Www.rgf.bg.ac.rs/restca Major deliverable: SEM-EDS laboratory.
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Equipment of the SEM-EDS lab at the UB-Equipment of the SEM-EDS lab at the UB-FMG:FMG:
JEOL JSM-6610LVJEOL JSM-6610LV Magnification:Magnification:
X 5-300.000X 5-300.000
Guns:Guns:
W filament, LaBW filament, LaB66; Accelerating voltage 0.3-30 kV; Accelerating voltage 0.3-30 kV
Vacuum system:Vacuum system:
Rotary pump + turbomolecular pump (included in basic instrument), Rotary pump + turbomolecular pump (included in basic instrument), Sputter Ion pump (for LaBSputter Ion pump (for LaB66))
RRotary pump for LV otary pump for LV ((10-270 Pa10-270 Pa))
Detectors:Detectors:
SE detector (Everhart-Thornley detector)SE detector (Everhart-Thornley detector)
BSE detectorBSE detector
EDS detector (X-MaxEDS detector (X-Max Large Area Analytical Silicon Drift Large Area Analytical Silicon Drift connected with connected with INCAEnergy 350 Microanalysis SystemINCAEnergy 350 Microanalysis System)); ; Z ≥ 6; d.l. 0.1 – 0.2 wt.%
CL detector CL detector Sample Sample chamberchamber::
Specimen movement: 5-axes (X, Y, Z, T, R)Specimen movement: 5-axes (X, Y, Z, T, R)
Maximal sample size: 20 cm (wide), 8 cm (thicknes), 1 kg (weight)Maximal sample size: 20 cm (wide), 8 cm (thicknes), 1 kg (weight)
Two IR camerasTwo IR cameras
Micro-analytical standardsMicro-analytical standards: :
64 natural minerals and synthetic compounds64 natural minerals and synthetic compounds
Sputter coating deviceSputter coating device (LEICA SCD005) for Au and C. (LEICA SCD005) for Au and C.
Other facilitiesOther facilities (ultrasonic cleaner, stereomicroscope, etc.) (ultrasonic cleaner, stereomicroscope, etc.)
www.rgf.bg.ac.rs/restca
www.rgf.bg.ac.rs/restca
Events and activities in the lab:Events and activities in the lab:
June 23-27, 2009 June 23-27, 2009 Installation of JEOL Installation of JEOL JSM-6610LVJSM-6610LV S SEMEM
August 17-20, 2009 August 17-20, 2009 Installation of Installation of EDS systemEDS system and and cathodolumincathodolumineescence detectorscence detector
September 18September 18thth, 2009, 2009
TThe opening ceremony and promotion of the SEM-EDS laboratoryhe opening ceremony and promotion of the SEM-EDS laboratory
MarchMarch,, 201 20111
Presentation of the first applications and resultsPresentation of the first applications and results
18 18 months months workingworking
Installation Installation and testand test
Aims:Aims:
1.1. SEM-EDS analyses of solid pollutant materialsSEM-EDS analyses of solid pollutant materials
2.2. SEM-EDS application in various sciences SEM-EDS application in various sciences
www.rgf.bg.ac.rs/restca
1.1. SEM-EDS analyses of solid pollutant materialsSEM-EDS analyses of solid pollutant materials
- Mining waste materialMining waste material
- Slags- Slags
- Dust and air particlesDust and air particles
- Fly ashFly ash
- Monuments protectionMonuments protection
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SEM-EDS application:SEM-EDS application: Environmental ProtectionEnvironmental Protection
Limonite Al, Si, K: <7 wt.%
0.4 – 0.6 wt.% S
0.3 – 0.4 wt.% As
Py
Rt
Qtz
Dsp
Prl Mining waste material of the Lipa deposit
Polished section of the mining waste material from the Lipa deposit
www.rgf.bg.ac.rs/restca
SEM-EDS application:SEM-EDS application: Environmental ProtectionEnvironmental Protection
Modified mining waste material – gypsumModified mining waste material – gypsum
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SEM-EDS application:SEM-EDS application: Environmental ProtectionEnvironmental Protection
SlagsSlags containing remained compounds of lead and other toxic containing remained compounds of lead and other toxic elements (polished sections)elements (polished sections)
www.rgf.bg.ac.rs/restca
SEM-EDS application:SEM-EDS application: Environmental ProtectionEnvironmental Protection
The particles from the air collected by the filters
www.rgf.bg.ac.rs/restca
SEM-EDS application:SEM-EDS application: Environmental ProtectionEnvironmental Protection
Crystals of gypsum and the carbon particle in the black Crystals of gypsum and the carbon particle in the black crusts of the historic monumentcrusts of the historic monument
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2. SEM-EDS application in various sciences
Scientific disciplinesScientific disciplines::
GeologyGeology
Material science and TechnologyMaterial science and Technology
MetallurgyMetallurgy
MMeechchanicalanical Engineering Engineering
BiologyBiology
MedicineMedicine
Food ScienceFood Science
ArchArchaaeologyeology
..
..
UsersUsers::
University of BelgradeUniversity of Belgrade::Faculty of Mining and GeologyFaculty of Mining and Geology, Faculty of , Faculty of Technology and Metallurgy, Faculty of Physical Technology and Metallurgy, Faculty of Physical Chemistry, Faculty of Chemistry, Faculty of Chemistry, Faculty of Chemistry, Faculty of Physics, Faculty of Mechanical Engineering, Physics, Faculty of Mechanical Engineering, Faculty of Dental Medicine, Faculty of Agriculture, Faculty of Dental Medicine, Faculty of Agriculture, Faculty of Forestry. Faculty of Forestry.
Scientific InstitutesScientific Institutes::IHTMIHTM, ITNMS, , ITNMS, VinčaVinča, , GošaGoša, , GISGIS, IMSI, IMGGI, IMSI, IMGGI
MuseumsMuseumsNational Museum, Natural History Museum Natural History Museum
Users from other places Users from other places Kosovska Mitrovica, Novi Sad, Kragujevac, Bor, Kosovska Mitrovica, Novi Sad, Kragujevac, Bor, Podgorica, Split, Hannover, LondonPodgorica, Split, Hannover, London
www.rgf.bg.ac.rs/restca
SEM-EDS application:SEM-EDS application: Material Science and TechnologyMaterial Science and Technology
Synthetic compounds
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SEM-EDS application:SEM-EDS application: Material Science and TechnologyMaterial Science and Technology
X 100 000 X 100 000nm~10nm
Nano-materials
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SEM-EDS application:SEM-EDS application: Material Science and TechnologyMaterial Science and Technology
100% Cotton
(Textile Engineering)
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SEM-EDS application:SEM-EDS application: Material Science and TechnologyMaterial Science and Technology
(Textile Engineering)
Oxidized and Ag-modified Cannabis
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(Geotextile)(Geotextile)
SEM-EDS application:SEM-EDS application: Material Science and TechnologyMaterial Science and Technology
www.rgf.bg.ac.rs/restca
SEM-EDS application:SEM-EDS application: MetallurgyMetallurgy
Alloys (polished sections)Alloys (polished sections)
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SEM-EDS application:SEM-EDS application: MetallurgyMetallurgy
Alloys (polished sections)Alloys (polished sections)
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SEM-EDS application:SEM-EDS application:
MetallurgyMetallurgy
Weld (polished section after etching)
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SEM-EDS application:SEM-EDS application: Material Science and TechnologyMaterial Science and Technology
Materials modified by lasers
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SEM-EDS application:SEM-EDS application: Material Science and TechnologyMaterial Science and Technology
Laser cleaning of the archeological objects (ceramics and metals)
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SEM-EDS application:SEM-EDS application: MMeechchanicalanical Engineering Engineering
www.rgf.bg.ac.rs/restca
SEM-EDS application: SEM-EDS application: Biology Biology
BacteriaBacteria Streptomycetes Streptomycetes
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SEM-EDS application:SEM-EDS application:
BiologyBiology
Leaf of the plantLeaf of the plant
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SEM-EDS application:SEM-EDS application:
Biology Biology
Leaf of the plantLeaf of the plant
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SEM-EDS application:SEM-EDS application: Pigments and BiologyPigments and Biology
Fungi’s spores on the painting
Line scan
Ca
C
O
P
Na
Sr
Mg
ClAl
SEM-EDS application:SEM-EDS application:
MedicineMedicine - Dentistry - Dentistry
www.rgf.bg.ac.rs/restca
Polished section of the tooth from the image left
www.rgf.bg.ac.rs/restca
SEM-EDS application:SEM-EDS application: Food ScienceFood Science
Cell walls of the yeast
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