2011 Inspection Report - US EPA · No documents were declared CBI during EPA’s inspection. Both EPA and the facility signed both forms and EPA concluded its in ... Lab Hood #1 PCB

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UNITED STATES ENVIRONMENTAL PROTECTION AGENCYREGION IX

75 Hawthorne StreetSan Francisco, CA 94105

WASTE MANAGEMENT DIVISIONRCRA ENFORCEMENT OWICE

TSCA COMPLIANCE EVALUATION INSPECTION REPORT

Purpose: TSCA Compliance Evaluation Inspection

Facility: Clean Harbors Los Angeles, LLC5756 Alba StreetLos Angeles, CA 90058

EPA ID Number: CAD 050 806 850

Date of Inspection: August 25, 2011

EPA Representatives: Jennifer DowneyEnforcement Officer(415) [email protected]

Christopher RollinsEnforcement Officer(415)[email protected]

Facifity Representatives: Dave CochranGeneral Manager(323) 277-2521

Joe ChristopherCompliance Manager(310) 835-0775 x 499

Mac HardawayGeneral Manager — Transformer Services(323) 277-2508

Jesus VelaOperations Supervisor

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Edgar MilitarLaboratory Manager

Report Prepared By: Jennifer Downey

Report Date: October 12, 2011

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Introduction

On August 25, 2011, U.S. Environmental Protection Agency (“EPA”) representatives conductedan unannounced Toxic Substances Control Act (“TSCA”) Compliance Evaluation Inspection(“CEr’) of Clean Harbors Los Angeles, LLC (“Clean Harbors”), located at 5756 Alba Street, inLos Angeles, California. The purpose of the inspection was to determine Clean Harbors’compliance with the Polychiorinated Biphenyls (“PCBs”) regulations under 40 Code of FederalRegulations (“C.F.R.”) parts 761, and the California Health and Safety Code (“HSC”), Division20, Chapter 6.5; and the California Code of Regulations (“C.C.R.”), Title 22, Division 4.5.

This inspection report summarizes the events that transpired during the inspection, theobservations and findings made by the EPA inspectors, and information received from thefacility subsequent to the inspection.

Facffitv Background

Facility Name Clean Harbors Los Angeles, LLC (“Clean Harbors”)Established EPA originally granted this facility location a TSCAApproval

under the name Oil Process Company in 1991. On February 15,2002, the TSCA PCB Approval for the 5756 Mba Street facilitylocation expired. However, the permit has been administrativelyextended until EPA can complete its review of Clean Harbors’application for permit renewal, which was submitted prior to thepermit expiration date.

Number of Employees 25 EmployeesHours of Operation 6:00 am to 10:30 pm (2 shifts)Filed Notification of This facility location first filed a Notification of PCB WastePCB Waste Activity Form Activity Form on January 24, 1990. Clean Harbors submitted an

additional Notification of PCB Activity Form notifying EPA ofits generator status on July 26, 2007.

Facility Processes Clean Harbors provides environmental and hazardous wastemanagement services in the United States. The facilityspecializes in decontamination, emergency response, disposaland recovery services related to hazardous waste and used oil.This location also stores and consolidates PCBs and PCBEquipment destined for disposal at TSCA regulated facilities.

Waste Streams Used Oil, PCB liquids, PCB Equipment and scrap metal from theprocessing of Non-PCB and PCB equipment.

PCB Facility Status PCB Commercial Storage FacilityLast Inspection EPA Region 9 last conducted a TSCA PCB inspection of the

Clean Harbors facility on July 16, 2009. Violations documentedin the report included failure to properly mark PCBs and PCBitems, failure to include the removal from service dates on PCBcontainers and manifests, and failure to mark all equipment usedfor handling PCBs with the PCB ML label.

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Google Earth Aerial View of the Clean Harbors Los Angeles Facility

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Facility Inspection

On August 25, 2011, EPA representatives arrived at Clean Harbors Los Angeles, Californiafacility at approximately 11:12 am. Two EPA Region 9 inspectors (Ms. Jennifer Downey andMr. Christopher Rollins) were present during the inspection.

During the in-brief, the inspectors presented their credentials. Mr. Rollins then presented andexplained the Notice of Inspection form (Attachment 3a.) and a TSCA Inspection ConfidentialityNotice form (Attachment 3b.) to the Clean Harbors representatives.

Under TSCA, the Notice of Inspection form is required to be signed prior to conducting aninspection and the TSCA Confidentiality Notice form outlines Clean Harbors’ right to claimPCB materials or documents collected during or after the inspection as TSCA ConfidentialBusiness Information (“CBI”). No documents were declared CBI during EPA’s inspection.Both EPA and the facility signed both forms and EPA concluded its in-brief.

EPA inspectors conducted a walk-through of the facility and collected eleven surface wipesamples to evaluate Clean Harbors’ management of PCBs.

The following summarize the areas inspected and the potential violations found near or adjacentto the Truck Loading Dock, Container Storage Warehouse, and On-Site Laboratory.

Area 1: Truck Loading Dock

The inspectors observed sixteen 55-gallon drums containing PCB waste on pallets in the TruckLoading Dock area that were ready to be shipped offsite (see Photo 2). The out of service datewas marked on the top of each drum. In addition, the drums were marked with a PCB ML label,a hazardous waste label (designating the PCB material as a California-only hazardous waste) andan internal tracking label. The hazardous waste labels and internal tracking labels were eachmarked with their own dates, which did not correspond with the out of service date. Theinspectors noted that all of the hazardous waste labels were marked with an accumulation startdate of 8/24/2011 (see Photo 3). According to facility representatives, the hazardous wastelabels had been affixed to the drums the day before when Clean Harbors generated themanifest(s) which will accompany the waste when it is shipped offsite for treatment and disposalat another facility. The inspectors expressed concern that Clean Harbors was not entering the outof service date as the hazardous waste accumulation start date.

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Area 2: Container Stqrage Warehouse

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Photo 3— Hazardous Waste Label Dated 8/24/2011

Location Waste Type Potential Violation Photo

Warehouse Floor PCB Wipe Sample None N/A

CH0825 1 1SW-1

Entrance PCB Wipe Sample None N/A

CH0825 1 1SW-2

Ramp PCB Wipe Sample None N/A

CH08251 1SW-3

Leaky Transformer PCB Wipe Sample None 4, 5

CH08251 1SW-4

Bay 1 PCB Wipe Sample None N/A

CH08251 1SW-5

Bay 4 PCB Wipe Sample None N/A

CH08251 1SW-6

Bay 2 PCB Wipe Sample None 7

CHO825I1SW-7

Bay 3 PCB Wipe Sample None 8

CH08251 1SW-8

.11kIZARDOUS WASTE‘•‘ “‘

AW Pfl(jpjg UPfOpl 04PQ*L4 Llti 1

• r* •‘

-

Photo 2— Containers in

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The inspectors observed 2 leaking transformers in Clean Harbors’ Container Storage Warehouse.The first transformer, located in Bay 4, had “330 ppm” written on the side of the transformer (seePhotos 4 and 5). EPA collected a PCB wipe sample of the oil on the day of the inspection(Sample CH0825 11 SW-4). However, according to the analytical results, EPA only detectedPCBs at 6.5 g/100 cm2. The action level for PCB wipe samples under TSCA is 10 .tg/l00 cm2.The second leaky transformer was marked as “6 ppm” and was stored in a containment unit inthe non-PCB (<50 ppm) storage area of the warehouse.

The inspectors observed a metal drum (Drum#24612696) in Bay 3 of the Container StorageWarehouse that had “Assume >500” writtenon the drum lid by the generator, but did nothave a PCB ML label affixed (see Photo 6).EPA asked that Clean Harbors provide EPAwith analytical and profile information for thedrum. On October 4, 2011, Clean Harborssent EPA the requested information(Attachment 4), including laboratory resultsshowing no detectable levels of PCBs in thedrum contents.

The inspectors observed 2 big stains on the floor near Clean Harbors’s electrical pump in Bay 2(see Photo 7). EPA collected a PCB wipe sample over one of the stains (Sample CHO82511SW-7). According to the analytical results, EPA only detected PCBs at .06 igIl00 cm2. Theinspectors also observed significant staining and residue in the gutter area of Bay 3 (see Photo 8).EPA collected a PCB wipe sample in the gutter area (Sample CH08251 1SW-8). According tothe analytical results, EPA only detected PCBs at .2 .tgI100 cm2.

Photo 4— Transformer Marked as “330 ppm”

Photo 6— Drum #24612696 Marked “Assume > 500”

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A total of eight surface wipes (CH08251 1SW-1 to CH08251 1SW-8) were collected inside the

Container Storage Warehouse. None of the wipe samples exceeded the threshold for unresthcted

use under TSCA (10 .tg/1O0 cm2).

Area 3: Onsite Laboratory

Location Waste Type Potential Violation Photo

Lab Hood #1 PCB Wipe Sample N/A — Field Blank N/ACH0825 1 1SW-9

Lab Hood #1 PCB Wipe Sample None N/A

CH08251 1SW-10

Lab Hood #2 PCB Wipe Sample None N/A

CH08251 1SW-1 1

The inspectors observed 3 containers in the temporary PCB storage area inside the Laboratory

(see Photos 9 and 10). A white container, partially filled with PCB oil, was not marked with a

PCB ML label as required. The drum also should be labeled as CA-only hazardous waste. Clean

Harbors affixed the appropriate labels prior to the end of the inspection.

- —- -) 7: Wipe Sample Near Pump in Bay 2

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A total of three surface wipes (CH0825 11 SW-9 to CH0825 11 Sw-il) were collected inside theLaboratory. The analytical results of the wipes were non-detect for PCBs.

Record Review

The inspectors requested that Clean Harbors subsequently provide EPA with an inventory ofPCB items on site at the time of the inspection, analytical and profile information for drum24612696, and analytical information and manifest(s) from decontamination of a PCB tankearlier in the year. Clean Harbors provided the requested information on October 4, 2011(Attachment 4).

Photo 9: Laboratory PCB Storage Area

Photo 10: White PCB Container Not Properly Labeled

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Potential Violation of TSCA PCB Requirements

1. Failure to Mark PCBs and PCB Items [40 C.F.R. § 761.40(a)(1)].Requirements:

TSCA requirement 40 C.F.R. § 761.40(a)(1) states each [PCB Containers] in existence onor after July 1, 1978 shall be marked as ifiustrated in Figure 1 in § 76 1.45(a): The markifiustrated in Figure 1 is referred to as ML throughout this subpart.

Findings:During the inspection, EPA observed a container of PCB oil in the laboratory which wasnot properly marked with a PCB ML label as required under TSCA.

Facility Response:Clean Harbors documented its, return to compliance by affixing a PCB ML label to thecontainer prior to the end of the inspection. Clean Harbors also re-trained their TSCA

facility laboratory teams on all waste standards of operation, including waste containerlabeling requirements, subsequent to the inspection.

List of Attachments

1. Inspection Photo Log2. EPA Region 9 Laboratory Analytical Testing Results3. TSCA Inspection Forms

a. Notice of Inspectionb. TSCA Inspection Confidentiality Noticec. Receipt for Samples and Documentsd. Chain of Custody Record

4. Clean Harbors October 4, 2011 Correspondence

Page 10 of 10

oATTACHMENT 1

Photograph Log for EPA’s August 25,2011Clean Harbors Los Angeles TSCA Inspection

All photographs on this log were taken with a Olympus Tough TG-310 digital camera byChristopher Rollins or Jennifer Downey, RCRA Enforcement Office, EPA Region IX. Pleasenote that each photograph number listed below begins with “P82500”.

01. Sign located at the front of the facility

02. Drums in Truck Loading Dock area

03. Close-up of drum in Truck Loading Dock area

04. Hazardous waste label on drum in Truck Loading Dock area (8/24/11 accumulation startdate)

05. Top of drum showing out of service date in Truck Loading Dock area

06. Drums in Truck Loading Dock area

07. Top of drum showing out of service date in Truck Loading Dock area

08. Clean Harbors Supplemental Drum Label on drum in Truck Loading Dock area

09. Hazardous waste container near entrance to Container Storage Warehouse

10. Drums near front of Container Storage Warehouse

11.. Labels on a drum near the front of Container Storage Warehouse

12. Labels on a drum near the front of Container Storage Warehouse

13. Leaking “330 ppm” transformer

14. Liquid and stains below “330 ppm” leaking transformer

15. Liquid and stains below “6 ppm” leaking transformer

16. “6 ppm” leaking transformer

17. Transformers and containers in TSCA area of Container Storage Warehouse




21. Labels and markings on top of TSCA regulated item in Container Storage Warehouse

0 022. Hazardous waste labels on non-TSCA PCB items in Container Storage Warehouse

23. Labels on container of potentially PCB contaminated debris in Container StorageWarehouse

24. Drum in Bay 3 of Container Storage Warehouse

25. Drum #246 12696 in Bay 3 of Container Storage Warehouse

26 Hazardous waste label on drum m Contamer Storage Warehouse

27 PCB label on small contamer m Container Storage Warehouse

28 PCB pump and equipment in Bay 2

29 EPA wipe sample CHO82511SW-1

30 EPAwipe sample CHO82511SW-2

31. EPA wipe sample CHO82511SW-3

32. Clean Harbors wipe sample next to CH08251 1SW-3

33. EPA wipe sample CH08251 1SW-4

34. Clean Harbors wipe sample next to C11082511SW-4

35. EPA wipe sample CJzIO82511SW-5


37. EPA wipe sample CH08251 1SW-7

38. PCB hose and staining on floor in Bay 2


40. After EPA wipe sample CH08251 1SW-8

41. Drums in Bay 3 of Container Storage Warehouse

42. Step can filled with potentially PCB contaminated gloves in Laboratory

43. Containers in Laboratory temporary PCB storage area

44. Containers in Laboratory temporary PCB storage area

45. EPA wipe sample CF108251 ISW-1O

46. EPA wipe sample CH0825 11 Sw-lI

1

P8250004

P8250028

$fr .r

P8250010

P8250005

P8250007 P8250008 P8250009

P8250011 P8250012 P8250013 P8250014 P8250015

P8250018 P8250019

P8250021

P8250020

P8250022 P8250023 P8250024 P8250025

P8250027

P8250031

P8250029 P8250030

P8250032--

P8250034P8250033 P8250035

0

P8250037 P8250038

P8250041 P8250042 P8250043 P8250044

P8250046

P8250045

-

4 _4

L;

2FNAL 09 22 11 1535

United States Environmental Protection Agency—- -

— Region 9-Laboratory---1337 S. 46th Street Building 201

Richmond, CA 94804

912212011

Subject: Analytical Testing Results -Project RIIRO8

- SDG1238-

From: Brenda Bettencourt, DirectoEPA Region 9 LaboratoryMTS-2

To: Jennifer DowneyRCRA Enforcement OfficeWST-3

Attached are the results from the analysis of samples from the Clean Harbors LosAngeles 2011 TSCA inspection project. These data have been reviewed in accordancewith EPA Region 9 Laboratory policy.

A full documentation package for these data, including raw data and sample custodydocumentation, is on file at the EPA Region 9 Laboratory. If you would like to requestadditional review and/or validation of the data, please contact Eugenia McNaughton at theRegion 9 QualIty Assurance Office.

If you have any questions, please ask for Richard Bauer, the Lab ProjectManager at (510)412-2300.

Analyses Included In this report:

Date:

PCB Aroclors by GC/ECD PCB Aroclors by OC/ECO

SDGID 112388

PCB wipe extraction: Wipes were transferred from the sample vial to soxhiet extraction apparatus. The sample vials weresubsequently rinsed with dichloromethane and the rinsate added to the soxhlet. Sample wipes 1108070-01 through -08were soiled with black stains, and wipes -09 through -11 appeared clean. Samples -04. -06, and -08 contained smalldebris particles.

Surrogate solke comciounds: Tetrachlora.m-xylene and decachiorobiphenyl were added toeaclTwipe sample assurrogate standards. Only decachlorobiphenyl was evaluated for QC flagging. Tetrachloro-m-xylene is used as asecondary surrogate and only evaluated when the presence of decachlorobiphenyl is suspected in the sample itself (aswhen aroclor 1268 is present in the sample).

Reporting units: All results are reported in ugIlOO cm2, based on the assumption that a 100 cm2 area was wiped.

Work Order(s)

1108070

,cc0SZ Unittates Environmental Protection Aenc

Region 9 Laboratory1337 S. 46th Street, Building 201, Richmond, CA 94804

‘L PRO0 Phone:(510) 412-2300 Fax:(510) 412-2302

Project Manager: Jennifer Downey RCRA Enforcement Office SDG: I 1238B

Project Numher: RIIRO8 75 Hawthorne Street Reported: 09/22/11 15:35

Project: Clean Harbors Los Angeles 2011 TSCA San Francisco CA, 94105

Inspection

Date Collected Date ReceivedSample ID Laboratory ID Matrix

CHO8251ISW-l 1108070-01 Wipe 08/25/11 13:16 08/26/11 11:00

CHO825IISW-2 1108070-02 Wipe 08/25/11 13:21 08/26/11 11:00

CH08251 I SW-3 1108070-03 Wipe 08/25/1 1 13:24 08/26/11 1 1:00

CHO825IISW-4 1108070-04 Wipe 08/25/11 13:32 08/26/11 11:00

CHO825IISW-5 1108070-05 Wipe 08/25/11 13:40 08/26/11 11:00

CHO825IISW-6 1108070-06 Wipe 08/25/11 13:44 08/26/11 11:00

CHO82SIISW-7 1108070-07 Wipe 08/25/11 13:53 08/26/11 11:00

CH082511SW8 1108070-08 Wipe 08/25/11 14:00 08/26/11 11:00

CH0825 I 1SW9 1108070-09 Wipe 08/25/11 14:38 08/26/li 11:00

CH082511SW10 1108070-10 Wipe 08/25/11 14:44 08/26/lI 11:00

CHO8251ISW-l1 1108070-11 Wipe 08/25/11 14:51 08/26/11 11:00

IIOBQThflNALO922 111535 Page I of7

Surrogate: Tetrachlaro-m.xylene

Surrogate: Decachiarobiphenyl

Lab ID:

Sample ID:

Aroclor 1016

Aroclor 1221

Aroclor 1232

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260

Aroclor 1262

Aroclor 1268

Wipe-Sampled: 08/25/11 13:24

Polychiorinated Biphenyla by EPA Method 8082A0.1 ugIl00cm B1H0152 08/30/Il 09/01/Il 8082A1S0P335

0.2 ‘ “ “ “ 8082A1S0P335

0.1 ‘ 8082A/S0P335

0.1 “ ‘ ‘ 8082A)S0P335

0.1 ‘ 8082AJS0P335

0.1 ‘ “ 8082A/S0P335

0.1 “ 8082A/S0P335

0.1 ‘ “ 8082AiSOP335

0.1 “ ‘ “ 8082A1S0P335

ited States Environmental Protectioncncy V

Region 9 Laboratory13375.46th Street, Building 201, Richmond, CA 94804

Phone:(51 0) 412-2300 Fax:(51 0) 412-2302

Project Manager: Jennifer Downey RCRA Enforcement Office SDG: 112388

Project Number: Ri 1R08 75 Hawthorne Street Reported: 09/22/1115:35

Project: Clean Harbors Los Angeles 2011 TSCA San Francisco CA, 94105inspection V

3ample ResuIts

_____ ______ ______

V Reanalysis / Qualifiers / QuantitationAnalyte Extract Result Comments LImit Units Batch Prepared Analyzed Method

Lab ID: 1108070-01 Wipe - Sampled: 08/25/1113:16

Sample ID: CH082511SW4 Polychiorinated Blphenyls by EPA Method 8082AAroclor 1016 ND U 0.1 ug/I00cm B1H0152 08/30/Il 09/01/Il 8082A/S0P335

Aroclor 1221 ND U 0.2 ‘ 8082A1S0P335

Aroclor 1232 ND U 0.1 0 ‘ 8082A1S0P335

Aroclor 1242 ND U 0.1 ‘ 0 0 0 8082A1S0P335

Aroclor 1248V ND U

V

0.1 0 0 8082A1S0P335

Aroclor 1254 ND U 0.1 0 0 8082A)S0P335

Aroclor 1260 ND 3, Q2, U 0.1 ‘ “ 8082A1S0P335

Aroclor 1262 ND U 0.1 ‘ “ ‘ 8082A1S0P335

Aroclor 1268 ND U 0.1 “ “ 8082AJS0P335

V

Surrogate: Tetrachloro-m-xylene 89 % 88.8-128%

Surrogate: Decachlorobiphenyl 80 % 47.4-136%

Lab ID: 1108070-02 Wipe - Sampled: 08/25/11 13:21

Sample ID: C1108251 ISW-2 Polychlorinated Biphenyls by EPA Method 8082AArocior 1016 ND U 0.1 ugiIOOcm2 BlH0152 08/30/li 09/01/11 8082A1S0P335

NLV0,2VVV V ‘_“ “ 8082A1S0P335

Aroclor 1232 ND U 0.1 “ 0“ 8082A1S0P335

Aroclor 1242 ND U 0.1 “ “ 8082A/S0P335

Aroclor 1248 ND U 0.1 “ 0“ 8082A1S0P335

Aroclor 1254 ND U 0.1 “ “ ‘ 8082AJS0P335

Aroclor 1260 ND 1, Q2, U ‘ “ ‘ 8082A1S0P335

Aroclor 1262 ND U ‘ “ ‘ 8082A1S0P335

Aroclor 1268 ND U ‘ ‘ “ “ 8082A/S0P335

1108070-03

C1108251 ISW-3

0.1

0.1

0.1

88.8-128%

4 7.4-136%

9! %

82%

ND U

ND U

ND U

ND U

ND U

ND U

ND J,Q2,U

ND U

ND U

11O7O FINAL 9 22 111535 Page 2 of 7

Lab ID: Wipe - Sampled: 08/25/11 13:32

Sample ID: Polychiorlnated Biphenyls by EPA Method 8082AAroclor 1016 ND U 0.1 ug/IOOcma B1H0152 08/30/Il 09/01/Il 8082AJS0P335

Aroclor 1221 ND U 0.2 ‘ “ 8082A1S0P335

Aroclor 1232 ND U 0.1 “ ‘ “ 8082A1S0P335

Aroclor 1242 ND U 0.1 0 8082AJS0P335

Aroclor 1248 ND U 0.1 “ 8082A1S0P335

Aroclor 1254 ND U 0.1 0 0 8082A1S0P335

Aroclor 1260 0.5 ‘ 09/07/Il 8082A/S0P335

Aroclor 1262 ND U 0.1 0 ‘‘ 09101/11 8082A1S0P335

Aroclor 1268 ND U 0.1 0 8082A1S0P335

Surrogate: Tetrachloro-m-xylene

Surrogate: Decachiorobiphenyl

Lab ID: Wipe - Sampled: 08/2511113:40

Sample ID: Polychlorlnated Biphenyls by EPA Method 8082AAroclor 1016 0.1 ug/loocm’ B1H0152 08/30/Il 09/01/Il 8082A1S0P335

Aroclor 1221 0.2 0 0‘ 8082A1S0P335

Aroclor 1232 0.1 0 0 0 0 8082A1S0P335

Aroclor 1242 0.1 0 0 0 8082A1S0P335

Aroclor 1248 0.10 0 0 0 8082A1S0P335

Aroclór 1254 0.1 0 0 8082A/S0P335

Aroclor 1260 0.1 0 0 0 8082A/S0P335

Aroclor 1262 0.1 0 0 0 0 8082A/S0P335

Aroclor 1268 0.1 0 0 0 8082A1S0P335

WIpe-Sampled: 08/25/11 13:44

Polychlorlnated Blphenyls by EPA Method 8082A0.1 ug/IOOcm2 BIHOI52 08/30/Il 09/01/Il 8082A1S0P335

8082A1S0P335

8082A1S0P335

8082A/S0P335

8082A/S0P335

8082A/S0P335

DS3q7, Unitates Environmental Protection Aeic

9 Laboratory% 1337 S. 46th Street, Building 201, Richmond, CA 94804

LPIO Phone:(510)412-2300 Fax:(510)412-2302

Project Manager: Jennifer Downey RCRA Enforcement Office SDG: I 1238B

Project Number: RI 1R08 75 Hawthorne Street Reported: 09/22/1115:35


Inspection

____

ReanalysIs / QualIfIers I QuantltatlonAnalyte

- Extract Result Comments LImIt UnIts Batch Prepared Analyzed Method

Lab ID: 1108070-03 Wipe - Sampled: 08/25/11 13:24

Sample ID: CHO8Z5I1SW3 Polychlorlnated Blphenyls by EPA Method 8082ASurrogate: Tetrachloro-m-xylene 92 % 88.8-128% BJHOI52 08/30/Il 09/01/11

Surrogate: Decachioroblphenyl 84 % 4 7.4-136% 0

1108070-04

CHOS2SI ISW-4

REl 6.5

1108070-05

CH08251 ISW-5

81 %

75 %

88,8-128%

4 7.4-136%

ND U

ND U

ND U

ND U

ND U

ND U

ND JQ2,U

ND U

ND U


Surrogate: Decachlorobiphenyl 81 % 4 7.4-136%

Lab ID: 1108070-06

Sample ID: CHO8251ISW-6

Aroclor 1016 ND U

Aroclor 1221 ND U 0.2

Aroclor 1232 0.4 0.1 0

Aroclor 1242 ND U 0.1 0



I 11L070 FINAL 092211 1535 Page 3 of 7

DS?4 ited States Environmental Protection ency

I Region 9 Laboratory%% J 1337 S. 46th Street, Building 201, Richmond, CA 94804

L PRO’ Phone:(51 0) 412-2300 Fax:(51 0) 412-2302

Project Manager: Jennifer Downey RCRA Enforcement Office SLOG: 112388

Project Number: RI 1R08 75 Hawthorne Street Reported: 09/22/11 15:35


Inspection

r Reanalysis I Qualifiers I Quantitatlon

1AtuuI Extract Result Comments Limit Units Batch Prepared Analyzed Method

Lab ID: 1108070.06 Wipe - Sampled: 08125111 13:44

Sample ID: CH08251 ISW-6 Polychiorinated Biphenyle by EPA Method 8082A

Aroclor 1260 ND 3, Q2, U 0.1 ug/l00cm1 BIHOI52 08/30/I I 09/01/Il 8082A/S0P335

Aroclor 1262 ND U 0.1 “ 8082A/S0P335

Aroclor 1268 ND U 0.1 ‘ 8082A/S0P335

Surrogate: Teirachloro-m-xylene 89 % 88.8-128%

Surrogate: Decachlorobiphenyl 87 % 4 7.4-136%

Lab ID: 1108070-07 Wipe-Sampled: 08/25/11 13:53

Sample ID: CHO825IISW-7 Polychiorinated Biphenyls by EPA Method 8082A

Aroclor 1016 ND U 0.1 ug/IOOcm3 BIHOIS2 08/30/Il 09/02/Il 8082A/S0P335

Aroclor 1221 ND U 0.2 ‘ 8082A/S0P335

Aroclor 1232 ND U 0.1 “ “ 8082A/S0P335

Aroclor 1242 ND U 0.1 ‘ 8082A1S0P335

Aroclor 1248 ND U 0.1 8082A/S0P335

Aroclor 1254 ND U 0.1 ‘ 8082A/50P335

Aroclor 1260 0.06 Cl,J,Q2 0.1 8082A/S0P335

Aroclor (262 - -. ND U 0.1 ‘ 8082A/S0P335

Aroclor 1268 ND U 0.1 ‘ 8082A1S0P335


Surrogate: Decachlorobiphenyl SI % 47.4-136%

Lab ID: 1108070-08 Wipe-Sampled: 08/25/11 14:00

Sample ID: CHOS25IISW4 Polychiorlnated Biphenyls by EPA Method 8082A

Aroclor 1016 ND U 0.1 ug/1D0cm B1H0152 08/30/Il 09/02/I I 8082A1S0P335

Aroclor 1221 ND U 0.2 ‘ ‘ 8082A/S0P335

Aroclor 1232 ND U 0.1 ‘ ‘ 8082A/S0P335

Aroclor 1242 ND U 0.1 ‘ ‘ ‘ 8082A./50P335

Aroclor 1248 ND U 0.1 ‘ 8082A/S0P335

Aroclor 1254 ND U 0.1 “8082A/S0P335

Aroclor 1260 0.2 J,Q2 0.1 “ 8082AJS0P335

Aroclor 1262 ND U 0.1 ‘ “ 8082A1S0P335

Aroclor 1268 ND Ii 0.1 ‘“ 8082A1S0P335

Surrogate: Teirachloro-m-xylene 95 % 88.8-128%

Surrogate: Decachlorobiphenyl 80 % 47.4-136%

Lab ID: 110807049 Wipe - Sampled: 08/25/11 14:38

Sample ID: CHO82S1ISW-9 Polychiorlnated Blphenyls by EPA Method 8082A

Aroclor 1016 ND U 0.1 ug/lOOcm2 B1H0152 08/30/Il 09/02/Il 8082A1S0P335

Aroclor 1221 ND U 0.2 ‘ ‘ ‘ 8082A1S0P335

Aroclor 1232 ND U 0.1 8082A1S0P335

11ClU7ONALO922115S5 Page4of7

Aroclor 1260

Aroclor 1262

Aroclor 1268

Surrogate: Tetrachlora-m-xylene

Surrogate: Decachiorobiphenyl

Lab ID:

Sample ID:

Aroclor 1016

Aroclor 1221

Aroclor 1232

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260

Aroclor 1262

Aroclor 1268

ND U

ND U

ND U

ND U

ND U

ND U

ND U

ND U

ND U

ND U

ND J,Q2,U

ND U

ND U

Wipe - Sampled: 08125/11 14:44

Polychlorinated Biphenyla by EPA Method 8082A0.1 ug/lOOcma B1H0152 08/30/Il 09/02/I I 8082A/S0P335

0.2 ‘ ‘ 8082A/S0P335

0.1 ‘ ‘ “ 8082A1S0P335

0.1 ‘ ‘ 8082A/S0P335

8082A/S0P335

8082A/S0P335

0.1 “ “ 8082A/S0P335

0.1 8082AJS0P335

8082A1S0P335

Wipe - Sampled: 08/25/11 14:5 1

Polychlorinated Biphënyls by EPA Method 8082A0.1 ug/IOOcm’ BlH0152 08/30/Il 09/02/11 8082A/S0P335

0.2 “ 8082A/S0P335

0.1 ‘ ‘ 8082AJS0P335

0.1 “ “ “ 8082A/S0P335

0,1 ‘ ‘ 8082A/S0P335

0.1 ‘ 8082AJS0P335

0.1 ‘ 8082A1S0P335

0.1 ‘ ‘ 8082A/S0P335

0.1 “ “ 8082A/S0P335

Unit.-étates Environmental Protection Ager

Region 9 Laboratory1337 S. 46th Street, Building 201, Richmond, CA 94804

Phone:(510) 412-2300 Fax:(510) 412-2302

Project Manager: Jennifer Downey RCR.A Enforcement Office SDG: 1 1238BProject Number: RI 1R08 75 Hawthorne Street Reported: 09/22/11 15:35

Project: Clean Harbors Los Angeles 2011 TSCA San Francisco CA, 94105Inspection

--

Reanalysis I QualIfiers I Quantitatlol,Analyte Extct Result Comments Limit Units Batch Prepared Analyzed Method

Lab ID: 1108070-09 Wipe-Sampled: 08125/Il 14:38Sample ID: CHO82SIISW4

PolychlorlnatedBlpltenyls by EPA Method 8082AAroclorI242 ND U 0.1 ug/100cm1 B1H0l52 08/30/Il 09/02/Il 8082A/S0P335Aroclor 1248 ND U 0.1 ‘ “ 8082A1S0P335Aroclor 1254 ND U 0.1 8082A/S0P335Aroclor 1260 ND 3, Q2, U 0.1 ‘ ‘ 8082A1S0P335Aroclor 1262 ND U 0.1 ‘ “ “ 8082A1S0P335Aroclor 1268 ND U 0,1 “ 8082AJS0P335

Surrogate: Tetrachloro-m-xylene 92 % 88.8-128%Surrogate: Decachlorobiphenyl 80 % 4 7.4-136%


Aroclor 1254 ND U 0,1

Lab ID:

Sample ID:

Aroclor 1016

Aroclor 1221

1108070-10

CH08251 ISW-IO

Aroclor 1232

Aroclor 1242

ND J,Q2,U

ND U

ND U

91 %

81 %

1108070-11

CH08251 ISW-l I

88.8-128%

47.4-136%

Surrogate: Tetrachloro-m-xylene

Surrogate: Decachiorohiphenyl

90% 88.8-128%

83 % 47.4-136%

1 1(070 fl’IAL 0922 11 55Page 5 of 7

ç€D 0%ited States Environmental Protection AgencyRegion9Laboratory

—J 1337 S. 46th Street, Buflding 201, Richmond, CA 94804Phone:(510) 412-2300 Fax:(510) 412-2302Project Manager: Jennifer Downey

RCRA Enforcement Omce SDG: I 1238BProject Number: RI 1R08

75 Hawthorne Street Reported: 09/22/11 15:35Project: Clean Harbors Los Angeles 201 1 TSCA San Francisco CA, 94105Inspection

-

AnalyteResIt

Batch B1H0152 - Soshlet Extraction - PCBs

Blank (B1HOI5Z-BLKI)Aroclor 1016

Qualifiers / Quantit3on Spike Source %REC RPI) RPDComments Limit Level Result Limits Limit

Prepared: 08/30/11 Analyzed: 09101111Polychlorlnated Biphenyls by EPA Method 8082A - QualIty ControlND U 0.1 ug/lOOc

mAroclor 1221

ND U 0.2Aroclor 1232ND U 0.1Aroclor 1242ND U 0.1Aroclor 1248ND U 0.1Aroclor 1254ND U 0.1Aroclorl26OND J,Q2,U 0.1Aroclor 1262ND U 0.1Aroclor 1268ND U 0.!

Surrogate: Tetrachloro-m.xyiene0.180

“ 0.200 90 88.8-128Surrogate: Decachlorobiphenyl

0.167“ 0.200 84 47.4-136

LCS (BIHOIS2-BSI)Aroclor 1016

0.8920.1 ug/lOOc 1.00 89 88.6-139 200m

Aroclor12600.847

0.1 1.00 85 86.5-139 200Surrogate: Tezrachloro-m-xylene0.175

“ 0.200 88 88.8-128Surrogate: IJecach/orobiphenyl

0.1670.200 84 4 7.4-136

11(8070 FINAL 09 22 111535

Page 6 of 7

0United States Environmental Protection Agen

Region 9 Laboratory

1337 S. 46th Street, Building 201, Richmond, CA 94804 —

Phone:(510) 412-2300 Fax:(510) 412-2302

Project Manager: Jennifer DowneyRCRA Enforcement Office SDG: I 1238B

Project Number: RI 1R0875 Hawthorne Street Reported: 09/22/11 15:35


Inspection

Qualifiers and Comments

Q2 The laboratory control standard associated with this sample did not meet recovery criteria for this analyte (see LCS

results for this batch in QC summary).

3 The reported result for this analyte should be considered an estimated value.

CI The reported concentration for this analyte is below the quantitation limit.

U Not Detected

NR Not Reported

RE 1, RE2, etc: Result is from a sample re-analysis.

4 4

—

p

4

..

;.

p

11 (O 10 rAL )9 22 111535

Page 7 of 7

( ‘pited States Environmental Protection AL )vWashington, D.C. 20460

Toxic Substances Control Act

NOTICE OF INSPECTION

The public reporting burden for this collection of information is estimated to average 5 minutes per response. This estimate includes time

for reviewing Instruct1ns. searching existing data sources, gathering and mairtialning the needed data, and completing and reviewing the

collection of information. Send comments regarding the burden estimate or any other aspect of this collection of information to the Chief,

Information Policy Branch (PM-223), US Environmental Protection Agency, 401 M Street, SW, Washington, DC 20480, and to the Office of

information and Regulatory Affairs, Office of Management and Budget. Washington, 0020503, marked ATrENTION: Desk Officer for EPA

inspec Sign tUr— -

-- Recipient Signepire

——----—--/ C’

Name U J N4ni /.-Q_’_•n(_

-

fill.- / Date lgned lit). Date Signed

-.,v. ---:r ‘‘2S \\ t71 /-A

Form Approved0MB No. 2070-0007Approval Expires 10-31-92

1. investIgation identificatIon 2. TIme 3. Firm Name

372/P;r(,.33 [oauYse.No.

W12 U,-trs Ls

4. Inspector Address . nrm Address

J5k S’zoo’- 75 .57S( ,tb’

4’‘S 5j A 9O)5’

N51-3

REASON FOR INSPECTION

Under the authority of Section 11 of the Toxic Substances Control Act:

‘jj For the purpose of inspecting (Including taking samples, photographs, statements, and other inspection activities) an

establishment, facility, or other premises in which chemical substances or mixtures or articles containing same are manufactured,

processed or stored, or held before or after their distribution in commerce (including records, tiles, papers, processes, controls, and

facilltlâ) and any conveyance being used to transport chemical substances, mixtures, or articles containing same in connection

with their distribution in commerce (including records, files, papers, processes, controls, and facilities) bearing on whether the

requirements of the Act applicable to the chemical substances, mbctures, or articles within or associated with such premises or

‘- conveyance have been complied with.

C] in addition, this inspection extends to (Check appropdate blocks):

L] A. Financial data C] D. Personnel data

C] B. Sales data [] E. Research data

C] C. Pricing data

The nature and extent of inspection of such data specified in A through E above is as follows:

C.rtmc.uonI certify that the statements I have made on this form and all attachments thereto are true accurate, and comDlete, I acknowledge that anyknowinalv false or misleadina statement may k I.hkI. by fin, or imprisonment or boh under annlhjihla law.

EPA 7740-3 Rev (8-91) Regional Office

0 0

WASH INcTON, 2UbU

a’TOXIC SUBSTANCES CONTROL ACT ()

T A INSPECTION CONFIDENTIALITY NOTICE

0MB No 2U70-0007Approval expires 10-31-92

1. INVESTIGATION IDENTIFICATION 2. FIRM NAME

DATE INSPECTOR NO. No.

. ‘‘ - _

.‘. L - f.?[)s

3. INSPECTOR NAME 4.IF)RM.DRESSW, •

%i1 ( $ - r.- ‘l

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TO AiERT A CONFIDENTIAL BUSINESS INFöRMAOM CLAIM

It is possible that EPA will receive public requests for release of the, ., 2, Th in? rrnatlDr, is not, end has not been, reasonably obtainable

information obtained during Inspection of the facility above. Such - withoul your company’s consent by other persons (other than

requests will be handled by EPA In accordance with provjsion* Of the governmental bodies) by use of legitimate means (other than

Freedom of Information Act (FOIA), S USC 552 EPA regulationS dIscovery based on sholng’of special need In a judicial or

issued thereunder 40 CFR Pert 2 and the Toxic Substances Control qasudlcsel proceeding)

Act (TSCA) Section 14 EPA is required to make Inspection data

available in response to FOIA request unless the Administrator of te 3, ‘‘ The informatIon ‘15 no; publicly available elsewhere.

Agency determines that the data contain Information entItled to conil- ,.• . .

dential treatment or may be withheld from release under othet excep- , : Disclosure of the InformatIOn would caUse substantial

tions of FOIA harm to your company’s competitive position

Any or all the information collected by EPA durhStr1aêC,Ie31 m At the completion of the InspectIon, you edil be given a receipt for all

be claimed confidential if it relates to trade secret, orcomrsati. documept, sampIes and other materIals collected At that time you

financial matters that you consider to be confIdential bUsines, nfbfr’2 . may make aIaIfnI that sOme’ or all of the Information I. confidential

mation. If you assert a CBI cOim, EPA will disclose the lnformatlQfl ‘ : ,buliies$ Information. .‘ ‘ ‘

only to the extent, and by means of the procedures set forth Imq -. ‘ ‘ ‘ ‘ .

regulations (cited above) governing EPA a treatmeflt of confI*I If you are not authorized by your cseflpany to essert a CBl claim this

business information. Among other things the regulations rqufreiha1 ,notige will be sent by cerlf led mail, along whit the receipt for docu

EPA notify you In advance of publicly discIoIng any lnfotat1lQW meqts samples, end other matrIaJi to tp Chiet Executive Officer of

you have claimed as confidential busineet intORn$l IOUr flrr WIthin 2 days of this date TI*’Phl** SegutIve Officer must

retu?n a stitemsflt specltylrig ary iqfbñflpWQflr Which should receive

A confidential business information (CSI) claim mdi’ be asserted aIas, -. confidential treafrner,t

time You may assert a CBl claim prior to during or after th’ -

mation is collected. The declaration form was developed by the

to assist you In asserting CBI claim. If it Is more coflvenlan* ferØ., , toi

assert a CBI claim ‘on yourown stationery or by marking the lndlylduI

documents or samples “TSA. confidential businesS lnformat)on,’ It Is

not necessary for you to use this-form. The iflipeajar will b g(

answer any questions you may have ragarØIrt)e Apency’S ,CRprocedures. ‘ ‘

- “ ,

While you may claim any collected Information or sample as coñfiden

tial busineSs information, such claims are unlikely to be upheld if they

are challenged unless the iiformation meets the following criteria:

1. Your company has taken measures to protect the confi

dentiality of the Information, and it intends to contiñu8 ‘

to take such measures.

The etUtemqflt trOth the Chief Executiw Officer should be addressed

,•r- .‘ ‘

.4

• ‘. -

and mailed by registered, returni-ecelpt requested mail within 7 calen

dar days of receIpt of this Notice. Claims may be made any time

after the inspection, but ins action data will not be entered into the

speciql security system for TSCA confidentIal business information

until an officIal confidentiality claim is made. The date will b handled

under the agency’s routine security system unless and until a claim Is

made. - .•,

TO BE COMPLETED BY FACILITY OFFICIAL Nr he’Ii onion ibe p isesä.iUWwho is authorized to maki

. -- -

•r,,’ .bdfleat - identielity claims for the a copy of this Notice and other

- ‘ ‘

‘ ‘ I - , erleis will bq sent to the company’s chief executive osticer. If

I have received and reed the notice pony official whe shOtild also receive this Information

SIGNATURE

‘— 4

NAME ‘1TrLE.

- ‘ ‘ ‘‘ ‘, “

:“.‘ •;

..— ‘‘— — — —

TITLE ‘- DATE SIGNED ‘ ADDRESS - ‘ -.

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EPA Form 77404 (12-82) REGIONAL OFFICE

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flUS ENVIRONMENTAL PROTECTION AGENCY

WASHINGTON, DC 20460

TOXIC SUBSTANCES CONTROL ACT

RECEIPT FOR SAMPLES AND DOCUMENTS

1. INVESTIGATION IDENTIFICATION 2. COMPANY NAME

DATE I INSPECTION NO. I DAILY SEQ. NO. C \e r- o oc o3 Pr is &LCI25/\\ IF1SV I

3 INSPECTOR ADDRESS uSE, 9 4. COMPANY ADDRESS

‘75 -- 54r€c-k 75(, Poe S4nath

Scir Fr4fc.sco) L Q) CA

For internal EPA use. Copres of this form may be provided to receipient as acknowledgement of the documents and samples of chemical substances and/or

mixtures described below collected in connection with the administration and enforcement of the Toxic Substances Contrdl Act.

RECEIPT OF DOCUMENT(S) AND/OR SAMPLE(S) DESCRIBED IS HEREBY ACKNOWLEDGED:

NO.DESCRIPTION

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DUPICATE OR SPLIT SAMPLES: REQUESTED AND PROVIDED E1 NOT REQUESTED El g€€6* riar Y&

INSPECTOR SIGNATURE CLAIMANT SIGNATURE

NAMENAME

J?YWr 1:k)cdk) (- I&’1L CoC_4PrNTITLE DATE SIGNED TITLE DATE SIGNED

Ev. Sc. r4 5 3)2 / v,ZA f1A4L- 1/

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FPA FORM 7740-1 (REVISED JULY 1996) rr’.v,juo v iJr.o OBSOLTh *Js GPO: 1998-444-861/90159 ir.,ijrCOPY

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Clean Harbors5657 Alba StreetLos Angeles, CA 90058

323.277.2500800282.0058www.cleanharbors.com

October 4, 2011

VIA EMAIL (Delivery notification requested)

Mr. Christopher RollinsU.S. EPA, Region IXWST-375 Hawthorne StreetSan Francisco, CA 94105

RE: Clean Harbors Los Angeles, LLC — TSCA Inspection August 25, 2011

Dear Mr. Rollins:

This letter is to update you in regards to the facility inspection conducted at Clean Harbors Los

Angeles, LLC on August 25, 2011. Based upon your observations and inspection fmdings, we

conducted some additional due diligence on the matters you raised during the post-inspection

briefing and would like to share our findings with you, for the record:

1. During the facility inspection, it was observed that Drumil 24612696 had the speculative

statement “Assume >500” written on the drum lid, by the generator. We have contacted

the generator in order to determine the PCB source of contamination as it is our usual

practice to learn as much about the waste characterization and source before we manage

PCB waste at our TSCA- permitted facilities. While we are awaiting confirmation from

the TSCA waste generator, Clean Harbors Los Angeles, LLC decided to sample and

analyze the contents of the 55-gallon drum to determine the chemical concentration of

PCB in this container, utilizing USEPA approved laboratory analytical methods. The

sample was sent to Advanced Technology Laboratories, an independent, NELAP and

California-certified laboratory, for PCB analysis. The results of the analysis indicate

there were no delectable PCBs. A copy of the Advanced Technologies Laboratory report

is enclosed for verification purposes.

2. During the facility inspection, the contents of a laboratory waste accumulation drum was

questioned. Although we believe that the laboratory waste accumulation drum was in

compliance with applicable RCRA and TSCA requirements, we have decided to re-train

our TSCA facility laboratory teams on all Clean Harbors Laboratory Waste Standards of

Operation (SOPs), to include waste container labeling requirements and waste

classification under applicable State and Federal Rules and regulations.

“People and Technology Creating a Better Environment”

0arbor®

3. During the facility inspection, you collected 10 wipe samples from floor areas that werediscolored or stained to determine if these areas were impacted by PCB spills. We alsocollected 2 additional split samples from each area you sampled, and sent one set of oursplit sampled to a California approved and certified laboratory for analysis in accord withthe TSCA requirements. The results of analysis indicates all samples tested below theTSCA surface contamination standard (<10 g/100cm2) with the highest sample resultbeing 2.2 .tgIl 00cm2. A copy of our laboratory report is also enclosed.

During the meeting, you requested four items from us. The site map was provided in themeeting and the remaining items are included in the email. These items include, the inventoryfor Bays 1 thru 6 as of 8/25/Il; profile and analytical for drum 24612696 (profile LASCE-0174);and the decontamination procedures, manifests and analytical for the February 2011 tankcontamination.

In summary, we believe that we have faithfully responded to your concerns. We have alsoprovided additional technical and analytical information, specific your inspection observations,which should assist you as you complete your inspection report.

Please do not hesitate to contact me if you have any further questions concerning thiscorrespondence and especially the analytical data enclosed with this correspondence. I can bereached at (323) 277-2521 or via email at cochrand(icleanharbors.com.

Sincerely,

Dave CochranFacility Manager

oClean Harbors TSCA Cleanup for Non-TSCA Tank

2/17/li — tote with 40 gallons oil of 242 ppm oil was mistakenly pumped into tank V-b.Tank V-b normally has oil <50 ppm.

2/22/11 — after reviewing lab analyticals, it was discovered that TSCA oil had beenpumped into tank V-I 0. The tank, piping, pump and hoses used for pumping the totewere all closed off at this time as they were deemed TSCA contaminated. Even thoughanalytical results showed that the oil in v-rn was 5.7 ppm, the 10,000 gallons in the tankwere considered TSCA because of contact with the oil mentioned above. We began touse a pump with other hoses to continue pumping <50 oil into a separate tank. Thatprocessing could continue. No oil had been removed from tank V-10 between 2/17 and2/22/il.

2/23/li — arrangements were being made to properly dispose of the contaminated oil aswell as decon the tank, piping, pump, and hoses. There was no spill of TSCA oil, sodecon procedures were being applied to those things that had touch ed the oil.

2/24/il — The 10,000 gallons were pumped into 2 isotainers to be shipped via rail toClean Harbors PPM in Coffeyville, KS. 5,800 gallons were put into one isotainer and theother 4,200 gallons were put into. Once tank V-iO was emptied, it was time for thedecontamination process of the tank, pump, hoses, and piping. As per federal regulationsin CFR 761.79, 2000 gallons of a cleaning solvent with <50 ppm PCB was used to deconthe tank and other equipment. Because the tank has a capacity of 20,000 gaLlons, 2000gallons of mineral oil with <50 ppm PCB were used for decontamination. The cleaningsolvent was flushed into the tank through the pump, piping and hoses that were used topump the original 242 ppm PCB oil into tank V-I 0. The cleaning solvent was put in thetank from the top to ensure it cleaned the walls of the tank. This process was done threetimes with this solvent to insure the tank was cleaned. After each cleaning/flushing, asample was taken of the solvent to check the PCB content. The results of the firstcleaning was 4.2 ppm. The solvent after the second cleaning was 4.8 ppm. The thirdcleaning took place after the second result was confirmed. The third sample was takenand then analyzed in the evening by the lab.

2/2 5/1 1 — Upon arrival on the next day, the sample results for the last cleaning was readywith a reading of 5.3 ppm. We reviewed that all the piping, hoses and pump had been partof the tank cieanout for all three flushings and that it was ready to be returned to service.The tank, piping, pump and hoses were all deemed as non-porous. The isotainerscontaining the now TSCA oil wcre shipped to the railcar. At the Clean HarborsCoffeyville facility, the oil will be put through a dechloration process to remove all PCBsfrom the oil. After everything was reviewed to make sure the cleaning process had beendone properly, the tank and equipment were returned to normal service.

•0 o

arbor

__

ENVIRONMENTAL SERVICES, INC. TSCA Tank Rinse Log

A. TankID V-10

B. Tank Capacity 20000 gallons

C. Date Rinsed 2/24/2011

D. Type of Rinsate Used mineral oil <50 ppm PCB

E. Rinsate Volume 2025 gallons

(3 rinses x 0.1 x Tank Capacity)

F. Rinse System GPM 45 gal/minute

G. Minimum Rinse Time Req’d 45 minutes

(Rinse Vol Req’dJ Rinse System GPM)

H. Actual Rinse Time

Start Time 7:15AM

Stop Time 8:00AM

Elapsed Time 45 mm.

I. Rinse Performed By JV (initials)

J. Rinsate Analytical Results

[ample ID: V-b-i Sample ID: Sample ID:

Test Result: 4.2 PP Test Result: ppm Test Result: ppm

K. Tank Interior InspectedReleased By TV (initials)

0

or

__

EN VIRONMENTAL SERVICES, INC. TSCA Tank Rinse Log

A. TankID V-b




E. Rinsate Volume 2025 gallons(3 rinses x 0.1 x Tank Capacity)


G. Minimum Rinse Time Req’d 45 minutes(Rinse Vol Req’dJ Rinse System GPM)


Start Time 10:10AM

Stop Time 10:55AM

Elapsed Time 45 mm.

I. Rinse Performed By JV (initials)


Sample ID: V-10-2 Sample ID: Sample ID:

Test Result: 4.8 ppm Test Result: ppm Test Result: ppm

K. Tank Interior InspectedReleased By JV (initials)

flarbor

__

ENV:ROHMENTAI. SffiVtCES INC. TSCA. Tank Rinse Log

A. Tank ID V-b




E. Rinsate Volume 2025 galLons

(3 rinses x 0.1 x Tank Capacity)


G. Minimum Rinse Time Req’d 45 minutes

(Rinse Vol Req ‘ dJ Rinse System GPM)


Start Time 1:20PM

Stop Time 2:05PM

Elapsed Time 45 mm.

I. Rinse Performed By JV


Sample ID: V-10-3 Sample ID: Sample ID:

Test Result: ppm Test Result: ppm Test Result: ppm

K. Tank Interior InspectedReleased By TV (initials)

0

CLEAN HARBORS LOS ANGELESg LLC TSCADECONTAMINATION OF TANK V-1O

What Happened

A tote containing 40 gallons of oil that contained 242 ppm PCBwas pumped by personnel into tank V-10 on 2/17/11. This tanknormally contains oil <50 ppm PCB. This occurred due toemployee error.The problem was identified on 2/22/11 when the supervisorbrought it to management’s attention. At this time the facilityceased pumping into tank V-i 0 and closed it down by shuttingdown the valves. The pump, piping and hose used to pump theTSCA oil were shut down as well. From the time of the incident on2/17/11 until the problem was discovered and the tank shut downon 2/22/11, only oil <50 ppm had been added to tank V-W.Nothing was removed from the tank during this same time period.At the time the tank was shut down, there was 8,100 gallons of oilinside. Due to the TSCA contact rule, all 8,100 gallons wereconsidered TSCA regulated.The EPA and California DTSC were notified on 2/22/11 of theincident.

Decontamination

The 8,100 gallons of contaminated oil were pumped through thesame pump and piping and hose into portable railcar containers forproper offsite disposal.It was determined that the tank decontamination must take placeaccording to 40 CFR 761.79 (c)( 1) as the tank is a PCB container.Tank V-i 0 needed to be rinsed three times with a predeterminedsolvent. Mineral oil < 50 ppm PCB was to be used.

9 0

The items that needed decontamination here were the tank, the

pump, and the piping. The hose was deemed to be made of porous

material. We delegated the hose to be PCB and put it with other

PCB equipment.Approximately 2,025 gallons were used to decontaminate the tank.

This satisfies the requirement that the volume of the rinsate solvent

must be at least 10% of the volume of the container. The solvent

was pumped from another tank through the contaminated piping

and the contaminated pump. The solvent was put into the tank V

10 to rinse the walls. After the rinsing, a sample of the rinsate

solvent was obtained to determine the current PCB level of the

solvent. The PCB content of the solvent after the first rinse was 4.2

PPM. The solvent was removed from the tank. The tank was rinsed

likewise a second time. Again, a sample was taken for analysis.

The PPM level showed to be 4.8 ppmPCB for this solvent. This

was done again a third time with the solvent. The result was 5.3

ppm for the third rinsing.The tank, the piping, and the pump were considered decontaminate

at this time.The rinsate solvent was added to the railcar containers to bedisposed of. Additional oil <50 ppm PCB was added to the lastrailcar container to make sure it was full.

Disposal

The material was put in these portable containers for rail. Theywere shipped to a railcar from the Clean Harbors Los Angelesfacility and loaded on the railcar. The railcar was then shipped tothe Clean Harbors PPM facility in Coffeyville, KS for disposal.

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August 29, 2011

Edgar MilitarV ELAP No.: 1838

Clean Harbors Environmental Services, inc. NELAP No.: 021 07CA

5756 Alba St. CSDLAC No.: 10196

Los Angeles, CA 90058-1946 ORELAP No.: CA300003

TEL: (323) 277-2501

FAX: (323) 277-2523 WorkorderNo.: 119573

RE:

Attention: Edgar MilitarV

Enclosed are the results for sample(s) received on August 26, 2011 by Advanced TechnologyLaboratories . The sample(s) are tested for the parameters as indicated in the enclosed chain ofcustody in accordance with the applicable laboratory certifications.

Thank you for the opportunity to service the needs of your company.

Please feel fiee to call me at (562W89-4045 if I can he of further assistance lO your company.

Sincerely,

Eddie F. ,ddguez

Laborat’ory Director

The cover lefler and the case narradve are an integra’ part of this analytical report and cannot be reproduced in part orin its entirety without written permission from the client and Advanced Technology Laboratories.

V Advwtcrd Technology 1 o 5- ——--—

3275 Walnut A’enue Sgno1 Hill, CA 90755 Tel: 562 989-4045 Fax: 562 989-4040

0Advanced TechnoIov Laboratories — Date: 29-Aug-il

CLIENT: Clean Harbors Environmental Services, Inc.

Project: CASE NARRATIVELab Order: 119573

Analytical Comments for EPA 8082

Sample 1] 9573-OO1A, surrogate recovery biased low possibly due to matrix interferences.

Id Page 1 of 4

:2.c lfr(rlUUl JJj? t::’i W1755 Tel: 562. 989.1945 1u.x: 562.989.404t’j

2of5

o 0ANALYTICAL RESULTS

Advanced Technology Laboratories Print Date: 29-Aug-Il

CLIENT: Clean Harbors Environmental Services, Inc. Client Sample ID: 24612696

Lab Order: 119573Collection Date: 8/26/2011 10:45:00 AM

Project:Matrii: SOLID

LabID: I19573-OQIA

Analyses Result PQL Qual Units OF Date Analyzed

PCBS BY GC/ECDEPA 355DB EPA 8082

RuniD: GC4_l 10827A DC Batch: 75167 PrepDate: 8/27/2011 Analyst: HL

Aroclor 1016 ND 50 pg/Kg 1 8/27/2011 07:45 PM



Aroclorl242 ND 50 pg/Kg 1 8/2712011 07:45 PM


Arodor 1254 ND 50 pg/Kg 1 8/27/201/ 07:45 PM

Aroc/or 1260 ND 50 pg/Kg 1 8/2712011 07:45 PM

Aroclsr 1262 ND 50 pg/Kg 1 8/27/2011 0745 PM


Surr: Decachlorobiphenyl 13.6 39-122 5 %REC 1 8/27/2011 07:45 PM

Suer: Telrachloro-m-xylene 67.6 - 45-111 %REC 1 8/27/2011 0745 PM

Qualifiers: Analyte detected in the associated Method Blank B Value above quantilotion range

It Ho/ding times for preporatiun or analysis exceeded Nt) Not Detected at the Reporting Limit

S Spike/Surrogate outside of I/torts duo to matrix interference Results are wet unless otherwise spent//mi

DO Surrogate Diluted Out

.td,tnceri irrchnoTh”,

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Analysis

Date:

8/27/2011S

eqNo:

2230422

Arialyte

Result

PQL

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SP

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16.47616.67

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ode:8082_S

Units:

pg/Kg

Prep

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8/27/2011R

uriNo:

135130

Client

ID:

ZZ

ZZ

ZZ

Batch

ID:

75167T

estNo:

EP

A8082

EPA

358/lBA

nalysisD

ate:8127I2011

SeqNo:

2230423

Anatyte

Result

PaL

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PD

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Aroclor

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159.60.0100

20

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16166.7

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172.60.238

20

Sure:D

ecachlorabiphenyt15.995

16.6795.9

39122

020

Sure:T

etrachlaro-m-uylene

16,74416.67

10049

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0

QualifrereB

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detectedin

theassociated

Method

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562.959.4040

f5

fleanHarij’MSTE MATERIAL PROFILE SHEO--‘-w-- lean Harbors_Profile No. lasce-O 174

_______________

A. GENERAL INFORMATIONGENERATOR EPA ID #IREGISTRATION S CA0006908BIB GENERATOR NAME: Southern California Edison

GENERATOR CODE (Assigned by Clean Harbors) 1NV0267,4 CITY Monrovia STATE/PROVINCE CA ZIP/POSTAL CODE 91016ADDRESS 1218 South Fifth Ave Waste and Water Division 2n

PHONE: (626) 3024187CUSTOMER CODE (Acognad by Clean Harbors) SOUIGO9 CUSTOMER NAME: Southern California Edison CompanyADDRESS PG Box 800 CITY Rosemead STATE/PROVINCE CA ZIP/POSTAL COOS 91770

B. WASTE DESCRIPTIONWASTE DESCRIPTION: Debits/Soil, Unknown PCB level. Assumed >SOOppmPROCESS GENERATING WASTE: Spill Cleanup

IS THIS WASTE CONTAINED IN SMALL PACKAGING CONTAINED WITHIN A LARGER SHIPPING CONTAINER? No

C. PHYSICAL PROPERTIES Id 25C or TiE)

PHYSICAL STATE NUMBER OF PHASES/LAYERS VISCOSITY (It liquId preserrl) COLORSOLID WITHOUT FREE LIQUID 1 2 3 TOP 0.00 1 . 100 (e.g. Waler)POWDER

MIDDLE 0,00 101- 500 (e.g. Molar 0/)MONOLITHIC SOLID % BY VOLUME (Appfox.(UQUID WITH NO SOLIDS BOTTOM 0.00 501 - 10.000 (eg. Molasses)LIQUID/SOLID MIXTURE

0 10,000% FREE LIQUID ODOR% SETTLED SOLID

e NONE BOILING POINT ‘F (‘C) MELTING POINT’F (‘C) I TOTAL ORGANIC% TOTAL SUSPENDED SOLID— CARBON0095 (e35(SLUDGE MILD

n 140 (=60) I = 1%95- 100 (35-38)GAS/AEROSOL STRONG140.200(00-93) I 1-9%101-129)38-54)

._.DescrIbe:.‘ = 200 (93) I 0 10%.

0= 130 )v54)I

FLASH POINT ‘F (‘C) pH SPECIFIC GRAVITY ASH BTUILB )MJ/kg)n 731=23) n 2 0 0.8 (e.g. Gasoline) 02,000(01.6)

‘i 001 =2073- 190 (23-38) 2.1- 6.9 0.81.O (e.g. Ethanol) s’ 2.000-5,000 (4.6-11.6)0.1- 1.0 Ueknown —

101 -140 (38-60) 7 (Non/ret) 1.0 (e.g. Waler) 5,000-10,000111 6-232)II. 5.0141 -200 (50-93) 7.1— 12.4 1.0-12 (e.g. Antifreeze) = 10.000)’23.2I5.1 -20.00 200 (=83) 0= 12.5 “, n 1.2 (e.g. Methylena Chlonde) Actual:

I). COMPOSITION (List the complete compositIon Dl the waste. Include any Inert uomponenTe and/ar debris. Ranges (or Individual components are actreptable. If a trade nasa isused, please supply an MOOS Please do not use abbreviations.)

CHEMICAL MIN MAX UOMASPHALT 0.0000000 — 100.0000000 %CABLE, MASONRY - - - 0.0000000 — 100.0000000 %CARDBOARD

. 0.0000000 — 100.0000000 %CERAMIC 0.0000000 — 100.0000000 %CITRUS BASED SOLVENTS - - 0.0000000 — 20.0000000 %DEBRIS 0.0000000 — 100.0000000 %DIESEL 0.0000000 — 5.0000000 %DRANIED EQUIPMENT LAST CONT. PCB 0.0000000 — 100.0000000 %GLASS 0.0000000 — 100.0000000 %METAL PARTS, PIPES 0.0000000 — 100.0000000 %

DOES THIS WASTE CONTAIN ANY HEAVY GAUGE METAL DEBRIS DR OTHER LARGE OBJECTS (EX - METAL PLATE OR PIPING =1/4’ THICK OR ‘12 YES NOLONG. METAL REINFORCED HOSE =12 LONG. METAL WIRE 012 LONG, METAL VALVES, PIPE FITTINGS. CONCRETE REINFORCING BAR ORPIECES OF CONCRETE u3V

It yes, describe, includIng drmenoionm

DOES THIS WASTE CONTAIN ANY METALS IN POWDERED OR OTHER FiNELY DIViDED FORM’ YES ,s’ NODOES THIS WASTE CONTAIN OR HAS IT CONTACTED ANY OF THE FOLLOWING: ANIMAL WASTES. HUMAN BLOOD. BLOOD PRODUCTS. BODY YES s’ NOFLUIDS, MICROBIOLOGICAL WASTE. PATHOLOGICAL WASTE, HUMAN OR ANIMAL DERIVED SERUMS OR PROTEINS OR ANY OTHERPOTENTIALLY INFECTIOUS MATERIAL?

I acknowledge that this waste material in nerther infectious sea does II contain any eaganlem known To Sea threat Ira human haellTr This crelilicehon isbased ott try knowledge a/the reeler/al. Soled I/re answer below Oral apples

The waste wan never enpnued To potenleliy electrons material.YES NO

Chemical disintedion or some other form eT olenhizahon has been applied To lire waste. YES NOI ACKNOWLEDGE THAT THIS PROFILE MEETS THE CLEAN HARBORS BATTERY PACKAGING REQUIREMENTS. YES NOI ACKNOWLEDGE THAT MY FRIABLE ASSESTOS WASTE IS DOUBLE BAGGED AND WETTED YES NOSPECIFY THE SOURCE CODE ASSOCIATED WITH THE WASTE. G15 SPECIFY THE FORM CODE ASSOCIATED WITH THE WASTE. W002

Repeal Prlntvd On-Thursday. August29 2011 lWINWEBlProt9ehWaste PraEte.rdl Page 1 014

NOCs

C!!a!r.$kL niors Profile No. lasce-0174 1DE. CONSTITUENTS

Are these vaNes bened on testing or knowledge? : Knsndedge Testing

It based on kttoteledge. please desmUe In detat. the rationale applied tn identity and charaderlze the waste matetial. Pleesa Include referenca Is Matenal Safety Data Sheets (MSOS)

when applicable. inclade the chemical or trade-came represented by the MSOS, and or deleted paocess Ce operatIng pemcedrjres which generate the waste.

[pee eentaeleetsd heart. 1.1>500 ppm peelH

Please indicate which constituents below apply. Concentrations must be entered when applicable to assist In accurate review and expedited approvat

of your waste profile. Please note thet the total regulated metals and other constituents sections require answers.

RCRA REGULATED METALS REGULATORY TCLP TOTAl. UDM NOT APPLICABLE

LEVEL (mall) mglt

0504 ARSENIC 0.5

Dcc EARILIM - -100.0

0050 CADMIUM 1.0

0007 CHROMIUM 5.0

DSO - LE 5.0ret

DOSS MERCURY 0.2 -

OStO SELENIUM 1.0

0511 SILVER 5.21

VOLATILE COMPOUNDS OTHER CONSTITUENTS MAX UOM NOT

0510 eENZENE 0.5APPLICABLE

0010 CARSON TETRACHLORIOE 0.5 BROMINE

D02t CNLOR005NZENE 100.0 CHLORINE .0

DS22 CHLOROFORM e.S FLUORINE‘5,

D020 1,2-DICHLOROETHANE 0.5 IODINE‘.0

D029 11-DICHLORDETHYLENE 0.7 SULFUR5,’ -

0035 MSTNYL ETNYL I4STDNE 200 S POTASStUMit - - - -

0030 TETRACHLOROEThYLENE 07 SODIUMit

0040 TRICHLDRDETHYLENE 0.5 AMMONIAit.

D043 VINYL CHLORIDE 0.2 CYAtdIOE AMENABLE ‘v’ - -

SEMI-VOLATILE CDMPOUNDSCYANIDE REACTIVE - -

—

5,

D523 o-CRESOL 200.0 CYANIDE TDTAL

D024 m-CRESOL 200.0 SULFIDE REACTIVE 5,,

0025 p-CRESDL 200.0 Pce.

DO2E CRESOL (TOTAL) 2000

0027 I4DICHLOR000NZENE 7.5‘ NONE NONE

0030 2,4.DGdITROTOLUEPIE 0i3CI000PPM n5OPPM

0032 HCHLOROFE 013OP ‘ v=SOPPM

D033 NEXACNLDRDBUTADIENE 05 WASTE REGULATO BY TSCA 40

0034 HEXACNLOROEFNANE 3.0CFR 701?

DO3E NITRDEENZENE — 3M . YES NO

0037 PENTACNLOROPHENOL 100.0

D038 PYRIDINE 5.0 -

D041 24,5-TRICHLOROPNENOL 400.0

D0d2 2,4,S-TRICHLOROPHENDL 2.0

PESTICIDES AND HERBICIDES

0012 ENDRIN 0.02

0013 UNDANS 04 -

D014 METHOXYCHLOR 10.0

0010 TOXAPHENE 0.5

0015 2.4-0 10.0

D017 2.4,5-TP)SILVSX) 1,0

0020 CHLORDAO4E 0.03

D031 NSPTACHLOR (AND ITS EPOXIDS) 0.000

ADDtTIONAL HAZARDSDOES THIS WASTE NAVE ANY UNDISCLOSED HAZARDS OR PRIOR INCIDENTS ASSOCIATED wtm IT. WHICH COULD AFFECT THE WAY IT SHOULD ES HANDLED?

YES :f NO (Ityes, captain)

CHOOSE ALL THAT APPLY

OSA REGULATEO SUBSTANCE EXPLOSIVE FUMING “ OSHA RSGULATEO CARCINOGENS

POLYMERtZABLE RAOIOACTIVE REACTIVE MATERIAL NONE OF THE ABOVE

Report Printed On: Thursday, Aegasl 20.2011Pege 2 of 4IWINWESIPreOIs\Weste PrsFde,nS

ricanHarbor Clean Harbors Profile No. lasce-0174

NO IS THIS WASTE PROHIBITED FROM LAND DISPOSAL WITHOUT FURTHER TREATMENT PER 40 CFR PART 268?

LOR CATEGORY: Not subject to LOftVARIANCE INFO:

YES ‘‘ NO ISTHISAUNIVERSALWASIE?

YES NO IS THE GENERATOR OF THE WASTE CLASSIFiED AS CONDITIONALLY EXEMPT SMALL QUANTiTY GENERATOR (CESQG)?

YES NO IS This MATERIAL GOING TO BE MANAGED AS A RCRA EXEMPT COMMERCIAL PRODUCT. WHICH IS FUEL (40 CFR 261.2 (CX2XII))?

YES ‘ NO DOES TREATMENT OF THIS WASTE GENERATE A FOOd OR PSi B SLUDGE?

YES NO IS THIS WASTE STREAM SUBJECT TO THE INORGANIC METAL BEARING WASTE PROHIBITION FOUND AT 40 CFR 268.3(C)?

YES ‘e NO DOES TI-RS WASTE CONTAIN VOC’S IN CONCENTRATIONS acr5Q PPM?

YES NO DOES THE WASTE CONTAIN GREATER THAN 20% OF ORGANIC CONSTITUENTS WITH A VAPOR PRESSURE cm .3KPA (.044 PSIA)?

YES T NO DOES THIS WASTE CONTAIN AN ORGANIC CONSTITUENT WHICH IN ITS PURE FORM HAS A VAPOR PRESSUREc 77 KPA (11 .2 PSIA)?

YES NO IS THIS CERCLA REGULATED (SUPERFUND ) WASTE?

YES ‘ NO IS THE WASTE SUBJECT TO ONE OF THE FOLLOWING NESHAP RULES?

Hazardous Orgasire NESHAP (HON) oslo (subpart 0) Pharmacosticels production (subpart GOD)

YES NO IF THIS IS A US EPA HAZARDOUS WASTE. DOES THIS WASTE STREAM CONTAIN BENZENE?

YES NO Doss the waste stream corns horn a facility wily one of the SIC codes listed Under benzene NESHAP or Is this waste regulated under the berlzeneNESHAP sates because the orIgInal source of tho waste shorn a eberolcal monnafactesring, wke by-product rsra,neay. or petroleum rethnecy prreccos7

YES NO Is the gereefstln source of the waste stream a taNdy arty Total Annual Beozene (TAB) trio Mg!year?

What 5 the TAB quantity too your tacdlty? I I Megagram(year (1 Mg = 2,200 Ibo)

The basis for this determination is: Knowledge of the Waste Or Test Data KnowledBe Testing

Describe tine knowledge: - “10. DOTITDG iNFORMATION

DOTITOG PROPER SHIPPING NAME:

UN3432, POLYCHLORINATED BIPHENYLS, SOLID, 9, PG (II

H. TRANSPORTATION REQUIREMENTSESTIMATED SHIPMENT FREQUENCY ONETIME WEEKLY MONTHLY QUARTERLY YEARLY OTHER

CONTAINERIZED BULK LIQUID BULK SOUD1.15 CONTAINERSISHIPMENT

STORAGE CAPACITYGALLONSISHIPMENT: 0Mb, -O Max GAL. SHIPMENT UOM: TON YARD

CONTAINER TYPE: TONSfYARDS/SHIPMENT: 0 Mm - 0 MaxCUBiC YARD BOX s.’ PALLET

TOTE TANK DRUMOTHER.

DRUM SIZE -

I. SPECIAL REQUESTc000MENTS OR 000UESTS

GENERATOR’S CERSFICAI105I reilly that I am anthorlast tin eercule thu doocnent as an outllotlrod agent. thereby mIsty Octal Intoinnation eubeniord In this art attached doosments Is canectto the best at my knowledge. I atlascodIfy that any samples subtnttled are ropresenlatlvs Ut the actual waste. It Clean Harbors dIscovers e doorspenoy dunn0 Ike appmcel pmcne, Generator grants Clean Harbors the authority to amendthe pmfle, as Clear darters deems necessary. ID teneca lye discrepancy.

AUTHORIZED SIGNATURE

[email protected]

____________________

ThIS waste pmgle has beer submlond using Clear Harbors ele000ntu elonetare system.

40 cyn Sec 204.12 required notice:Au reqvhnd by Fedeeh Resource Coese’aatre.r erd neawaray tart regrilatione laced br4tl CFR Pact 204.12101 met ad rqctvslret State hazardous weste tnasdeawns. sakes Is hereby presIded that dl ClaacHflrtOve tanirltes Oar cray to Used IC treat slam. .rd toe dIspose at fire hazesdous resale duscrtbnd en this walE petite have the ep000peiale prenrits and the capacity to macsee Ores. waste..

Places note this par.rua must be eubnrdled for ro evehauao It these Ire, borer a strange In era aaua goolcealleg pruersa or wires Store hens bOon slreigeo th lire dnwnactr nornposeren 0 phytcd drarautorotco Ofthe Inatecat.

NAME (PRINT) TITLE DATE

F. REGULATORY STATUS

YES ‘p’, NO USEPA HAZARDOUS WASTE?

YES NO DO ANY STATE WASTE CODES APPLY?

1261TUbas Waste Code [0u1s0021

YES ‘ NO DO ANY CANADIAN PROVINCIAL WASTE CODES APPLY?

YES

-i

Report Pnrnted On : Thursday, August25 2011 NIIINWEB)ProIEe\Weate Prattle nil Page 3 of 4

jgnIiar&Sj EiDarbors Profile No. lasce-0174 C)Addendum

0. COMPOSITION

CHEMICAL

MEl — MAX UOM

PAPER

0.00000 — 100.000 %

00 0000

PCBS

0.05000 — 100.000 %

00 0000

PIPE

0.00000 — 100.000 %

00 0000

PLASTIC.

0.00000 — 100.000 V.

00 0000

SOIL0.00000 — 100.000 %00 0000

W0000.00000 — 100.000 %00 0000

Report Printed On Thursday, August 25.2011 AuIIdwEOIPmme\wasra PsoIIIesdI Page 4 of 4

0 0.

Advanced Technoloay Laboratories Date: 29-Aug-il

CLIENT: Clean Harbors Environmental Services, Inc.

Project: CASE NARRATIVELab Order: 119573

Analytical Comments for EPA 8082

Sample II 9573-OOIA, surrogate recovery biased low possibly due to matrix interferences.

Page 1 of 4tdt’a,wcd icvi’imfogi

3275 H’,,’nur 4 n-flue. Signal 1111!. CA 90755 ‘Tel: 562. 989.4045 Fax: .S62.989 4040

2 of 5

ANALYTICAL RESULTSPrint Date: 29-Aug-li

PrepDate: 8/27/2011 Analyst: HL

1 8/27/2011 07:45 PM

1 8/27/2011 07:45 PM

1 8/2712011 07:45 PM

1 8/27/2011 07:45 PM

1 8/27/2011 07:45 PM

1 8/27/2011 07:46 PM

1 8/27/2011 07:45 PM

1 8127/2011 07:45 PM

1 8/2712011 07:45 PM

1 8/2712011 07:45 PM

1 8/27/2011 07:45 PM

5275 Walnut ‘henna, Signal Hill. C4 9//755 Tel: 562. 989.4045 Fax: 562.9ç9.41140

0

Advanced Technology Laboratories

0

CLIENT: Clean Harbors Environmental Services, Inc. Client Samp)e ID: 24612696

Lab Order: 119573Collection Date: 8/26/2011 10:45:00 AM

Project:,

Matrix: SOLID

Lab ID: 1I9573-OOIA

Analyses Result PQL Qual Units DF Date Analyzed

PCBS BY GC1ECI2

RufliD: GC4110827A

EPA 35506 EPA 8082

QC Batch: 75167

Aroctor 1016 ND 50 hg/Kg

Aroctor 1221 ND 99 pg/Kg

Aroclor 1232 ND 50 pg/Kg

Aroclor 1242 ND 50 pglKg


Aroctor 1254 ND 50 pg/Kg


Nec/or 1262 ND 50 pg/Kg


Surr: Decachlorobiphenyl 13.6 39-122 S %REC

Surr Tetrachloro-m-xytene 67.6 45-111 %REC

Qualifiers: B Analyte detected in the associated Method Blank

It Holding times for preparation or analysis exceeded

S Spike/Surrogate outside of limits due to matrix interference

DO Surrogate Diluted Out

.tdvinwcdrerhnolagj

E Va/se above quantitation range

NI) Not Detected at the Reporting Limit

Results are wet unless otherwise specified

3 of 5

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