, and federal governments; and academic institutions. These services included performing audits, radiological surveys, instrument calibrations, site decontamination services, writing license applications and amendments, maintaining radiological safety programs, providing technical advice and performing training.

September 1983·to October 1991 United States Navy, Submarine Qualified. Served on-board two nuclear-powered submarines. Qualified as Leading Engineering Laboratory Technician, Engineroom Supervisor, Quality Assurance Inspector, Duty Section Leading Mechanic and Ship's Diver.

Supervised and performed chemistry and radiological controls on reactor plant primary and secondary systems. Sampled primary coolant and secondary water chemistry and analyzed results to detect abnormal trends and out of specification conditions. Established and certified radiologically controlled areas, conducted radiation and contamination surveys, evaluated man-rem exposure and processed radioactive waste. Calibrated and operated radiation detectors and chemistry analytical equipment.

Directed the day-to-day efforts of five junior Laboratory Technicians. Awarded a Navy Achievement Medal for being "the driving force behind a dramatic turnaround in the professionalism of the (Reactor Laboratory) division." Instituted a training program that significantly upgraded the level of knowledge of the division.

Drafted detailed work procedures and quality assurance work packages for nuclear and non-nuclear maintenance efforts. Performed in-process inspections to verify that materials and procedures met required specifications.

PROFESSIONAL ACTIVITIES: Registered Radiation Protection Technologist (NRRPT)

PUBLICATIONS "NRC License Application, Renewal, or Amendment for Byproduct Material" RSO Magazine, I :6: pp. 25-30; Nov/Dec, 1996.

"Personal Whole-Body Dosimetry" RSO Magazine, l :4: pp. 26-28; Jul/ Aug, 1996.

"Prenatal Radiation Exposure," RSOMagazine, 1:2: pp. 12-13; Mar/Apr, 1996.

"Loose Contamination Survey Methods," RSO Magazine, 1: 1: pp. 19-20; Jan/Feb, 1996.

Steinmeyer, K. Paul, David J. Durkee and Paul R. Steinmeyer. Mathematics Review for Health Physics Technicians. Hebron, CT: RSA Publications, 1994. (393 pages).

Attachment C

Detection Sensitivity Calculations and Instrument Calibration Information

Equations used for determining detection sensitivities

Variables: MDC = Minimum Detectable Concentration in dpm/100 cm2

MDCR = Minimum detectable count rate Si = minimum number of source counts in interval d' = 1.3 8 (95% true positives/60% false positives acceptable - Table 6.5 NUREG-1575) bi= Number of background counts in interval i = Count interval (Assume 2 seconds) Ei = Instrument efficiency Es= Surface efficiency (Assume 0.54) p = Surveyor efficiency (Assume 0.5) A= Active detector area in cm2 (126 cm2

)

Rb = Background count rate in cpm t = Counting time when background time equals sample time

MDCR for surface scans using Ludlum Model 43-68: (NUREG-1575)

Si= d'(bi) 112 = J .38(212 X (1/60)) 1/2 = 2.59 MDCR =Six (60/i) = 2.59(60/2) = 77.7 cpm

MDC for surface scans using Ludlum Model 43-68: (NUREG-1575)

MDC (C-14) = MDCRl(pY12 ti Es (A/100) = 77.7/ (0.5rl/2 (0.086)(0.54)(1.26) = 1,878 dpm/100 cm2

MDCR for surface scans using Ludlum Model 43-37: (NUREG-1575)

Si= d'(bi) 112 = 1.38(504 X (1/60)) 112 = 4.0 MDCR =Six (60/i) = 4.0(60/2) = 120 cpm

MDC for surface scans using Ludlum Model 43-37: (NUREG-1575)

MDC (C-14) = MDCRl(pY12 Ei Es (A/100) = 120/ (0.5ru2 (0.0869)(0.54)(5.84) = 619 dpm/100 cm2

MDA for counting 100 cm2 wipe samples on LSC:

MDC= [2.71 + 4.65 {(Rb)(t)} 112] + (t)(Ei)

MDC (H-3) = [2.71 + 4.65{(23 cpm)(l min.)} 112] + (1 min.)(0.40) = 62.5 dpm/100 cm2

MDC (C-14) = [2.71 + 4.65{(40 cpm)(l min.)} 112] + (1 min.)(0.75) = 42.8 dpm/100 cm2

Instrument Calibration Information

Bicron uRem LE B466Y. Calibrated by RSCS of Stratham, NH on 01/15/19.

Ludlum Model 2241-2 with 43-68. Calibrated by Ludlum Measurements of Sweetwater TX on O 1/07 /19.

PE Microbeta 2450: Calibrated by the manufacturer on 04/01/19.

Designer and Manufacturer

Scientific an~~ndustrial Instruments

www.ludlums.com

LUDLUM MEASUREMENTS, INC, .

CERT/FICA TE OF CAL/BRA TION 501 oak street l~~~ .-Jla ·

325-235-5494 ~ ~, ,,~_J' {Acg!EOITyii)

Sweetwater, TX 79556, U.S.A. .• ,,,,,2S:,->'' CERT# 4084.01 Customer RADCOR LLC ORDER NO. 20346891/472864 rv1'· Ludlum Measurements, Inc.

rv .. _ Ludlum Measurements, Inc.

Model 2241-2 Serial No. /377 S Model 43-68A Serial No. -f1~:,Z.~J-lz~'O-fill_1,_9 ___ _

Cal. Date ______ 7_-J_a_n_-_19 ____ Cal Due Date -----~7_-J_a_n_-2_0 ____ Cal. Interval 1 Year Meterface cpm

Check mark 0pplies to applicable instr. and/or detector IAW mfg. spec. T. 73 °F RH 48 % Alt __ ~6=88~.o=- mm Hg

D New Instrument Instrument Received @Within Toler. +-10% D 10-20% D Out ofTol.

~ Mechanical ck. D Meter Zeroed D Background Subtract ® F/S Resp. ck G3-'Reset ck. D Window Operation

D Requiring Repair D Other-See comments

D Input Sens. Linearity

~ Audio ck. ~ Alarm Setting ck. ~ Batt. ck.

ia-c-alibrated in accordance with LMI SOP 14.8 D Calibrated in accordance with LMI SOP 14.9 Threshold

Instrument Volt Set Comments V Input Sens. 4 mV Det. Oper. Comments V at 4 mV Dial Ratio

COMMENTS: Det.1 (Alpha)

Deadtime: 12uSec Cal Cons: 1 OOe-2

Alarm: 50kcpm Alert: 50kcpm

43-68 HV: 1250v 43-37 HV: 1250v

*Si32 sub for P32 ; Firmware: P-06-01 ; OL checked but not set 'Ratemeter calibration' achieved with no deadtime.

Det.2(Beta) 15µSec

100e-2 50kcpm 20kcpm 1725v

43-68 (Det.2) C14 SN:1476, Size:229767dpm, Counts:20073cpm, BG:293cpm, 4pi Eff:8.60% *Si32 SN:422-44 Size:86329dpm, Counts:28205cpm, BG:293cpm, 4pi Eff:32.33%

43-37 (Det.2) C14 SN:1476, Size:229767dpm, Counts:21144cpm, BG:1174cpm, 4pi Eff:8.69% *Si32 SN:422-44 Size:86329dpm, Counts:30418cpm, BG:1174cpm, 4pi Eff:33.87%

1725v

Gamma Calibration: GM detectors ositioned

=

RANGE/MULTIPLIER

Dig.rate

CAL POINT "AS FOUND READING" METER READING*

Dig.rate

•uncertainty within ± 10% C.F. within ± 20% Range(s) Calibrated Electronically

REFERENCE INSTRUMENT INSTRUMENT REFERENCE INSTRUMENT INSTRUMENT

mV

CAL. POINT RECEIVED CAL. POINT RECEIVED METER READING* Ratemeter

~'$-~) 799:ro{g) Readout 800K q~m BOOK q~m 200K CQm 200KcQm

~ L2'2-~

80K CQm 80K CQm 'i!l~f 20K CQm 20K CQnl 8KcQm 8KcQm 79?._ 1 2KcQm 2KcQm o/' L9'l I .

800 CQm 800 CQm 'O "3"-0 !.. 200 CQm 200 CQm ~a ~o 7

Ludlum Measurements, Inc. certifies that the above instrument has been calibrated by standards traceable to the National Institute of Standards and Technology, or to the calibration facilities of other International Standards Organization members, or have been derived from accepted values of natural physical constants or have been derived by the ratio type of calibration techniques. The calibration system conforms to the requirements of ANSI/NCSL 2540-1-1994 and ANSI N323-1978. ISO/IE 17025:2005(E) State of Texas Calibration License No. L0-1963

Reference Instruments and/or Sources: Cs-137 SIN: 0 059 0 2171CP O 2261CP O 720 0 734 0 781 0 1131 01616 0 1696 0 1909 0 1916CP D 2324/2521 0 5717CO O 5719CO 060646 070897 073410 0 E552 0 G112 0 216BCP O S-394 0 S-1054 0 T10081 0 T10082 NeutronAm-241 Be O T-304 Ra-226 0 Y982

~ Alpha S/N Pu239 SN:7053 24900dpm

~ m 500 SIN ___ c....=....=-=--=-=--=----

ator Jason Flores

QC'd By

FORM C22E 10/03/2017 Page j__of S-

~ Beta S/N Tc99 SN:5280 93200dpm

Title Calibrator

Title Final QC

D Other

~ Multimeter S/N ---~8~6~2~5~03~9~0~---

Date 7,-----;?}...-- "'/9 Date ") ~6'l\\1

This certificate shall not be reproduced except in full, without the written approval of Ludlum Measurements, Inc.

•

RSCS Calibration Certificate

ID Number: B466YI28770-0

Customer: David J Durkee Radcor, LLC. 345 Laurelwood Drive Salem, CT 06420-

Test 1 I Test2 1.50 mrem/hr I 1.50 mrem/hr

Range Target Value X1000 160 mrem/hr X1000 40 mrem/hr X100 16 mrem/hr X100 4 mrem/hr X10 1.6 mrem/hr X10 0.4 mrem/hr X1 160 µrem/hr X1 40 µrem/hr

X0.1 16 µrem/hr X0.1 4 µrem/hr

I I

Instrument

Bicron Model MicroRem

Precision Check Test 3 I Mean

1.50 mrem/hr I 1.50 mrem/hr

Accuracy Check· As Found

160 mrem/hr 40 mrem/hr

16.5 mrem/hr 4 mrem/hr

1.5 mrem/hr 0.4 mrem/hr 160 µrem/hr 40 µrem/hr#

15.5 µrem/hr# 4.µrem/hr#

I I

Serial Number 8466Y

Results Satisfactory

As Left 160 mrem/hr 40 mrem/hr

16.5 mrem/hr 4 mrem/hr

1.5 mrem/hr 0.4 mrem/hr 160 µrem/hr 40 µrem/hr#

15.5 µrem/hr# 4 µrem/hr#

Readings with • indicate ranges where As-Found readings are >20% of Target value. Readings with .. indicate As-left readings are >10.00% of Target value Readings with# indicate ranges where pulser was used.

MTE Instrument Type ·Model· Ca1Duebate

Pulser Ludlum 500-4 SN: 66151 01/17/2019

Outer Physical Check: Pass Mechanical Zero: Pass Internal Check: Pass Tap Test: Pass

Geotropism Check: Pass

Comments: Unless indicated with a"#" in the table above to indicate a pulser was used, all readings were obtained using the Tech Ops Model 773 Cs-137 Beam Calibrator (S/N: S-1110). Pulsed measurements are outside of the scope of IS0-17025 accreditation.

Patrick Cashman Calibration Technician

QA Review:

Atmospheric Conditions - Temperature: 69°F Humidity: 24% Barometric Pressure: 30.15"hg

This calibration was performed by RSCS using one or more of the follo\\ing NIST Traceable radiation sources:

Calibration Date: 01/15/2019

Expires: 01/15/2020

Tech Ops Model 773 Cs-137 Beam Calibrator (S/N S-1110), characterized using Exradin Model AS (S/N 185) and Keithley Electrometer Model 617 (SIN 0547677) in accordance \\ith methods specified in RSCS TSO 11-008, \\ith estimated uncertainty of 6.0%. J.L. Shepherd and Associates Model 89 Cs-137 Box Calibrator (S/N 9141), characterized using Exradin, Model A6 (S/N 185), A3 (S/N 197), A12 (S/N XA091124), and Keithley Electrometer Model 617 (SIN 0547677) in accordance with methods specified in RSCS TSD 11-001, with estimated uncertainty of 2.7%. RSCS Neutron Calibrator, AmBe Source Model NUMEC-AM-31 (S/N Anc478), characterized using Far West Technologie~ Model FWA0-1 "HAWK" TEPC (S/N 021) in accordance \\ith the methods specified in RSCS TSO 13-002, \\ith estimated uncertainty of 9.4% The reported expanded uncertainty of measurement is stated as the standard uncertainty of measurement multiplied by the coverage factor k such that the coverage probability corresponds to approximately 95% Unless otherwise stated, calibrations performed in confo1111ance to the follo\\ing documents: ANSI N323AB-2013; RSCS New Hampshire Radioactive Material License Number 381 R. RSCS calibration services are performed in accordance with the RSCS Radiation Protection Program Manual and Standard Operating Procedures. Calibration Laboratory is operated in accordance with ANSI/NCSL 2540-1-1994 RSCS, Inc. has been assessed by ANAB and meets the requirements of ISO/IEC 17025:2005 v,!Jile demonstrating technical competence in the field of calibration. Refer to the Scope of Accreditation AC-2079 for info1111ation on the types of calibrations to ooich this accreditation applies. This calibration certificate shall not be reproduced except in full \\ilhout the express written consent of RSCS, Inc.

Radiation Safety and Control Services, Inc. 91 Portsmouth Ave. Stratham. NH 03885 1-800-525-8339 (603) 778-2871 Fax (603) 778-6879 www.radsafety.com

Page 1 of 1 ArlAa ol\CCJ.ICOITCO -=m-

C>J.ronJ.110:N V,D:>"AlOflV

SPodos, 7/16/2019 2:23 PM, Microsoft Word - Dbcument1 ''

:1 ! I ,,. I '!

·., I· I•

'fl . . IPARepo,1'_1:for~licroB~~" _ 1_ , __ ... _1. :\\ _ ·-·· :_;i

· . C€!111nter serial 111umi!Der 3130209 . . . . , i . • . , ·:fl,=:·= 1 j/·Eff;::;:ft~-5il Hl. · 1 119 .. 0! · 985!!6; · • 52.9511; 8'.0: ' · t' 1

2i ·· 119_2: · . 91o~f )2:~2a~L _:. ___ fo! __ _ .. - ; . .:

. 1 ·;

•. • C14: =_~-r: :- _-:_-·!;.:· -.·::~::~r-~~~:~:r·-:::~~~~r-:---~:~~:-~· --_ --:·.·) · .. ~· ;',_ i_'. ·--r::~:,;:,;;.:,. :r,:,--. I ~··11- ···'t' .,, .. '

... · ......... ~---··>--·-··-·-·---·,-·-· ···---·-·.- ·--., ••• • ··-· ·····---·c ' '

-·--·- ---·-·---· ' ' . ----·-··· --·. --- -- ------- --··-·- ·- - ___ .... ----- --· ....... - .

. ·.· ... ··---- ·--: - .. - --~-------·---.- : . .

·-··---··-·- -- '!' __ ,,,_. ·-- --·i-·--. · ..

' .. '

----·- ... .,_ ... --· - -·-·r

·---·····--------- ----,- . . ,.

--······--·----- ··- _____ , ____________ i_ --------- .-----·-··- :. ·--·-·--· ..

I

l I 1) 'I,

,I I· I

'1: ,, ii I ~'

i , . . 1,

I I

'i' :·

I I

II: ,, I, ;I. I

,11 :, t

Attachment D

Survey Data

Job Location: Achillion Pharmaceuticals, Inc. New Haven, CT Page: _1_of_7_ s p urvey urpose: ecomm1ss1ornnq issue u ure D T C It a an a L b d H II D t 10/14/19 a e: Performed By: David Durkee

~ - -- ., I

Inst. No. 1 (Model/SN) Inst. No. 2 (Model/SN) I Inst. No. 3 (Model/SN) PE Microbeta 2450 #04130262 Ludlum 2241-2 #137751 Bicron uRem LE B466Y Detector (Model/SN) Detector (Model/SN) Detector (Model/SN) Internal Ludlum 43-68 #140899/ Ludlum Internal

43-37 #143616

Efficiency:== 40% 3H / 75% 14C Efficiency: 8.6%/8.69% C-14 Efficiency: 100% Type Rad.: S Type Rad: S Type Rad.: V Bkad.: See #1 Below Bkad.: 256 com/ 864 com Bkad.: 4 - 8 uRem/hour Cal. Due: 04/01/20 Cal. Due: 01/07/20 Cal. Due: 01/15/20

Number Time Location Inst. 3H Activity 14C Activity Used (dpm/100 cm2) (dpm/100 cm2)

1 0800 Background 1 18 cpm 30cpm 2 Uooer wall 1 30.0 12.0 3 Counter 1 -5.0 1.3 4 Side of drawers 1 -15.0 6.7 5 Front of drawers 1 -5.0 4.0 6 Top drawer 1 -22.5 -5.3 7 Drawer 1 . -7.5 8.0 8 Drawer 1 -2.5 2.7 9 Bottom drawer 1 -15.0 0.0 10 Uooer door 1 -15.0 -6.7 11 Lower door 1 0.0 10.7 12 Upper wall 1 -22.5 -6.7 13 Lower wall 1 -2.5 -4.0 14 Uooer wall 1 -2.5 21.3 15 Lower wall 1 0.0 18.7 16 Uooer wall 1 -10.0 4.0 17 Upper wall 1 7.5 12.0 18 Shelf 1 -15.0 -1.3 19 Counter 1 0.0 1.3 20 Front of cabinet 1 -10.0 0.0 21 Inside cabinet 1 -10.0 -6.7 22 Uooer wall 1 -22.5 -10.7 23 Shelf 1· -25.0 -14.7 24 Counter 1 -20.0 -1.3 25 Front of cabinet 1 15.0 13.3 26 Inside cabinet 1 -22.5 -12.0 27 Cubby 1 -27.5 . -16.0 28 u er wall 1 2.5 -2.7 29 Counter 1 -10.0 -9.3 30 \ . Front of drawers 1 -30.0 -14.7

Job Location: Achillion Pharmaceuticals, Inc. New Haven, CT Page: _2_of_7_ Survey Purpose: Decommissioning Tissue Culture Lab and Hall Date: 10/14/19

Number Time Location Inst. H-3 Activity 14C Activity Used (dpm/100 cm2) (dpm/100 cm2)

31 Inside drawers • 1 2.5 1.3 32 Upper wall 1 -5.0 8.0 33 Sink 1 -20.0 -6.7 34 Sink drain 1 -10.0 -1.3 35 Front of sink 1 -15.0 -5.3 36 · Upper wall 1 -17.5 -2.7 37 Counter 1 -7.5 1.3 38 Upper wall 1 -7.5 0.0 39 Lower wall 1 -17.5 -16.0 40 Upper wall 1 -22.5 -9.3 41 Lower wall 1 -12.5 -8.0 42 Upper wall 1 -17.5 -9.3 43 Shelf 1 -15.0 -6.7 44 Counter 1 12.5 18.7 45 Front of drawers 1 -22.5 -1.3 46 Top drawer 1 0.0 9.3 47 Drawer 1 -7.5 -2.7 48 Drawer 1 -7.5 -6.7 49 Bottom drawer 1 -2.5 5.3 50 Cubbv 1 -15.0 -12.0 51 Uooerwall 1 -20.0 ~1.3 52 Counter 1 -17.5 -6.7 53 Front of drawers 1 -5.0 5.3 54 Top drawer 1 5.0 12.0 55 Drawer 1 5.0 9.3 56 Drawer 1 -20.0 -13.3 57 Bottom drawer 1 -2.5 5.3 58 Upper wall 1 -17.5 -13.3 59 Counter 1 -20.0 -13.3 60 Front of left drawer 1 17.5 13.3 61 Inside drawer 1 -7.5 -1.3 62 Front of riaht drawer 1 -7.5 2.7 63 Inside drawer 1 -15.0 -5.3 64 Front of cabinet 1 -12.5 -5.3 65 Inside cabinet 1 -20.0 -9.3 66 Uooer wall 1 -10.0 12.0 67 Uooer wall 1 0.0 5.3 68 ,i. Lower wall 1 -10.0 6.7

Job Location: Survey Purpose:

Number Time

69 70 71 72 73 74 75 76 77 78 79 80 81 82 83 84 85 86 87 88 89 90 91 92 93 94 95 96 97 98 99 100 101 102 103 104 105 106 107 108 1 •

Achillion Pharmaceuticals, Inc. New Haven, CT Decommissioning Tissue Culture Lab and Hall

Location Inst. H-3 Activity

Page: Date:

3 of 7 · 10/14/19 -----

14C Activity Used (dpm/100 cm2) (dpm/100 cm2)

Upper wall 1 -12.5 -8.0 Lower wall 1 -7.5 10.7 Upper wall 1 -2.5 5.3 Lower wall 1 0.0 -2.7 Upper wall 1 -22.5 -17.3 Lower wall 1 -22.5 -8.0 Upper wall 1 -22.5 -8.0 Lower wall 1 -20.0 -2.7 Upper door 1 -20.0 -2.7 Lower door 1 -10.0 -2.7 Floor 1 -7.5 5.3 Floor 1 2.5 5.3 Floor 1 -10.0 -1.3 Floor 1 -20.0 -8.0 Floor 1 -15.0 -2.7 Floor 1 -7.5 4.0 Floor 1 -12.5 -8.0 Floor 1 -15.0 -5.3 Floor 1 -27.5 -16.0 Floor 1 -7.5 -5.3 Floor 1 -10.0 10.7 Floor 1 -2.5 2.7 Floor 1 -32.5 -13.3 Upper door 1 -25.0 -12.0 Lower door 1 -15.0 -5.3 Upper wall 1 -15.0 1.3 Lower wall 1 -5.0 5.3 Upper wall 1 -7.5 8.0 Lower wall 1 2.5 5.3 Uooer wall 1 40.0 26.7 Lower wall 1 -15.0 -6.7 Uooer wall 1 7.5 16.0 Lower wall 1 0.0 5.3 Uooer wall 1 12.5 10.7 Lower wall 1 10.0 22.7 Upper wall 1 -5.0 10.7 Lower wall 1 2.5 5.3 Upper wall 1 -7.5 9.3 Lower wall 1 -10.0 4.0 Uooer wall 1 -10.0 -4.0

Job Location: Achillion Pharmaceuticals, Inc. New Haven, CT Page: _4_of_7_ Survey Purpose: Decommissioning Tissue Culture Lab and Hall Date: 10/14/19


109 Lower wall 1 -10.0 4.0 110 Upper wall 1 -17.5 -6.7 111 Lower wall 1 -12.5 5.3 112 Upper wall 1 -10.0 1.3 113 Lower wall 1 -12.5 2.7 114 Upper wall 1 -12.5 -4.0 115 I Lower wall 1 7.5 9.3 116 Uooer wall 1 -10.0 1.3 117 Lower wall 1 -15.0 -9.3 118 Upper wall 1 -7.5 5.3 119 Lower wall 1 -2.5 0.0 120 I Uooer wall 1 -7.5 2.7 121 Lower wall 1 -2.5 -2.7 122 I Uooer wall 1 -12.5 -2.7 123 Lower wall 1 -20.0 0.0 124 Uooer wall 1 -2.5 0.0 125 Lower wall 1 -7.5 -1.3 126 Upper wall 1 -15.0 5.3 127 Lower wall 1 -27.5 -16.0 128 Upper wall 1 -17.5 -6.7 129 Lower wall 1 -7.5 6.7 130 Floor 1 -7.5 5.3 131 Floor 1 -7.5 -6.7 132 Floor 1 -15.0 -1.3 133 Floor 1 -17.5 -17.3 134 Floor 1 -22.5 1.3 135 Floor 1 -17.5 -10.7 136 Floor 1 -25.0 -2.7 137 Floor 1 -12.5 -6.7 138 Floor 1 -7.5 2.7 139 Floor 1 5.0 14.7 140 Floor 1 -15.0 -1.3 141 Floor 1 0.0 9.3 142 Floor 1 -2.5 -4.0 143 Floor 1 -5.0 -1.3 144 Floor 1 -10.0 -8.0 145 Floor 1 7.5 4.0 146 Floor 1 5.0 10.7 147 Floor 1 2.5 -9.3 148 'g Floor 1 7.5 1.3

\.

Job Location: Achillion Pharmaceuticals, Inc. New Haven, CT Page: 5 of 7 Survey Purpose: Decommissioning Tissue Culture Lab and Hall Date: 10/14/19 __ ____;........;.._


149 ~ Floor 1 -12.5 -4.0

"

. . . - - - - ·1r· ---i::n-~ • .-i-::-~.~~r-:--:rr.:r?.~~...,.~~....,~~.,,...'l\"--,--,:;,-""' .... ""1c"'!-~'.. .. - - -:- •• - ~ ....... :- .. - -~ - - - .. . .. - .••• -:- .. - -

o o O I I 0 ... - ·~ -- - ~ - - ... : - - ... - ~ ... - .. :- -- .. ! - - .... : .. -.- .. :- .. - -

o o ' I I • ' ' T I 'T • • • --•• •

I O O I 0 --·..:.::..:- .. -:- -~ .. ~ ----;. -... -~- ...... ; -.. -.. ~ -- .. -: .... -0 f I I '

-- I ~ •

0

I : I ! •••, ••• .••••

I ,; o o • • - • -r • • • -:· • • •, • • • • ~ • • ·-. ·"' • ·: - • • • r • • • ·- .. - ..

. . . . . :v~ --~----!----~---i·-·--:----~---~----· {--/~(~ :---~---+---f----~@e·.:··· ·:···-~---:··:·(@.:qa--:···f--·-

• 0 CJ I 1 • o , • o ' o I I I I • 0 o I I • I I I • I I I 0 ···-··-•r- ···~··••• .. ••·~·-··- ····•···~·•••••-••r -~---•·-·· I I o I I • I I

. . • • • • .. • ,. • •:• • • • O •,. •: •,. I•• • • : •••I • • • • ,.• • • •

O I .. I I • ~ I • f I ••, ••• ,..,..,. .. ••-•••• .

I I I I

f I • I

:: :: :: :: : -.:r... -i :J:__;.: ..)_ :_ r-h~--t ---+---1-...t q/· -~ ---~-.. q- ----~ --3·-·:··-1- -- · i· · .. f ·· · -~ · ·-: ·---/· · --~---~--- -~· ---~ @ f I I f I O I o I I I I I I · ---· ---· -~- ---r- ---~ -· -·:· · --: · --· :· ----~ --~ ~ ----8-·:· ---:-· --~ ----~ ---~------rr---- L ._i ®.@.:_· ___ J ____ ; ____ ~--- _i ____ t----~ ___ J ____ ; ___ ·-~-:-~---· ~ 1 0 o O I I I I I I I I I 0

·---: ---..: ....... :-- ... · --- ~-- ... ; ...... : -- ... :- .....

' ' I ' ' I -------- .--·-~----:---~----~-------------I I ' I I I o 0 .................. "': ... -- -:·- --~ -- . •,. -. ·;- .. •:- . .......... ... I ' • I • -· .--~ ---..:--- -.. ---- ~ ----- -- -~- ---· ... ----:. -- .. o • • o • I •

I I I I I I ' I • I . . . . . -·--:·---:--·-: ---:---·:---·-:--- :----~----:-

I I I I o I --~--- .. -----~--------,----~-

: : : ~: ; : : =@ • . • . • • • ,:1 1 I , f I I I I. r -...... --~ ----.. ---·'- --......... --: ) ....... -. - .. .. . : : : : : . +> : @'

4¥<--a~---;.--;---<~ -+·--:~ -®1 .. '8P . . /§';j). . . -.- -.. -~- -~· .. -:--·--:----~~----:- ....

-·--:----·;----:----: ---:----~----:----.---· I I I I

.... ~ ............... L .. ,..,.-. ...................... ~ .............. . I I I I

I I I I I . -.......... - ........... --· .... .,. __ --·- -............ ---• I O o I I •

. . --- :- --·: -- .. -: --- .. :- -- -~----: ·-. -:- ·--· :· ---r- --·-: ·---:--· .. ~----: ----:·--- :----:----=-···

I I o I I I I I

... : ... J ...... ~-- ..... ~ ••• ~ ... ---·----~---~--·-·----~-' ' ' i • • • • •

. . . . .............. ! ............................. ----~----~·- ~ - ' . . ----~------·-···--·---J··--~--·-~-------· I •• • • • I I o

---(. ·(- .; -··t ·-- i -- . -~ -- · ,; . · - ~ ----i · -. -;---i 3· (--i -· -1----;---t -- . 1tt . . . --------- --- .............. -- ................................ .. . .

1 - i i i r i 1 -i t i ! i !® r 1 1 . ----:--- :----:-·--: ..... ·:-·---:----~-- .. :----• I I •, I • . . . -..... -:··":"::~-- -·~----:----~------~-- --:- -·- ~-- --~ -- -:- -- .. ~-··- ~-·---:--·-..1-- --! ---~~ ..... ~ ......... . . '

.. ....... L ....... -'- • • .. J • ...... • • • ... • ......... 4 .. • •. I. ... • .. •"- ..... : I I I O t I I . ' • I I r • I I I ·---·----··--·-·-·---·-·--·----------·----~· ----· .......... --·. ----- ------ .... -·- --------··· I o o I I

• 1· • • • I • I ••••r•••, , '"'"t 1 .... , ........ ,••••r••••r••-• . : . ' : .

• • I o ----· -- ............ .I - - --~ ...... ··---· ......... 1. ............... . 1 0 1 I • I I t

,· I I o I I I 1 . . . --·~----··---~----··-·------------------·-- ____ .. ----- ............................ - -- ....... --- ........ _ ---. . . Swipe

I o I t I I I o I ··--~----y--••r•·-~·-••,.-·•·r··-~----,----r•• I I O •

o I I I. I O I f t I -,- ........ , ....... • r• -- -,- ...... ., ........ ,. ..... ·r • .... "'·• -· -- --~ • ... • -.- -. . I o I o • I I f ........ • ................... • ....... • ........ • ........ L ........ , ...... J ........ • .. ... I I O I I t I I I :"': ~:;::: --·-:----:- ...

0 D Air Sample I I I O I t I I I I ----~---------~--------4 .................. ~ ....................... -----~-----··------------·-·------4·--- ----~----·-. ' .

,. I I I I I I I I I• I I I ~--·' o I o r I o • ........ • .... ,- .... • •·-··r··--,-••• r·---r -- - ,.. .... • .. ,. ·-· -r ----.--- • "'-·····• -- • ..._ .......... ··-r• ·--,• ....... -· ••r ......... ,. • f 1 I I I I I I I I I er- I • I • I I I ' • I I • I

Meter Reading = Rad . Sunrey' iil µrem/h 1 I I o o I 1

: ~ : : : ~ : ~ : : : ~ : ; : .: : ! : . : I d loc.il. -:. I Pr

Job Location: /Jat11..UJ}J P,/M4YIM..='-v_.;"UI-O='--=---/.,.; ___ c._;;.;...· _ ...... M::W-=-:........lf-lbM!........_ ____ cr-___ Page: 7 of 7 Survey Purpose: (k-Cvw\.VII\.Lssto,,mv<,, 1-ftt:tLL. ~-_ Date:_::..../0+/..:...!'-f.L.j/i...:.r...1..1=====--Performed By: Wt o QY!&(£.eli ~ =

. . ' ' . . • • - - : ....... r - ..... ~ - - -:- .. - - ~ - .. -:- - .... ~ .. - ... i .. - .... ~ ........ ; .. - -·. : - .. - -:- · .... -:- - - • ~ .. - .... ~ ....... -:- • - ..

....... '····~----· --·-:----. ---·~--· ·--·. ~---' · ....... ; ....... ·-··-~---. ·--~···-. -·--~--. I I I t I I o • - - · - , • • •• ........ --,· - ----· --r .. ··--·- ,--· -·· ·-·r ·-· ·- · ..... , ·· · ---- ., .......... ••. ·-r ···---·· o • I I I : I • I • I

t O I I I I ... -~-- .... ; •. --~ ........ : .. ---~ .......... ;.. .... ··:· ---~- ---!----:- ---~ -·--~- ---:--'

' I I I I • I I ....................... - .......................... • ............... , .............. • ................................ .J ................. 1 ... .. I I I •I • I t I : I '

o I • I I I I I • "''"'., • .. "'"' •"" • '"'• f' • • • - • '"' - 't • • • """ • • •,• • • • • - • •"' r • • • •- .. •'"' 1 •"' "'•'"'"' • • "'1• .. "" '"'••"" .. "' T • • • .. "" • .. • . . . . . . . . :

i2~ ~ .;--~~--{ ~i ····:r··--:--·. -:~ .. --~-- ·:- ---·:---·~---.... --·-

I I I • O o o

-·\-·@)·1·-··f ·-·©.····f--·+·:_. -··· !1i····;····1··1··-·t··-1····f-···;\ ..... . ·---;---~---·: ··":··--;---~----i----·d -... . . , . • . . . . ~I

···+-~~···+··+---~~I-)··+··+·:· o I o 1 • o I o I I ,:; I O I I 0 • •••! ,..., ••~••• •: • •• ..:,- •--~-- --:-~ • • ~• •• -~ • • ••: • • • ,.::., •• •f-• ••~•• • •:••• • :••••: • ,..,,.;_,. .... ••• -~ ••• I .,,. ..;,. • •" ': •• ... ;.... 0 •• ••; ••••:••"'•• •oo• • I I t O I • O I

I O I I I I I I I O O ! I I I o' 0 o I • O I ...... ·----J,· .......... · ....... : ---· ----.~--- . _____ : ....... ' ...... :. --- · ... _:_ ....... :. ..... J,· ...... • ....... ~.· -- ,·; ~ : • : • : • .--·· .... ·- .. ··--. ··- .-·--.--··. ----' I I o I I O I I I I O o i : ; : : ~ : : ... '." ·-·:. ·- ·r·•··t .. -,----;--··' .... :· -··r ·- --:-·-;·· --~--. -:·-· --~--- .•. -· ·:-··- rcw·-;. -· r- ··:.· -. --@~ ·1·~, .. --~.·. ·-·;·r~-;; I I o I I I I I I I I I I I ~ ,o ---:----~·-··:--- .. :-- .... : .. --.~--··:----~··--:---·~·--:--.-~----: ..... ..: ..... · :----:. ............ ; .. ·.-- .. ..:----~---- ·-·- .... ; __ .. _ --

' . ' . ' . . ~ t I I I o • ' • , t I I 1 : I I I • I , I I I f -~•-••:....,..,..,J.,,...,..,~••••~•••~"'•••! ..... .' •• * . . ~ : . . . -: : ~ . . . -: . ~ : . .· . .· . ·. .3. .· ' I I I ' . I ' . I • • .......... ---~---- ... ----:-- ..... , ........ ~--- .. ----~----"···-~---··---~-- ............ ~--··•-·.·-~--- -------- .................. ~--------·~--·-·-- .. .

I I • I I I I I I I I I

:~:.: : @' . : : ~-. ~---~ 1·1; ··-:····:-···. •-,1-··:-···:··-· .... • .I I • ' • ;, , • • I I O t I I ••

I I I f I O r I I I I I I t I ---- :·-·-' -----: ..... .,: ...... :----:.. ..... : ........ ; ........ ! ----~--- ·:----~- .... :·---~----: ...... :.. ......

.... -; ........ .;. ...... -~-- .... ~ .. ·-! ... -- -~-- .. ""!'"' .... -.:----:-----;..---~ ··-· ~·--·:- ---..:----! ----·-~·-- ---- ~-·--- ... ---..:- .... -~ ....... ;. ___ .,._ -- -.;----· ...... . . . . .

. . I o • 0 I I f , I , • , t • • • f I I O • I o --"· tri~ · r · ·r--·®. -.~-!" ••• t ·-1 ·· ··®:· 4 -~ ·--i~.:;-r · ·· ·t~---;---·r ---~ ~-·-r-· -?- · · ;----r~·-1----r-~-

- - . _;_. ~--~- --.:. ---~ L_ _ ____ :. .. - ~- --- .. - . -·. ;..,s __ ; ____ ~ ~---:----~--- .:.\.!g;J'---~----=- -- . : ---- :-~--~- -__ : ___ _ I I • I t t • I I I I I I I I I I I I I I t f o I I I I I I I O f I I I O f I I t t I

·1 1 1 1 ·,. ; , o I f I I I I o , 1 · ( ! i t 1 1 · i t i 1 i ! 1 t ~ 1 i i 1 . '. ! ·1 -~ ,~o ......... • .. • ~ .. ~L,:..::.- L ..................... _. .......... lo ...... •'• ...... _. ....... • L • ... •,.to. ...... .J .. ,.,.. • •• .. ••'• .. ..,.,J .... -- J. ....... .b-....... • ........ ~ ......... L ...... - ......... •• _. ........ ., .. • ... •'• .. ,. .. C-.. • l • ' • I I I t I I I t I I • I I I ,I I I I I ' o • I I O I t I I f I O I I I I • I I I • I O I t • t t . -. -; . --~-- -+ .. ~--. ~~(~ --. ~- .. -~ .. -t~ f--. ~ -- .. ; .. -~ ----;--. -~ -·- ~-~ . -~ .. -i_ ... ·· . \- -- -~ -·. :- . -. ;- . --: -~-... ..:. ·®·. ;. ---:- ·--~ ~--.. ; .... -:-- --'C3'-~ ---..:----}----~----;. ··+·-~-~---~ ----:- ~-- ; ____ (i@ __ + -.. ; ·-·· : . : : : : :? : : : : : : : : : : : : : : : : : : . 1 I I I I I~ o I , I I O I I O t I o O t O I I I - - .. -:- .. - ·!- - - ·:----J···--~ ·-·-:-·-- -:-· -- ~ ----;- -- -·- - .) ....... ~ ...... •:---- _. ____ !.... -:- ..... {'----~---·'· -- . ---~ - .. --~ .... ·-:·---'- ·--~ ......... . '

, 1 I I I I 1 1 f 1 1 0 Io I I I I I I 0 .... • - ., ... - - 1' - • • •r-•••·,· ·• .. T .. • •·r··· .,. .. ·-- ,-- - •r • ...... , ...... ·, ..... •• r• ........... ., ......... , ........ ·r • ·-"' •• •• r •• .... ,.. • •'" ..... . I I I 1 • I I I I I I I . Swipe I I I I I o I I I I ----:-·- .. ~ .. -..... : ----.--·- :--·-~--·-: ---~-----: --··~--- : .. -·-!·---:---:----;----~--- :----~--·-: ·--·: - D I I I I f I I t I •

' Air Sample I o I • I I I I I I I I --.. """· -- ............. ---------· ....................... --- ............ ·---- ....................................................... --- ........... -- - ... -- .. -- .. I I t I I • I o • I • I I

0 I I I I I • I I I I I O t t t I t I I ···~ ....... , ................... ~---,-••·r·-·-r··-,---·~····r··-~--··1····•···~··••,••··r··-~···-,····•·-··~-' I : I I I O I : I I I I t : I I I

Meter Reading = Rad . Survey" iil µrem/h I I I I I o I I I t I ---- :------t .. ··-: --- :---· :-·--~----:·---~·--·: ----:---- :·-·-t----: --- :·---:·-- .: ---~----~-·-·: ---:·-• I

I I I I •• I tjc.tlf.. ::= I ,er

Job Location: Achillion Pharmaceuticals, Inc. New Haven, CT Page:~1~of~8~ Survey Purpose: Decommissioninq Molecular Bioloqy (A&B) Date: 10/14/19 Performed By: David Durkee ......... , r-.. ~~

Inst. No. 1 (Model/SN) Inst. No. 2 (Model/SN) I Inst. No. 3 (Model/SN)

PE Microbeta 2450 #04130262 Ludlum 2241-2 #137751 Bicron uRem LE B466Y Detector (Model/SN) Detector (Model/SN) Detector (Model/SN) Internal Ludlum 43-68 #140899/ Ludlum Internal

43-37 #143616

Efficiency::::: 40% 3H / 75% 14C Efficiency: 8.6%/8.69% C-14 Efficiency: 100% Type Rad.: 13 Type Rad: 13 Type Rad.: V Bkad.: See #1 Below Bkgd.: 256 cpm / 864 cpm Bkad.: 4 - 8 uRem/hour Cal. Due: 04/01/20 Cal. Due: 01/07/20 Cal. Due: 01/15/20

Number Time Location Inst. 3H Activity 14C Activity Used (dpm/100 cm2) ( d pm/100 cm2)

1 1000 Background 1 10 cpm 40cpm

2 Upper Wall 1 10.0 -16.0 3 Lower Wall 1 27.5 -12.0 4 Upper Wall 1 12.5 -16.0 5 Lower Wall 1 0.0 -18.7 6 Upper Wall 1 -5.0 -21.3 7 Lower Wall 1 27.5 -16.0 8 Upper Wall 1 12.5 -13.3 9 Counter 1 7.5 -16.0 10 Sink 1 7.5 -13.3 11 Sink Drain 1 -2.5 -22.7 12 Front of Drawers 1 7.5 -20.0 13 Front of Cabinets 1 10.0 -16.0 14 Left Drawer 1 22.5 -2.7 15 Riqht Drawer 1 25.0 -5.3 16 Inside Cabinet 1 32.5 -6.7 17 Front of Sink 1 -2.5 -21.3 18 Upper Wall 1 0.0 -14.7 19 Lower Wall 1 -7.5 -25.3 20 Upper Door 1 10.0 -17.3 21 Lower Door 1 5.0 -20.0 22 Wall 1 5.0 -20.0 23 Side of Hood 1 20.0 -12.0 24 Outside Hood Sash 1 17.5 -17.3 25 Inside Hood Sash 1 12.5 -16.0 26 Hood Counter 1 7.5 -12.0 27 Back of Hood 1 12.5 -9.3 28 Left Wall Inside Hood 1 10.0 -13.3 29 Riqht Wall Inside Hood 1 15.0 -12.0 30 I • Hood Duct 1 2.5 -25.3

Job Location: Achillion Pharmaceuticals, Inc: New Haven, CT Page: 2 of 8 Survey Purpose: Decommissioning Molecular Biology (A&B) Date: 10/14/19 -----


31 Front of Cabinets 1 2.5 -24.0 32 Inside Left Cabinet 1 10.0 -10.7 33 Inside Riqht Cabinet 1 5.0 -20.0 34 Side of Hood 1 2.5 -17.3 35 Upper Wall 1 20.0 0.0 36 Lower Wall 1 7.5 -10.7 37 Shelf 1 17.5 -1.3 38 Shelf 1 27.5 1.3 39 Counter 1 17.5 -9.3 40 Front of Drawers · 1 17.5 -1.3 41 Left Drawer 1 0.0 -14.7 42 Riqht Drawer 1 12.5 -9.3 43 Front of Cabinets 1 22.5 6.7 44 Inside Cabinets 1 15.0 -5.3 45 Shelf 1 -2.5 -22.7 46 Shelf 1 7.5 -18.7 47 Counter 1 2.5 -14.7 48 Cubbv 1 5.0 -12.0 49 Shelf 1 30.0 -4.0 50 Shelf 1 5.0 -26.7 51 Counter 1 25.0 ·-5.3 52 Front of Drawers 1 -5.0 -13.3 53 Left Drawer 1 12.5 -10.7 54 Riqht Drawer 1 35.0 1.3. 55 Front of Cabinets 1 12.5 -9.3 56 Inside Cabinets 1 35.0 4.0 57 Side of Cabinet 1 5.0 -20.0 58 Side of Cabinet 1 7.5 -13.3 59 Counter 1 -2.5 -14.7 60 Front of Drawers 1 2.5 -20.0 61 Left Drawer 1 37.5 1.3 62 Riaht Drawer 1 10.0 -9.3 63 Front of Cabinets 1 25.0 -5.3 64 Inside Cabinets 1 25.0 -6.7 65 Counter 1 10.0 -8.0 66 Cubbv 1 5.0 -5.3 67 Counter 1 7.5 -13.3 68 , , Front of Drawers 1 12.5 -13.3

Page: 3 of 8 - -Job Location: Achillion PharmaceuticalsLlnc. New Haven, CT Survey Purpose: Decommissioning Molecular Biology (A&B) 10/14/19 Date:_....;..;;.;....;._ __


69 Left Drawer 1 7.5 -22.7 70 Riqht Drawer 1 0.0 -8.0 71 Outside Cabinet 1 2.5 -16.0 72 Inside Cabinet 1 0.0 -21.3 73 Front of Drawers 1 17.5 -12.0 74 Left Drawer 1 25.0 -2.7 75 Riqht Drawer 1 -7.5 -25.3 76 Inside Cabinet 1 20.0 -16.0 77 Outside Cabinet 1 27.5 2.7 78 Cubbv 1 -7.5 -26.7 79 Front of Drawers 1 10.0 -13.3 80 Left Drawer 1 12.5 -16.0 81 Riqht Drawer 1 22.5 -14.7 82 Front of Drawers 1 2.5 -25.3 83 ii Inside Cabinet 1 25.0 -12.0 84 Side Counter 1 17.5 -17.3 85 Floor 1 12.5 -17.3 86 Floor 1 27.5 -6.7 87 Floor 1 -5.0 -22.7 88 Floor 1 15.0 -12.0 89 Floor 1 202.5 250.7 90 Floor 1 -7.5 -17.3 91 Floor 1 10.0 -21.3 92 Floor 1 22.5 -6.7 93 Floor 1 5.0 -8.0 94 Floor 1 12.5 -10.7 95 '; Floor 1 2.5 -16.0

' 96 Floor 1 27.5 -2.7 97 Floor 1 42.5 4.0 98 Floor 1 42.5 13.3 99 Floor 1 5.0 -20.0 100 Floor 1 22.5 -4.0 101 Floor 1 25.0 0.0 102 Floor 1 27.5 -9.3 103 Floor 1 25.0 -13.3 104 Floor 1 · 22.5 -1.3 105 Floor 1 17.5 -5.3 106 Floor 1 7.5 -18.7 107 Floor 1 0.0 -20.0 108 1\1' Shelf 1 12.5 -16.0

Job Location: Achillion Pharmaceuticals, Inc. New Haven, CT Page: _4_of_8_ Survey Purpose: Decommissioning Molecular Biology (A&B) Date: 10/14/19


109 Shelf 1 12.5 -12.0 110 Counter 1 22.5 -5.3 111 Shelf 1 22.5 -2.7 112 Shelf ' 1 22.5 -4.0 113 Counter 1 22.5 -8.0 114 Shelf 1 -5.0 -18.7 115 Shelf 1 17.5 -4.0 116 Counter 1 17.5 -2.7 117 Counter 1 5.0 -25.3 118 Counter 1 7.5 -16.0 119 Front of Drawers 1 5.0 -21.3 120 Left Drawer 1 27.5 10.7 121 RiQht Drawer 1 0.0 -14.7 122 Front of Cabinets 1 10.0 -9.3 123 Inside Cabinet 1 20.0 -13.3 124 Counter 1 2.5 -24.0 125 Cubbv 1 5.0 -10.7 126 Counter 1 12.5 -14.7 127 Front of Drawers 1 -5.0 -26.7 128 Left Drawer 1 7.5 -18.7 129 Riqht Drawer 1 -2.5 -18.7 130 Front of Cabinets 1 15.0 -16.0 131 Inside Cabinet 1 5.0 -21.3 132 Side of Cabinet 1 2.5 -17.3 133 Side of Cabinet 1 2.5 -22.7 134 Front of Drawers 1 15.0 -24.0 135 Front of Cabinets 1 5.0 -20.0 136 Left Drawer 1 0.0 -17.3 137 Rioht Drawer 1 12.5 -9.3 138 Inside Cabinet 1 12.5 1.3 139 Uooer Door 1 10.0 -12.0 140 Lower Door 1 17.5 -5.3 141 Uooer Wall 1 2.5 -16.0 142 Lower Wall 1 22.5 1.3 143 Uooer Wall 1 12.5 -6.7 144 Counter 1 12.5 -12.0 145 Uooer Wall 1 30.0 -6.7 146 Shelf 1 17.5 -9.3 147 Front of Drawers 1 25.0 -6.7 148 • Inside Drawer 1 20.0 -10.7

I

Job Location: Achillion Pharmaceuticals, Inc. New Haven, CT Page: _5_of_8_ Survey Purpose: Decommissioning Molecular Biology (A&B) Date: 10/14/19


149 Front of Cabinet 1 -2.5 -28.0 150 Inside Cabinet 1 10.0 -16.0 151 Front of Drawer 1 -5.0 -20.0 152 Inside Drawer 1 30.0 -6.7 153 Front Cabinet 1 7.5 -18.7 154 Inside Cabinet 1 2.5 -13.3 155 Front of Drawer 1 22.5 -8.0 156 Inside Drawer 1 5.0 -9.3 157 Front of Cabinet 1 12.5 -12.0 158 Inside Cabinet 1 37.5 -2.7 159 Front of Drawer 1 27.5 -5.3 160 I Inside Drawer 1 27.5 -6.7 161 Front Cabinet 1 45.0 8.0 162 Inside Cabinet 1 17.5 -6.7 163 Cubby 1 12.5 -13.3 164 Front of Drawer 1 20.0 -6.7 165 ~ Inside Drawer 1 0.0 -22.7 ' 166 Front of Cabinet 1 7.5 -25.3 167 Inside Cabinet 1 12.5 -16.0 168 Front of Drawer 1 20.0 -4.0 169 ~ Inside Drawer 1 12.5 -13.3 170 ~ Front of Cabinet 1 -5.0 -30.7 171 Inside Cabinet 1 5.0 -14.7 172 Side Cabinet 1 25.0 -10.7 173 Upper Wall 1. 10.0 -13.3 174 Shelf 1 25.0 -8.0 175 Counter 1 40.0 -1.3 176 Upper Wall 1 12.5 -10.7 177 Shelf 1 7.5 -14.7 178 Counter 1 10.0 -8.0 179 Upper Wall 1 25.0 -4.0 180 Shelf 1 12.5 -14.7 181 Upper Wall 1 10.0 -17.3 182 I Lower Wall 1 22.5 -12.0 183 Upper Wall 1 15.0 -14.7 184 Lower Wall 1 7.5 -16.0 185 Upper Door 1 20.0 -10.7 186 Lower Door 1 5.0 -16.0 187 '. Upper Wall 1 0.0 -14.7 188 Lower Wall 1 -2.5 -20.0


Number Time

189 190 191 192 193 194 195 196 197 198 199 200 201 202 203 204 1 •

205 1700 206 I 207 J,

Achillion Pharmaceuticals, Inc. New Haven, CT Decommissioning Molecular Biology (A&B)

Location '

Inst. H-3 Activity

Page: Date:

6 of 8 10/14/19 -----

14C Activity Used (dom/100 cm2) (dom/100 cm2)

Upper Door 1 22.5 0.0 Lower Door 1 2.5 -13.3 Floor 1 20.0 -12.0 Floor 1 7.5 -12.0 Floor 1 12.5 -22.7 Floor 1 17.5 -9.3 Floor 1 22.5 -9.3 Floor 1 -5.0 -28.0 Floor 1 12.5 -12.0 Floor 1 2497.5 1312.0 Floor 1 2.5 -21.3 Floor 1 -10.0 -30.7 Floor 1 7.5 -16.0 Floor 1 12.5 -2.7 Floor 1 2.5 -12.0 Floor 1 12.5 -20.0 Post Decon #89 1 30.0 -4.0 Post Decon #198 1 22.5 -12.0 Post Decon Counter 1 20.0 -4.0

I I I e I t I I I I I ' I .. ---: ... ---~·---: ----, ....... ; .. ---~----: ·--~--·-:--·-:---- :--·-!·---: ---~----;-- .. -~--- :----~----: ......... :--' ' '

I I o I I f f I I f I I I --......................... --------" ....................................... ----- .......... --- .............. -------· ........................... --- ..... - ....... .. • I I I t I t I t I I t • 1 I

' ' ' t I 1•

-.... ..: .. ... --~- ..... -~--- .. :---- ~--- .. ~-·--~ .. -- ~ ....... -~- ....... ~---..:- .... -; ........ :.. .... . ..:; .. ...... ~ .. ---~ ..... .; ........ ~ - -..... ~ ......... : .... I I • I I I I I I I 1

' ' I I I I I I t t f I I I I I I I ....... :-- .. ·t--·-: ....... ----:---·~---·:·---~--·-: ...... : ........ :·---;-·-·: -·-:----:·-- .: ...... :---·!----· --- :-• I I I I,

0 D

7 of 8 A, 1t,d1 ,---, ,

Swipe

Air Sample

Meter Reading = Rad . Survey in .µrem/h

Is~ 'e.. 1,:.r

'·\ #If

I ob Location: l-k,#11..u~ _ _J,J?1,4,n14-(.o.JnU4f...b h.: c.. rvtW /.11MJ,u1 c.T Survey Purpose: &.:..'YV\11'11\l!.5.<l}w,wb MQL.eLuL.M.. &ot.c~ Ld3 Performed By: i)twi) Ov.a.fu~ . ~

tnPr(" l!,

I I O I ----:----~----~ - - -· - .. - - .. - - . ·' - - • - " .. - - . ! • - - - .. - - - ·'· ...... - • - - ·- •• -• I I I O I I 1 ,

' ' ' :· •i. --~ -···:· ·- ·: ----~- .. ~--· ~; ... ! : .. --~ .. ·: .... ;

.... J .. _! :- . ~~~-- -~'-94 .<n~--0~~~ -/~{1!) -~--'

. . T I I I I J ____ ._ ____ • ____ .. ____ • ___ ... ____ • ................. , --··--· -·

I ' 0 I I I I I 0

I I O I I I • • •, .. • - • I • .. • •r .. • • I.,.• .. •.,. - • • -. • •.., ... • •" • '• • • •,. • • "•, ., • • f' • - •"I • • •

1 1 I I I o I I I , I ---~----~----;----~---r----r---~----,----:----~---7·-~-~---• 1 I ' I r ' I

• I I I I I I ............. ; ........... : ................ ; ···-·----:----~·---:----·-·--:-··

• I I I I I . --- ... ----·----~----~--··----'-----.----·----~-----·-···---·---. , . . . . . 1 I I I I I I

····-i·---~----:----~---+---~----:·-··:····!····-~--~f-··-~---{ >F+z: (.I . . I I I I I I I ---~----T----•----~---~----~---~----~----•·---~---~----~---' t • I • •

' O "o I I I T I I o ----i----~----~---~----J----~---~----~----~---~----i----~--~ . ' . . . , . -- -·-- .. -.. -........ --·---- ............ --- -·- -.. -·-- .... ·--- ...... --4- ... -·---• I I I I I 1 0 0 I

1 I I I I I o I I ••"'- • •• •• ---r-•• ........ • , .. • ........... •,• • .,_ "' .... ·-r•• • . . .

Page: 8 of & Date: 1r:>/t'J..V'I

t·•

I • ' o ··;····.·--·~---·.-·---. ...... . . ~-~---~----i----·----~-~-

----:- --.. ~ -- · -~ ----i- -- -~----; ......... : ... -- ~ .. -.. -r--- .. : .. - .. - ~ .. · --:--- -· -u ... : .. ---i -. --·~- ..... -: .. ---f-- --:- ----:- ··- -~ - --:- -- .. :- -· · ~-· --~-- ... :- -: : : ' : : : : : : : : : : J : : : : : -i (['Tu');: : : ··"-~----1-···r ---+---t··-·t··-~----1-·-·t-··t·--1·-··t··· -···(·-1 --(··1----(··t---~--, -~ · 1···j-@··\·· ···-:·---~----~---.:.·-·:·---~----~---!·---~----~·-·:····:··- ·--~---~· 4--~---~----~· q6: ···-:- f;?; -~--- .-·· ~-- :----~-·-' Iii\ . . . . . . . . . . ••••.;••••i ....... :.,. .. .,,.: ..... ~.,.,,..., ..... -~----~----~- •---~•-• I .... :,. ... .,~----, .. : ..... ., .. :., I : ,: : : : : · : : : : : : ·: : : : : : : : : : : : ~l : 162 ·: jt,'b ----!-··--~----~---~ioo1 ~~ ; @j [5q --·i·--+--:~----!--·-1---+---~ ·--~---+---;----~--··: -___ ; __ ) __ .[._ __ : __ .; -) .... : _ ;_J.__( ___ : i' .L .. L.L.] .. : __ j__ __ j ____ [ __ _j. ___ i .. ..t.):j ____ : L.

·: :t:t::r::+,::r::,:t:::f ::f :~::::i:::L:~::J::::f :::t:i~:t::t!t: . . . . . . . . . . . . . ' . . . . . .-------....... ---~---. . . : : : : : ! : : : : ; : : ;.3 : : : I - - - _,;_ - -- ; - -- -~ -- ··[·· •• ;. • --:-- •• .;. --- ; c') · -~ • •· -:- -- • ~ • • -- ~----!--- -~ ----: -·- ·i- • ··, • ··, -- --:.- • • ~-- Q Swipe o I I I I I I ,t,._.:. I I I I I I I I f I I I I I I I I I I I I • I I I f f I I I I O I I I I O O I I I I I I I I f f I I I :- .. --:- -.. · t · .. --:- .. -~--- -:-- .. -:- -- -"t .. -· t. -.. -:-· -~- -- -:-- -·:-- --;-. -- :- .... -:- .. --:-- .. --: .. -··t .. ---:

I r I I I I t I I I I I I o I I I I I I I I I o I o I I o I I t I I I I I I I I ----~--···----~---~ .......... ~---~---------~-----·-··----·----~------- .. ·--------~-------·-~-----· I I I I O I I I I I I I I I I o • .1 I I I I I t I I o I I • 0 1 o I I O I I I I I I" I f I -.... ..: .. -..... ~-- .... ~ ----:---- ~-- .. -~ ........ ~ --- ~--- .. :- -- ... ;. .. --..:- -- .; ..... -~-- . ...; ... --- ~- -- -~- __ ..; ........ ~ .. ---~ ........ : .. -f I I I I I I I o I I I I . . .

D Air Sample

Meter Reading = Rad . Survey in µrem/h I I I I o I O I I I - --- ----~·--- ....... :---- :·---~--·-:-·--~----: ----:-·-- :·---~----:---- :·---:··- .; --- ;----!-- ..... : ----:--

I (J!d<./c. :. / ,Cr

Job Location: Achillion Pharmaceuticals, Inc. New Haven, CT Page: 1 of 7 Survey Purpose: Decommissioninq Molecular Bioloqy (C&D) Date: 10/14/19 Performed By: David Durkee ~ -,

Inst. No. 1 (Model/SN) Inst. No. 2 (Model/SN)' Inst. No. 3 (Model/SN) PE Microbeta 2450 #04130262 Ludlum 2241-2 #137751 Bicron uRem LE B466Y Detector (Model/SN) Detector (Model/SN) Detector (Model/SN) Internal Ludlum 43-68 #140899/ Ludlum Internal

43-37 #143616

Efficiency: ::::: 40% 3H / 75% 14C Efficiency: 8.6%/8.69% C-14 Efficiency: 100% Type Rad.: B Tvpe Rad: S Type Rad.: V

Bkgd.: See #1 Below Bkgd.: 256 com/ 864 com Bkgd.: 4 - 8 uRem/hour Cal. Due: 04/01/20 Cal. Due: 01/07/20 Cal. Due: 01 /15/20


1 1245 Background 1 23 cpm 36cpm 2 Upper Door 1 -17.5 -5.3 3 Lower Door 1 -25.0 -18.7 4 Upper Wall 1 -10.0 9.3 5 Lower Wall 1 -25.0 -10.7 6 Upper Wall 1 -20.0 1.3 7 Lower Wall 1 -32.5 -13.3 8 Upper Wall 1 -15.0 -12.0 9 Lower Wall 1 -27.5 -20.0 10 Upper Wall 1 -10.0 8.0 11 Lower Wall 1 -10.0 0.0 12 Counter 1 -22.5 -10.7 13 Counter 1 -7.5 1.3 14 Counter 1 -25.0 -9.3 15 Upper Wall 1 -17.5 -6.7 16 Lower Wall 1 -25.0 -17.3 17 Upper Wall 1 -32.5 -22.7 18 Lower Wall 1 -22.5 -6.7 19 Uooer Wall 1 -7.5 0.0 20 Shelf 1 -20.0 -16.0 21 Shelf 1 -27.5 -5.3 22 Counter 1 -32.5 -14.7 23 Front of Drawers 1 -22.5 -8.0 24 Left Drawer 1 -37.5 -10.7 25 Riqht Drawer 1 -27.5 -5.3 26 Front of Cabinets 1 -10.0 -2.7 27 Inside Cabinet 1 -7.5 -4.0 28 Shelf 1 -15.0 -10.7 29 Shelf 1 -17.5 -10.7 30

, ,, Counter 1 -5.0 6.7


Number Time

31 32 33 34 35 36 37 38 39 40 41 42 43 44 45 46 47 48 49 50 51 52 53 54 55 56 57 58 59 60 61 62 63 64 65 66 67 68 1 ,

Achillion Pharmaceuticals, Inc. New Haven, CT Page: 2 of 7 10/14/19 Decommissioning Molecular Biology (C&D) Date: -----

Location Inst. H-3 Activity 14C Activity Used (dpm/100 cm2) (dpm/100 cm2)

Cubby 1 -12.5 -5.3 Shelf 1 -30.0 -8.0 Shelf 1 -22.5 -9.3 Counter 1 -35.0 -5.3 Front of Drawers 1 2.5 8.0 Left Drawer 1 -27.5 -14.7 RiQht Drawer 1 -20.0 -2.7 Front of Cabinets 1 -25.0 -10.7 Inside Cabinets 1 -20.0 -6.7 Front of Drawers 1 -25.0 -9.3 Front of Cabinets 1 -10.0 -5.3 Left Drawer 1 -17.5 -9.3 Rioht Drawer 1 -32.5 -20.0 Inside Cabinets 1 -15.0 -9.3 Counter Around Sink 1 -37.5 -25.3 Side of Cabinet 1 -17.5 2.7 Sink 1 -45.0 -25.3 Sink Drain 1 -27.5 -13.3 Front of Drawers 1 -32.5 -6.7 Front of Cabinets 1 -2.5 0.0 Left Drawer 1 -22.5 -14.7 Rioht Drawer 1 -27.5 -22.7 Side of Cabinet 1 -20.0 -5.3 Counter 1 -25.0 -16.0 Counter 1 -27.5 -8.0 Counter 1 -22.5 -12.0 Front of Drawers 1 -2.5 -1.3 Front of Cabinets 1 -2.5 6,7 Left Drawer 1 -15.0 -12.0 Rioht Drawer 1 -22.5 -6.7 Inside Cabinets 1 -27.5 -12.0 Front of Drawers 1 -37.5 -13.3 Left Drawer 1 -17.5 -5.3 RiQht Drawer 1 -20.0 -5.3 Front of Cabinets 1 -32.5 -13.3 Inside Cabinets 1 -22.5 -9.3 Cubbv 1 -17.5 -8.0 Front of Drawers 1 -30.0 -6.7

Job Location: Achillion Pharmaceuticals, Inc. New Haven, CT Page: 3 of 7 Survey Purpose: Decommissioning Molecular Biology (C&D) Date: 10/14/19 .


69 Front of Cabinets 1 -15.0 1.3 70 Left Drawer 1 -27.5 -8.0 71 Riaht Drawer 1 -32.5 -12.0 72 ' Inside Cabinet 1 -22.5 -12.0 73 11 Uooer Wall 1 -25.0 -13.3 74 Lower Wall 1 -15.0 -9.3 75 Floor 1 -12.5 -2.7 76 Floor 1 -32.5 -17.3 77 Floor 1 -5.0 2.7 78 Floor 1 -25.0 -18.7 79 Floor 1 -37.5 4.0 80 Floor 1 -7.5 8.0 81 I Floor 1 -15.0 -9.3 82 ~ Floor 1 -22.5 -6.7 83 Floor 1 -12.5 -9.3 84 Floor 1 -5.0 2.7 85 Floor 1 -35.0 -4.0 86 Floor 1 -15.0 -1.3 87 Floor 1 -2.5 4.0 88 Floor 1 -22.5 -4.0 89 Floor 1 32.5 18.7 90 Floor 1 -22.5 -14.7 91 Floor 1 -10.0 1.3 92 Floor 1 -30.0 -25.3 93 Floor 1 -17.5 -9.3 94 Wall 1 -27.5 -16.0 95 Front of Drawers 1 -35.0 -12.0 96 Front of Cabinets 1 -27.5 -8.0 97 ~ Left Drawer 1 -12.5 -2.7 98 I Riaht Drawer 1 -22.5 -2.7 99

,\

I Inside Cabinet 1 -5.0 4.0 100 Counter 1 -27.5 -8.0 101 Shelf 1 -27.5 -12.0 102 Shelf 1 -22.5 -10.7 103 Shelf 1 -15.0 4.0 104 Shelf 1 -12.5 -9.3 105 Counter 1 -15.0 -1.3 106 Cubby 1 -25.0 -10.7 107 Shelf 1 -25.0 -13.3 108 I 7 Shelf 1 -30.0 -5.3

Job Location: Achillion Pharmaceuticals, Inc. New Haven, CT Page: _4_of_7_ Survey Purpose: Decommissioning Molecular Biology (C&D) Date: 10/14/19


109 Shelf 1 -12.5 -2.7 110 Shelf 1 -22.5 0.0 111 Counter 1 -10.0 2.7 112 Counter 1 -17.5 1.3 113 Front of Drawers 1 -35.0 -5.3 114 Front of Cabinet 1 -22.5 -13.3 115 Left Drawer· 1 -10.0 2.7 116 Rioht Drawer 1 -25.0 -12.0 117 Inside Cabinet 1 -22.5 -6.7 118 Cubby 1 -20.0 -9.3 119 Front of Drawers 1 -17.5 5.3 120 Front of Cabinet 1 -37.5 -18.7 121 Left Drawer 1 -32.5 -6.7 122 Riqht Drawer 1 -30.0 -1.3 123 Inside Cabinet 1 -22.5 -10.7 124 Side of Cabinet 1 -32.5 -5.3 125 Side of Cabinet 1 -20.0 -2.7 126 Counter 1 -27.5 -6.7 127 Counter 1 -17.5 -6.7 128 Counter 1 -32.5 -12.0 129 Counter 1 -22.5 -12.0 130 Front of Drawers 1 -30.0 -13.3 131 Front of Cabinet 1 -25.0 -1.3 132 Left Drawer 1 -20.0 0.0 133 Riqht Drawer 1 -15.0 -12.0 134 Inside Cabinet 1 -15.0 -6.7 135 Cubbv 1 -17.5 1.3 136 Front of Drawers 1 -10.0 -5.3 137 Front of Cabinet 1 -30.0 -13.3 138 Left Drawer 1 -25.0 -4.0 139 Riqht Drawer 1 -15.0 1.3 140 Inside Cabinet 1 -17.5 -1.3 141 Cubby 1 -12.5 1.3 142 Front of Drawers 1 -25.0 -17.3 143 Front of Cabinet 1 -30.0 -17.3 144 Left Drawer 1 -12.5 -6.7 145 Riqht Drawer 1 -15.0 -9.3 146 Inside Cabinet 1 -20.0 -14.7 147 UooerWall 1 -15.0 -8.0 148 '1 Lower Wall 1 -27.5 -16.0

Job Location: Achillion Pharmaceuticals, Inc. New Haven, CT Page: _5_of_7_ Survey Purpose: Decommissioning Molecular Biology (C&D) Date: 10/14/19


149 Upper Wall 1 -27.5 -12.0 150 LowerWall 1 -7.5 4.0 151 Uooer Wall 1 -10.0 -2.7 152 Lower Wall 1 -17.5 -6.7 153 Uooer Wall 1 -10.0 -4.0 154 Lower Wall 1 -25.0 -9.3 155 Uooer Wall 1 -10.0 1.3 156 Lower Wall 1 -30.0 -14.7 157 Uooer Wall 1 -37.5 -1.3 158 Lower Wall 1 -5.0 1.3 159 Floor 1 -27.5 -20.0 160 Floor 1 -35.0 -13.3 161 Floor 1 -32.5 -10.7 162 Floor 1 -32.5 -16.0 163 Floor 1 -10.0 -12.0 164 Floor 1 . -15.0 -5.3 165 Floor 1 -17.5 1.3 166 Floor 1 -27.5 -6.7 167 Floor 1 -27.5 -9.3 168 Floor 1 -25.0 -17.3 169 Floor 1 -32.5 -21.3 170 Floor 1 -17.5 -6.7 171 Floor 1 -30.0 -18.7 172 ~ . Floor 1 -17.5 -5.3

Job Location: /k..l+'lluow 11~Acwnq...tLJ - twc. /U.w ~ c;:r- Page: ~ of 7 Survey Purpose: De-~~~-s,,w,w<. (?1QLe-cvL...11l.. 61c:>Lo&j U'irl Date: tolr'.f,.h? -~-Performed By: t)l'VI b \)~tus- ~*== r I

frl~ ·c

I I I I I I I I I I I I I I I I I I I •·y·---~---~--·-!····r--·~----~----~----~·-•,••••r··-~---- .. ---·:··-·r··-~----r----~---~--' . 0 Swipe

I I I I t I I f I

Air Sample ----:----~--·-: ----: .. ---:----~----: .. ---:----:----~--- :---·! .... ---: ---~----;----~--- :----~----: ----!-- D I I • I I I I I I I I

01 I I

I I I I I I I I f I I I I I - -................. --~ --------· .................... --- _____ .. ----- ·-· ............... --'-·-··----·-·------ ........... -- - ... -- .. -- -• I I I I • • 1 I

I I I I I I O I I I • I f o I t f I I Meter Reading = Rad . • ·• .... "'·-,- • • •,. - ·-·.---- ., •••• ,. ....... ~ ··- ...... '"'" ·-- -,----~- ·· ·, ........ •• .... , .............. -·-r• ... .., ........ , • · ........... ,. • I I I I I I • I I I I I I I I I I I I . . Survey in µrem/h I I I I I I I I I I t I --·- : ... ·-·~···-: ....... : .......... : ... -..... ~ ........ :- .. --~·---:-·--:--·-:·---;-·-·:---· :----:·-- .; .... -:---·!·-·-:--- :--/ /3loUL = 1 r-1

\ \

..

Job Location: /laf1LJ.w>J -P~wn(:(4ls /pie 1z.ov ,~ er Page: ~ of 7 -----s u rvey purpose :_:::;~.,:cr_..C.vW\=:..;:.:.;ll'lllc:::l,.,SS..,_( u.:..:.n=-''......;""--=(,'---__ MiJ...;.=£.Gc..:;:r._~..:;_1-:...,i,tt.._..c.8_1o_Lo ___ o'1+---iL-,1j Date: A, ./ry U2 Performed By: Ol'-/10 Ov(U6:.u- · ~ --'--'-'"'--,-F--1----

D

:: :L :i:: :L:L:L.t:LI:LJ::t::(~i::::i::::f:::Cf :::L: L :i:: .i:l::=:::i :::LI : : , : : : : f : : : I : :_ .. t · -- ; : : : : : : : : : : : : .. _ L .. L.J ___ f . .t. .. .l. : .. : ... ~; ___ ./.. __ ; ... L..t ... .!.. _; ____ t ___ _;__ .L .i ____ l __ . L _; ___ .i ... L __ i ... .i ___ _; ___ . : : : :, :@c-: : : : :~-: : : : : : .; ; : : ; @: : : : : 1 I I I 1.)1 I I I I w I O I I , 1 I I I I O • 0 •

••••••••.,'-••••:..,...,..,..I ............. I••-••••-'--•••••••'•• ••- ,.,.\. .. ..,,,.,.,. .. ,..J,,..,,. •• ..,.,.,.1,.,.,.,.,.,.,. ... .,I,, ....... -••••-'••,.:,•••• • rt •••!••••""•••-"••••

___ J_ ... ! .... L .. J ... L.--! ___ ! ... ·! . .-.. L.) ... J..) ... L .. ! .... L.) ... L .. ! ... L .. ! .... l·----: --- ; ____ :----.L .. } ... 0 o o I I I I I O o I I o I I O o -r-· -+; · -1- -- -i · · ~-j- ---+ ---t---+-- · ·1----1-- --~ ---+---~~---·I· -- ~- ---t -- --~ ---1---- i----i·--·+---

:::;: ::::::: :: ::::: ..; ... L:~: ; ; 1:. . ..;._ .( _ i--~,:;. ; . --1-.: .: ... r.1 .... 1 . .) ... !~- .. J .... l.

2) ••. 1 .... L .. 1 .. :.

I I ""' I I I I I \A! o I I r I I r 1.c.; I • o I 1 ----:---·:····;-··-·:- ~---~----: -- .. ---+---~---+----:- -:-----~---+·-·r··+-~:t1~~.: : : ; : ·~---;---.-~---. • ;:,;1: • ' . • • • • •. j;,v. ";If. • • • • • l~ ·---·----:----~--- :- 1~<o·-·: ···:···· :··· ·:··-·:····:·--·: ···:···· :·--·:·--·: ···:· 1; ·w, :-··-~--'i~ --~-··:··--___ .:. ___ ... _ -~- ··-. .. : .... ~--. ~- ... ~- ... ~- .. -~- _. : ... c: .. . L.-~--- .;. ----~ ---~-. · · 1 .:. -~-.: ... ~- ---: : : : : : : : : : : . : : tY:i : f.m : t.r· ' ' . -- ~ ----~-- -_: __ -. ~- ---~--. -~- .. .: f--- -~-- .... : ..... -~-- --~ ----~---i·-·· · ... · .. -~- -~ --~ ~ -- ... : . : ~ : : (f;']_): : : : ~ : : : . : r::';\D . : : : : -- • ~- - - ... .; --- ....... --:- -- ... -- -~---~----• -- .. -~---"'-· ~ ---~--·- • ...... :-~................. . .- ----!- ... - .... ---- ~ --- .., ___ -.... :----:----: ... :- .. L . .) .... L .. ) .. ..!. .. ..!. ... L.--~---L-.J .... L ... @ .. 1i1~ . ... ) .... 1..) .. .1.... +-·-:----: : : ' : : . : . : : : ·(IjL. :.@) :riii\l\l:: i\{{: : ·--~---- .----~---- ·1!f.;-·f·--r··r·-r-·T··r··1···r-·r·T···r-·t@· @@··;~---- ,·,·1 -~1·;;·· --~- t. -~---.: .... ; .... ~ .... ; .... ! .... ~ ... .: .... ~ .... : .... ;. ... ; .. tfdi'r_._ ---~--- .. : . . :.. :-1(,,~·-: : : : : : : : : : : : . \!.:J>' : : : : . I G ilUI. • --- :----:----: -·--:- -·f···f·@·--·~----/··--(@··--j-···/···)·-··l···@y- ····j---~i~i·t~---- . -. ·- ~- ... : ... -~ .. -~- -+---~ -·- ~-. ·· i .. --~- .. -~ ---! ··- -~ ... +- --~---+---~--- i --·;·;.~-. ~~ .. t:. ">l~f

• f I t • I I • • I O I I ~ ~ I O --- ,'"·--:·--<----!.- -:----:----~---~---·:----~---:·-··:----~--~~----:·---~---~·---: - -··-:-·· . ---:---~---- ---------~--·

-::: r:::r:: T:+ ·;~:t:~:J :::r:: J::~~::::j::::t ::::[~:;· ;~ :::r:::cf T:: : : ::;:::r:: ····(·t·tt -: ·r·-, ·· r-·r-~---1-- ·;·· t""·t·(t···( :4:!·~·l··t···'.;···· -~-~t·· ... -:·. --~ .. -. ~. -- ·,·. ·: .. --~ ... ·:· -.. :··. -~ ... ·:· --- ~- ·-- :· -··: ·· -·:·· ·-: ... -~- ---:-· -. : -~ -.. ·:· ~ .. :· -··@·:·qi IO;'QY·:··· ---+---~----~---~- +--ii--,-;~i-1----r---+---~-1----!---+---1----f--1·4~ ; .). :~ .. ) ' ; ·

I I I "J ~ I I_. ~ .~. I r I f • --..... ---1-- -..... ·--

. . ----:----; ........ : --- .

--:-;, 1 I I I I I I I I I I I I I I • - .. --..:-- -- ; .. -- -:.- ---:- -· .. ; .... --r- ... ~-- ..... ; .... -.. ~. -- -:- .... ~--- -~ ----!---. ; ......... ; .. -- -r ··- ~-- ... ~ -- --~ ...... ~-.. 0 f

I I I I I I I

' Swipe

I I I I • I I I I ---·:··--~----: --- .-·--:----~----: ---~----:---·:----· :--·-!·---: --- ......... ;----:--- :----~- : - : D . . Air Sample I I I • I I o I I I I - -"' .. ·- -- -........... ________ ................ ---- ..... _____ .... ---- --- ................ ,- ................... ·--- --- ................... -- --- .. I • I I I I I I I I I I O • 1 I ' . -- .. ..;_ "' -- ~- ... -- ~ ----:----~----~··--:..--- .; ...... ; .. -- -~ ..... .: .. -- . ; ........ ~ -- .. .: ........ ~ .. ---~- ... .:. --- ~ ---·~----:- .. I I I f I I I I I 1

' '

Meter Reading = Rad . Survey- iil µrem/h f I I I I I I o I I I O I f I - .... :--·-t-·--: --- :----:----~----:--- .. ~----: ----:----: t : : -:--- .: --- : ·! :. :

/ ,:3lo£.Jt. '='- I Pr

Job Location: Achillion Pharmaceuticals, Inc. New Haven, CT Page:~1~of~6~ s p urvey urpose: D VV t St ecomm1ss1on1nq as e oraqe an d BL2 D t 10/14/19 a e: Performed By: David Durkee 3:\- ~---Inst. No. 1 (Model/SN) Inst. No. 2 (Model/SN) Inst. No. 3 (Model/SN)

PE Microbeta 2450 #04130262 Ludlum 2241-2 #137751 Bicron uRem LE B466Y Detector (Model/SN) Detector (Model/SN) Detector (Model/SN) Internal Ludlum 43-68 #140899/ Ludlum Internal

43-37 #143616

Efficiency::::: 40% 3H / 75% 14C Efficiency: 8.6%/8.69% C-14 Efficiency: 100% Type Rad.: 13 Type Rad: 13 Type Rad.: v Bkgd.: See #1 Below Bkgd.: 256 cpm / 864 cpm Bkgd.: 4 - 8 uRem/hour Cal. Due: 04/01/20 Cal. Due: 01/07/20 Cal. Due: 01 /15/20


1 10:45 Background 1 11 cpm 26cpm 2 Upper wall 1 -5.0 -2.7 3 1 Lower \/Vall 1 7.5 4.0 4 Electrical Outlet 1 5.0 5.3 5 Upper \/Vall 1 5.0 0.0 6 Lower \/Vall 1 5.0 -4.0 7 Outlet 1 0.0 -1.3 8 Upper \/Vall 1 12.5 -4.0 9 Lower \/Vall 1 5.0 -8.0 10 ~ Yellow Crate 1 1 -7.5 1.3 11 Yellow Crate 2 1 2.5 -8.0 12 Floor Around Crates 1 -5.0 -6.7 13 Uooer \/Vall 1 15.0 17.3 14 Lower \/Vall 1 10.0 4.0 15 Uooer \/Vall 1 22.5 6.7 16 Lower \/Vall 1 5.0 -2.7 17 Uooer \/Vall 1 -2.5 1.3 18 Lower \/Vall 1 0.0 -6.7 19 l Electrical Outlets 1 12.5 10.7 20 Uooer \/Vall 1 22.5 16.0 21 Lower \/Vall 1 2.5 4.0 22 \/Vall 1 0.0 -6.7 23 Counter 1 7.5 6.7 24 \/Vall 1 0.0 9.3 25 Sink 1 12.5 6.7 26 \/Vall 1 10.0 0.0 27 Floor 1 2.5 0.0 28 Floor 1 -5.0 -6.7 29 Floor 1 7.5 13.3 30 • ? Floor 1 -2.5 -6.7


Number Time

31 32 33 34 35 36 37 38 39 40 41 42 43 44 45 46 47 48 49 50 51 52 53 54 55 56 57 58 59 60 61 62 63 64 65 66 67 68 1 •

Achillion Pharmaceuticals, Inc. New Haven, CT Page: 2 of 6 10/14/19 _Decommissioning Waste Storage and BL2 Date: -----


Floor 1 12.5 9.3 Floor under crate 1 0.0 -1.3 Floor under crate 1 -7.5 -1.3 Uooer Door 1 2.5 -2.7 Lower Door 1 7.5 -5.3 UooerWall 1 7.5 13.3 Lower Wall 1 2.5 8.0 UooerWall 1 22.5 16.0 Lower Wall 1 -7.5 10.7 Outlet 1 27.5 32.0 Glass window left 1 -2.5 -2.7 Glass window riqht 1 -22.5 -18.7 UooerWall 1 2.5 0.0 Lower Wall 1 2.5 0.0 Floor under hood 1 22.5 5.3 Floor qlass windows 1 7.5 10.7 Floor 1 -2.5 -13.3 Floor 1 2.5 2.7 Floor 1 7.5 -5.3 Floor 1 7.5 13.3 Floor 1 2.5 2.7 Floor 1 -2.5 -8.0 Floor in front of hood 1 7.5 -8.0 Floor under hood 1 12.5 13.3 Floor (front of cab) 1 -12.5 -8.0 Floor under sink 1 12.5 2.7 Floor (front of cab) 1 7.5 8.0 Floor 1 32.5 8.0 Floor 1 7.5 0.0 Floor 1 12.5 16.0 Floor 1 17.5 8.0 Floor 1 7.5 0.0 Floor 1 2.5 2.7 Floor 1 7.5 13.3 Floor 1 7.5 -5.3 Floor 1 -2.5 2.7 Floor 1 -2.5 -10.7 Floor 1 2.5 -5.3

Job Location: Achillion Pharmaceuticals, Inc. New Haven, CT Page: _3_of_6_ Survey Purpose: Decommissioning Waste Storage and BL2 Date: 10/14/19


69 Upper Wall 1 7.5 2.7 70 Lower Wall 1 17.5 10.7 71 Uooer Wall 1 -2.5 -13.3 72 Lower Wall 1 -7.5 0.0 73 UooerWall 1 17.5 13.3 74 Lower Wall 1 2.5 0.0 75 Outlet 1 -7.5 · -18.7 76 Upper Wall 1 42.5 34.7 77 Lower Wall 1 -2.5 -2.7 78 i

~ Upper Wall 1 17.5 2.7 79 " Lower Wall 1 7.5 16.0 80 Door 1 7.5 2.7 81 Upper Wall 1 -17.5 -13.3 82 Lower Wall 1 37.5 16.0 83 Upoer Wall 1 27.5 13.3 84 Lower Wall 1 17.5 5.3 85

j

Upper Wall 1 7.5 10.7 86 Countertop 1 -2.5 5.3 87 Outlets 1 37.5 26.7 88 Shelves 1 42.5 18.7 89 Outside Drawers 1 -2.5 -8.0 90 0 uts ide Cab Doors 1 17.5 18.7 91 I Inside Drawers 1 7.5 8.0 92 Shelves Inside Cabinets 1 -12.5 -10.7 93 Inside Cabinet Doors 1 17.5 10.7 94 Front of Sink 1 12.5 21.3 95 Sink 1 12.5 16.0 96 Sink Drain 1 2.5 5.3 97 t Sink Faucets 1 -2.5 0.0 98 ~ ;, Wall 1 2.5 -5.3 99 Wall 1 17.5 2.7 100 Wall 1 12.5 8.0 101 Wall 1 -7.5 -5.3 102 Wall 1 2.5 -8.0 103 Shelves too/bottom 1 2.5 2.7 104 Shelves top/bottom 1 12.5 0.0 105 Outlet 1 -2.5 10.7 106 Side Cabinet 1 -7.5 -5.3 107 Countertoo 1 17.5 8.0 108 'f Countertop 1 2.5 8.0


Number Time

109 110 111 112 113 114 115 116 117 118 119 120 121 122 123 124 125 126 127 128 129 130 131 132 133 134 135 136 137 138 139 140 141 142 143 144 145 ' .

Achillion Pharmaceuticals, Inc. New Haven, CT Decommissioning Waste Storage and BL2

Location Inst. H-3 Activity

Page: Date:

4 of 6 10/14/19 -----

14C Activity Used (dpm/100 cm2) (dpm/100 cm2)

Wall 1 -12.5 -8.0 Wall 1 7.5 2.7 Wall 1 -12.5 -2.7 Wall 1 -7.5 -10.7 Countertoo 1 17.5 21.3 Countertop 1 22.5 16.0 Outside Drawers 1 22.5 5.3 Inside Drawers 1 12.5 -2.7 Outside Drawers 1 -2.5 8.0 Inside Drawers 1 7.5 2.7 Outside Drawers 1 17.5 8.0 Inside Drawers 1 7.5 0.0 Outside Drawers 1 7.5 -8.0 Inside Drawers 1 -2.5 -2.7 Side Cabinet 1 32.5 42.7 Countertop 1 22.5 13.3 Countertoo 1 7.5 10.7 Shelves 1 -2.5 -2.7 Outlets 1 2.5 -10.7 Side Cabinet 1 -7.5 5.3 Outside Drawers 1 2.5 -8.0 Inside Drawers 1 22.5 10.7 Outside Drawers 1 57.5 24.0 Inside Drawers 1 -2.5 -5.3 Outside Drawaers 1 2.5 0.0 Inside Drawers 1 -2.5 10.7 Outside Drawaers 1 -17.5 -5.3 Inside Drawers 1 27.5 18.7 Outside Drawaers 1 -17.5 -5.3 Inside Drawers 1 2.5 -5.3 Outside Drawaers 1 17.5 8.0 Inside Drawers 1 42.5 16.0 Outside Drawaers 1 7.5 0.0 Inside Drawers 1 7.5 2.7 Outside Drawaers 1 17.5 21.3 Inside Drawers 1 7.5 2.7 Poles and Hoses 1 -2.5 10.7

·, \

..

I o I • ---~,----~---,·--------~--·--·---. - .. ~ -. -. : ... -· .. -... : - ... -: -- ._.;.. -..

I I I O e ----·----:--- .. -- ... • ............. · ..... .. ' I ' ' o ------·--. ---~----~----·--------I I O I O I

• i - .. - - ~ .. - - •, • - .. - : - - .... - • - ...... - • -

0 0 I 0

- ... - - "' -- .... .;. --- ........ ·'I- - -·. -· .... ;.. ---

' . . . --·:- .. --: ·-- :- ·--!----: ----.----0 I I I ----~----·---~---------:--------. . . . ... . . .. - .. -......... .

-- .. ; -- .. -: ----:- ..... :- .. - .. : ...... -: -.. . .

- - .. ! - - - - :'" ...... -:- - .... - ~ - .. - - ~ - - - -;- - - ..

. . . ____ :· .... :.~,.,. .. a: .... I I I I o o f I I I • ?)1 I -··-:---·~--- :·---~----: ..... · ......... ~----~·---:----~-·--~-·--:·-·: ' . ' I I I o I I o I - --- ...... -........ -- - .. - .. ---- : : ®' : . -····-···--·· ~ ·-······· I I ,:,- o I

I I I I

• I I I - .. -.. -------.. - --...... --.. - .. --- .. -..

Q Swipe I o I I o I o I o I I ---·t· --1- ---r----r-·-1--- · f-· --r-- -~-- --r --- -~----~.: ··--.. t··--i-----_(---f ·---.1--·-r· --f""· -.r-1 I I I • I o I , f I I I

0 AfrSample

Meter Reading = Rad

----~----·----~---~----·--------~---------~--------~---------~--------·--------~----·----~------' I I I I I I I I I I I I : 1 • : I

1 I I I I I I I I I I O I o O I I I I I

Survey in µ.rem/h ---:· ··- :· -· ·; -·--: ~--:··--:----:?Jr~ 1 ··-;: ~~ :· ·- ·: · ·- ·: ·· · :· --·:· -- ·=- ·-:· ···: · · --:-· · ·:· ·

-----:- ---~ ----~ ----:-. --i. -- .; .. .. ;.la!=-"-i-. ~~~--. -~ ----:- ---~- ---i--- ~:--- -~- -- -!- -.. :. -- --:- - l&cx.k- "' , ,c.,-

·, l

I O I I > 0 • o I ' I o I I -- --:- -- -~-- -_ ... -- -:-- --~ - . --:----.,~--- .; ..... -~ ----:- ... -~- ---:-- ·--:----';- ---~ --- -:----: ·~\--~-·--:··. - -:-- - .. ~----;- ... ~. -·-,--·-:"'··· -:- ---' . , ©© t!): , ' ·---~---;-···.:·-·-t<----: @--I-: -®-.,.,-.. -.~o4----~····:··-·~---~·--·:-···~·-··:···· .... , .... -···:····-:··--~--:f···t··:····:··--:·-·rf ·:··--:··-·f· r···-· ;.... ---~----;·-··:··-;···-~----:----~---· '.3: ... : . : . : ' ... ' . . .. -.. ~-. -- -. ~-f. -- ·:-g ·@r. -c~t ·· -; ·-- ·:. ··; ·. ·-: ···r ·:····t "":·· ~@ . -. -:--. -~ ... ·r .. -~- -.. ; . ·-·~ .... ; ....

· .. · j· -... · ···t ··- ·j· · -·t · .. t ··· 1- .. a/· ···t · · ··j· · · · t· · · ·r~t .. ·i·· · · t · -· ·/··· · i--~- · · -~- · -'; · · --~ · · · :· -· -~ · ·--~ · · ·-:- · · · .. --~---- ·©-~- .. .:. ...... ; ....... ~--- .. : ...... -~- -- .. ~ ·- ... :. ..... ; ....... : .... -::- ..... ..: ....... ~ -..... : ..... .,: ..... " . . . . . ' '3· . . . . . . ' . zj . . .. .. .. -:· • .... , ........ : ............ : - .... r ..... ·- .... ..

. . . --------- : t:_~t:rt--~J::J::i::t:LL:i:J:::i:::li _ . _ , _ . _ . ~) . _ . J. .® _ L. _ J .... l. __ . t . __ -~ .. _ i. _ . _ t ... J. ... 1. _ ~ . f .... ~ ... t. _ .. ~ _ . _ .

--~----~----~---~-----:----~---~-----.. -:- .. -. :- ...... ~---~·---;-- --~----:-- ...

I • I I : : . : __ .) ____ ~---L--L~i.. .. 1..02 . .L .. L .. @. ---~---~,----~---~---·:·---~--------

. . - .. --:- - - .. -- - ..:- --. ~ ----~ . -. -· -.. -: ---. ; ---...... --0 0 I I 0

: : : .: : : : : (!!) : : : : : : ---------: : ; ft)::: :~r: !: _"j: ;r::: L -CL I::/::::[;:!::.:/~ ...... :----~----:---~----:----..... :----I O I I 0 . .. ~ .. ~ .... ---......

········· ~ .... J.3.; .... ~----!-·· ~ ... '· I O O f O o I I I I t o I : ' : ' : ' : .. -~: . : ' : ' : ~-··· : : : : : : : : . : : ; : : : : :· : : - - --~ "@" - -~ -- - ~ .. - . :·· --~ ---~: · -~-~---~- ---~ 1i . --- ~- -.. ~ ····: ··· ~-- --~-- .. ~ ----~ ... Io o I o.~I t I I' I' I' Io o

I O I I ----·----~---~----~-·-~----. . I I f I O • I O o I I I I t • 0 0 o ----: ----:----:----: --- :---- -----:----.----:----: ........ :---- ;-----: ··--: ---:----~-- .. -: ·--·:----:----: --- :- ·--f----: --- ,----,, 2..tt: , ;uJ . . . . -. ~-- -. ~-!---~,.,... ... -.__~-~---+-----!-o--"lai,j,"'-~~-~-!' ' ~ ' . ~ ·- ....... --~ .. . : : : : ~-,,.c:~ .: --"' n,,..: : . : : : : : : : I I I I ~·,f'T~ ~ ,.~ 1 I I ' O I o ' • '"""'" • .. • • • ....... f'" ...... -· • .. • '9 .. • • .... • • • •,• .. •"' • • • • .. r '" • • .... • "' .. • • .. • • • • • • .. ,.. .......... - .. • 'P .... • .. ,.. .. • .. -. • • .. • •

' . I I I I I I I I I I I I o O I o · - - -: - - - • i • - • - :- - - - -:- - - -1- - - • ;- • - - -:- • • - -! • - - • - - • -: • - - : - - - - ; - • • .. : - - - :- - - - T • • - - ~ - - - :- • - - : • - .. ·: • - • -: .. • - • : - - - - : - - - -:- - - • :- • • ·: • - • -: - • • I o I I I I I o I , I I I I • O ,

- - :. - ~ - .... - : - - - ·:- - .... --:- - - .. ! - - - --:- - - .. -:- . - - : - - .. - ~ - - ........ - - ~ - .. - - ; - - - ":· ..... - ~ - .. - - ~ - - ... -:- - - - ~ - - - - : - - .. -:- - - - -. ~ .. - .. ! - - - .. :- .... - ~ .. - - - : - - - -~ .. - - -:- - .... o I o I o I , I o O I t t

I .. - - -· - - •9 --- -- - .......... --- - ................. _ --- .... - - ..... -- -- - - • --·-· ........... -- ·--·-- -- - - ...................... ------ ---- -- - • - - -- ... - - -· ... --- - ................ ..

• O I I O t I t I o I • • ' • . I I I a t • o o I I 4 •t t I I I o ----~----: ........ : ..... :----;--- ... : -- ·~----.:----~----:- ... --~---·: ·---:----:----~---·: ---~-·--=---·: --- :---... ; ....... ; ---·:----:----~ ... -- :---· • I I I

a ' o t I • I I o I t • I • I f t I , • I - -- -:- .. ':" --~ -- - .. ~ -- --:--- -~----~---- -:· ·---:- -..... ~.-- -:- ..... ~- ...... ~- ---:---·-:---· :--- ~~ .. -- -:----~- ---~-- .. -;-, --- ~ --- - ~ --- -:- -- -~- .. -- ~ -·--; .. ·-I • I I t I O I , I I I I I f I

--......... -... ·- .. -- -- ----· ............. ··---- ................ --- - ............ ··---- .. ·--------- ................ __ ......................... --- . ----- ----· -- .. - ---- --- -.... . 1 I I I t I I • o I I t • • o I 1 I • I I I I O O a O a t f • -.. .. ..:. -.... ; . --.. ~ --- .. · .. ---~ ·---r--- -:- .. ---·--- -~ ........ · .. --- ..; ........ ! ....... ~ -- --·---- ~- - ... ;. ....... ~-- --~ - ·--~ - -·-:- - -- ~ .. - -- :. --- -:- - .... .! .. -- -~ ---·'----

I I I I O I I o O o I I t I I o .... ---:-· - -~ - ---:- -----;---·-~ ...... -~----:-. -.. ~ ----; ...... -:· ---~ --- -~-- .. -:- --- ~-- -- ;-- --:- --· -:·- --~ .. -·-:- ---~- .. --~ .. ---~ .. ---:-- .. -~ .. ·--~ ----:· .... '

I I I I I 9 f I I 0

-- ................. -..... --- ------ --· .. --- ----· .. -- . -- .. -- ------- - -- ........ -----· -- ---- ............. ---· .......... ----- --- .. _ .. __ -- -- - ......... -- .. ----- ·--• I I I f t I ' O f I

'o If o I I I I If I IO Io O I' I 0 -- --~-- .... ~----~ ........ , ........ .,. .... ··r---~- ...... " ........ ,. ...... , ....... ~ ........ r·---:····,-·-·: ··- ·; ··- ~-- --~ -- --~ ....... ~-- Swipe I I f o I I f I I : ~ : : : : : ~ : :- : : ; : : : : : : : 0 Air Sample

o t • I I f , I o I I - - ....... -- ....... __ ,., - ----- --· .................... --- --- ..... ·---- .. -- • - .......... ·-~ ·----·- -· - ------- 4• --- • -- ..... -- - -- • • I I

t o I • • t I

I I I t I I I I I I • I I o O o I O O I ·--~···-,····•--·•r···~--··r··--~---~---•-r····r··-~--··T···•P•·•~·-·-~----r---~----,··••,r••••,•• I I I I I o t I I I I I I I I 1 0

I I I o I I t I : ~ : : : ~ : ~ : : : ; : ; : .: : ; : ;

Meter Reading = Rad Survey' iil µrem/h

I tJld:sc. = I ,c,

Job Location: Achillion Pharmaceuticals, Inc. New Haven, CT s p urvey urpose: ecomm1ss1onina 10c em1s rv a D B" h ·t Lb Performed By: David Durkee - - ___,,

~ r--..... -,1

Inst. No. 1 (Model/SN) Inst. No. 2 (Model/S "') PE Microbeta 2450 #04130262 Ludlum 2241-2 #137751 Detector (Model/SN) Detector (Model/SN)

Page: D t a e:

1 of 12 10/14/19

Inst. No. 3 (Model/SN)

Bicron uRem LE B466Y Detector (Model/SN)

Internal Ludlum 43-68 #140899/ Ludlum Internal

43-37 #143616

Efficiency:~ 40% 3H / 75% 14C Efficiency: 8.6%/8.69% C-14 Efficiency: 100% Type Rad.: S Type Rad: S Type Rad.: V Bkgd.: See #1 Below Bkgd.: 256 cpm / 864 cpm Bkad.: 4 - 8 uRem/hour Cal. Due: 04/01/20 Cal. Due: 01/07/20 Cal. Due: 01/15/20

Number Time · Location Inst. 3H Activity 14C Activity Used (dpm/100 cm2) (dpm/100 cm2)

1 1530 Background 1 10 cpm 29cpm 2 Uooer Wall 1 10.0 4.0 3 Lower Wall 1 22.5 -1.3 4 Uooer Wall 1 15.0 2.7 5 Left Sink 1 10.0 9.3 6 Left Sink Drain 1 27.5 5.3 7 Riaht Sink 1 40.0 13.3 8 RiQht Sink Drain 1 10.0 5.3 9 Counter 1 22.5 4.0 10 Upper Wall 1 25.0 2.7 11 Lower Wall 1 0.0 -14.7 12 Uooer Wall 1 5.0 -2.7 13 Lower Wall 1 2.5 -9.3 14 Uooer Wall 1 22.5 13.3 15 Counter 1 12.5 -5.3 16 Top Shelf 1 7.5 -4.0 17 Shelf 1 12.5 -4.0 18 Front of Drawers 1 -2.5 -2.7 19 Front of Drawers 1 -5.0 -38.7 20 Top Drawer 1 27.5 9.3 21 Second Drawer 1 0.0 -14.7 22 Third Drawer 1 15.0 8.0 23 Fourth Drawer 1 22.5 20.0 24 Top Drawer 1 20.0 6.7 25 Second Drawer 1 -2.5 -4.0 26 Third Drawer 1 20.0 4.0 27 Fourth Drawer 1 15.0 -2.7 28 Side of Drawers 1 12.5 9.3 29 Uooer Wall 1 15.0 -1.3 30 '? Lower Wall 1 7.5 -5.3


Number Time

31 ij 32 • I 33 34 35 36 37 38 39 40 41 I 42 • 43 44 ' 45 I ,;

46 47 48 49 50 51 52 53

' 54 f

55 56 57 " 58 59 60 j

61 62 63 64 65 66 67 68 1;'

Achillion Pharmaceuticals, Inc. New Haven, CT Page: 2 of 12 10/14/19 Decommissioning Biochemistry Lab Date: -----


Upper Wall 1 22.5 14.7 Lower Wall 1 20.0 -4.0 Uooer Wall 1 15.0 -4.0 Lower Wall 1 2.5 8.0 Upper Wall 1 10.0 9.3 Lower Wall 1 12.5 -2.7 Shelf 1 17.5 12.0 Counter 1 -10.0 -14.7 Shelf 1 0.0 -1.3 Shelf 1 -2.5 -2.7 Counter 1 30.0 5.3 Front of Drawers 1 -2.5 -2.7 Top Drawer 1 32.5 22.7 Second Drawer 1 7.5 9.3 Third Drawer 1 -5.0 -4.0 Fourth Drawer 1 2.5 5.3 Front of Drawers 1 -5.0 -17.3 Top Drawer 1 7.5 -1.3 Second Drawer 1 5.0 -5.3 Third Drawer 1 10.0 10.7 Fourth Drawer 1 7.5 2.7 Front of Drawers 1 5.0 -12.0 Top Drawer 1 7.5 1.3 Second Drawer 1 10.0 4.0 Third Drawer 1 20.0 5.3 Fourth Drawer 1 -12.5 -16.0 Cubbv 1 15.0 4.0 Front of Drawers 1 12.5 6.7 Left Drawer 1 10.0 17.3 Riaht Drawer 1 10.0 0.0 Top Drawer 1 10.0 0.0 Second Drawer 1 15.0 -2.7 Third Drawer 1 5.0 1.3 Side of Cabinet 1 7.5 0.0 Side of Cabinet 1 15.0 4.0 Counter 1 -2.5 -4.0 Counter 1 10.0 5.3 Front of Drawers 1 7.5 6.7

Job Location: Achillion Pharmaceuticals, Inc. New Haven, CT Page:~3~of___.1l_ Survey Purpose: Decommissioning Biochemistry Lab Date: 10/14/19


69 Top Drawer 1 20.0 4.0 70 Second Drawer 1 2.5 -4.0 71 Third Drawer 1 17.5 -4.0 72 Fourth Drawer 1 2.5 -1.3 73 Front of Drawers 1 10.0 -2.7 74 Too Drawer 1 27.5 21.3 75 Second Drawer 1 22.5 9.3 76 Third Drawer 1 30.0 12.0 77 Fourth Drawer 1 7.5 -2.7 78 Cubbv· 1 10.0 -6.7 79 Front of Drawers 1 35.0 12.0 80 Too Drawer 1 20.0 13.3 81 Second Drawer 1 17.5 0.0 82 Third Drawer 1 12.5 6.7 83 Fourth Drawer 1 -2.5 -4.0 84 Front of Drawers 1 10.0 21.3 85 Too Drawer 1 5.0 -4.0 86 Second Drawer 1 20.0 12.0 87 Third Drawer 1 7.5 9.3 88 Fourth Drawer 1 0.0 -9.3 89 Front of Drawers 1 5.0 -6.7 90 Too Drawer 1 10.0 -9.3 91 Second Drawer 1 -5.0 -1.3 92 Third Drawer 1 -5.0 -10.7 93 Fourth Drawer 1 5.0 10.7 94 Side of Drawers 1 2.5 -4.0 95 Uooer Wall 1 15.0 5.3 96 Lower Wall 1 15.0 10.7 97 Uooer Wall 1 2.5 -4.0 98 Lower Wall 1 20.0 8.0 99 Upper Wall 1 15.0 10.7 100 Lower Wall 1 7.5 -6.7 101 Upper Wall 1 25.0 6.7 102 Lower Wall 1 12.5 -2.7 103 Uooer Wall 1 10.0 -5.3 104 Lower Wall 1 25.0 12.0 105 Uooer Wall 1 22.5 1.3 106 Lower Wall 1 7.5 -1.3 107 Uooer Wall 1 7.5 0.0 108 , . Lower Wall 1 20.0 12.0

Job Location: Achillion Pharmaceuticals, Inc .. New Haven, CT Page: 4 of 12 - -Survey Purpose: Decommissioning Biochemistry Lab 10/14/19 Date: _-=...::;~;_;__-


109 Floor 1 2.5 8.0 110 Floor 1 12.5 4.0 111 Floor 1 2.5 0.0 112 Floor 1 10.0 1.3 113 Floor 1 0.0 -5.3 114 Floor 1 0.0 -2.7 115 Floor 1 12.5 1.3 116 Floor 1 -2.5 -2.7 117 Floor 1 7.5 -21.3 118 Floor 1 10.0 5.3 119 Floor 1 30.0 12.0 120 Floor 1 12.5 2.7 121 Floor 1 10.0 5.3 122 Floor 1 22.5 10.7 123 Floor 1 -5.0 -14.7 124 Floor 1 15.0 2.7 125 Floor 1 27.5 2.7 126 Floor 1 15.0 0.0 127 Floor 1 10.0 1.3 128 Floor 1 -5.0 -16.0 129 ii Floor 1 5.0 5.3 130 Floor 1 -5.0 -5.3 131 Floor 1 5.0 -5.3 132 Floor 1 5.0 1.3 133 Floor 1 35.0 6.7 134 Floor 1 2.5 -5.3 135 Shelf 1 15.0 8.0 136 Shelf 1 7.5 2.7 137 Shelf 1 32.5 18.7 138 Shelf 1 20.0 -2.7 139 Counter 1 15.0 8.0 140 Counter 1 15.0 12.0 141 Counter 1 2.5 -8.0 142 Counter 1 17.5 12.0 143 Wall 1 7.5 1.3 144 Wall 1 15.0 -2.7 145 Wall 1 35.0 9.3 146 Wall 1 17.5 8.0 147 Counter 1 20.0 0.0 148 ,, Counter 1 2.5 4.0

Job Location: Achillion Pharmaceuticals, Inc. New Haven, CT Page: _5_of ___:!L Survey Purpose: Decommissioning Biochemistry Lab Date: 10/14/19


149 Counter 1 2.5 0.0 150 Side of Cabinets 1 17.5 5.3 151 Front of Drawers 1 17.5 4.0 152 Top Drawer 1 2.5 0.0 153 Second Drawer 1 2.5 9.3 154 Third Drawer 1 12.5 2.7 155 Fourth Drawer 1 20.0 9.3 156 Front of Drawers 1 20.0 1.3 157 Too Drawer 1 27.5 12.0 158 Second Drawer 1 15.0 5.3 159 Third Drawer 1 20.0 9.3 160 Fourth Drawer 1 2.5 -6.7 161 Front of Drawers 1 5.0 -5.3 162 Top Drawer 1 17.5 8.0 163 Second Drawer 1 5.0 2.7 164 Third Drawer 1 -5.0 -2.7 165 Fourth Drawer 1 17.5 13.3 166 Front of Drawers 1 5.0 -2.7 167 Top Drawer 1 -2.5 -6.7 168 Second Drawer 1 7.5 -12.0 169 Third Drawer 1 22.5 2.7 170 Fourth Drawer 1 40.0 20.0 171 Drawer 1 -12.5 -18.7 172 Cubbv 1 5.0 -10.7 173 Front of Drawers 1 15.0 0.0 174 Top Drawer 1 15.0 18.7 175 Second Drawer 1 7.5 -10.7 176 Third Drawer 1 12.5 -4.0 177 Fourth Drawer 1 7.5 -6.7 178 Front of Drawers 1 5.0 -6.7 179 Front of Drawers 1 5.0 -1.3 180 Too Drawer 1 5.0 -6.7 18·1 Second Drawer 1 10.0 -2.7 182 Third Drawer 1 7.5 -9.3 183 Fourth Drawer 1 10.0 1.3 184 Too Drawer 1 12.5 -4.0 185 Second Drawer 1 10.0 6.7 186 Third Drawer 1 15.0 -6.7 187 Fourth Drawer 1 0.0 2.7 188 '. Side of Cabinet 1 5.0 -5.3

Job ~ocation: Survey Purpose:

Number Time

189 190 191 192 193 194 195 196 197 198 199 200 201 202 203 204 205 206 207 208 209 210 211 212 213 214 215 216 217 218 219 220 221 222 223 224 225 226 227 'g

_Achillion Pharmaceuticals, Inc. New Haven, CT Page: 6 of 12 10/14/19 Decommissioning Biochemistry Lab Date: -----

Location Inst. H-3 Activity 14C Activity Used (dom/100 cm2) Cdom/100 cm2)

Front of Drawers 1 5.0 6.7 Front of Drawers 1 17.5 10.7 Drawer 1 -2.5 -2.7 Cubbv 1 15.0 8.0 Front of Drawers 1 7.5 -1.3 Front of Drawers 1 10.0 -2.7 Front of Drawers 1 27.5 17.3 Front of Drawers 1 42.5 12.0 Too Drawer 1 25.0 20.0 Second Drawer 1 12.5 -2.7 Third Drawer 1 15.0 6.7 Fourth Drawer 1 7.5 -5.3 Too Drawer 1 7.5 -5.3

' Second Drawer . 1 27.5 4.0 Third Drawer 1 7.5 5.3 Fourth Drawer 1 12.S -2.7 Left Drawer 1 25.0 14.7 Riqht Drawer 1 -5.0 -1.3 Top Drawer 1 7.5 0.0 Second Drawer 1 0.0 -5.3 Third Drawer 1 12.5 -10:7 Too Drawer 1 -7.5 -16.0 Second Drawer 1 10.0 8.0 Third Drawer 1 30.0 9.3 Fourth Drawer 1 5.0 -8.0 Top Drawer 1 7.5 4.0 Second Drawer 1 ' 5.0 -8.0 Third Drawer 1 0.0 -9.3 Third Drawer 1 15.0 2.7 Shelf 1 10.0 2.7 Shelf 1 -2.5 -8.0 Shelf 1 10.0 2.7 Side of Cabinet 1 7.5 -2.7 Counter 1 12.5 5.3 Counter 1 22.5 20.0 Counter 1 15.0 12.0 Side of Cabinet 1 0.0 -1.3 Counter 1 7.5 -2.7 Counter 1 -5.0 -14.7

Job Location: Achillion Pharmaceuticals, Inc. New Haven, CT Page: 7 of 12 Survey Purpose: Decommissioning Biochemistry Lab Date: 10/14/19 _ __;__;;...._,;__

Number Time Location Inst. H-3 Activity 14C Activity Used ldom/100 cm2\ ldom/100 cm2\

228 Counter 1 15.0 0.0 229 Front of Drawers 1 2.5 ' 0.0 230 Front of Drawers 1 22.5 1.3 231 Front of Drawers 1 7.5 9.3 232 Front of Drawers 1 10.0 6.7 233 Front of Drawers 1 2.5 -4.0 234 Front of Drawers 1 -2.5 -10.7 235 Cubby 1 15.0 5.3 236 Front of Drawers "1 12.5 6.7 237 Front of Drawers 1 7.5 4.0 238 Front of Drawers 1 17.5 6.7 239 Top Drawer 1 17.5 -5.3 240 Second Drawer 1 5.0 1.3 241 Third Drawer 1 15.0 1.3 242 Fourth Drawer 1 15.0 2.7 243 Top Drawer 1 12.5 -5.3 244 Second Drawer 1 22.5 9.3 245 Third Drawer 1 -5.0 -8.0 246 Fourth Drawer 1 7.5 2.7 247 Top Drawer 1 17.5 10.7 248 Second Drawer 1 35.0 4.0 249 Third Drawer 1 0.0 6.7 250 Fourth Drawer 1 2.5 5.3 251 Inside Cabinet 1 2.5 :..2.7 252 Top Drawer 1 7.5 5.3 253 Second Drawer 1 2.5 -16.0 254 Third Drawer 1 5.0 4.0 255 Fourth Drawer 1 30.0 6.7 256 Top Drawer 1 22.5 6.7 257 Second Drawer 1 7.5 -1.3 258 Third Drawer 1 -2.5 -6.7 259 Fourth Drawer 1 2.5 2.7 260 Top Drawer 1 12.5 -1.3 261 Second Drawer 1 22.5 16.0 262 Third Drawer 1 10.0 -16.0 263 Fourth Drawer 1 12.5 1.3 264 Top Drawer 1 2.5 8.0 265 Second Drawer 1 15.0 -6.7 266 1, Third Drawer 1 20.0 5.3

Job Location: Achillion Pharmaceuticals, Inc. New Haven, CT Page:~8~of____:!l_ Survey Purpose: Decommissioning Biochemistry Lab Date: 10/14/19

Number Time Location Inst. H-3 Activity 14C Activity Used (dom/100 cm2) (dom/100 cm2)

267 Fourth Drawer 1 10.0 8.0 268 Top Drawer 1 -5.0 -1.3 269 Second Drawer 1 7.5 -1.3 270 Third Drawer 1 -2.5 -13.3 271 Fourth Drawer 1 -2.5 -5.3 272 Front of Drawers 1 30.0 9.3 273 Front Cabinet 1 7.5 -8.0 274 Front Cabinet 1 25.0 6.7 275 Front of Drawers 1 2.5 -'1.3 276 Front of Drawers 1 17.5 -1.3 277 Front of Drawers 1 15.0 2.7 278 Front of Drawers 1 10.0 1.3 279 Left Drawer 1 10.0 -4.0 280 Riqht Drawer 1 10.0 2.7 281 Too Drawer 1 10.0 6.7 282 Second Drawer 1 15.0 4.0 283 Third Drawer 1 20.0 0.0 284 Inside Cabinet 1 17.5 4.0 285 Inside Cabinet 1 -5.0 -4.0 286 Top Drawer 1 2.5 -4.0 287 Second Drawer 1 12.5 -8.0 288 Third Drawer 1 35.0 18.7 289 Fourth Drawer 1 32.5 13.3 290 Top Drawer 1 12.5 -6.7 291 Second Drawer 1 17.5 2.7 292 Third Drawer 1 22.5 6.7 293 Fourth Drawer 1 2.5 -8.0 294 Too Drawer 1 17.5 1.3 295 Second Drawer 1 2.5 5.3 296 Third Drawer 1 17.5 6.7 297 Fourth Drawer 1 7.5 -4.0 298 Top Drawer 1 27.5 0.0 299 Second Drawer 1 7.5 0.0 300 Third Drawer 1 -7.5 -9.3 301 Fourth Drawer 1 20.0 9.3 302 Counter 1 -2.5 -10.7 303 Counter 1 0.0 -8.0 304 Front Cabinet 1 27.5 18.7 305 1 • Front Cabinet 1 15.0 -2.7

Job Location: Achillion Pharmaceuticals, Inc. New Haven, CT Page: _9_of __g_ Survey Purpose: Decommissioning Biochemistry Lab Date: 10/14/19

Number Time Location Inst. H-3 Activity 14C Activity Used ldom/100 cm2} (dom/100 cm2\

306 Front of Drawers 1 7.5 -12.0

307 Front of Drawers 1 -7.5 -6.7 308 Inside Cabinet 1 10.0 2.7 309 Left Drawer 1 -5.0 -12.0 310 Rioht Drawer 1 15.0 10.7 311 Top Drawer 1 20.0 4.0 312 Second Drawer 1 0.0 -2.7 313 Third Drawer 1 37.5 8.0 314 Fourth Drawer 1 12.5 10.7 315 Top Drawer 1 15.0 -6.7 316 Second Drawer 1 5.0 1.3 317 Third Drawer 1 15.0 -10.7 318 Fourth Drawer 1 15.0 1.3 319 Counter 1 30.0 16.0 320 Sink 1 22.5 0.0 321 Sink Drain 1 10.0 -1.3 322 Front of Drawers 1 10.0 -5.3

l

323 Front of Drawers 1 20.0 6.7 324 Front of Drawers 1 15.0 9.3 325 Cabinet 1 12.5 -12.0 326 Cabinet 1 10.0 -2.7 327 Cabinet 1 12.5 2.7 328 Side of Cabinet 1 15.0 1.3 329 Wall 1 20.0 5.3 330 Uooer Wall 1 10.0 2.7 331 Upper Wall 1 10.0 2.7 332 Lower Wall 1 20.0 2.7 333 Uooer Wall 1 -2.5 -4.0 334 Lower Wall 1 7.5 -1.3 335 Upper Wall 1 17.5 0.0 336 Lower Wall 1 2.5 1.3 337 Uooer Wall 1 12.5 -4.0 338 Lower Wall 1 2.5 -6.7 339 UooerWall 1 5.0 -5.3 340 Lower Wall 1 22.5 21.3 341 Upper Wall 1 7.5 1.3 342 Lower Wall 1 7.5 -5.3 343 Uooer Wall 1 27.5 4.0 344 < ~ Lower Wall 1 0.0 -9.3

Job Location: Achillion Pharmaceuticals, Inc. New Haven, CT Page:_J_Q_of~ Survey Purpose: Decommissioning Biochemistry Lab Date: 10/14/19

Number Time Location Inst. H-3 Activity 14C Activity Used· (dom/100 cm2) (dom/100 cm2)

345 Upper Wall 1 10.0 0.0 346 Lower Wall 1 12.5 1.3 347 Uooer Wall 1 0.0 -13.3 348 Lower Wall 1 5.0 -5.3 349 Uooer Wall 1 15.0 -5.3 350 Uooer Wall 1 20.0 8.0 351 Uooer Door 1 27.5 14.7 352 Lower Door 1 5.0 2.7 353 Uooer Wall 1 25.0 12.0 354 Lower Wall 1 12.5 -5.3 355 Uooer Wall 1 17.5 -1.3 356 Lower Wall 1 17.5 4.0 357 Uooer Wall 1 5.0 1.3 358 Lower Wall 1 12.5 5.3 359 Floor 1 22.5 14.7 360 Floor 1 0.0 -10.7 361 Floor 1 -10.0 -6.7 362 Floor 1 27.5 8.0 363 Floor 1 15.0 0.0 364 Floor 1 -10.0 -10.7 365 Floor 1 12.5 -12.0 366 Floor 1 5.0 -14.7 367 Floor 1 12.5 0.0 368 Floor 1 32.5 5.3 369 Floor 1 10.0 2.7 370 Floor 1 15.0 -2.7 371 Floor 1 12.5 -10.7 372 Floor 1 12.5 9.3 373 Floor 1 20.0 4.0 374 Floor 1 42.5 4.0 375 Floor 1 25.0 1.3 376 Floor 1 12.5 12.0 377 Floor 1 7.5 6.7 378 Floor 1 12.5 2.7 379 Floor 1 -2.5 -8.0 380 Floor 1 22.5 2.7 381 Floor 1 2.5 -4.0 382 I • Floor 1 17.5 0.0

·, " l

II cf, 12-

-:, of 85!! 10)¢2

' .

I I

• I

f I

I o

I I

I ~

... : .... ~----~-:.~ ... +---~---·1 ... ·-r ... r···: '

• •

• ,u

'-~:!:: :i::'t:~LJT::J l

. .

' '

. 8.

C/l·

..... ~ .... ; .. ) .. ··:":·;· .. j--···:····i ~

~ "'""''·'"'"'"

' !

• :. .... ~

----: ···:····:····:···

. IO

D

I I

I

f :

I f

.. , ........ ~---~-·-·: L...:==-~~~-:~~:-~--;-~--i '

I I

I o

••• ; •

•••

1. •••~

-•••I••• •

r

' :.

' ·,

, . ---', .. · --. : .. ---: .. · .

·t--···i·@·:_:;···t···:

. .l. ... ~:-··-:----~.-.-·-~---·:·--· I

I \,

j"' .,•

. \.

• •

• ·'•

•

'····'· !\-<: ••••

• '

• '

.®: ~ ·'J;

. ·---~

---,··--:····;--·~"··

1r, .: .. --, .... : -. -

-~ -

: :

. :

t I

I I

•:••••

.... -~ -... -:-.. -.. , . --.. ~ --.. .

. .

I :

I -

• ~ •

• •

.:~

• •"

-·!----~---.. :-

-:

: I

O

I 1

I I

I I

... --~. --.:. -.... -... ~ .. -. ·:· .... -I

I I

I I

I

I I

I I

.: •• ,.,.

... --~ ...... -:--... : ...... "[ .. --•

I

..... ; .. -~ .. ~ ... --:--... .. -.... ~ ..... ·:.·

' .

I :

: I

..... -~ .... .; .. -. : -.... -~ .... ~-..... '

. . -.. :, ..... -i ....... ~ ...... :.-....

. . ... -r I I

: :

I I

I I

"'"

""~

"""~

""""!"

'"'"

'"'~

""'"

I

' '

. I

o

-. -.. t .. -....... --~ -.. --~ ----:---.. I

I :

t

.. l .. --.1 .... ! · · --~ -·_ -·:· · · -I

I I

I

. . .. -~ ----~ .. ---:-....

•"• "·:

0

"

0

·:•

: I

I

! : _ .. -: -..... ~ -...... --..

-............ -~

I :

' •

,.__:~..,. .... i-_..,._ •. -~ ----:----~ -.. --~ --. -,----

.. ORIGIN ID:EFBA . . . (203) 624-7000 .SHIP DATE: 12NOV19. · . · STEVE PODOS . · : . . · . · · . ACTVVGT: 2.00 LB · . · · . ACHILLION PHARMACEUTICALS, INC. · . · CAD: 101020183/INET4160

. 300GEORGE ST .. ·· . . . . . . . .

NEW HAVEN, CT 06511 . . . · BILL SENDER·· · . UNITED STATES US·

·•· 10 LICENSING ASSISTANT SECTION • · i .· ·. · . US NRC· REGION I • • . • . • ·· · • ·

. . . . . . . .. ' . . . . . . . . . . .. ·. .

.• · NUCLEAR.SAFETY BRANCH . . . . . · 2100 RENAISSANCE BLVD., SUITE 100·

.. · ·· ·•·· .. · KING OF PRUSSIA PA 19406 · ... · · . ·· (610) 3J7s50QQ . . . . . ·· REF: . ·.· · · . · . ·.INV:.· .. · .. ·

:.~ b~t

. · · .. 111 IIIIUIIIIHIIII II ii 1111111111 IIIJ 11111 HIHI HI 111111111111111111 Ill 1111 ·· ··

.. g.··.· .·

.. ai .. . 15 · .. · .. . ~.

·. I .•. ... . . al . C) . . ~ · .. · ... ·

m ~. O.· ... :c. (/)

'(

. ·.~ LO . . . .

· ..•. ~ < . .. ·~· ..

. . . --:J .· . .r--- .

.. . ·~

.· .. ·. . .... · ··11:;..;.~

··• ~Im: :· .. · .• Express® .. : •.· .. ·· ..•.

···E····· iii········.·· ... ·. : . . .. ··· . 'jf :: : ........ : . . . . . :: .

. . N· . . . -~ .. . ~ .

.. ~ . .,..

• Jj . . _.;...;...---'-""""-'-----'-'----'------'----'------'----'-'------'-'------'----'-'------'-----'----'-'-----'------'---'-

· · ·~ · · · ·. •: ·.: · WED-13 NOV 10:30A ... · · .. .

. ···•·· T~K#. •···•.·••.····· .·.: :· .. ··• ···•· ·: • ·•·. ·· PRIORITYOVERNIGHT : •... ·.: ........ . . · .. · I 0201: I\ 776.9 6108 5878 .· · .. ·. : . . .. · ... : ..... >DSR ..

. . . . al . - . ...: " ::s

.. ·. .· ,'

... ·.·. > 19406. · ... i EE KPDA .. · ···•···.·•• pfus PHL

C) ...

. o·: N .· N ..

-~-- .. '

. ::· .· .... '.

. Ql·· ... C: . ·c. . . -~. '§; : .. · 8

' Qi' . : .·_ ·.g . ? . -l!,·

.. 5 .·. ~. . Q).'.:' ... ~ .·

. ·~ ... · .~ :S .... · . =o . · a.· . ·•iii·

>, . . .c:

: B-_·:- .··. ·.g-. ··.~.. .tf-

.!!! ... ·.· ~:

. l_f :·. t· ~ . §.

· .. 11· ~ ... ·.ff:·.~.·

. Cl.c: .· .. ·.: ~· . . m al . o.. ~-=. -~ .

. : . ;sc:- _·§ .. : · .. -a,_-. . . C:

.:...: a.Ill .•. [ .... ·.!c:~ . :E

. .!!! ,g ~ : "'. UI ::I .· . E. ·- .c 'O . 0 . ·= +Jc:" . .Pl .. . . ~

C: .. )( .

. giit '§;. . ·.· ~ .

. ,·.. .~ ... -~--!:' . ~. . Cl. ai ~ .. :_f

·· .. ~-~~-. ~.. i ...... ..-C',I.. '·:i::

:r:.

Achillion Pharmaceuticals, Inc., Termination Request Ltr ...copy of the sewer disposal records for the long-lived isotopes (H-3 an~f C-14) disposed are attached. Regarding records

Documents