06 0620 51 3RP - Egypt IG Student Room · white ppt. bromide (r –) in solution ... sulfur dioxide produced will turn DFLGL¿HGDTXHRXVSRWDVVLXP manganate(VII) from purple to colourless
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READ THESE INSTRUCTIONS FIRST
Write your Centre number, candidate number and name on all the work you hand in.Write in dark blue or black pen.You may use an HB pencil for any diagrams or graphs.Do not use staples, paper clips, glue or correction fluid.DO NOT WRITE IN ANY BARCODES.
Answer all questions.Electronic calculators may be used.You may lose marks if you do not show your working or if you do not use appropriate units.Notes for use in qualitative analysis are provided on pages 7 and 8.
At the end of the examination, fasten all your work securely together.The number of marks is given in brackets [ ] at the end of each question or part question.
CHEMISTRY 0620/51
Paper 5 Practical Test May/June 2017
1 hour 15 minutes
Candidates answer on the Question Paper.
Additional Materials: As listed in the Confidential Instructions
Cambridge International ExaminationsCambridge International General Certificate of Secondary Education
1 You are going to investigate the reaction between aqueous sodium thiosulfate and two different aqueous solutions of potassium iodate labelled solution C and solution D.
Read all the instructions carefully before starting the experiments.
Instructions You are going to carry out two experiments.
(a) Experiment 1
● Filltheburetteprovideduptothe0.0cm3 mark with the aqueous sodium thiosulfate. ● Useameasuringcylindertopour20cm3 of solution C into a conical flask. ● Add10cm3ofdilutesulfuricacidintotheflaskand1gofpotassiumiodide.Swirltheflask
to mix the contents. ● Addtheaqueoussodiumthiosulfateslowlyfromtheburettetotheflask,andswirltomix
thoroughly. ● Whenthecontentsoftheflaskarepaleyellow,add1cm3 of starch solution to the flask. ● Continuetoaddaqueoussodiumthiosulfateslowlytotheflaskuntilthesolutionjustturns
colourless. ● Recordtheburettereadingsinthetable.
(b) Experiment 2
● Emptytheconicalflaskandrinseitwithdistilledwater. ● RepeatExperiment1,usingsolutionD instead of solution C. ● Recordtheburettereadingsinthetableandcompletethetable.
Experiment1 Experiment2
finalburettereading/cm3
initialburettereading/cm3
difference/cm3
[4]
(c) Describe the appearance of the solution in the conical flask before adding the aqueous sodium thiosulfate.
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Tests for gases Flame tests for metal ions
gas test and test results metal ion flame colour
ammonia (NH3) turns damp, red litmus paper blue lithium (Li+) red