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File No. 12015/02/2017-QA Food Safety and Standards Authority of India (A statutory Authority established under the Food Safety and Standards Act, 2006) (Quality Assurance Division) FDA Bhawan, Kotla Road, New Delhi – 110002 Dated, the 02 nd Jan, 2018 RFP No. 05/2017-18 FOR PROCUREMENT OF MINOR EQUIPMENTS: CORRIGENDUM Further to this office Tender Enquiry No. 05/2017-18 dated 07 th December 2017 and Pre-Bid conference held on 21 st Dec 2017. 2. The following amendment are made in the ibid tender: (a) Last Date and Time for Receipt of Tenders: 23 Jan 2018 at 1500hrs (b) Date and Time of Opening of Tenders: 23 Jan 2018 at 1530hrs (c) Part II- Essential Details of items/services required is revised as under: 1. Schedule of Requirements – List of items/services required is as follow :- Sl. No Items Qty (Nos) Purpose 1. Atomic Absorption Spectrophotometer [GTA /FLAME / VGA] 01 For trace metal analysis in food and water 2. Lovibond Tintometer 01 For sesame oil / Color in oil tests 3. Flame Photometer 01 For minerals viz. Na, K, Ca. 4. Muffle Furnace 02 For determination of Ash 5. Gas Chromatograph with FID and ECD Detectors 01 For analysis of Pesticides residues and other Food & Water related applications as per FSSAI requirements 6. Gas Chromatograph with NPD and Thermal Conductivity Detector(TCD ) Detectors 01 7. Microwave Digestion System 01 For sample preparation prior to metal analysis by AAS 8. Digital BUTRYO Refractometer 01 For BR, RI, Brix measurements in Oils and Fats 9. Flash point apparatus 01 For flash point determination in refined Oils 10. Water Purification System 01 For lab. HPLC Grade / AAS grade water generation Note 1 : The bidders has to quote for all the items mentioned above. In Case bidder fails to quote for all the items mentioned above his bid will not be considered for evaluation. Consortium is allowed as a single entity or a subsidiary. Note 2 : Necessary Civil/Electrical work required for installation of equipment’s mentioned above shall be carried out by the successful bidder.
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2017-18 FOR PROCUREMENT OF MINOR EQUIPMENTS: … · Digital BUTRYO Refractometer 01 For BR, RI, Brix measurements in Oils and Fats 9. Flash point apparatus 01 For flash point determination

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Page 1: 2017-18 FOR PROCUREMENT OF MINOR EQUIPMENTS: … · Digital BUTRYO Refractometer 01 For BR, RI, Brix measurements in Oils and Fats 9. Flash point apparatus 01 For flash point determination

File No. 12015/02/2017-QAFood Safety and Standards Authority of India

(A statutory Authority established under the Food Safety and Standards Act, 2006)(Quality Assurance Division)

FDA Bhawan, Kotla Road, New Delhi – 110002Dated, the 02nd Jan, 2018

RFP No. 05/2017-18 FOR PROCUREMENT OF MINOR EQUIPMENTS: CORRIGENDUM

Further to this office Tender Enquiry No. 05/2017-18 dated 07th December 2017 andPre-Bid conference held on 21st Dec 2017.

2. The following amendment are made in the ibid tender:

(a) Last Date and Time for Receipt of Tenders: 23 Jan 2018 at 1500hrs

(b) Date and Time of Opening of Tenders: 23 Jan 2018 at 1530hrs

(c) Part II- Essential Details of items/services required is revised as under:

1. Schedule of Requirements – List of items/services required is as follow :-

Sl.No

Items Qty(Nos)

Purpose

1. Atomic Absorption Spectrophotometer[GTA /FLAME / VGA]

01 For trace metal analysis in foodand water

2. Lovibond Tintometer 01 For sesame oil / Color in oiltests

3. Flame Photometer 01 For minerals viz. Na, K, Ca.

4. Muffle Furnace 02 For determination of Ash5. Gas Chromatograph with FID and ECD

Detectors01 For analysis of Pesticides

residues and other Food &Water related applications asper FSSAI requirements

6. Gas Chromatograph with NPD andThermal Conductivity Detector(TCD )Detectors

01

7. Microwave Digestion System 01 For sample preparation prior tometal analysis by AAS

8. Digital BUTRYO Refractometer 01 For BR, RI, Brix measurementsin Oils and Fats

9. Flash point apparatus 01 For flash point determination inrefined Oils

10. Water Purification System 01 For lab. HPLC Grade / AASgrade water generation

Note 1 : The bidders has to quote for all the items mentioned above. In Case bidder fails to quote for allthe items mentioned above his bid will not be considered for evaluation. Consortium is allowed as a singleentity or a subsidiary.

Note 2 : Necessary Civil/Electrical work required for installation of equipment’s mentioned above shall becarried out by the successful bidder.

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2. Revised Technical Details:

REVISED SPECIFICATIONS

Sl.No Item Specifications1. ATOMIC ABSORPTION

SPECTROPHOTMETER[GTA /FLAME / VGA]

Atomic Absorption Spectrophotometer(GTA/FLAME/VGA), Computer Controlled withbuilt-in flame emission mode, Unit for Flame (AirAcetylene and nitrous oxide- acetylene), GraphiteTube Atomizer (GTA), Chiller / Water circulatingunit, Auto samplers for GTA and flame

Wave length range 190 – 800 nm wave length Sensitivity at least 0.9 abs for 5µg/ml aqueous

copper standard solution with air – acetylene flame Optics: Double Beam dual blazed / holographic

Czerny turner Monochromator Focal length At least 250 mm focal length Resolution 1800 lines / mm Width Automatic bandwidth of 0.2 to 1.0 nm

Flame Atomizer: All titanium or equivalent burnerwith impact bead / Flow spoiler, premix Design

Movement Automatic movement into thesample compartment

Affect from Acids /Organic solventUnaffected from attacks by acid solution ororganic solvents (e.g. Methyl isobutyl Ketonei.e. MIBK

Flame Alignment in liquid beam Fullyautomatic, optimized with motorized burnermount for vertical and horizontal burneradjustment

Nebulizer High precision able to providemanually adjustable uptake rates material ofthe nebulizer and related Venturi should beinert to acid solutions and organic solventssuch as MIBK

Flame Control Computer controlled ignition Gas Control Computer controlled with oxidant and

fuel gases monitoring to monitor constant fuel /oxidant ration ignition

Safety Function Interlocking system to preventignition

Essential Interlock Monitor Burner type as well asits presence in position, air selector, flame sensor,liquid trap level, gas supply pressure and air supplyanywhere in the network of gas tubings in thesystem

Automatic Lamp Selection Function Computercontrolled Hollow Cathode Lamp selection andalignment Lamp Holder At least 8 lamp holder withbuilt in power supplies for hollow cathode lamps

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Sl.No Item Specificationsand electrode – less discharge lamps or equivalentOperating Parameter setting Automatic Setting

Read Out /Display Display facility for absorbance aswell as concentration, Display of errors or errorcodes, absorbance range at least up to 2.0 Abs.

Scale Expansion Scale expansion at least upto 100x

Integration time Integration time shouldcover at least 0.2 to 50 seconds range

Measurement Measurements of mean, RSDand CV, Background only mode, Integrationof peak height and peak areas.

Accessories / Spares with Flame AA System Vapour Generation Assembly: Should be

continuous flow based hydride / mercuryvapour generator with option of using with orwithout a programmable auto sampler

Precision Precision of better than or atleast 1% at ppb levels of mercury,arsenic etc.

Absorption Cell The absorption cell’smaterial should have no effect of thehigh heat of the flame and the cell forthe analysis of mercury should be of aclosed cell design

Flame Arrester Flame arrester shouldbe provided in the tube whichconnects the assembly to theabsorption cell

Cell Design holder. The design of thecell holder should give a firm andeasily adjustable (for alignment)mounting on the burner head.

System accessories Complete withnecessary reagent bottles,connectors etc.

Hollow Cathode lamps 16 hollow cathodelamps. One lamp each for the elements:Arsenic, Antimony, Boron, Calcium,Chromium, Cobalt, Copper, Iron, 19 Nickel,Lead, Manganese, Mercury, Selenium, Tin,Vanadium and Zinc. Equivalent coded lampswill also be acceptable.

Air Compressor with Air Filter or equivalentAir Service Unit Complete with pressureregulator quite in operation, necessarytubing and connectors and should meet theair supply requirements of AAS operation.Oil Free Pump Oil- free pump and moisturetrap Corrosion Resistant Resistant to acidicvapour and the drain value (if any) should be

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Sl.No Item Specificationsmade of stainless steel of equivalentcorrosion resistant material

Gas Regulators Nitrous – oxide gasregulator Nitrous Oxide Gas regulator (twostage) with heater, with necessary tubingsand connectors. Necessary transformershould be provided to transform this supplyto the requirements of the heater. The heatershould work on 230±10volts 50 Hz AC powersupply. Acetylene Gas regulator Acetylenegas regulator (two stage) with necessarytubing and connectors. Nitrogen Gasregulator Nitrogen regulator (two stage) withnecessary tunings and connectors.

Graphite Furnace System: Graphite Tube: Atomizer Should be

computer controlled fully enclosed graphitetube system consisting of stabilizedtemperature / total pyrolytic graphite plateform.

Gas Supplies: Provision of two gas supplies(programme selectable) with independentcontrol over the gas supply through thefurnace.

Heating Rate: Heating rate of at least2000°C per second Cooling Time

Cooling time: 20 seconds Temperature Range: Temperature range

ambient to 2600°C or more in 1°Cincrements Feed back system

Feed back system for furnace temperaturecontrol, interlocks for water, gas,temperature, furnace door, graphite tubedamage and mains power.

Temp. Programming: At least eight stepstemperature programming facility withflexibility of programme selection, ramp time,gases, gas flow and read trigger for 20 eachtemperature step.

Control: Computer controlled withappropriate provision for print out of thefurnace and sample parameters

Display: Calibration data / graphs,temperature profiles, signal graphics and theinstrument status.

Memory: Memory should be able to store atleast ten non volatile programmes

Ciller / Cooling Water Re-circulation Unit:Refrigerating water circulation unit ofappropriate capacity. No discharge of waterfrom this water circulation unit.

DATA WORK STATION

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Sl.No Item Specifications

Application Software: Programme facility with multitasking

software Should provide complete control of

instrument with instrument statusdisplay and its various accessories.

Provide accurate and reproducibletime averaged, integration, non –averaged integration, multi levelcalibration.

Software should handle instrumentlinear absorbance reading,concentration, or emission intensity,integration time, built-in statistics,calibration equation control, slope ofanalytical curve using operatorselective calibration standard

Built-in interface for computerconnection and use of optionalaccessories.

Comprehensive quality controlprotocols facility including blank,multiple quality control standards,QA/QC audit trail and calibrationfailure.

Computer System: Make: Reputed brand such as

HP/Compaq/IBM/ Dell Processor: Intel core 2 duo processor

3.00 GHz or above RAM: 4 GB ( upgradable up to 8 GB)

HDD 500 GB ultra DMA or higherHDD ( 7200 RMP)

Monitor: 21” TFT – LCD Flat Colour CD ROM: 52X CD- ROM DVD-CDRW: 32X DVD-ROM and

CDRW – combo Drive Max speed48x24x48

Ports: 2 serial, 1 parallel and 2 USBfront 6 rear USB2 PS/2 Port, 1 VGAintegrated Port 1line in/out port

Key Board: 104 keys Mouse: Optical mouse with pad Ethernet: 32 bit auto selectable

10/100 MBPS Graphics: Internet ready with

integrated graphics Sound: Integrated sound card and

inbuilt stereo speakers Printer HP Laserjet Printer 1200 x

1200 dpi 12 PPM black Operation Software:

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Sl.No Item Specifications

Preloaded Windows XP Professionaloperating system with Licensed CD

MS Office 2000 Standard with media,manual and Licensed CD

Preloaded Antivirus with latestversion along with Licensed CD

ADDITIONAL ITEMS Operation Kit: Manufacturers Standard

Operation Kit including all required items,tubings, fittings for start up / regularoperation of instrument.

Operation / maintenance: Manual Operation/ maintenance Manual for each unitAnalytical manual

Analytical manual: including applications forflame, VGA and graphite system ServiceManual

Service manual: with one set of requiredtools for each system / unit

Trouble Shooting Charts, Spare partsCatalogue, Application Notes for trace metalanalysis in food and water samples

Dust Cover One for each unit Consumables: For three years operation for

each of the following units: Flame AAS (basic unit, burner system) Vapourgeneration assembly Graphite FurnaceAtomizer Auto sampler

Operation and Maintenance Training: Twoweeks training to be provided to two scientiston software training, operation, maintenanceand troubleshooting aspects of instrument.

General Conditions of Supply The instrument and all its units should

operate on 230 ±10 volts 50Hz power supply All the operation and maintenance manuals,

circuit diagrams, application notes andapplication softwares to be supplied shouldbe in English Language.

The supplier / manufacturer should haveIndian Agent to provide after sales service.

The main unit and all the sub units of theinstrument should be serviced by the Indianrepresentative of supplier.

The Bidder should be a manufacturer /authorized representative of a manufacturer,who must have designed, manufactured,tested and supplied two numbers of suchequipment similar to the type specified in thepast five years, which shall be in successfuloperation for at least 2 years as on the dateof bid opening.

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Sl.No Item Specifications

The bidder should furnish the information onpast supplies and their satisfactoryperformance.

Bidders shall invariably furnish documentaryevidence (client’s certificate – at least two) insupport of the satisfactory operation of theequipment as specified above.

Notwithstanding anything stated above thepurchaser reserves the right to assess thecapability and capacity of the bidder toperform the contract, should thecircumstances warrant such an assessmentin the overall interest of the purchaser.

Comprehensive warranty with spares for fiveyears from the date of installation of theinstrument should be covered.

Buy-back price for old Atomic AbsorptionSpectrophotometer [Make: GBC ScientificEquipments, Australia, Model: Avanta PM andSystem AVANTA ULTRA Z1 & PAL4000 Auto-sampler Year of Installation: 2001] may also bequoted

2. LOVIBOND TINTOMETER Measuring principle: Visual, in terms of Lovibond®units

Modes: Transmittance, reflectance Range 0.1 -79.9 Red, Yellow; 0.1 - 49.9 Blue; 0.1 - 3.9 Neutral

Resolution: 0.1 Lovibond® unit Optical system: 11 glass-filled nylon racks

containing a graduated range ofLovibond® colour glasses

Viewing system Fully adjustable, prismatic withintegral blue filter for lightstandardization

Light source 2 x 12 Volt, 10 Watt tungsten halogenlamp Illuminant approximates to daylight

Path length Up to 153 mm (6”) Power pack 12 Volt ac, switchable to suit 220/110

Volt supply Approvals CEInstrument housing Fabricated sheet steel with atough, textured paint finish

Conformance filters and certified colour referencesolutions representing a range of Lovibond®colours, for quick and simple quality control checkson instruments and operators.

Certifications: Product certification: CE / US FDA / BIS

certified. Quality Certification: ISO certified. Should provide calibration certificates from

NIST traceable agencies during warranty &CMC period. Calibration cost will have to beborne by the supplier.

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Sl.No Item Specifications

DQ, IQ, OQ, PQ Documentation during installation. For validation vender should having it own

capability with their own company trained serviceengineer to perform validation. No third partvalidation will be entertained. One validation at thetime of installation should be done by companypersonnel.

Warranty: Comprehensive warranty with spares forfive years from the date of installation of theinstrument should be covered.

Buy-back price for old Digital Lovibond Tintometer[Make: Tintometer Ltd., U.K. Model: PFX 995 Yearof Installation: 2003] may also be quoted

3. FLAME PHOTOMETER Range Na+: 0 to 199.9 ppm, K+: 0 to 9.99 ppm,Li+: 0 to 9.99 ppm

Sensitivity 0.1 ppm Na+; K=100 units Specificity less than 0.5% interference when

concentrations are equal to test sampleconcentrations

Reproducibility less than 0.5% C.V. Linearity less than 1% Display dual display; 3-1/2-digit LED, 12.5 mm

(1/2") Fuel supply high-grade propane/butane mixture

regulated at approximately 30 psi Air supply 6 liters/min at 12 psi; oil and moisture

free Recorder output 0.05 to 5 V (switchable) Certifications:

Product certification: CE / US FDA / BIScertified.

Quality Certification: ISO certified. Should provide calibration certificates from

NABL accredited agency every year duringwarranty & CMC period. Calibration cost willhave to be borne by the supplier.

Equipment should be FDA / CE certified orequivalent standard of repute. It should be ISO9001:2000 or other equivalent quality certification.

All electrical peripherals required for smoothfunctioning e.g. voltage stabilizer should beprovided with the equipment.

Warranty: Comprehensive warranty with spares forfive years from the date of installation of theinstrument should be covered.

4. MUFFLE FURNACE 1200 degree with 23 liter capacity or more Double Shell case, Stainless Steel High Purity insulation material with efficient low

thermal insulation Bench top model

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Sl.No Item Specifications

Vertically lift break switch/side lift break with frontloading

Door: positive break switch Inside Chamber Size: 245-280 mm x 340-400 mm x 230-

250 mm (WDH) Maximum temperature: 1200oC Standard

continuous temperature 1050 oC or more Heating Rate: The furnace should be fast heating

type with maximum attainable temperature shouldreach in 110 mins or better

Temperature control: Should be microprocessorbased & at least 8 segment programmable 3216P1or equivalent controller with necessary safetyfeatures. Programmable Temperature controllerwith heating rate control from 10 deg. min-1 to 100deg.min-1 preferable

Temperature Accuracy: ± 5oC over the wholetemperature range of operation and in the entiremuffle

Safety: Over Temperature protection should beadded

Gas purging: Gas purging facility (inert gas inlet andoutlet)

Weight : less than 80 kg The furnace should be CE certified with suitable

power supply Installation, training and commissioning: Vendor

must ensure satisfactory installation andcommissioning of the system at CFL, Kolkata. Adetailed training on handling, operation andapplications must be provided to at least 5scientists. Installation services must includeIQ/OQ/PQ

For validation vender should have its own capabilitywith their own company trained service engineer toperform validation. No third part validation will beentertained. One validation at the time of installationshould be done by company personnel.

Warranty: Comprehensive warranty with spares forfive years from the date of installation of theinstrument should be covered.

Buy-back price for old Muffle furnace [Make:Heraeus Instrument, Germany, Model: M110, Yearof Installation: 2000] may also be quoted

5. GASCHROMATOGRAPHYWITH FID AND ECDDETECTORS

Pesticides residues and other Food & Water relatedapplications as per FSSAI requirements

Gas chromatograph with capability of operatingconcurrently with two injectors or better and threedetectors. The system should be quoted with allaccessories required to make it fully operationaland any other item required for stated applicationsbe quoted as optional.

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Sl.No Item SpecificationsOven Upto 450 oC, Fast Oven with 120 oC/min ramp,

≥20≥7ramps Cool-down time from 450 oC to 50oC within 5

minutes Should be able to accommodate two or more

injectors and three detectors Automatic leak test of system through single key

Pneumatic Controls 0-140 psi or better, all Electronic PneumaticControls with 0.1 psi precision

Injector ( 2 or more) Should be capable of large volume injectionTemperature ramped splitless, Split and Cold on-column modes ≥450 OC max. and ≥10 ramps.

Multimode/PTV with 250µL or better InjectionVolume capability with complete solvent vaporizersystem or Equivalent.

Injector must be able to operate with capillary & widebore columns

Injector must be provided with Backflush system.Autosampler ( Liquid andHeadspace)

Robust Liquid autosampler capable of injecting ≥100samples or better with syringe capacity of 0.5-100 µl

The type and volume of the syringe must beautomatically detected by the system.

Must allow installation and automation of syringefeaturing volumes from 0.5 to 100 µl.

Must be able to achieve combined multiple solventrinsing with upto 4 different solvents.

Head space auto sampler with a capacity ≥50 vials orbetter that support 10 & 20ml vial capacity withPnuematic control Incubation Oven Temperature Range 50 to 200 °C in

1 °C steps Syringe Temperature 50 °C to 150 °C in 1 °C steps Incubation Oven Capacity vials or better

Detectors The GC must have complete integrated control of allparameters (no external control module) for thefollowing detectors: FID, and ECD.

Detector must be independently controlled andoperational for maximum sensitivity

Flame Ionization Detector(FID

Linear range : better than 107

Minimum detectable amount with makeup gases : 1.5pgC/sec

Operating temperature limits: 450oC with standardceramic/quartz flame jet

Auto flame out detection. Acquisition rate 50 Hz or more.

Electron Capture DetectorECD

Linear dynamic range : better than 104

Complete with 63Ni source and low voltage heaters.

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Sl.No Item Specifications

Minimum detectable amount: Less than 10 fg oflindane.

Operating temperature limits : 400oCGas Supplies Required High purity Gas cylinders (2 No. Each)SOFTWARE AND HARDWARE ( Single point control of Software & Hardware)Software Complete system and software configuration must be 21

CFR Part 11 compliant. Software: Windows Basedsoftware with multitasking and capable of performing thefollowing functions: Control the MS, acquire, store,process and reproduce the data. It must be able tocontrol all the devices from same software. Softwareshould allow monitoring of one molecular ion and uptofour confirmatory ions. Quantification software for batchprocess must confirm the analytes as per regulatoryrequirements in food and environmental sample analysisas per the applications specified.All Flow Controller i.e.Carrier flow, Make-up flow, Hydrogen flow, Air flow etc.value should set through Software by PC.Head SpaceAuto Sampler, Automation and event control from PCthrough same software.IQOQ of the system as well assoftware must be provided. Software update upto fiveyears

Communication Hardware: Latest Factory set, branded system with 22-23” Full HDMonitor with Printer - B/W - duplex - laser - Legal, A4 -1200 dpi x 1200 dpi - up to 21 ppm – capacity withNetwork Card and Bluetooth facility.

IQOQPQ IQOQPQ of instrument and Software should beprovided along with document.

Training Technical and application training to the personnel atsite immediately after installation as per terms &conditions of tender.

Application Support The Application support for stated applications requiredduring method development and validations.

Pre InstallationRequirements (PIR)

Provide PIR of the system.

OTHER REQUISITES FOR GC WITH ECD, FIDAutomatic Change Over Manifold for each gas lineComplete Gas Purification Panel with fittings & installation of all gasesRenewable In Line Gas Purification SystemRenewable gas purifier cartridge, Spare SetGas clean filters/Traps (6 No.)Septa for injectors Non stick, Low bleed, high puncture tolerance and Max.

Temp 400 oC (for each injector). (400 No.)Liners Suitable Ultra Inert Injector Liner for SS & SSL (20

No.) Suitable Injector Liner upto 10 µL (6 No.) Suitable Injector Liner upto 250 µL (6 No.) Suitable Injector Liner upto 500 µL (6 No.) Liner O-Rings Max Temp 375 oC (100 No.)

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Sl.No Item Specifications

Liners types required as per the applicationFerrules and Nuts 50 No. (for each column end and other interfaces as

applicable), 50 No. for GC with ECD, NPD, FIDColumns for GC Applications Pesticide column (30m x 0.250mm x 0.25µm (HP-

5MS / DB-1MS or equivalent) (02 no.) Column for Fatty Acid Profiling with main concern of

Trans Fatty Acid Application (02 No.) Column for Cholesterol Application (02 No.)

Vials, caps and tool forautosampler(Only Compatible sizesshould be supplied)

2000 No. each Vial sets (1, 2 mL, Crimp type, Amberand Clear glass )

200 No. Vials (10,20ml Crimp type with cap & septa) 1000 No. 300/500 µL Recovery vials 6000 No. Septa PTFE/Silicone (for 1, 2 mL Vials) 6000 No. Septa PTFE/Silicone (for 10, 20 mL

Headspace Vials) Ergonomic Crimping Tools for different vial types Ergonomic Decapping Tools for different vial types 10 No. each Storage Racks for (for 1, 2 mL Vials) Head Space vials 10,20 ml capacity (500no. each)

Autosampler Syringe 10 µL (12 No.), 100 and 250 µL (04 No. each); Manualsyringe-2µl, 5µl and 500 µl (04 No. each).Headspace syringe (02 no.10µl, 500µl,02 no. 1ml)

Sample Preparation(Water & Food)

QuEChERS Kits for Pesticides and Herbicides infollowing Matrices:

Water (1000 No.) Matrices with high fat (1000 No.) Matrices with high Water content and (1000 No.) Matrices with high pigmented (1000 No.)

Tools and Kits Septa Removing toolTubing Cutter with rotating diamond blade for columnTubing Cutter for stainless steel tubing (1/16 & 1/8 inchtubing)Tubing Cutter for Plastic tubing with spare blade set

Miscellaneous Consumables required for each detector must beprovided

Warranty Comprehensive warranty with spares for five years fromthe date of installation of the instrument should becovered.

Buy Back Buy back price for old Gas Chromatograph - MassSpectrometer (GC / MS) With Headspace (HS) sampler, ECD,FID and Single Quadruple MS detector [Make: Perkin ElmerUSA Model: Clarus® 500, Year of Installation: 2006 may alsobe quoted.

6. GASCHROMATOGRAPHYWITH NPD ANDTHERMALCONDUCTIVITIYDETECTOR(TCD)DETECTORS

Pesticides residues and other Food & Water relatedapplications as per FSSAI requirements

Gas chromatograph with capability of operatingconcurrently with two injectors or better and threedetectors. The system should be quoted with allaccessories required to make it fully operational

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Sl.No Item Specificationsand any other item required for stated applicationsbe quoted as optional.

Oven Upto 450 oC, Fast Oven with 120 oC/min ramp,≥20≥7ramps

Cool-down time from 450 oC to 50oC within 5minutes

Should be able to accommodate two or moreinjectors and three detectors

Automatic leak test of system through single keyPneumatic Controls 0-140 psi or better, all Electronic Pneumatic

Controls with 0.1 psi precision

Injector ( 2 or more) Should be capable of large volume injectionTemperature ramped split-less, Split and Cold on-column modes ≥450 OC max and ≥10 ramps.

Multimode/PTV with 250µL or better InjectionVolume capability with complete solvent vaporizersystem or Equivalent.

Injector must be able to operate with capillary & widebore columns

Injector must be provided with Backflush system.Autosampler Robust Liquid autosampler capable of injecting ≥100

samples or better with syringe capacity of 0.5-100 µl The type and volume of the syringe must be

automatically detected by the system. Must allow installation and automation of syringe

featuring volumes from 0.5 to 100 µl. Must be able to achieve combined multiple solvent

rinsing with upto 4 different solvents.

Detectors The GC must have complete integrated control of allparameters (no external control module) for thefollowing detectors: NPD, and TCD.

Detector must be independently controlled andoperational for maximum sensitivity

Nitrogen PhosphorusDetector (NPD)

Minimum detectable amount: 100fg N/sec, 100fgP/sec

Linear dynamic range: better than 104

Operating temperature limits: 450 C with standard jetThermal ConductivityDetector TCD

Capillary-column compatible Proven constant current design Software protection to prevent filament burnout Ideal for series operation 1/8-in. fittings PPC pneumatics - software flow control of reference

gas Operating temperature 100 ˚C to 350 ˚C in 1 ˚C

increments

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Sl.No Item Specifications

Sensitivity 9 µV/ppmnonane at 160 mA at the bridgewith a detector temperature of 100 ˚C or 100pgtridecane, /mL with He

Minimum detectable quantity Typically < 1 ppmnonane

Linear dynamic range: better than 105 +/- 5% Operating temperature limits: 400 C

Gas Supplies Required High purity Gas cylinders (2 No. Each)SOFTWARE AND HARDWARE ( Single point control of Software & Hardware)Software Complete system and software configuration must be 21

CFR Part 11 compliant. Software: Windows Basedsoftware with multitasking and capable of performing thefollowing functions: Control the MS, acquire, store,process and reproduce the data. It must be able tocontrol all the devices from same software. Softwareshould allow monitoring of one molecular ion and uptofour confirmatory ions. Quantification software for batchprocess must confirm the analytes as per regulatoryrequirements in food and environmental sample analysisas per the applications specified.All Flow Controller i.e.Carrier flow, Make-up flow, Hydrogen flow, Air flow etc.value should set through Software by PC.Head SpaceAuto Sampler, Automation and event control from PCthrough same software.IQOQ of the system as well assoftware must be provided.Software update upto five years

Communication Hardware: Latest Factory set, branded system with 22-23” Full HDMonitor with Printer - B/W - duplex - laser - Legal, A4 -1200 dpi x 1200 dpi - up to 21 ppm – capacity withNetwork Card and Bluetooth facility.

IQOQPQ IQOQPQ of instrument and Software should beprovided along with document.

Training Technical and application training to the personnel atsite immediately after installation as per terms &conditions of tender.

Application Support The Application support for stated applications requiredduring method development and validations.

Pre InstallationRequirements (PIR)

Provide PIR of the system.

OTHER REQUISITES FOR GC WITH NPD, TCDAutomatic Change Over Manifold for each gas lineComplete Gas Purification Panel with fittings & installation of all gasesRenewable In Line Gas Purification SystemRenewable gas purifier cartridge, Spare SetGas clean filters/Traps (6 No.)Septa for injectors Non stick, Low bleed, high puncture tolerance and Max.

Temp 400 oC (for each injector). (400 No.)Liners Suitable Ultra Inert Injector Liner for SS & SSL (20

No.)

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Sl.No Item Specifications

Suitable Injector Liner upto 10 µL (6 No.) Suitable Injector Liner upto 250 µL (6 No.) Suitable Injector Liner upto 500 µL (6 No.) Liner O-Rings Max Temp 375 oC (100 No.) Liners types required as per the application

Ferrules and Nuts 50 No. (for each column end and other interfaces asapplicable), 50 No. for GC with ECD, NPD, FID

Columns for GC Applications Pesticide column (30m x 0.250mm x 0.25µm (HP-5MS / DB-1MS or equivalent) (02 no.)

Column for Fatty Acid Profiling with main concern ofTrans Fatty Acid Application (02 No.)

Column for Cholesterol Application (02 No.)Vials, caps and tool forautosampler(Only Compatible sizesshould be supplied)

2000 No. each Vial sets (1, 2 mL, Crimp type, Amberand Clear glass )

200 No. Vials (10,20ml Crimp type with cap & septa) 1000 No. 300/500 µL Recovery vials 6000 No. Septa PTFE/Silicone (for 1, 2 mL Vials) Ergonomic Crimping Tools for different vial types Ergonomic Decapping Tools for different vial types 10 No. each Storage Racks for (for 1, 2 mL Vials)

Autosampler Syringe 10 µL (12 No.), 100 and 250 µL (04 No. each); Manualsyringe-2µl, 5µl and 500 µl (04 No. each).

Sample Preparation(Water & Food)

QuEChERS Kits for Pesticides and Herbicides infollowing Matrices:

Water (1000 No.) Matrices with high fat (1000 No.) Matrices with high Water content and (1000 No.) Matrices with high pigmented (1000 No.)

Tools and Kits Septa Removing toolTubing Cutter with rotating diamond blade for columnTubing Cutter for stainless steel tubing (1/16 & 1/8 inchtubing)Tubing Cutter for Plastic tubing with spare blade set

Miscellaneous Consumables required for each detector must beprovided

Warranty Comprehensive warranty with spares for five years fromthe date of installation of the instrument should becovered.

7. MICROWAVE DIGESTIONSYSTEM

A latest model of microwave digestion system shouldenable rapid digestion for different inorganic/organicsamples like; Different types of FSSAI food and foodproducts, Fish and Fishery products, tea, seasoningpowder, biscuits etc.

Application A latest model of microwave digestion system shouldenable rapid digestion for different inorganic/organicsamples like; Different types of FSSAI food and foodproducts, Fish and Fishery products, tea, seasoningpowder, biscuits etc

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Sl.No Item SpecificationsGeneral The instrument should have a superior pressure venting

so as to prevent any loss of volatile metals and shouldhave homogeneous microwave field to avoid sampleburning

System Microwave digestion system should have temperatureand pressure controlling/monitoring system. The systemshould be software controlled. Different types of rotorsavailable for the digestion of the different type samplesshould also be quoted. Necessary consumables andmaintenance parts should also be quoted to runinstrument trouble free

Instrument The system should be a stand alone work station andshould have The System should have the feature of simply

choose a method and it automatically recognizesthe vessel type, counts the vessels and determinesall of the parameters necessary for a fast, completedigestion

Should have provision that user can set the desiredparameters for digestion

Should have Automatic Microwave powerapplication depending on the load

Auto sensing of temperature and pressure insidethe vessel

Be capable of processing different amounts ofsamples (from 0.3 g up to 10g) in the same runassuring the same conditions of temperature andpressure

Display The Instrument should have the high-resolution, colourtouch screen, acid resistant, LED/LCD screen shouldserve as controller and display. Should be providedtraining videos for sample preparation vessel assembly,system use, and maintenance. Should have Datamanagement – Easy access to stored methods, real-time data and results of past runs. Should be able todisplay the detailed methods, graphs o f temperatureand power against time and temperature of individualvessels.

Interlocks The system should have good interlocking system forsafety and cavity door.

Vessel The system should be high throughput which can holdatleast 24 high pressure vessels. Must be supplied withdigestion vessel racks and suitably handle differentdigestion volumes.

System The material of construction should be high purity TFMfluropolymer. Vessel should be capable of handlingvolumes between 10 ml and > 25 ml, if required. Itshould be operated for maximum temperature capacityof 250ºC or more and maximum pressure of 35 Bar ormore. The system should be provided with temperaturesensor (Thermocouple type/ Fiber optics/IR Sensor)

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Sl.No Item Specificationswhich will measure real temperature of the vessels andcontrol it. The vessels should have automatic ventingand re-sealing system in case there is excess pressuredevelopment essential. After Digestion, vessels mustbe vent-able before uncapping the vessel for safetyreasons. For ease of use, the vessels must not requirethe use of an energizing tool in order to reform seals priorto operation. Additional twelve numbers of vesselsshould be supplied along with the system.

Microwave Power andoutput with uniform energydistribution

The Instrument should have single/dual magnetron 1500W (or more of delivered energy, should provide thetemperature needed (300 °C) for difficult samplesand high-throughput vessel sets delivering unpulsedcontinuous power & precisely tuned wave guide.Disperses microwave energy uniformly throughout thecavity. No need for motor driven diffusers or attenuators.System software must automatically adjust the powerdelivery based upon sample load and pre-programmed control settings. Automatic Power controlTechnology delivers maximum energy to the sample,ensuring complete digestions. Controllable viamicroprocessor 230 V input, pulsed and unpulsed-essential 50 Hz, AC Operated. The Instrument shouldhave “waveguide” between the magnetron (themicrowave energy source) and the cavity. Thiswaveguide fed system should provide maximum tunedtransfer of microwave energy from the magnetron to theload in the microwave cavity. planes. This should resultin uniform heating of the sample load.

Microwave Cavity The microwave cavity should be heavy duty and havesufficient space to mount and dismount vesselsindividually and all parts inside the cavity should betotally microwave transparent. The Cavity should beconstructed with non magnetic Rugged high-grade 316solid steel cavity. The vessel assembly during a runshould be visible from outside The coating inside thecavity should be acid/ chemical. resistant specialpolymer coating like fluro-polymer / PTFE.

Controls The Instrument should have a) Reliable Temperatureand b) Pressure controls independent of each other

Automatic temperature control system,temperature sensor should be protected properlyfrom any chemical attack, sensor should monitorand control all vessels simultaneously-essential

Automatic Pressure control: should have apressure sensor which has a total capability of upto 500psi automatically control the pressure. Itshould be possible to remove the pressure deviceat a high pressure. The Vessels should actas self-regulators of pressure

Control The control terminal should have high resolutionLED/LCD Acid Resistant display. Touch screen which

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Sl.No Item Specificationsshould have method storage capacity. All the featuresshould be in built in the software. Should have provisionfor manual programming storage apart from pre-installed programme. Continuous display of temperatureand power inside the reaction vessels is required.

Safety There has to be multiple levels of safety. A safemechanism to tackle the unused or reflected microwaveenergy Capable of shutting off in the event of the A veryloud noise or bang in the instrument. If the temperatureof the vessel is near its highest tolerance limit. Haveinbuilt exhaust system to cool the vessels and to driveaway if any fumes in the cavity-essential

Quality Standards The manufacturer should be ISO 9001 certified fordesign and manufacture of microwave digestion system

Certification required for signoff

IQ/OQ compliance Calibration certificates for titrator GLP-validated software for controlling the system

Operation andmaintenancetraining component

The supplier will have to carry out successfulinstallation at our laboratory premises (where ever thesystem has to be installed) and provide on – sitecomprehensive training for scientific personneloperating the system and support services till customersatisfaction with the system.

Warranty Comprehensive warranty with spares for five years fromthe date of installation of the instrument should becovered. This will include yearly calibration start-up /commissioning routine servicing, regular maintenance,preventive maintenance of equipment and componentsand break down repairs as and when occurring,ensuring that system does not remain out of service fora period more than 24 hours in case of majorbreakdowns and 6-8 hour in the case of minorbreakdowns due to any unforeseen break down. Theinstitution will provide Water / Electricity power, etc. formaintenance work. The successful tenderer shall keepthe essential spares at site during the Contract Periodto avoid the delay in attending faults / maintenance.

Service contract clauses,including prices

List of all spares and accessories (including minor) withpart numbers and price, required for maintenance andrepairs in future after guarantee/warranty period shouldbe attached.

Operating manuals, servicemanuals, other manuals

Should provide 2 sets (hardcopy and soft-copy) of:- User, technical and maintenance manuals to be

supplied in English language along with machinediagrams;

List of equipment and procedures required for localcalibration and routine maintenance;

Service and operation manuals (original and copy) tobe provided;

Advanced maintenance tasks documentation;

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Sl.No Item Specifications

Certificate of calibration and inspection

Certificates Performanceand safety standards(specific to the devicetype);Local and/orinternational

Should be FDA/CE/BIS approved product.

Manufacturer and Supplier should have ISO13485 certification under ISO 9001for qualitystandards.

Electrical safety conforms to the standards forelectrical safety IEC 60601- Generalrequirements (or equivalent BIS Standard)

Certified to be compliant with IEC 61010-1, IEC61010-2-40 for safety

Supplier/ Manufacturer Must be ISO certified for quality

Service Support Contactdetails (Hierarchy Wise;including a toll free/landlinenumber)

Contact details of manufacturer, supplier andlocal service agent to be provided; Any Contract(AMC/CMC/adhoc) to be declared by themanufacturer;

Recommendations orwarnings

Any warning signs would be adequately displayed

Buy Back Microwave Digestion System [Make: CEM Corp., USAModel: MARS 5, Year of Installation: 2008.

8. DIGITAL BUTRYOREFRACTOMETER

For checking purity and adulteration of fats and oils

System Automated Operating LCD screen directly withoutmanual alignment, can connect PC with RS232 interface

Display The required data to be displayed on the screen,including: the date, temperature, refractive index,concentration, and amended in accordance with thecurrent temperature

Measurement Range(Automatic TemperatureControlled)

Concentration 0;95% Refractive Index 1.32422-1.7000

Minimum Indication Butyro 0.1%RI 0.00001

Measurement Accuracy Butyro ±0.5% (at 40˚C)RI ±0.0003 (at 40˚C)

Precision (Reproducibilty RI ± 0.00005Butyro ± 0.05

Measurement Temperature 10 to 50˚CAmbient TemperatureSample

10 to 40˚C

Volume Measurement Time Less than 5 secSample Volume > 0.1 mlCalibration certificateAccessories Reference Material Oil minimum 10 ml

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Sl.No Item SpecificationsOperation and trainingcomponent

The supplier will have to carry out successfulInstallation at the laboratory premises (where ever thesystem has to be installed) and provide on – sitecomprehensive training for a minimum of two scientificpersonnel operating the system till customersatisfaction

Certificates Performanceand safety standards(specific to the devicetype);Local and/orinternational

Should be FDA/CE/BIS approved product. Manufacturer and Supplier should have ISO 13485

certification under ISO 9001for quality standards. Electrical safety conforms to the standards for

electrical safety IEC 60601- General requirements(orequivalent BIS Standard)

Certified to be compliant with IEC 61010-1, IEC61010-2-40 for safety

Supplier/ Manufacturer Must be ISO certified for qualityService Support Contactdetails (Hierarchy Wise;including a toll free/landlinenumber)

Contact details of manufacturer, supplier and localservice agent to be provided; Any Contract(AMC/CMC/adhoc) to be declared by themanufacturer;

Recommendations orwarnings

Any warning signs would be adequately displayed

Warranty Comprehensive warranty with spares for five yearsfrom the date of installation of the instrument shouldbe covered.

Service contract clauses,including prices

List of all spares and accessories (including minor)with part numbers and price, required for maintenanceand repairs in future after guarantee/warranty periodshould be attached;

Operating manuals, servicemanuals, other manuals

Should provide 2 sets(hardcopy and soft-copy) of:- User, technical and maintenance manuals to be

supplied in English language along with machinediagrams;

List of equipment and procedures required for localcalibration and routine maintenance;

Service and operation manuals (original and copy) tobe provided;

Advanced maintenance tasks documentation; Certificate of calibration and inspection

Buy Back Buy back price for old Refractometer [Make: BellinghamStanley, U.K. Model: RFM 330, Year of Installation:1996 may also be quoted.

9. Flash point apparatus Instrument designed in strict accordance with thetest method ASTM D93, Method A and B.

Microprocessor controlled unit with digital easy toread display of the results.

Ignition :-Electric ignition and should also provide anautomatic reignition facility.

Thermal detection (with metal sample temperatureprobe) of the flash to eliminate interference fromwater or silicone containing compound.

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Sl.No Item Specifications

Cooling : - Facility for built-in cooling connection. Automatic correction for standard barometric

pressure vis-à-vis with final result. Unit should have diagnostic program to check every

key component and assembly and calibrationfacility.

Unit should automatically determine flash point instrict compliance with the appropriate test method.

Heating should be microprocessor controlled at thespecified rate; the ignitor is activated and dipped atprecisely the correct temperature and frequency.

Safety device for fire protection with alarm. Resistance check box for temperature calibration

with calibration certificate. The unit should be operable on 230v / 50 Hz. The system should be ISO 9001 quality standard

and supplied with operation manual. Merely copying our specifications in the quotation

shall not make the parties eligible for considerationof the quotation. A quotation has to be supportedwith the printed technical leaflet/literature of thequoted model of the item by the quotingparty/manufacturer and the specificationsmentioned in the quotation must bereflected/supported by the printed technicalleaflet/literature.

Calibration : The firm must ensure that theequipment supplied is fully calibrated as perspecification requirements and also source of futurecalibration at New Delhi & their frequency ofcalibration needed

Spares : Vendor should quote recommendedspares for two years alongwith the equipment forsmooth functioning of the equipment.

Spare Parts : Availability of spare parts of theequipment/instrument must be guaranteed for aperiod of at least seven years from the date ofsupply.

After Sales Services: It should be clearly mentionedin the quotation whether the after sales servicesduring and after the completion of warranty shall beprovided directly by the supplier or their authorizedagent/ representative. Terms of the after salesservices, if any, may be mentioned in the offer.However, in both the cases the original suppliershall be responsible for poor performance/services.

Inspection: The inspection of the system will bedone by our technical expert in the presence of firmrepresentative.

Users List : The list of users specifically for the samemodel/make of the quoted item ( not the list ofgeneral users) along with the complete name,

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Sl.No Item Specificationsaddress & contract numbers of the userorganizations/persons may be submitted with thequotation along with the performance certificatesfrom all/some of them.

Training: Our Scientist/Technical persons should betrained by the supplier at the project site free of cost.NOTE:- Firms having equipment wherein singlemother unit can be used for carrying out Flash Pointby Abel Flash Point using interchangeable analyzerunit shall be considered, if otherwise found suitablevis-à-vis price factor & performance. Otherspecification requirement for Abel Flash Pointapparatus is enclosed.

Certifications: Product certification: CE / US FDA / BIS

certified. Quality Certification: ISO certified. Should provide calibration certificates from

NIST traceable calibration solutions by anyagency every year during warranty & CMCperiod. Calibration cost will have to be borneby the supplier.

Comprehensive warranty with spares for five yearsfrom the date of installation of the instrument shouldbe covered.

Buy-back price for old Automated Pensky-Martensclosed-cup flash point tester with sample changermeasures the flash point of up to 12 samplesautomatically [Make: Petrotest, Germany Model:PMA-4, Year of Installation: 2004] may also bequoted.

10. Water Purification system Table top Water Purification System (Tap WaterFeed) should be capable of produce water for usein HPLC solvents, Microbiology and reagent gradewith the help of pre-treatment module; RO Module,DI Module, Storage tank, UV Oxidation Chamber,Polishing module and final membrane filter 0.22um

Pre-treatment System Should consists: 5 micron,1 micron and Activated Carbon wrapped

type depth filter Pressure gauge with regulator The unit should have automatic low/high

pressure cut-offReverse Osmosis withElectro Deionization Stage:

Pre-treatment cartridge with auto-scalingcompounds, 0.5 micron filter and activated carbon orbetter.

Prefilter combination to protect the RO Membraneslife or better.

RO Module with high performance thin filmcomposite membrane with salt retention rate up to98%. The retention rate for dissolved organiccompounds, particles & colloids & bacteria exceeds

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Sl.No Item Specifications99%

Deionization Module: Mixed bed resin moduleutilized for a reduction of the inlet conductivity. Usedfor inorganic applications.

Conductivity measurement is to be done after RO, DI& Polishing module to monitor the performance ofIndividual cartridge.

Should have suitable back wash programme beforeevery operation or better

Storage Tank: 30 L or better Storage Tank with UV Lamp, Air filter,CO2 Trap & Level Sensor.

The tank should made of pure water resistant PolyEthylene material with an outlet to drain the tanktotally and a pressure sensor for the tank levelcontrol

The storage tank should be 100% drainable.

General requirements Online UV oxidation chamber: UV Light Energy at 185nm & 254 nm wavelengths. TOC Measurement: Online continuous TOC

measurement with Live Display. Sterile Filter with 0.22 µm or better with Autoclavable

option for re-use System should meet reagent water quality standards

including ASTM Type 1, CLSI and ISO 3696 Type Ι System should have flexible remote dispenser to

dispense water whenever needed System should have built-in automatic self-cleaning

mechanism to extend the life of cartridge Automatic flushing and recirculation in standby mode

to maintain consistent peak water purity User can collect RO Quality water from the Storage

tank & ultrapure water from flexible dispenser Should have cartridge change indicator The system should incorporate a fully comprehensive,

graphic colour LCD display to provide system status,performance parameters, routine maintenance statusand alarms of troubleshooting, tank level status andautomatic warning of reordering of consumables and Provision for digital display to indicate status of

operation, resistivity or conductivity, temperature andalso alarm system in case of malfunctioning.

Pure Water Specification:(Type-2)

Production Rate : 10 LPH or better Conductivity : <2µs/cm at 298K (25°C) or better pH at 298K (25°C) => 6.6 or effectively neutral Total silica max 3ug/L or better

The Ultrapure Product Watershould of the followingspecifications: (Type-1)

Flow Rate : 1.0 L/min or better Should have conductivity @ 25 Deg C : 0.055

µs/cm or better Should have resistivity @ 25 Deg C : 18.2 MΩ-

cm or better

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Sl.No Item Specifications

TOC : < 1 ppb or better Bacteria : <1 cfu/ml or better Particles >0.1µm : <1 per ml or better pH at 298K (25°C) = > 6.6 or Effectively neutral

Certification required for signoff

IQ/OQ compliance Calibration certificates for titrator

Operation andmaintenancetraining component

The supplier will have to carry out successfulinstallation at our laboratory premises (where ever thesystem has to be installed) and provide on – sitecomprehensive training for scientific personneloperating the system and support services till customersatisfaction with the system.

Warranty Comprehensive warranty with spares for five yearsfrom the date of installation of the instrument should becovered. This will include yearly calibration start-up /commissioning routine servicing, regular maintenance,preventive maintenance of equipment and componentsand break down repairs as and when occurring,ensuring that system does not remain out of service fora period more than 24 hours in case of majorbreakdowns and 6-8 hour in the case of minorbreakdowns due to any unforeseen break down. Theinstitution will provide Water / Electricity power, etc. formaintenance work. The successful tenderer shall keepthe essential spares at site during the Contract Periodto avoid the delay in attending faults / maintenance.

Service contract clauses,including prices

List of all spares and accessories (including minor)with part numbers and price, required formaintenance and repairs in future afterguarantee/warranty period should be attached;

Operating manuals, servicemanuals, other manuals

Should provide 2 sets(hardcopy and soft-copy) of:- User, technical and maintenance manuals to be

supplied in English language along with machinediagrams;

List of equipment and procedures required for localcalibration and routine maintenance;

Service and operation manuals (original and copy) tobe provided;

Advanced maintenance tasks documentation; Certificate of calibration and inspection

Certificates Performanceand safety standards(specific to the devicetype);Local and/orinternational

Should be FDA/CE/BIS approved product. Manufacturer and Supplier should have ISO

13485 certification under ISO 9001for qualitystandards.

Electrical safety conforms to the standards forelectrical safety IEC 60601- Generalrequirements (or equivalent BIS Standard)

Certified to be compliant with IEC 61010-1, IEC61010-2-40 for safety

Supplier/ Manufacturer Must be ISO certified for quality

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Sl.No Item SpecificationsService Support Contactdetails (Hierarchy Wise;including a toll free/landlinenumber)

Contact details of manufacturer, supplier and localservice agent to be provided; Any Contract(AMC/CMC/adhoc) to be declared by themanufacturer;

Recommendations orwarnings

Any warning signs would be adequately displayed

Buy Back Buy Back price for old Deionized water generationsystem [Make: Millipore, U.S.A Model: ELIX 3, 10 ANDMILLI Q, Year of Installation: 2008 may also be quoted.

6. Revised Eligibility Criteria for Pre-Qualification of bidders:

(a) Average Annual financial turnover, during the last three years should not be lessthan Rs. One Crore. Documentary evidence duly attested by a CharteredAccountant/Company Secretary should be submitted alongwith the Technical Bid.Bidders should also enclose notary attested copy of IT returns filed for the last threefinancial years, notary attested audited copy of audited accounts, balance sheet,annual report etc.

Note : There is no change from para 6(b) to 6(j).

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REVISED TECHNICAL BID FORM (B)

The bids of only the technically qualified bidders will be eligible for consideration for opening offinancial bid. The technical bid of the bidders will be evaluated on the basis of specification of theoffered model vis-à-vis the prescribed specification given below :

Sl.No Item Specifications PleaseSpecify

whether thequotedmodel

meets thespecification

(Yes/No)

Name ofthe Model

and itsSpecificati

on

1. ATOMICABSORPTIONSPECTROPHOTMETER [GTA /FLAME /VGA]

Atomic AbsorptionSpectrophotometer(GTA/FLAME/VGA), ComputerControlled with built-in flameemission mode, Unit for Flame (AirAcetylene and nitrous oxide-acetylene), Graphite Tube Atomizer(GTA), Chiller / Water circulatingunit, Auto samplers for GTA andflame

Wave length range 190 – 800 nmwave length

Sensitivity at least 0.9 abs for5µg/ml aqueous copper standardsolution with air – acetylene flame

Optics: Double Beam dual blazed /holographic Czerny turnerMonochromator

Focal length At least 250 mmfocal length

Resolution 1800 lines / mm Width Automatic bandwidth

of 0.2 to 1.0 nm Flame Atomizer: All titanium or

equivalent burner with impact bead/ Flow spoiler, premix Design

Movement Automaticmovement into the samplecompartment

Affect from Acids /Organicsolvent Unaffected fromattacks by acid solution ororganic solvents (e.g. Methylisobutyl Ketone i.e. MIBK

Flame Alignment in liquidbeam Fully automatic,optimized with motorizedburner mount for vertical andhorizontal burner adjustment

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Sl.No Item Specifications PleaseSpecify

whether thequotedmodel

meets thespecification

(Yes/No)

Name ofthe Model

and itsSpecificati

on

Nebulizer High precisionable to provide manuallyadjustable uptake ratesmaterial of the nebulizer andrelated Venturi should beinert to acid solutions andorganic solvents such asMIBK

Flame Control Computer controlledignition

Gas Control Computer controlledwith oxidant and fuel gasesmonitoring to monitor constant fuel /oxidant ration ignition

Safety Function Interlocking systemto prevent ignition

Essential Interlock Monitor Burnertype as well as its presence inposition, air selector, flame sensor,liquid trap level, gas supplypressure and air supply anywhere inthe network of gas tubings in thesystem

Automatic Lamp Selection FunctionComputer controlled HollowCathode Lamp selection andalignment Lamp Holder At least 8lamp holder with built in powersupplies for hollow cathode lampsand electrode – less dischargelamps or equivalent OperatingParameter setting AutomaticSetting

Read Out /Display Display facilityfor absorbance as well asconcentration, Display of errors orerror codes, absorbance range atleast up to 2.0 Abs.

Scale Expansion Scaleexpansion at least up to 100x

Integration time Integrationtime should cover at least 0.2to 50 seconds range

MeasurementMeasurements of mean,RSD and CV, Background

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Sl.No Item Specifications PleaseSpecify

whether thequotedmodel

meets thespecification

(Yes/No)

Name ofthe Model

and itsSpecificati

on

only mode, Integration ofpeak height and peak areas.

Accessories / Spares with Flame AASystem

Vapour GenerationAssembly: Should becontinuous flow basedhydride / mercury vapourgenerator with option ofusing with or without aprogrammable auto sampler

Precision Precision ofbetter than or at least1% at ppb levels ofmercury, arsenic etc.

Absorption Cell Theabsorption cell’smaterial should haveno effect of the highheat of the flame andthe cell for theanalysis of mercuryshould be of a closedcell design

Flame Arrester Flamearrester should beprovided in the tubewhich connects theassembly to theabsorption cell

Cell Design holder.The design of the cellholder should give afirm and easilyadjustable (foralignment) mountingon the burner head.

System accessoriesComplete withnecessary reagentbottles, connectorsetc.

Hollow Cathode lamps 16hollow cathode lamps. Onelamp each for the elements:Arsenic, Antimony, Boron,

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Sl.No Item Specifications PleaseSpecify

whether thequotedmodel

meets thespecification

(Yes/No)

Name ofthe Model

and itsSpecificati

on

Calcium, Chromium, Cobalt,Copper, Iron, 19 Nickel,Lead, Manganese, Mercury,Selenium, Tin, Vanadiumand Zinc. Equivalent codedlamps will also beacceptable.

Air Compressor with Air Filteror equivalent Air Service UnitComplete with pressureregulator quite in operation,necessary tubing andconnectors and should meetthe air supply requirementsof AAS operation. Oil FreePump Oil- free pump andmoisture trap CorrosionResistant Resistant to acidicvapour and the drain value (ifany) should be made ofstainless steel of equivalentcorrosion resistant material

Gas Regulators Nitrous –oxide gas regulator NitrousOxide Gas regulator (twostage) with heater, withnecessary tubings andconnectors. Necessarytransformer should beprovided to transform thissupply to the requirements ofthe heater. The heatershould work on 230±10volts50 Hz AC power supply.Acetylene Gas regulatorAcetylene gas regulator (twostage) with necessary tubingand connectors. NitrogenGas regulator Nitrogenregulator (two stage) withnecessary tunings andconnectors.

Graphite Furnace System: Graphite Tube: Atomizer

Should be computercontrolled fully enclosed

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graphite tube systemconsisting of stabilizedtemperature / total pyrolyticgraphite plate form.

Gas Supplies: Provision oftwo gas supplies(programme selectable) withindependent control over thegas supply through thefurnace.

Heating Rate: Heating rate ofat least 2000°C per secondCooling Time

Cooling time: 20 seconds Temperature Range:

Temperature range ambientto 2600°C or more in 1°Cincrements Feed backsystem

Feed back system forfurnace temperature control,interlocks for water, gas,temperature, furnace door,graphite tube damage andmains power.

Temp. Programming: Atleast eight steps temperatureprogramming facility withflexibility of programmeselection, ramp time, gases,gas flow and read trigger for20 each temperature step.

Control: Computer controlledwith appropriate provision forprint out of the furnace andsample parameters

Display: Calibration data /graphs, temperature profiles,signal graphics and theinstrument status.

Memory: Memory should beable to store at least ten nonvolatile programmes

Ciller / Cooling Water Re-circulation Unit: Refrigeratingwater circulation unit of

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appropriate capacity. Nodischarge of water from thiswater circulation unit.

DATA WORK STATION Application Software:

Programme facilitywith multitaskingsoftware

Should providecomplete control ofinstrument withinstrument statusdisplay and its variousaccessories.

Provide accurate andreproducible timeaveraged, integration,non – averagedintegration, multi levelcalibration.

Software shouldhandle instrumentlinear absorbancereading,concentration, oremission intensity,integration time, built-in statistics,calibration equationcontrol, slope ofanalytical curve usingoperator selectivecalibration standard

Built-in interface forcomputer connectionand use of optionalaccessories.

Comprehensivequality controlprotocols facilityincluding blank,multiple quality controlstandards, QA/QCaudit trail andcalibration failure.

Computer System:

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Make: Reputed brandsuch asHP/Compaq/IBM/ Dell

Processor: Intel core2 duo processor 3.00GHz or above

RAM: 4 GB (upgradable up to 8GB) HDD 500 GBultra DMA or higherHDD ( 7200 RMP)

Monitor: 21” TFT –LCD Flat Colour

CD ROM: 52X CD-ROM

DVD-CDRW: 32XDVD-ROM andCDRW – combo DriveMax speed 48x24x48

Ports: 2 serial, 1parallel and 2 USBfront 6 rear USB2PS/2 Port, 1 VGAintegrated Port 1linein/out port

Key Board: 104 keys Mouse: Optical

mouse with pad Ethernet: 32 bit auto

selectable 10/100MBPS

Graphics: Internetready with integratedgraphics

Sound: Integratedsound card and inbuiltstereo speakers

Printer HP LaserjetPrinter 1200 x 1200dpi 12 PPM black

Operation Software: Preloaded Windows

XP Professionaloperating system withLicensed CD

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MS Office 2000Standard with media,manual and LicensedCD

Preloaded Antiviruswith latest versionalong with LicensedCD

ADDITIONAL ITEMS Operation Kit: Manufacturers

Standard Operation Kitincluding all required items,tubings, fittings for start up /regular operation ofinstrument.

Operation / maintenance:Manual Operation /maintenance Manual foreach unit Analytical manual

Analytical manual: includingapplications for flame, VGAand graphite system ServiceManual

Service manual: with one setof required tools for eachsystem / unit

Trouble Shooting Charts,Spare parts Catalogue,Application Notes for tracemetal analysis in food andwater samples

Dust Cover One for each unit Consumables: For three

years operation for each ofthe following units: FlameAAS ( basic unit, burnersystem) Vapour generationassembly Graphite FurnaceAtomizer Auto sampler

Operation and MaintenanceTraining: Two weeks trainingto be provided to twoscientist on software training,operation, maintenance andtroubleshooting aspects ofinstrument.

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General Conditions of Supply The instrument and all its

units should operate on 230±10 volts 50Hz power supply

All the operation andmaintenance manuals,circuit diagrams, applicationnotes and applicationsoftwares to be suppliedshould be in EnglishLanguage.

The supplier / manufacturershould have Indian Agent toprovide after sales service.

The main unit and all the subunits of the instrument shouldbe serviced by the Indianrepresentative of supplier.

The Bidder should be amanufacturer / authorizedrepresentative of amanufacturer, who musthave designed,manufactured, tested andsupplied two numbers ofsuch equipment similar to thetype specified in the past fiveyears, which shall be insuccessful operation for atleast 2 years as on the dateof bid opening.

The bidder should furnish theinformation on past suppliesand their satisfactoryperformance.

Bidders shall invariablyfurnish documentaryevidence (client’s certificate– at least two) in support ofthe satisfactory operation ofthe equipment as specifiedabove.

Notwithstanding anythingstated above the purchaserreserves the right to assessthe capability and capacity of

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the bidder to perform thecontract, should thecircumstances warrant suchan assessment in the overallinterest of the purchaser.

Comprehensive warrantywith spares for five yearsfrom the date of installation ofthe instrument should becovered.

2. LOVIBONDTINTOMETER

Measuring principle: Visual, in termsof Lovibond® units

Modes: Transmittance, reflectanceRange 0.1 - 79.9 Red, Yellow; 0.1 -49.9 Blue; 0.1 - 3.9 Neutral

Resolution: 0.1 Lovibond® unit Optical system: 11 glass-filled nylon

racks containing a graduated rangeofLovibond® colour glasses

Viewing system Fully adjustable,prismatic with integral blue filter forlightstandardization

Light source 2 x 12 Volt, 10 Watttungsten halogen lamp Illuminantapproximates to daylight

Path length Up to 153 mm (6”) Power pack 12 Volt ac, switchable

to suit 220/110 Volt supplyApprovals CEInstrument housing Fabricatedsheet steel with a tough, texturedpaint finish

Conformance filters and certifiedcolour reference solutionsrepresenting a range of Lovibond®colours, for quick and simple qualitycontrol checks on instruments andoperators.

Certifications: Product certification: CE / US

FDA / BIS certified. Quality Certification: ISO

certified.

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Should provide calibrationcertificates from NISTtraceable agencies duringwarranty & CMC period.Calibration cost will have tobe borne by the supplier.

DQ, IQ, OQ, PQ Documentationduring installation.

For validation vender should havingit own capability with their owncompany trained service engineerto perform validation. No third partvalidation will be entertained. Onevalidation at the time of installationshould be done by companypersonnel.

Warranty: Comprehensive warrantywith spares for five years from thedate of installation of the instrumentshould be covered.

3. FLAMEPHOTOMETER

Range Na+: 0 to 199.9 ppm, K+: 0to 9.99 ppm, Li+: 0 to 9.99 ppm

Sensitivity 0.1 ppm Na+; K=100units

Specificity less than 0.5%interference when concentrationsare equal to test sampleconcentrations

Reproducibility less than 0.5% C.V. Linearity less than 1% Display dual display; 3-1/2-digit

LED, 12.5 mm (1/2") Fuel supply high-grade

propane/butane mixture regulatedat approximately 30 psi

Air supply 6 liters/min at 12 psi; oiland moisture free

Recorder output 0.05 to 5 V(switchable)

Certifications: Product certification: CE / US

FDA / BIS certified. Quality Certification: ISO

certified.

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Should provide calibrationcertificates from NABLaccredited agency everyyear during warranty & CMCperiod. Calibration cost willhave to be borne by thesupplier.

Equipment should be FDA / CEcertified or equivalent standard ofrepute. It should be ISO 9001:2000or other equivalent qualitycertification.

All electrical peripherals required forsmooth functioning e.g. voltagestabilizer should be provided withthe equipment.

Warranty: Comprehensive warrantywith spares for five years from thedate of installation of the instrumentshould be covered.

4. MUFFLE FURNACE 1200 degree with 23 liter capacity ormore

Double Shell case, Stainless Steel High Purity insulation material with

efficient low thermal insulation Bench top model Vertically lift break switch/side lift

break with front loading Door: positive break switch Inside Chamber Size: 245-280 mm x 340-

400 mm x 230-250 mm (WDH) Maximum temperature: 1200 oC

Standard continuous temperature1050 oC or more

Heating Rate: The furnace shouldbe fast heating type with maximumattainable temperature shouldreach in 110 mins or better

Temperature control: Should bemicroprocessor based & at least 8segment programmable 3216P1 orequivalent controller with necessarysafety features. ProgrammableTemperature controller with heating

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rate control from 10 deg. min-1 to100 deg.min-1 preferable

Temperature Accuracy: ± 5 oC overthe whole temperature range ofoperation and in the entire muffle

Safety: Over Temperatureprotection should be added

Gas purging: Gas purging facility(inert gas inlet and outlet)

Weight : less than 80 kg The furnace should be CE certified

with suitable power supply Installation, training and

commissioning: Vendor mustensure satisfactory installation andcommissioning of the system atCFL, Kolkata. A detailed training onhandling, operation andapplications must be provided to atleast 5 scientists. Installationservices must include IQ/OQ/PQ

For validation vender should haveits own capability with their owncompany trained service engineerto perform validation. No third partvalidation will be entertained. Onevalidation at the time of installationshould be done by companypersonnel.

Warranty: Comprehensive warrantywith spares for five years from thedate of installation of the instrumentshould be covered.

5. GASCHROMATOGRAPHY WITH FIDAND ECDDETECTORS

Pesticides residues and other Food& Water related applications as perFSSAI requirements

Gas chromatograph with capabilityof operating concurrently with twoinjectors or better and threedetectors. The system should bequoted with all accessories requiredto make it fully operational and anyother item required for statedapplications be quoted as optional.

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Oven Upto 450 oC, Fast Oven with 120oC/min ramp, ≥20≥7ramps

Cool-down time from 450 oC to50oC within 5 minutes

Should be able to accommodatetwo or more injectors and threedetectors

Automatic leak test of systemthrough single key

Pneumatic Controls 0-140 psi or better, all ElectronicPneumatic Controls with 0.1 psiprecision

Injector ( 2 or more) Should be capable of large volumeinjection Temperature rampedsplitless, Split and Cold on-columnmodes ≥450 OC max. and ≥10 ramps.

Multimode/PTV with 250µL or betterInjection Volume capability withcomplete solvent vaporizer system orEquivalent.

Injector must be able to operate withcapillary & wide bore columns

Injector must be provided withBackflush system.

Autosampler (Liquid andHeadspace)

Robust Liquid autosampler capable ofinjecting ≥100 samples or better withsyringe capacity of 0.5-100 µl

The type and volume of the syringemust be automatically detected bythe system.

Must allow installation andautomation of syringe featuringvolumes from 0.5 to 100 µl.

Must be able to achieve combinedmultiple solvent rinsing with upto 4different solvents.

Head space auto sampler with acapacity ≥50 vials or better that support10 & 20ml vial capacity with Pnuematiccontrol Incubation Oven Temperature Range

50 to 200 °C in 1 °C steps Syringe Temperature 50 °C to 150

°C in 1 °C steps

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Incubation Oven Capacity vials orbetter

Detectors The GC must have completeintegrated control of all parameters(no external control module) for thefollowing detectors: FID, and ECD.

Detector must be independentlycontrolled and operational formaximum sensitivity

Flame IonizationDetector (FID

Linear range : better than 107

Minimum detectable amount withmakeup gases : 1.5 pgC/sec

Operating temperature limits: 450oCwith standard ceramic/quartz flamejet

Auto flame out detection. Acquisition rate 50 Hz or more.

Electron CaptureDetector ECD

Linear dynamic range : better than 104

Complete with 63Ni source and lowvoltage heaters.

Minimum detectable amount: Lessthan 10 fg of lindane.

Operating temperature limits : 400oCGas Supplies Required High purity Gas cylinders (2

No. Each)SOFTWARE AND HARDWARE ( Single point control ofSoftware & Hardware)Software Complete system and software

configuration must be 21 CFR Part 11compliant. Software: Windows Basedsoftware with multitasking and capable ofperforming the following functions:Control the MS, acquire, store, processand reproduce the data. It must be ableto control all the devices from samesoftware. Software should allowmonitoring of one molecular ion and uptofour confirmatory ions. Quantificationsoftware for batch process must confirmthe analytes as per regulatoryrequirements in food and environmentalsample analysis as per the applicationsspecified.All Flow Controller i.e. Carrier

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flow, Make-up flow, Hydrogen flow, Airflow etc. value should set throughSoftware by PC.Head Space AutoSampler, Automation and event controlfrom PC through same software.IQOQ ofthe system as well as software must beprovided. Software update upto fiveyears

CommunicationHardware:

Latest Factory set, branded system with22-23” Full HD Monitor with Printer - B/W- duplex - laser - Legal, A4 - 1200 dpi x1200 dpi - up to 21 ppm – capacity withNetwork Card and Bluetooth facility.

IQOQPQ IQOQPQ of instrument and Softwareshould be provided along with document.

Training Technical and application training to thepersonnel at site immediately afterinstallation as per terms & conditions oftender.

Application Support The Application support for statedapplications required during methoddevelopment and validations.

Pre InstallationRequirements (PIR)

Provide PIR of the system.

OTHER REQUISITES FOR GC WITH ECD, FIDAutomatic Change Over Manifold for each gas lineComplete Gas Purification Panel with fittings & installation of allgasesRenewable In Line Gas Purification SystemRenewable gas purifier cartridge, Spare SetGas clean filters/Traps (6 No.)Septa for injectors Non stick, Low bleed, high puncture

tolerance and Max. Temp 400 oC (foreach injector). (400 No.)

Liners Suitable Ultra Inert Injector Liner forSS & SSL (20 No.)

Suitable Injector Liner upto 10 µL (6No.)

Suitable Injector Liner upto 250 µL(6 No.)

Suitable Injector Liner upto 500 µL(6 No.)

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Liner O-Rings Max Temp 375 oC(100 No.)

Liners types required as per theapplication

Ferrules and Nuts 50 No. (for each column end and otherinterfaces as applicable), 50 No. for GCwith ECD, NPD, FID

Columns for GCApplications

Pesticide column (30m x 0.250mm x0.25µm (HP-5MS / DB-1MS orequivalent) (02 no.)

Column for Fatty Acid Profiling withmain concern of Trans Fatty AcidApplication (02 No.)

Column for Cholesterol Application(02 No.)

Vials, caps and toolfor autosampler(Only Compatiblesizes should besupplied)

2000 No. each Vial sets (1, 2 mL,Crimp type, Amber and Clear glass)

200 No. Vials (10,20ml Crimp typewith cap & septa)

1000 No. 300/500 µL Recovery vials 6000 No. Septa PTFE/Silicone (for

1, 2 mL Vials) 6000 No. Septa PTFE/Silicone (for

10, 20 mL Headspace Vials) Ergonomic Crimping Tools for

different vial types Ergonomic Decapping Tools for

different vial types 10 No. each Storage Racks for (for

1, 2 mL Vials) Head Space vials 10,20 ml capacity

(500no. each)Autosampler Syringe 10 µL (12 No.), 100 and 250 µL (04 No.

each); Manual syringe-2µl, 5µl and 500µl (04 No. each).Headspace syringe (02 no.10µl,500µl,02 no. 1ml)

Sample Preparation(Water & Food)

QuEChERS Kits for Pesticides andHerbicides in following Matrices:

Water (1000 No.) Matrices with high fat (1000 No.) Matrices with high Water content

and (1000 No.)

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Matrices with high pigmented(1000 No.)

Tools and Kits Septa Removing toolTubing Cutter with rotating diamondblade for columnTubing Cutter for stainless steel tubing(1/16 & 1/8 inch tubing)Tubing Cutter for Plastic tubing withspare blade set

Miscellaneous Consumables required for each detectormust be provided

Warranty Comprehensive warranty with spares forfive years from the date of installation ofthe instrument should be covered.

6. GASCHROMATOGRAPHY WITH NPDAND THERMALCONDUCTIVITIYDETECTOR(TCD)DETECTORS

Pesticides residues and other Food& Water related applications as perFSSAI requirements

Gas chromatograph with capabilityof operating concurrently with twoinjectors or better and threedetectors. The system should bequoted with all accessoriesrequired to make it fully operationaland any other item required forstated applications be quoted asoptional.

Oven Upto 450 oC, Fast Oven with 120oC/min ramp, ≥20≥7ramps

Cool-down time from 450 oC to50oC within 5 minutes

Should be able to accommodatetwo or more injectors and threedetectors

Automatic leak test of systemthrough single key

Pneumatic Controls 0-140 psi or better, all ElectronicPneumatic Controls with 0.1 psiprecision

Injector ( 2 or more) Should be capable of large volumeinjection Temperature ramped split-less, Split and Cold on-column modes≥450 OC max and ≥10 ramps.

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Multimode/PTV with 250µL or betterInjection Volume capability withcomplete solvent vaporizer system orEquivalent.

Injector must be able to operate withcapillary & wide bore columns

Injector must be provided withBackflush system.

Autosampler Robust Liquid autosampler capable ofinjecting ≥100 samples or better withsyringe capacity of 0.5-100 µl

The type and volume of the syringemust be automatically detected bythe system.

Must allow installation andautomation of syringe featuringvolumes from 0.5 to 100 µl.

Must be able to achieve combinedmultiple solvent rinsing with upto 4different solvents.

Detectors The GC must have completeintegrated control of all parameters(no external control module) for thefollowing detectors: NPD, and TCD.

Detector must be independentlycontrolled and operational formaximum sensitivity

Nitrogen PhosphorusDetector (NPD)

Minimum detectable amount: 100fgN/sec, 100fg P/sec

Linear dynamic range: better than 104

Operating temperature limits: 450 Cwith standard jet

Thermal ConductivityDetector TCD

Capillary-column compatible Proven constant current design Software protection to prevent filament

burnout Ideal for series operation 1/8-in. fittings PPC pneumatics - software flow

control of reference gas Operating temperature 100 ˚C to 350

˚C in 1 ˚C increments

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Sensitivity 9 µV/ppmnonane at 160mA at the bridge with a detectortemperature of 100 ˚C or 100pgtridecane, /mL with He

Minimum detectable quantityTypically < 1 ppm nonane

Linear dynamic range: better than 105

+/- 5% Operating temperature limits: 400 C

Gas Supplies Required High purity Gas cylinders (2No. Each)

SOFTWARE AND HARDWARE ( Single point control ofSoftware & Hardware)Software Complete system and software

configuration must be 21 CFR Part 11compliant. Software: Windows Basedsoftware with multitasking and capable ofperforming the following functions:Control the MS, acquire, store, processand reproduce the data. It must be ableto control all the devices from samesoftware. Software should allowmonitoring of one molecular ion and uptofour confirmatory ions. Quantificationsoftware for batch process must confirmthe analytes as per regulatoryrequirements in food and environmentalsample analysis as per the applicationsspecified.All Flow Controller i.e. Carrierflow, Make-up flow, Hydrogen flow, Airflow etc. value should set throughSoftware by PC.Head Space AutoSampler, Automation and event controlfrom PC through same software.IQOQ ofthe system as well as software must beprovided.Software update upto five years

CommunicationHardware:

Latest Factory set, branded system with22-23” Full HD Monitor with Printer - B/W- duplex - laser - Legal, A4 - 1200 dpi x1200 dpi - up to 21 ppm – capacity withNetwork Card and Bluetooth facility.

IQOQPQ IQOQPQ of instrument and Softwareshould be provided along with document.

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Training Technical and application training to thepersonnel at site immediately afterinstallation as per terms & conditions oftender.

Application Support The Application support for statedapplications required during methoddevelopment and validations.

Pre InstallationRequirements (PIR)

Provide PIR of the system.

OTHER REQUISITES FOR GC WITH NPD, TCDAutomatic Change Over Manifold for each gas lineComplete Gas Purification Panel with fittings & installation of allgasesRenewable In Line Gas Purification SystemRenewable gas purifier cartridge, Spare SetGas clean filters/Traps (6 No.)Septa for injectors Non stick, Low bleed, high puncture

tolerance and Max. Temp 400 oC (foreach injector). (400 No.)

Liners Suitable Ultra Inert Injector Liner forSS & SSL (20 No.)

Suitable Injector Liner upto 10 µL (6No.)

Suitable Injector Liner upto 250 µL (6No.)

Suitable Injector Liner upto 500 µL (6No.)

Liner O-Rings Max Temp 375 oC(100 No.)

Liners types required as per theapplication

Ferrules and Nuts 50 No. (for each column end and otherinterfaces as applicable), 50 No. for GCwith ECD, NPD, FID

Columns for GCApplications

Pesticide column (30m x 0.250mm x0.25µm (HP-5MS / DB-1MS orequivalent) (02 no.)

Column for Fatty Acid Profiling withmain concern of Trans Fatty AcidApplication (02 No.)

Column for Cholesterol Application(02 No.)

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Vials, caps and toolfor autosampler(Only Compatiblesizes should besupplied)

2000 No. each Vial sets (1, 2 mL,Crimp type, Amber and Clear glass )

200 No. Vials (10,20ml Crimp typewith cap & septa)

1000 No. 300/500 µL Recovery vials 6000 No. Septa PTFE/Silicone (for

1, 2 mL Vials) Ergonomic Crimping Tools for

different vial types Ergonomic Decapping Tools for

different vial types 10 No. each Storage Racks for (for

1, 2 mL Vials)Autosampler Syringe 10 µL (12 No.), 100 and 250 µL (04 No.

each); Manual syringe-2µl, 5µl and 500µl (04 No. each).

Sample Preparation(Water & Food)

QuEChERS Kits for Pesticides andHerbicides in following Matrices:

Water (1000 No.) Matrices with high fat (1000 No.) Matrices with high Water content

and (1000 No.) Matrices with high pigmented

(1000 No.)Tools and Kits Septa Removing tool

Tubing Cutter with rotating diamondblade for columnTubing Cutter for stainless steel tubing(1/16 & 1/8 inch tubing)Tubing Cutter for Plastic tubing withspare blade set

Miscellaneous Consumables required for each detectormust be provided

Warranty Comprehensive warranty with spares forfive years from the date of installation ofthe instrument should be covered.

7. MICROWAVEDIGESTIONSYSTEM

A latest model of microwave digestionsystem should enable rapid digestion fordifferent inorganic/organic samples like;Different types of FSSAI food and foodproducts, Fish and Fishery products, tea,seasoning powder, biscuits etc.

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Application A latest model of microwave digestionsystem should enable rapid digestion fordifferent inorganic/organic samples like;Different types of FSSAI food and foodproducts, Fish and Fishery products, tea,seasoning powder, biscuits etc

General The instrument should have a superiorpressure venting so as to prevent anyloss of volatile metals and should havehomogeneous microwave field to avoidsample burning

System Microwave digestion system shouldhave temperature and pressurecontrolling/monitoring system. Thesystem should be software controlled.Different types of rotors available for thedigestion of the different type samplesshould also be quoted. Necessaryconsumables and maintenance partsshould also be quoted to run instrumenttrouble free

Instrument The system should be a stand alonework station and should have The System should have the feature

of simply choose a method and itautomatically recognizes the vesseltype, counts the vessels anddetermines all of the parametersnecessary for a fast, completedigestion

Should have provision that user canset the desired parameters fordigestion

Should have Automatic Microwavepower application depending on theload

Auto sensing of temperature andpressure inside the vessel

Be capable of processing differentamounts of samples (from 0.3 g upto 10g) in the same run assuring thesame conditions of temperature andpressure

Display The Instrument should have the high-resolution, colour touch screen, acid

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and itsSpecificati

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resistant, LED/LCD screen should serveas controller and display. Should beprovided training videos for samplepreparation vessel assembly, systemuse, and maintenance. Should haveData management – Easy access tostored methods, real-time data andresults of past runs. Should be able todisplay the detailed methods, graphs o ftemperature and power against time andtemperature of individual vessels.

Interlocks The system should have goodinterlocking system for safety and cavitydoor.

Vessel The system should be high throughputwhich can hold atleast 24 high pressurevessels. Must be supplied with digestionvessel racks and suitably handledifferent digestion volumes.

System The material of construction should behigh purity TFM fluropolymer. Vesselshould be capable of hanlding volumesbetween 10 ml and > 25 ml, if required.It should be operated for maximumtemperature capacity of 250ºC or moreand maximum pressure of 35 Bar ormore. The system should be providedwith temperature sensor (Thermocoupletype/ Fiber optics/IR Sensor) which willmeasure real temperature of the vesselsand control it. The vessels should haveautomatic venting and re-sealing systemin case there is excess pressuredevelopment essential. After Digestion,vessels must be vent-able beforeuncapping the vessel for safety reasons.For ease of use, the vessels must notrequire the use of an energizing tool inorder to reform seals prior to operation.Additional twelve numbers of vesselsshould be supplied along with thesystem.

MicrowavePower and output

The Instrument should have single/dualmagnetron 1500 W (or more of deliveredenergy, should provide the temperature

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with uniform energydistribution

needed (300 °C) for difficult samplesand high-throughput vessel setsdelivering unpulsed continuous power &precisely tuned wave guide. Dispersesmicrowave energy uniformly throughoutthe cavity. No need for motor drivendiffusers or attenuators. Systemsoftware must automatically adjust thepower delivery based upon sample loadand pre-programmed control settings.Automatic Power control Technologydelivers maximum energy to the sample,ensuring complete digestions.Controllable via microprocessor 230 Vinput, pulsed and unpulsed-essential 50Hz, AC Operated. The Instrumentshould have “waveguide” between themagnetron (the microwave energysource) and the cavity. This waveguidefed system should provide maximumtuned transfer of microwave energy fromthe magnetron to the load in themicrowave cavity. planes. This shouldresult in uniform heating of the sampleload.

Microwave Cavity The microwave cavity should be heavyduty and have sufficient space to mountand dismount vessels individually and allparts inside the cavity should be totallymicrowave transparent. The Cavityshould be constructed with non magneticRugged high-grade 316 solid steelcavity. The vessel assembly during a runshould be visible from outside Thecoating inside the cavity should be acid/chemical. resistant special polymercoating like fluro-polymer / PTFE.

Controls The Instrument should have a) ReliableTemperature and b) Pressure controlsindependent of each other

Automatic temperature controlsystem, temperature sensorshould be protected properly fromany chemical attack, sensorshould monitor and control allvessels simultaneously-essential

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Automatic Pressure control:should have a pressure sensorwhich has a total capability of upto 500psi automatically control thepressure. It should be possible toremove the pressure device at ahigh pressure. The Vesselsshould act as self-regulators ofpressure

Control The control terminal should have highresolution LED/LCD Acid Resistantdisplay. Touch screen which shouldhave method storage capacity. All thefeatures should be in built in thesoftware. Should have provision formanual programming storage apartfrom pre-installed programme.Continuous display of temperature andpower inside the reaction vessels isrequired.

Safety There has to be multiple levels of safety.A safe mechanism to tackle the unusedor reflected microwave energy Capableof shutting off in the event of the A veryloud noise or bang in the instrument. Ifthe temperature of the vessel is near itshighest tolerance limit. Have inbuiltexhaust system to cool the vessels andto drive away if any fumes in the cavity-essential

Quality Standards The manufacturer should be ISO 9001certified for design and manufacture ofmicrowave digestion system

Certification requiredfor sign off

IQ/OQ compliance Calibration certificates for titrator GLP-validated software for

controlling the system

Operation andmaintenancetraining component

The supplier will have to carry outsuccessful installation at our laboratorypremises (where ever the system has tobe installed) and provide on – sitecomprehensive training for scientificpersonnel operating the system and

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support services till customersatisfaction with the system.

Warranty Comprehensive warranty with spares forfive years from the date of installation ofthe instrument should be covered. Thiswill include yearly calibration start-up /commissioning routine servicing, regularmaintenance, preventive maintenanceof equipment and components andbreak down repairs as and whenoccurring, ensuring that system does notremain out of service for a period morethan 24 hours in case of majorbreakdowns and 6-8 hour in the case ofminor breakdowns due to anyunforeseen break down. The institutionwill provide Water / Electricity power,etc. for maintenance work. Thesuccessful tenderer shall keep theessential spares at site during theContract Period to avoid the delay inattending faults / maintenance.

Service contractclauses, includingprices

List of all spares and accessories(including minor) with part numbers andprice, required for maintenance andrepairs in future afterguarantee/warranty period should beattached.

Operating manuals,service manuals,other manuals

Should provide 2 sets (hardcopy andsoft-copy) of:- User, technical and maintenance

manuals to be supplied in Englishlanguage along with machinediagrams;

List of equipment and proceduresrequired for local calibration androutine maintenance;

Service and operation manuals(original and copy) to be provided;

Advanced maintenance tasksdocumentation;

Certificate of calibration andinspection

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Sl.No Item Specifications PleaseSpecify

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CertificatesPerformance andsafety standards(specific to the devicetype);Local and/orinternational

Should be FDA/CE/BIS approvedproduct.

Manufacturer and Supplier shouldhave ISO 13485 certificationunder ISO 9001for qualitystandards.

Electrical safety conforms to thestandards for electrical safety IEC60601- General requirements (orequivalent BIS Standard)

Certified to be compliant with IEC61010-1, IEC 61010-2-40 forsafety

Supplier/Manufacturer

Must be ISO certified for quality

Service SupportContact details(Hierarchy Wise;including a tollfree/landline number)

Contact details of manufacturer,supplier and local service agent tobe provided; Any Contract(AMC/CMC/adhoc) to be declaredby the manufacturer;

Recommendations orwarnings

Any warning signs would beadequately displayed

8. DIGITAL BUTRYOREFRACTOMETER

For checking purity and adulteration offats and oils

System Automated Operating LCD screendirectly without manual alignment, canconnect PC with RS232 interface

Display The required data to be displayed on thescreen, including: the date, temperature,refractive index, concentration, andamended in accordance with the currenttemperature

Measurement Range(AutomaticTemperatureControlled)

Concentration 0;95% Refractive Index 1.32422-1.7000

Minimum Indication Butyro 0.1%RI 0.00001

MeasurementAccuracy

Butyro ±0.5% (at 40˚C)RI ±0.0003 (at 40˚C)

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Precision(Reproducibilty

RI ± 0.00005Butyro ± 0.05

MeasurementTemperature

10 to 50˚C

Ambient TemperatureSample

10 to 40˚C

Volume MeasurementTime

Less than 5 sec

Sample Volume > 0.1 mlCalibration certificateAccessories Reference Material Oil minimum 10 mlOperation andtraining component

The supplier will have to carry outsuccessful Installation at the laboratorypremises (where ever the system hasto be installed) and provide on – sitecomprehensive training for a minimumof two scientific personnel operatingthe system till customer satisfaction

CertificatesPerformance andsafety standards(specific to the devicetype);Local and/orinternational

Should be FDA/CE/BIS approvedproduct.

Manufacturer and Supplier shouldhave ISO 13485 certification underISO 9001for quality standards.

Electrical safety conforms to thestandards for electrical safety IEC60601- General requirements(orequivalent BIS Standard)

Certified to be compliant with IEC61010-1, IEC 61010-2-40 for safety

Supplier/Manufacturer

Must be ISO certified for quality

Service SupportContact details(Hierarchy Wise;including a tollfree/landline number)

Contact details of manufacturer,supplier and local service agent to beprovided; Any Contract(AMC/CMC/adhoc) to be declared bythe manufacturer;

Recommendations orwarnings

Any warning signs would beadequately displayed

Warranty Comprehensive warranty with sparesfor five years from the date ofinstallation of the instrument shouldbe covered.

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Service contractclauses, includingprices

List of all spares and accessories(including minor) with part numbersand price, required for maintenanceand repairs in future afterguarantee/warranty period should beattached;

Operating manuals,service manuals,other manuals

Should provide 2 sets(hardcopy andsoft-copy) of:- User, technical and maintenance

manuals to be supplied in Englishlanguage along with machinediagrams;

List of equipment and proceduresrequired for local calibration androutine maintenance;

Service and operation manuals(original and copy) to be provided;

Advanced maintenance tasksdocumentation;

Certificate of calibration andinspection

9. Flash pointapparatus

Instrument designed in strictaccordance with the test methodASTM D93, Method A and B.

Microprocessor controlled unit withdigital easy to read display of theresults.

Ignition :-Electric ignition and shouldalso provide an automatic reignitionfacility.

Thermal detection (with metalsample temperature probe) of theflash to eliminate interference fromwater or silicone containingcompound.

Cooling : - Facility for built-in coolingconnection.

Automatic correction for standardbarometric pressure vis-à-vis withfinal result.

Unit should have diagnosticprogram to check every keycomponent and assembly andcalibration facility.

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Unit should automatically determineflash point in strict compliance withthe appropriate test method.

Heating should be microprocessorcontrolled at the specified rate; theignitor is activated and dipped atprecisely the correct temperatureand frequency.

Safety device for fire protection withalarm.

Resistance check box fortemperature calibration withcalibration certificate.

The unit should be operable on 230v/ 50 Hz.

The system should be ISO 9001quality standard and supplied withoperation manual.

Merely copying our specifications inthe quotation shall not make theparties eligible for consideration ofthe quotation. A quotation has to besupported with the printed technicalleaflet/literature of the quoted modelof the item by the quotingparty/manufacturer and thespecifications mentioned in thequotation must bereflected/supported by the printedtechnical leaflet/literature.

Calibration : The firm must ensurethat the equipment supplied is fullycalibrated as per specificationrequirements and also source offuture calibration at New Delhi &their frequency of calibration needed

Spares : Vendor should quoterecommended spares for two yearsalongwith the equipment for smoothfunctioning of the equipment.

Spare Parts : Availability of spareparts of the equipment/instrumentmust be guaranteed for a period ofat least seven years from the date ofsupply.

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After Sales Services: It should beclearly mentioned in the quotationwhether the after sales servicesduring and after the completion ofwarranty shall be provided directlyby the supplier or their authorizedagent/ representative. Terms of theafter sales services, if any, may bementioned in the offer. However, inboth the cases the original suppliershall be responsible for poorperformance/services.

Inspection: The inspection of thesystem will be done by our technicalexpert in the presence of firmrepresentative.

Users List : The list of usersspecifically for the samemodel/make of the quoted item ( notthe list of general users) along withthe complete name, address &contract numbers of the userorganizations/persons may besubmitted with the quotation alongwith the performance certificatesfrom all/some of them.

Training: Our Scientist/Technicalpersons should be trained by thesupplier at the project site free ofcost. NOTE:- Firms havingequipment wherein single motherunit can be used for carrying outFlash Point by Abel Flash Pointusing interchangeable analyzer unitshall be considered, if otherwisefound suitable vis-à-vis price factor& performance. Other specificationrequirement for Abel Flash Pointapparatus is enclosed.

Certifications: Product certification: CE / US

FDA / BIS certified. Quality Certification: ISO

certified. Should provide calibration

certificates from NIST

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traceable calibrationsolutions by any agencyevery year during warranty &CMC period. Calibration costwill have to be borne by thesupplier.

Comprehensive warranty withspares for five years from the date ofinstallation of the instrument shouldbe covered.

Buy-back price for old AutomatedPensky-Martens closed-cup flashpoint tester with sample changermeasures the flash point of up to 12samples automatically [Make:Petrotest, Germany Model: PMA-4,Year of Installation: 2004] may alsobe quoted.

10. Water Purificationsystem

Table top Water Purification System(Tap Water Feed) should becapable of produce water for use inHPLC solvents, Microbiology andreagent grade with the help of pre-treatment module; RO Module, DIModule, Storage tank, UV OxidationChamber, Polishing module andfinal membrane filter 0.22um

Pre-treatment System Should consists: 5 micron,1 micron and Activated

Carbon wrapped type depth filter Pressure gauge with regulator The unit should have automatic

low/high pressure cut-offReverse Osmosiswith ElectroDeionization Stage:

Pre-treatment cartridge with auto-scaling compounds, 0.5 micron filterand activated carbon or better.

Prefilter combination to protect theRO Membranes life or better.

RO Module with high performancethin film composite membrane withsalt retention rate up to 98%. Theretention rate for dissolved organiccompounds, particles & colloids &bacteria exceeds 99%

Deionization Module: Mixed bed

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resin module utilized for a reductionof the inlet conductivity. Used forinorganic applications.

Conductivity measurement is to bedone after RO, DI & Polishing moduleto monitor the performance ofIndividual cartridge.

Should have suitable back washprogramme before every operationor better

Storage Tank: 30 L or better Storage Tank with UVLamp, Air filter, CO2 Trap & LevelSensor.

The tank should made of pure waterresistant Poly Ethylene material withan outlet to drain the tank totally anda pressure sensor for the tank levelcontrol

The storage tank should be 100%drainable.

General requirements Online UV oxidation chamber: UV LightEnergy at 185 nm & 254 nmwavelengths. TOC Measurement: Online continuous

TOC measurement with Live Display. Sterile Filter with 0.22 µm or better with

Autoclavable option for re-use System should meet reagent water

quality standards including ASTM Type1, CLSI and ISO 3696 Type Ι System should have flexible remote

dispenser to dispense water wheneverneeded System should have built-in automatic

self-cleaning mechanism to extend thelife of cartridge Automatic flushing and recirculation in

standby mode to maintain consistentpeak water purity User can collect RO Quality water from

the Storage tank & ultrapure water fromflexible dispenser Should have cartridge change indicator The system should incorporate a fully

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comprehensive, graphic colour LCDdisplay to provide system status,performance parameters, routinemaintenance status and alarms oftroubleshooting, tank level status andautomatic warning of reordering ofconsumables and Provision for digital display to indicate

status of operation, resistivity orconductivity, temperature and alsoalarm system in case ofmalfunctioning.

Pure WaterSpecification: (Type-2)

Production Rate : 10 LPH or better Conductivity : <2µs/cm at 298K

(25°C) or better pH at 298K (25°C) => 6.6 or

effectively neutral Total silica max 3ug/L or better

The UltrapureProduct Water shouldof the followingspecifications: (Type-1)

Flow Rate : 1.0 L/min or better Should have conductivity @ 25

Deg C : 0.055 µs/cm or better Should have resistivity @ 25 Deg

C : 18.2 MΩ-cm or better TOC : < 1 ppb or better Bacteria : <1 cfu/ml or better Particles >0.1µm : <1 per ml or

better pH at 298K (25°C) = > 6.6 or

Effectively neutralCertification requiredfor sign off

IQ/OQ compliance Calibration certificates for titrator

Operation andmaintenancetraining component

The supplier will have to carry outsuccessful installation at our laboratorypremises (where ever the system hasto be installed) and provide on – sitecomprehensive training for scientificpersonnel operating the system andsupport services till customersatisfaction with the system.

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Warranty Comprehensive warranty with sparesfor five years from the date ofinstallation of the instrument should becovered. This will include yearlycalibration start-up / commissioningroutine servicing, regular maintenance,preventive maintenance of equipmentand components and break downrepairs as and when occurring, ensuringthat system does not remain out ofservice for a period more than 24 hoursin case of major breakdowns and 6-8hour in the case of minor breakdownsdue to any unforeseen break down. Theinstitution will provide Water / Electricitypower, etc. for maintenance work. Thesuccessful tenderer shall keep theessential spares at site during theContract Period to avoid the delay inattending faults / maintenance.

Service contractclauses, includingprices

List of all spares and accessories(including minor) with part numbersand price, required for maintenanceand repairs in future afterguarantee/warranty period should beattached;

Operating manuals,service manuals,other manuals

Should provide 2 sets(hardcopy andsoft-copy) of:- User, technical and maintenance

manuals to be supplied in Englishlanguage along with machinediagrams;

List of equipment and proceduresrequired for local calibration androutine maintenance;

Service and operation manuals(original and copy) to be provided;

Advanced maintenance tasksdocumentation;

Certificate of calibration andinspection

CertificatesPerformance andsafety standards(specific to the device

Should be FDA/CE/BIS approvedproduct.

Manufacturer and Suppliershould have ISO 13485

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type);Local and/orinternational

certification under ISO 9001forquality standards.

Electrical safety conforms to thestandards for electrical safety IEC60601- General requirements (orequivalent BIS Standard)

Certified to be compliant with IEC61010-1, IEC 61010-2-40 forsafety

Supplier/Manufacturer

Must be ISO certified for quality

Service SupportContact details(Hierarchy Wise;including a tollfree/landline number)

Contact details of manufacturer,supplier and local service agent tobe provided; Any Contract(AMC/CMC/adhoc) to be declaredby the manufacturer;

Recommendations orwarnings

Any warning signs would beadequately displayed

Note : List of Installations of the quoted Model or a comparable model of equivalent sensitivitypreferably in food analysis sector in India (Attach Performance certificate from the organizationswhere the quoted model or a comparable model of equivalent sensitivity has already beeninstalled)

(d) Part IV- Special Conditions of RFP is revised as under:

14 (b) Response time: The response time of the Seller should not exceed 72hours from the time the breakdown intimation is provided by the Buyer.

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(e) Part V- Evaluation Criteria and Price Bid issue is revised as under:

2. Revised Price Bid Format :The Revised Price Bid Format is given below and Biddersare required to fill this up correctly with full details, as required under Part-II of RFP :-

(a) Basic cost of the item/items:

Cost Details

Sl.No Item Specifications Price in INR

1. ATOMICABSORPTIONSPECTROPHOTMETER[GTA /FLAME/ VGA]

Atomic Absorption Spectrophotometer(GTA/FLAME/VGA), Computer Controlled withbuilt-in flame emission mode, Unit for Flame(Air Acetylene and nitrous oxide- acetylene),Graphite Tube Atomizer (GTA), Chiller / Watercirculating unit, Auto samplers for GTA andflame

Wave length range 190 – 800 nm wave length Sensitivity at least 0.9 abs for 5µg/ml aqueous

copper standard solution with air – acetyleneflame

Optics: Double Beam dual blazed / holographicCzerny turner Monochromator

Focal length At least 250 mm focallength

Resolution 1800 lines / mm Width Automatic bandwidth of 0.2 to 1.0

nm Flame Atomizer: All titanium or equivalent

burner with impact bead / Flow spoiler, premixDesign

Movement Automatic movement into thesample compartment

Affect from Acids /Organic solventUnaffected from attacks by acid solutionor organic solvents (e.g. Methyl isobutylKetone i.e. MIBK

Flame Alignment in liquid beam Fullyautomatic, optimized with motorizedburner mount for vertical and horizontalburner adjustment

Nebulizer High precision able to providemanually adjustable uptake ratesmaterial of the nebulizer and relatedVenturi should be inert to acid solutionsand organic solvents such as MIBK

Flame Control Computer controlled ignition Gas Control Computer controlled with oxidant

and fuel gases monitoring to monitor constantfuel / oxidant ration ignition

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Safety Function Interlocking system to preventignition

Essential Interlock Monitor Burner type as wellas its presence in position, air selector, flamesensor, liquid trap level, gas supply pressureand air supply anywhere in the network of gastubings in the system

Automatic Lamp Selection Function Computercontrolled Hollow Cathode Lamp selection andalignment Lamp Holder At least 8 lamp holderwith built in power supplies for hollow cathodelamps and electrode – less discharge lamps orequivalent Operating Parameter settingAutomatic Setting

Read Out /Display Display facility forabsorbance as well as concentration, Display oferrors or error codes, absorbance range atleast up to 2.0 Abs.

Scale Expansion Scale expansion atleast up to 100x

Integration time Integration time shouldcover at least 0.2 to 50 seconds range

Measurement Measurements of mean,RSD and CV, Background only mode,Integration of peak height and peakareas.

Accessories / Spares with Flame AA System Vapour Generation Assembly: Should

be continuous flow based hydride /mercury vapour generator with option ofusing with or without a programmableauto sampler

Precision Precision of better thanor at least 1% at ppb levels ofmercury, arsenic etc.

Absorption Cell The absorptioncell’s material should have noeffect of the high heat of the flameand the cell for the analysis ofmercury should be of a closed celldesign

Flame Arrester Flame arrestershould be provided in the tubewhich connects the assembly tothe absorption cell

Cell Design holder. The design ofthe cell holder should give a firmand easily adjustable (foralignment) mounting on theburner head.

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System accessories Completewith necessary reagent bottles,connectors etc.

Hollow Cathode lamps 16 hollowcathode lamps. One lamp each for theelements: Arsenic, Antimony, Boron,Calcium, Chromium, Cobalt, Copper,Iron, 19 Nickel, Lead, Manganese,Mercury, Selenium, Tin, Vanadium andZinc. Equivalent coded lamps will alsobe acceptable.

Air Compressor with Air Filter orequivalent Air Service Unit Completewith pressure regulator quite inoperation, necessary tubing andconnectors and should meet the airsupply requirements of AAS operation.Oil Free Pump Oil- free pump andmoisture trap Corrosion ResistantResistant to acidic vapour and the drainvalue (if any) should be made ofstainless steel of equivalent corrosionresistant material

Gas Regulators Nitrous – oxide gasregulator Nitrous Oxide Gas regulator(two stage) with heater, with necessarytubings and connectors. Necessarytransformer should be provided totransform this supply to therequirements of the heater. The heatershould work on 230±10volts 50 Hz ACpower supply. Acetylene Gas regulatorAcetylene gas regulator (two stage) withnecessary tubing and connectors.Nitrogen Gas regulator Nitrogenregulator (two stage) with necessarytunings and connectors.

Graphite Furnace System: Graphite Tube: Atomizer Should be

computer controlled fully enclosedgraphite tube system consisting ofstabilized temperature / total pyrolyticgraphite plate form.

Gas Supplies: Provision of two gassupplies (programme selectable) withindependent control over the gas supplythrough the furnace.

Heating Rate: Heating rate of at least2000°C per second Cooling Time

Cooling time: 20 seconds

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Sl.No Item Specifications Price in INR

Temperature Range: Temperaturerange ambient to 2600°C or more in 1°Cincrements Feed back system

Feed back system for furnacetemperature control, interlocks for water,gas, temperature, furnace door, graphitetube damage and mains power.

Temp. Programming: At least eightsteps temperature programming facilitywith flexibility of programme selection,ramp time, gases, gas flow and readtrigger for 20 each temperature step.

Control: Computer controlled withappropriate provision for print out of thefurnace and sample parameters

Display: Calibration data / graphs,temperature profiles, signal graphicsand the instrument status.

Memory: Memory should be able tostore at least ten non volatileprogrammes

Ciller / Cooling Water Re-circulationUnit: Refrigerating water circulation unitof appropriate capacity. No discharge ofwater from this water circulation unit.

DATA WORK STATION Application Software:

Programme facility withmultitasking software

Should provide complete controlof instrument with instrumentstatus display and its variousaccessories.

Provide accurate andreproducible time averaged,integration, non – averagedintegration, multi level calibration.

Software should handleinstrument linear absorbancereading, concentration, oremission intensity, integrationtime, built-in statistics, calibrationequation control, slope ofanalytical curve using operatorselective calibration standard

Built-in interface for computerconnection and use of optionalaccessories.

Comprehensive quality controlprotocols facility including blank,multiple quality control standards,

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QA/QC audit trail and calibrationfailure.

Computer System: Make: Reputed brand such as

HP/Compaq/IBM/ Dell Processor: Intel core 2 duo

processor 3.00 GHz or above RAM: 4 GB ( upgradable up to 8

GB) HDD 500 GB ultra DMA orhigher HDD ( 7200 RMP)

Monitor: 21” TFT – LCD FlatColour

CD ROM: 52X CD- ROM DVD-CDRW: 32X DVD-ROM and

CDRW – combo Drive Max speed48x24x48

Ports: 2 serial, 1 parallel and 2USB front 6 rear USB2 PS/2 Port,1 VGA integrated Port 1line in/outport

Key Board: 104 keys Mouse: Optical mouse with pad Ethernet: 32 bit auto selectable

10/100 MBPS Graphics: Internet ready with

integrated graphics Sound: Integrated sound card

and inbuilt stereo speakers Printer HP Laserjet Printer 1200 x

1200 dpi 12 PPM black Operation Software:

Preloaded Windows XPProfessional operating systemwith Licensed CD

MS Office 2000 Standard withmedia, manual and Licensed CD

Preloaded Antivirus with latestversion along with Licensed CD

ADDITIONAL ITEMS Operation Kit: Manufacturers Standard

Operation Kit including all requireditems, tubings, fittings for start up /regular operation of instrument.

Operation / maintenance: ManualOperation / maintenance Manual foreach unit Analytical manual

Analytical manual: including applicationsfor flame, VGA and graphite systemService Manual

Service manual: with one set of requiredtools for each system / unit

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Trouble Shooting Charts, Spare partsCatalogue, Application Notes for tracemetal analysis in food and watersamples

Dust Cover One for each unit Consumables: For three years operation

for each of the following units: FlameAAS ( basic unit, burner system) Vapourgeneration assembly Graphite FurnaceAtomizer Auto sampler

Operation and Maintenance Training:Two weeks training to be provided to twoscientist on software training, operation,maintenance and troubleshootingaspects of instrument.

General Conditions of Supply The instrument and all its units should

operate on 230 ±10 volts 50Hz powersupply

All the operation and maintenancemanuals, circuit diagrams, applicationnotes and application softwares to besupplied should be in English Language.

The supplier / manufacturer should haveIndian Agent to provide after salesservice.

The main unit and all the sub units of theinstrument should be serviced by theIndian representative of supplier.

The Bidder should be a manufacturer /authorized representative of amanufacturer, who must have designed,manufactured, tested and supplied twonumbers of such equipment similar tothe type specified in the past five years,which shall be in successful operationfor at least 2 years as on the date of bidopening.

The bidder should furnish theinformation on past supplies and theirsatisfactory performance.

Bidders shall invariably furnishdocumentary evidence (client’scertificate – at least two) in support of thesatisfactory operation of the equipmentas specified above.

Notwithstanding anything stated abovethe purchaser reserves the right toassess the capability and capacity of thebidder to perform the contract, shouldthe circumstances warrant such an

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assessment in the overall interest of thepurchaser.

Comprehensive warranty with spares forfive years from the date of installation ofthe instrument should be covered.

2. LOVIBONDTINTOMETER

Measuring principle: Visual, in terms ofLovibond® units

Modes: Transmittance, reflectance Range 0.1 -79.9 Red, Yellow; 0.1 - 49.9 Blue; 0.1 - 3.9Neutral

Resolution: 0.1 Lovibond® unit Optical system: 11 glass-filled nylon racks

containing a graduated range ofLovibond® colour glasses

Viewing system Fully adjustable, prismatic withintegral blue filter for lightstandardization

Light source 2 x 12 Volt, 10 Watt tungstenhalogen lamp Illuminant approximates todaylight

Path length Up to 153 mm (6”) Power pack 12 Volt ac, switchable to suit

220/110 Volt supply Approvals CEInstrument housing Fabricated sheet steel witha tough, textured paint finish

Conformance filters and certified colourreference solutions representing a range ofLovibond® colours, for quick and simple qualitycontrol checks on instruments and operators.

Certifications: Product certification: CE / US FDA / BIS

certified. Quality Certification: ISO certified. Should provide calibration certificates

from NIST traceable agencies duringwarranty & CMC period. Calibration costwill have to be borne by the supplier.

DQ, IQ, OQ, PQ Documentation duringinstallation.

For validation vender should having it owncapability with their own company trainedservice engineer to perform validation. No thirdpart validation will be entertained. Onevalidation at the time of installation should bedone by company personnel.

Warranty: Comprehensive warranty with sparesfor five years from the date of installation of theinstrument should be covered.

3. FLAMEPHOTOMETER

Range Na+: 0 to 199.9 ppm, K+: 0 to 9.99 ppm,Li+: 0 to 9.99 ppm

Sensitivity 0.1 ppm Na+; K=100 units

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Specificity less than 0.5% interference whenconcentrations are equal to test sampleconcentrations

Reproducibility less than 0.5% C.V. Linearity less than 1% Display dual display; 3-1/2-digit LED, 12.5 mm

(1/2") Fuel supply high-grade propane/butane

mixture regulated at approximately 30 psi Air supply 6 liters/min at 12 psi; oil and

moisture free Recorder output 0.05 to 5 V (switchable) Certifications:

Product certification: CE / US FDA / BIScertified.

Quality Certification: ISO certified. Should provide calibration certificates

from NABL accredited agency everyyear during warranty & CMC period.Calibration cost will have to be borne bythe supplier.

Equipment should be FDA / CE certified orequivalent standard of repute. It should be ISO9001:2000 or other equivalent qualitycertification.

All electrical peripherals required for smoothfunctioning e.g. voltage stabilizer should beprovided with the equipment.

Warranty: Comprehensive warranty with sparesfor five years from the date of installation of theinstrument should be covered.

4. MUFFLEFURNACE

1200 degree with 23 liter capacity or more Double Shell case, Stainless Steel High Purity insulation material with efficient low

thermal insulation Bench top model Vertically lift break switch/side lift break with

front loading Door: positive break switch Inside Chamber Size: 245-280 mm x 340-400 mm x

230-250 mm (WDH) Maximum temperature: 1200 oC Standard

continuous temperature 1050 oC or more Heating Rate: The furnace should be fast

heating type with maximum attainabletemperature should reach in 110 mins or better

Temperature control: Should bemicroprocessor based & at least 8 segmentprogrammable 3216P1 or equivalent controllerwith necessary safety features. Programmable

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Temperature controller with heating rate controlfrom 10 deg. min-1 to 100 deg.min-1 preferable

Temperature Accuracy: ± 5 oC over the wholetemperature range of operation and in theentire muffle

Safety: Over Temperature protection should beadded

Gas purging: Gas purging facility (inert gas inletand outlet)

Weight : less than 80 kg The furnace should be CE certified with suitable

power supply Installation, training and commissioning:

Vendor must ensure satisfactory installationand commissioning of the system at CFL,Kolkata. A detailed training on handling,operation and applications must be provided toat least 5 scientists. Installation services mustinclude IQ/OQ/PQ

For validation vender should have its owncapability with their own company trainedservice engineer to perform validation. No thirdpart validation will be entertained. Onevalidation at the time of installation should bedone by company personnel.

Warranty: Comprehensive warranty with sparesfor five years from the date of installation of theinstrument should be covered.

5. GASCHROMATOGRAPHYWITH FIDAND ECDDETECTORS

Pesticides residues and other Food & Waterrelated applications as per FSSAIrequirements

Gas chromatograph with capability of operatingconcurrently with two injectors or better andthree detectors. The system should be quotedwith all accessories required to make it fullyoperational and any other item required forstated applications be quoted as optional.

Oven Upto 450 oC, Fast Oven with 120 oC/min ramp,≥20≥7ramps

Cool-down time from 450 oC to 50oC within 5minutes

Should be able to accommodate two or moreinjectors and three detectors

Automatic leak test of system through single keyPneumaticControls

0-140 psi or better, all Electronic PneumaticControls with 0.1 psi precision

Injector ( 2 ormore)

Should be capable of large volume injectionTemperature ramped splitless, Split and Coldon-column modes ≥450 OC max. and ≥10 ramps.

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Multimode/PTV with 250µL or better InjectionVolume capability with complete solventvaporizer system or Equivalent.

Injector must be able to operate with capillary &wide bore columns

Injector must be provided with Backflush system.Autosampler( Liquid andHeadspace)

Robust Liquid autosampler capable of injecting≥100 samples or better with syringe capacity of 0.5-100 µl

The type and volume of the syringe must beautomatically detected by the system.

Must allow installation and automation ofsyringe featuring volumes from 0.5 to 100 µl.

Must be able to achieve combined multiplesolvent rinsing with upto 4 different solvents.

Head space auto sampler with a capacity ≥50 vialsor better that support 10 & 20ml vial capacity withPnuematic control Incubation Oven Temperature Range 50 to 200

°C in 1 °C steps Syringe Temperature 50 °C to 150 °C in 1 °C

steps Incubation Oven Capacity vials or better

Detectors The GC must have complete integrated controlof all parameters (no external control module) forthe following detectors: FID, and ECD.

Detector must be independently controlled andoperational for maximum sensitivity

FlameIonizationDetector (FID

Linear range : better than 107

Minimum detectable amount with makeup gases: 1.5 pgC/sec

Operating temperature limits: 450oC withstandard ceramic/quartz flame jet

Auto flame out detection. Acquisition rate 50 Hz or more.

ElectronCaptureDetector ECD

Linear dynamic range : better than 104

Complete with 63Ni source and low voltageheaters.

Minimum detectable amount: Less than 10 fg oflindane.

Operating temperature limits : 400oCGas Supplies Required High purity Gas cylinders (2 No. Each)SOFTWARE AND HARDWARE ( Single point control of Software& Hardware)Software Complete system and software configuration must

be 21 CFR Part 11 compliant. Software: WindowsBased software with multitasking and capable ofperforming the following functions: Control the MS,acquire, store, process and reproduce the data. It

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must be able to control all the devices from samesoftware. Software should allow monitoring of onemolecular ion and upto four confirmatory ions.Quantification software for batch process mustconfirm the analytes as per regulatory requirementsin food and environmental sample analysis as perthe applications specified.All Flow Controller i.e.Carrier flow, Make-up flow, Hydrogen flow, Air flowetc. value should set through Software by PC.HeadSpace Auto Sampler, Automation and event controlfrom PC through same software.IQOQ of the systemas well as software must be provided. Softwareupdate upto five years

Communication Hardware:

Latest Factory set, branded system with 22-23” FullHD Monitor with Printer - B/W - duplex - laser -Legal, A4 - 1200 dpi x 1200 dpi - up to 21 ppm –capacity with Network Card and Bluetooth facility.

IQOQPQ IQOQPQ of instrument and Software should beprovided along with document.

Training Technical and application training to the personnelat site immediately after installation as per terms &conditions of tender.

ApplicationSupport

The Application support for stated applicationsrequired during method development andvalidations.

Pre InstallationRequirements(PIR)

Provide PIR of the system.

OTHER REQUISITES FOR GC WITH ECD, FIDAutomatic Change Over Manifold for each gas lineComplete Gas Purification Panel with fittings & installation of all gasesRenewable In Line Gas Purification SystemRenewable gas purifier cartridge, Spare SetGas clean filters/Traps (6 No.)Septa forinjectors

Non stick, Low bleed, high puncture tolerance andMax. Temp 400 oC (for each injector). (400 No.)

Liners Suitable Ultra Inert Injector Liner for SS & SSL(20 No.)

Suitable Injector Liner upto 10 µL (6 No.) Suitable Injector Liner upto 250 µL (6 No.) Suitable Injector Liner upto 500 µL (6 No.) Liner O-Rings Max Temp 375 oC (100 No.) Liners types required as per the application

Ferrules andNuts

50 No. (for each column end and other interfaces asapplicable), 50 No. for GC with ECD, NPD, FID

Columns forGCApplications

Pesticide column (30m x 0.250mm x 0.25µm(HP-5MS / DB-1MS or equivalent) (02 no.)

Column for Fatty Acid Profiling with mainconcern of Trans Fatty Acid Application (02 No.)

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Column for Cholesterol Application (02 No.)Vials, caps andtool forautosampler(OnlyCompatiblesizes shouldbe supplied)

2000 No. each Vial sets (1, 2 mL, Crimp type,Amber and Clear glass )

200 No. Vials (10,20ml Crimp type with cap &septa)

1000 No. 300/500 µL Recovery vials 6000 No. Septa PTFE/Silicone (for 1, 2 mL

Vials) 6000 No. Septa PTFE/Silicone (for 10, 20 mL

Headspace Vials) Ergonomic Crimping Tools for different vial

types Ergonomic Decapping Tools for different vial

types 10 No. each Storage Racks for (for 1, 2 mL

Vials) Head Space vials 10,20 ml capacity (500no.

each)AutosamplerSyringe

10 µL (12 No.), 100 and 250 µL (04 No. each);Manual syringe-2µl, 5µl and 500 µl (04 No. each).Headspace syringe (02 no.10µl, 500µl,02 no. 1ml)

SamplePreparation(Water & Food)

QuEChERS Kits for Pesticides and Herbicides infollowing Matrices:

Water (1000 No.) Matrices with high fat (1000 No.) Matrices with high Water content and (1000

No.) Matrices with high pigmented (1000 No.)

Tools and Kits Septa Removing toolTubing Cutter with rotating diamond blade forcolumnTubing Cutter for stainless steel tubing (1/16 & 1/8inch tubing)Tubing Cutter for Plastic tubing with spare blade set

Miscellaneous Consumables required for each detector must beprovided

Warranty Comprehensive warranty with spares for five yearsfrom the date of installation of the instrument shouldbe covered.

6. GASCHROMATOGRAPHYWITH NPDANDTHERMALCONDUCTIVITIYDETECTOR(TCD)

Pesticides residues and other Food & Waterrelated applications as per FSSAIrequirements

Gas chromatograph with capability ofoperating concurrently with two injectors orbetter and three detectors. The system shouldbe quoted with all accessories required tomake it fully operational and any other itemrequired for stated applications be quoted asoptional.

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DETECTORS

Oven Upto 450 oC, Fast Oven with 120 oC/minramp, ≥20≥7ramps

Cool-down time from 450 oC to 50oC within 5minutes

Should be able to accommodate two or moreinjectors and three detectors

Automatic leak test of system throughsingle key

PneumaticControls

0-140 psi or better, all Electronic PneumaticControls with 0.1 psi precision

Injector ( 2 ormore)

Should be capable of large volume injectionTemperature ramped split-less, Split and Cold on-column modes ≥450 OC max and ≥10 ramps.

Multimode/PTV with 250µL or better InjectionVolume capability with complete solventvaporizer system or Equivalent.

Injector must be able to operate with capillary &wide bore columns

Injector must be provided with Backflush system.Autosampler Robust Liquid autosampler capable of injecting

≥100 samples or better with syringe capacity of 0.5-100 µl

The type and volume of the syringe must beautomatically detected by the system.

Must allow installation and automation ofsyringe featuring volumes from 0.5 to 100 µl.

Must be able to achieve combined multiplesolvent rinsing with upto 4 different solvents.

Detectors The GC must have complete integrated controlof all parameters (no external control module) forthe following detectors: NPD, and TCD.

Detector must be independently controlled andoperational for maximum sensitivity

NitrogenPhosphorus Detector(NPD)

Minimum detectable amount: 100fg N/sec, 100fgP/sec

Linear dynamic range: better than 104

Operating temperature limits: 450 C withstandard jet

ThermalConductivityDetector TCD

Capillary-column compatible Proven constant current design Software protection to prevent filament burnout Ideal for series operation 1/8-in. fittings PPC pneumatics - software flow control of

reference gas

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Operating temperature 100 ˚C to 350 ˚C in 1 ˚Cincrements

Sensitivity 9 µV/ppmnonane at 160 mA at thebridge with a detector temperature of 100 ˚C or100 pgtridecane, /mL with He

Minimum detectable quantity Typically < 1 ppmnonane

Linear dynamic range: better than 105 +/- 5% Operating temperature limits: 400 C

Gas Supplies Required High purity Gas cylinders (2 No. Each)SOFTWARE AND HARDWARE ( Single point control of Software& Hardware)Software Complete system and software configuration must

be 21 CFR Part 11 compliant. Software: WindowsBased software with multitasking and capable ofperforming the following functions: Control the MS,acquire, store, process and reproduce the data. Itmust be able to control all the devices from samesoftware. Software should allow monitoring of onemolecular ion and upto four confirmatory ions.Quantification software for batch process mustconfirm the analytes as per regulatory requirementsin food and environmental sample analysis as perthe applications specified.All Flow Controller i.e.Carrier flow, Make-up flow, Hydrogen flow, Air flowetc. value should set through Software by PC.HeadSpace Auto Sampler, Automation and event controlfrom PC through same software.IQOQ of the systemas well as software must be provided.Software update upto five years

Communication Hardware:

Latest Factory set, branded system with 22-23” FullHD Monitor with Printer - B/W - duplex - laser -Legal, A4 - 1200 dpi x 1200 dpi - up to 21 ppm –capacity with Network Card and Bluetooth facility.

IQOQPQ IQOQPQ of instrument and Software should beprovided along with document.

Training Technical and application training to the personnelat site immediately after installation as per terms &conditions of tender.

ApplicationSupport

The Application support for stated applicationsrequired during method development andvalidations.

Pre InstallationRequirements(PIR)

Provide PIR of the system.

OTHER REQUISITES FOR GC WITH NPD, TCDAutomatic Change Over Manifold for each gas lineComplete Gas Purification Panel with fittings & installation of allgasesRenewable In Line Gas Purification System

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Renewable gas purifier cartridge, Spare SetGas clean filters/Traps (6 No.)Septa forinjectors

Non stick, Low bleed, high puncture tolerance andMax. Temp 400 oC (for each injector). (400 No.)

Liners Suitable Ultra Inert Injector Liner for SS & SSL(20 No.)

Suitable Injector Liner upto 10 µL (6 No.) Suitable Injector Liner upto 250 µL (6 No.) Suitable Injector Liner upto 500 µL (6 No.) Liner O-Rings Max Temp 375 oC (100 No.) Liners types required as per the application

Ferrules andNuts

50 No. (for each column end and other interfaces asapplicable), 50 No. for GC with ECD, NPD, FID

Columns forGCApplications

Pesticide column (30m x 0.250mm x 0.25µm(HP-5MS / DB-1MS or equivalent) (02 no.)

Column for Fatty Acid Profiling with mainconcern of Trans Fatty Acid Application (02 No.)

Column for Cholesterol Application (02 No.)Vials, caps andtool forautosampler(OnlyCompatiblesizes shouldbe supplied)

2000 No. each Vial sets (1, 2 mL, Crimp type,Amber and Clear glass )

200 No. Vials (10,20ml Crimp type with cap &septa)

1000 No. 300/500 µL Recovery vials 6000 No. Septa PTFE/Silicone (for 1, 2 mL

Vials) Ergonomic Crimping Tools for different vial

types Ergonomic Decapping Tools for different vial

types 10 No. each Storage Racks for (for 1, 2 mL

Vials)AutosamplerSyringe

10 µL (12 No.), 100 and 250 µL (04 No. each);Manual syringe-2µl, 5µl and 500 µl (04 No. each).

SamplePreparation(Water & Food)

QuEChERS Kits for Pesticides and Herbicides infollowing Matrices:

Water (1000 No.) Matrices with high fat (1000 No.) Matrices with high Water content and (1000

No.) Matrices with high pigmented (1000 No.)

Tools and Kits Septa Removing toolTubing Cutter with rotating diamond blade forcolumnTubing Cutter for stainless steel tubing (1/16 & 1/8inch tubing)Tubing Cutter for Plastic tubing with spare blade set

Miscellaneous Consumables required for each detector must beprovided

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Warranty Comprehensive warranty with spares for five yearsfrom the date of installation of the instrument shouldbe covered.

7. MICROWAVEDIGESTIONSYSTEM

A latest model of microwave digestion systemshould enable rapid digestion for differentinorganic/organic samples like; Different types ofFSSAI food and food products, Fish and Fisheryproducts, tea, seasoning powder, biscuits etc.

Application A latest model of microwave digestion systemshould enable rapid digestion for differentinorganic/organic samples like; Different types ofFSSAI food and food products, Fish and Fisheryproducts, tea, seasoning powder, biscuits etc

General The instrument should have a superior pressureventing so as to prevent any loss of volatile metalsand should have homogeneous microwave field toavoid sample burning

System Microwave digestion system should havetemperature and pressure controlling/monitoringsystem. The system should be software controlled.Different types of rotors available for the digestion ofthe different type samples should also be quoted.Necessary consumables and maintenance partsshould also be quoted to run instrument trouble free

Instrument The system should be a stand alone work stationand should have The System should have the feature of simply

choose a method and it automaticallyrecognizes the vessel type, counts the vesselsand determines all of the parameters necessaryfor a fast, complete digestion

Should have provision that user can set thedesired parameters for digestion

Should have Automatic Microwave powerapplication depending on the load

Auto sensing of temperature and pressureinside the vessel

Be capable of processing different amounts ofsamples (from 0.3 g up to 10g) in the same runassuring the same conditions of temperatureand pressure

Display The Instrument should have the high-resolution, colour touch screen, acid resistant,LED/LCD screen should serve as controller anddisplay. Should be provided training videos forsample preparation vessel assembly, system use,and maintenance. Should have Data management– Easy access to stored methods, real-time dataand results of past runs. Should be able to displaythe detailed methods, graphs o f temperature and

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power against time and temperature of individualvessels.

Interlocks The system should have good interlocking systemfor safety and cavity door.

Vessel The system should be high throughput which canhold atleast 24 high pressure vessels. Must besupplied with digestion vessel racks and suitablyhandle different digestion volumes.

System The material of construction should be high purityTFM fluropolymer. Vessel should be capable ofhanlding volumes between 10 ml and > 25 ml, ifrequired. It should be operated for maximumtemperature capacity of 250ºC or more andmaximum pressure of 35 Bar or more. The systemshould be provided with temperature sensor(Thermocouple type/ Fiber optics/IR Sensor) whichwill measure real temperature of the vessels andcontrol it. The vessels should have automaticventing and re-sealing system in case there isexcess pressure development essential. AfterDigestion, vessels must be vent-able beforeuncapping the vessel for safety reasons. For ease ofuse, the vessels must not require the use of anenergizing tool in order to reform seals prior tooperation. Additional twelve numbers of vesselsshould be supplied along with the system.

MicrowavePower andoutput withuniform energydistribution

The Instrument should have single/dual magnetron1500 W (or more of delivered energy, should providethe temperature needed (300 °C) for difficultsamples and high-throughput vessel sets deliveringunpulsed continuous power & precisely tuned waveguide. Disperses microwave energy uniformlythroughout the cavity. No need for motor drivendiffusers or attenuators. System software mustautomatically adjust the power delivery based uponsample load and pre-programmed control settings.Automatic Power control Technology deliversmaximum energy to the sample, ensuring completedigestions. Controllable via microprocessor 230 Vinput, pulsed and unpulsed-essential 50 Hz, ACOperated. The Instrument should have“waveguide” between the magnetron (themicrowave energy source) and the cavity. Thiswaveguide fed system should provide maximumtuned transfer of microwave energy from themagnetron to the load in the microwave cavity.planes. This should result in uniform heating of thesample load.

MicrowaveCavity

The microwave cavity should be heavy duty andhave sufficient space to mount and dismountvessels individually and all parts inside the cavityshould be totally microwave transparent. The

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Cavity should be constructed with non magneticRugged high-grade 316 solid steel cavity. Thevessel assembly during a run should be visible fromoutside The coating inside the cavity should be acid/chemical. resistant special polymer coatinglike fluro-polymer / PTFE.

Controls The Instrument should have a) ReliableTemperature and b) Pressure controls independentof each other

Automatic temperature control system,temperature sensor should be protectedproperly from any chemical attack, sensorshould monitor and control all vesselssimultaneously-essential

Automatic Pressure control: should have apressure sensor which has a total capabilityof up to 500psi automatically control thepressure. It should be possible to remove thepressure device at a high pressure. TheVessels should act as self-regulators ofpressure

Control The control terminal should have high resolutionLED/LCD Acid Resistant display. Touch screenwhich should have method storage capacity. All thefeatures should be in built in the software. Shouldhave provision for manual programming storageapart from pre-installed programme. Continuousdisplay of temperature and power inside the reactionvessels is required.

Safety There has to be multiple levels of safety. A safemechanism to tackle the unused or reflectedmicrowave energy Capable of shutting off in theevent of the A very loud noise or bang in theinstrument. If the temperature of the vessel is nearits highest tolerance limit. Have inbuilt exhaustsystem to cool the vessels and to drive away if anyfumes in the cavity-essential

QualityStandards

The manufacturer should be ISO 9001 certified fordesign and manufacture of microwave digestionsystem

Certificationrequired forsign off

IQ/OQ compliance Calibration certificates for titrator GLP-validated software for controlling the

system

Operation andmaintenancetrainingcomponent

The supplier will have to carry out successfulinstallation at our laboratory premises (where everthe system has to be installed) and provide on –site comprehensive training for scientific personneloperating the system and support services tillcustomer satisfaction with the system.

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Warranty Comprehensive warranty with spares for five yearsfrom the date of installation of the instrument shouldbe covered. This will include yearly calibration start-up / commissioning routine servicing, regularmaintenance, preventive maintenance ofequipment and components and break downrepairs as and when occurring, ensuring thatsystem does not remain out of service for a periodmore than 24 hours in case of major breakdownsand 6-8 hour in the case of minor breakdowns dueto any unforeseen break down. The institution willprovide Water / Electricity power, etc. formaintenance work. The successful tenderer shallkeep the essential spares at site during the ContractPeriod to avoid the delay in attending faults /maintenance.

Servicecontractclauses,includingprices

List of all spares and accessories (including minor)with part numbers and price, required formaintenance and repairs in future afterguarantee/warranty period should be attached.

Operatingmanuals,servicemanuals, othermanuals

Should provide 2 sets (hardcopy and soft-copy) of:- User, technical and maintenance manuals to be

supplied in English language along with machinediagrams;

List of equipment and procedures required forlocal calibration and routine maintenance;

Service and operation manuals (original andcopy) to be provided;

Advanced maintenance tasks documentation; Certificate of calibration and inspection

CertificatesPerformanceand safetystandards(specific to thedevicetype);Localand/orinternational

Should be FDA/CE/BIS approved product.

Manufacturer and Supplier should have ISO13485 certification under ISO 9001for qualitystandards.

Electrical safety conforms to the standardsfor electrical safety IEC 60601- Generalrequirements (or equivalent BIS Standard)

Certified to be compliant with IEC 61010-1,IEC 61010-2-40 for safety

Supplier/Manufacturer

Must be ISO certified for quality

ServiceSupportContact details(HierarchyWise; includinga toll

Contact details of manufacturer, supplier andlocal service agent to be provided; AnyContract (AMC/CMC/adhoc) to be declaredby the manufacturer;

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free/landlinenumber)Recommendations orwarnings

Any warning signs would be adequatelydisplayed

8. DIGITALBUTRYOREFRACTOMETER

For checking purity and adulteration of fats and oils

System Automated Operating LCD screen directly withoutmanual alignment, can connect PC with RS232interface

Display The required data to be displayed on the screen,including: the date, temperature, refractive index,concentration, and amended in accordance with thecurrent temperature

MeasurementRange(AutomaticTemperatureControlled)

Concentration 0;95% Refractive Index 1.32422-1.7000

MinimumIndication

Butyro 0.1%RI 0.00001

MeasurementAccuracy

Butyro ±0.5% (at 40˚C)RI ±0.0003 (at 40˚C)

Precision(Reproducibilty

RI ± 0.00005Butyro ± 0.05

MeasurementTemperature

10 to 50˚C

AmbientTemperatureSample

10 to 40˚C

VolumeMeasurementTime

Less than 5 sec

SampleVolume

> 0.1 ml

CalibrationcertificateAccessories Reference Material Oil minimum 10 mlOperation andtrainingcomponent

The supplier will have to carry out successfulInstallation at the laboratory premises (where everthe system has to be installed) and provide on –site comprehensive training for a minimum of twoscientific personnel operating the system tillcustomer satisfaction

CertificatesPerformanceand safety

Should be FDA/CE/BIS approved product.

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Sl.No Item Specifications Price in INR

standards(specific to thedevicetype);Localand/orinternational

Manufacturer and Supplier should have ISO13485 certification under ISO 9001for qualitystandards.

Electrical safety conforms to the standards forelectrical safety IEC 60601- Generalrequirements(or equivalent BIS Standard)

Certified to be compliant with IEC 61010-1, IEC61010-2-40 for safety

Supplier/Manufacturer

Must be ISO certified for quality

ServiceSupportContact details(HierarchyWise; includinga tollfree/landlinenumber)

Contact details of manufacturer, supplier andlocal service agent to be provided; Any Contract(AMC/CMC/adhoc) to be declared by themanufacturer;

Recommendations orwarnings

Any warning signs would be adequatelydisplayed

Warranty Comprehensive warranty with spares for fiveyears from the date of installation of theinstrument should be covered.

Servicecontractclauses,includingprices

List of all spares and accessories (includingminor) with part numbers and price, required formaintenance and repairs in future afterguarantee/warranty period should be attached;

Operatingmanuals,servicemanuals, othermanuals

Should provide 2 sets(hardcopy and soft-copy) of:- User, technical and maintenance manuals to be

supplied in English language along with machinediagrams;

List of equipment and procedures required forlocal calibration and routine maintenance;

Service and operation manuals (original andcopy) to be provided;

Advanced maintenance tasks documentation; Certificate of calibration and inspection

9. Flash pointapparatus

Instrument designed in strict accordance withthe test method ASTM D93, Method A and B.

Microprocessor controlled unit with digital easyto read display of the results.

Ignition :-Electric ignition and should alsoprovide an automatic reignition facility.

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Sl.No Item Specifications Price in INR

Thermal detection (with metal sampletemperature probe) of the flash to eliminateinterference from water or silicone containingcompound.

Cooling : - Facility for built-in coolingconnection.

Automatic correction for standard barometricpressure vis-à-vis with final result.

Unit should have diagnostic program to checkevery key component and assembly andcalibration facility.

Unit should automatically determine flash pointin strict compliance with the appropriate testmethod.

Heating should be microprocessor controlled atthe specified rate; the ignitor is activated anddipped at precisely the correct temperature andfrequency.

Safety device for fire protection with alarm. Resistance check box for temperature

calibration with calibration certificate. The unit should be operable on 230v / 50 Hz. The system should be ISO 9001 quality

standard and supplied with operation manual. Merely copying our specifications in the

quotation shall not make the parties eligible forconsideration of the quotation. A quotation hasto be supported with the printed technicalleaflet/literature of the quoted model of the itemby the quoting party/manufacturer and thespecifications mentioned in the quotation mustbe reflected/supported by the printed technicalleaflet/literature.

Calibration : The firm must ensure that theequipment supplied is fully calibrated as perspecification requirements and also source offuture calibration at New Delhi & their frequencyof calibration needed

Spares : Vendor should quote recommendedspares for two years alongwith the equipmentfor smooth functioning of the equipment.

Spare Parts : Availability of spare parts of theequipment/instrument must be guaranteed for aperiod of at least seven years from the date ofsupply.

After Sales Services: It should be clearlymentioned in the quotation whether the aftersales services during and after the completionof warranty shall be provided directly by thesupplier or their authorized agent/representative. Terms of the after salesservices, if any, may be mentioned in the offer.

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Sl.No Item Specifications Price in INR

However, in both the cases the original suppliershall be responsible for poorperformance/services.

Inspection: The inspection of the system will bedone by our technical expert in the presence offirm representative.

Users List : The list of users specifically for thesame model/make of the quoted item ( not thelist of general users) along with the completename, address & contract numbers of the userorganizations/persons may be submitted withthe quotation along with the performancecertificates from all/some of them.

Training: Our Scientist/Technical personsshould be trained by the supplier at the projectsite free of cost. NOTE:- Firms havingequipment wherein single mother unit can beused for carrying out Flash Point by Abel FlashPoint using interchangeable analyzer unit shallbe considered, if otherwise found suitable vis-à-vis price factor & performance. Otherspecification requirement for Abel Flash Pointapparatus is enclosed.

Certifications: Product certification: CE / US FDA / BIS

certified. Quality Certification: ISO certified. Should provide calibration certificates

from NIST traceable calibration solutionsby any agency every year duringwarranty & CMC period. Calibration costwill have to be borne by the supplier.

Comprehensive warranty with spares for fiveyears from the date of installation of theinstrument should be covered.

Buy-back price for old Automated Pensky-Martens closed-cup flash point tester withsample changer measures the flash point of upto 12 samples automatically [Make: Petrotest,Germany Model: PMA-4, Year of Installation:2004] may also be quoted.

10. WaterPurificationsystem

Table top Water Purification System (Tap WaterFeed) should be capable of produce water foruse in HPLC solvents, Microbiology andreagent grade with the help of pre-treatmentmodule; RO Module, DI Module, Storage tank,UV Oxidation Chamber, Polishing module andfinal membrane filter 0.22um

Pre-treatmentSystem

Should consists: 5 micron,1 micron and Activated Carbon

wrapped type depth filter Pressure gauge with regulator

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Sl.No Item Specifications Price in INR

The unit should have automatic low/highpressure cut-off

ReverseOsmosis withElectroDeionizationStage:

Pre-treatment cartridge with auto-scalingcompounds, 0.5 micron filter and activatedcarbon or better.

Prefilter combination to protect the ROMembranes life or better.

RO Module with high performance thin filmcomposite membrane with salt retention rate upto 98%. The retention rate for dissolved organiccompounds, particles & colloids & bacteriaexceeds 99%

Deionization Module: Mixed bed resin moduleutilized for a reduction of the inlet conductivity.Used for inorganic applications.

Conductivity measurement is to be done afterRO, DI & Polishing module to monitor theperformance of Individual cartridge.

Should have suitable back wash programmebefore every operation or better

Storage Tank: 30 L or better Storage Tank with UV Lamp, Airfilter, CO2 Trap & Level Sensor.

The tank should made of pure water resistantPoly Ethylene material with an outlet to drain thetank totally and a pressure sensor for the tanklevel control

The storage tank should be 100% drainable.

Generalrequirements

Online UV oxidation chamber: UV Light Energy at185 nm & 254 nm wavelengths. TOC Measurement: Online continuous TOC

measurement with Live Display. Sterile Filter with 0.22 µm or better with

Autoclavable option for re-use System should meet reagent water quality

standards including ASTM Type 1, CLSI and ISO3696 Type Ι System should have flexible remote dispenser to

dispense water whenever needed System should have built-in automatic self-

cleaning mechanism to extend the life of cartridge Automatic flushing and recirculation in standby

mode to maintain consistent peak water purity User can collect RO Quality water from the

Storage tank & ultrapure water from flexibledispenser Should have cartridge change indicator The system should incorporate a fully

comprehensive, graphic colour LCD display toprovide system status, performance parameters,routine maintenance status and alarms of

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Sl.No Item Specifications Price in INR

troubleshooting, tank level status and automaticwarning of reordering of consumables and Provision for digital display to indicate status of

operation, resistivity or conductivity, temperatureand also alarm system in case of malfunctioning.

Pure WaterSpecification:(Type-2)

Production Rate : 10 LPH or better Conductivity : <2µs/cm at 298K (25°C) or better pH at 298K (25°C) => 6.6 or effectively neutral Total silica max 3ug/L or better

The UltrapureProduct Watershould of thefollowingspecifications:(Type-1)

Flow Rate : 1.0 L/min or better Should have conductivity @ 25 Deg C :

0.055 µs/cm or better Should have resistivity @ 25 Deg C : 18.2

MΩ-cm or better TOC : < 1 ppb or better Bacteria : <1 cfu/ml or better Particles >0.1µm : <1 per ml or better pH at 298K (25°C) = > 6.6 or Effectively

neutralCertificationrequired forsign off

IQ/OQ compliance Calibration certificates for titrator

Operation andmaintenancetrainingcomponent

The supplier will have to carry out successfulinstallation at our laboratory premises (where everthe system has to be installed) and provide on –site comprehensive training for scientific personneloperating the system and support services tillcustomer satisfaction with the system.

Warranty Comprehensive warranty with spares for five yearsfrom the date of installation of the instrument shouldbe covered. This will include yearly calibration start-up / commissioning routine servicing, regularmaintenance, preventive maintenance ofequipment and components and break downrepairs as and when occurring, ensuring thatsystem does not remain out of service for a periodmore than 24 hours in case of major breakdownsand 6-8 hour in the case of minor breakdowns dueto any unforeseen break down. The institution willprovide Water / Electricity power, etc. formaintenance work. The successful tenderer shallkeep the essential spares at site during theContract Period to avoid the delay in attendingfaults / maintenance.

Servicecontractclauses,includingprices

List of all spares and accessories (includingminor) with part numbers and price, required formaintenance and repairs in future afterguarantee/warranty period should be attached;

Operatingmanuals,

Should provide 2 sets(hardcopy and soft-copy) of:-

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Sl.No Item Specifications Price in INR

servicemanuals, othermanuals

User, technical and maintenance manuals to besupplied in English language along with machinediagrams;

List of equipment and procedures required forlocal calibration and routine maintenance;

Service and operation manuals (original andcopy) to be provided;

Advanced maintenance tasks documentation; Certificate of calibration and inspection

CertificatesPerformanceand safetystandards(specific to thedevicetype);Localand/orinternational

Should be FDA/CE/BIS approved product. Manufacturer and Supplier should have ISO

13485 certification under ISO 9001for qualitystandards.

Electrical safety conforms to the standardsfor electrical safety IEC 60601- Generalrequirements (or equivalent BIS Standard)

Certified to be compliant with IEC 61010-1,IEC 61010-2-40 for safety

Supplier/Manufacturer

Must be ISO certified for quality

ServiceSupportContact details(HierarchyWise; includinga tollfree/landlinenumber)

Contact details of manufacturer, supplier andlocal service agent to be provided; AnyContract (AMC/CMC/adhoc) to be declared bythe manufacturer;

Recommendations orwarnings

Any warning signs would be adequatelydisplayed

GROSS TOTAL (A)

BUY BACK1. Buy-back price for old Atomic Absorption Spectrophotometer [Make:

GBC Scientific Equipments, Australia, Model: Avanta PM and SystemAVANTA ULTRA Z1 & PAL4000 Auto-sampler Year of Installation:2001].

2. Buy-back price for old Digital Lovibond Tintometer [Make: TintometerLtd., U.K. Model: PFX 995 Year of Installation: 2003].

3. Buy-back price for old Muffle furnace [Make: Heraeus Instrument,Germany Model: M110, Year of Installation: 2000].

4. Buy back price for old Gas Chromatograph – Mass Spectrometer (GC / MS)With Headspace (HS) sampler, ECD, FID and Single Quadruple MS detector[Make: Perkin Elmer USA Model: Clarus® 500, Year of Installation: 2006.

5. Buy Back Price for old Microwave Digestion System [Make: CEMCorp., USA Model: MARS 5, Year of Installation: 2008.

6. Buy back price for old Refractometer [Make: Bellingham Stanley, U.K.Model: RFM 330, Year of Installation: 1996.

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Sl.No Item Specifications Price in INR

7. Buy-back price for old Automated Pensky-Martens closed-cup flashpoint tester with sample changer measures the flash point of up to 12samples automatically [Make: Petrotest, Germany Model: PMA-4,Year of Installation: 2004].

8. Buy Back price for old Deionized water generation system [Make:Millipore, U.S.A Model: ELIX 3, 10 AND MILLI Q, Year of Installation:2008.Buy Back Total (B)Net Amount (A-B)

Note1:(a) The financial bid has to be filled necessarily in the format given above and hasto be signed by the authorized representative of the bidder with full name designationand seal on each page. The above quote should include Clearing and Transportationcharges and cost of necessary civil/electrical work required for installation ofequipments to be carried out by the successful bidder.

(b) The bidder has to quote price for all the items mentioned above. In case bidderfails to quote price for all the items his bid will not be considered for evaluation.Consortium is allowed as a single entity or a subsidiary

(c) Price quoted should be valid for minimum 06 months from the last date ofsubmission of the bids.

(d) Explanatory notes, if so desired, can be separately submitted along with thefinancial bid but financial bid in the above format is required to be submitted.

(e) Equipment delivery time will be 90 days from the date of issue of Supply order.

(f) Please indicate separately any duties, taxes.

Note 2 : The rate may be quoted in foreign currency and/or in Indian currency, however, forcomparison/evaluation purpose the bills selling market rate of exchange established by RBIfor similar transaction as on date of opening of price bid shall be used to convert foreigncurrencies to the Indian rupees.

Note 3 : Determination of L-1 will be done based on Net amount after Buy Back adjustment(not including levies, taxes and duties levied by Central/State/Local governments such asexcise duty, GST, Octroi/entry tax, etc. on final product) of all items/requirements asmentioned above.

Signature of tenderer_______________Name in Block letter _______________Date ____________________________Capacity in which Signed____________

Sd/-

(Umesh Kumar Jain)Joint Director(QA)

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Revised Annexure: II

CERTIFICATE OF GUARANTEE/WARRANTY

i. I/We certify that the standard guarantee/warranty shall be for a period of 05years starting from the date of satisfactory installation, commissioning andhanding over of the equipment and of the works conducted therewith coveredunder the Supply order in working order. During the guarantee/warranty period.I/we shall provide free “after sale service” and the replacement of any part(s) ofthe equipment or rectification of defects of work of the equipment will be free ofcost. The replacement of the parts shall be arranged by us, at our own cost andresponsibility. We undertake that the above guarantee/warranty shall begin onlyfrom the date of satisfactory and faultless functioning of the equipment at CFL,Kolkata premises. The benefit of change in dates of the guarantee/warrantyperiod shall be in the interest of the user/your organization.

ii. During the warranty period, we shall provide at least 02 preventivemaintenance service per year.

iii. Uptime Guarantee: During the guarantee/warranty period, we will be responsibleto maintain the equipment in good working conditions for a period 328 days (i.e.90% uptime) in a block of 365 days, for 05 years.a. All the complaints will be attended by us within 03 working days of receipt of

the complaint in our office.b. In case there is delay of more than 03 days in attending to a complaint from

our side then you can count the number of days in excess of the permissibleresponse time in the downtime. The above said response time of 03 days forattending to a complaint by us will not be counted in the downtime.

c. Penalty: We shall pay a penalty equivalent to 0.5 % of the order value of theequipment for every week or part thereof delay in rectifying the defect.

Note: The right to accept the reason (s) for delay and consider reduction or waiveoff the penalty for the same shall be at the sole discretion of Director, CFL,Kolkata

iv. We undertake that all the spares/consumables related to equipment &exclusively supplied by manufacturer/supplier of the equipment shall be coveredunder warranty. Nothing shall be payable on account of these items duringwarranty by the Buyer.

v. We certify that the equipment being/quoted is the latest model and that sparesfor the equipment will be available for a period of at least 10 years and we alsoguarantee that we will keep the organization informed of any up date of theequipment over a period of 5 years.

vi. We guarantee that in case we fail to carry out the maintenance within thestipulated period, Director, CFL, Kolkata reserves the right to get themaintenance work carried out at our risk, cost and responsibility. All theexpenses including excess payment for repairs/maintenance shall be adjustedagainst the Performance Bank Guarantee. In case the expenses exceed theamount of Performance Bank Guarantee, the same shall be recoverable fromus with/without interest in accordance with the circumstances.

vii. We shall try to repair the equipment at CFL, Kolkata premises itself. However,the equipment will be taken to our site on our own expenses in case it is notpossible to repair the same at CFL, Kolkata. We shall take the entireresponsibility for the safe custody and transportation of the equipment taken outfor repairs till the equipment is rehabilitated to the CFL, Kolkata after repairsAny loss of equipment or its accessories under its charge on account of theft,fire or any other reasons shall be at our sole risk and responsibility which will be

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compensated to the Buyer for such losses at the order value for thedamaged/lost equipment/part, including accessories.

viii. We undertake to perform Quality check after every majorrepair/breakdown/taking the equipment for repair out of CFL, Kolkata premises.

ix. In case of extended guarantee/warrantee, we undertake to carry out annualcalibration/IPV of the equipment.

x. We guarantee that we will supply spare parts if and when required on agreedbasis for an agreed price. The agreed basis could be an agreed discount on thepublished catalogue price.

xi. We guarantee to the effect that before going out of production of spare parts,we will give adequate advance notice to you so that you may undertake toprocure the balance of the life time requirements of spare parts.

xii. We guarantee the entire unit against defects of manufacture, workmanship andpoor quality of components.

xiii. We undertake to provide PM kit as per requirement to meet uptime guaranteecondition.

1. Authorized signatory(with seal)

Date

Place

2. Authorized signatory

NOTE:

1. This should be submitted on the letter head of the bidder company/firm.